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WQ0029804_Residual Annual Report 2014_20150213
Winston-Salem a Forsyth County City/County . Water - Sewer a Solid Waste Disposal Manson Meads Complex City of Winston-Salem 27 99 Griffith Road Winston-Salem, NC 27103 CityGnk 311(336.727.8000) Fax 336.659.4320 www.cityaji org February 6, 2014 NC Division of Water Resources Aquifer Protection Section Land Application Unit 1636 Mail Service Center Raleigh, NC 27699-1636 Please find attached" the 2014 annual monitoring report for the Winston-Salem/Forsyth County Utilities Commission POTW's Class A Biosolids Distribution program. The Utilities Commission owns two Wastewater Treatment Plants (WWTP's), the Archie Elledge WWTP (NPDES # NC0037834) and the Muddy Creek WWTP (NPDES # NC0050342). ~! Stabilized Digested Sludge products from both WWTPs' Anaerobic Digesters are blended prior to being dewatered, in order to produce a Class A dried pelletized product. This product is marketed under the brand name "Winston-Salem ' Soil Solutions". This facility is operated under North Carolina Division of Water Quality Permit #WQ0029804 and is permitted as the "Thermal Biosolids Dryer Management Facility". Please find attached Certification Form DMSDF; a Contractor Handout, signed by the current contractor; laboratory data for metals, nutrients and TCLP testing; Pathogen and Vector Attraction Reduction certifications (Form PVRF 503); data on Fecal Coliform testing; and operational data for the Dryer facility. All 40 CFR Part 503 regulatory limits' were met for the classification of these biosolids as a Class A, EQ product in 2014. Also, as support documentation for the Dryer Facility's Class A compliance, the Archie Elledge and Muddy Creek WWTPs' Class B compliance certifications and operational data are included. Please note for all three sets of Operational reports (Dryer, Elledge and Muddy Creek): Blank spaces may be generated due to either a particular system being offline or no flow that specific .4,. day, therefore no analytical data. In addition to the bulk Agricultural Distribution of pellets, the, City, has a small-scale Pellet Giveaway Program. ' However, no pellets -were actually distributed in 2014 through the Giveaway Program. See the Certification and Summary Form DMSDF and attached summary of dry tons for specific tonnages distributed to Agriculture. Although the NCDENR Division of Water Quality Non -Discharge Permit #WQ0000094 covers the land application of the City's Class B Biosolids, no Class Bland application occurred in 2014.. Please find attached a cover letter and completed DENR Form ACF for the City's 2014 Class B Land Application Program. Various Class B Biosolids products were analyzed for TCLP parameters, but since there was no land application of Class B Biosolids for 2014, the TCLP information is not included here. It is available for review if so desired. If you should have questions, please .call me (336)397-7662 or Ron Hargrove at (336)747-7312. Sincerely, RECEIVEDIDENWR Bruce M. Casey FEti 1 .t 2015 Utility Plant Supervisor (Biosolids) W8terQ08l 1 Permatt ng Se on Chy Council: Mayor Allen Joines; Vivian H. Burke, Mayor Pro Tempore, Northeast Ward; Denise D. Adams, North Ward; Dan Besse, Southwest Ward; Robert C. Clark; West Ward; Molly (right, South Ward; Jeff Machnosh, Nord—t Ward; Derwin L Montgomery, East Ward; Jame; Taylor, jr., Southeast Ward; City Manager.- Lce D. Garrity Forsyth County Commisslonerin David R. Plyler, Chairman; Don Martin, Vice Chair, Ted Kaplan; Richard V. Linville, Walter Marshall; Gloria D. Whisenhunr, Everette Witherspoon; Call,311 or336-727-8000 co-tyMmag—DndleyWam,Je eltyllnk@Cityof vvs.or J , Cttyteo"ty utility Commissiom David Neill, Chairman; Randall S. Tuttle, Vice -chair, Wedey Curtis, Jr.; Harold"E. Day; Tom Griffin; Harold R: Holmes Charles D. Jewell, II; Pmd S. McGill: Chris, Parker, Al H. Seymour; J. HUI Stockton January 7; 2013 Winston•Salem Mr. Charles Wakild Office of the Director of Water Quality Division NCDENR-DWQ GregoryM. Turner, P.E. 1636 Mail.Service Center Assiamt ciry MW&W Raleigh, NC 27699=163.6 City of \wnston-Salem ro. non zd ► WIn'ston-Salem, NC 27302 .1 Subject: Delegation of Signature, Authority Tel 336.747.6806 Winston SalemlForsyth County Utility Commission ,Fax 336.748,3060 e�Jn�f•o>x Dear Mr. Wakild: By 'notice of this letter, I hereby delegate signatory authority to the position of Utilities Director for the City of Winston Salem as the Owners Representative for all permit applications, discharge monitoring reports, .and other information relating to the Commissions Facilities listed below as required by all applicable federal,, state, and local environmental agencies specifically with the requirements for signatory authority as specified in 15A NCAC 2B.0506. ,Call 3`J.1 or,336427=$000 :ciWink@cityofmorg NPDES PERMITS NCO037834 City of WS Archie Elled a WWTP NCO050342 City of WS Muddy Creek WWTP NCO079821 City of WS Thomas WTP NCO086011 City of WS Neilson WTP NCO086762 I City of WS Swann WTP LAND APPLICATION / DISTRIBUTION PERMITS WQ0000094 Ci of WS Residuals Pro am WQ0020804 City of WS Thermal. Biosolids Facility WQ0031314 City of WS Swann WTP If you have any questions, please Director) at (336) 747-7312. Sin4giory. eurner, PE Assistant City Manager feel free to contact Ron Hargrove (Acting Utilities cc: Winston-Salem Regional Office City Councils Mayor Allen Joiner:,Vivian H. Burke, Mayor Pro'knipore, Nnrtheasr Ward; Denise D: Adams, North Wand; Dan Besre, Smthwcrt Want; Robert 4' tl trk, Wot Ward; Molly Icight. South Ward: Wanda Merschel, Nonh%,m Ward: Derwin L Montgomery. Fitt Wand; Jamcs'layfor, Jr., Southeast Ward; City Manager. Lee D. Garrity CITY OF WINSTON-SALEM 2014 Class A & Class B Biosolids Monitoring Reports TABLE OF CONTENTS 1. Class A Annual Distribution & Marketing / Surface Disposal Certification & Summary Form (DENR FORM DMSDF); Pellet Handout Sheet (Contractor); Dry Ton Distribution Summary 2. Residuals Sampling Summary Explanation; Laboratory Data Certification; Laboratory Data (FORM RSSF; FORM RSSF-B) Toxicity and Hazardous testing results on Class A Pellets 4. Pathogen Reduction and Vector Attraction Reduction Certifications (DENR FORM PVRF 503) Pathogen Reduction Summary Chart of Fecal Coliform Analysis; Fecal Coliform Analysis Lab Results and Corresponding Chain of Custody Forms 6. Dryer Facility Compliance Operational Reports 7. City of Winston-Salem Class A EQ "Soil Solutions" Information Handouts 8. City of Winston-Salem Thermal Biosolids Dryer Management Facility Permit 9. Pathogen and Vector Attraction Reduction Explanation; Pathogen and Vector Attraction Reduction Certifications (DENR FORM RF) (Archie Elledge WWTP; Muddy Creek WWTP) 10. Pathogen and Vector Attraction Reduction Summaries & Operational Data (Archie Elledge WWTP; Muddy Creek WWTP) 11. City of Winston-Salem Class B cover letter; DENR FORM ACF City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 1. Class A Annual Distribution & Marketing / Surface Disposal Certification & Summary Form (DENR FORM DMSDF); Pellet Handout Sheet (Contractor); Dry Ton Distribution Summary i CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0029804 FACILITY NAME: Winston-Salem/Forsyth County Utilities Commission Thermal Biosolids Dryer Management Facility PHONE: (336)397-7662 COUNTY: Forsyth OPERATOR: Bruce M. Casey FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual I'n" Volume only) and Part C) Calendar Year: 2014 0 Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes 0 No ❑ --► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) combined NCO037834 + NCO050342 Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January as shown above None Soil Plus 593.32 Agriculture February as shown above None Soil Plus 423.84 Agriculture March as shown above None Soil Plus 548.23 Agriculture April as shown above None Soil Plus 462.17 Agriculture May as shown above None Soil Plus 568.10 Agriculture June as shown above None Soil Plus 442.44 Agriculture July as shown above None Soil Plus 584.40 Agriculture August as shown above None Soil Plus 468.11 Agriculture September as shown above None Soil Plus 480.21 Agriculture October as shown above None Soil Plus 405.79 Agriculture November as shown above None Soil Plus 456.72 Agriculture December r7777aTshown above None Soil Plus 452.50 Agriculture Total from FORM DMSDF (sup) 0 ................... Totals: Annual (dry tons): 0 .............................. 5885.83 .................. Amendment(s) used: None Bulking Agent(s) used: None * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) Part C: Facility was compliant during the past calendar year with all conditions of the land application permit v❑ Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." i 41 Signature of Permi a Date Signature of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM DMSDF (12/2006) Wiinston-Salem Forsyth CouznY • sewer • solid wane Disposal WINS,TON-SALEI'VI SOIL SOL UTION A high quality biosolids product for use as a• soil amendment for agriculture (by "Contractor.) Produced by the Winston-Salem/Forsyth County Utilities Commission's Thermal Biosolids Dryer Management Facility 27-99 Griffith Road, Winston-Salem; North Carolina 27103 Permit Number: WQ0.029804 - Winston-Salem Soil Solution is a pelletized material produced from the heat treatment of'residuals from Exceptions! Quality biosolids product municipal wastewater. This product meets the standards for a Class A> according to the EPA's 40CFR Part 503 regulations. The recipient is responsible for applying the product at a rate that does not exceed the agronomic requirement for that:crop or vegetation. Applications of this product shall be made only in accordance with the following prohibitions: 1. A minimum buffer of 10 feet shall be kept from any public or private water supply source (including. wells) or any streams, lakes, rivers or other drainageways when applying this residuals product to soil. as an ashendrnert. r snow-covered. 2. This residuals product shall not.be applied to any site that is flooded, frozenocedures adequate 3. The application or storage of. this residuals product shall be conducted by p to prevent surface runoff from carrying any disposed or stored product into any surface waters. The City/County Utilities Commission will accept no liability for misuse of the Winston-Salem Soil Solution product. For further information on the use of this produot, contact Mr. Bruce Casey at 336-391-7662 or the above address. Although no guarantee is made as to the plant nutrient.content-of this product, analysis has shown the following approximate N-P-K concentrations: Total Nitrogen 2.5 - 3.9' Phosphorus 1.3 - •1.9� % Potassium 0.12 - 0.,I6 % Receiver's Signature t _ P Date Y Zc.ised 119114 Winston-Salem/Forsyth County 2014 Annual Monitoring Report for Class A Biosolids Thermal Biosolids Dryer Management Facility North Carolina Division of Water Quality Permit #WQ0029804 Combined Biosolids Class A Pelletized Product Bulk Distributed to Land: 5886 English Dry Tons - 5340 Metric Dry Tons Combined Biosolids Class A Pelletized Product Distributed through Pellet Giveaway Program to Lawn & Home Garden or Agriculture: 0 English Dry Tons - 0 Metric Dry Tons Combined Biosolids Class A Pelletized Product Bulk Distributed to Landfill: 0 English Dry Tons - 0 Metric Dry Tons NOTE: - Biosolids that were produced in 2014 at Archie Elledge and Muddy Creek WWTP's (prior to being combined and treated in the Class A treatment facility) are described in the Class B sections of this report (see Sections 9 — 10). - Tons produced and tons disposed may be different because some biosolids are temporarily stored from one calendar year to the next. City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 2. Residuals Sampling Summary Explanation; Laboratory Data Certification; Labotatory Data (FORM RSSF; FORM RSSF-B) Winston-Salem r Forsyth County VUtt'!'1'!0tu!e*s Water � Sewer r Solid Waste Disposal City of Winston-Salem Annual Monitoring Report for Class A Biosolids for 2014 Thermal Biosolids Dryer Management Facility Manson Meads Complex North Carolina Division of Water Quality Permit # WQ0029804 City ofWinsron-Salem ANNUAL SAMPLING SUMMARY FORM and TCLP Analysis 27 99 Griffith [toad Explanations Winston-Salem, NC 27103 CityLink 311(336.727.8000) This product is a combination of Archie Elledge WWTP (NPDES# NC0037834) Fax 336.659.4320 and Muddy Creek WWTP (NPDES# NC0050342) wastewater biosolids, and is wu�w.tiryofwr.osg indicated as "Elledge/Muddy Mix Dryer Pellets" on the SAMPLING SUMMARY. (A) Laboratory analysis for metals reported on this form was performed by SW-846 methods. (B) TCLP and Hazardous Waste Testing was performed on the Pellets in September, 2014; results are attached. (C) Listed below are the labs used to generate 2014 data, their respective North Carolina Laboratory Certification numbers, and the specific parameters analyzed by each. (1) Archie Elledge WWTP Laboratory - NC Certification #69 TKN, Ammonia -Nitrogen, Phosphorus Aluminum, Arsenic, Cadmium, Calcium, Chromium, Copper, Lead, Magnesium, Molybdenum, Nickel, Potassium, Selenium, Sodium and Zinc %Total Solids for the above parameters pH (2) Rogers and Callcott Engineers, Inc. - NC Certification #27 Mercury %Total Solids (3) Environment 1, Incorporated - NC Certification #10 Nitrate + Nitrite Nitrogen (4) Pace Analytical - Raleigh - NC Certification #67 Fecal Coliform MPN % Total Solids (5) Summit Environmental Technologies, Inc. - NC Certification #631 TCLP parameters Ignitability or Flashpoint Reactivity — Sulfide, Cyanide (D) The City's Land Application staff will make available for inspection the original individual laboratory reports. City Council.- Mayor Allen Joiner; Vivian H. Burke, Mayor Pm Tempore, Northeast Wand; Denise D. Adams, North Ward; Dan Besse, Southwest Ward; Robert C. Clark, West Ward; Molly Leight, South Ward; JeffMadmmh, Northwmi Ward; Derwin L Mon ggomery, East Ward; James Taylor, Jr., Southeast Ward; City Manager: Lee D. Garrity Forsyth County Comma on= David R. Plykr. Chairman; Don Martin, Vice Chair, Ted Kaplan; Richard V. Linville, Walter Marshall; Gloria D. Whisenhunt; Everette Witherspoon; Call311 or336-727-8000 CoomyManager:Dudley Warts,Je cl`Y 9 u Ilnk cityofws.or City/County Utility Commission: David Neill, Chairman; Randall S. Tuttle, Vice -chair, Waly Curtis, It.; Harold E. Day; Tom Griffin; Harold R. Holmes, Charles D. Jewell,11; Paul S. McGill; Chris Parker, Al H. Seymour; J. Hill Smduon M: Winston-Salem v Fc�rsytE-t County unty utliffies ater • Seger i Solid Waste Disposal FACILITY: Dryer Facility, WQ0029804 REPORTING PERIOD: January -December 2014 LABORATORY DATA CERTIFICATION I certify under penalty of applicable State and Federal laws that the attached laboratory information and results are true, accurate and complete to the best of my knowledge and belief. This affirmation is made based on my inquiry of those individuals immediately responsible for obtaining and preparing the information. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment. See 18 U.S.C. 1001 and 33 U.S.C. 1319. %1 Lab Supervisor: � LC 4 A'_A _7 'Pxx Date: J / (0 1 /5 WATER AND SEWER SYSTEM OPERATOR/SUPERVISOR INTERIM DMR CERTIFICATION I certify under penalty of applicable State and Federal laws that the information which has been recorded for the periods during which I was responsible for data collection, recording and processing at the Plant, during the month indicated below, to the best of my knowledge and belief, is true, accurate and complete. This affirmation is made based on my inquiry of those individuals immediately responsible for obtaining the information. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment. See 18 U.S.C. 1001 and 33 U.S.C. 1319. Signature of Supervisor: Date: 1-14 - ad! S ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0029804 Laboratory: Facility Name: Winston-Salem/Forsyth Co. Utilities Commission Thermal Biosolids Dryer Management Facility Residual Source WQ # or , NPDES #: NPDES 9's NCO037834 & NCO050342 Combined WWTP Name: Elledge/Muddy Mix Dryer Pellets l?ncirinn1 A is Viato 1) Archie Elledge WWTP Laboratory - NC Cert #69 2) Rogers & Callcott Engineers, Inc. - NC Cert #27 3) Environment 1, Inc. - NC Cert # 10 4) Pace Analytical, Raleigh - NC Cert #67 55) Summit Environmental Tech., Inc - NC Cert #631 6) UU Ali hi Parameter (mg/kg) Ceiling Cone. Limit (mg/kg)a Sample or Composite Date 1/3/2014 2/7/2014 3/7/2014 4/4/2014 5/2/2014 6/6/2014 7/11/2014 8/1/2014 9/5/2014 10/3/2014 11/7/2014 12/5/2014 Percent Solids (%) NA 87.69 94.88 89.34 91.81 89.00 91.68 94.28 93.04 91.56 93.38 94.38 88.46 Arsenic 75 <5.50 <5.21 <5.53 <5.33 <5.61 <5.35 <5.21 <5.21 <5.41 1 <5.23 <5.23 <5.64 Cadmium 85 1.76 1.56 1.66 1.60 1.68 1.60 1.77 1.87 1.73 1.67 1.67 1.47 Copper 4,300 273 252 263 256 262 271 279 275 281 288 317 295 Chromium NA 53.3 50.2 50.5 48.1 45.8 44.2 47.3 44.0 43.5 55.5 53.6 44.2 Lead 840 42.9 38.4 .38.3 34.7 34.6 34.4 40.8 39.2 42.6 41.5 44.5 39.4 Mercury 57 1.0 1 0.85 0.88 0.72 0.8 0.85 0.9 0.92 0.99 1.0 1.1 1.2 Molybdenum 75 10.5 9.38 9.07 9.49 8.97 9.09 10.53 11.45 13.86 12.97 11.60 10.26 Nickel 420 19.4 22.9 23.9 27.1 23.7 23.9 24.4 24.6 29.6 27.1 28.2 20.7 Selenium 100 <5.50 <5.21 <5.53 7.04 <5.61 5.77 6.05 <5.21 5.85 7.84 <5.23 <5.64 Zinc 7,500 1569 1485 1479 1472 1450 1407 1449 1532 1396 1566 1648 1599 Total Phosphorus NA 16685 14022 14877 14204 1 15637 15805 13907 14187 14981 15662 13540 16212 TKN NA 34051 26770 27589 29182 32592 29828 28234 33939 33799 36296 27910 38269 Ammonia -Nitrogen NA 1 4273 1 3680 5176 4620 4524 3761 3382 3647 4656 3591 3863 4794 Nitrate and Nitrite NA 25.31 1 16.53 17.79 17.37 19.26 1 22.37 21.69 1 21.35 32.26 16.78 24.07 20.90 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. " I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility f fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r)-and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ,I r ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0029804 Laboratory: 1) Archie Elledge WWTP Laboratory - NC Cert. #69 Facility Name: Winston-Salem/Forsyth Co. Utilities Commission Thermal Biosolids Dryer Management Facility 2), Rogers & Callcott Engineers, Inc. - NC Cert. #27 Residual Source NPDES # or WQ#: NPDES #'s NCO037834 and NCO050342 Combined WWTP Name: Elledge/Muddy Mix Dryer Pellets Residual Analvsis Data 3) . Environment 1, Inc. - NC Cert. # 10 4) Pace Analytical, Raleigh - NC Cert. #67 5) Summit Environmental Tech., Inc. - NC Cert. #631 6) Parameter (mg/kg) Sample or Composite Date 1/3/2014 2/7/2014 3/7/2014 4/4/2014 5/2/2014 6/6/2014 7/11/2014 8/1/2014 9/5/2014 10/3/2014 11/7/2014 12/5/2014 Aluminum 10424 14175 12727 105.81 9928 8938 8509 8599 8248 8860 8842 9381 Calcium 23666 20220 22023 21119 21875 23628 23566 23945 23272 24058 20380 20408 Magnesium 3809 3711 4228 4362 4151 3795 3848 3477 4514 4163 4348 4082 Potassium 1486 1480 1572 1547 1571 1561 1700 1582 1537 1485 1756 1691 Sodium 550 478 584 536 529 542 585 586 612 579 702 656 pH 7.54 7.32 7.33 7.32 7.27 6.91 6.94 7.12 7.21 7.08 6.99 7.21 Duplicate pH 7.54 7.33 7.35 7.35 7.29 6.91 6.97 7.15 7.22 7.10 7.02 7.24 P.A.N. 8117 6474 7088 7239 7895 7116 6683 7903 8189 8353 6765 9113 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer, * (� *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) i/ /.s Date DENR FORM RSSF - B (12/2006) City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 3. Toxicity and Hazardous testing results on Class A Pellets Winston-Salem a Forsyth County Cry/County Utilities Water t Sewer t Solid Waste Disposal Manson Meads Complex City of Winston-Salem 27 99 Griffith Road Winston-Salem, NC 27103 CityLink 311(336.727.8000) Fax 336.60.4320 . WWW.cityofmorg City of Winston-Salem Annual Monitoring Report for Class A Biosolids for 2014 Thermal Biosolids Dryer Management Facility North Carolina Division of Water Quality Permit #WQ0029804 TCLP and Hazardous Waste Testing Attached are the results of testing for Toxicity and Hazardous Characteristics for Winston-Salem's Class A biosolids product. This product was analyzed by Summit Environmental Technologies, except for pH analysis, which was done by Archie Elledge WWTP Lab personnel. In the Summit lab report, the abbreviated sample name for the City's Class A pellet product is "BMPELLET" (short for Elledge/Muddy Pellets), and is listed as "Dryer, Pellets" on the attached TCLP summary chart. Please note on the summary chart that the EPA Hazardous Level for Reactivity for Sulfide and Cyanide is shown as "Not Applicable". This is due to EPA havingwithdrawn the test methods for these characteristics from the SW-846 manual and also having withdrawn the guidance threshold levels. EPA instructs that generators must use waste knowledge to determine reactivity. However, although the test method and threshold levels have been withdrawn, the City's North Carolina Non -Discharge permit still requires the tests. Summit Environmental Technologies is willing to analyze and report the results of those tests using the withdrawn methods, and those results are included here. Please find attached a copy of a downloaded EPA memo which discusses the withdrawal of these methods. City Cou cih Mayor Allen Joines; Vivian H. Burke, Mayor Pro Tempore, Northeast Ward; Denise D. Adams, North Ward; Dan Besse, Southwest Ward; Robert C. Clark, West Ward; Molly Leight, South Ward; Jeff Madnrosh, Northwest Ward; Denvin L Montgomery, East Ward; James Taylor, Jr., Southeasr Ward; City Manager. Lee D. Garrity Porsyda Cou tty Commlssionas: David R. Plyler, Chairman; Don Martin, Vice Chair, Ted Kaplan; Richard V. Linville; Walter Marshall; Gloria D. W hisenhunr Evtm m W thetspoon; Call311 or336-727-8000 County Manager: Dudley Watts, Jr. CltyllnlC@CltyOfwS.Drg CityrCoonry Utility Commissions Datid Neill, Chairman; Randall S. Turtle, Vice -chair, Wesley Curtis, Jr.; Harold E. Day; Tom Griffin; Harold R: Holmes; Charles D. Jewell,11; Paul S. McGill; Chris Parker, Al H. Seymour; J. Hill Stockton Reactivity Questions I Test Methods 1 Wastes I US EPA Page 1 of 1 http://www.epa.gov/osw/hazard/testmethods/faq/freact,htm La t updated on Thursday,, August 28th, 2008. Wastes - Hazardous Waste - Test Methods n r41 PRO!,c4 You are here, EPA_Home Wastes Fi.azardous _lyaste Test Methods Frequent QVesti9Reactivity Rgaqu rces...Home. ® Fre4uent Que t oU Reactivit Questl0n: What is.the current guidance regarding the Freactivity TestMcEYtt characteristic? Iheard that EPA had withdrawn the method for Reactive Cyanide and Reactive Sulfide as specified in .Chapter 7 of SW846. Is this true? Answer: 40 CFR Section 261.23 includes 8 different properties of a .waste which is hazardous because of the characteristic of reactivity, A waste is a reactive hazardous waste if it exhibits one or more of those properties, The regulations do not require specific test methods for any of these properties, Therefore, generators must use waste knowledge to determine if their waste exhibits the characteristic. of reactivity. According to property (5) under 261.23, a waste is hazardous if it is a cyanide- or sulfide -bearing waste which generates toxic gases or vapors at a quantity sufficient to present a health danger. In July 1985, EPA issued interim guidance describing certain threshold levels for cyanide- and sulfide -bearing wastes and laboratory methods for evaluating such wastes. In April 1998, EPA withdrew the July 1985 guidance, Therefore, EPA does not recommend use of the interim threshold levels or methods to determine if a waste is hazardous based on the characteristic of reactivity. In the near future, EPA will be removing the guidance threshold levels and the laboratory methods from Chapter Seven of SW-846. A gM PDE),.(s pp, 18K, About P.D_,F) of the EPA memorandum which withdrew the reactivity characteristic guidance is now available for downloading. http://wWw.epa.gov/osw/hazard`/tegtmethods/faq/freact.htm 12/7/2009 Winston-Salem/Forsyth County Utilities Commission Thermal Biosolids Dryer Management Facility North Carolina Division of Water Quality Permit #WQ0029804 Pellets Toxicity and Hazardous Testing 9/2014 Toxicity Parameter EPA Hazardous Level (mg/1) Dryer Pellets Concentration of Extract (mg/l) Arsenic 5.0 <0.50 Barium 100.0 <5.0 Cadmium 1.0 <0.10 Chromium 5.0 <0.20 Lead 5.0 <0.50 Mercury 0.2 <0.0020 Selenium 1.0 <0.50 Silver 5.0 <0.50 Benzene 0.5 <0.10 Carbon Tetrachloride 0.5 <0.10 Chlorobenzene 100.0 <0.10 Chloroform 6.0 <0.10 1,4-Dichlorobenzene 7.5 <0.10 1,1-Dichloroethylene 0.7 <0.10 Methyl ethyl ketone 200.0 <2.0 Trichloroethylene 0.5 <0.10 Vinyl Chloride 0.2 <0.20 1,2-Dichloroethane 0.5 <0.10 Ortho-Cresol 200.0 - Meta -Cresol 200.0 - Para -Cresol 200.0 - Total Cresol 200.0 <5.0 Pentachlorophenol 100.0 <0.25 2,4,5-Trichlorophenol 400.0 <0.25 2,4,6-Trichlorophenol 2.0 <0.25 2,4-Dinitrotoluene 0.13 <0.10 Hexachlorobenzene 0.13 <0.10 Hexachloroethane 3.0 <0.10 1,1,2,2-Tetrachloroethylene 0.7 <0.10 Nitrobenzene 2.0 <0.10 Pyridine 5.0 <0.25 Hexachloro-1,3-butadiene 0.5 <0.10 2,4-D 10.0 <0.10 Silvex 1.0 <0.10 g-BHC (Lindane) 0.4 <0.0020 Endrin 0.02 <0.0020 Methoxychlor 10.0 <0.0020 Toxaphene 0.5 <0.040 Chlordane 0.03 <0.020 Heptachlor 0.008 <0.0020 Hazardous Parameter EPA Hazardous Level Reactivity - Sulfide Not Applicable Not Detected Reactivity - Cyanide Not Applicable Not Detected Corrosivity (pH) <_ 2 or >_ 12.5 7.21; Duplicate pH 7.22 Ignitability (Flash Point) < 140 ° F >140 ° F Pellets and Cake Method SW-846 9045D- Archie El edge WWTP Laboratory City of Winston Salem Date 9 YIN Analystia pH Calibration Record Meter: Orion Model �*i r I Qi L with a Triode pH electrode Meter # The meter and electrode provide automatic temperature compensation All buffer results, before and after analysis, must be within 0.0.5 pH units of the theoretical value Time am pm Theoretical Buffer Initial BUFFER LOT # (4) Value at Temp QO C Calibration pH Value Mid -Range Buffer Check for Calibration and Midrange Buffer Checks EXP..DATE 13`1a3`� i(Dj�S i0,06 Weigh 20 g ± 0.5 g sample. Stir with DI water for 5 minutes, then centrifuge or settle for up to 15 minutes prior to pH measurement. W-S Pelletized Biosolids EMPEL.LET' Weight of pellets mixed with 40ml DI water o� C) g Wainh+ of rlatnl.ir:_ntP nPll.ets mixed with 40.m1 DI water oZQ o 9 Collection Collection Analysis Sample Sample Sample Date Time Start Time Temp °C pH S.U. Duplicate Time Temp Theo Buffer Value Observed pH Post Midrange Buffer Check Q • Q '7. D D W-S Cake Biosolids Weight of cake mixed with 40ml DI water g Weight of dup:l.icate cake mixed with 40ml DI water g Collection Date Collection Time Analysis Start Time Sample Sample Temp °C Sample pH S.U. Duplicate Post Midrange Buffer Check Time Temp Theo Buffer Value Observed pH All pH values on this data sheet are in units of S.U. Slope % 0513 FORM 10 (3/11) SAMPLE LOG/CHAIN OF CUSTODY (Sewage Sludge) (336)765-0130 1 City of Winston-Salem Compliance Monitoring Analysis Laboratory Name: ** Archie Elledge WWTP Laboratory SAMPLER(s) (Signature) Use SW-846 method for pH. Analysis should be begun Method within 15 minutes of collection. 9045D PELLETS pH Sample Delivered to Lab by. Sample Sample Name Description Date:L/(tJ Time: l �� 1 ( PH r DRYER Received for Lab by: PI'i'm4 H PELLETS Date: Time:7 D T C G Sample Sample 3 1 O r LOCATION LOCATION (Use if Relinquished to a Sample OTHER t m m a SOUZ'Ce Discharge to person other than Sampler P P e e p b Pellet Cooler (Identify) to be delivered to lab.) 0 ' 3? A Elledge/Muddy Mix PELLETS t� Relinquished by: Date Time Received by: is 1 �s,�� rvtb33�yy}gygzxyn y �y ¢ jtxiDY4�i"R,dt(k YdiaL}A'i 1�i.,�L��ii�CCL+Li�{a.Il�C Ji 4gT �s October 14, 2014 Diane Herndon City of Winston-Salem 2799 Griffith Road Winston-Salem, NC 27103-6417 TEL: (336) 397-7624 FAX: RE: TCLP, Hazardous Waste Dear Diane Herndon: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489 Website: ham://www.settek.com Order No.: 14092144 Summit Environmental Technologies, Inc. received 1 sample(s) on 9/18/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Alq_� Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 CC: Diane Herndon A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho 01100923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LAI2004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas TI04704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 8 Summit Environmental Technologies, Inc. summly- 3310 Win St. i llR�rtdhil f3TIsL T1it4�L4�1s5,?G Cuyahoga Falls, Ohio 44223 w Arml, 0ral i a. icJa a$Cst ass TEL: (330) 253-8211 FAX: (330) 253-4489 Website: http:/Aviviv.settek.com CLIENT: City of Winston-Salem Project: TCLP, Hazardous Waste Lab SampleID Client Sample ID 14092144-001 EMPELLET Tag No Date Collected 9/16/2014 7:50:00 AM Workorder Sample Summary WO#: 14092144 14-Oct-14 Date Received Matrix 9/18/2014 9:45:00 AM Sludge Page 2 of 8 Summit Environmental Technologies, Inc. Case Narrative SUMMOT 3310 Win St. NIVIRONMENTAL STECFN0LGwE.>, ;E4c. Cuyahoga Falls, Ohio 44223 WO#: 14092144 7 Ar., ythvi f-es:orata4e,, TEL: (330) 253-8211 FAX: (330) 253-4489 Website: http:/hvww.settek.com Date: 10/14/2014 CLIENT: City of Winston-Salem Project: TCLP, Hazardous Waste This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as estimated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. REVISED REPORT: Client name corrected per client request. Revision v1 Page 3 of 8 Summit Environmental Technologies, Inc. WO#: 14092144 sum A 3310 Win St. NVIROMM Ei NTAL TF CwAbLorliet Cuyahoga Falls, Ohio 44223 Date Reported: 10/14/2014 Anaryf;'ezf !Uwwrafakh9 TEL: (330) 253-8211 FAX: (330) 253-4489 Company: City of Winston-Salem Website: htly.-Ilwww.settek.com Address: 2799 Griffith Road Winston-Salem NC- 27103-6417 Received: 9/18/2014 Project#: TCLP, Hazardou TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst EMPELLET 001 9/16/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 9/29/2014 VVK EMPELLET 001 9/16/2014 TCLP Barlum(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 9/29/2014 VVK EMPELLET 001 9/16/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 9/29/2014 VVK E . MPELLET 001 9/16/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 601.0 C 1 5.0 9/2912014 VVK EMPELLET 001 9/16/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 &0 9/29/2014 VVK 'APELLET 001 9/16/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 9/29/2014 VVK EMPELLET 001 9/16/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 60101 C 1 5.0 9/26/2014 VVK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst EMPELLET 001 9/16/2014 TCLP Mercury 0.0020 ND mg1L Sludge EPA 7470 A 1 0.20 9/26/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ID# LabID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl - Run Analyst EMPELLET 001 9/16/2014 Chlordane, total 0.020 ND mg/L Sludge EPA 8081 B 1 0.030 9/30/2014 JBN EMPELLET 001 9/16/2014 Toxaphene 0.040 ND mg/L Sludge EPA 8081 B 1 0.50 9/30/2014 JBN EMPELLET 001 9/16/2014 En'drin 0,0020 ND mg/L Sludge EPA 8081 B 1 0.020 9/30/2014 JBN EMPELLET 001 9/16/2014 gamma-BHC 0.0020 ND mg/L Sludge EPA 8081 B 1 0.40 9/3012014 JBN W — ,PELLET 001 9/1612014 Heptachlor 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 9/30/2014 JBN .,:MPELLET 001 9/16/2014 Heptachlor epoxide 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 9/30/2014 JBN EMPELLET 001 9/1612014 Methoxychlor 0.0020 ND mg/L Sludge EPA 8081 B 1 10 9/30/2014 JBN SVOC SW-846: 8151 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst EMPELLET 001 9/16/2014 2,4-D 0.10 ND mg/L Sludge EPA 8151 A 1 10 10/2/2014 JBN EMPELLET 001 9/16/2014 2,4,5-TP 0.10 ND mg/L Sludge EPA 8151 A 1 1.0 1012/2014 JBN Page 4 of 8 _� : _ Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14092144 ;. F� r & ,�talp,9k�^rL tfsrrLp�, Ilya Cuyahoga Falls, Ohio 44223 Date Reported: 10/14/2014 AhBly th.,,aA 1..�.? o) , forlp, TEL: (330) 253-8211 FAX (330) 253-4489 Company: City of Winston-Salem Website: hiin://wiviv.settek.com Address: 2799 Griffith Road Winston-Salem NC 27103-6417 Received: 9/18/2014 Project#: TCLP, Hazardou VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst EMPELLET 001 9/16/2014 1,1-Dichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 9/26/2014 MES EMPELLET 001 9/16/2014 1,2-Dichloroethane 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 9/26/2014 MES EMPELLET 001 9/16/2014 Benzene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 9/26/2014 MES EMPELLET 001 9/16/2014 Carbon tetrachloride 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 9/26/2014 MES EMPELLET 001 9/16/2014 Chlorobenzene 0.10 ND mg/L Sludge EPA 8260 B 1 100 9/26/2014 MES IMPELLET 001 9/16/2014 Chloroform 0.10 ND mg/L Sludge EPA 8260 B 1 6.0 9/26/2014 MES &MPELLET 001 9/16/2014 Tetrachloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 9/26/2014 MES EMPELLET 001 9/16/2014 Trichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 9/26/2014 MES EMPELLET 001 9/16/2014 Vinyl chloride 0.20 ND mg/L Sludge EPA 8260 B 1 0:20 9/26/2014 MES EMPELLET 001 9/16/2014 MEK 2.0 ND mg/L Sludge EPA 8260 B 1 200 9/26/2014 MES SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst EMPELLET 001 9/16/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 10/9/2014 AKE EMPELLET 001 9/16/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 400 10/9/2014 AKE EMPELLET 001 9/16/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 10/9/2014 AKE EMPELLET 001 9/16/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 10/9/2014 AKE EMPELLET 001 9/16/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 10/9/2014 AKE EMPELLET 001 9/16/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 10/9/2014 AKE butadiene "APELLET 001 9/16/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 10/9/2014 AKE APELLET 001 9/16/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 10/9/2014 AKE EMPELLET 001 9/16/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 10/9/2014 AKE EMPELLET 001 9/16/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 10/9/2014 AKE EMPELLET 001 9/16/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 10/9/2014 AKE Page 5 of 8 Summit Environmental Technologies, Inc. WO#: 14092144 3310 Win St. rCuyahoga Fw II�C�#AtalEf rAL'e i id4Lit � s, INC3ra Fa!!s, Ohio 49223 Date Reported: 10/14/2014 z AnR;ytical t4,: raraxoiles TEL: (330) 253-8211 FAX: (330) 253-4489 Company: City of Winston-Salem Website: htto://www.settek.com Address: 2799 Griffith Road Winston-Salem NC 27103-6417 Received: 9/18/2014 Project#: TCLP, Hazardou Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst EMPELLET 001 9/16/2014 Flashpoint (140°F) >140 °F Sludge EPA 1010 1 9/22/2014 TAH EMPELLET 001 9/16/2014 Cyanide, Reactive ND ppm Sludge EPA 9014 1 0.50 9/22/2014 TIR EMPELLET 001 9/16/2014 Percent Solids 85 % Sludge SM 2540 B 1 9/29/2014 AYS EMPELLET 001 9/16/2014 pH 7.1 s.u. Sludge EPA 9045 D 1 9/19/2014 AYS EMPELLET 001 9/16/2014 Sulfide, Reactive ND ppm Sludge EPA 9034 1 25 9/22/2014 TIR Page 6 of 8 fv fD O h 03 Summit Environmental rechnologies, lne. 3310 Win Street Cuyahcr�tt falls. 0--h' fo = 4-2,22 i Tel: 330.25192l.T T iR 3301255 448c Analysis Request/Chain of Custody } „ _F`t�r.Snrltil?it F;lIvil.unrrriental Rchnolnaie;. Inc. use oniv Rim, _of- FFNo 1..t11r1�?alty Ntune (Ple"Ise.. POW) Proicet Mine,w Analytical. Parameters and Methods City of Winston-Salem TCLP, Hazardous Waste C:ttmp.,ny� acldreas Pio cct A,hin: Y 7 � 2799 Griffith Road Same Winstt.:,-Salem, NC 27103-6417 C- O p - ( ilent Ilt13t tits, Repall to Diane Herndon 33�-3y,-7624 U U C p chinit f a� 'N 1x E'tC.uac E-xI Itcwults �/_ i�Invoice as one charge, all at (lient Lmsil 1'_le.:ISe k:RtA j-1 - Rq-tiiult ✓ Oaerie titr. $3920. 00, per dianeh@cityof}•rs.or Dr. Osman - L:1 t f1 �_ w �y y.r L O C r O v) - v O � CQittitt:t i'i t'?lr12 Diane a � rJ r � � `� �_ �' t� u > '- o 1- 4 C �- 0 +J 59 11'd CItCCL if Ohio 1Ap sanrt)1Fa ✓ � pletd A�,i c' Tw a- U in 0 o-Sa[nple O N E Identificatirt FQ.`d : c Z _ `" torte I ']-In'(, Recu}ed in lah by-. Gate I Tillie Itusb tectvc teti tis Ntua; he:1t1 ratted t7;rtc by I:tb ntzwa,, LVhsic su �t } 'ilou 's 'hot tld n,:c„lly� oe "umple, to the l,uhwaM'ry. :tiute%*Cnrtnnents: Please report Reactivity on an -as Is•• basis, in mg/kg. Please analyze %TS within 7 days o collection. Please return large Zipiock bag with blue & white cooler. ACCOUNTING: Bill all 7 samples as one charge. retain+ rhs pink pagr. K Rev. '12 Date: 07/27/13 Summit Environmental Te Cooler Receipt Initials of client : t i�t�i Ci �;nb4 on- ] i ti Order Nu Date Received: Time Received: Date; Num5er of CooiersrBoxes: i N/A Shipper: FED EX UPS DHL ,;,born US Postal Walk-in I Packaging: Peanuts Bubble Wrap Paper Foai Tape on coolerlbox: f .y tnc.; inspecting cooler and samples* . opened and samples inspected; Q- Er- fe up Other: None Other: - WA Custody Seals intact Y N WA-' C-O-C in p stic .ate N NIA lce Blue ice ,,print ! absent !aCtrbid NIA Sample Temperature IR Gun #1k02Q 5k CF QAD 'c °C NIA Radiological Testing Instrument serial #35127 Yt N/A (see page 2 for scan results) "Use 1 sheet per sample for Radiological Testing. If sample is H T, the Radiological Safety Officer must be notified Immediately. C-Q•C filled out properly X ' 1 N N;A Samples in separate bags ' Sample containers intact' 'if no, list broken sample(s): N NIA N N/A Sample label(s) Complete (1D, date, etc.) C 7 N NIA Label(s) agree with C-O-CY N N/A Correct containers used cG N NIA Sufficient Sample received N WA Bubbles absent from 40 mL vials" Y N NIA " Samples with bubbles <6mm are acceptable. Indicate bubble size 1 >6mm. Was client contacted about samples Y N Will client send new samples Y N Clieit contact: Date/Time`. Logged in by: i Comments: G:,QC SHAREMDocument eontrot Templates - TrackinglCooler re ipt form Rev. 12 07-27-13.doc Page 1 of 2 s Page 8 of 8 City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 4. Pathogen Reduction and Vector Attraction Reduction Certifications (DENR FORM PVRF 503) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WQ Permit Number: W00029804 WWTP Name: Thermal Biosolids Dryer Management Facility NPDES Number: NCO037834 & Monitoring Period: From 1/1/2014 To 1/31/2014 NCO050342 „ � . w,r+. n n'lrr 11 f l _ V1n000 1"Aira*P 1AVPI nehieved and alternative performed: Pathogen Keauction Class A: kinti IM-A - U.— •11%P%FF - _�»�� ••-�-•�»-- -_. __ _____ . _ Alt. A (time/temp) <] Alt, B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Pryor Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable_ to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com osting ❑ Aerobic Digestion ❑ obr Digestion 'c Di esto ❑ .................................. .. ......... Anaerobic r lowing monitoring data: If applicable to alternative performed (Class A or Class B) complete the following Der ona yt�ca Allowable Level Pathogen Density Frequency Sample Tech - Excee- Parameter of Analysis Type in Sludge Minim Geo. Mean axim Unitsdences 2 x 10 to the MPN 6th power per gram of CFU Fecal Coliform total solids ND N/A 2.4 mpn/gr 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams .(in lieu of fecal total solid (dry coliform) weight) nPrfnrmerl! Vector Attraction Keauctlon 11.DH 0%-1'L%- VA. 1 •liV I - - •�»�� ---�-____ _____ ___ - - Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) 0 JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ ..A CERTIFICATION STA UIMLEn t tplease cnesrx LIM 4ppi VFA X"&w -y 0/"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information. used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Aef� --, -*IV. 9 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WWTP Name: Thermal Biosolids Dryer Management Facility Monitoring Period: From 2/1/2014 To WQ Permit Number: NPDES Number: 2/28/2014 WQ0029804 NCO037834 & NCO050342 �..�....,.,,., noa,...+;.,.. fIce carer m.T _t 1061 - Please indicate level achieved and alternative performed: 1 i1611Vb'Cll 1\ICY Ya.4aVu Class A: �a✓cs a.va�v ..�� .�_.. Alt. A (time/temp) 0 _� — ----- Alt B (Alk Treatment) ❑ _ - Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) [3 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate"Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ a Ra Gamm El ❑ Pasteurization Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ ' Digestion An aerobic ❑ If applicable to alternative performed (Class A or Class B) complete the.following monito ng data:. Allowable Level Pathogen Density Number OT Frequency Sample Analytical Excee- Tech - Parameter of Analysis Type niaue in Sludge Minim Geo. Mean axim Units dences 2 x 10 to the mpN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry ND N/A 218 mpn/gr weight) Salmonella bacteria 3 MPN.per 4 grams (in lieu of fecal total solid (dry 'coliform) weight) ITT 41 d%P7 "1- »a: .,4•o n1+ ... 7t;vF TPrfhrmi d! vector Attraction tceuumi Alt.l (VS reduction) ❑ H kiz)ri �. �.n� v.+� •11v. f Alt. 2 (40-day bench) ❑ a •v» _.____�__ �_ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) 0 Alt. 8 (Drying : Unstable) ❑ ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERRTIIFICATION STATEMENT• (please cnecK the appruprialc SLa1G111G11&,j t� "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the re uirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) j 3i_AV Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WQ Permit Number: WQ0029804 WWTP Name: Thermal Biosolids Dryer Management Facility NPDES Number: NCO037834 & Monitoring Period: From 3/1/2014 To 3/31/2014 NCO050342 15A NCAC 02T 1106) - Please indicate level achieved and alternative performed: Pathogen Reduction Class A: Alt. A (time/temp) 0I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic O Ra Paon ' ti ❑ eunza steurization Ray ❑ Beta R y Gamma ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ composting. ❑ Aerobic Digestion ❑ est is ion Anaerobic Di ❑ g If applicable to alternative performed (Class A or Class B) com lets the in data: Numbfollowingmonitor um er o Analytica Allowable Level Pathogen Density Frequency Sample Tech - Excee- Parameter of Analysis Type ninue in Sludge MinimumGeo. Mean axim Unitsdences 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 1.9 N/A 13.9 mpn/gr weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Vector Attraction Reduction (15A 1V UAU UZ r .IIU /) - riMbe lnuacaty aaw■ Al-- Alt.l (VS reduction) 0 Alt. 2 (40-day bench) ❑ At. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) L] Alt. 8 (Drying -Unstable) ❑ Alt 9 (Tniection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CE�R,TIIFICATION STATEMENT (please check the appropriate statement) ud' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and tine vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." .(Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or. print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WWTP Name: Thermal Biosolids Dryer Management Facility Monitoring Period: From 4/1/2014 To WQ Permit Number: WQ0029804 NPDES Number: NCO037834 & 4/30/2014 NCO050342 P th R duction (15A NCAC 02T 1106) - Please indicate level achieved and alternative performed: a ogen e Class Ai I Alt. A (time/temp) 0 1 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ I Thermophilic ❑ Ray ❑ Gamma Ray te un zation ❑ Pas Class B: Alt. (1) Fecal Density [31 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Digestion estion Anaerobic ❑ .g If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Number o Excee- Frequency Sample e Analytical a Parameter in Sludge inim Geo. Mean axim Units of Analysis TYPeTech- nioue 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 2.0 N/A 8.6 mpn/gr weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) wei t V CI:W[C I'Xttl acuvai AX%iULIMLIVu Alt.l (VS reduction) ❑ k -. -- --- ---- • I Alt. 2 (40-day bench) ❑ - ----- - Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) R1 I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check ,the appropriate statement) ❑� "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that -qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WWTP Name: Thermal Biosolids Dryer Management Facility Monitoring Period: From 5/1/2014 To WQ Permit Number: W00029804 NPDES Number: NCO037834 & 5/31/2014 NCO050342 n...7....4:.... 11 G A N!" A 0 fl'fT I t nfil - PlPa.cp indiente level achieved and alternative performed: r {i 1.11V�'GL 1�Gli LLB. Class A: �:lV ll `i ✓c'a t�vcav via .��.. Alt. A (time/temp) R1 ..�----------------- -- -i Alt B (Alk Treatment) ❑ - - Alt. C (Prior Testing) ❑ AIt.D (No Prior Test) El Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying 0 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ GammaRay ❑ ation ❑ Pasteurization Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ stion is Die ❑ Anaerobic If applicable to alternative pierformed (Class A or Class B) complete -the following monitoring data: Analytical um er o Allowable Level Pathogen Density Excee- Frequency Sample Tech - Parameter in Sludge MinimumGeo. Mean axim Units of Analysis 'I e yp nioue 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 1.9 N/A 4.9 mpri/gr weight) 3 WN per 4 grams Salmonella bacteria (in lieu of fecal total solid (dry coliform) wei t)— - I 1 nT Dl------ A—Z ml+arnativP ne.rformed: vector Attract -ion iC,euucumix �iar� i��.n�- ��� •��� - -- - Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-d4y bench) ❑ 1 Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) I3 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Cl� "I certify, under penalty of law, that the pathogen requirements in 15A 1NUAU ul l .tivo and ine vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WWTP Name: Thermal Biosolids Dryer Management Facility Monitoring Period: From 6/1/2014 To nMZA NrAr WT _11(161 - Please indicate level achieved and alternative performed: WQ Permit Number: W00029804 NPDES Number: NCO037834 & 6/30/2014 NCO050342 1 �LLLL V�GLL ita.u,L{ruvL Class A: �a✓ca a.vaav ..�� •�-.. Alt. A (time/temp) 0 .-/ - ------ Alt B (Alk Treatment) ❑ - Alt. C (Prior Testing) ❑ AID (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray El B y Gamma R ❑ Ray ation uriz ❑ Pasteurization Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ 1 Aerobic Digestion ❑ bic Digestion ❑ Anaerobic If applicable to alternative performed (Class A or Class B) complete'the followin monitorin data: um e; o Allowable Level Pathogen Density Excee- Analytical Frequency Sample Tech - Parameter in Sludge MinimumGeo.-Mean MaximumUnits of Analysis Type � 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 1.9 N/A 4.9 mpn/gr weight) 3 1VIPN per 4 grams Salmonella bacteria (in lieu of fecal total solid (dry coliform) weight), _ - ._m ,,AEI. ni------- i...,+o nATfarmed: vectorAura1:tiuu xwuuutiou `1J 1\vaav -- •t--•1 ------ - Alt. 1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) R1 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) DrIll- "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .11u6 ana the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Prepa'rer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) _Z//_/! Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) i ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WQ Permit Number: WQ0029804 WWTP Name: Thermal Biosolids Dryer Management Facility NPDES Number: NCO037834 & Monitoring Period: From 7/1/2014 To 7/31/2014 NCO050342 Pathogen Reduction (15A NCAC 02T .1106) - Plea.4 indicate level achieved and alternative performed: Class A: Alt. A (time/temp) L7 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ 'on ' h ❑ a Ray ❑ Pasteurization Beta Ray [3 Gamma R B y Class B: Alt. (1) Fecal Density [3Alt. (2) jProcess to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ i Composting ❑ Aerobic Digestion ❑ 'Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitorin data: na Ica Allowable Level Pathogen Density um er o Frequency Sample Tech - Parameter Excee- of Analysis Type nicue in Sludge MinimumGeo. Mein aximu Units yp i 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 1.8 N/A, I 1.9 mpn/gr Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry colifonn) weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) 13 Alt. 3 (30-day bench) [3Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt.7 (Drying - Stable) 0 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed ElCERTIFICATION STATEMENT (please check thr appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and .the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer* Date _*Preparer is defined in 40 CFR Part 503.9(r) and 15A N( Land Applier Name and Title (if applicable)(type or"print) Signature of Land Applier (if applicable) Date i C 2T .1102 (26) I ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WQ Permit Number: W00029804 d D M ement Facility NPDES Number: NCO037834 & WWTP Name: Thermal Biosoh s ryer anag Monitoring Period: From 8/1/2014 To 8/31/2014 NCO050342 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) , 0 Alt B (Alk Treatment) ❑ ❑ Alt. C (Prior Testing) Process to Further Reduce Patho Alt.D (No Prior Test) ❑gengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ on tr ❑ a Pas teurization za R Beta Ray L] Gamma ❑ Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ I Composting ❑ Aerobic Digestion ❑ tion i es ❑ An aerobic aero b is D g. If applicable to alternative performed -(Class A or Class B). complete the followin monitorin -Analytical Ica Allowable Level Pathogen Density ITum7er of Excee Frequency Sample Tech - Parameter in Sludge inimu Geo. Mean Maximu Units of Analysis Type nioue 2 x 10 to the MPN 6th power per gram of CFU Fecal Coliform total solids 1000 mpn per gram of total solid (dry 1.9 N/A 1.9 mpn/gr weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry OV111V1111 T .1107) -Please indicate alternative per orme Vector Attraction Reduction (15A NCAC 02 Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) l] Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ °GI certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) °This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 'y Signature of Preparer* Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Bate r1GKIP Grwr%A over: n)T t1,)1,)n r,) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WWTP Name: Thermal Biosolids Dryer Management Facility Monitoring Period: From 9/1/2014 To WQ Permit Number: NPDES Number: 9/30/2014 WQ0029804 NCO037834 & NCO050342 Pathnaen Reduction f119A NCAC 02T .11061- Please indicate level achieved and alternative performed: - ------a-- ---.----- Class A:+'Alt.D -- lt. A (time/temp) 0 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Gl Heat Drying .❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray Y a Ra Gamm ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion [3. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density um er o Excee- na Ica Frequency Sample Tech - Parameter in Sludge Minimum Geo. Mean Maximurr Units of Analysis Type 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 1.9 N/A 2.0 mpn/gr weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) 'V....4. A +++;.,.. 7?nA..n+inn 11 GA NVAl ' COT - I i n 7 i - rlease lrlQlcate UlLCUU21LIVU [Jul Aul uJIcu. ♦li�...V■ ALL. N�..•aVu a�vVa�v..v.. Alt.l (VS reduction) ❑ ��-..-. `..—� --- _--_ Alt. 2 (40-day bench) ❑ - Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) R Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 111 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system. designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) . Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date nature of Land Applier (if applicable) Date Sig *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) 1'1CA1[J CrIC)MA rnioc nn-r r�nin'nnc� ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WQ Permit Number: W00029804 WWTP Name: Thermal Biosolids Dryer Management Facility NPDES Number: NCO037834 & Monitoring Period: From 10/1/2014 To 10/31/2014 NCO050342 r _ A_ _` _ /-I G A ATrl A 1� n7T > > nAl _ Plnacn indicate level achieved and alternative performed: Pathogen nCUMAIVu Class A: I k.LOZ& vim.a -..» - ------ -- --- -- -- - Alt. A (time/temp) R1 I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable.to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ ation Ray ❑ Pasteurization Beta Ray ❑ Gamma R Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": ❑ Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion77 ...................... ion61 is Digestest ❑ ............................ Anaerobic g If applicable to alternative performed (Class A or Class B) complete-thefollowingmonitorin data: na ytica Allowable Level m er o Pathogen Density uFrequency Sample Excee- Tech - Parameter of Analysis Type in Sludge MinimumGeo. Mean Maximum Unitsdences 2 x 10to the MPN 6th power per gram of CFU Fecal Coliform total solids 1000 mpn per gram of total solid (dry 1.9 N/A 2.1 mpn/gr weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. OZ uptake) ❑ ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) R1 I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please cliecx the approprlalC blalclucuaj R1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the'pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) i//.?6 Z4,Z Date Signature of Land Applier. (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WWTP Name: Thermal Biosolids Dryer Management Facility Monitoring Period: From 11/1/2014 To WQ Permit Number: W00029804 NPDES Number: NCO037834 & 11/30/2014 NCO050342 „_.L _ ___ .1...&.' .. „e A Nr A r mT 11 n6) _ Please indicate level achieved and alternative performed: raniugen Re ucuvn Class A: Tart 11 v-- vra .aa , - -- ----------- -- - Alt. A (time/temp) R1 I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ ........ ... d Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ElThermophilic ❑ Ray Beta R y GammaRay❑ ❑ Pasteurization❑ Class B: Alt. (1) Fecal Density [3 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Digestion c Die ❑ aerobic Anaero bi g If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Number o naIca Frequency Sample Tech - Excee- Parameter of Analysis Type nioue in Sludge MinimumGeo. Mean MaximumUnitsdences 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 1.9 N/A 2.0 mpn/gr weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry colifonn weight) vector Attracuon tCeuucuvu Mari 11..cw �.. _ .__� • i - ----- ---- - Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) v Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATE1VMN r (piease cnecx thu app, uY=.a.Z J 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Z�� c Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) /a h6 // Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Winston-Salem WWTP Name: Thermal Biosolids Dryer Management Facility Monitoring Period: From 12/1/2014 To WQ Permit Number: NPDES Number: 12/31 /2014 WQ0029804 NCO037834 & NC0050342' Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) C1 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ ..................... A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Y eu iza ion Past i t ❑ Class B: Alt. (1) Fecal Density ❑ X. Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ tion ❑ e ' Anaerobic Digestion g If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Number ot Excee- Frequency Sample Analytical Tech- Parameter in Sludge dences Minimum Geo. Mean Maximu Unitsnioue of Analysis Type 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry 1.9 N/A 13.8 mpn/gr weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I wei t 'Vector Attraction Reduction (15A NCAC 02`1' .1107) -Please indicate alternative pertormea: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) 0 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) ncnio rrnonn n%ioc nnT 141)1nnnc% City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section S. Pathogen Reduction Summary Chart of Fecal coliform Analysis; Fecal coliform Analysis Lab results and corresponding Chain of Custody Forms Winston-Salem r Forsyth County CItj1/County eutfilities Water t Sewer r Solid Waste Disposal Manson Meads Complex City of Winston-Salem 27 99 Griffith Road Winston-Salem, NC 27103 CityLink 311 (336.727.8000) Fax 336.659.4320 www.dtyofws,erg City of Winston-Salem Annual Monitoring Report for Class A Biosolids for 2014 Thermal Biosolids Dryer Management Facility North Carolina DWQ Permit # WQ0029804 Pathogen and Vector Attraction Reduction Explanation Pathogen Reduction Requirements were met as follows: 1. A Fecal Coliform density was demonstrated to be less than 1,000 MPN per gram of total dry solids on each sample collected per 40CFR 503.32(a)(3), Class A -Alternative 1(i). In addition to the Certification form, DENR FORM PVRF, see the attached monthly "DRYER COMPLIANCE REPORT" for "Daily Maximum" values for Fecal Coliform analysis performed on samples collected in 2014. Also see individual Fecal Coliform results attached in the following summary, followed by each month's individual laboratory data sheets. Only bi-monthly monitoring is required; however, Fecal Coliform analysis is performed on a monthly basis. All samples analyzed for Fecal Coliform had a result of less than 1000 MPN/dry gram. 2. Time and temperature requirements were met per 40 CFR §503.32 (a)(3), Class A -Alternative 1(B) based on pelletizer specifications provided by Andritz..Please see attached on the monthly "DRYER COMPLIANCE REPORT" right-hand column ("Time Temp Met"), showing that daily Time and Temperature requirements were met for distributed Class A pellets. Also see the daily, average, maximum and minimum values for Pellet Temperatures at the Preseparator and the Solids Retention Times "Drum SRT" achieved. Vector Attraction Reduction Requirements were met by: Option 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals (stabilized by Anaerobic Digestion).. In addition to the Certification Statement on Form DENR FORM PVRF, please see attached the monthly -"DRYER COMPLIANCE REPORT" with daily, average, maximum and minimum values for % Total Solids for Distributed Class A pellets in the far left column. All values were greater than the required 75% Total Solids. City Council: Mayor Allen Joiner, Vivian H. Bu&c, Mayor Pm Tempose, Northeast Ward; Denise D. Adams, North Ward; Dan Besse, South— Ward; Robert C. Clark, Wcst Ward; Molly Leight, South Ward; Jeff Madmosh, Northwest Ward; Derwin L Montgomery, East Ward; Janus Taylor, Jr., Southeast Ward; City Manager: Lee D. Garrity 3MEM Forsyth County Cornmissionexs: David R. Plyler, Chairman; Don Martin, Vice Chair; Ted Kaplan; Richard V. Mavillr, Walter Marshall; Gloria D. Whisenhunt; Everette Witherspoon; Call 311 or 336-727-8000 County Manager: Dudley Warn, jr, eitylink@eiiyofws.org City/County Utility Commission David Neill, Chairman; Randall S. Turtle, Vice -chair, Wesley Curtis, Jr.; Harold E. Day; Tom Griffin; Harald R. Holmes; Charles D. Jcavell, 11; Paul S. McGill; Chris Parker; M H. Seymour, J. Hill Srackron Page 1 Winston-Salem/Forsyth County Class A Biosolids Annual Monitoring Report for 2014 Thermal Biosolids Dryer Management Facility (North Carolina DWQ Permit # WQ0029804) "Winston-Salem Soil Solutions" Class A EQ Pelletized Product Fecal Coliform Compliance Anal sis results for 2014: Sample Date Sample Name Sample Time Total Solids % Fecal Coliform MPN/dr ram 1/7/2014 PF140107A 7:48am 84.5 2.4 1/7/2014 PF140107B 7:52am 84.6 2.4 1/7/2014 PF140107C 7:55am 84.7 2.4 1/7/2014 PF140107D 7:58am 84.4 2.4 1/14/2014 PF140114E 7:33am 90.7 ND 1/14/2014 PF140114F 7:34am 90.8 ND 1/14/2014 PF140114G 7:35am 90.9 ND 2/4/2014 PF140204A 7:44am 92.0 ND 2/4/2014 PF140204B 7:45am 91.9 ND 2/4/2014 PF140204C 7:47am 92.0 218 2/4/2014 PF140204D 7:48am 92.0 4.9 2/11/2014 PF140211E 7:27am 90.0 5.0 2/11/2014 PF140211F 7:29am 89.8 5.0 2/11/2014 PF140211G 7:31am 89.9 2.2 3/4/2014 PF140304A 7:11am 92.2 2.0 3/4/2014 PF140304B 7:12am 91.5 4.9 3/4/2014 PF140304C 7:14am 91.5 4.9 3/4/2014 PF140304D 7:15am 91.5 4.9 3/11/2014 PF140311E 7:55am 93.7 1.9 3/11/2014 PF140311F 7:56am 93.8 1.9 3/11/2014 PF140311G 7:58am 93.8 13.9 4/1/2014 PF140401A 7:44am 90.7 2.0 4/1/2014 PF140401B 7:45am 90.4 2.0 4/1/2014 PF 140401 C 7:47am 90.7 2.2 4/1/2014 PF140401D 7:48am 90.5 5.0 4/8/2014 PF140408E 7:35am 90.4 2.0 4/8/2014 PF140408F 7:37am 90.2 2.0 4/8/2014 1 PF140408G 7:39am 90.4 8.6 * ND = Non -Detectable Page 2 Thermal Biosolids Dryer Management Facility (North Carolina DWQ Permit # WQ0029804) Fecal Coliform Compliance Analysis Results for 2014: Sample Date Sample Name Sample Time Total Solids % Fecal Coliform MPN/dr ram 5/6/2014 PF140506A 7:31am 91.0 2.2 5/6/2014 PF140506B 7:32am 91.1 4.9 5/6/2014 PF140506C 7:35am 92.4 2.2 5/6/2014 PF140506D 7:36am 92.4 2.2 5/13/2014 PF140513E 7:36am 92.8 1.9 5/13/2014 PF140513F 7:37am 92.6 4.3 5/13/2014 PF140513G 7:38am 88.5 2.0 6/17/2014 PF140617A 7:15am 92.8 1.9 6/17/2014 PF 140617B 7:16am 92.8 1.9 6/17/2014 PF140617C 7:19am 92.6 1.9 6/17/2014 PF140617D 7:20am 92.6 4.9 6/26/2014 PF140626E 7:35am 89.4 2.2 6/26/2014 PF140626F 7:36am 89.4 2.2 6/26/2014 PF140626G 7:39am 89.6 2.0 7/1/2014 PF140701A 7:39am 93.9 1.9 7/1/2014 PF140701B 7:41am 93.6 1.9 7/1/2014 PF140701C 7:43am 93.6 1.9 7/1/2014 PF140701D 7:44am 93.4 1.9 7/8/2014 PF140708E 7:35am 94.1 1.9 7/8/2014 PF140708F 7:37am 97.3 1.8 7/8/2014 PF140708G 7:40am 93.7 1.9 8/5/2014 PF140805A 7:40am 93.3 1.9 8/5/2014 PF 140805B 7:41 am 93.3 1.9 8/5/2014 PF140805C 7:43am 93.3 1.9 8/5/2014 PF 140805D 7:44am 93.1 1.9 8/12/2014 PF140812E 7:32am 94.1 1.9 8/12/2014 PF140812F 7:34am 94.2 1.9 8/12/2014 PF140812G 7:35am 94.2 1.9 9/2/2014 PF140902A 7:45am 90.4 2.0 9/2/2014 PF140902B 7:45am 90.7 2.0 9/2/2014 PF140902C 7:49am 90.5 2.0 9/2/2014 PF140902D 7:50am 90.6 2.0 9/9/2014 1 PF140909E 7:53am 93.5 1.9 Page 3 Thermal Biosolids Dryer Management Facility (North Carolina DWQ Permit # WQ0029804) Fecal Coliform ComDliance Analvsis Results for 2014: Sample Date Sample Name Sample Time Total Solids % Fecal Coliform MPN/dr ram 9/9/2014 PF 140909F 7:54am 93.6 1.9 9/9/2014 PF140909G 7:55am 93.6 1.9 10/7/2014 PF141007A 7:35am 93.7 1.9 10/7/2014 PF141007B 7:37am 93.4 1.9 10/7/2014 PF141007C 7:39am 93.4 1.9 10/7/2014 PF141007D 7:40am 93.4 1.9 10/14/2014 PF141014E 7:34am 87.9 2.0 10/14/2014 PF141014F 7:36am 87.8 2'.1 10/14/2014 PF141014G 7:39am 87.9 2.0 11/4/2014 PF141104A 7:53am 93.4 1.9 11/4/2014 PF141104B 7:54am 93.4 1.9 11/4/2014 PF141104C 7:56am 93.6 1.9 11/4/2014 PF141104D 7:58am 93.4 1.9 11/11/2014 PF141111E 7:30am 89.9 2.0 11/11/2014 PF141111F 7:32am 90.0 2.0 11/11/2014 PF141111G 7:35am 91.2 2.0 12/2/2014 PF141202A 7:31am 91.8 2.0 12/2/2014 PF141202B 7:32am 91.9 2.0 12/2/2014 PF141202C 7:34am 92.4 1.9 12/2/2014 PF141202D 7:35am 92.1 2.0 12/9/2014 PF141209E 7:39am 94.3 13.8 12/9/2014 PF 141209F 7:41 am 94.2 13.8 12/9/2014 PF141209G 7:44am 94.3 13.8 ace Analytical www.pacelabs.com 1 ANALYTICAL RESULTS Project: Sludge Fecals Class A Pellets Pace Project No.: 92185410 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF 140107A Lab ID: 92185410001 Collected: 01/07/14 07:48 Received: 01/07/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 15.5 % 0.10 0.10 1 01/09/14 15:01 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.4 MPN/g 0.021 0.021 1 01/07/14 13:10 Sample: Sludge Pellets PF 140107B Lab ID: 92185410002 Collected: 01/07/14 07:52 Received: 01/07/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual-- Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 15.4 % 0.10 0.10 1 01/09/14 15:01 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.4 MPN/g 0.021 0.021 1 01/07/14 13:10 Sample: Sludge Pellets PF 140107C Lab ID: 92185410003 Collected: 01/07/14 07:55 Received: 01/07/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 15.3 % 0.10 0.10 1 01/09/14 15:01 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.4 MPN/g 0.021 0.021 1 01/07/14 13:10 Sample: Sludge Pellets PF 140107D Lab ID: 92185410004 Collected: 01107/14 07:58 Received: 01/07/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 15.6 % 0.10 0.10 1 01/09/14 15:01 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.4 MPN/g 0.021 0.021 1 01/07/14 13:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/09/2014 03:58 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 aceA'nalytical - wesw.pacetabs.eot» / CHAIN -OF -CUSTODY ! Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem ReportTo: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799Griffith Road Copy To: Company Name: City of Winston-Salem REGULATORY Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F_ NPDES F_ GROUNDWATER r DRINKING WATER F UST I- RCRA I✓ OTHER Distrib.- Resid. Solids Email To: dlaneh(a)cltyofws.orq Purchase Order No.: See Carol Bell -Credit Card Pace Quote Reverence: Phone: 336-397-7624 Fax 336-774 8862 Project Name: j Sludge FeCals (Class "A" Pellets) Pace Project r §ite L`ocatiiiii Manager. ,� STATED, NC Requested Due DaterrAT: Std Turnaround Project Number. Pace Profile #: Regiieste l:AYtalys s,Filfered;(Y/Nrh . Section D Valid Matrix Codes Required Client Information MATRIX CODE -_ COLLECTED Preservatives N N DRINIGNG WATER OW U WATER WT v O WASTEWATER WW PRODUCT P '� U Q COMPETE START COMP, EN U w t Z_ SOILISOUD SL Of x �j N N � OIL OL SAMPLE ID WIPE WIP AIR AR U ¢ to a (I) o (A-Z, 0-9 /) OTHER oT W p w d Z Q Fes--,^ u7 L Sample IDS MUST BE UNIQUE TISSUE Ts O U D_ w r F ZO fll _ _• N U qt K w w U a2i 2 @ 'f6t 2 w ¢ O c O Z U Oto I w 'a` aa) < DATE TIME DATE TIME w # _ _, = Z Z 2 O; 0) LL. o Pace Project No.l Lab I.D. Sludge Pellets PF IA}o I o. A OTI G I :+,?4 N/A 1 X; `_ X X ;_i Y Sludge Pellets.FFj, o f b7 or c /y 7'5-aA.� NIA 1 x' '. x x 3" SludgePellets:PF-14o1o7C. oT G I 7.•S,T N. 1 x x x Sludge, Pellets PF IH-o 10 7D OT G 117t14 -7:5-SAA NIA 1 X 'Collection Terri erature OT G 17 'f A-e / ,6, 8' S. . 10 12 ADDITIONAL •RELINQUISHED BYIAFFIt.lAT10N'-�• DATE^'`-- TIME- h' ACG TED�BY TION A-E fNIE'• SAMPLE CONDITIONS -COMMENTS. PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. It ' 1 Go Class "A" treatment of sludge. Please calculate MPN on a dry h i weight basis. Analyze %TS within 7 days of collection. �Y 'U y I I LL ISM_! r U Samples packed in ice as collected; delivered in ice. I Dryer Facility Control Room: 336-397-7663 $AMPLER'NAMEANDSIGNATURE.' z� ^ 2 g _ .-: ,. _ PRINT Name of SAMPLER:p1,4 M - �s`,IC'>t::;;5, o •a -rAr�,s' SIGNATURE of SAMPLER:"~'•. 4eA., DATE Signed . _- �15'-r_•c..i+� O� >• (MMIDDIYY}: J "ate U :- r 'Important Note: By signing this torn you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 7.5 % per month for any invoices not paid Within 3D days. F-ALL-Q-020rev.06, 12-Oct-2007 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Sludge Fecals Class A Pellets Pace Project No.: 92186245 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF140114E Lab ID: 92186245001 Collected: 01/14/14 07:33 Received: 01/14/14 11:13 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.3 % 0.10 0.10 1 01/16/14 13:57 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN ND MPN/g 0.20 0.20 10 01/14/14 13:12 Sample: Sludge Pellets PF140114F Lab ID: 92186245002 Collected: 01/14/14 07:34 Received: 01/14/14 11:13 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.2 % 0.10 0.10 1 01/16/14 13:57 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN ND MPN/g 0.20 0.20 10 01/14/14 13:12 Sample: Sludge Pellets PF140114G Lab ID: 92186245003 Collected: 01/14/14 07:35 Received: 01/14/14 11:1:i matrix: Solis Results reported on a "dry -weight" basis Report Parameters Results Units, Limit MDL DF Prepared Analyzed CAS No. Qua] Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.1 % 0.10 0.10 1 01/16/14 13:58 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Col]forms, MPN ND MPN/g 0.20 0.20 10 01/14/14 13:12 Date: 01 /21 /2014 10:15 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 ZkalXical CHAIN-OF-CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company., City of Winston-Salem Report TO: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F NPDES F GROUNDWATER F DRINKING WATER F UST r_ RCRA W OTHER Dist rib. - Resid. Solids Email To: dianeh(ftitycIflivs.org Purchase Order No.: see Carol Bell credit Gard Pace Quote lw. Reference: Phone: 336-397-7624 Fax: 336-774-8862 Project Name: Sludge Fecals (Class "N' Pellets) IPace Project , In Manager. ,,o , NO Requested Due Date/TAT: Std Turnaround Project Number. IPace Profile M. Analysis:Filt6fid, Section D Valid Matrix Codes Required Client Information MATRIX CODE COLLECTED Preservatives =>r N] N DRINIUNGWATER OW 0 C> z WATER WT WASTEWATER WIN V0 11 COMPOSITE PRODUCT P SOILISOLID SIL a START C,4 04 OIL OL SAMPLE ID WIPE WP to on, za (9 6 .9 AIR M (A-Z, 0-9 OTHER OT Lu 0 w Lu z 'r Lo Sample IDs MUST BE UNIQUE TISSUE TS 0, a W z 0 X F- 0 0 0 co F. I aLL 0 Co — do Co < < 0 z re cc a) 4 0 a) adi U) DATE TIME DATE TIME U<) :It a: :E Y_ z z 2 IL o Pace Project No./ Lab I.D. Sludge Pellets PF1 +01 14E7 OT G i Nf 14 7.'3Y AA N/AI i I I I X X X Sludge Pellets PF 14o 11 -4 F oT G 14 47-14 A4 N/Al I X X Sludge Pellets P F I "+o OT G IMF 7.'I!r Am N/AI i I X X X I I Sludge Pellets PF OT G IN/Al i I X X X Collection Temperature OT G '.174st 7 44 111. 2 �DPITIONALCOMM ii U E -, �@ ,,,'RE NISH D , A6CIEP'T66 Wi" J Fil- SAMPLE CONDITIONS 'I, PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. 19 -f .- 6_4 vftl -2-140 CA) 2 Class "A" treatment of sludge. Please calculate MPN on a dry 53s weight basis. Analyze %TS within 7 days of collection.. A'. 13 3 Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 -SAMPLERE'AND'66NkTki, ,NAM, PRINT Name of SAMPLER: -t A At a E AN D a Al E 0 E SIGNATURE of SAMPLER: ATE Signed (M M.. *Important Note: By signing this form you are accepting Paces NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid Mhin 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Skudge Fecals Class A Pellets Pace Project No.: 92188435 Sample: Sludge Pellets PF140204A Lab ID: 92188435001 Collected: 02/04/14 07:44 Received: 02/04/14 11:50 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.0 % 0.10 0.10 1 02/11/14 14:08 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN ND MPN/g 2.0 2.0 100 02/04/14 13:36 Sample: Sludge Pellets PF140204B Lab ID: 92188435002 Collected: 02/04/14 07:45 Received: 02/04/14 11:50 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.1 % 0.10 0.10 1 02/11/14 14:09 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN ND MPN/g 2.0 2.0 100 02/04/14 13:36 Sample: Sludge Pellets PF140204C Lab ID: 92188435003 Collected: 02/04/14 07:47 Received: 02/04/14 11:50 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.0 % 0.10 0.10 1 02/11/14 14:09 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 218 MPN/g 2.0 2.0 100 02/04/14 13:36 Sample: Sludge Pellets PF140204D Lab ID: 92188435004 Collected: 02/04/14 07:48 Received: 02/04/14 11:50 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.0 % 0.10 0.10 1 02/11/14 14:09 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 4.9 MPN/g 0.020 0.020 1 02/04/14 13:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/11 /2014 04:03 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 aceAnalytical-- www,pacalabs.m.n iectlon A teoulred Client Information: CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C Required Project Information: Invoice Information: Page: of ;ompany. City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Wdress: 2799 Griffith Road Copy To- Company Name: City of Winston-Salem F2EGU.l ATORYAGEIGY.' s«"fi4"7 .4 .; Address: 2799 Griffith Rd., Winston-Salem, NC r NPDE_ S r GROUNDWATER r DRINKING WATER Winston-Salem, NC 27103 =mail To: dianeh(cciNofws.orgReference: Purchase order No.: see Carol Bell - credit lard PacQuote r UST r RCRA ri OTHER Disbib. - Resid. Solids a Proect Name: SIUd <nelg�: iGi none: 336-397-7624 Fax 336-774-8862 i ge Fecals (Class "A" Pellets) Pace Project ? $ite;Locatiori Manager. NC Sld Tumamund Project Number. Requested Due Date1TAT: 1 Pace Profile p: 3Regtiested,�A�ialys'isrFilte�eil'(YI�J);�` �� Section D Valid Matrix Codes COLLECTED Preservatives 3% N N I - Required client information MATRIX CODE o o DRINMNGWATFR DW WATER WT () a Z v::: 111 WASTEWATER W W v TE -Zb W "; PRODUCT P > m START N SOILWUO SL aL o< m O k C SAMPLE ID WFE WP W d; d o AIR AR w '' r Z 2 to t (A-Z, 0-9 ! ,-) OTHER or O w a U Sample IDS MUST BE UNIQUE TISSUE Ts M'T U w O a O c a s E00 p N W� ¢ a o c H z '° m arQ o Z Z O 4 � Pace Project No./ Lab I.D. F- DATE TIME DATE TIME � 4t _ _ = LL c s Sludge Pellets PF1+0o2.-0 Ai OT G M NIA 1 g :^t X X X '::z X X > X X X £K Sludge Pellets PFt4 0a20 1 B OT G /�{ yASNN WA 1 X M }3 Sludge Pellets PF jAfo 9_b 4 C. OT G rf /ef 6 IA N 1 Sludge Pellets PF J oao D OT G :off AA NIA 1 X t; X �. X Collection Temperature crr If 11 :5os41r G �+^sz $.0 Si ': F2ELINQUISH z"`*-.• :"ADD'I IONAL COSifNENT ,%i=`' -'a•,>- TIONY- :'•s+� DAATE<• F',� . +�+. ado „,: �d;> �';i1.' D'B<r'`<AFFI' . TION•.�- a ;* ��DA SAMPLE CONDITIONS -.� • * PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS.�L4-r�+at'" yn' -O g /C //'f'l I• Class "A" treatment of sludge. Please calculate MPN on a dry weight basis. Analyze %TS within 7 days of collection. ✓'� Samples packed in ice as collected: delivered in ice. - Dryer Facility Control Room: 336397-7663 SAMFLERNAME'ANDSPGtjQTURE PRINT Name of SAMPLER:_Drl'i /JE L.£NE_RNOCAI�>< . m. $ "o o- SIGNATURE of SAMPLER: �a <y/�„-,��y DATE Signed (MMIDDIYY): � / ' t— - -imoortanl Note- By sionim this form you are acceolina Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08, 12-Ott-2007 .. aceAnalytical www pacerebs com: ANALYTICAL RESULTS Project: Sludge Fecals Class A Pellets .Pace Project No.: 92189552 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF140212E Lab ID: 92189552001 Collected: 02/12/14 07:27 Received: 02/12/14 10:45 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.0 % 0.10 0.10 1 02/17/14 08:58 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 5.0 MPN/g 0.020 0.020 1 02/12/14 12:00 Sample: Sludge Pellets PF140212F Lab ID: 92189552002 Collected: 02/12/14 07:29 Received: 02/12/14 10:45 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.2 % 0.10 0.10 1 02/17/14 08:58 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 5.0 MPN/g 0.020 0.020 1 02/12/14 12:00 Sample: Sludge Pellets PF140212G Lab ID: 92189552003 Collected: 02/12/14 07:31 Received: 02/12/14 10:45 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.1 % 0.10 0.10 1 02/17/14 08:58 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.2 MPN/g 0.020 0.020 1 02/12/14 12:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/17/2014 04:22 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of.9 ace Analytical CHAIN -OF -CUSTODY i Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem Report TO: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F NPDES F GROUNDWATER f- DRINKING WATER F LIST F RCRA W OTHER Distrib. - Resid. Solids Email To: dianeh(dcitvofws.org Purchase Order No.: see Carol Bell - credit card Pace Quote Reference: Phone: 336-397-7624 FSK 336-774-8862 Project Name, Sludge Fecals (Class "N' Pellets) Pace Project Manager. x NC Requested Due DaterrAT., Sid Turnaround Project Number. pace Profile N Section D Valid Matrix Codes Required Client Information MATRIX COD COLLECTED Preservatives N IN DR[NkGN WATER DW 0 0 11 z WATER WT WASTEWATER WW 0 co COMPOSITE START C OMN� PRODUCT P SolLIS SL C-4 OIL OL SAMPLE ID WIPEWF` AIR AIR 0 co w A z a) (A-Z, 0-9 1,) OTHER OT w 0 In (L < a) Q to .2 Sample IDS MUST BE UNIQUE TISSUE TS 0 p. 2 w I.- Z0 " jw C, C"I L) w w (51 a Zi a- 0 LL 0 CL 0 :5 Z5 Cf) (0) t: < DATE TIME DATE TIME co 0 4t 7) U) = z = z z 2 LT I (D it Pace Project NoJ Lab I.D. Sludge Pellets PFI+0,2- IV OT G oha h4 1 NIAx X X Sludge Pellets PFJ+00_ ).;Z' F or ihxhl 7.*i7-4-m NIA X X F Sludge Pellets P JAfoz k&C7 OT G 4,, N/A 1 X--in, X X Sludge Pellets PF OT G N/A 1 X X Collection Temperature or G 10 ELI,�"�Q , S AMPLECONDITIONS , • PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. 7'5�AA Class "A" treatment of sludge. Please calculate MPN on a dry V 0 5.2- .ight basis. Analyze %TS within 7 days of collection. . Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336397-7663 0' b z PRINT Name ofSAMPLER: .D a -a.6 E SIGNATURE of SAMPLER: DATE Signed (M. ,-F, r 0 'Important Note: By signing this form you are accepting Paces NET 30 day payment loons and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08. 12-Oct-2007 _ aceAnalyiical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Fecals Class A Pellets Pace Project No.: 92191702 Sample: Sludge Pellets PF140304A Lab ID: 92191702001 Collected: 03/04/14 07:11 Received: 03/04/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.8 % 0.10 0.10 1 03/07/14 13:12 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.020 0.020 1 03104/1412:51 1g Sample: Sludge Pellets PF140304B Lab ID: 92191702002 Collected: 03/04/14 07:12 Received: 03/04/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.5 % 0.10 0.10 1 03/06/14 19:00 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 4.9 MPN/g 0.020 0.020 1 03/04/14 12:51 Sample: Sludge Pellets PF140304C Lab ID: 92191702003 Collected: 03/04/14 07:14 Received: 03/04/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.5 % 0.10 0.10 1 03/06/14 19:00 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 4.9 MPN/g 0.020 0.020 1 03/04/14 12:51 Sample: Sludge Pellets PF140304D Lab ID: 92191702004 Collected: 03/04/14 07:15 Received: 03/04/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.5 % 0.10 0.10 1 03/06/14 19:00 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 4.9 MPN/g 0.020 0.020 1 03/04/14 12:51 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/07/2014 06:07 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 /!2ceAnalyfical' CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company. City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem ULATORYAGENCY Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F_ NPDES F_ GROUND WATER rDRINKING F_ UST F_ RCRA rv- OTHER DIStrib. - Resid. Solids Email To: dianeh(cDcitYofws.ori;l Purchase Order No.: see Carol Bell - credit Gard Pace Quote Reference: Phone: 336-397-7624 Fax: 336-774-8862 Project Name: Sludge Fecals (Class 'IN' Pellets) Pace Project Site Location Manager. STATE. , NC Requested Due DaterTAT: Sid Turnaround Project Number. Pace Profile tk. (Y Section D Valid Matrix Codes Z' — z Required Client Information MATRIX CODE 0, 2 COLLECTED Preservatives N N WATER DW 0 z DRINKING WATER WT WASTEWATER WW u COMPOSITE COM PRODUCT P Sol SL OIL OL D, START ENA=> w 0 C\j 0) N(9 NLISOLID SAMPLE ID WIPE WP AIR AR (A-7- 0-9 IF,) OTHER OT W 0 LU LLI Z a Lo I_ - qA I q Sample IDS MUST BE UNIQUE TISSUE TS 0 C.) fo- U1 F- z . L< W 0 In cc C) a- LL 0 cL C Cl) z C) do w a) r- , DO 0 u) < DATE TIME I DATE TIME co 4t c,; X: J: z z :E 0 _*.' Oil LL P... Project No./ Lab I.D. V Sludge Pellets PF 1,+ 0 304A OT G I -A/V* 711,441 N/A I I IX1 X X1 Sludge Pellets PFJ1+0_3 0# & OT G 7,12AAk N/A N 1 X X :3 Sludge Pellets PF10f0301 C, OT G 7�'1,11 A41 N NIA 1 X X X 4' Sludge Pellets PF I Af 0 3 01f D OT G 31411-Y TIT AA It- 1 X X X X1 I I Collection Temperature OT, G /I # -7 S"" 10" 12,%it NA �,RELINQUISHED BY I AFFILIATION DATE ii�E -4cdt 0 N" A6 ATE' �,:',*E" SAMPLE CONDITIONS PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. fd3l -& Z== T Class "A" treatment of sludge. Please calculate MPN on a dry weight basis. Analyze %TS Within 7 days of collection. Samples packed in ire as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 SAMPLER NAME AND SIGNATURE U). 5- PRINT Name of SAMPLER: DIAve NEPJoeig E 00 E SIGNATURE of SAMPLER: &.' ME Signed CAS' (M . IDD *important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-0-020rev.08, 12-Oct-2007 aceAnalXical www.pecefabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: SLUDGE FECALS ("A" PELLETS) Pace Project No.: 92193099 Sample: SLUDGE PELLETS Lab ID: 92193099001 Collected: 03/11/14 01:55 Received: 03/11/14 11:35 Matrix: Solid PF140311E Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.3 % 0.10 0.10 1 03/18/14 15:01 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 03/11/14 12:50 1g Sample: SLUDGE PELLETS Lab ID: 92193099002 Collected: 03/11/14 07:56 Received: 03/11/14 11:35 Matrix: Solid PF140311F Results reported on a "dry -weight" basis Parameters Report Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.2 % 0.10 0.10 1 03/18/14 15:01 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 03/11/14 12:50 1g Sample: SLUDGE PELLETS Lab ID: 92193099003 Collected: 03/11/14 07:58 Received: 03/11/14 11:35 Matrix: Solid PF140311G Results reported on a "dry-weightt' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua] Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.2 % 0.10 0.10 1 03/18/14 15:01 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 13.9 MPN/g 0.019 0.019 1 03/11/14 12:50 Date: 03/18/2014 04:32 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 1�2cek7alytical` CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: Of Required Client Information: Required Project Information: Invoice Information: Company., City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: company Name: City of Winston-Salem � AGENCY REGULATORY Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F_ NPDES [- GROUNDWATER DRINKING WATER F LIST I- RCRA R OTHER Distdb. - Resid. Solids Email To: Purchase Order No.: see Carol Bell - credit card Pace Quote dianeh(dDcityofws.orq Reference: Phone: 336-397-7624 Fax: 336-774-8862 Project Name: Sludge Fecals (Class "N' Pellets) Pace Project Manager. Site L6c i16�1n NC TA TE., Requested Due Date/TAT: Std Tumamund 1Project Number. Pace Profile #: eq9it i6dAnoily� s� filtefe d,"(YIN),'• Section D Valid Matrix Codes MATRIXCODE (L COLLECTED N N Required Client Information z —Preservatives DRIN)ONG WATER DW 0 Lu WATER WT WASTEWATER WW M COMTAPROTTE co P Sol LID SL m 0 cPRODUCT OIL OL SAMPLE ID WIPE WP o) w LU z 0 6 0 AIR AR LU < Z Lo :E OT (A-Z, 0-9 OTHER0 TISSUE TS 0 w EL 0- 2 :�z , (D N Sample IDS MUST BE UNIQUE 0 LU Z 6 76 0 (D (5 C) < U_ 0 S DZ (5 z 0 Co co a) Co (D U) rn a) Pace Project NoJ Lab I.D. < U) DATE TIME DATE TIME TIME In I I 7) X I 2: I I z LIL) 1 Sludge Pellets PF 1+ 0 3 11 F_ -I- V AK 7J4,, N/A X X X X X X X X T _X — — — — — — — — — — — — — 2 Sludge Pellets PF JAf o3 I I E_ _2T G 6 -6 AM N/A — — — — — — — — — — — — — — 3:. Sludge Pellets PFIA+ 0311 OT G 3&h4 7.'OAIA NIA — — — — — .4 Sludge Pellets PF OT G NIA — — — — — — — — — — — — — — — — — — s. Collection Temperature OT G I — — — — — — — — — 6 7 — — — — — — — — - 8, .10 11 TIME , X4 DATE,,,, SAMPLE CONDITIONS • PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. 9 glllll-�- I � A,,, Class "A" treatment of sludge. Please calculate MPN on a dry ' - A 11, weight basis. Analyze %TS Within 7 days of collection. Samples packed in ire as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 SAMPLEf 'NAME'A PRINT Name of SAMPLER: 011NE L . ,Z DATE Signed SIGNATURE of SAMPLER: ,n " _ "> (MMI 1YY) I Do E In I I I -important Note: By signing this form you am accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.6% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 aceAnalytical www pacelabs:com ANALYTICAL RESULTS Project: SLUDGE FECALS "A" PELLETS Pace Project No.: 92195434 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: SLUDGE PELLETS Lab ID: 92195434001 Collected: 04/01/14 07:44 Received: 04/01/14 10:30 Matrix: Solid PF140401A Results reported on a "dry -weight" basis Parameters Results Units Limit MDL DF Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.3 % 0.10 0.10 1 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.020 0.020 1 Prepared Analyzed CAS No. Qua[ 04107114 16:07 04/01/14 12:42 1 g Sample: SLUDGE PELLETS Lab ID: 92195434002 Collected: 04/01/14 07:45 Received: 04/01/14 10:30 Matrix: Solid PF140401B Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.6 % 0.10 0.10 1 04/07/14 16:07 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.020 0.020 1 04/01/14 12:42 1g Sample: SLUDGE PELLETS Lab ID: 92195434003 Collected: 04/01/14 07:47 Received: 04/01/14 10:30 Matrix: Solid PF140401C Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.3 % 0.10 0.10 1 04/07/14 16:07 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.2 MPN/g 0.020 0.020 1 04/01/14 12:42 Sample: SLUDGE PELLETS Lab ID: 92195434004 Collected: 04/01/14 07:48 Received: 04/01/14 10:30 Matrix: Solid PF140401D Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.5 % 0.10 0.10 1 04/07/14 16:07 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 5.0 MPN/g 0.020 0.020 1 04/01/14 12:42 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/08/2014 02:19 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 aceAnalytical CerabsCam CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Informatiorr. Required Project Information: Invoice Information: Company: City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem REGULAT9 Ky, Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC I- NPDES [--GROUNDWATER 17, DRINKINGWATER LIST 1`7 RCRA W OTHER Distrilb. - Resid. Solids Email To: dianehAcityofws.orq Purchase Order No.: see Carol Bell - credit Card Pace Quote Reference: Phone: 336-397-7624 Fax: 336-774-8862 Project Name: Sludge Fecals (Class "K Pellets) Pace Prqect A Manager. NC Requested Due errAT: Stcl Turnaround JProject Number. Pace Pmfiie *I. a "Y Section D Valid Matrix Codes Required Client Information MATRIX CODE COLLECTED Preservatives NJ NJ I I W DRINIONG WATER DW WATER WT 0 0 Is z L3 WASTEWATER WW 0 COMPOSITE co I- z PRODUCT P > M < START w C 5- SOILISOUD SL OL w 0 Cl) OIL W SAMPLE ID IP WP 0 0 of Lu z R AR 0-91,-) OTHER OT (A-Z.0 w LU z �k to Sample IDS MUST BE UNIQUE TISSUE TS 0 O w z C"! 0 1 X Lu w 5 10) 00 �5 , 1� Cf) 0. (L LL 0 1(:5 C/) 1 C3 z 5 0 w a> LU < U) DATE TIME DATE TIME 20 z 2 a) LL wl Pace Project No./ Lab I.D. Sludge Pellets PF1404olA OT G W, X X1 I I ludge Pellets PFI+o4o I D OT G 40A NIA Sr X X 33:k Sludge Pellets PFI"40 I C OT G "+7 Am - NIA X X Sludge Pellets PFIJ+0401 OT I G r-'PA 7. .! A11A 7. ICAN NIA 1 X X X X Collection Temperature OT I G 7, 15t, A" LCO NA MENTS U 7777-1-7,77, UISHED I P N 171-11"t", TIME SAMPLE CONDITIONS PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. Class "A" treatment of sludge. Please calculate MPN on a dry de k weight basis. Analyze %TS within 7 days of collection. Samples packed in ice as collected: delivered in ice. Dryer Facility Control Room: 336397-7663 G T RE�*�' SAMPLER"NAME AND U co PRINT Name of SAMPLER: DIAN E L. RCANDI)d 6 i. z SIGNAL) TIME of SAMPLER: DATE Signed0 E w CO *Important Note: By signing this form you awaccepting Pace's NET 30 day payment terns and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08,12-Oct-2007 aceAnalytical —paceraba.com ANALYTICAL RESULTS Project: Sludge Fecals Class A Pellets Pace Project No.: 92196423 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets 140408E Lab ID: 92196423001 Collected: 04/08/14 07:35 Received: 04/08/14 12:02 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.6 % 0.10 0.10 1 04/14/14 17:51 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/9 0.020 0.020 1 04/08/14 14:34 1g Sample: Sludge Pellets 14040817 Lab ID: 92196423002 Collected: 04/08/14 07:37 Received: 04/08/14 12:02 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.8 % 0.10 0.10 1 04/14/14 17:51 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.020 0.020 1 04/08/14 14:34 1g Sample: Sludge Pellets 140408G Lab ID: 92196423003 Collected: 04/08/14 07:39 Received: 04/08/14 12:02 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.6 % 0.10 0.10 1 04/14/14 17:51' 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 8.6 MPN/g 0.020 0.020 1 04/08/14 14:34 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/15/2014 03:12 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 1�12ce/lnalytical Ww 'pacwabs.com CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C 'action A Page: Of Inquired Client Information. Required Project Information: Invoice Information: ,Gmpany.* City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention r Carol Bell - Lab Supervisor Wdress: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem ;""A �Y'4 Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F_ NPDES F_ GROUNDWATER r DRINKING WATER F_ LIST 17 RICRA W OTHER Distrib. - ResId. Solids :Mail To. dianehAcilyoftus.om Purchase Order No.: see Carol Bell - credit card Pace Quote Reference - 'hone: 336-397-7624 F— 336-7 Name: Sludge Fecals (Class "K Pellets) Pace Project I m—ager: NC tecluested Due Date/TAT: Std Turnaround Project Number. Pace Profile M rxg- Section D Valid Matrix Codes Required Client Information MATRI CODE COLLECTED Preservatives 31'i M I NJ I DRINKINGWATER DW 0 0 z WATER WT WASTEWATER WW z 1 11 0 COMPOSITE C3 -:� LLI PRODUCT P Sol SL no g START w 0 Z� Of 0) Co. OL W WP SAMPLE ID IPE 0 w z DL Gl f`/�r/(,i.(if AIR AR (A-Z. 0-9 1,-) OTKER OT w aw < 0. Z a) lzj , C%I 0 Sample IDS MUST BE UNIQUE TISSUE TS .0 IL W z 6 .1, 0 w w 0 (5 .. 0 I (L C.) u- 2 CL 0 U) 2 < < 0 C '�� z M z W z (D 2 Pace Project NoJ Lab I.D. V) DATE TIME DATE TIME w LL Sludge Pellets PF 1Jf0q-8 E OT G 141111 7 *J-lr AfA NIAI I L X i X X 1 I I I Sludge Pellets PFI-+040'9 F OT G 7AAIWAI i I + I I I X X X 1 I I Sludge Pellets PFI 'to q0 9 G OT G .':;t A.] NIAI 1 1 1 1 X X X1 I I Sludge Pellets PF OT G I WAI I I I X X X 1 I I Collection Temperature OT G */I—t All & i -#I .11 L SAMPLE CONDITIONS PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. 4 ZtJ418J•I-It V Class "A" treatment at sludge. Please calculate MPN on a dry U 0 1 -.5 weight basis. Analyze %TS within 7 days of collection. Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-3977663 -6 7z Co PRINT Name of SAMPLER: b D ATE 51 SIGNATURE of SAMPLER: CM",q RIZ-1-le - : ro 0 =0 *Important Note. By signing this form you are accepting Pace's NET 30 day payment terms and agmeing.to late charges of 1.5% per month for any invoices not Paid yifthin 30 days. F-ALL-Q-020rev.08,12-Oct-2007 (�IaceAnalXicale _pacefabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pellets- Class "A" Pace Project No.: 92199923 Sample: SLUDGE PELLETS Lab ID: 92199923001 Collected: 05/06/14 07:31 Received: 06/06/14 11:44 Matrix: Solid PF140506A Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.0 % 0.10 0.10 1 05/13/14 08:36 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.2 MPN/g 0.020 0.020 1 05/06/14 13:25 Sample: SLUDGE PELLETS Lab ID: 92199923002 Collected: 05/06/14.07:32 Received: 05/06/14 11:44 Matrix: Solid PF140506B Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.9 % 0.10 0.10 1 05/13/14 08:38 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 4.9 MPN/g 0.020 0.020 1 05/06/14 13:25 Sample: SLUDGE PELLETS Lab ID: 92199923003 Collected: 05/06/14 07:35 Received: 05/06/14 11:44 Matrix: Solid PF140506C Results reported on a "dry -weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.6 % 0.10 0.10 1 05/13/14 15:47 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.2 MPN/g 0.019 0.019 1 05/06/14 13:25 Sample: SLUDGE PELLETS, Lab ID: 92199923004 Collected: 05/06/14 07:36 Received: 05/06/14 11:44 Matrix: Solid PF140506D Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.6 %. 0.10 0.10 1 05/13/14 15:47 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.2 MPN/g 0.019 0.019 1 05/06/14 13:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/13/2014 04:32 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10 Analytkal CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody Is a LEGAL DOCUMENT. At relevant flelds must be completed accurately. Section A Section B Section C Of Required Client Information: Required Project InfOrMflOrr. Invoice Information: Company; City of Winston-Salem Report To. Bruce Casey - Dryer Fatality Supervisor Attenlioft Carol Bell - Lob Supervisor Address: 27N Griffith Road Copy To: Company Name: CittyofWnston-Salem REGULATORX- A cy. Winston-Salem, NC 27103 � Address: 2799 Griffith Rd., Winston-Salem, NC r- NPDES r GROUNDWATER F. DRINKING WATER of ulu.-Rs�a. scum f- LIST F RCRA to OTHER Ernall To. d1aneh(ZWtyofvvs,org Purchase Order No.: see Carol Bell - credit card Pace 0"n' Phone: 33 336-774-8862 Pellets) IP,4- --: Sludge Fecals; (Class W P Pate P,*d Manager STATE NC Requested DAWTAR W jurnaround Protect Number. P.-PMMX. -Khque9t6d---Anatysis r- ime w Section 0 Valid Matrix Codes Requked Cuent leftimsficn MATR 9M WATER VVT R WASTEWATER WW PRcoucT P S0Lf50LKP SL OL 0L SAMPLE ID wp PIR AR (A-Z 0-9 1,-) on*R OT Semple iDs MUST BE UNIQUE TISsLE T$ Z g i6 0 X 67 0 pI co w a. COLLECTED z C) - 0 (L cc w z < z c.) 0 U I Preservatives tvalives i7. COMPOSITE START mW5 — o (D ow — 16 nt — — Y, 6 z ;j- CIA cj (ZL u- 0 6. .21 (AM Pace Project NoJ Lab I.D. DATE TIME DATE TIME Sludga Pellets PF1fo56(j OT G S/6 111- 17,-:?/ A., wA 1 X F i�.: i x x x x Sludge Pellets PF14,050 Ig8 OT G s N Sae Win 1 X x x 3. Stud e Pellets PFl+050/-0- OT T G 7, Isr X X .4 udge Pellets PF Of D&D rIOTT G 3-1 — — — — x — Collection Temperature OT G 117�471M F -7- , - �C• Ttw SAMPLECONDITIONS PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. Aa —4d- lilt 7 -4- Class -A- treatment of sludge. Plane calcuWe MPN on a cry welghf bash. Analyze %TS wftHn 7 days of collectionLy Samples packed in ice as coliocled; delivered In Ice. zr Dryer Facilly Control Room: 336-397-7663 Ix PRINT Name of SAMPLER: L— FA E-P-M D6?J ----ATUREofs"PLER: A.,. 4, I DATE Si (MWI>D=- 67/(-Ilt 9.POHMN01e: By sigri.g Mh form you — a..PUng Pace's NET 70dwy Payment ms aM agreeing to Ime charges or 1.5%. M mnIh ral AnYmOkes not pawghm W days F-ALL-0-020r&4.08.12-Oct-2007 aceAnaly ical W WW-pacefabs com: ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Fecals "Class A" Pace Project No.: 92200956 Sample: PF140513E Lab ID: 92200956001 Collected: 05/13/14 07:36 Received: 05/13/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Parameters Percent Moisture Percent Moisture 92210E Fecal Coliform, MPN RAL Fecal Coliforms, MPN Report Results Units Limit MDL Analytical Method: ASTM D2974-87 7.2 % 0.10 0.10 Analytical Method: SM9221C E (MPN) 503 1.9 MPN/g 0.019 0.019 DF Prepared Analyzed CAS No. Qual 1 05/15/14 14:36 1 05/13/14 13:30 1g Sample: PF140513F Lab ID: 92200956002 Collected: 05/13/14 07:37 Received: 05/13/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.4 % 0.10 0.10 1 05/15/14 14:36 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 4.3 MPN/g 0.019 0.019 1 05/13/14 13:30 Sample: PF140513G Lab ID: 92200956003 Collected: 05/13/14 07:38 Received: 05/13/14 11:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 11.5 % 0.10 0.10 1 05/15/14 14:36 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.020 0.020 1 05/13/14 13:30 1g . Date: 05/16/2014 06:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 CHAIN -OF -CUSTODY I Analytical Request Document 2ceAnalytical The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 7 www.pacerabs,00m Section B Section C Page: of action A aquired Client Information: Required Proled Information: Invoice Informatlon: Attention: Carol Bell - Lab Supervisor xnpany. City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Company Name: City of Winston-SalemREGU,LTOZXAGNGY.;,-;; idress: 2799 Griffith Road ca�yTo: Address: 2799 Griffith Rd., Winston-Salem, NC F NPDES F GROUND WATER F DRINKING WATER Winston-Salem, NC 27103 (— UST r RCRA �/ OTHER Distnb Resid. Solids mail To: dianehCa)cityofws.orq Purchase order No.: see Carol Bell -credit card Pace Quote Reference: hone: 336-397-7624 Fax 336-774-8862 Project Name: Stud a Fecals (Class "A' Pellets) 9 Pace Project Site!Loaation Manager. NC Pace Profile W. .eeuested Due DaterrAT: SW Tumamund P ect Number rot _ . _ . ....... .... . - - - Lion D Valid Matrix Codes _ aMDATETIME CTED Preservatives zy> N N ulred Client INormation MATRIX CODE O , DRWInNGWATER DW UZ _ w WATER Wi WASTEWATER W W v 11 Vt,O�MP�1S1K�.� co0 W M `-• PRODUCT F SOIUSOLID Sl P �y v" KO J - I Ol yx z 6 SAMPLE ID �E vo W a Z s AIR ARw (A-Z, 0-9 / , J OTHER OT a u7 U l6 Sample IDS MUST BE UNIQUE TISSUE TS O O W Z o `T O w O w O@ U U) v tr 1— aa ,., LL o O p =;C cn o c z v m m •: o w Pace Project No./ Lab I.D. CoDATE TIME N = Z Z O- LL o 5 3 NIA 1 X X X `,, Sludge Pellets PF1 rf 6 5/3 E OT G Sludge Pellets PF1+0513 F OT G 3 i :3 M NIA 1 x ;• x x Sludge Pellets PF14o513G or c /3 i 38 AA NIA 1 x ' > x x Sludge Pellets PF OT G N/A 1 x =': x x x r1AI +;^n Tomnornhlrp OT G rh 3I .� �'� -. 11f RELINQUISHED,BY/.-AEFI[]ATIR... ADDITIONALCOMMENTS=' - PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS.' Class "A" treatment of sludge. Please calculate MPN on a dry r LIA = ON. SAMPLE CONDITIONS weight basis. Analyze %TS Within 7 days of collection. Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 m ;SAMPLER NAME AND.SIGNATURE PRINT Name of SAMPLER: DO r1) SIGNATURE of SAMPLER: w�y� .9 DATE Signed (MM/DD/YY): v a Im o w >- ?� m � a cDi m£ _...-- -------- F-ALL-Q-020rev.08, 12-Oct-2007 aceAnalytical" www. pecelabsxom; ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Pellets Class A Pace Project No.: 92205554 Sample: Sludge Pellets PF 140617A Lab ID: 92205554001 Collected: 06/17/14 07:15 Received: 06/17/14 12:15 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.2 % 0.10 0.10 1 06/19/14 17:27 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 06/17/14 14:40 1g Sample: Sludge Pellets PF 140617B Lab ID: 92205554002 Collected: 06/17/14 07:16 Received: 06/17/14 12:15 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.2 % 0.10 0.10 1 06/19/14 17:23 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 06/17/14 14:40 1g Sample: Sludge Pellets PF 140617C Lab ID: 92205554003 Collected: 06/17/14 07:19 Received: 06/17/14 12:15 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.4 % 0.10 0.10 1 06/19/14 17:23 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 06/17/14 14:40 1g Sample: Sludge Pellets PF 140617D Lab ID: 92205554004 Collected: 06/17/14 07:20 Received: 06/17/14 12:15 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.4 % 0.10 0.10 1 06/19/14 17:23 92210E Fecal Col[form, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 4.9 MPN/g 0.019 0.019 1 06/17/14 14:40 Date: 06/20/2014 03:02 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 /aceAnalytical' CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C page: Of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem Repo To: - Bruce Casey - Dryer Facility SupervisorAttention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: company Name: City of Winston-Salem - Address: 2799 Griffith Rd., Winston-Salem, NC F_ NPDES r- GROUNDWATER 17- DRINKINGTER Winston-Salem, NC 27103 17— LIST F_ RCRA Fv� OTHER Distrib. - Resid. Solids Email To: dianehAciWofws-019 Purchase Order No.: see Carol Bell - credit Gard Pace Quote Reference: Phone: 336-397-7624 _33 774-8862 Project Name: Sludge Fecals (Class "N'Pellets) Pace Project ,ManaSkerLcatlon uer. P NC Requested Due Date/TAT: Sid Turnaround Number. Ir" !47" y Section D Valid Matrix Codes COLLECTED Preservatives N N 1 Required client Information MATRIXCODE 0 z DRIN)ONG WATER DW WATER WT WASTEWATER WW 1) It 0 COMPOSITE cc M 9 F_ w PRODUCT P M 9 START U1 N NSOft,S0UD SL I OL OIL C' W; 0) WIPE WP SAMPLE ID S of LLI z AIR AR Lu < z ur) :E (A-Z, 0-9 1,-) OTHER OT 0 w M — - C) Sample IDS MUST BE UNIQUE TISSUE TS 0 EL z 0 a) (5 0 �,w 0 tt X w a. UI 0 LL 0) 2 CL (5 0 U) < < 0 z = X z z 01 Pace Project No./ Lab I.D. co DATE TIME DATE E TIME co U LL Sludge Pellets PFI+o i IA OT G NIA I X X X X _ X X X X X X — — — — X X Sludge Pellets PFJ*0(� I 'J 8 _2T G 6 NIA 1 Sludge Pellets PF 1*0 12- OT G li-1114 .18 AA, NIA Sludge Pellets PF1 Aft) 1-7 C� OT G -1� I, '7,2.e AA r2 NIA — — Collection Temperature OT G 1,11711'� WA I A'V� , &_d J_ Ft- --r p FIL 7� VrN� DAT E "M 4k SAMPLE CONDITIONS PULVERIZE SAMPLES PRIOR 10 ANALYSIS. 47 PLEASE 1/9 x Class "A" treatment of sludge. Please calculate MPN on a dry 6 -11-1 17; 116 weight basis. Analyze %TS within 7 days of collection. Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: &%-397-7663 NAME77, PRINT Name of SAMPLER: 0 0 DATE Signed SIGNATURE of SAMPLER: )�3 (MMfDDIYY): 0 Z ; w F-ALL-Q-020rev.06, 12-Oct-2007 -Important Note: By signing this,form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within30 days. (��aceAnalyfical" wwW. pacelaft com, ANALYTICAL RESULTS Project: Sludge Fecals Class A Pellets Pace Project No.: 92206942 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF140626E Lab ID: 92206942001 Collected: 06/26/14 07:35 Received: 06/26/14 12:06 Matrix: solia Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.6 % 0.10 0.10 1 06/30/14 15:28 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.2 MPN/g 0.020 0.020 1 06/27/14 07:13 Sample: Sludge Pellets PF140626F Lab ID: 92206942002 Collected: 06/26/14 07:36 Received: 06/26/14 12:06 Matrix: 5oua Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.6 % 0.10 0.10 1 06/30/14 15:28 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.2 MPN/g 0.020 0.020 1 06/27/14 07:13 Sample: Sludge Pellets PF140626G Lab lD: 92206942003 Collected: 06/26/14 07:39 Received: 06/26/14 12:06 Matrix: cioua Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.4 % 0.10 0.10 1 06/30/14 15:29 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.020 0.020 1 06/27/14 07:13 1g Date: 07/01/2014 09:52 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 Analytical'" w ,pacafabs.cam f CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor ay Cany Name: City of Winston-Salem ompG Address: 2799 Griffith Road Address: 2799 Griffith Rd., Winston-Salem, NC (- NPDES f GROUND WATER (- DRINKING WATER Winston-Salem, NC 27103 Email To: dlaneh(fDCityofWs,Orp Purchase Order No.: See Cat016011 - Credlt Card Pace Quote E- UST I- RCRA Iv OTHER Distnb. - Resid. Solitls Phone: 336-397-7624 Fax 336-774-8862 Project Name: Reference: , Pace Project �'�` `�-_•�" Sludge Fecals (Class "A" Pellets)5ita t ocatio Manager, E• NC Requested Due Date/TAT: Slid Turnaround Project Number. - Pace Profile '` ;Fiegii',esteil AiialysisPFilfere¢;{Y/N);_, Section D Valid Matrix Codes c^ -_ ' COLLECTED Preserva8ves ^.> N N Required Client Information MATRIX CODE O _ DRINIdNGWATER DW WATER W7 U ItU Z M°-^• W WA�R WW U m' COMPOSITE CAM ~ START F1dD W " N z } PRODUCTWASTE Q _ N SOIUSOUD SL OL a: _` ilil�; y C OIL SAMPLE ID WIPE WP 0 (� U � Z a H W d O "Fa 0 AIR AR lL (A-Z, 0.9 / ,) OTHER OT O Z "O � _ N U Sample IDs MUST BE UNIQUE nssuE rs a w Z Z o L` o 3 X W w p to \. U� () y = N N M!, — D cn t d1 m v w ¢ a c a LL O p , q= fn a o c z U m m t Q= m o , w tY Pace Project NoJ Lab I.D. 1 F ro DATE TIME DATE TIME to * Z I Z Z c Sludge Pellets PFI/'i-O(oaloE Or c 1 x x xlud Xr x x a Pellets PF( bfo9_t F OT G 4 NIASlud a Pellets PF►AFo(o�G OT GN/A F._-ANIA 1 Sludge Pellets PF OT G N/A 1 S=k Collection Temperature OT G x % sR� a•Y' fS"k'-4""y"--1 BY 1iAF<flL1ATI0r4 x.,.,,a.., DA7E:�,YR ��.,-,:z <•�,t�:. SAMPLE CONDITIONS , -... < . .. ,. ,e ,.. -....� .-:v-c,r �,.,-, z:. <,,.. -Y ; ;a-Y. _:..,.,.t,...,.,�..,,,�,,.�.,•�,,::,,.>,,,�,,,.,,x•..,-,�,;,..,-.,�.,,.�„��,,.,K e, ,.,. .,r,:� +&:, *;s.'� HED'•BY/,AF.FILIA ON,:>' T(- .., =,fir - -DATE-�" , =z�s-4-.. .:a-�'i.' b�ITIONA1s MBNT5i• ..> . µ �~ H , _ PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. ^ �-- J 6 / : �� �, �Zd / f/ Class "A" treatment of sludge. Please calculate MPN on a dry �J ft L D ) weight basis. Analyze %TS within 7 days of collection. Samples packed in ice as collected; delivered in ice. _ Dryer Facility Control Room: 336397-7663 SA111p1E12;NAtAEA1JB, SIGNATUIii "` m c PRINT Name of SAMPLER: E 2 o o DATE'Signed t0- tom) m `-' D �- w SIGNATURE of SAMPLER: Im *Important Note: B signing this torte u are accepting Paces NET 30 d payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 ' po Y 9 9 you P 9 day P Yrn 9 9 r9 acei nnl ical www paeelabscom: ANALYTICAL RESULTS 'Project: ' Sludge Fecals- Class A Pellets Pace Project No.: 92207457 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF140701A Lab ID: 92207457001 Collected: 07/01/14 07:39 Received: 07/01/14 10:30 Matrix: Solio Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.1 % 0.10 0.10 1 07/03/14 18:17 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 07/01/14 11:27 1g Sample: Sludge Pellets PF140701B Lab ID: 92207457002 Collected: 07/01/14 07:41 Received: 07/01/14 10:30 Matrix: Solid Results reported on a "City -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.4 % 0.10 0.10 1 07/03/14 18:17 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 _ 0.019 1 07/01/14 11:27 1g Sample: Sludge Pellets PF140701C Lab ID: 92207457003 Collected: 07/01/1407:43 Received: 07/01/14 10:30 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.4 % 0.10 0.10 1 07/03/14 18:17 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 07/01/14 11:27 1g Sample: Sludge Pellets PF140701D Lab ID: 92207457004 Collected: 07/01/14 07:44 Received: 07/01/14 10:30 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 % 0.10 0.10 1 07/03/14 18:17 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 07/01/14 11:27 1g REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/03/2014 07:58 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 /72ceAnaIjIfical- CHAIN-OF-CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT: All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company City of Winston-Salem Report To' Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address 2799 Griffith'Road c°Py To: - company Name: City of Winston-Salem REGU,tI„%TORYFwA,GENGY'`_ _ -- Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC f- NPDES.F GROUND WATER I— DRINKING WATER Email To: dianehCcDcitvofws.orQ Purchase Order No.: see Carol Bell - credit Card Pace Quote I— UST i 1 RCRA W OTHER Distdb. - Resid. Solids Phone: 336-397-7624 Fax 336-774-,8862 Project Name: Reference: Pace Pm act"` Sludge Fecals (Class "A" Pellets) j -Si wwolitioti Manager. f''' �"` NC Requested Due DaterrAT' Std Turnaround Project Number, Pace Profile#. 9¢TT sxReges4ed AnaljssF(itgedP(Y1�1j;«i-'„ Section D Valid Matrix Codes Required client information MATRIX CODE — o `$ti COLLECTED Preservatives 'zr ; N N DRINIeNGWATFR WATER DIN m WT U II Z OF? lJ.l . WASTEWATER WIN u U COMPOSITE COM�,p,�Or��eppE�l V "yb Z PRODUCT P Q START -.7M) W y= N y C.• SOIL50UD OIL SL OL or � V SAMPLE ID WIPE N1° w SONi a o 0 AIR AR w}= v (A-Z„0-9 r,-) OTHER O7 0 w C"! C)Sample IDs MUST BE UNIQUE nssuE Ts O v a w w Z Z p m>r U 3 .�. X J a. (0 w ¢ a Q IL O .i? N a 0 c z U to t 'Q: o 0 In t Pace Project No./ Lab I.D.ro DATE TIME DATE TIME rn 4t I Z Z Z r+t Lt.. o Sludo a Pellets PFI$o701 A OT c 7't 1 f :.1 wA 1 X z; X X i x Sludge Pellets PFI` o 01 B OT c N/A 1 x H' x x Sludge Pellets PFPf 0701 C OT G 7 11` 3A NIA 1 x ? F, x x 1 �. Sludge Pellets PF /Ifo7ol D IT c 1# 7; NIA 1 x r . x x Collection Temperature OT c I t $ 71-7AM +FtE' QUI$HED'•BYiAFF11:1�1 O,N; ` �'�, � ::i'� x._•u 4 "s'•.":� a:F:u' - =gym ;>. ,_ "_. CONDITIONS SAMPLE O at ; _� PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. ,� �. 05� �i - J 10 Class "A" treatment of sludge. Please calculate MPN on a dry C�` !� 7 �)^') �l 1 r.0 •2r weight basis. Analyze %TS within 7 days of collection. �"'�/ Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 - 'SAMPLER NAME°AND"SIGNATURE s � � �- z °' ;y o w ? 1O _�, , PRINT Name of SAMPLER: p• (_ , (A CAM 0 0 A1 n E $m oo m nY .. DATE Signed �[ SIGNATUREdf SAMPLER- �, �O - (MM/DD/YY): %/�/�"[ r at .2 Iz ° U E CO., -importantNote: Sy signing this form you are accepting Pace's NET 30 day payment terns and agreeing to late charges of 1.6%'per month for any invoices not paid within 30 days. F-ALL-0-020rev.06, 12-Oct-2007 W Angljdical www.pacelabs:com- ANALYTICAL RESULTS Project: Sludge Fecals Class A Pellets Pace Project No.: 92208178 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF140708E Lab ID: 92208178001 Collected: 07/08/14 07:35 Received: 07/08/14 11:47 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.9 % 0.10 0.10 1 07/11/14 17:24 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 07/08/14 12:33 1g Sample: Sludge Pellets PF140708F Lab ID: 92208178002 Collected: 07/08/14 07:37 Received: 07/08/14 11:47 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.7 % 0.10 0.10 1 07/11/1417:21 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal. Coliforms, MPN 1.8 MPN/g 0.018 0.018 1 07/08/14 12:33 1g Sample: Sludge Pellets PF140708G Lab ID: 92208178003 Collected: 07/08/14 07:40 Received: 07/08/14 11:47 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.3 % 0.10 0.10 1 07/11/14 17:21 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 0.019 1 07/08/14 12:33 Date: 07/11 /2014 05:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual 1g Page 5 of 9 aceAnalytical •" www,pac8/abs.can Section A CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section B Section C R-1—cl Prn,—t Infnnnatinn' Invoice information: Page: of I ..may ........ ......... .................. Company- City of Winston-Salem --_�----... , Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor copy To: company Name: City of Winston-Salem .�:N;:..�:,,..-,.Y....�- .,.x..*s.,e,,,,c. 3h°As„�..,.;'�.z:,�N>'x,'?^�7.�ix[i'�,�,,xg•.., :��: :.?�..';e':!* , R�GWls1�TgRYAG6NG1f<<.^<,` Address: 2799 Griffith Road ,.,;-,...,,;4.,.�,,, _ m3°.. • �.�.,=c :.., sr Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC (— . NPDES GROUND WATER r-. DRINKING WATER F UST F— RCRA rv— OTHER Distdb.- Resid. Solids Email To: dianeh0cityofws.Ora Purchase Order No.: see Carol Bell - credit Card Pace Quote Reference: Phone: 336 397-7624 Fax 336-774-8862 Project Name: Sludge Fecals (Class "A" Pellets) Pace Pmicict ;Site Locatoh $TATEc NC Requested Due Date/TAT' Std Turnaround Project Number. Pace Profile tk;-, ����Fieq�es{el�Analysts �iifeted (YIN) , Section D Valid Matrix Codes Required Client lnformation -MATRIX CODE — a COLLECTED Preservatives )• N N - COMPOSITE START CAMPO EN tL i(•//JJ,t' DRINIOND WATER DW WATER WT WASTEWATER WW 90 U Z PRODUCT P Q J ra N SOIUSODD SL OIL OL ummi Ir V fn - SAMPLE ID WI E W �? ¢ Lu F a v o (A-Z, 0-9 / :) OTHER OT w D- Q D } ""s t U Sample IDs MUST BE UNIQUE TISSUE TS O U a 2 LLI F ^ 0 (V X w w o U m 2 0 c ro y` 't65 co 3 ;g a.d rn z m L4 w ¢ a Q o c v ra Z 2 O a�i o tr Pace Project No./ Lab I.D. � F to DATE TIME DATE TIME U) # _ _ = Z !!!�` ILL o Sludge Pellets PF 0 0 8 E OT G 8 �� NIA 1 x KtxX x x Sludge Pellets PF O O S OT G 7 I :3 �M wn 1 x x 'XII Sludge Pellets PF o D i?G oT G 7 Q /yf : SFo WAl 1 I Sludge Pellets PF OT G I wA 1 x„ x x Collection Temperature OT G 7 $ rF �lE 8- i. := -1 It c,� x •. ,, tv �,,.,.... ,....- ,..tt...•.o -' �r.:r-.'�,._�«,�, >�'..:''" .`,.�':.':...,..,•'..�.X a.COMMENSDT10NAl A9R` Tua'Me, e.i &;-.„•�>'s.?.r�,: ',...a�r,:c._. .�-;..• :,. .• .:�.','.a.t...�;.r.F,.>,a=.?Nt...,.... . .;. z•.-3:a".;.� < ;RF..E,a�L2I'Y N.Q..U, IS£� HED:BY:IrG�F, IL° IAT'fnOYN9.•`: r_W;z ' ::r'r-. D�As.::f<;Eg.. •� S3`.,.�SnTa;iKMetEc.„r: 'Y�.'t rµ a - : a ?CC.eE.,P.„T r�xNe�;^.3L.,°.i,:✓ _,. -� • • � :::D:+Aa-,T-�E'F;,- b=;_ ,/ µ•;TIME'I: •....;N'.•- -�+'� SAMPLE CONDITIONS aa',+�':3 u�bon�a. PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. r S !/(. �'00 it,• "/ Class "A" treatment of sludge. Please Calculate MPN on a dry •'F' -_ $ `I. ' t� weight basis. Analyze %TS within 7 days of collection. _ V D Samples packed in ice as collected; delivered in ice.'`;T Dryer Facility Control Room: 336.397-7663- SAMtf?lER=NAl1A AND SIGNATURE -::ac, t : ;� 6 Z. m c .. -PRINT Name of SAMPLER: , L , H E!-�n(0 aN i E D . o } SIGNATURE of SAMPLER:, �/�� DATE Signed ;F.`��`�� ��" o �'L) .'`Et... •rmn{• -Important Note: 9y signing this tone you are accepting Pace's NET 30 day payment terns and agreeing to late charges of 1.5% per month for any Invoices not paid within 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 aceAnalytical www.p8cerabS,C0M, ANALYTICAL RESULTS Project: Sludge Fecals- Class A Pellets Pace Project No.: 92211951 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF140805A Lab ID: 92211951001 Collected: 08/05/14 07:40 Received: 08/05/14 11:51 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.7 % 0.10 0.10 1 08/07/14 15:08 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 08/05/14 13:07 1g Sample: Sludge Pellets PF140805B Lab ID: 92211951002 Collected: 08/05/14 07:41 Received: 08/05/14 11:51 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL. DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.7 % 0.10 0.10 1 08/07/14 15:08 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 08/05/14 13:07 1g Sample: Sludge Pellets PF140805C Lab ID: 92211951,003 Collected: 08/05/14 07:43 Received: 08/05/14 11:51 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.7 % 0.10 0.10 1 08/07/14 15:09 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 08/05/14 13:07 1g Sample: Sludge Pellets PF140805D Lab ID: 92211951004 Collected: 08/05/14 07:44 Received: 08/05/14 11:51 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.9 % 0.10 0.10 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 Date: 08/07/2014 04:03 PM DF Prepared Analyzed CAS No. Qual 1 08/07/14 15:09 1 08/05/14 13:07 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. a 1g Page 5 of 9 ��aceAnalyfical- vWpacelabs.&n CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. iction A Section B Section C Page: of quired Client Information: Required Project Information: Invoice Information: .mpany: City of Winston-Salem Report TO: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor dress: 2799 Griffith Road Copy To: Company Name; City of Winston-Salem VA GEN W Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F_ NPDES F_- GROUND WATER F. DRINKING WATER f- LIST (- RCRA R OTHER Distrib. - Resid. Solids ?ail To: dianeh(cDcityofws.org Purchase Order No.: see Carol Bell - credit Gard Pace Quote [Reference: ione: 336-397-7624 Fax: 336-774-8862 Project Name: Sludge Fecals (Class "A" Pellets) IPace Project,a Si a Lodafiott EN Manager. NC -_ 1, M iquested Due Date/TAT. Std Turnaround Project Number IPace Profile I - - - - - - - - - - - - lk(p� Mr Valid Matrix Codes Section D . 'I I ism Required Client Information MATRIXCOD COLLECTED Pre servatives N NJ DRINION WATER DIN 0 z WATER WT 11 0 2 T U.1 WASTEWATER Ww PRODUCT P 113 < COMPOSITE START cc I-_ 0 �9 CN SOIUSOUD SL OIL OL (9 0 U)a) i N 0) 0 SAMPLE ID WIPE WIP AR Lu A-, z CL 6 AJR (A-Z. 0-9 OTHER OT w 0 w < g " a) "F% 2 Lo Sample I Ds MUST BE UNIQUE TISSUE TS 0 0. w —0 A —0 0 ik C) w t- U.1 z 0 0 to :3 < (L 2 LL 0 CL C 1(d(d C0 z G 0 - , R 0Q) � E at Fw-< U) DATE TIME DATE TIME < U) U Z) z: 1 zo 1z 2E u- � Pace Project No./ Lab I.D. Sludge Pellets PF1+0L?05 A OT G 7.y0,e, N. 1 X X X ;Q Sludge Pellets PF1+6 805' a OT G 71 qlaNfA I A X X Sludge Pellets PFJ/fo? 5 5'11, OT G 15 7 /A I Sludge Pellets PF VWS ()5- D OT G Ll� Llq NfA 1 X Collection Temperature OT G I.,q �?A3q6 I "p- L "T 'Qbg A AT SAMPLE CONDITIONS :ADDITIONAL COMMEtT.SI; IRE'hoq! LEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. C,/-% W-5 Ace W-!�- 0 11 0 bllf�;' lass "A" treatment of sludge. Please calculate MPN on a dry s v eight basis. Analyze %TS within 7 days of collection. amples packed in ice as collected; delivered in ice. ryer Facility Control Room: 336-397-7663 0— Z PRINT Name of SAMPLER: 0 r ixe— U,45?-WLi 1 o. E 1. . i2 0 I Of 0 0 -6) 0 L) E co SIGNATURE of SAMPLER: ,qll, DATE 'Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 aceAnalj6dal in www•pecdabs.com, ANALYTICAL RESULTS Project: Sludge Fecals Class "A" Pellet Pace Project No.: 92212932 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF 140812E Lab ID: 92212932001 Collected: 08/12/14 07:32 Received: 08/12/1411:43 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.9 % 0A 0 0.10 1 08/14/14 19:50 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 08/12/14 14:20 1g Sample: Sludge Pellets PF 140812F Lab ID: 92212932002 Collected: 08/12/14 07:34 Received: 08/12/1411:43 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.8 % 0.10 0.10 1 08/14/14 19:50 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 08/12/14 14:20 1g Sample: Sludge Pellets PF 140812G Lab ID: 92212932003 Collected: 08/12/14 07:35 Received: 08/12/14 11:43 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 i Percent Moisture 5.8 % 0.10 0.10 1 08/14/14 19:51 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 08/12/14 14:20 1g Date: 08/15/2014 01:31 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 Ana,Wical- 1�;alce ._pacefabs.:o I CHAIN -OF -CUSTODY i Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem Report TO: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem y R 3 Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F NPIDES F GROUNDWATER r7 DRINKING WATER WATER F LIST F RCRA W OTHER Distnb. - Resid. solids Email To: dianeh(cilcity6fws.ora Purchase Order No.: see Carol B611 credit card Pace Quote Reference: Phone: 336-397-7624 F— 33 I act Name: Sludge Fecals (Class "N' Pellets) ct Pace ProleSi4e Location manager. Requested Due DatefTAT. Std Turnaround 113roject Number. Pace Profile -,Requested _0 Section D Valid Matrix Codes e. za I Required client Information MATRIXCODE 2 2 COLLECTED Preservatives NJ N DRINMN WATER DW WATER WT 0 C-) 11 L) z 0 LU WASTEWATER WW M COMPOSITE START COM LU PRODUCT P SOILISOLIO SL 04 -4 C OIL OL WIPE WP SAMPLE ID A1R AR w (9 8 — 0 < o) of w z 0) (D 6 0 (A-Z, 0-9 OTHFR Or Sample IDS MUST BE UNIQUE TISSUE TS 0 0 f) w O_ w t- Z 0 U) C'4 X w F_ w 0 0 V) -15 0 0) IT, :3 _0 w _J CL 0 U) 0 1121 Fo 0 U) F_ < 2 < U) DATE TIME DATE TIME 0 4t z a: 05 z co z a) 2 U 65 a) u_ Pace Project N Lab LD. Sludge Pellets PF1qD1I/;L,6 OT G NIA I X X1 Sludge Pellets PF 1410 VA OT G WA X [NA X X Sludge Pellets PF NO 19 OT G A Sludge Pellets PF OT G - NA N/A I X X X Collection Temperature OT G 73161A WN A ".41 SAMPLE CONDITIONS PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. Class "A" treatment of sludge. Please calculate MPN on a dry 'i weight basis. Analyze %TS Within 7 days of collection. V Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 10 -a z ci Z N..-.ofSAMPLER: PRINT rucc & jzz: DATE Signed SIGNATURE &SAMPLER: &ILCI f ii �//Z/ E Q 0 , D � L) *Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08,12-Oct-2007 or aceAnalytica! wwwpecefabs.com: ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Fecals Class "A" Pace Project No.: 92215553 Sample: Sludge Pellets PF140902A Lab ID: 92215553001 Collected: 09/02/14 07:45 Received: 09/02/14 11:03 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.6 % 0.10 0.10 1 09/08/14 14:22 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 09/02/14 13:43 1g Sample: Sludge Pellets PF140902B Lab ID: 92215553002 Collected: 09/02/14 07:45 Received: 09/02/14 11:03 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.3 % 0.10 0.10 1 09/08/14 14:22 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 09/02/14 13:43 1g Sample: Sludge Pellets PF140902C Lab ID: 92215553003 Collected: 09/02/14 07:49 Received: 09/02/14 11:03 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.5 % 0.10 0.10 1 09/08/14 1.4:23 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 09/02/14 13:43 1g Sample: Sludge Pellets PF140902D Lab ID: 92215553004 Collected: 09/02/14 07:50 Received: 09/02M4 11:03 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.4 % 0.10 0.10 1 -09/08/14 14:23 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 09/02/14 13:43 lg Date: 09/08/2014 03:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 �ace Analytical - .Pacelabs,mn CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. .lion A Section B Section C page:of uIred Client Information: Required Project Information: Invoice Information: ip - any: City of Winston-Salem Report TO: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor ress: 2799 Griffith Road Copy To: CompanyName: City of Winston-Salem N Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC r— NPIDES F_ GROUNDWATER r—... DRINKING WATER Distrib. - R-Id. Solids F_ LIST F_- RCRA OTHER 0 To: dianeh(cDcitvofws.org Purchase Order No.: see Carol Bell - credit card Pace Quote Reference: ne: 336-397-7624 Fax 336-774-8862 I Project Name: Sludge FeGals (Class "N' Pellets) I Pace Project Manager. NC luested Due Date/TAT: Sid Turnaround Project Number. Pace Profile Section D Valid Matrix Codes Required Client Information MATRIx CODE 2 COLLECTED Preservatives N N LU DRWKING WATER DW WT WATER 0 WASTEWATER WW P to COMPOSITE START COM CNQ� C) U.) z PRODUCT S OIUSOUD SL < w I I C\1 OIL OL 0 0 to SAMPLE ID WIPE WP 1_ W w z AR AR (A-z* 0-9 1,-) OTHER Or UU 0 w < 0- z EL Lo Sample IDS MUST BE UNIQUE TISSUE TS o C) rL 2 U.) a) 0 do X w 0 LL W 1,51 0rn cc :5 < < DATE TIME DATE TIME to 0 T 10 z to z 2 S LL Pace Project No./ Lab I.D. Sludge Pellets PFII+Dq 02A OT G N/A 1 x X X X X Sludge Pellets PF 1,1f 0 1 a 2,8 OT G N. 1 X Sludge Pellets PF1-'fO9 6 ZC OT G 9-2-A/ 7.- V 9,J NIA 1 X X X X Sludge Pellets PFI+oq 62- D OT G -1-2 _Jy .11 NIA 1 X X Collection Temperature OT G o/._2_1q 7Cr.;.,,I p" R SAMPLE CONDITIONS 0, R .EASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. ig -r- Ict g!107c,�z ass "A" treatment of sludge. Please calculate MPN on a dry Tight basis. Analyze %TS within 7 days of collection. imples packed in ice as collected; delivered in ice. yer Facility Control Room: 33r,397-7663 02 m z PRINT Name of SAMPLER; V rfVt m m E 12 2 w 0 0 Z; .0 L) E SIGNATURE of SAMPLER: IDAI.Slgne)d M'Do *Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5%per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08.12-Oct-2007 Pace Analytical Services, Inc. 6701 Conference Drive aceAna1Xkal ® Raleigh, NC 27607 www.pe0olabs.com: (919)834-4984 ANALYTICAL RESULTS Project: Sludge Fecals Class A Pellets Pace Project No.: 92216507 Sample: Sludge Pellets PF140909E Lab ID: 92216507001 Collected: 09/09/14 07:53 Received: 09/09/14 11:32 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.5 % 0.10 0.10 1 09/11/14 14:56 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 09/09/14 13:02 1g Sample: Sludge Pellets PF140909F Lab ID: 92216507002 Collected: 09/09/14 07:54 Received: 09/09/14 11:32 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.4 % 0.10 0.10 1 09/11/14 14:56 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 09/09/14 13:02 1g Sample: Sludge Pellets PF140909G Lab ID: 92216507003 Collected: 09/09/14 07:55 Received: 09/09/14 11:32 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.4 % 0.10 0.10 1 09/11/14 14:57 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 09/09/14 13:02 1g f REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/11/2014 03:52 PM without.the written consent of Pace Analytical Services, Inc:. Page 5 of 9 aceAnalXical --pacetabs.com CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. lotion A Section B Section C Page: of quired Client Information: Required Project Information: Invoice Information: mpany: City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor (dressGriffithoad 2799 Griffit Copy To: Company Name: City Of Winston-Salem REGULATORY�AGENCY=':: • Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC r NPDES r- GROUNDWATER r DRINKING WATER r UST r RCRA NY OTHER Distrib. -Resid. Solids nail To: dianeh(a)cityofws.org Purchase Order No.: see Carol Bell -credit card Pace Quote Reference: cone: 336-397-7624 Fax 336-774 8862 Pro'eclName: J Sludge Fepls (Class "A" Pellets) Pace Project :Site:L"ooatwn Manager. NC rquested Due DatertAT: Std Turnaround Pro ect Number: J Pace Profile rk. 'jReguesteIArialysis'.,Filtereilr(Y!N) Section D Valid Matrix Codes s a? Required Client Information MATRIX CODE P 2 COLLECTED Preservatives }* N N COMPOSITE START COMP¢S4 EN GLT aA iy LLI//)] / ' DRINKING WATER DW WATERWT WASTEWATER WW PRODUCT P = O U O ¢ z O U Lid SOILISOLID SL OIL OL � O' 1 O V) N SAMPLE ID WIPE WP AIR AR 11 0 < W _� z a o o (A-Z, 0-9 / ,) OTHER OT p w a ¢ re 'r,=H V to N L Sample IDS MUST BE UNIQUE Tissue TS O a w F- i) ., N x OU m U S U m ;R` U w 121 v w ¢ a a a Q u_ o ) X O z U p m co _ � ar L Q N IL) rA n F- 2 W DATE TIME DATE TIME Z I Z Z Z O LL. 0 pace Project Nod Lab I.D. 1 ke1R Sludge Pellets PF(+D9 09 E oT G 9 r 7:53 A. NIA 1 x x x Sludge Pellets PFI+01? oT G 9 4 I'j l fir n� NIA 1 x a x x 3f Sludge Pellets PF1409 G oT G 4� y �tss NIA 1 x kzg x x x x 42 4, Sludge Pellets PF OT G N/A 1 x -xs <r5r; Collection Temperature oT G '` K �Rs�t W,T t ' "r' '+_` � "x' ' _1raIr„=.=,- _ RELINQUISHED'BYrIfAFF.IL:lA710N. r-• - Ex' - CCEFTEDmB)f-/'AFFILIATIONF�'�,,_,� ,,DAT''r-�TIME`ssa+ �n SAMPLE _ � „ ,<„ z?.. „ .., �,.h . ., . _., -..� -.... -.. ., .> A ,.<... ,- : a,, ,,,,,,,,, , ; � b. ;r�DQTE�`;s''.v�TIM, T9S.,. �� ?'li; fi?"• - �, . ar!t:.,,.r.'.TL-' _ - �t- LEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. f t q, ?' -7 YA G D -0 '✓t i D :lass "A" treatment of sludge. Please calculate MPN on a dry ✓ `� ��•4(.� J K ,eight basis. Analyze %TS within 7 days of collection. amples packed in ice as collected; delivered in ice. n 14 V_ it )ryer Facility Control Room: 336-397-7663 SAMP;LER>NAME=AND'SIGNATURE t ;? ` o m ? PRINT Name of SAMPLER: I� rl ✓,S I-,j a ' m m E ^m $ m `—' o 0 o E - SIGNATURE SAMPLER: DATE Signed 4 i ~ 1 U of (MMIDD": ED -Important Note: By signing this form you are accepting Pace's NET 30 day payment terns and agreeing to tale charges of 1.5% per month for any invoices not paid vrithin 30 days. F-ALL-Q-020fev.08, 12-Oct-2007 aceAnalXical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Fecals Class A Pellets Pace Project No:: 92220195 Sample: Sludge Pellets PF141001A Lab ID: 92220195001 Collected: 10/07/14 07:35 Received: 10/07/14 12:20 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua] Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.3 % 0.10 0.10 1 10/10/14 13:48 92210E Fecal Collform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 10/07/14 12:18 1g Sample: Sludge Pellets PF141001 B Lab ID: 92220196002 Collected: 10/07/14 07:37 Received: 10/07/14 12:20 Matrix: Solid Results reported on a "dry, weight' basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua] Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 % 0.10 0.10 1 10/10/14 13:48 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 10/07/14 12:18 1g Sample: Sludge Pellets PF141001C Lab ID: 92220195003 Collected: 10/07/14 07:99 Received: 10/07/14 12:20 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua] Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 % 0.10 0.10 1 10/10/14 13:49 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 10/07/14 12:18 1g Sample: Sludge. Pellets P0141001D Lab ID: 92220196004 Collected: 10/07/14 07:40 Received: 10/07/14 12:20 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 % 0.10 0.10 1 10/10/14 13:49 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 10/07/14 12:18 1g Date: 10/14/2014 08:52 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 0 0 .!ZAn*IkW- -- Section A SKS" a CHAIN -OF -CUSTODY ! Analytical Request Document MW tmarwr-custo* is a LEGAL DOCUMEW. AI ndevaM news meat oe comptetea 80=0uy. mod= t UST 1 KQM -'.WIMtNose.er.�uMf=yaOa &"QPIVVP40&'& Eraomypc�e+ente�n.na.gKxngtoutaenmseadt5uvermartl+r«amk&0Mnoipde.ehmsoaya FALLQ-0ALL12Oct-Got ace Analytical www.pecolabs.com: ANALYTICAL RESULTS Project: Sludge Fecals Class "A" Pace Project No.: 92221407 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF141014E Lab ID: 92221407001 Collected: 10/14/14 07:34 Received: 10/14/14 11:27 Matrix: Solid Results reported on a '-dry-weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 12.1 % 0.10 0.10 1 10/17/14 13:33 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 10/14/14 12:26 1g Sample: Sludge Pellets PF141014F Lab ID: 92221407002 Collected: 10/14/14 07:36 Received: 10/14/14 11:27 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 12.2 % 0.10 0.10 1 10/17/14 13:33 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.1 MPN/g 0.018 0.018 1 10/14/14 12:26 1g Sample! Sludge Pellets PF141014G Lab ID: 92221407003 Collected: 10/14/14 07:39 Received: 10/14/14 11:27 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 12.1 % 0.10 0.10 1 10/17/14 13:33 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 10/14/14 12:26 1g Date: 10/17/2014 04:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 aceAnalytical" w—pacarabs cdm CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C page: of Required Client Information: Required Project Information: Invoice Information: _ Company-. City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor 2799 Griffith Road Co To: Address: PY Company Name: CI of Winston-Salem City -ENGy "_ RE,GU"A YINI-AG K"'r :ems!. , '"''- Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F . NPDES !- GROUND WATER (- DRINKING WATER Email To: dianehilcityofws.org Purchase order No.: see Carol Bell - credit card (c Pace Quote i- UST r RCRA �• OTHER Distdb. - Resid. Solids Phone: Fax: Project Name: 336-397-7624 336-774-8862 I Sludge Fecals (Class "A" Pellets) Reference- Pace Project''°`''"' S e;L`ocatltin Std Turnaround ProjectPace Requested Due Date/TAT: Number. Manager. Profile NC m ^GSTA?•7.�E RegitestedAni+lyslsitered(Y1N)t: F; Section D Valid Matrix Codes Z. - COLLECTED >' Preservatives N INRequired Client Information MATRIX CODE 3 O a DRINKING WATER 'DW m U II Z �; ;.,� 0 W WATER WT o WASTEWATER WIN COMPOSITECOMpp&i� W PRODUCT P = SOILISOLID SL Q w ,;e y N •€ ; } OIL. 0 SAMPLE ID AIR AR i? a W d"s a CD (A-7- 0-9 / :) OTHER OT 0 w Q ;tlJ LO iL.i , Sample IDs MUST BE UNIQUE TISSUE Ts O U IL w t- O m c `T U co # a a O p Oz� D`t rC; (n w w a a Q o c "� z v m to O Pace Project No./ Lab I.D. F- rn DATE TIME DATE TIME N Z I I !'!�; u_ o Sludge Pellets PF1+l D J/f oT G D / /# !4 N/A 1 X ,,Y X x X X X `; r2F`rp Slud a Pellets PFj I D 14F OT G a / .4 N/A 1 Sludge Pellets PF O I G or G p N/A 1 X X Sludge Pellets PF oT G NIA 1 x .'Fxi.' x x 5 Collection Temperature or G o �1� /� . 5� - _ n _ - ,..".a. ..,.. .,. ., r:i_". t, .v.';�..>�. _. .. ...". Wit, •-..,rxt,,.st�.a..,�,.�':_...,-y5�" ,,.~r- " € Y'F F ILIATIOt1g•s N A F, CE?TED�BY:9'AFFILIATION^"'i--"S=DATE?TIME,?= SAMPLECONDITIONS a ,Y. ADDITIONALCOh1MENT3 :, }> RELINgIjISF1ED,B .,,<'. Ica,.... .<, '�.. -orr.• „ ,,,,,, ,,,,,,,,, t.., ._ ,:`:. ',a,=` ;��*. <;; - PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. Class "A" treatment of sludge. Please Calculate MPN on a dry _47 0 ID "/ y �� weight basis. Analyze %TS within 7 days of collection! Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 SAMPLER NAMEAND SIGNATURE- - ;� o o ? m = PRINT Name of SAMPLER: L!-I Ef�nl AOnI a F m 0 `—� o d -a o m a SIGNATUREofSAMPLER: ,(1 /i �7,j„_ -/�, DATE Signed ,/ (MMIDDIYY): /6 1* 1 ' � U� m - N 'Important Note: By signing this form you are accepting Pace's NET 30 day payment terns and agreeing to late charges of 1.5%per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 aceAnalytical www.pacefebs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Fecals Class "A" Pace Project No.: 92223946 Sample: Sludge Pellets PF141104A Lab ID: 92223946001 Collected: 11/04/14 07:53 Received: 11/04/14 12:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 % 0.10 0.10 1 11/06/14 13:19 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal,Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 11/04/14 13:10 1g Sample: Sludge Pellets PF141104B Lab ID: 92223946002 Collected: 11/04/1407:54 Received: 11/04/14 12:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 % 0.10 0.10 1 11/06/14 13:19 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 11/04/14 13:10 1g Sample: Sludge Pellets OF141104C Lab ID: 92223046003 Collected: 11/04/14 07:56 Received: 11/04/14 12:10 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.4 % 0.10 0.10 1 11/06/14 13:19 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 11/04/14 13:10 1g Sample: Sludge Pellets PF141104D Lab ID: 92223946004 Collected: 11/04/14 07:58 Received: 11/04/14 12:10 Matrix: Solid, Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua] Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.6 % 0.10 0.10 1 11/06/14 13:19 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 1 11/04/14 13:10 1g REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11 /07/2014 11:41 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 aceAnalytical" ,pawfabs c" CHAIN -OF -CUSTODY/ Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention:. Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem Winston-Salem, NC 27103 Address: '2799 Griffith Rd., Winston-Salem, NC 1- NPIDES f- LIST I^ GROUNDWATER r- DRINKING WATER r_. RCRA 5_0 OTHER Distrib. - Resid. Solids Email To: dianeh(cDcitvofws.org Purchase Order No.: see Carol Bell - credit card Pam Quote Phone: 336-397 Fax 336-774-8862 Project Name: Sludge FeGals (Class "K Pellets) Reference: Pace Project P jSitelLocatioo .624 Manager. P NC Requested Due Date/ Sid Turnaround Project Number. Pace Profile Section 0 Valid Matrix Codes Required Client Information MATRIX CODE COLLECTED Preservatives N N ............... k LL, DR1NIONGWATER 6w WATER VVT 0 H z 0 WASTEWATER VVW 0 0 .M COMPOSITE START %M4ff1_> z PRODUCT P SOILISOLID SL 'Ri A NOIL OL W SAMPLE ID nip wP R AR (A Zr 0-9 OTHER OT w 0 w 0 U) 'Lu z CL z 0 Sample IDS MUST BE UNIQUE TISSUE TS 0 IL z Go ut 0 0 4) W 0 c,i M �W () 2 (,3 I LIL CL 0 R , r crei U) 0 'It z X 20 z 2 (D (D (D Of . . o.1 Lab I.D. Pace Project N' DATE TIME DATE TIME (<O I I I LL LL I I I Sludge Pellets PF1,41 I o *A OT G 1111411* 17.1r.UA N/A X X X X Sludge Pellets PFIA+ I OT G IJQI* IT -7!,Y*A4( 4( X X X X X 2�_ Sludge Pellets PF 1411 DV_ OT G -4h# 7:51(,&, NIA I X Sludge Pellets PF JA+ 110 40 OT G I I[ If A P4, Ta4A Nffi 1 X X X X Collection Temperature OT G 1 14 — — — — — — E & U SAMPLE CONDITIONS PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. lilYln- T" Class "A" treatment of sludge. Please calculate MPN on a dry S y 1, 114] Iq 1).1)1r weight basis. Analyze %TS within 7 days of collection. Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 1 31 SAMPLER AM �A PRINT Name of SAMPLER:• ib 14CIpWID 6AI •E E 0 Q 9 , 0- 0: 0 � 0 0 E Cn SIGNATURE of SAMPLER: OATESigned (MM.. *Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late chargesof1_5% per month for any invoices not paid within 30 days. I . F-ALL-Q-020rev.08. 12-Oct-2007 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Sludge Fecals Class "A" Pace Project No.: 92224987 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF141111E Lab ID: 92224987001 Collected: 11/11/14 07:30 Received: 11/11/14 11:18 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.1 % 0.10 0.10 1 11/14/14 13:31 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 603 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 11/11/14 12:06 1g Sample: Sludge Pellets PF141111F Lab ID: 92224987002 Collected: 11/11/14 07:32 Received: 11/11/14 11:18 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No; Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10 % 0.10 0.10 1 11/14/14 13:31 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 11/11/14 12:06 1g Sample: Sludge Pellets PF141111G Lab ID: 92224987003 Collected: 11/11/14 07:35 Received: 11/11/14 11:18 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.8 % 0.10 0.10 1 11/14/14 12:55 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.0 MPN/g 0.018 0.018 1 11/11/14 12:06 1g REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /14/2014 02:52 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 10 ��acmnaljdical- CHAIN-OF-CUSTODY I Anailytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: 2799 Griffith Road Copy To., Company Name: City of Winston-Salem Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC F_ NPIDES F GROUNDWATER r- DRINKING WATER f— LIST T_ RCRA W OTHER Distdb. - ResId. Solids Email To: dianeh(@cityofWs.orq Purchase Orcleir No.: see Carol Bell Credit card Pace Quote Reference: Phone: 336-397-7624 Fax 336-774-8862 Project Name: Sludge-Fecals (Clas�qV Pellets) Pace Project n Manager. NC Requested Due DaterrAT. Sid Turnaround Project Number. Pace Profile V. 7 T' y1si NY Section D Valid Matrix Codes I I Required Client Information MATRIX CODE COLLECTED Preservatives NJ NJ DRINMG WATER DW 0 0 Z WATER WT 11 0 2 Lu WASTE WATER WIN PRODUCT P 03 COMPOSITE START co EN GRAa LU SOIL/SOUD SL 11L OL (9 0 rJ) c'J N C3) SAMPLE ID WIPE WP w ZCL AIR AR (A-Z, 0-9 1.-) OTHER OT W 0 W (L ur) Sample IDS MUST BE UNIQUE TISSUE 7S 0 ( ) (L r w < l'- Z (o i-- 0 C'J 0 L< W 0 a) 0 (L am 0 -0 2 (Z) 0 C8 20 �5 < n DATE TIME DATE TIME < U) * 7) M Z 7: W Z Z :R 0 4, LL Pace Project NO./ Lab I.D. Sludge Pellets PFI* I I I I OT 7.13oA14 1A N/A 1 X x Sludge Pellets PFI+ I I I I F' OT /11/1�1* 74 0 /A NIA 1 x 'g t'A X X Sludge Pellets PFJ� OT G. A ALk 7, -35- AK N/A N/A X X Sludge Pellets PF OT G NIA N/A 1 x x all" Collection Temperature OT, G , '11h, 114 -7 '37/4. SAMPLE CONDITIONS 71 X PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. 4 it) 72 2Ykm C tff Class "N'tibatmerit of sludge. Please calculate MPN o n a dry weight basis. Analyze %TS within 7 days of collection. Samples packed in ice as collected; delivered in ice. V Dryer Facility Control Room: 336-397-7663 <SAMPLER NAME AN'D SIGNATURE-ai ai Z Z PRINT Name of SAMPLER: D. H ERN D 6AI E .2 SIGNATURE of SAMPLER: DATE Signed d 11111114 *Important Note: By signing this form you are accepting Paces NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-0-020rev.08, 12-Oct-2007 aceAnalXical www.pecerebs com, ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Sludge Fecals Class "A" Pace Project No.: 92227615 Sample: Sludge pellets PF141202A Lab ID: 92227615001 Collected: 12/02/14 07:31 Received: 12/02/14 10:12 Matrix: Solid Results reported on a "dry -weight" basis Parameters Percent Moisture Percent Moisture 92210E Fecal Coliform, MPN RAL Fecal Coliforms, MPN Report Results Units Limit MDL Analytical Method: ASTM D2974-87 8.2 % 0.1.0 0.10 Analytical Method: SM9221C E (MPN) 503 2.0 MPN/g 0.018 0.018 DF Prepared Analyzed CAS No. Qual 1 12/06/14 10:40 1 12/02/14 13:09 1 g Sample: Sludge pellets PF141202B Lab ID: 92227615002 Collected: 12/02/14 07:32 Received: 12/02/14 10:12 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qua[ Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 8.1 % 0.10 0.10 1 12/05/14 10:40 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms; MPN 2.0 MPN/g 0.018 0.018 1 12/02/14 13:09 1g Sample: Sludge pellets PF141202C Lab ID: 92227615003 Collected: 12/02/14 07:34 Received: 12/02/14 1 0: 12 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.6 % 0.10 0.10 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 0.018 DF Prepared Analyzed CAS No. Qua] 1 12/05/14 10:40 1 12/02/14 13:09 1 1g Sample: Sludge pellets PF141202D Lab ID: 92227615004 Collected: 12/02/14 07:35 Received: 12/02/14 10:12 Matrix: Solid Results reported on a "dry -weight" basis Parameters Percent Moisture Percent Moisture 92210E Fecal Coliform, MPN RA Fecal Coliforms, MPN Date: 12/05/2014 02:28 PM Report Results Units Limit MDL DF Analytical Method: ASTM D2974-87 7.9 % 0.10 0.10 1 L Analytical Method: SM9221C E (MPN) 503 2.0 MPN/g 0.018 0.018 1 Prepared Analyzed CAS No. Qual REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, Inc.. 12/05/14 10:40 12/02/14 13:09 1g Page 5 of 9 1�52ceAnalXical CHAIN-OF-CUSTODY I Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Company: City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Attention: Carol Bell - Lab Supervisor Address: Copy To: Company Name: City of Winston-Salem 2799 Griffith Road REGULATORY, � Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC r- NPIDES i- GROUNDWATER DRINKING WATER Distrib. - Resid. Solids F_ LIST F RCRA rv- OTHER Email To: dianeh(a)citvofws.org Purchase Order No.: see Carol Bell - credit card Pace Quote Reference: Phone: 336-397-7624 Fax: 336-774-8862 Project Name: Sludge Fecals (Class "N' Pellets) Pace Proje ct te,Lc(8ition ManagesNC TE' Requested Due Date/TAT: Stcl Turnaround Project Number. Pace Profile :'Requested Section D Valid Matrix Codes E., -; 2 COLLECTED Preservatives N N Required Client Information MATRIX CODE 0 — — — LU ORINIQNGWATER DW WATER WT . L) 11 zuax 0 WASTEWATER WW W 0 00 COMPOSITE START COM 0 III RODUCT P ol D SL SUSOU OILOL SAMPLE ID WIPE WP NR w < w I _1 0 U) Lu z -* a) Z 0 CD V- Lo a) qw% (A -9/,-) OT -7_ 0 OTHER 0 w CIL C) Sample IDs MUST BE UNIQUE TISSUE Ts 0 w 0 >< LU w 0 6 to :f: Co Co c ca U) < U 0 z 5 0 ca 8 :5 a) 0 a) 1.- Pace Project No./ Lab I.D. < w DATE TIME DATE TIME U<) M: z z 2 Sludge Pellets PFI+I,.)-O,;LA OT G N/A 1 X yY X X Sludge Pellets PFJA�la,0.-13 OT G laW,4 7:_U.4A NIA X X X Sludge Pellets PF 1 14 zLo aiL OT I G 7:q 11AA( NIA — — — — -- Sludge Pellets PH OT G 7.'95-hm NIA 1 _X Collection Temperature OT G J7 +Al 5'7. ;Z, 11 IN 10 E,Mk, - U, M, ITI c �Rl D I SH"E" B'Y'� 16ATIO�7 "777, 77, ""77 Til SAMPLE CONDITIONS "��,.,PMMENT PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. t) 4 e -A &W*J 1,g�ll g.66,44( Class "A" treatment of sludge. Please calculate MPN on a dry 6( Lb kZ- weight basis. Analyze %TS Within 7 days of collection. Samples packed in ice as collected; delivered in ice. Dryer Facility Control Room: 336-397-7663 777�77,7 ... 77777-7777=71 S' T U) - PRINT Name of SAMPLER: J). L. HCp 14DOlil E 2.2 .2 E DATE Signed SIGNATURE of SAMPLER: (M ) 0 0 -important Note: By signing this form you are accepting Pace's NET30 day payment terms and agreeing to late charges of 1.51% per month for any invoices not paid within 30days- F-ALL-Q-020rev.08, 12-Oct-2007 (�acieAnalj&al _pacefabs:com. ANALYTICAL RESULTS Project: Sludge Fecals Class "A" Pace Project No.: 92228676 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Sludge Pellets PF141209E Lab ID: 92228676001 Collected: 12/09/14 07:39 Received: 12/09/14 10:59 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.7 % 0.10 0.10 1 12/12/14 14:15 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 13.8 MPN/g 0.018 0.018 1 12/09/14 11:55 Sample: Sludge Pellets PF141209F Lab ID: 92228676002 Collected: 12/09/14 07:41 Received: 12/09/14 10:59 Matrix: Solid Results reported on a "dry -weight" basis Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.8 % 0.10 0.10 1 12/12/14 14:15 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 13.8 MPN/g 0.018 0.018 1 12/09/14 11:55 Sample: Sludge Pellets PF141209G Lab ID: 92228676003 Collected: 12/09/14 07:44 Received: 12/09/14 10:59 Matrix: Solid Results reported on a "dry -weight' basis Report-- - - --- - -- — - Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.7 % 0.10 0.10 1 12/12/14 14:15 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 13.8 MPN/g 0.018 0.018 1 12/09/14 11:55 Date: 12/12/2014 04:14 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 9 �;ZeAnalytical` wlxvpac�JaDs.cnm t i CHAIN -OF -CUSTODY / Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Page: of Required Client Information: Required Project Information: Invoice Information: Attention: Carol Bell - Lab Supervisor Company: City of Winston-Salem Report To: Bruce Casey - Dryer Facility Supervisor Address: 2799 Griffith Road Copy To: Company Name: City of Winston-Salem Winston-Salem, NC 27103 Address: 2799 Griffith Rd., Winston-Salem, NC i— NPDES F GROUND WATER F DRINKING WATER F— UST F—: RCRA 1✓ OTHER Distdb. - Resid. Solids Email To: dianeh(C�CIfVOfWS.Orp Purchase Order No.: see Carol Bell - credit Card { Pace Quote Reference: Phone: 336-397-7624 Fax 336-774-8862 Pro ecI Name: i Sludge Fecals (Class "A" Pellets) Pace Project Site L'bcaii Manager. `' %I' '' 1a NC Requested Due DaterAT: Std Turnaround qSTATE: Project Number. Pace Profile #: _,Regiiested'AnalysIS' :Filtered'(Y/N)' Section D Valid Matrix Codes -_ Required Client Information MATRIX CODE COLLECTED Preservatives N N DRINIaNG WATER DIN00 z O �%s WATER WT WASTEWATER WW PRODUCT P Lr OIL OL17 = n O COMPOSITE START ('AM F1J U W ,%%, Y`Il'-^ ;sry^. w Z _ ///��� ZVI q SAMPLE ID WIPE WP AR W '021 o 0 v/J1�' (A-Z, 0.9 / . OTHER OT AIR 0 W CL 0_ Z H ) 0 t~ ^y i � Lri N L U Sample IDS MUST BE UNIQUE TISSUE Ts O U w ~ • at Ja O O E O 2 c Y �+ ;10 U76 a °-L F C. i O c N Z U 1z1z Om co z L--Qr v h' F- y DATE TIME DATE TIME 4 _ _ = O �4 LT o � Pace Project No./ Lab I.D. Sludge Pellets PF)AHaL a Ll E OT G / 4 1.39.n. N/A 1 x;s .,`2 ; :,;,`: x x Sludge Pellets PF �d 9 F' oT G 4/ 7"t`/R N/A 1 X X X Slud a Pellets PFI I,zo Cr or G 9 / i, `'/,f wA 1 x x x Sludge Pellets PF Or c NIA 1 X X Collection Temperature Or c - - DDTf' l'COMMENTS;'..-''>.".4''=w`''REIINQUISHEO'BY/-AFFICIATION�' :,DATE,:i'; = •7T1ME.`°;`� CSC ,,� BY'CAFF LIATIOfV EP.,TED .,I N DATE:;-,' ��*TIMEu SAMPLE CONDITIONS ,.AC y w PLEASE PULVERIZE SAMPLES PRIOR TO ANALYSIS. ��-'9••OSAM` p� is 4i Gf// 2 I •� y m3 3 (}� Class "A" treatment of sludge. Please calculate MPN on a dry weight basis. Analyze %TS Within 7 days of collection. Samples packed in ice as collected; delivered in ice. - G Dryer Facility Control Room: 336-397-7663 ;SAMPLER:NAME'-ANDSIGNATURE. 9 'n z } d } r `m iD 0 PRINT Name! of SAMPLER: D voa.t( m m 00 o �� E SIGNATUREIofSAMPLER:� DATE Signed ap ,��� (MM/DD/YY): /�- Q / rn 'Impadanl Note: By signing this forth you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1l5% per month for any invoices not paid within 30 days. F-ALL-Q-020rev.08, 12-Oct-2007 City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 6. Dryer Facility Compliance Operational Reports DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 01/01/14 to 01/31/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT um SRT Time Temp % %TS % %TS % Temp MIN Deg F Achievedequired MintuesMinutes [Alt Met 1 = Yes Daily Must Be �35% V732 V968 V970 V1010 1 B Time V1013 0 = No V1014 V877 01 /01 /14 92.29 22.14 72.10 187 61.40 0.17 1 01/02/14 91.67 21.93 71.30 187 59.42 0.17 1 01/03/14 89.01 21.29 67.03 183 73.53 0.34 1 01/04/14 90.75 22.10 68.53 184 68.20 0.29 1 01/05/14 91.33 22.21 67.97 186 69.57 0.20 1 01/06/14 89.75 22.39 68.01 184 74.361 0.29 1 01/07/14 88.05 20.66 62.78 180 116.37 0.58 1 01/08/14 92.96 20.58 64.89 186 113.70 0.20 1 01 /09/14 01/10/14 91.54 21.30 69.83 187 90.78 0.17 1 01/11/14 90.90 21.55 68.05 185 69.89 0.24 1 01/12/14 91.11 21.71 69.24 183 65.121 0.34 1 01/13/14 90.93 21.91 67.95 185 71.19 0.24 1 01/14/14 89.84 21.99 66.94 181 79.39 0.49 1 01/15/14 01/16/14 01/17/14 93.14 22.08 73.11 187 80.38 0.17 1 01/18/14 94.501 22.74 75.67 193 66.241 0.06 1 01/19/14 94.35 22.481 74.12 193 66.76 0.06 1 01/20/14 94.15 22.33 75.53 191 58.02 0.08 1 01/21/14 94.52 23.22 77.25 192 54.28 0.07 1 01/22/14 94.75 23.08 73.75 192 70.57 0.07 1 01/23/14 94.06 22.72 75.28 193 64.60 0.06 1 01/24/14 94.64 23.32 76.46 193 50.54 0.06 1 01/25/14 01/26/14 01/27/14 94.73 22.51 75.58 193 85.681 0.06 1 01 /28114 94.29 22.931 76.76 192 53.41 0.07 1 01/29/14 94.72 22.781 76.47 194 42.76 0.05 1 01/30/14 94.95 22.40 73.88 194 121.67 0.05 1 01 /31 /14 93.96 25.361 85.54 193 41.14 0.06 1 AVERAGE 92.57 22.30 72.08 188 71.88 MAXIMUM 94.95 25.35 85.54 194 121.67 MINIMUM 88.05 20.581 62.78 180 41.14 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 01/07/14 2A 01/07/14 2.4 01/14/14 ND 01/14/14 ND Monthly Monthly Maximum 2.4 Minimum ND ND - Not Detectable DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. W00029804 02101/14 to 02/28/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be Z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 02/01/14 93.16 24.34 70.71 187 94.09 0.17 1 02/02/14 91.08 24.06 69.37 186 82.56 0.20 1 02/03/14 90.92 24.88 72.78 182 77.16 0.41 1 02/04/14 91.01 25.19 71.53 182 95.16 0.41 1 02/05/14 92.48 24.92 72.68 186 94.38 0.20 1 02/06/14 90.81 22.82 66.92 185 72.59 0.24 1 02/07/14 90.93 22.70 64.15 185 95.64 0.24 1 02/08/14 90.49 23.04 65.87 185 96.18 0.24 1 02/09/14 89.66 22.81 66.73 184 70.09 0.29 1 02/10/14 90.15 22.28 67.64 183 63.27 0.34 1 02/11/14 88.09 22.25 64.84 185 85.32 0.24 1 02/12/14 88.67 22.21 63.91 186 56.39 0.20 1 02/13/14 02/14/14 93.35 22.14 68.83 194 73.94 0.05 1 02/15/14 90.75 21.83 68.16 187 71.83 0.17 1 02/16/14 90.06 21.98 69.55 182 60.27 0.41 1 02/17/14 91.87 22.19 69.09 187 62.33 0.17 1 02/18l14 91.14 21.91 68.74 187 60.53 0.17 1 02/19/14 90.44 21.19 65.89 184 65.51 0.29 1 02/20/14 91.92 20.311. 67.67 188 62.34 0.14 1 02/21/14 02/22/14 02/23/14 92.52 22.27 69.28 188 90.48 0.14 1 02/24/14 90.80 22.47 69.501 186 61.60 0.20 1 02/25/14 91.30 21.64 69.591 188 56.28 0.14 1 02/26/14 90.25 21.27 65.63 189 55.05 0.12 1 02/27/14 90.08 21.36 68.48 187 52.50 0.17 1 02/28/14 89.12 21.89 68.78 186 56.96 0.20 1 AVERAGE 90.84 22.56 68.25 186 72.50 MAXIMUM 93.35 25.191 72.781 1941 96.18 MINIMUM 88.09 20.31 63.91 1821 52.50 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 02/04/14 218 02/04/14 ND 02/11/14 5.0 02/11/14 2.2 Monthly Monthly Maximum 218 Minimum ND ND - Non -Detectable DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 03/01 /14 to 03/31 /14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp %TS %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be% Z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 03/01/14 91.95 21.90 69.97 189 62.75 0.12 1 03/02/14 92.10 22.20 68.52 190 69.27 0.10 1 03/03/14 92.39 21.31 71.65 192 57.22 0.07 1 03/04/14 92.71 21.18 70.82 188 44.13 0.14 1 03/05/14 03/06/14 03/07/14 85.63 21.78 62.38 178 131.39 0.84 1 03/08/14 93.57 22.87 75.12 188 55.09 0.14 1 03/09/14 89.78 22.13 63.81 186 69.08 0.20 1 03/10/14 91.95 21.84 67.14 188 61.82 0.14 1 63/11/14 93.41 22.33 71.58 192 51.26 0.07 1 03/12/14 03/13/14 93.58 22.08 73.89 183 138.45 0.34 1 03/14/14 94.45 23.30 73.29 190 33.93 0.10 1 03/15/14 92.68 23.85 68.04 186 291.33 0.201 03/16/14 23.40 03/17/14 90.33 22.811 73.22 188 89.11 0.14 1 03/18/14 91.16 22.621 70.91 188 59.48 0.14 1 03/19/14 91.04 22.59 68.56 187 59.16 0.17 1 03/20/14 93.94 22.41 67.34 187 66.09 0.17 1 03/21/14 90.88 22.53 71.82 188 48.29 0.14 1 03/22/14 92.42 22.92 72.21 190 70.37 0.101 1 03/23/14 90.42 22.87 65.38 187 84.84 0.171 1 03/24/14 93.89 23.08 74.791 190 62.04 0.10 1 03/25/14 03/26/14 03/27/14 93.58 22.49 72.61 191 85.61 0.08 1 03/28/14 91.21 22.53 70.03 189 69.00 0.12 1 03/29/14 91.85 22.72 68.03 188 69.53 10.141 1 03/30/14 93.59 23.421 71.86 190 72.94 0.10 1 03/31/14 1 80.25 22.591 66.52 185 56.93 0.24 1 AVERAGE 91.55 22.53 69.98 188 78.36 MAXIMUM 94.45 23.85 75.12 192 291.33 MINIMUM 80.25 21.18 62.38 178 33.93 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 03/04/14 4.9 03/04/14 2.0 03/11/14 13.9 03/11/14 1.9 Monthly Monthly Maximum 13.9 Minimum 1.9 DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 04/01/14 to 04/30/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be Z75% V732 I V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 04/01/ 4 -91.13 23.15 68.12 187 57.19 0.17 1 04/02/14 04/03/14 04/04/14 92.61 22.52 68.22 190 83.14 0.10 1 04/05/14 91.63 22.43 69.79 190 60.95 0.10 1 04/06/14 92.09 22.16 71.05 186 59.03 0.20 1 04/07/14 90.68 22.44 68.97 189 64.22 0.12 1 04/08114 90.53 22.29 '` 70.24 189 48.72 0.12 1 04/09/14 04/10/14 04/11/14 04/12/14 93.77 22.51 69.40 188 83.03 0.14 1 04/13/14 90.69 22.59 70.71 187 56.82 0.171 1 04/14/14 91.10 22.67 68.45 188 58.89 0.14 1 04/15/14 91.18 21.89 70.68 189 59.05 0.12 1 04/16/14 92.41 22.56 67.73 187 75.35 0.17 1 04/17/14 90.69 23.67 71.85 187 61.58 0.17 1 04/18/14 90.02 22.71 67.68 186 61.25 0.20 1 04/19/14 90.28 22.35 64.84 188 76.64 0.14 1 04/20/14 91.45 22.63 71.45 188 62.25 0.14 1 64/2 //14 90.98 22.43 70.32 188 56.64 0.14 1 04/22/14 92.16 22.29 70.69 189 58.87 0.12 1 04/23/14 93.23 21.90 71.70 189 58.63 0.12 1 04/24/14 95.81 22.44 67.45 189 75.26 0.12 1 04/25/14 04/26/14 04/27/14 04/28/14 04/29/14 04/30/14 AVERAGE 91.71 22.51 69.43 188 64.08 MAXIMUM 95.81 23.67 71.85 190 83.14 MINIMUM 90.02 21.89 64.84 186 48.72 Note: %TS data for 4/8/14 samples is qualified due to duplicate out of QC. Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 04/01/14 5.0 04/01/14 2.0 04/08/14 8.6 04/08/14 2.0 Monthly Monthly Maximum 8.6 Minimum 2.0 DATE DRYER COMPLIANCE REPORT . Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. W00029804 05/01/14 to 05/31/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 05/01/14 89.04 21.05 60.99 187 107.64 0.17 1 05/02/14 89.32 21.06 66.47 187 60.53 0.17 1 05/03/14 92.24 21.61 72.91 188 54.63 0.14 1 05/04/14 89.73 22.19 69.14 187 58.29 0.17 1 05/05/14 89.07 20.88 68.31 186 44.43 0.20 1 05/06/14 89.50 21.81 68.49 187 51.681 0.17 1 05/07 4 94 90.37 20.58 68.30 188 51.06 0.14 1 05/08/14 91.44 -20.231 69.30 191 53.20 0.08 1 05/09/14 91.45 20.94 68.06 191 52.20 0.08 1 05/10/14 05/11/14 91.53 21.06 69.33 190 66.84 0.10 1 05/12/14 91.08 21.05 67.73 191 49.90 0.08 1 05/13/14 92.44 21.04 72.28 190 37.69 0.10 1 05/14/14 05/15/14 89.50 20.86 67.00 189 56.69 0.12 1 05/16/14 92.61 21.30 71.62 189 53.89 0.12 1 05/17/14 91.65 21.13 71.83 189 50.51 0.12 1 05/18/14 91.96 21.59 70.10 188 59.20 0.14 1 05/19/14 05/20/14 05/21/14 92.99 21.77 69.65 190 69.37 0.10 1 05/22/14 91.82 21.65 71.03 189 52.27 0.12 1 05/23/14 92.05 21.49 71.94 189 48.74 0.12 1 05/24/14 91.08 21.61 69.05 190 60.47 0.10 1 05/25/14 91.84 21.70 70.60 190 48.52 0.10 1 05/26/14 92.32 21.53 71.38 190 56.64 0.10 1 05/27/14 93.75 22.931 71.77 190 63.32 0.10 1 05/28/14 91.98 22.23 70.60 189 60.37 0.12 1 05/29/14 92.14 22.31 69.49 192 68.10 0.07 1 05/30/14 93.82 22.09 69.78 193 70.401 0.06 1 05/31/14 92.54 22.27 69.82 188 61.311 0.14 1 AVERAGE 91.45 21.48 69.52 189 58.07 MAXIMUM 93.82 22.93 72.91 193 107.64 MINIMUM 89.04 20.231 60.99 186 37.69 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 05/06/14 4.9 05/06/14 2.2 05/13/14 4.3 05/13/14 1.9 Monthly Monthly Maximum 4.9 Minimum 1.9 DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 06/01/14 to 06/30/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be Z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 06/01/14 90.66 22.23 68.04 188 58.37 0.14 1 06/02/14 90.64 21.52 66.72 188 55.16 0.14 1 06/03/14 91.54 22.56 68.74 188 51.97 0.14 1 06/04/14 91.41 22.05 70.94 188 51.17 0.14 1 06/05/14 90.71 20.70 68.97 188 70.81 0.14 1 06/06/14 91.96 20.71 68.75 190 58.911 0.10 1 06/07/14 06/08/14 06/09/14 06/10/14 06/11/14 06/12/14 06/13/14 90.71 21.06 66.92 188 70.52 0.14 1 06/14/14 92.15 21.22 69.87 190 52.78 0.10 1 06/15/14 91.23 21.46 70.56 188 51.83 0.14 1 06/16/14 90.96 21.73 66.88 189 59.23 0.12 1 06/17/14 91.31 21.11 67.52 190 47.93 0.10 1 06/18/14 06/19/14 06/20/14 06/21/14 93.68 20.88 69.01 190 82.62 0.10 1 06/22/14 90.74 21.74 68.25 188 60.30 0.14 1 06/23/14 92.20 21.581 70.75 190 61.18 0.10 1 06/24/14 92.06 21.22 68.52 185 77.77 0.24 1 06/25/14 89.79 21.32 69.71 186 49.54 0.20 1 06/26/14 90.42 21.09 70.06 189 53.09 0.12 1 O6/27/14 91.11 20.44 67.78 189 61.59 0.12 1 06/28/14 91.74 20.82 69.70 190 52.01 0.10 1 06/29/14 92.45 20.84 76.31 189 43.68 0.12 1 06/30/14 95.03 21.37 70.18 194 91.17 0.05 1 AVERAGE 91.55 21.32 69.25 189 60.08 MAXIMUM 95.03 22.56 76.31 194 91.17 MINIMUM 89.79 20.44 66.72 185 43.68 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 06/17/14 4.9 06/17/14 1.9 O6/26/14 2.2 06/26/14 2.0 Monthly Monthly Maximum 4.9 Minimum 1.9 DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 07/01/14 to Pellet %TS Cake Cake Mix Preseperator Drum SRT Dirum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues equired Minutes Met 1 = Yes Daily Must Be Z75% V732 V968 I V970 V1010 Alt 1 B Time I V1013 0 = No I V1014 V877 07/01/14 94.66 20.39 79.37 191 36.89 0.08 1 07/02/14 07/03/14 92.83 21.14 69.72 191 122.20 0.08 1 07/04/14 93.24 22.85 67.38 190 71.56 ( 0.10 1 07/05/14 07/06/14 94.77 21.91 72.61 192 85.691 0.07 1 07/07/14 93.98 22.07 71.92 189 82.14 0.12 1 07/08/14 94.12 22.60 73.73 191 63.29 0.08 1 07/09/14 93.52 22.23 72.30 191 74.84 0.08 1 07/10/14 92.95 22.16 72.32 191 65.49 0.08 1 07/11/14 93.89 22.12 76.04 193 41.70 I 0.06 1 07/12/14 93.88 21.36 71.07 191 85.75 0.08 1 07/13/14 92.29 21.23 72.21 191 71.16 0.08 1 07/14/14 92.65 20.78 72.44 191 61.90 0.08 1 07/15/14 92.37 20.98 72.42 191 64.66 1 0.081 1 07/16/14 92.38 20.60 69.61 191 71.61 1 0.08 1 07/17/14 93.10 20.67 72.45 192 67.64 0.071 07/18/14 92.76 21.07 72.89 192 53.83 0.07 1 07/19/14 1 07/20/14 1 .07/21/14 93.33 20.17 69.18 192 81.18 0.07 1 07/22/14 91.37 20.26 70.42 189 61.701 ' 0.12 1 07/23/14 92.40 20.46 71.551 191 69.38 0.08 1 07/24/14 92.73 21.30 74.84 191 54.17 0.08 1 07/25/14 92.98 21.19 72.48 191 76.05 0.08 1 07/26/14 92.12 21.12 71.29 192 61.89 0.07 1 07/27/14 92.04 21.09 71.56 190 67.40 j 0.10 1 07/28/14 93.59 20.62 72.22 191 55.80 0.08 1 07/29/14 93.40 2047. 70.571 192 62.79 0.07 1 07/30/14 07/31/14 93.81 21.351 72.691 1901 106.961 1 0.10 1 AVERAGE 93.12 21.24 72.13 191 69.91 MAXIMUM 94.77 22.85 79.371 193 122.20 MINIMUM 91.37 20.17 67.38 189 36.89 Daily Fecal Colifonn, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 07/01/14 1.9 07/01/14 1.9 07/08/14 1.9 07/08/14 1.8 Monthly Monthly Maximum 1.9 Minimum 1.8 DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 08/01/14 to 08/31/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be Z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 08/01/14 93.30 20.60 74.10 191 65.80 0.08 1 08/02/14 92.83 20.77 76.00 191 53.34 0.08 1 08/03/14 93.58 20.56 74.53 190 94.39 0.10 1 08/04/14 91.98 20.78 73.77 191 59.90 0.08 1 08/05/14 92.89 20.98 73.52 189 46.61 0.12 1 08/06/14 08/07/14 93.88 20.43 74.19 192 114.72 0.071 1 08/08/14 92.04 21.36 73.12 192 59.53 0.071 1 08/09/14 92.63 21.20 72.01 191 52.09 0.081 1 08/10/14 92.23 21.55 70.77 190 65.76 0.10 1 08/11/14 92.49 20.69 71.76 190 60.05 0.10 1 08/12/14 92.89 20.91 74.19 191 50.42 0.08 1 08/13/14 08/14/14 08/15/14 95.48 22.00 78.03 190 71.93 0.101 1 08/16/14 95.05 21.96 73.41 191 87.22 0.081 1 08/17/14 92.84 21.51 68.40 192 88.76 0.071 1 08/18/14 95.37 21.48 75.44 192 63.68 0.07 1 08/19/14 94.20 22.10 74.18 190 141.14 0.10 1 08/20/14 95.27 22.19 75.97 193 54.70 0.06 1 08/21/14 08/22/14 08/23/14 93.01 20.90 68.641 186 105.62 0.20 1 08/24/14 92.33 21.60 70.94 187 66.26 0.17 1 08/25/14 93.32 21.81 69.47 188 77.86 0.141 1 08/26/14 91.64 22.20 71.07 185 68.09 0.24 1 08/27/14 93.06 22.31 70.27 190 72.24 0.10 1 08/28/14 92.67 21.97 72.20 189 64.27 0.12 1 08/29/14 91.67 22.14 61.47 186 125.60 0.20 1 08/30/14 08/31/14 95.37 22.70 74.71 190 71.80 0.10 1 AVERAGE 93.28 21.47 72.49 190 75.27 MAXIMUM 95.48 22.70 78.03 193 141.14 MINIMUM 91.64 20.43 61.47 185 46.61 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 08/05/14 1.9 08/05/14 1.9 08/12/14 1.9 08/12/14 1.9 Monthly Monthly Maximum 1.9 Minimum 1.9 DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 09/01/14 to 09/30/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be 2:75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 09/01/14 92.54 22.10 67.59 187 73.35 0.17 1 09/02/14 92.05 22.27 68.46 187 67.83 0.17 1 09/03/14 92.16 22.50 68.61 187 57.77 0.17 1 09/04/14 09/05/14 91.54 21.94 70.42 185 80.61 0.24 1 09/06/14 93.31 22.00 70.57 1911 66.40 0.08 1 09/07/14 09/08/14 92.87 20.75 70.92 189 75.90 0.12 1 09/09/14 93.85 21.89 72.35 190 66.38 0.10 1 69/10/14 91.70 21.60 70.59 188 68.09 0.14 1 09/11/14 91.34 21.761 67.76 185 50.371 0.24 1 09/12/14 09/13/14 191 0.08 09/14/14 91.68 22.04 63.36 187 100.80 0.17 1 09/15/14 91.24 22.23 68.93 186 71.66 0.20 1 09/16/14 89.55 22.07 69.341 185 69.54 0.241 1 09/17/14 89.791 22.20 68.46 1831 63.25 0.34 1 09/18/14 92.25 21.82 71.75 186 73.39 0.20 1 09/19/14 91.50 22.14 67,36 188 87.12 0.14 1 09/20/14 92.64 22.29 70.58 188 81.76 0.14 1 09/21 /14 189 0.12 09/22/14 09/23/14 92.52 20.44 69.87 187 134.371 0.17 1 09/24/14 93.02 21.74 73.52 189 70.83 0.121 1 09/25/14 91.96 22.43 71.41 188 81.17 0.141 1 09/26/14 91.93 22.63 70.75 187 75.78 0.17 1 09/27/14 90.33 21.94 67.30 186 79.38 0.20 1 09/28/14 09/29/14 93.03 22.25 69.27 188 88.47 0.14 1 09/30/14 90.61 22.10 67.41 186 93.71 0.20 1 AVERAGE 91.89 21.96 69.42 187 77.30 MAXIMUM 93.85 22.63 73.52 191 134.37 MINIMUM 89.55 20.44 63.36 183 50.37 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 09/02/14 2.0 09/02/14 2.0 09/09/14 1.9 09/09/14 1.9 Monthly Monthly Maximum 2.0 Minimum 1.9 DATE DRYER COMPLIANCE REPORT Thermal Siosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 10/01/14 to 10/31/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be Z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 10/01/14 95.07 23.05 70.84 182 100.29 0.41 1 10/02/14 90.32 ;; 21.54 * 68.40 185 82.96 0.24 1 10/03/14 93.32 22.04 67.15 189 95.27 0.12 1 10/04/14 90.44 22.36 71.41 189 80.76 0.12 1 10/05/14 10/06/14 90.25 21.46 71.03 185 88.19 0.241 1 10/07/14 94.02 21.98 74.39 186 57.48 0.20 1 10/08/14 10/09/14 10/10/14 10/11/14 90.57 21.86 67.67 181 92.80 0.49 1 10/12/14 90.16 22.461 62.81 183 123.261 0.34 1 10/13/14 90.09 22.881 65.75 185 86.011 0.24 1 10/14/14 88.46 22.54 65.15 182 96.771 0.41 1 10/15/14 92.42 22.44 65.31 184 91.231 0.29 1 10/16/14 86.66 22.33 64.84 185 57.271 0.24 1 10/17/14 10/18/14 10/19/14 92.01 20.38 64.33 187 69.831 0.17 1 10/20/14 92.65 20.46 64.38 189 72.35 0.12 1 10/21/14- 90.89 20.65 67.12 187 47.69 0.17 1 10/22/14 91.10 19.65 67.03 188 48.50 0.14 1 10/23/14 90.42 16.45 65.12 183 41.68 0.34 1 10/24/14 91.15 23.45 70.79 185 47.15 0.24 1 10/25/14 10/26/14 10/27/14 91.51 23.58 67.81 183 92.77 0.34 1 10/28/14 93.20 23.50 70.08 182 91.81 0.41 1 10/29/14 92.30 23.35 62.44 183 87.90 0.34 1 10/30/14 90.01 22.05 63.30 1811 73.491 0.491 1 10/31/14 88.62 20.51 64.10 186 48.901 0.201 1 AVERAGE 91.11 21.78 67.01 185 77.15 MAXIMUM 95.07 23.58 74.39 189 123.26 MINIMUM 86.66 16.451 62.44 181 41.68 ;; Data qualified. Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE_ V1053 10/07/14 1.9 10/07/14 1.9 10/14/14 2.1 10/14/14 2.0 Monthly Monthly Maximum 2.1 Minimum 1.9 DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 11 /01 /14 to 11 /30/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp % %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 11/01/14 90.60 20.82 66.36 187 44.91 0.171 1 11/02/14 92.92 20.34 66.34 189 59.92 0.121 1 11/03/14 92.62 21.85 68.57 191 61.36 0.08 1 11/04/14 95.66 22.18 76.00 192 38.72 0.07 1 11/05/14 93.70 19.89 67.75 194 137.85 0.05 1 11/06/14 92.16 20.98 71.451 184 57.20 0.29 1 11/07/14 92.91 21.86 67.30 182 81.05 0.41 1 11/08/14 92.91 22.83 73.01 186 48.59 0.201 1 11/09/14 92.05 22.86 70.89 188 67.94 0.14 1 11/10/14 91.44 22.63 72.42 186 65.37 0.20 1 11/11/14 90.90 22.78 69.23 187 51.88 0.17 1 11/12/14 11/13/14 86.84 22.51 64.55 183 106.55 0.34 1 11/14/14 91.73 22.05 70.78 187 57.181 0.17 1 11/15/14 91.70 22.43 71.87 187 64.20 0.17 1 11/16/14 90.52 22.481 70.34 185 70.93 0.24 1 11/17/14 89.63 22.17 71.41 185 46.78 0.24 1 11/18/14 11/19/14 91.41 21.67 69.79 185 90.92 0.24 1 11/20/14 91.06 20.88 68.47 190 93.56 0.10 1 11/21/14 92.40 22.15 69.94 183 70.73 0.34 1 11/22/14 89.14 21.90 69.59 184 68.96 0.29 1 11/23/14 89.48 22.091 67.77 185 64.56 0.24 1 11/24/14 90.67 21.79 70.02 184 70.27 029 1 11/25/14 88.84 22.77 71.76 183 69.77 0.34 1 11/26/14 89.55 22.33 69.18 184 76.55 0.29 1 11 /27/14 11/28/14 88.88 21.94 68.43 186 104.10 0.20 1 11/29/14 88.18 21'.77 67.16 184 52.50 0.29 1 11/30/14 90.64 21.571 70.091 185 57.95 0.24 1 AVERAGE 91.06 21.91 69.65 186 69.64 MAXIMUM 95.66 22.86 76.00 194 137.85 MINIMUM 86.84 19.89 64.55 182 38.72 Daily Fecal Coliform, MPN/dry g Minimum 7MaxImum DATE V876 DATE V1053 Monthly Monthly Maximum 2.0 Minimum 1.9 DATE DRYER COMPLIANCE REPORT Thermal Biosolids Dryer Management Facility Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 12/01/14 to 12/31/14 Pellet %TS Cake Cake Mix Preseperator Drum SRT Drum SRT Time Temp %TS % %TS % Temp MIN Deg F Achieved Mintues Required Minutes Met 1 = Yes Daily Must Be z75% V732 V968 V970 V1010 Alt 1 B Time V1013 0 = No V1014 V877 12/01/14 89.40 21.86 67.13 184 79.29 0.29 1 12/02/14 91.43 21.84 69.24 185 63.18 0.24 1 12/03/14 12/04/14 12/05/14 91.15 21.07 58.66 185 172.14 0.24 1 12/06/14 92.86 20.681 72.55 188 52.79 0.14 1 12/07/14 88.58 21.16 67.63 186 64.43 0.20 1 12/08/14 12/09/14 91.67 20.82 69.23 186 61.94 0.20 1 12/10/14 90.61 21.52 68.11 186 _ 63.32 0.20 1 12/11/14 89.53 21.22 66.92 187 74.26 0.171 1 12/12/14 91.55 20.691 68.50 186 56.56 0.20 1 12/13/14 93.46 21.30 71.38 188 67.33 0.14 1 12/14/14 90.64 21.61 69.54 189 83.19 0.12 1 12/15/14 88.95 20.75 67.16 187 65.66 0.17 1 12/16/14 88.31 20.73 64.52 186 63.36 0.20 1 12/17/14 - 12/18/14 87.70 20.18 64.65 182 95.65 0.41 1 12/19/14 89.08 20.41 66.49 187 51.85 0.17 1 12/20/14 88.84 20.44 68.22 186 84.34 0.20 1 12/21/14 90.13 20.36 65.94 186 71.411 0.20 1 12/22/14 90.06 20.68 67.60 187 68.26 0.17 1 12/23/14 12/24/14 12/25/14 12/26/14 12/27/14 12/28/14 12/29/14 12/30/14 1 88.18 20.57 66.62 183 93.76 0.34 1 12/31/14 90.87 21.42 63.37 186 92.91 0.20 1 AVERAGE 90.15 20.971 67.17 186 76.28 MAXIMUM 93.46 21.86 72.55 189 172.14 MINIMUM 87.70 20.181 58.66 182 51.85 Daily Fecal Coliform, MPN/dry g Maximum Minimum Must Be <1000 DATE V876 DATE V1053 12/02/14 2.0 12/02/14 1.9 12/09/14 13.8 12/09/14 13.8 Monthly Monthly Maximum 13.8 Minimum 1.9 City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 7. City of Winston-Salem Class A EQ "Soil Solutions" Information Handout 4 Winston-Salem • Forsyth County iq Wildes Sw w * Solid Wash Disposal WINSTON-SALEM SOIL SOLUTION A high quality biosolids product for use as a soil amendment for agriculture (by Contractor) Produced by the Winston-Salem/Forsyth County Utilities Commission's Thermal Biosolids Dryer Management Facility 2799 Griffith Road, Winston-Salem, North Carolina 27103 Permit Number: WQ0029804 Winston-Salem Soil Solution is a pelletized material produced from the heat treatment of residuals from municipal wastewater. This product meets the standards for a Class A, Exceptional Quality biosolids product according to the EPA's 40CFR Part 503 regulations. The recipient is responsible for applying the product at a rate that does not exceed the agronomic requirement for that crop or vegetation. Applications of this product shall be made only in accordance with the following prohibitions: 1. A minimum buffer of 10 feet shall be kept from any public or private water supply source (including wells) or any streams, lakes, rivers or other drainageways when applying this residuals product to soil as an amendment. 2. This residuals product shall not be applied to any site that is flooded, frozen or snow-covered. 3. The application or storage of this residuals product shall be conducted by procedures adequate to prevent surface runoff from carrying any disposed or stored product into any surface waters. The City/County Utilities Commission will accept no liability for misuse of the Winston-Salem Soil Solution product. For further information on the use of this product, contact Mr. Bruce Casey at 336-397-7662 or the above address. Although no guarantee is made as to the plant nutrient content of this product, analysis has shown the following approximate N-P-K concentrations: Total Nitrogen 2.7 — 3.8 % Phosphorus 1.4 — 1.7 % Potassium 0.15 - 0.18 % Receiver's Signature Revised 1/12/15 Date Winston-Salem * Forsyth County YU UNIRW Water • Sewer • "Id Wseoa Diaposel WINSTON-SALEM SOIL SOLUTION A high quality biosolids product for use as a soil amendment (by Individuals) Produced by the Winston-Salem/Forsyth County Utilities Commission's Thermal Biosolids Dryer Management Facility 2799 Griffith Road, Winston-Salem, North Carolina 27103 Permit Number: WQ0029804 Winston-Salem Soil Solution is a pelletized material produced from the heat treatment of residuals from municipal wastewater. This product meets the standards for a Class A, Exceptional Quality biosolids product according to the EPA's 40CFR Part 503 regulations. It is intended for lawn and home garden use only. The recipient is responsible for applying the product at a rate that does not exceed the agronomic requirement for that crop or vegetation. Applications of this product shall be made only in accordance with the following prohibitions: 1. A minimum buffer of 10 feet shall be kept from any public or private water supply source (including wells) or any streams, lakes, rivers or other drainageways when applying this residuals product to soil as an amendment. 2. This residuals product shall not be applied to any site that is flooded, frozen or snow-covered. 3. The application or storage of this residuals product shall be conducted by procedures adequate to prevent surface runoff from carrying any disposed or stored product into any surface waters. 4. This product is intended for immediate application and is not intended for long term storage. The City/County Utilities Commission will accept no liability for misuse of the Winston-Salem Soil Solution product. For further information on the use of this product, contact Mr. Bruce Casey at 336-397-7662 or the above address. Although no guarantee is made as to the plant nutrient content of this product, analysis has shown the following approximate N-P-K concentrations: Total Nitrogen 2.7 — 3.8 % Phosphorus 1.4 - 1.7 % Potassium 0.15 - 0.18 % Receiver's Name (Please PRINT) Tare weight: Gross weight: Net weight: Revised 1/12/15 Signature Date City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 8. City of Winston-Salem Thermal Biosolids Dryer Management Facility Permit W AT �9QG r April 13, 2006 Mr. Ron Hargrove, Deputy Utilities Director Winston-Salem/Forsyth County Utilities Commission P.O. Box 2511 Winston-Salem, North Carolina 27102 Dear Mr. Hargrove: Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E. Director Division of Water Quality RECEIVED-, ER2GdS 1 �TUTIES DIVIS101\1 Subject: Permit No. WQ0029804 Winston-Salem/Forsyth County Utilities Commission Thermal Biosolids Dryer Management Facility Distribution of Residual Solids (503) In accordance with your permit application package received on February 7, 2006, we are forwarding herewith Permit No. WQ0029804, dated April 13, 2006, to the Winston-Salem/Forsyth County Utilities Commission, North Carolina for the subject residuals Thermal Biosolids Dryer Management Facility and Class A EQ residuals product distribution program. This permit shall be effective from the date of issuance until April 12, 2011, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements in this permit. Failure to establish an adequate system for collecting and maintaining the required operational information will result in future compliance problems. Please note that the frequency with which monitoring must be performed is based entirely on the amount of product that is distributed for application to the land. The Division urges the Permittee to carefully estimate its amount of annual product distribution, so that the correct monitoring frequency is selected for implementation. See Condition III.4. and Condition III. 5. for more detail. The EPA guidance document entitled "Control of Pathogens and Vector Attraction in Sewage Sludge (EPA/625/R-92-013)" states "all Class A material,must be tested to show that the microbiological requirements are met at the time when it is ready to be used... If a facility stores material before it is distributed for use or disposal, microbiological testing should take place after storage... In each case, the timing represents the last practical monitoring point before the biosolids are applied to the land or placed on a surface disposal site.... Biosolids that are sold or given away cannot be monitored just prior to actual use; instead monitoring is required as it is prepared for sale or given away..., which in most cases is the last time the biosolids are under the control of a biosolids preparer." The Division encourages the Permittee to contact the Aquifer Protection Section/Land Application Unit or EPA's Region IV to ensure that any -monitoring program employed is in complete compliance with 40 CFR Part 503. _ Aoe Caro ina Ntura�llb North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone (919) 733-7015 Customer Service Internet: www.ncwaterquality.org Location: 512 N. Salisbury St. Raleigh, NC 27604 FAX (919) 733-2496 1-877-623-6748 An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper Mr. Ron. Hargrove, Deputy Utilities Director April 13, 2006 Page 2 Prior to the initial distribution of any Class A EQ residuals product generated from this facility, Conditions I. 1., 2., and 3. must be completed. In particular, the analytical results and operational data that demonstrate that the residuals thermal dryer facility is capable of meeting the required pathogen reduction and vector attraction reduction requirements shall be submitted to the Division for review and approval. You are reminded that the construction of this facility was authorized under Authorization to Construct No. 037834A02, and the associated certification must be received from a professional engineer certifying that the permitted facility has been installed in accordance with the approved plans and specifications. If any parts, requirements, or limitations contained in this permit are unacceptable, you have the right to request an adjudicatory hearing upon written request within thirty (30) days following receipt of this permit. This request must be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of i Administrative Hearings, 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made this permit shall be final and binding. If you need additional information concerning this matter, please do not hesitate to contact Cecil G. Madden, Jr., P.E. at (919) 715-6203. Kimek, P. . ID:cgm cc: Randall D. Ashburn, P.E., Black and Watch, Charlotte Forsyth County Health Department Winston-Salem Regional Office, Aquifer Protection Section DWQ/Technical Assistance and Certification Unit DWQ/Aquifer Protection Section/Land Application Unit/Central Files DWQ/Aquifer Protection Section/Land Application Unit/LAU Files Daniel Blaisdell, P.E. Cecil G. Madden, Jr., P.E. Ishwar Devkota, P.E. PMB NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES RALEIGH DISTRIBUTION OF RESIDUAL SOLIDS (503) PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO THE • Winston-Salem/Forsyth County Utilities Commission In Forsyth County FOR THE Operation of the Thermal Biosolids Dryer Management Facility and Class A Exceptional Quality ("EQ") distribution program at the Archie Elledge WWTP located at NCSR 2972 (Griffith Road) Winston-Salem, North Carolina (N 36°02' 17" latitude and W 80°18'26" longitude), and consisting of a total of 26,076 (existing 8,320 and new 17,756) square -foot total biosolids management facility, capable of producing up to 12,264 dry tons per year of Class A pelletized biosolids (equating to 13,330.4 tons per year of pelletized biosolids at an average pellet solids content of 92%), which includes: (a) Two sludge blending tanks which are recommissioned secondary digesters, four 30-HP blending tank mixers, one new centrifuge (capable of dewatered cake production at 2,600 dry pounds/hour at 21 % solids) with a 395 gpm feed pump, digester gas control equipment, (b) one 600 gpm sludge macerator with a maximum particle size of 0.5 inch passing the grinder, two dewatered sludge screw conveyors with capacities of 350 cu. ft./hr. and 500 cu. ft./hr., a dewatered sludge screw conveyor and a dewatered sludge belt conveyor (existing modified to be reversible) with a capacity of 900 cu ft./hr., and two 60 GPM dewatered sludge cake pumps driven by adjustable frequency drives, (c) a polymer feed system consisting of dual 6,500 gallon polymer storage tanks, two polymer blending units with a 15 gph transfer pump, a 100 gpm dilution water pump, and a 5 HP mechanical blender, two 3,600 ! gallon stainless steel polymer aging tanks, polymer metering pumps, a dispersant feed system, Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 2 (d) a front end loader cake receiving hopper with a material conveyance capacity of 500 cu. ft./hr., one dewatered sludge screw conveyor with a capacity of 500 cu. ft. per hour, and pipeline lubrication system, (e) two 275 gpm dewatered sludge centrate transfer pumps, (f) a direct hot air contact triple pass rotary drum residuals dryer (51.4 dry tons per day capacity operating maximum of six days per week) consisting of hot air furnace, drum drier, air/solids separator, product screening, product cooler, off -gas scrubbing, and a regenerative thermal oxidizer (RTO) to thermally oxidize off -gasses, building traveling bridge crane (TB-1) with a 5 ton capacity, two dried product storage silos with minimum storage capacity of 360 dry tons total with baghouse controls, a trucks scale having a 50 ton capacity, miscellaneous piping, electrical work, controls, and all site work necessary to make a complete and functional residuals thermal dryer facility, (g) and replacement of three new non -potable water pumps of 1,670 gpm capacity each in the existing NPW pump station. and the operation of a program for the distribution of up to 12,264 dry tons per year of a Class A EQ residuals product from the sources listed in the most recently -certified Attachment A of this permit, pursuant to the application received February 7, 2006, and in conformity with, the project plan, specifications, and other supporting data subsequently filed and approved by the Department of Environment and Natural Resources and considered a part of this permit. This permit shall be effective from the date of issuance until April 12, 2011, and shall be subject to the following specified conditions and limitations: I. PERFORMANCE STANDARDS The Aquifer Protection Section of the Division of Water Quality's Winston-Salem Regional Office at telephone number (919) 771-5000 shall be notified at least 48 hours in advance of the initial distribution of any Class A EQ residuals product so that an in -place inspection can be made. Such notification to the Regional Aquifer Protection Supervisor shall be made during normal office hours (i.e., from 8:00 a.m. until 5:00 p.m.) between Monday and Friday, but excluding State Holidays. 2. Prior to the initial distribution of any Class A EQ residuals product, analytical results and operational data that demonstrate that the residuals thermal dryer facility is capable of meeting the required pathogen reduction and vector attraction reduction requirements, as is required by Condition I.9., shall be submitted to the Division. Mail two copies of the results/data to the NCDENR-DWQ, Aquifer Protection Section, Land Application Unit, Residuals Program Coordinator, 161'7 Mail Service Center, Raleigh, NC 27699-1617. 3. Prior to the initial distribution of any Class A EQ residuals product, a final version of the information sheet that will be provided to the person who receives the Class Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 3 A EQ residuals product sold or given away in another container for application to the land, as is required by Condition H. 7., shall be submitted to the Division. Mail two copies of the information sheet to the NCDENR-DWQ, Aquifer Protection Section, Land Application Unit, Residuals Program Coordinator, 1617 Mail Service Center, Raleigh, NC 27699-1617. 4. The residuals thermal dryer facility and Class A EQ residuals product distribution program shall be effectively maintained and operated as a non -discharge system to prevent the discharge of .any wastes to waters of the state resulting from the operation of this facility or program. 5. This permit shall become voidable in the event of failure of the residuals thermal dryer facility or Class A EQ residuals product distribution program to adequately protect the assigned water quality standards of the surface waters and groundwater. 6. The issuance of this permit shall not relieve the Permittee of the responsibility for damages to surface water or groundwater resulting from the operation of this residuals thermal dryer facility or Class A EQ residuals product distribution program. 7. In the event that the residuals thermal dryer facility or Class A EQ residuals product distribution program is not operated satisfactorily, including the creation of nuisance conditions, the Permittee shall take any immediate corrective actions as may be required by the Division. 8. Diversion or bypassing of untreated residuals through the residual thermal dryer facility shall be prohibited. 9. When wastewater residuals are sold or given away, one of the Class A pathogen requirements in 40 CFR Part 503.32(a) and one of vector attraction reduction requirements in 40 CFR Part 503.33 shall be met. Additionally, an evaluation shall be performed which demonstrates the residuals' ability to comply with this requirement. Upon request, a copy of this evaluation, including all test results and calculations, shall be submitted. 10. No Class A EQ residuals product that tests or is classified as a hazardous or toxic waste under 40 CFR Part 261 shall be sold or given away under the conditions of this permit. H. OPERATION AND MAINTENANCE REQUIREMENTS The residuals thermal dryer facility and Class A EQ residuals product distribution program shall be properly operated and maintained at all times. 2. Upon classification of .the residuals thermal dryer facility and Class A EQ residuals -- product distribution program by the Water Pollution Control System Operators Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 4 Certification Commission (WPCSOCC), the Permittee shall employ a certified operator to be in responsible charge (ORC) of the facility and program. The operator shall hold a certificate of the type classification assigned to the facility and program by the WPCSOCC. The Permittee shall also employ a certified back-up operator of the appropriate type to comply with the conditions of 15A NCAC 8G .0202.. 3. No waste or residuals other than those generated by the residuals source -generating facilities listed in the most recently -certified Attachment A shall be approved for processing, marketing, and distribution in accordance with this permit. 4. All residuals and Class A EQ residuals product shall be adequately stored to prevent leachate runoff prior to and following treatment. Following treatment, the Class A EQ residuals product may be stored in an elevated silo, placed on a concrete pad, kept under shelter, covered, or stored in a manner as otherwise approved by the Division until such time as it is distributed to the user. If an alternative storage site is to be used, approval shall first be obtained from the Division. 5. Adequate provisions shall be taken to prevent wind erosion and surface runoff from conveying pollutants from residuals or the Class A EQ residuals product from the residuals thermal dryer facility onto adjacent property or into any surface waters. 6. For a Class A EQ residuals product to be sold or given away in bags or other container for application to the land, the following shall be satisfied: The Ceiling Concentrations (Dry Weight Basis) and the Pollutant Monthly Average Concentrations (Dry Weight Basis) shall be maintained: Parameter Ceiling Concentration (milligrams per kilogram) Monthly Average Concentration (milligrams per kilogram) Arsenic 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 2,800 7. A label shall be affixed to the bag or other container in which a Class A EQ residuals product is sold or given away for application to the land, or an information sheet shall be provided to the person who receives the Class A EQ residuals product sold or given away in another container for application to the land. The label or information sheet shall contain the following information: Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 5 a. The name and address of the person who prepared the Class A EQ residuals product that is sold or given away in a bag or other container for application to the land. b. A statement that application of the Class A EQ residuals product to the land is prohibited except in accordance with the instructions on the label or information sheet. C. A statement regarding all buffers from the area to which the Class A EQ residuals product is applied, including a minimum 10-foot buffer from any public or private water supply sources (i.e., including wells), streams, lakes, rivers, or drainageways. d. A statement that the Class A EQ residuals product shall not be applied to any site that is flooded, frozen, or snow-covered. e. A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored Class A EQ residuals product • into any surface waters. III. MONITORING AND REPORTING REQUIREMENTS 1. Any monitoring (i.e., including groundwater, surface water, residuals, soil, or plant tissue analyses) deemed necessary by the Division to ensure protection of the environment shall be established and an acceptable sampling ,and reporting schedule shall be followed. 2. Proper records shall be maintained by the Permittee to track all residuals generated at the thermal dryer facility and Class A EQ residuals product distribution activities. These records shall include, but are not necessarily limited to, the following information: a. Source, amount, and analysis (as applicable) of residuals accepted for treatment in the residuals thermal dryer facility. b. Source and amount of each amendment material used for treatment in the residuals thermal dryer facility. C. Analysis of the Class A EQ residuals product. d. Name of the initial recipient of the Class A EQ residuals product, the amount distributed, and the intended use. 3. The Class A EQ residuals product shall be analyzed to demonstrate that it is non- hazardous under the Resource Conservation and Recovery Act (RCRA). A corrosivity, ignitability, and reactivity analysis as well as a Toxicity Characteristics Leaching Procedure (TCLP) analysis shall be conducted by the Permittee annually, and the results of the analyses shall be maintained on file by the Permittee for a minimum of five years. • Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 6 The TCLP analysis shall include the following parameters (i.e., note the regulatory level in milligrams per liter in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane,(0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) ethoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) 4. An analysis shall be conducted by the Permittee on the Class A EQ residuals product at a frequency that is dependent on the dry tons of Class A EQ residuals product distributed or expected to be distributed during the calendar year for application to the land. The monitoring frequency schedule shall be as stipulated in the following table: Amount of Product Amount of Product Distributed for Distributed for Application to the Land Application to.the Land Monitoring Frequency (metric tons per (short tons per 365-day period) 365-day period) 0 < mDT/yr < 290 0 < DT/ r < 319 Once per Year 290 < mDT/yr < 1,500 319 < DT/yr < 1,650 - Once per Quarter (Four Times per Year) 1,500 < mDT/yr < 15,000 1,650 < DT/yr < 16,500 Once per Days (Six Timeser Year) 15,000 < mDT/yr 16,500 < DT/yr - Once per Month (12 Times per Year) The results of all analyses shall be maintained on file by the Permittee for a minimum of five years. The analysis shall include the following minimum parameters: Aluminum Magnesium Phosphorus Ammonia -Nitrogen Mercury Potassium Arsenic Molybdenum Selenium Cadmium Nickel Sodium Calcium Nitrate -Nitrite Nitrogen Total K'eldahl Nitrogen Copper PH Total Solids (Percent) Lead Plant Available Nitrogen (By Calculation) Zinc • Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 7 5. The Class A EQ residuals product shall be monitored by the Permittee for compliance with Condition I. 9. of this permit at a frequency that is dependent on the dry tons of Class A EQ residuals product distributed or expected to be distributed during the calendar year for application to the land. The monitoring frequency schedule shall be as stipulated in the following. table: Amount of Product Amount of Product Distributed for Distributed for Application to the Land Application to the Land Monitoring Frequency (metric tons per (short tons per 365-daperiod) 365-dayperiod) 0 < mDT/yr < 290 0 < DT/yr < 319 Once 2er Year 290 <_ mDT/yr < 1,500 319 <_ DT/yr < 1,650 Once per Quarter (Four Times per Year) 1,500 < mDT/yr < 15,000 1,650 5 DT/yr < 16,500 Once per 60 Days (Six Times per Year) 15,000 <_ mDT/yr 16,500 < DT/yr Once per Month (12 Times per Year) The results of all analyses and records of all operational data shall be maintained on file by the Permittee for a minimum of five years. Data to verify stabilization of the product shall be maintained by the Permittee. The required data shall be specific to the stabilization process utilized, but should be sufficient to demonstrate compliance with the Class A pathogen requirements in 40 CFR Part 503.32(a) and the vector attraction reduction requirements in 40 CFR Part 503.33 clearly. In addition, the Environmental Protection Agency (EPA) certification statements concerning compliance with pathogen requirements, vector attraction reduction requirements, and management practices shall be completed at the above frequency by the proper authority or authorities if more than one is involved, either the person who generates the residuals or the person who prepares the Class A EQ residuals product to be sold or given away for application to the land. 6. Laboratory analyses and/or operational data, as required by Condition III.4., and Condition III.5. shall be performed/gathered on the Class A EQ residuals product as it is to be distributed. Furthermore, analytical determinations made pursuant to the monitoring and reporting requirements of this permit shall be made by a laboratory certified by the Division for the required parameter(s) under 15A NCAC 2H .0800 or 15A NCAC 2H .l 100. 7. Three copies of all required monitoring and reporting requirements as specified in Condition III. 1., Condition III. 3., Condition IH. 4., Condition III. 5., and Condition III. 6. shall be submitted annually on or before March 1" of the year following the distribution event to the following address: Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 8 NC Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 8. Noncompliance Notification: The Permittee shall report by telephone to the Aquifer Protection Section of Division's Winston-Salem Regional Office at telephone number (336) 771-5000, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence with the residuals thermal dryer facility or Class A EQ residuals product distribution program that results in the land application of significant amounts of wastes which are abnormal in quantity or characteristic. b. Any failure of the residuals thermal dryer facility or Class A EQ residuals product distribution program resulting in a release of material to receiving waters. C. Any time that self -monitoring information indicates that the residuals thermal dryer facility or Class A EQ residuals product distribution program has gone out of compliance with the conditions and limitations of this permit or the parameters on which .the system was designed. d. Any process unit failure, due to known or unknown reasons, that render the residuals thermal dryer facility incapable of adequate residual treatment. e. Any spillage or discharge from a vehicle or piping system during transportation of residuals or Class A EQ residuals product. Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to be taken to ensure that the problem does not recur. IV. GROUNDWATER REQUIREMENTS 1. The COMPLIANCE BOUNDARY for the residuals thermal dryer facility shall be as specified by regulations in 15A NCAC 2L (i.e., "Groundwater Classifications and Standards"). The Compliance Boundary for a disposal system individually permitted after December 31, 1983, shall be established at either (1) 250 feet from the waste disposal area or (2) 50 feet within the property boundary, whichever is closest to the residuals thermal dryer facility. An exceedance of groundwater quality standards at or beyond the Compliance Boundary shall be subject to immediate remediation action according to 15A NCAC 2L .0106(d)(2). 2. The REVIEW BOUNDARY shall be established around the residuals thermal dryer facility midway between the Compliance Boundary and the perimeter of the waste Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 9 disposal area. Any exceedance of groundwater quality standards at the Review Boundary shall require action in accordance with 15A NCAC 2L .0106(d)(1). 3. Any groundwater quality monitoring, as deemed necessary by the Division, shall be provided. V. INSPECTIONS 1. The Permittee or his designee shall inspect the residuals thermal dryer facility as well as the facilities related to the Class A EQ residuals product distribution program, residuals storage, transport, and treatment facilities to prevent malfunctions and deterioration, operator errors and discharges which may cause or lead to the release of wastes to the environment, a threat to human health, or a nuisance. The Permittee shall maintain an inspection log or summary including at least the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken by the Permittee. This log of inspections shall be maintained by the Permittee for a period of five years from the date of the inspection and shall be made available to the Division or other permitting authority, upon request. 2. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and inspect any property, premises, or place on or related to the residuals thermal dryer facility or Class A EQ residuals product distribution program at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records that must be kept under the terms and conditions of this permit; and may obtain samples of groundwater or surface water.. VI. GENERAL CONDITIONS 1. A set of approved plans and specifications for the subject residuals thermal dryer facility shall be retained by the Permittee for the life of the facility. 2. This permit shall become voidable unless the residuals thermal dryer facility and Class A EQ residuals product distribution program are constructed and operated in accordance with the conditions of this permit, the approved plans, and supporting materials, as approved by the Division. 3. Failure to abide by the conditions and limitations contained in this permit may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes § 143-215.6A through § 143-215.6C. 4. The annual administering and compliance fee shall be paid by the Permittee within 30 days after being billed by the Division. Failure to pay the fee accordingly may cause the Division to initiate action to revoke this permit, as specified by 15 NCAC 2H .0205 (c)(4). Winston-Salem/Forsyth County Utilities Commission Permit No. WQ0029804 April 13, 2006 Page 10 5. The issuance of this permit does not preclude the Permittee from complying with any and all statutes, rules, regulations, or ordinances that may be imposed by other government agencies (i.e., local, state, and federal) which have jurisdiction, including, but not limited to, applicable river buffer rules in 15A NCAC 2B .0200, soil erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO10000, and any requirements pertaining to wetlands under 15A NCAC 2B .0200 and 15A NCAC .0500. 6. This permit may be modified, revoked, and/or reissued to incorporate any conditions, limitations and monitoring requirements the Division deems necessary in order to protect the environment and public health adequately. 7. The Permittee, at least six months prior to the expiration of this permit, shall request its extension. Upon receipt of the request, the Division shall review the adequacy of the residuals thermal dryer facility and Class A EQ residuals product distribution program described therein, and if warranted, shall extend the permit for such period of time and under such conditions and limitations as it may deem appropriate. 8. This permit shall not be automatically transferable. In the event that there is a desire for the residuals thermal dryer facility and Class A EQ residuals product distribution program to change ownership or to change the name of the Permittee, a formal permit request shall be submitted to the Division with documentation from the parties involved and other supporting materials as may be appropriate. The approval of this request shall be considered on its merits, and may or may not be approved. Permit issued this 13t' day of April 2006 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION 0jl Alan W mek, P.E., Director Divisi P-, Water Quality By Aotfiority of the Environmental Management Commission Permit No. WQ0029804 ATTACHMENT A - Approved Residual Source-Generatine Facilities Permit No. WQ0029804 Winston-Salem/Forsyth County Utilities Commission Thermal Biosolids Dryer Management Facility and Distribution Program 1. No residuals other than those generated by the following residuals source -generating facilities shall be approved for acceptance for storage or treatment in the Winston-Salem/Forsyth County Utilities Commission, Thermal Biosolids Dryer Management Facility in accordance with this permit: Owner Facility Name County Permit Number Issued By Is 503? Maximum Monitoring Monitoring Frequency Dry Tons Per Frequency for for Condition III.4. Year Condition HI. and Condition III.5. 3. Winston-Salem/Forsyth County Utilities Commission Archie Elled e WWTP Forsyth NCO037834 DWQ 503 8,322' See Below See Below Winston-Salem/Forsyth County Utilities Commission Muddy Creek WWTP Forsyth NCO050342 DWQ 503 3,942' See Below See Below 'Based on residual production in Year 2023. 2. No residuals other than those generated by the following residuals source -generating facilities shall be approved for distribution under the residuals distribution program in accordance with this permit: Owner Facility Name County Permit Number Issued By Is 503? Maximum Monitoring Monitoring Frequency Dry Tons Per Frequency for for Condition III.4. Year Condition III. and Condition III. 5. 3. See Tables in Condition Winston-Salem/Forsyth County Utilities Commissionj Archie Elled e WWTP Forsyth W00029804 DWQ 503 12,264 Annually III 4. and 5. of Permit. Total I 1 1 12,264 Permit No. W00029804 Page 1 of I Certification Date: April 13, 2006 City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 9. Pathogen and Vector Attraction Reduction Explanation; Pathogen and Vector Attraction Reduction Certifications (DENR FORM RF) (Archie Elledge WWTP; Muddy Creek WWTP) Winston-Salem - Forsyth County t*'UlCi0tuie*s Water r Sewer r Solid Waste Disposal Manson Meads Complex City of Winston-Salem 27 99 Griffith Road Winston-Salem, NC 27103 CityLink 311 (336.727.8000) Fax 336.659.4320 www..dVofw.org City of Winston-Salem Annual Monitoring Report for Class B Biosolids for 2014 Pathogen and Vector Attraction Reduction Explanation Both the Archie Elledge Wastewater Treatment Plant and the Muddy Creek Wastewater Treatment Plant use Activated Sludge followed by Anaerobic Digestion for biological treatment. Both treatment plants utilize lagoons for storage if needed prior to land application. Stabilized Digested Sludges from both Archie Elledge and Muddy Creek WWTPs are combined in Blending Tanks prior to being dewatered, in preparation for drying and pelletizing into a Class A product. Although there was no land application of Class B biosolids in 2014, Pathogen and Vector Attraction Reduction information for both WWTPs' Class B biosolids is being provided. This is to show the continuity in treatment at both WWTPs, and to show that requirements have been met should any of this material be in storage and then be land applied as a Class B product in the future. Please find attached the signed certifications (DENR FORM RF) for the Archie Elledge WWTP, followed by the signed certifications for Muddy Creek WWTP. These forms are then followed by: - A Pathogen Reduction Summary and a Vector Attraction Reduction Summary for the Archie Elledge WWTP, along with formulas and operational data. - A Pathogen Reduction Summary,and a Vector Attraction Reduction Summary for the Muddy_ Creek WWTP, along with formulas and operational data. Please note for both WWTPs: Beginning June, 2014, the City began calculating each month's %VSR using the previous month's SRT average. This more accurately reflects current digester operations. (Examples are included within_ each plant's set of operational data showing the previous method as well as the current method of determining compliance.) Also, please note in the Operational Reports for either WWTP: a blank, space is generated when there is no flow; and therefore no analytical data. City Councib Mayor Allen Joines; Vivian H. Burke, Mayor ProTempore, Norrheasr Ward; Denise D. Adams; North Ward; Dan Besse, Soudrvnar Ward; Robert C. Clark, West W Molly Leighr, South W"; Jeff Madntosh, Northwest Ward; Derwin L Montgomery, East Ward; James Taylor, Jr., Southeast Ward'; City Manager: Lee D. Garrity Forsyth County Commlw onus David IL Plylec Chairman; Don Martin, Vice Chair, Ted Kaplan; Richard V. Linville; Walrer Marshall; Gloria D. Whisenhunt; Everette Withers Call311 or336-727-8000 County Manager: DudleyWaroje. Cltyllnk@eltyofws.org City/County Utility Commission David Neill, Chairman; Randall S. Tuttle, Vice -chair, Weslcy Curtis, Jr.; Harold E. Day; Tom Griffin; Harold R. Holmes, Charles D. Jewell, II; Paul S. McGill: Chris Parker, Al H. Seymour, J. Hill Stockton - ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Archie Elledge WWTP NPDES Number: NC00037834 Monitoring Period: From 1/1/2014 To 1/31/2014 ran rWu cnz 121- PIPa-.P indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo ❑ Beta Ray ❑ Gamma Ra ❑ a n P ast eurYz tio ❑ Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com ostin ❑ Aerobic Digestion ❑ ' e tron Anaerobic D r s If applicable to alternative performed (Class A or Class B) complete the following monito ing data: Pathogen Density Number o requency Sample Analytical Allowable Level gExcee- of . Tech - Parameter in sludge Minimum Geo. Mean Maximum Units g dences Analysis Type ' `rii 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per ram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform (dry weight) [7o,.+-, A++rartinn T2Prinetinn (40 CPR 503.33) -Please indicate option performea: Option 1 21Option 2 El Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ 1 Option 10 ❑ �:;::;:;:;:; No vector attraction reduction options were pe rformed rme d CERTIFICATION STATEMENT (please check the appropriate statement) O "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment.". Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Archie Elledge WWTP NPDES Number: NC00037834 Monitoring Period: From 2/1/2014 To 2/28/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If 'applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": ........:.:.:.:.:.... Compost El Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ :::::::::::: Beta Ray ❑ Y a a Gamma R ❑ Y steurization ❑ Pazatio n Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ composting ❑ jAerobic Digestion ❑ t' n ' Diesto Anaerobic Ana If applicable to alternative performed (Class A or Class B) complete the following monito ing data: Allowable Level Pathogen Density Number of Frequency Sample Analytical Excee- of Tech - Parameter in Sludge Minimum Geo. Mean Maximum.Units dences Anal sis Type niclue 2x10tothe 6th power WN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per 2ram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 WN per 4 (in lieu of fecal grams total solid coliform) (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 21 Option 2 ❑Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were pe rformed rmed O CERTIFICATION STATEMENT (please check the appropriate statement) 0 " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) /G em - 3 17 Signature of Preparer Date Signature of Land Applier (if applicable) DENR FORM RF (5/2003) Date ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Archie Elledge WWTP NPDES Number: Monitoring Period: From 3/1/2014 To 3/31/2014 WQ0000094 NC00037834 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ® Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ a Bet Ray ❑ a Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ® Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion I.❑ ' es tron ❑ Anaerobic Dr If applicable to alternative performed (Class A or Class B) complete the following monito ing data: en Patho Density Number o requency Sample Analytical Allowable Level g Excee- of p Tech - Parameter in Sludge inim Geo. Meanaxim Units dences Analvsis Type nioue 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per ram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 NON per 4 (in lieu of fecal grams total solid coliform) I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 11 Option 2 El Option 3 ❑ Option 4 ❑ Option 5 El Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ re No vector attraction reduction options we per formed ed El CERTIFICATION STATEMENT (please check the appropriate statement) ® "1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) . &�wz �;W. 4�Leg I - yam/ Signature of Preparer T Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Archie Elledge WWTP NPDES Number: NC00037834 Monitoring Period: From 4/1/2014 To 4/30/2014 D.,4-r.,,,.e„ uoA,,..+;n„ ran rFR - Please indicate level achieved and alternative performed: - ------a-- --- - Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Be y a Ra Gamin ❑ Y ization Pasteun ❑ Pasteur Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ es 1 ' honc D Anaerobic g If applicable to alternative performed (Class A or Class B) complete the following monito ing data: Number oreq Allowable Level Pathogen Density uency Sample Ana ytica Excee- of Tech - Parameter in Sludge Minimum Geo. Mean Maximum Units deuces Analysis Typenigue —Tx 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU Per eram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 NTN per 4 (in lieu of fecal grams total solid coliform) (dry weight) Vpr+nr A+trnrtinn Reduction (40 CFR 503.33) - Please indicate option periormect: Option 1 ^0 Option 2 ElOption 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 El Option 8 ❑ Option 9 ❑ Option 10 f ❑ ' ' ' ' ' No vector attraction reduction options were pe rformed rm ed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Prepp�arer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) /✓�/ %??• ( O.IA s/ate/r Signature of Preparer 0 Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Archie Elledge WWTP NPDES Number: NC00037834 Monitoring Period: From 5/1/2014 To 5/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 . ❑ Alternative 3 ❑ ..................:..:.:.: Alternative 4❑ Alternative 5 [3 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 0 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta❑ Gamma Ray ❑" zation ❑ Pasteurization, Class B: Alternative 1 ❑ Alternative 2' 21 1 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ is Dr ge stro n Anaerobic If applicable to alternative performed (Class A or Class'B) complete the follow' g monito ing data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- deuces requency of Anal sis Sample TypeWoue Analytical Tech - Minimurr Geo. Mean Maxim Units Fecal Coliform 2x 10tothe 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per eram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 211 Option 2 ❑ 7077ion 3 ❑ Option 4 ❑ 1 Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ e i No vector attraction reduction options were performed ❑ erfor CERTIFICATION STATEMENT (please check the appropriate statement) 0 " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system- designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) 9i 1-6 /'Y i Signature of Preparer Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Archie Elledge WWTP NPDES Number: Monitoring Period: From 6/1/2014 To 6/30/2014 WQ0000094 NC00037834 Pathoeen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ only) indicate "Process to Further Reduce Pathogen If 'applicable to alternative performed (Class A s": ........... Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting , ❑ jAerobic Digestion ❑ " e 'on w Anaerobic Drsh If applicable to alternative performed (Class A or Class B) complete the following moinWAito ing data: Allowable Level Pathogen Density Number ot Prequency Sample Analytical Excee- of Tech - Parameter in Sludge MinimumGeo. MeanMaxi Units dences Analysis Type nioue 2 x 10 to the 6th power NTN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU pergram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 WN per 4 (in lieu of fecal grams total solid coliform) I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 Option 2 ❑Option 3 ❑ Option 4 ❑ Option 5 ❑ p p p P Option 10 ❑ O tion 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 No vector attraction reduction options were pe rformed ed CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, thatthe pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) DENR FORM RF (5/2003) Date ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM 'Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Archie Elledge WWTP NPDES Number: NC00037834 Monitoring Period: From 7/1/2014 To 7/31/2014 _ .An nVn cnz z1N _ Plaaea indicate level achieved and alternative performed: r QL11Vb'Gll 1\VUY�.�avu Class A: ��v �+ a�----•--/ - Altenative 1 ❑ alternative 2 ❑::T Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Ra Pasteurization ❑ aroma ❑ G Beta Ray ❑ Y Class B: Alternative 1 ❑ alternative 2 Q Alternative 3 ❑ If applicable to alternative performed (Class B only indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ composting ❑ Aerobic Digestion ❑ Anaerobic Di estion❑ If applicable to alternative performed (Class A or Class B) complete the following in OnWito ing data: Patho Allowable Level g'Excee- n Densityum er o requency Sample Analytical of Tech - Parameter in Sludge N4inimurr Geo. Me .. nMaxhhurr Units dences Analysis Type nicue -Tx 10 to the 6th power MPN per gram of total solids or 2 x 10 to ;Fecal Coliform the 6th power ... _ _ .. CFU per gram of 10oo mpn per gram of total solid (dry weight) Salmonella bacteria 3 WN per 4 '(in lieu of fecal grams total solid coliform) (dry wei ht Vector Attraction Reduction (40 CFR 503.33) Ply ase,indicate option performed: Option 1 © Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ ...... •. •. •.. •... •. •... . Option 6 [3 Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ :`•: ': ::::: ' :: ector attraction reduction o Nov tions were performgd P CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the�l pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation whyY you have not met one or both of the -requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified persorm f�1 properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for alse certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date _Klm rr+nne nr icinnnn% ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Archie Elledge WWTP NPDES Number: Monitoring Period: From 8/1/2014 To 8/31/2014 WQ0000094 NC00037834 1D.,+i6_"n„ RPrinetion (40 CFR 503.32) - Please indicate level achieved and alternative performed: 1 RILLV�vaa a�va. �.�.��� Class A: t •— -- -- — -- -- - i Alternative 'l ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ ::::: If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization r7zation ❑ '' ``.` Class B: Alternative 10, Alternative 2 21 Alternative 3 ❑ :: ': If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ I Air Drying ❑ I composting ❑ Aerobic Digestion ❑ ges tron r is ' D Anaerobic If applicable to alternative performed (Class A or Class B) complete the following monito ing data: Allowable Level Pathogen Density um er orequencyAnalytical Sample Excee- of Tech - Parameter in Sludge Nfinim Geo. Mean axim Units dences Anal sis Type ni u 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU ber gram of = . 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) . (dry weight) VPotor Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were per formed ed CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) ;? I l Signature of Preparer Date Signature of Land Applier (if applicable) Date ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Archie Elledge WWTP NPDES Number: Monitoring Period: From 9/1/2014 To 9/30/2014 WQ0000094 NC00037834 Pa+hnaPn RPrinrtinn (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ . Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermoplulic ❑ Beta Ray ❑ a na Ra G mt ❑ Y Pasteurization ❑ Class B: Alternative 1® Alternative 2 ® Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ gestionR. e tton "s An a erobic Di If applicable to alternative performed (Class A or Class B) complete the following monitoring data: o req Allowable Level Pathogen Density Numberuency Sample Analytical Excee- of Tech - Parameter in Sludge inimu Geo. MeanMaximut Units dences Analysis Type niaue 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per ram of 1000 mpn per._ -- -_- = gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 L] (in lieu of fecal grams total solid coliform). (dry weight) _ - I I Vertnr Attrnrtinn Reductinn (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ Option 2 ❑Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 Cl Option 7 ❑ Option 8 El Option 9 ❑ Option 10 ® {: ::::::::::::::::. No vector attraction reduction options were pe rformed rrrt ed CERTIFICATION STATEMENT (please check the appropriate statement) Q "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of -the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date nr�in r�n�n nr ir_�nnnn� ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Archie Elledge WWTP NPDES Number: Monitoring Period: From 10/1/2014 To 10/31/2014 WQ0000094 NC00037834 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Ray El Gamma Ray P as tou iationBeto ElClass B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ omposting ❑ 1 Aerobic Digestion ❑ AnaerobicDi estion ❑ If applicable to alternative erformed (Class A or Class B) complete the folio'—w Monitorin data: um er o requency a yttca Allowable Level Pathogen Density Sample Excee- of Tech - Parameter in Sludge inim Geo. Mean Maxim Units dences Anal sis Type nioue —Tx 10 to the 6th power MPN per gram of total .solids or 2 x 10 to Fecal Coliform the 6th power CFU Ver ram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) (dryeight) Veetnr Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 Option 2 ❑ I Option 3 ❑ Option 4 ❑ Option 5 ❑ ..•.•.•.•.............•.,.....•...,.., Option 6 ❑ Option 7 ❑Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were pe rformed rme d ❑ CERTIFICATION STATEMENT (please check the appropriate statement) O "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of.law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) /LCuy %�% L/ it4Qv�f, Signature of Preparer 0. Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Archie Elledge WWTP NPDES Number: Monitoring Period: From 11/1/2014 To 11/30/2014 WQ0000094 NC00037834 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑.......... ........... Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ElThermophilic ❑ :::::....:::::.. . Beta Ray ❑ Gamma Ray ❑ teu Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 21 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ ' 'c Drestron Anaerobic g If applicable to alternative performed (Class A o I r Class B) complete the following monitoring data: Number o requency Analytical Allowable Level Pathogen Density Sample Tech - Parameter Excee- of in Sludge Minimum Geo. Mean Maxirnur Units dences Analvsis Type ni u 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Colifolm. the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ ...,.... ....•.•.•. . Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 El Option 10 El:. <>:a e No vector attraction reduction options wer performe d ❑ CERTIFICATION STATEMENT (please check the appropriate statement) R1 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) /a- /6 Signature of Preparer 6 Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTIONFORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Archie Elledge WWTP NPDES Number: NC00037834 Monitoring Period: From 12/1/2014 To 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate 1PvP1 anti Class A: Alternative 1 ❑ Alternative 2 p Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ . If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":_ Compost 01 Heat Drying ❑ Heat Treatment El L Thermoplulic ❑ Beta Ray❑ Gamma Ray ❑ Pasteurization ' ❑ Class B: Alternative 1 ❑ Alternative 2 p Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Ihying ❑ CompostiEE ❑ Aerobic Digestion ❑ An aero ' bic D'g e t' n t s to ❑ If applicable to alternative erfor med Class A of Class B) complete the fol pp R ( lowing monito -ing data: - Parameter Allowable Level Pathogen Density Number ot Frequency Sample Analytical inim Geo. Mean Maxi mui Units in Sludge g Excee- dences of Anal sis Type Tech- 2 x 10 to the 6th nioue power MPN per gram of total solids or 2 x 10 to :Fecal Colifolm. the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 IVIPN per 4 (in lieu of fecal grams total solid coliform) (dry weight v ecLor attraction Keduction (40 UYK 503.33) - Please indicate option nerfnt•mPd- Option 1. 211 Option 2 ❑ Option 3 ❑ Option 4 ❑ t7ntinn 5 El r Option 6 ❑ Option 7 ❑ I Option 8 ❑ Option 9 ❑. (apt [on 10 El No vector attraction reduction er were options o ti p performed ❑ &-r'72T1r_VYi-ATri-%xT CTATT1TirWXTm i__I 1AAl Iyx1l1\ 1 1pica,C -1—K tiie appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor .Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Muddy Creek WWTP NPDES Number: Monitoring Period: From 1/1/2014 To 1/31/2014 WQ0000094 NCO050342 u r.,.,.e„ noa,,..*;.,., tAn rFR sn1_121- Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray El teurization Paseurrzation ❑ Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ is D r estr on 2 Anaerobic If applicable to alternative performed (Class A or Class B) complete the following monito ing data: um er o Frequency Analytical Allowable Level Pathogen Density Sample Excee- of Tech - Parameter in Sludge MinimumGeo. Meanaxim Units deuces Anal sis Type nkfue 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per eram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 WN per 4 (in lieu of fecal grams total solid coliform) I (dry weight) xi—+nr A++rartinn iPpanetinn (46 CFR 503.33) - Please indicate option performea: Option 1 0 Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were per formed ed CERTIFICATION STATEMENT (please check the appropriate statement) Rl "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) xyzu.�-- /a s/ Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Muddy Creek WWTP NPDES Number: Monitoring Period: From 2/1/2014 To 2/28/2014 WQ0000094 NCO050342 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray Gamma Ray ❑ Pasteurization ation ❑ Class B: Alternative 1 ❑ Alternative 2 21 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic D r estion :..:.:....:......... ................... . te the followin monitorin data: If applicable to alternative performed (ClasssAA or Class B) complete um er o requency Analytical Allowable LevelPathogen Density Sample Tech Parameter Excee- of - in Sludge Minimum Geo. Mean MaximUnits deuces Anal sis Type ni u 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) Ary weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 R1 Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑Option 8 ❑ Option 9 ❑ Option 10 ❑ ' w No vector attraction reduction options were performe d ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ® "I'certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) V71i Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) f _r ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Muddy Creek WWTP NPDES Number: Monitoring Period: From 3/1/2014 To 3/31/2014 WQ0000094 NCO050342 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 El If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens' Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ y Gamma Ra G ElB ation Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting,❑ Aerobic Digestion ❑ - brc Dr esh on w Anaerobic g If applicable to alternative performed (Class A or Class B) complete the following monitorin data: . Allowable Level Pathogen Density Number o r'quency SampleAnalytical Excee- of Tech - Parameter in Sludge MinimumGeo. Meanaxim Units deuces Anal sis Type nigue 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU er 2ram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 El jOption2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ .•.......,.•.:.....:.:.:.•.•.....•...• Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ :;:::::: No vector attraction reduction options were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement). 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction ,requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) a Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Muddy Creek WWTP NPDES Number: NCO050342 Monitoring Period: From 4/1/2014 To 4/30/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens': Compost 01 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Y a Gamma Ra Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 21 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com ostin ❑ Aerobic Digestion ❑ Anaerobic Di estion w If applicable to alternative performed (Class A or Class B) complete the following moindito ing data: Number o Frequency Allowable Level Pathogen Density SampleAnalytical Tech Parameter Excee- of - in Sludge Minimum Geo. Mean axim Units deuces Anal sis Type nioue 2 x 10 to the 6th power WN per gram of total solids or 2 x 10 to Fecal Colifoim the 6th power CFU ver gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 WN per 4 (in lieu of fecal grams total solid colifonn) (dry wei ht Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 Li Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ were pe rformed ❑ options No vector attraction reduction p CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Muddy Creek WWTP NPDES Number: Monitoring Period: From 5/1/2014 To 5/31/2014 WQ0000094 NCO050342 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to' alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray❑ a Ray Gamin ❑ 0 eu 'zati n Past i7 ❑ Class B: Alternative 10 Alternative 2 1] Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ is D t estion W Anaerobic If applicable to alternative performed (Class A or Class B) complete the following monflito ing data: Number o requency Analytical Allowable Level Pathogen Density Sample Excee- of Tech - Parameter in Sludge Minimum Geo. Mean axim Units dences Anal sis Typenioue 2 x 10 to the 6th power WN per gram of total solids or 2 x 10 to Fecal Coliforrn the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 iVIPN per 4 (in lieu of fecal grams total solid coliform) (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 Option 2 ❑ Fc7tion 3 ❑ Option 4 ❑ Option 5 ❑ ........................ ... Option 6 0 Option 7 ❑ 1 Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were pe rformed tined CERTIFICATION STATEMENT (please check the appropriate statement) 0 " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 .and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) -aa,41,a 61i7 Signature of Preparer Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Muddy, Creek WWTP NPDES Number: NCO050342 Monitoring Period: From 6/1/2014 To 6/30/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 413 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": :.........••• Compost Li Heat Drying El Heat Treatment ❑ Thermophilic El:::::::::::::::::::: Beta Ray ❑ Y R Ray Gamma ❑ ization- asteut7 P ❑ Class B: Alternative 10-7— Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization [3. Air Drying ❑ Composting ❑ Aerobic Digestion ❑ is D t e shonW Anaerobic If applicable to alternative erformed (Class A or Class B) complete the follow* n monitorin data: um er o requency. Analytical Allowable Level Pathogen Density .Sample Tech - Parameter Excee- of in Sludge MinimumGeo. Meanaxim Units dences Anal sis Typenicue 2 x 10 to the 6th power NTN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per aram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 NTN per 4 (in lieu of fecal grams total solid coliform) (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5' ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ :•..1 No vector attraction reduction options were pe rformed rmed CERTIFICATION STATEMENT (please check the appropriate statement) 21 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND Facility Name: City of Winston WWTP Name: Muddy Creek I Monitoring Period: From 7/1/2014 Pathogen Reduction (40 CFR 503.32) - Please it Class A: Alternative 1 ❑ Alternative 40 If applicable to alternative performed (Class A Compost ❑ Heat Drying ❑ Beta Ray ❑ Gamma Ray ❑ Class B: Alternative 1 ❑ If applicable to alternative performed (Class B Lime Stabilization ❑ Air Drying ❑ on Anaerobic Dr estr Ana g ::................... . If applicable to alternative performed (Class A Allowable Level Path Parameter in Sludge Minimurr Geo. 1 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power . 1000 mpn per gram of total solid Salmonella bacteria I 3 MPN per 4 (in lieu of fecal grams total solid Vector Attraction Reduction (40 CFR 503.33) - P Option 1 0 Option 2 ❑ I Option 3 ❑ Option 6 ❑ I Option 7 ❑ Option 8 ❑ No vector attraction reduction options were perforn CERTIFICATION STATEMENT (please check R1 "I certify, under penalty of law, that th attraction reduction requirement in 40 ❑ "1 certify, under penalty of law, that tl attraction reduction requirement in 40 this statement attach an explanation w] "This determination has been made under my di system designed to ensure that qualified personn used to determine that the pathogen and vector, am aware that there are significant penalties for Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) - G' Signature of Preparer Date FOR ATTRACTION REDUCTION FORM Clem Permit Number: WQ0000094 TTP NPDES Number: NCO050342 _ To 7/31/2014 -ate level achieved and alternative performed: klternative 2 ❑ Alternative 3 ❑ klternative 5 ❑ Alternative 6 ❑ ly) indicate "Process to Further Reduce Pathogens": eat Treatment ❑ Thermophilic ❑ tion 'a ❑ as t eunz Alternative 2 ❑ Alternative 3 ❑ ::::::::::::::::::.. . ly) indicate "Process to Significantly Reduce Pathogens": Composting ❑ 1 Aerobic Digestion ❑ Class B) complete the followin monitorin data: m Density, Number of FrequencySample Analytical Excee- of Tech- i axim Units deuces Analysis Type nioue ease indicate option performed: Option 4 ❑ 10ptioD 5 ❑ Option 9 ❑ 10ption 10 ❑' �d ❑ ..:::: :he appropriate statement) pathogen requirements in 40 CFR 503.32 and the vector "-FR 503.33 have been met." e pathogen requirements in 40 CFR 503.32 and the vector --FR 503.33 have not been met." (Please note if you check y you have not met one or both of the requirements.). -ection and supervision in accordance with the 4 properly gather and evaluate the information ttraction reduction requirements have been met. I false certification including fine and imprisonment." Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date nrnin ranee or i9:innn'3\ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Muddy Creek WWTP NPDES Number: Monitoring Period: From 8/1/2014 To 8/31/2014 WQ0000094 NC0050342 Patho en Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: g Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ ........... Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ If 'applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermoplulic ❑ Beta Ray ❑ Gamma Ray steurization Pateurrzation ❑ Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 El;:;:::::::; If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ ............... obi rionc Dies Anaerobic g If applicable to alternative performed Class A or Class B complete the following monito ing data: Number o Sample requencyAnalytical Allowable Level Pathogen Density Excee- of Tech - Parameter in Sludge Minimum Geo. Mean Maxi mui Units deuces Anal sis Type niciue 2 x 10 to the 6th , power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per gram of l00o mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) (dry wei ht x7—+..r A#rar+inn Ro inrtinn /4(1 CYR 503-331- Please indicate option performed: Option 1 Option 2 ❑ 1 Option 3 10ption 4 ❑ Option 5 L7 Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 [3Option lO ❑ No vector attraction reduction options were pe rformed rm ed CERTIFICATION STATEMENT (please check the appropriate statement) Q "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement`in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information. - used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) I Signature of Preparer Date Signature of Land Applier (if applicable) n[fnio rnonn or Date ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Muddy Creek WWTP NPDES Number: Monitoring Period: From 9/1/2014 To 9/30/2014 WQ0000094 NCO050342 n,...t,ran CVP Sn3321- Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4® Alternative 5 ❑ Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray❑ Gamrd a Ray Y tion za r Pasteurization ❑ Class B: Alternative 1® Alternative 2 ® Alternative 3 ® If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com osting ❑ jAerobic Digestion ❑ t on ' es i Rl bic Dg e r Anaero r If applicable to alternative performed (Class A or Class B) complete the forllo ling goencyr1Sa data: er of r na ytica Allowable Level Pathogen Density ple Excee- of Tech - Parameter in Sludge Minimurr Geo. Mean Maximurr Units dences Anal sis Type ni ue 2x 10tothe 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN .per 4 (in lieu of fecal grams total solid coliform) I (dry weight) 17,...b..... A " noalinfinn yen ('TM - Please indicate option geriormect: ♦ GL:LVI 11LL1KV LIV LJ- Option 1 211 Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option , ®Option 8 ® Option 9 ❑ Option 10 El�::::::::: ::: : : No vector attraction reduction options were pe rformed e d ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Q "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information - used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) ;41, may Signature of Preparer Date Signature of Land Applier (if applicable) ncnio rnonn or ir»nnON Date ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WWTP Name: Muddy Creek WWTP NPDES Number: Monitoring Period: From 110/1/2014 To 10/31/2014 WQ0000094 NCO050342 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 © Alternative 3 ❑ Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": ....:.:.:.:.:.:. Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermop hilic ❑ . Beta Ray ❑ Gamma RaY ' ❑ Pasteurization rizah on ❑ Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Com ostin ❑ jAerobic Digestion ❑ :.:<.:.:;.:.::.;:.:;.>:.:.>::.:::;:.:::.;:.:<::::.:::.:.:..:.....,.:.....:..::.:..::.::.:..:...:.::.:::,:..................................... . ' 'c DrestronW erobr Anaerobic g If applicable to alternative performed (Class A or Class B) complete the following monito ing data: en Patho Density Number o requency Sample Analytical Allowable Level g �' Excee- of p Tech - Parameter in Sludge inim Geo. Meanaxim Units dences Anal sis Type nioue 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per aram of 1000 mpn per gram of total solid dry weight) Salmonella bacteria 3 NUN per 4 (in lieu of fecal grams total solid coliform) I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 Option 2 ❑ I Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ 'Option 9 ❑ Option 10 ❑ :;:::: No vector attraction reduction options were pe rformed ed CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title ,(type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer 0 Date Signature of Land Applier (if applicable) DENR FORM RF (5/2003) Date ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQ0000094 WWTP Name: Muddy Creek WWTP NPDES Number: NCO050342 Monitoring Period: From 11/1/2014 To 11/30/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and .alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ ••• ••...:.;:.:.::. . . . ....... Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ ..... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hilic ❑ Beta Ray❑ G aroma Ray teui7z ation Pas ❑ Class B: Alternative 1 ❑ Alternative 2 0 Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying ❑_ _ _ Composting ❑ jAerobic Digestion ❑ ' W robic Di estio n Anaerobic • If applicable to alternative performed (Class A or Class B) complete the following monito ing data• Allowable Level Pathogen Density Number ot Erequency Sample Analytical Excee- of Tech - Parameter in Sludge nim Geo. Meanaxim Units deuces Analvsis Type nicue 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per am of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 (in lieu of fecal grams total solid coliform) I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 0 10ption2 ❑Option 3 ❑ Option 4 ❑ 17tion 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were pe rformed formed CERTIFICATION STATEMENT (please check the appropriate.statement) 0 " l[ certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty 'of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you .check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for,false certification including fine and imprisonment." Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Signature of Preparer Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date DENR FORM RF (512003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: City of Winston-Salem Permit Number: WQOOOOO : 9 . 4 WWTP Name: Muddy Creek WWTP NPDES Number: NC0-0-50342 MonitoringPeriod: V rom I /-/ I U 1,4 - I To 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 111 Alternative 2 ❑ Alternative 3 [1 --T- Alternative 40 Alternative 5 13 • Alternative 6 ❑ If applicable to alternative Performed (Class A only) indicate "Process to Further Reduce Pathos Compost El Heat Drying El Heat Treatment El Thermopl-fflic [I Beta Ray 13 Gamma Ray [I Pasteurization❑ Class B: - Alternative 01 —Altel-natiTe-2 Cj Alternative . 3 [1 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce P: Lime Stabilization ❑ ... Air .. Drying 11 Composting El Aerobic Dipestic Anaerobic Digestion2l If applicable to alternative erfo Parameter Allowable Level in Sludge N 2 x 10 to the-6th power MPN per gram of total solids or 2 x 10 to Fecal Colifotm . the 6th power ed (Class A or Class B) Pathogen Density .MWA Geo. Mean[Maxirni complete the fo Excee- UrlltS A-- logens": monito ing data: requency Sample Analytical of Tech -- final sis Type nl 1000 mpli per ...... . ..... gram of total solid Sdhnonella bacteria .3 N per 4 '(in lieu of fecal grams s total solid i. coliform) (dry weiqlit) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 Cl1 Option 2 111 Option 3 D Option 4 El Option 5 ❑ Option 6 11 IOption 7 111 Option 8 D 1Option 9 11 Option 10 ❑ .. ........ No vector attraction reduction options were performed [I XX 'CERTIFICATION STATEMENT (please check the appropriate statement) 0. "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." E3 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503-32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note ifyou check this statement attach an explanation why you have not met one or both of the requirements.) ."This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information' used to determine that the pathogen and vector attraction reduction requirements have been met. 1* ram aware that there are significant penalties for false certification including fine and imprisonment." .Bruce M. Casey, Utility Plant Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or prip.l.). IdU4e.e Pre parer of Preparer Date Signature of Land Applier (if applicable) Date City of Winston-Salem 2014 Class A Biosolids Monitoring Report Section 10. Pathogen and Vector Attraction Reduction Summaries & Operational Data (Archie Elledge WWTP; Muddy Creek WWTP) ARCHIE ELLEDGE WWTP NPDES Permit # NCO037834 2014 Pathogen and Vector Attraction Reduction Summary and Operational Data Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Archie Elledge WWTP NPDES Permit 4 NC0037834 2014 Compliance Summary Pathogen Reduction PSRP Data for Class B Residuals Anaerobic Digester System Month * * Primary Digester SRT(days)* Monthly Average Temp. °F Monthly Average January 39 97 February 35 96 March 32 96 April 29 97 May 32 98 June 34 97 July 34 97 August 47 97 September 46 98 October 65 97 November 45 97 December 73 97 * SRT = Solids Retention Time; based on % Total Solids ** Bi-monthly monitoring is required but is actually done on a monthly basis. Page 2 ARCME ELLEDGE WWTP Pathogen Reduction NPDES Permit # NC0037834 Shown in the above summary on Page 1 are the Digester SRT (or MCRT) values calculated from %Total Solids. SRTs reported in this summary are the monthly averages of daily values since daily values fluctuate so greatly from day to day. An example of the SRT calculation is shown below. Please see attached the January 2014 LAND APPLIED BIOSOLIDS REPORT, Page 4, for the Archie Elledge WWTP from which the daily data for January 1 is taken for the example calculation below. The Primary Digesters at the Archie Elledge Plant are Digesters 1, 2, 3, 4, 5 and 8. Any estimated data or qualified data is marked as such in these reports. Also, any estimates are not included in the monthly average shown on the previous Page 1. Please find each month's Digester Temperature records (Page 2) attached behind its respective Page 4 report. FORMULA:. [Primary Digester Volume x 8.34 x Primary Digester Transfer %Total Solids] (Pounds of solids in Primary Digesters) [Transfer %Total Solids x 8.34 x Primary Transfer Flow] (Pounds of solids being transferred to Blending Tanks) = PriDigSRT (Days %TS) FROM ATTACHED DATA SHEETS for January 1, 2014: [[PriDigVOL (MG)] x 8.34 x [Trans%TS (%)]] [[Trans%TS (%)] x 8.34 x [PrTranFlo (TGD)/1000]] or [7.568 x 8.34 x 0.01821 = 1.1487 = 25.64 or [0.0182 x 8.34 x (294.9/1000)] 0.0448 as shown on the report, 26 days SRT --------------------------------------------------------------------------------- 02/25/2014 09:38:42 AM LAND APPLIED BIOSOLIDS EXAMPLE ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 111 /2014 to 1 /31/2014 Page 4 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 VolFrac 11+18+GB 32 DTrVoFrac % 419 PDig%VSR % 718 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 1/1/2014 0.8241 0.8163 0.8196 67.58 54 26 55 7.568 1.82 294.9 1l2/2014 1 /3/2014 0.8292 0.8119 0.8127 0.8129 0.8209 0.8124 68.75 69.32 52 48 36 35 55 55 7.568 7.568 1.76 1.76 212.1 216.8 1 /4/2014 0.8408 0.8203 0.8306 69.10 54 30 54 7.568 1.78 248.3 1/5/2014 0.8370 0.8231 0.8301 68.68 55 62 55 7.568 1.82 122.E 1 /6/2014 0.8221 0.8226 0.8224 69.32 51 34 55 7.568 1.76 221.2 1/7/2014 0.8264 0.8652 0.8726 0.8281 0.8333 0.8381 0.8272 0.8492 0.8541 69.10 71.35 68.48 53 56 63 25 77 68 55 55 57 7.568 7.568 7.568 1.78 1.78 1.84 301.9 97.9 111.0 1 /8/2014 1 /9/2014 1/10/2014 C8074 0.8416 0.8259 68.89 53 38 57 7.568 1.80 200.3 1 /11 /2014 1/12/2014 3/2014 1/14/2014 0.7889 0.6255 0.7768 0,7934 0.7865 0.7957 0.8277 0.8418 0.8134 0.7953 0.7953 0.7990 0.7956 0.8073 0.6255 0.7975 0.7946 0.7918 0.7976 0.8098 70.37 68.47 66.67 66.85 67.18 66.86 67.06 43 -30 49 48 46 49 52 32 36 83 30 26 27 29 57 56 58 57 57 57 56 7.568 7.568 7.568 7.568 7.568 7.568 7.568 1.89 2.03 1.77 1.78 1.95 1.75 1.70 2 212..2 91.1 250.1 291.4 281.2 260.9 1/15/2014 1/16/2014 1117/2014 1/18/2014 0.82 99 0.8275 0.8009 0.8044 0.8119 0.8143 66.47 66.67 54 54 31 30 54 54 7.568 7.568 1.73 1.71 240.4 252.5 1/19/2014 0.7967 0.79 66 0.8164 0.8097 0.8106 0.8091 0.8036 68015 0.8123 66.67 67.66 66.28 51 48 55 27 57 23 50 50 50 7,568 7.568 7.568 1.71 1.67 1.72 279.1 133.E 329.4 1/20/2014 1/21/2014 1 /22/2014 0.8309 0.8395 0.8728 0.8708 0.8788 0.8153 0.8182 0.8255 0.8276 0.8261 0.8224 0.8277 0.8450 0.8450 0.8477 67.06 67.05 67.26 67.63 67.66 56 58 62 62 62 24 38 34 34 30 49 48 47 47 47 7.568 7.568 7.568 7.568 7.568 1.70 1.76 1.68 1. 1.67 317.3 198.E 223.E 220.1 250.E 1 /23/2014 1/24/2014 1/25/2014 1/26/2014 1/27/2014 /03/2014 0.8444 0.8333 0.8384 68.07 59 40 38 7.568 1.66 189.5 9/2014 0.8391 0.8418 1 0.8406 68.07 60 30 37 7.568 1.66 256.4 1 /30/2014 0.8452 0.8352 0.8395 69.18 57 86 39 7.568 1.59 88.1 1 /31 /2014 0.8452 0.8384 0.8414 68.52 59 22 39 7.568 1.62 346.2 Total 25.4561 24.5856 25.3076 2,108.28 1,594 1,200 1,603 234.608 54.38 6,975.2 Samples 31 30 31 31 31 31 31 31 31 31 Averaae 0.8212 0.8195 0.8164 68.01 51 39 52 7.568 1.75 225.0 Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Archie Elledge WWTP NPDES Permit # NCO037834 2014 Compliance Summary Vector Attraction Reduction Requirements for Class B Residuals Compliance determination by calculation of Volatile Solids Reduction (VSR) across the Anaerobic Digesters as the treatment system. Calculated %VSR (3 8% Minimum) Monthly Average VAR Option -1 Month * Prim Digester System January 51 February 56 March 50 April 46 May 42 June 42 ** July 38 August 44 September 45 October 46 November 45 December 47 * Bi-monthly monitoring is required but is actually done on a monthly basis. ** Beginning in June, 2014, there is an offset of time factored in regarding digester solids retention time (or MCRT). A given month's %VSR is now calculated using the previous month's SRT average. See page 2 of this section for the formula used for the first 5 months of 2014, as well as the formula now used beginning in June of 2014. The equation used for calculating the above %VSRs is from the EPA White House Manual, Control of Pathogens and Vector Attraction in Sewage Sludge, Chapter 10 and Appendix C. Page 2 Archie Elledne WWTP Vector Attraction Reduction NPDES Permit # NCO037834 Data submitted in the chart on the previous Page 1 of this summary shows that the calculated monthly average Volatile Solids Reduction meets the minimum of 38% VSR requirement over the Primary Digester System at the Archie Elledge Plant for the year 2014. Volatile Solids Reduction (VSR) is calculated by the Van Kleeck equation using the digester feed and digester stabilized transfer sludge volatile fractions. While there was previously no offset necessary for digester Solids Retention Times (or MCRTs) due of the consistency with which these digesters were operated, upon in-house review, the City began in June of 2014 calculating one month's %VSR using the previous month's SRT average. This more accurately reflects current digester operations. Any data qualified by the lab is marked as such on data sheets. Also, in instances when a daily sample was not collected for %Volatile Solids analysis of Transfer (`Trans') sludges, an estimated value was used along with actual flows for that day in order to calculate treatment in the digesters. Any estimated values are marked as such on attached data sheets. However, the monthly average values (shown on the previous Page 1) were calculated excluding this estimated data in order to certify compliance. The values for January 1, 2014 from the attached LAND APPLIED BIOSOLIDS report Page 4 are used in the example equation below. This is the formula used for the period of Jan. — May, 2014. The heading `VolFrac 11+18+GB' refers to the VolatileTraction of the digester feed samples; the heading `DTrVoFrac' refers to the Volatile Fraction of the transfer digester samples. The calculated Percent Volatile Solids Reduction is indicated by the heading `PDig%VSR (%)'. FORMULA January — May, 2014: [VolFrac 11 + 18 + GB] - [DTrVoFrac/100] (Feed) (Transfer) = PDigVSR (%) [VolFrac 1 l+ 18 + GB] - [(VolFrac 11 + 18 + GB) x (DTrVoFrac/100)] (Feed)- (Feed) (Transfer) FROM ATTACHED DATA SHEETS for January 1, 2014: 0.8196 - 0.6758 = 0.1438 = 0.5412 or as shown on the report, 54% VSR 0.8196 - (0.8196 x 0.6758) 0.2657 See on the attached LAND APPLIED BIOSOLIDS report Page 4, June 1, 2014, for the current method of calculating %VSR. The new heading of "Feed Vol Frac 30 day mavg" is the Feed Volatile Fraction 30 day moving average. See monthly averages June — Dec. in the chart on the previous Page 1 of this summary and attached daily data. FORMULA June —December, 20'14: [Feed Vol Frac 30 day mavg] - [DTrVoFrac/100] (Feed) (Transfer) = PDigVSR (%) [Feed Vol Frac 30 day mavg] - [(Feed Vol Frac 30 day mavg) x (DTrVoFrac/100)] (Feed) (Feed) (Transfer) FROM ATTACHED DATA SHEETS for June 1, 2014: 0.8048 - 0.6842 = 0.1206 = 0.4744 or as shown on the report, 47% VSR 0.8048 - (0.8048 x 0.6842) 0.2542 Van Kleeck Equation used: %VS Reduction = [%VS (Feed)] - [%VS (Stabilized)] [%VS (Feed)] - [%VS (Feed) x %VS (Stabilized)] %VS (Feed) = Volatile fraction of raw and thickened sludges fed to primary digesters %VS (Transfer ) = Volatile fraction of stabilized sludge transferred from primary digesters EXAMPLE 02/25/2014 02:23:39 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 1/1/2014 to 1/31/2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 VolFrac 11+18+GB 32 DTrVoFrac % 419 PDig%VSR % 718 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 1/1/2014 0.8241 0.8163 0.8196 67.58 54 26 55 7.568 1.82 294.9 1/2/2014 0.8292 0.8127 0.8209 68.75 52 36 55 7.568 1.76 212.1 1 /3/2014 0.8119 0.8129 0.8124 69.32 48 35 55 7.568 1.76 216.8 1 /4/2014 0.8408 0.82 33 0.8306 69.10 54 30 54 7.568 1.78 248.3 1 /5/2014 0.8370 0.8231 0.8301 68.68 55 62 55 7.568 1.82 122.6 1 /6/2014 0.8221 0.8226 0.8224 69.32 51 34 55 7.568 1.76 221.2 1 /7/2014 0.8264 0.8281 0.8272 69.10 53 25 55 7.568 1.78 301.9 1/8/2014 0.8652 0.8333 0.8492 71.35 56 77 55 7.568 1.78 97.9 1 /9/2014 0.8726 0.8381 0.8541 68.48 63 68 57 7.568 1.84 111.0 1/10/2014 0.8074 0.8416 0.8259 68.89 53 38 57 7.568 1.80 200.3 1 /11 /2014 0.7889 0.8418 0.8073 70.37 43 32 57 7.568 1.89 235.9 1/12/2014 0.6255 0.6255 68.47 -30 36 56 7.568 2.03 212.2 1/13/2 114 0.7768 0.8134 0.7975 66.67 49 83 58 7.568 1 1.77 91.1 1 /14/2014 0.7934 0.7953 0.7946 66.85 48 30 57 7.568 1.78 250.1 1/15/2014 0. 7865 0.7953 0.7918 67.18 46 26 57 7.568 1.95 291.4 1/16/2014 0.7957 0.7990 0.7976 66.86 49 27 57 7.568 1.75 281.2 1/17/2014 0.8277 0.7956 0.8098 67.06 52 29 56 7.568 1.70 260.9 1 /18/2014 0.8269 0.8009 0.8119 66.47 54 31 54 7.568 1.73 240.4 1 /19/2014 0.8275 0.8044 0.8143 66.67 54 30 54 7.568 1.71 252.5 1/20/2014 0.7967 0.8097 0.8036 66.67 51 27 50 7.568 1.71 279.1 1/21/2014 0.7906 0.8106 0.8015 67.66 48 57 50 7.568 1.67 133.6 1/22/2014 0.8164 68091 0.8123 66,28 55 23 50 7.568 1.72 329.4 1 /23/2014 0.8309 0.8153 0.8224 67.06 56 24 49 7.568 1.70 317.3 1/24/2014 0.8395 0.8182 0.8277 67.05 58 38 48 7.568 1.76 198.6 1 /25/2014 0.8728 0.8255 0.8450 67.26 62 34 47 7.568 1.68 223.6 1 /26/2014 0.67 88 0.8 776 0.8450 67.63 62 34 47 7.568 1.73 220.1 1/27/2014 0.8788 0.8261 0.8477 67.66 62 30 47 7.568 1.67 250.6 1/28/2014 0.8444 0.8333 0.8384 68.07 59 40 38 7.568 1.66 189.5 1 /29/2014 0.8391 0.8418 0.8406 68.07 60 30 37 7.568 1.66 256.4 1 /30/2014 0.8452 0.8352 0.8395 69.18 57 86 39 7.568 1.59 88.1 1 /31 /2614 0.8452 0.8384 0.8414 68.52 59 22 39 7.568 1.62 346.2 Total 25.4561 24.5856 25.3076 2,108.28 1,594 1,200 1.603 234.608 54.38 6,975.2 Samples 31 30 31 31 31 31 31 31 31 31 Average 0.8212 0.8195 0.8164 68.01 51 39 52 7.568 1.75 225.0 EXAMPLE 08/12/2014 03:39:56 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 6/1 /2014 6/30/2014 11 21 Feed DTrVoFrac PDig%VSR PriDigSRT PriDigSRT PriDig Trans ELL VolFrac VolFrac Vol Frac VOL %TS PrTranFlo 30 day ratio ratio Mavg % % Days %TS Days %TS MG % TGD Date 683 684 1320 419 1319 483 30 DAY V483 529 136 3" 6/1/2014 0.8019 0.7795 0.8048 68.42 47 23 32 7.568 2.09 335.0 6/2/2014 0.8192 0.7824 0.8046 70.21 43 57 33 7.568 1.88 132.7 6/3/2014 0.8045 0.7778 0.8038 69.47 44 21 33 7.568 1.90 359.2 6/4/2014 0.7845 0.7743 0.8025 69.57 44 25 33 7.568 1.84 298.4 6/5/2014 0.8250 0.7741 0.8022 69.57 44 29 33 7.568 1.84 257.4 6/6/2014 0.8137 0.7500 0.8015 68.68 46 22 32 7.568 1.82 344.3 6!7/2014 0.8307 0.7727 0.8012 33 7.568 0.0 6/8/2014 0.8784 0.7727 0.8015 32 7.568 0.0 6/9/2014 0.8101 0.7773 0.8007 32 7.568 0.0 6/10/2014 0.8055 0.7778 0.7993 70.06 41 86 34 7.568 1.77 88.1 6/11 /2014 0.8273 0.7778 0.7993 69.83 42 32 33 7.568 1.79 235.9 6/12/2014 0.7834 0.7656 0.7981 69.44 42 27 33 7.568 1.80 282.8 6/13/2014 0.8039 676 77 0.7967 69.19 43 38 33 7.568 1.85 198.4 6/14/2014 0.8151 0.7766 0.7966 68.51 44 37 33 7.568 1.81 _ 202.6 6/15/2 114 0.8315 0.7476 0.7962 68.98 43 29 33 7.568 1.87 257.4 6/16/2014 0.8253 0.7373 0.7951 69.19 42 28 33 7.568 1.85 270.0 6/17/2014 0.8300 0.7462 0.7938 69.02 42 39 33 7.568 1.84 194.2 6/18/2014 0.8438 0.7463 0.7927 69.73 40 23 32 7.568 1.85 328.7 6/19/2014 0.8078 0.7336 0.7911 68.72 42 31 32 7.568 1.79 245.5 6/20/2014 0.8295 0.7376 67910 69.57 40 29 32 7.568 1.84 265.3 6/21 /2014 0.8430 0.7368 0.7918 69.32 41 47 32 7.568 1.76 162.0 6/22/2014 0.8379 0.7331 0.7915 69.23 41 47 33 7.568 1.82 159.5 6123/2 114 0.8293 0.7276 0.7907 69.32 40 28 33 7.568 1.76 266.2 6/24/2014 0.8234 0.7423 0.7903 69.10 41 35 34 7.568 1.78 216.6 6/25/2014 0.8078 67381 0.7892 69.06 40 27 33 7.568 1.81 284.0 6/26/2014 0.8238 0.7413 0.7880 69.49 39 31 33 7.568 1.77 242.7 6/27/2014 0.8240 0.7431 0.7870 69.54 38 29 34 7.568 1.74 259.2 6/28/2014 0.8300 0.7343 0.7861 69.40 38 31 34 7.568 1.83 243.6 6/29/2014 0.8427 0.7413 0.7852 70.22 35 53 34 7.568 1.78 142.7 6/30/2014 0.8550 0.7390 0.7848 69.10 39 25 34 7.568 1.78 305.9 Total 24.6880 22.6509 23.8569 1,871.94 1,121 930 989 227.040 49.26 6,578.3 Samples 30 30 30 27 - 27 27 30 30 27 30 Averaqe 0.8229 0.7550 0.7952 69.33 42 34 33 7.568 1.82 219.3 02/24/2014 01:40:38 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 1/1/2014 to 1/31/2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 VOIFrac 11+18+GB 32 DTrVoFrac % 419 PDig%VSR % 718 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 1/1/2014 0.8241 0.8163 --------------- 0.8196 67.58 54 26 55 7.568 1.82 294.9 1/2/2014 0.8292 0.8127 0.8209 68.75 52 36 55 7.568 1.76 212.1 1/3/2014 0.8119 0.8129 0.8124 69.32 48 35 55 7.568 1.76 216.8 0.8408 0.8203 0.8306 69.10 54 30 54 7.568 1.78 248.3 014 0.8370 0.8231 0.8301 68.68 55 62 55 7.568 1.82 122.6 014 0.8221 0.8226 0.8224 69.32 51 34 55 7.5681.76 221.2 [1/4/2014 014 0.8264 0.8281 0.8272' 69.10 53* 25 55 7.568 1.78 301.9 014 0.8652 0.8333 0.8492 71.35 56 77 55 7.568 1.78 97.9 014 0.8726 0.8381 0.8541 68.48 63 68 57 7.568 1.84 111.0 /2014 0.8074 0.8416 0.8259 68.89 53 38 57 7.568 1.80 200.3 1 /11 /2 114 0.7889 0.8418 0.8073 70.37 43 32 57 7.568 1.89 235.9 1/12/2014 0.6255 0.6255 68.47 -30 36 56 7.568 2.03 212.2 1/13/2 114 0.7768 0.8134 0.7975 66.67 49 83 58 7.568 1.77 91.1 1 /14/2 114 0.7934 0.7953 0.7946 66.85 48 30 57 7.568 1.78 250.1 1/15/2014 0.7865 0.7953 0.7918 67.18 46 26 57 7.568 1.95 291.4 1 /16/2 114 0.7957 0.7990 0.7976 66.86 49 27 57 7.568 1.75 281.2 1 /17/2014 0.8277 0.7956 0.8098 67.06 52 29 56 7.568 1.70 260.9 1 /18/2014 0.8269 0.8009 0.8119 66.47 54 31 54 7.568 1.73 240.4 1/19/2014 0.8275 0.8044 0.8143 66.67 54 30 54 7.568 1.71 1 252.5. 1 /20/2014 0.7967 0.8097 0.8036 66.67 51 27 50 7.568 1.71 279.1 1/21/2014 0.7906 0.8106 0.8015 67.66 48 57 50 7.568 1.67 133.6 1/22/2014 0.8164 0.8091 0.8123 66.28 55 23 50 7.568 1.72 329.4 1 /23/2014 0.8309 0.8153 0.8224 67.06 56 24 49 7.568 1.70 317.3 1/24/2014 0.8395 0.8182 0.8277 1 67.05 58 38 48 7.568 1.76 198.6 1/25/2014 0.8728 0.8255 0.8450 67.26 62 34 47 7.568 1.68 223.6 1 /26/2014 0.8708 0.8276 0.8450 67.63 62 34 47 7.568 1.73 220.1 1/27/2014 0.8788 0.8261 0.8477 67.66 62 30 47 7.568 1.67 250.6 1 /28/2014 0.8444 0.8333 0.8384 68.07 59 40 38 7.568 1.66 189.5 1/29/2014 0.8391 0.8418 0.8406 68.07 60 30 37 7.568 1.66 256.4 1/30/2014 0.8452 0.8352 0.8395 69.18 57 86 39 7.568 1.59 88.1 [1/31l2014j 0.8452 0.8384 0.8414 68.52 59 22 39 7.568 1.62 346.2 Total 25.4561 2-1.7575 24.4804 2,108.28 1541 1,200 1,603 234.608 54.38 6,975.2 Samples 31 29 30. Average 0.8212 0.8192 0.81*60 * Estimate. 31 30 68.01 51 31 31 31 31 31 39 52 7.568 1.75 225.0 02/24/2014 01:40:35 PM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NC0037834 1/1/2014 to 1/31/2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 1 /1 /2014 99 96 97 96 98 97 1/2/2014 97 98 98 98 98 97 1/3/2014 96 100 99 99 99 97 1/4/2014 97 98 100 99 99 96 1/5/2014 99 97 99 98 98 96 1 /6/2014 99 98 98 97 97 96 1/7l2014 98 99 97 97 96 96 1 /8/2014 99 98 98 98 98 97 1/9/2014 98 98 100 100 97 97 1/10/2014 98 97 98 98 97 97 1/11/2014 96 98 96 96 97 96 1/12/2 114 97 97 96 96 97 97 1 /13/2014 98 97 98 97 97 97 1/14/2014 97 98 97 98 97 96 1 /15/2014 96 99 95 98 98 96 1/16/2014 98 96 97 97 98 96 1/17/2014 99 97 98 96 97 96 1/18/2014 98 99 98 97 97 95 1l19/2014 96 98 99 98 97 95 1/20/2014 98 96 99 97 97 95 1 /21 /2014 97 95 98 98 97 95 1/22/2014 97 97 96 98 96 95 1/23/2014 98 98 96 97 97 95 1 /24/2014 96 97 97 97 97 95 1 /25/2014 99 98 98 98 98 97 1 /26/2014 96 98 97 96 97 95 1 /27/2014 98 96 97 97 96 96 1 /28/2014 97 95 98 98 97 96 1 /29/2014 96 98 97 97 97 96 1 /30/2014 97 100 95 97 97 96 1 /31 /2014 97 99 96 97 97 96 Total 3,021 3,025 3,022 3,020 3,015 2,977 Samples 31 31 31 31 31 31 Average 97 98 97 97 97 96 Digester Temperature monthly average is 97°F• 03/13/2014 04:22:19 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT 2/112014 to 2/2812014 Permit No. NCO037834 Page 4 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 VolFrac 11+18+GB 32 DTrVoFrac % 419 PDig%VSR % 718 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 62 24 29 37 24 22 26 74 30 42 40 40 40 39 38 38 37 37 37 37 7.568 7.568 7.568 7.568 7.568 7.568 7.568 7.568 7.568 7.568 1.78 1.68 1.72 1.66 1.67 1.72 1.70 1.68 1.59 1.69 122.9 311.5 265.3 207.0 312.9 345.5 285.8 102.8 251.3 182.3 2/1 /2014 2/2/2014 2/3/2014 2/4/2014 2/5/2014 2/6/2014 1 2!7/2014 2/8/2014 2/9/2014 2/10/2 114 0.8369 0.8316 0.8272 0.8249 0.8429 0.8544 0.8243 0.8293 0.8206 0.8191 0.8408 0.8421 0.8380 0.8454 0.8400 0.8451 0.8447 0.8491 0.8458 0.8414 0.8391 0.8373 0.8329 6.8360 0.8413 0.8492 0.8350 0.8398 0.8351 0.8322 66.29 67.86 68.02 68.07 68.26 68.02 67.65 70.24 70.44 68.64 62 59 57 58 59 62 59 55 53 56 2/11 /2014 2/12/2014 0.8014 0.8071 0.8356 0.8500 0.8181 0.8287 69.33 67.82 50 56 25 28 37 35 7.568 7.568 1.63 1.74 297.9 269.3 2/13/2 114 0.8447 0.8485 0.8468 67.84 62 78 36 7.568 1.71 97.2 2/14/2014 2/15/2014 0.8012 0.7626 0.8452 0.8465 0.8272 0.8088 68.29 68.55 55 48 44 29 37 37 7.568 7.568 1.64 1.59 170.4 264.6 2/16/2 114 0.7967 0.8493 0.8248 67.84 55 32 37 7.568 1.71 238.9 2/17/ 0014 0.8192 0.8469 0.8346 68.86 56 26 37 7.568 1.67 290.5 2/18/2014 0.8282 0.8472 0.8392 69.51 56 45 37 7.568 1.64 168.7 2/19/2 114 0.8305 0.8478 0.8402 69.09 57 21 37 7.568 1.65 354.6 2/20/2014 0.8307 0.8489 0.8407 68.90 58 25 36 7.568 1.64 304.0 2/21/2014 0.8353 0.8502 0.8431 68.39 60 27 36 7.568 1.74 282.1 2/22/2014 0.8484 0.8404 0.8446 68.71 60 23 36 7.568 1.63 335.2 2/23/2014 0.8498 0.8430 0.8459 69.38 59 18 36 7.568 1.60 420.6 2/24/2014 0.8122 0.8370 0.8276 68.83 54 57 36 7.568 1.54 132.7 2/25/2014 0.8182 0.8378 0.8284 68.52 55 26 36 7.568 1.. 2/26/2014 0.8136 0.8341 0.8236 69.62 51 46 36 7.568 1.58 16666.2 2/27/2014 0.8232 6.8326 0.8278 69.62 52 25 36 7.568 1.58 307.3 2/28/2014 0.8176 0.8267 0.8221 68.90 52 47 37 7.568 1.64 162.5 Total 23.0516 23.6002 23.3500 1,921.49 1,578 989 1,036 211.904 46.44 6,945.4 Samples 28 28 28 28 28 28 28 28 28 28 Average 0.8233 0.8429 0.8339 68.62 56 35 37 7.568 1.66 248.1 03/13/2014 04:22:17 PM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 2/1/2014 to 2/28/2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 2/1/2014 1 97 97 98 97 96 96 2/2/2014 97 95 98 96 97 96 2/3/2014 97 95 99 96 97 96 2/4/2014 96 98 99 97 97 96 2/5/2014 96 98 97 97 97 96 2/6/2014 97 97 97 96 97 96 2/7/2014 96 97 97 97 97 96 2/8/2014 97 97 97 97 97 96 2/9/2014 97 97 97 96 97 96 2/10/2014 97 98 96 97 97 96 2/11/2014 96 98 97 96 97 96 2/12/2014 97 97 97 97 97 96 2/13/2 114 97 96 96 97 97 96 2/14/2014 96 98 97 96 97 96 2/15/2014 97 97 97 96 96 96 2/16/2014 96 97 97 96 96 96 2/17/2014 97 97 96 97 96 96 2/18/2014 98 96 96 96 96 96 2/19/2014 96 97 95 97 96 96 2/20/2014 97 97 96 97 96 96 2/21 /2014 96 96 97 96 96 96 2/22/2014 95 96 96 96 96 96 2/23/2014 95 97 96 96 95 96 2/24/2014 97 97 97 97 95 96 2/25/2014 98 97 97 97 96 96 2/26/2014 98 97 97 97 96 96 2/27/2014 97 98 97 96 96 96 2/28/2014 98 97 96 98 97 97 Total 2,708 2,714 2,712 2,704 2,700 2,689 Samples 28 28 28 28 28 28 Averaae 97 97 97 97 96 96 Digester Temperature monthly average is 96°F. 04/16/2014 04:37:39 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 3/1/2014 to 3/31/2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 VolFrac 11+18+GB 32 DTrVoFrac % 419 PDig%VSR % 718 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 3/1 /2014 0.8457 0.8193 0.8310 69.09 55 47 35 7.568 1.65 160.2 3/2/2014 0.8415 0.8240 0.8320 68.86 55 28 35 7.568 1.67 271.8 3/3/2014 0.8581 0.8206 0.8383 69.05 57 59 35 7.568 1.68 128.5 3/4/2014 0.8245 0.8235 0.8239 67.18 56 27 35 7.568 1.31 283.7 3/5/2014 0.8621 0.8235 0.8391 70.00 55 33 36 7.568 1.60 229.2 3/6/2014 0.8021 0.8225 0.8143 70.00 47 48 36 7.568 1.70 157.6 3/7/2014 0.8174 0.8263 0.8228 70.37 49 30 36 7.568 1.62 249.7 3/8/2014 0.7799 0.9254 0.8650 69.94 64 32 37 7.568 1.63 239.4 3/9/2014 0.7933 0.8252 0.8114 70.06 46 27 37 7.568 1.67 282.6 3/10/2014 0.7685 0.8221 0.7977 69.38 43 37 35 7.568 1.60 205.4 3/11/2014 0.7748 0.8216 0.7991 68.55 45 22 35 7.568 1.24 339.2 3/12/2014 0.8272 0.8259 0.8266 70.25 50 22 34 7.568 1.58 342.2 3/13l2014 0.8378 0.8205 0.8290 69.88 52 48 35 7.568 1.66 156.7 3/14/2014 0.8399 0,8197 0.8289 69.33 53 41 36 7.568 1.63 185.8 3/15/2014 0.8413 0.8217 0.8313 70.25 52 25 34 7.568 1.58 307.0 3/16/2014 0.8584 0.8264 0.8391 70.06 55 29 33 7.568 1.57 263.2 3/17/2014 0.8521 0.8245 0.8350 70.89 52 30 33 7.568 1.58 252.5 3/18/2014 0.8313 0.8214 0.8256 70.51 49 31 33 7.568 1.56 245.7 3/19/2014 0.8261 0.8210 0.8233 70.32 49 29 33 7.568 1.55 1 261.6 3/20/2014 0.7818 0.8182 0.7994 70.44 40 25 33 7.568 1.59 302.5 3/21 /2014 0.8121 0.8158 0.8138 70.19 46 31 33 7.568 1.61 245.9 3/22/2014 0.8227 0.8091 0.8156 70.00 47 24 33 7.568 1.60 311.5 3/23/2014 0.8285 0.8161 0.8215 69.94 49 24 33 7.568 1.63 311.5 3/24/2014 0.8266 0.8142 0.8194 69.51 50 35 33 7.568 1.64 218.9 3/25/2014 0.8541 0.8119 0.8315 70.37 52 26 34 7.568 1.62 290.5 3/26/2014 0.8544 0.8093 0.8307 70.44 51 19 32 7.568 1.59 389.8 3/27/2014 0.8405 0.8152 0.8265 72.83 1 44 52 33 7.568 1.84 146.6 3/28/2014 0.8305 0.8080 0.8180 70.00 48 29 33 7.568 1.60 263.7 3/29/2014 0.8333 0.8140 0.8216 70.89 47 29 33 7.568 1.58 258.3 3/30/2014 0.8371 0.8233 0.8284 70.81 50 27 1 32 7.568 1.61 280.0 3/31/2014 0.8203 0.8178 0.8187 73.16 40 37 32 7.568 1.90 206.1 Total 25.6238 25.5082 25.5588 2,172.53 1,549 1,002 1,059 234.608 49.89 7,787.3 Samples 31 31 31 31 31 31 31 31 31 31 Averaqe 0.8266 0.8228 0.8245 70.08 50 32 34 7.568 1.61 251.2 04/16/2014 04:37:36 PM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 3/1/2014 to 3/31/2014 Date Dig#,Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#6Temp Deg F 386 Dig#BTemp Deg F 387 3/1/2014 97 97 98 97 97 97 3/2/2014 97 98 98 97 96 98 3/3/2014 98 98 97 98 96 98 3/4/2014 99 98 97 97 95 98 3/5/2014 97 98 99 97 95 98 3/6/2014 96 97 100 98 95 97 Y712014 98 96 98 99 96 96 3/8/2014 96 98 97 97 95 95 3/9/2014 95 99 97 97 94 95 3/10/2 114 98 98 97 97 95 95 3/11 /2014 99 98 97 96 95 95 3/12/2014 98 97 96 98 96 95 3/13/2014 97 97 98 97 97 95 3/14/2014 97 97 98 96 97 95 3/15/2014 98 97 96 97 98 95 3/16/2014 98 98 97 97 97 96 3/17/2014 96 97 97 97 96 96 3/18/2014 96 97 97 96 96 95 • 3/19/2014 96 97 97 96 96 95 3/20/2014 99 98 98 98 98 97 3/21 /2014 96 97 97 96 96 95 3/22/2014 96 97 97 97 96 95 3/23/2014 97 97 98 97 97 96 3/24/2014 98 98 99 96 97 96 3/25/2014 98 99 98 98 98 97 3/26/2014 98 97 98 98 98 98 3/27/2014 96 97 99 97 98 98 3/28/2014 97 97 98 96 97 97 3/29/2014 97 97 96 95 97 97 3/30/2014 96 96 95 96 96 96 3/31 /2014 96 96 96 96 96 96 Total 3,010 3,018 3,020 3,004 2,986 2,982 Samples 31 31 31 31 31 31 Average 97 97 97 97 96 96 Digester Temperature monthly average is 96°F. 05/20/2014 10:42:10 AM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 411/2014 to 4130/2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 VolFrac 11+18+GB 32 DTrVoFrac % 419 PDig%VSR % 718 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 4/1/2014 0.8115 0.8120 0.8118 70.78 44 30 32 7.568 1.54 248.5 4/2/2014 0.8346 0.8044 0.8175 71.08 45 26 31 7.568 1.66 289.1 4/3/2014 0.8476 0.8000 0.8207 70.52 48 29 31 7.568 1.73 257.6 4/4/2014 0.8301 0.7941 0.8106 70.83 43 31 31 7.568 1.68 242.7 4/5/2014 0.8214 0.7981 0.8090 71.59 40 23 30 7.568 1.76 322.4 4/6/2014 0.8257 0.8000 0.8122 70.52 45 16 30 7.568 1.73 460.4 4/7/2014 0.7963 0.7983 0.7973 71.11 37 64 31 7.568 1.80 117.5 4/8/2014 0.7591 %; 0.7944 0.7757 %; 71.35 28* 26 31 7.568 1.71 c 294.7 4/9/2014 0.8192 0.7926 0.8050 71.01 41 33 30 7.568 1.69 229.6 4/10/2014 0.8211 0.7919 0.8039 69.64 44 27 31 7.568 1.68 277.7 4/11 /2014 0.8338 0.7920 0.8099 69.88 46 32 31 7.568 1.66 235.9 4/12/2014 0.8432 0.7957 0.8267 69.88 51 39 31 7.568 1.66 193.5 4/13/2014 0.8414 0.8017 0.8198 70.66 47 24 30 7.668 1.67 313.3 4/14/2014 0.8454 0.8000 0.8192 70.48 47 33 30 7.568 1.66 226.8 4/15/2014 0.7927 0.8122 0.8036 70.48 42 29 30 7.568 1.66 256.9 4/16/2014 0.7432 0.8148 0.7827 70.06 35 24 30 7.568 1.67 317.3 4/17/2014 0.8160 0.8073 0.8111 69.88 46 27 30 7.568 1.66 275.3 4/18/2014 0.8301 0.8072 0.8170 70.00 48 22 30 7.568 1.70 338.5 4/19/2014 0.8466 0.8060 0.8240 70.76 48 22 30 7.568 1.71 344.1 4/20/2014 0.8550 0.8093 0.8291 69.14 54 21 29 7.568 1.62 358.8 4/21 /2014 0.8389 0.8155 0.8260 70.91 49 23 29 7.568 1.65 336.2 4/22/2014 0.8455 0.8167 0.8304 69.70 53 21 29 7.568 1.65 352.5 4/23/2014 0.8391 0.8182 0.8286 70.06 52 22 29 7.568 1.67 341.5 4/24/2014 0.8368 0.8190 0.8281 29 7.568 0.0 4/25/2014 0.8352 0.8128 0.8242 71.26 47 49 30 7.568 1.74 155.7 4/26/2014 0.8676 0.8155 0.8381 71.51 52 46 30 7.568 1.72 163.4 4/27/2014 0.8848 0.8112 0.8417 70.93 54 28 30 7.668 1.72 274.4 4/28/2014 0.8836 0.8120 0.8460 71.10 55 28 30 68 1.73 274.4 4/29/2014 0.8709 0.8091 0.8374 71.60 51 29 30 68 1.69 260.9 4/30/2014 0.8011 0.8056 0.8032 71.51 39 27 29 !7.568 1.72 282.3 Total 24.9178 24.1675 24.5103 2,048.23 1,330 854 904 227.040 48.94 8,041.9 Samples 30 30 30 29 29 29 30 30 29 30 Averacie 0.8306 0.8056 0.8170 70.63 46 29 30 7.568 1.69 268.1 * Data qualified by Lab. 05/20/2014 10:42:08AM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 4/1/2014 to 4/30/2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 4/1l2014 96 96 96 96 96 96 4/2/2014 97 97 96 96 96 96 4/3/2014 98 97 97 96 96 96 4/4/2014 97 97 97 97 96 96 4/5/2014 97 97 97 98 96 96 4/6l2014 98 97 96 98 96 96 4/7/2014 98 97 97 97 96 96 4/8/2014 98 98 98 97 96 97 4/9/2014 98 96 97 98 97 97 4/10/2014 96 97 96 99 98 98 4/11/2014 97 97 98 98 99 97 4/12/2014 98 99 99 97 99 97 4/13/2014 97 98 98 97 98 98 4/14/2014 96 96 97 97 97 98 4/15/2014 96 96 96 97 97 98 4/16/2014 1 96 97 97 96 96 97 4/17/2014 97 96 96 97 96 97 4/18/2014 96 96 98 98 97 97 4/19/2014 98 97 98 98 97 97 4/20/2014 99 98 99 98 98 97 4/21 /2014 99 97 98 98 98 98 4/22/2014 1 98 98 97 97 99 98 4/23/2014 97 98 97 96 99 99 4/24/2014 96 97 97 96 99 98 4/25/2014 96 96 97 97 99 97 4/26/2014 98 96 97 98 98 96 4/27/2014 99 97 97 97 98 96 4/28l2014 98 98 97 97 98 97 4/29/2014 97 98 97 97 98 97 4/30/2014 96 98 96 97 1 98 97 Total 2,917 2,912 2,913 2,915 2,921 2,910 Samples 30 30 30 30 30 30 Avera4e 97 97 97 97 97 97 Digester Temperature monthly average is 97°F• 06/12/2014 03:04:18 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 5/1/2014 to 5/31/2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 VolFrac IVOL 11+18+GB 32 DTrVoFrac % 419 PDig%VSR % 718 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 5/1/2014 0.8205 0.8049 0.8129 71.43 42 24 29 7.568 1.75 313.3 5/2/2014 0.8168 0.7992 0.8081 71.43 41 31 29 7.568 1.68 240.8 5/3/2014 0.8160 0.8000 0.8077 71.69 40 28 29 7.568 1.66 270.4 5/4/2014 0.8371 0.7932 0.8138 71.18 43 29 29 7.568 1.70 262.5 615120 44 0.8459 0.7964 0.8192 71.60 44 26 29 7.568 1.69 296.1 5/6/2014 0.8245 0.7976 0.8106 70.83 43 48 30 7.568 1.68 158.5 5/7/2014 1 0.8147 0.7958 0.8053 71.18 40 31 29 7.568 1.70 246.6 5/8/2014 0.8169 0.7960 0.8068 70.76 42 23 29 7.568 1.71 333.6 5/9/2014 0.8226 0.7992 0.8118 70.93 43 55 30 7.568 1.72 138.5 5/10/2014 0.8276 0.8021 0.8169 71.68 43 22 30 7.568 1.73 338.5 5/11/2014 0.8676 0.8052 0.8388 70.86 53 29 30 7.568 1.75 262.3 5/12/2014 0.8048 0.8033 0.8041 71.26 40 68 31 7.568 1.74 111.2 5/13/2014 0.8118 0.8044 0.8087 71.01 42 35 31 7.568 1.69 214.0 5/14/2014 0.8371 0.7978 0.8202 70.93 47 20 31 7.568 1.72 378.4 5/15/2014 0.7970 0.7909 0.7944 70.69 38 42 31 7.568 1.74 181.4 5/16/2014 0.7945 0.7909 0.7929 70.17 39 28 31 7.568 1.81 268.3 5/17/2014 0.8216 0.7866 0.8085 71.02 42 26 31 7.568 1.76 290.9 5/18/2014 0.8503 0.7836 0.8275 70.79 49 57 32 7.568 1.78 132.2 5/19/2 114 0.8396 0.7891 0.8225 70.69 48 29 33 7.568 1.74 257.4 5/20/2014 1 0.8227 * 0.7917 ,; 0.8089 :'; 69.94 ;; 45 ;; 49 ;; 34 7.568 1.73. ;; 153.4 5/21/2014 0.7685 0.7932 0.7784 70.35 32 27 34 7.568 1.72 284.4 5/22/2014 0.7298 0.7886 0.7538 70.11 23 29 34 7.568 1.74 263.4 5/23/2014 0.7929 0.7844 0.7893 69.89 38 25 34 7.568 1.76 301.0 5/24/2014 0.8175 0.7732 0.7972 70.00 41 35 34 7.568 1.80 218.9 5/25/2014 0.8196 0.7695 0.7938 69.23 42 17 33 7.568 1.82 437.8 5/26/2014 0.8324 0.7750 0.8026 33 7.568 0.0 5/27/2014 0.8225 0.7881 0.8071 71.05 41 34 33 7.568 1.90 1 219.5 5/28/2014 0.8099 0.7918 0.8011 69.61 43 23 33 7.568 1.81 333.0 5/29/2014 0.8035 0.7937 0.7987 69.15 44 17 32 7.568 1.88 450.9 6/30/2014 0.8280 0.7893 0.8105 69.49 47 47 33 7.568 1.77. 161.6 5/31 /2014 0.8154 0.7885 0.8020 69.27 44 20 33 7.568 1.79 378.8 Total 25,3295 24.5634 24.9743 2,118.21 1,260 973 973 234,608 52.47 7,897.6 Samples 31 31 31 30 30 30 31 31 30 31 Averaqe 0.8171 0.7924 0.8056 70.61 42 32 31 7.568 1.75 254.8 * Data qualified by Lab. 06/12/2014 03:04:15 PM LAND APPLIED BIOSOLIDS Page 2 ARCHIE.ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NC0037834 5/1/2014 to 5/31/2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 5/1/2014 98 97 95 98 97 97 5/2/2014 98 97 96 97 97 97 5/3/2014 97 98 98 96 97 98 5/4/2014 96 99 99 98 98 98 5/5/2014 98 98 98 98 98 98 5/6/2014 100 97 98 98 98 98 5/7/2014 99 97 99 99 98 98 5/8/2014 98 98 100 99 98 98 5/9/2014 97 99 99 99 98 98 5/10/2014 97 99 98 99 98 98 5/11/2014 97 98 97 98 98 99 5/12/2014 96 97 97 98 99 100 5/13/2014 96 97 96 98 99 100 5/14/2014 97 98 97 98 99 100 5/15/2014 98 98 97 98 99 99 5/16/2014 98 97 97 98 99 97 5/17/2014 97 96 99 99 100 97 5/18/2014 96 97 98 99 99 97 5/19/2014 96 99 98 99 98 97 5/20/2014 98 99 97 98 97 97 5/21 /2014 99 98 99 99 98 98 5/22/2014 98 97 100 98 98 98 5/23/2014 97 97 101 99 98 99 5/24/2014 97 96 100 99 98 99 5/25/2014 96 95 99 100 99 100 5/26/2014 97 96 99 100 100 100 5/27/2014 98 97 98 99 100 100 5/28/2014 99 99 97 99 100 100 5/29/2014 100 99 97 99 100 100 5/30/2014 99 99 98 101 99 98 5/31 /2014 99 98 99 101 1 98 Total 3,026 3,026 3,040 3,058 3,051 3,051 Samples 31 31 31 31 31 31 Averaae 98 98 98 99 98 98 Digester Temperature monthly average is 98°F. 07/17/2014 04:42:56 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 6/1/2014 6/30/2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 Feed Vol Frac 30 day Mavg 1320 DTrVoFrac % 419 PDig%VSR % 1319 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 6/1 /2014 0.8019 0.7795 0.8048 68.42 47 23 32 7.568 2.09 335.0 6/2/2014 0.8192 0.7824 0.8046 70.21 43 57 33 7.568 1.88 132.7 6/3/2014 0.8045 0.7778 0.8038 69.47 44 21 33 7.568 1.90 1 359.2 6/4/2014 0.7845 0.7743 0.8025 69.57 44 25 33 7.568 1.84 298.4 6/5/2014 0.8250 0.7741 0.8022 69.57 44 29 33 7.568 1.84 257.4 6/6/2014 0.8137 0.7500 0.8015 68.68 46 22 32 7.568 1.82 344.3 6/7/2014 0.8307 0.7727 0.8012 33 7.568 0.0 6/8/2014 0.8784 0.7727 0.8015 32 7.568 0.0 6/9/2014 0.8101 0.7773 0.8007 32 7.568 0.0 6/10/2014 0.8055 0.7778 0.7993 70.06 41 86 34 7.568 1.77 88.1 6/11/2014 0.8273 0.7778 0.7993 69.83 42 32 33 7.568 1.79 235.9 6/12/2014 0.7834 0.7656 0.7981 69.44 42 27 33 7.568 1.80 282.8 6/13/2014 0.8039 0.7667 0.7967 69.19 43 38 33 7.568 1.85 198.4 6/14/2014 0.8151 0.7766 0.7966 68.51 44 37 33 7.568 1.81 202.6 6/15/2014 0,8315 0.7476 0.7962 68.98 43 29 33 7.568 1 1.87 257.4 6/16/2014 0.8253 0.7373 0.7951 69.19 42 28 33 7.568 1.85 270.0 6/17/2014 0.8300 0.7462 0.7938 1 69.02 42 39 33 7.568 1.84 194.2 6/18/2014 0.8438 0.7463 0.7927 69.73 40 23 32 7.568 1.85 328.7 6/19/2014 0.8078 0.7336 0.7911 68.72 42 31 32 7.568 1.79 245.5 6/20/2014 0.8295 0.7376 0.7910 69.57 40 29 32 7.568 1.84 265.3 6/21 /2014 0.8430 0.7368 0.7918 69.32 1 41 47 32 7.568 1.76 162.0 6/22/2014 0.8379 0.7331 0.7915 69.23 41 47 33 7.568 1.82 159.5 6/23/2014 0.8293 0.7276 0.7907 69.32 40 28 33 7.568 1.76 266.2 6/24/2014 0.8234 0.7423 0.7903 69.10 41 35 34 7.568 1.78 216.6 6/25/2014 0.8078 0.7381 0.7892 69.06 40 27 33 7.568 1.81 284.0 6/26/2014 0.8238 0.7413 0.7880 69.49 39 31 33 7.568 1.77 242.7 6/27/2014 0.8240 0.7431 0.7870 69.54 38 29 34 7.568 1.74 259.2 6/28/2014 0.8300 0.7343 0.7861 69.40 38 31 34 7.568 1.83 243.6 6/29/2014 0.8427 0.7413 0.7852 70.22 35 53 34 7.568 1.78 142.7 6/30/2014 0.8550 0.7390 0.7848 69.10 39 25 34 7.568 1.78 305.9 Total 24.6880 22.6509 23.8569 1,871.94 1,121 930 989 227.040 49.26 6,578.3 Samples 30 30 30 27 27 27 30 30 27 30 Average 0.8229 0.7550 0.7952 69.33 42 34 33 7.568 1.82 219.3 07/17/2014 09:07:48 AM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 6l1 /2014 to 6/30/2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 6/1 /2014 98 97 100 100 97 98 6/2/2014 97 97 100 99 97 98 6/3/2014 97 96 99 99 97 98 6/4/2014 98 98 98 98 98 98 6/5/2014 97 98 98 98 98 98 6/6/2014 97 98 97 97 98 97 6/7/2014 96 97 97 97 97 96 6/8/2014 96 97 96 96 97 96 6/9/2014 96 97 96 96 96 96 6/10/2014 96 97 96 96 96 95 6/11/2014 95 97 96 96 96 95 6/12/2014 95 96 96 96 95 95 6/13/2014 97 96 96 97 95 96 6/14/2014 98 98 98 98 95 98 6/15/2014 99 98 98 98 96 98 6/16/2014 98 98 98 97 98 98 6/17/2014 99 97 97 98 98 98 6/18/2014 100 97 97 98 98 97 6/19/2014 99 97 97 99 98 97 6/20/2014 99 98 98 98 98 97 6/21/2014 99 98 98 98 98 97 6/22/2014 97 98 98 98 98 97 6/23/2014 97 100 100 99 98 98 6/24/2014 97 100 100 98 98 98 6/25/2014 98 100 100 98 98 98 6/26/2014 98 100 99 98 98 99 6/27/2014 97 99 99 97 99 99 6/28/2014 97 98 98 97 98 1 99 6/29/2014 97 98 97 97 98 99, 6/30/2014 99 98 97 97 98 98 Total 2,923 2,933 2,934 2,928 2,919 2,921 Samples 30 30 30 30 30 30 Average 97 98 98 98 97 97 Digester Temperature monthly average is 97°F. 09/24/2014 09:52:43 AM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 711 /2014 7/31 /2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 Feed Vol Frac 30 day Mavg 1320 DTrVoFrac % 419 PDig%VSR % 1319 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 3" 7/1/2014 0.8415 0.7341 0.7844 68.16 41 67 36 7.568 1.79 112.6 7/2/2014 0.8359 0.7287 0.7834 68.51 40 31 35 7.568 1.81 240.4 7/3/2014 0.8305 0.7284 0.7826 67.39 43 25 35 7.568 1.84 305.6 7/4/2014 0.8132 0.7323 0.7820 69.06 38 73 37 7.568 1.81 103.0 7/5/2014 0.8178 0.7317 0.7807 66.99 43 59 38 7.568 2.06 127.3 7/6/2014 0.8398 0.7309 0.7802 68.75 38 20 38 7.568 1.92 386.1 7/7/2014 0.8386 0.7358 0.7792 69.54 35 80 40 7.568 1.74 95.1 7/8/2014 0.8270 0.7446 0.7778 68.59 38 35 39 7.568 1.91 218.9 7/9/2014 0.8268 0.7854 0.7782 69.23 36 32 39 7.568 1.82 238.0 7/10/2014 0.8116 0.7409 0.7775 68.04 39 34 37 7.568 1.94 223.6 7/11/2014 0.8442 0.7431 0.7770 69.23 35 23 37 7.568 1.95 327.5 7/12/2014 0.8349 0.7366 0.7775 68.06 39 29 37 7.568 1.91 265.1 7/13/2014 0.8362 0.7411 67777 68.62 37 33 37 7.568 1.88 231.7 7/14/2014 0.8285 0.7443 0.7774 69.54 35 47 37 7.568 1.74 162.5 7/15/2014 0.8204 0.7500 0.7775 68.48 38 28 37 7.568 1.84 271.4 7/16/2014 7/17/2014 0.7815 0.8348 0.7674 0.7888 0.7776 0.7784 68.65 66.86 37 43 21 42 37 37 7.568 7.568 1.85 1.69 357.2 178.3 711812014 0.8179 0.7576 0.7783 69.27 36 26 37 7.568 1.79 287.7 7/19/2014 0.8400 0.7564 0.7795 68.98 37 22 37 7.568 1.87 339.0 7/20/2014 0.8598 0.7639 0.7807 69.57 36 32 37 7.568 1.84 234.5 7/21/2014 0.8500 0.7560 0,7814 70.06 35 36 37 7.568 1.77 208.7 7/22/2014 7/23/2014 0.8297 0.8313 0.7650 0.7692 0.7821 0.7830 70.35 69.49 34 37 43 41 37 37 7.568 7.568 1.72 1.77 174.8 183.0 7/24/2014 0.8197 0.7700 0.7835 68.93 39 28 37 7.568 1.77 268.3 7/25/2014 0.8238 0.7624 0.7843 69.49 37 24 37 7.568 1.77 321.7 7/26/2014 0.8430 0.7598 0.7853 69.89 37 26 37 7.568 1.76 295.8 7/27/2014 0.8462 0.7697 0.7868 69.71 38 58 37 7.568 1.75 129.E 7/28/2014 0.8524 0.7895 69.64 39 49 38 7.568 1.68 154.8 7/29/2014 0.8324 0.7911 69.71 39 191 43 7.568 1.75 39.6 7/30/2014 0.8612 0.8382 0.7933 68.97 42 34 43 7.568 1.74 222.2 7/31 /2014 0.8511 0.8261 0.7952 69.01 43 30 42 7.568 1.71 253.2 Total 25.8216 21.9585 24.2430 2,136.76 1,182 1,320 1,170 234.608 56.19 6,957.2 Samples 31 29 � 31 31 31 31 31 31 31 31 Average 0.8330 0.7572 0.7820 68.93 38 43 38 7.568 1.81 224.4 08/12/2014 03:30:50 PM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREP�TMENT PLANT Permit No. NCO037834 7/1/2014 to 7/31/2014 I Date Dig #1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig Del 385 4Temp g F Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 7/1/2014 102 97 97 100 98 98 7/2/2014 101 99 97 99 97 98 7/3/2014 101 99 98 99 97 1 98 7/4/2014 100 98 99 98 97 98 7/5/2014 100 98 100 98 97 98 7/6/2014 99 97 100 98 97 97 7/7/2014 99 97 100 98 97 97 7/8/2014 99 97 99 97 97 97 7/9/2014 98 96 99 97 97 97 7/10/2014 98 97 98 97 97 96 7/11/2014 97 99 98 96 97 96 7/12/2014 98 99 97 96 96 96 7/13/2014 98 98 97 1 98 96 96 7/14/2014 98 98 99 98 96 96 7/15/2014 97 98 99 99 96 96 7/16/2014 98 98 98 98 96 95 7/17/2014 100 100 98 99 96 95 7/18/2014 100 100 100 100 96 95 7/19/2014 99 99 99 100 96 95 7/20/2014 98 98 99 99 96 95 7/21/2014 98 98 98 99 96 95 7/22/2014 98 98 98 99 96 95 7/23/2014 97 97 97 98 95 95 7/24/2014 97 97 97 98 95 95 7/25/2014 97 97 97 98 95 94 7/26/2014 96 96 97 j 97 95 94 7/27/2014 98 97 97 j 97 95 94 7/28/2014 99 98 98 97 95 95 7/29/2014 99 98 98 97 98 99 7/30/2014 98 98 98 97 99 100 7/31/2014 98 97 97 i 97 98 99 Total 3,055 3,033 3,043 3,038 2,989 2,984 Samples 31 31 31 31 31 31 Averaae 99 98 98 98 96 96 I , ye5•1er %froperc� �vr Nto.r�!^ �Y V:'r4 y L, = 7 ° F 09/16/2014 10:25:26 AM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 8/1/2014 8/31 /2014 Page 4 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 Feed Vol Frac 30 day Mavg 1320 DTrVoFrac % 419 PDig%VSR % 1319 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 8/1/2014 0.8401 0.8459 0.7976 70.35 40 47 42 7.568 1.72 162.5 8/2/2014 0.8163 0.8413 0.7997 1 70.22 41 36 43 7.568 1.78 208.0 8/3/2014 1 0.8466 0.8321 0.8022 70.18 42 27 41 7.568 1.71 282.3 8/4/2014 0.8420 0.8246 0.8045 70.69 41 36 40 7.568 1.74 211.9 8/5/2014 0.8348 0.8068 0.8063 70.52 43 26 40 7.568 1.73 293.0 8/6/2014 0.8519 0.7947 0.8079 71.02 42 25 39 7.5 88 1.76 301.4 8/7/2014 0.8545 0.7857 0.8093 70.00 45 41 39 7.568 1.80 182.7 8/8/2014 0.8444 0.7947 0.8099 1 70.65 44 44 39 7.568 1.84 170.9 8/9/2014 0.8471 0.7992 0.8118 71.58 42 65 40 7.568 1.83 116.6 8/10/2014 0.8333 0.7977 0.8127 70.11 46 17 40 7.568 1.84 450.9 8/11 /2014 0.8333 0.8058 0.8140 70.69 45 86 42 7.568 1.74 88.1 8/12/2014 0.7844 0.8066 0.8142 70.63 45 52 43 7.568 1.60 146.6 8/13/2014 0.8610 0.8133 0.8163 70.95 45 27 42 7.568 1.79 280.2 8/14/2 114 0.8560 0.8103 0.8181 70.45 47 48 43 7.568 1.76 156.7 8/15/2014 0.8349 0.8161 0.8198 43 7.568 0.0 8/16/2014 0.8261 0.8165 0.8202 71.35 45 24 43 7.568 1.78 316.4 8/17/2014 0.8327 0.8072 0.8213 71.11 46 31 43 7.568 1 1.80 247.6 8/18/2014 0.8378 0.8158 0.8222 71.57 46 221 50 7.568 2.04 34.3 8/19/2014 0.8038 0.8193 0.8223 73.89 39 27 50 7.568 2.03 282.8 8/20/2014 0.8441 0.8213 0.8234 72.53 43 41 50 7.568 1.82 184.4 8/21/2014 0.8670 0.8166 0.8249 71.82 46 32 49 7.568 1.81 236.4 8/22/2014 0.8380 0.8041 0.8256 71.91 46 56 50 7.568 1.78 135.2 8/23/20a4 0.8414 0.8057 0.8265 72.22 45 28 50 7.568 1 1.80 274.4 8/24/2014 0.8400 0.7956 0.8274 71.84 47 43 51 7.568 1.74 175.1 8/25/2014 0.8350 0.7917 0.8278 72.00 47 39 51 7.568 1.75 192.3 8/26/2014 0.8293 0.7932 0.8278 71.84 47 33 50 7.568 1.74 232.0 8/27/2014 0.8329 0.7890 0.8264 72.32 45 27 49 7.568 1.77 279.3 8/28/2014 0.8295 0.7957 0.8258 72.00 46 31 44 7.568 1.75 240.6 8/29/2014 0.8317 0.7792 0.8243 71.27 47 19 43 7.568 1.81 396.3 8/30/2014 0.8315 0.7851 0.8234 70.76 48 159 48 7.568 1.71 47.6 8/31/2014 0.8359 0.7783 0.8222 72.28 44 27 47 7.568 1.84 282.6 Total 25.9373 24.9891 25.3361 2,138.76 1,333 1,414 1,385 234.608 53.61 6,609.1 Samples 31 31 31 30 30 30 31 31 30 31 Averaae 0.8367 0.8061 0.8173 71.29 44 47 45 7.568 1.79 213.2 09/16/2014 10:25:23 AM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 8/1/2014 to 8/31/2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 8/1/2014 97 97 97 96 98 99 8/2/2014 97 96 97 96 98 98 8/3/2014 97 98 97 98 97 98 8/4/2014 99 98 97 98 97 97 8/5/2014 99 98 97 98 97 97 8/6/2014 99 98 97 98 97 97 8/7/2014 99 98 97 97 96 97 8/8/2014 99 97 97 97 96 96 8/9/2014 98 97 97 97 96 96 8/10/2014 98 97 96 97 96 97 8/11/2014 97 96 97 97 97 98 8/12/2014 97 97 99 97 98 98 8/13/2014 96 99 99 97 99 99 8/14/2014 96 99 99 99 99 99 8/15/2014 96 98 99 100 98 99 8/16/2014 96 98 98 100 98 98 8/17/2014 96 98 98 100 98 98 8/18/2014 96 97 98 99 98 98 8/19/2014 96 97 98 99 97 97 8/20/2014 96 97 98 99 97 97 8/21/2014 96 96 98 98 97 97 8/22/2014 98 97 98 98 97 97 8/23/2014 98 98 98 98 97 96 8/24/2014 98 98 97 97 98 97 8/25/2014 97 97 97 97 98 97 8/26/2014 97 97 97 97 98 97 8/27/2014 97 96 97 97 98 97 8/28/2014 96 97 98 96 97 97 8/29/2014 96 98 99 96 97 97 8/30/2014 97 99 99 97 97 97 8/31/2014 97 98 99 97 97 98 Total 3,011 3,021 3,029 3,027 3,018 3,020 31 31 31 97 97 98 31 31 31 98 97 97 Teter q7� f7i y zs few % 10/15/2014 05:25:42 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 9/1/2014 9/30/2014 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 Feed Vol Frac 30 day Mavg 1320 DTrVoFrac % 419 PDig%VSR % 1319 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 9/1/2014 0.8168 0.7783 0.8211 71.18 46 91 49 7.568 1.70 83.2 9/2/2014 6.8241 0.7768 0.8199 71.51 45 44 50 7.568 1.79 170.6 9/3/2014 0.8177 0.7826 0.8189 1 71.02 46 24 49 7.568 1.76 314.3 9/4/2014 0.8287 0.7860 0.8186 71.02 46 26 49 7.568 1.76 288.1 9/5/2014 0.8144 0.7826 0.8180 71.59 44 31 49 7.568 1.76 240.4 9/6/2014 0.7916 0.7778 0.8168 71.11 45 30 49 7.568 1.80 250.4 9/7/2014 0.8482 0.7753 0.8166 70.29 47 31 49 7.568 1.75 244.3 9/8/2014 0.8384 0.7712 0.8159 70.22 47 37 48 7.568 1.78 207.0 9/9/2014 0.8229 0.7778 0.8153 70.62 46 38 48 7.568 1.77 201.4 9/10/2014 0.8312 0.7778 0.8147 71.35 43 31 46 7.568 1.78 243.6 9/11/2014 0.8438 0.7703 0.8155 70.06 47 36 46 7.568 1.77 212.8 9/12/2014 0.8693 0.7854 0.8149 72.88 39 101 48 7.568 1.77 74.8 9/13/2014 0.8547 0.7745 0.8142 70.39 46 24 48 7.568 1.79 318.5 9/14/2014 0.8333 0.7785 0.8137 70.73 45 41 47 7.568 1.64 184.4 9/15/2014 0.8199 0.7540 0.8128 70.26 46 43 48 7.568 1.95 177.6 9/16/2014 0.8162 0.7862 0.8123 71.18 43 44 48 7.568 1.70 172.5 9/17/2014 0.7893 0.7882 0.8110 70.95 43 66 43 7.568 1.79 114.9 9/18/2014 0.7896 0.7965 0.8104 69.89 46 31 43 7.568 1.86 242.2 9/19/2014 0.8222 0.7946 0.8098 70.05 45 45 44 7.56 1 1.87 167.1 9/20/2014 0.8294 0.7975 0.8089 70.35 44 86 45 7.568 1.72 88.1 9/21/2014 0.8264 0.7950 0.8087 70.16 44 26 44 7.568 1.91 296.3 9/22/2014 0.8579 0.7978 0.8091 71.08 42 34 45 7.568 1.66 224.5 9/23/2014 0.8415 0.7962 0.8093 68.91 48 32 44 7.568 1.93 233.8 9/24/2014 0.8152 0.8007 0.8091 70.93 42 62 45 7.568 1.72 122.4 9/25/2014 0.8151 0.7953 0.8088 70.52 43 37 45 7.568 1.73 202.4 9/26/2014 0.8232 0.7852 0.8086 69.27 47 64 46 7.568 1.79 118.9 9/27/2014 0.8264 0.7898 0.8085 71.98 39 52 47 7.568 1.82 146.9 9/28/2014 0.8563 0.7908 0.8093 69.66 46 21 47 7.568 1.78 359.2 9/29/2014 0.8578 0.7905 0.8100 69.32 47 119 46 7.568 1.76 63.4 9/30/2014 0.8371 0.7966 0.8104 70.00 45 29 46 7.568 1.80 261.1 Total 24.8586 23.5497 24.3911 2,118.49 1,341 1,375 1,404 227.040 53.41 6,025.1 Samples 30 30 30 30 30 30 30 30 30 30 Averaae 0.8286 0.7850 0.8130 70.62 45 46 47 7,568 1.78 200.8 9 10/15/2014 05:25:39 PM LAND. APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NC0037834 9/1/2014. to' 9/30/2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4iemp Deg-F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 9/1/2014 97 98 98 99 98 98 9/2/2014 98 98 98 99 98 97 9/3/2014 99 98 98 99 97 97 9/4/2014 99 98 98 99 98 97 9/5/2014 99 99 100 98 99 99 9/6/2014 98 100 101 98 99 99 9/7/2014 98 99 100 98 99 98 9/8/2014 98 99 99 97 98 98 9/9/2014 97 98 98 97 98 97 9/10/2014 97 97 97 97 97 96 9/11/2014 97 97 97 96 97 99 9/12/2014 97 97 97 96 98 100 9/13/2014 96 96 96 96 99 99 9/14/2014 96 96 96 96 99 99 9/15/2014 96 96 96 96 98 99 9/16/2014 97 97 96 97, 98 98 9/17/2014 98 98 98 97 98 98 9/18/2014 98 98 101 96 97 97 9/19/2014 97 98 101 97 97 97 9/20/2014 97 97 100 99 97 97 9/21/2014 97 97 100 100 97 97 9/22/2014 97 96 100 100 96 96 9/23/2014 97 96 99 100 98 98 9/24/2014 1 98 97 99 99 98 99 9/25/2014 99 98 98 99 98 98 9/26/2014 100 98 98 98 97 97 9/27/2014 99 98 98 98 97 97 9/28/2014 99 97 1 97 97 97 97 9/29/2014 98 97 97 97 97 96 9/30/2014 98 97 97 97 96 96 Total 2,931 2,925 2,948 2,932 2,930 2,930 Samples 30 30 30 30 30 30 Average 98 98 98 98 98 98 %V �[i ices ler %e,y�era�ur �'S 11/24/2014 11:13:35AM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 10/1/2014 10/31/2014 Page 4 Date 11 VolFrac ratio 683 21 VolFrac ratio 684 Feed Vol Frac 30 day Mavg 1320 DTrVoFrac % 419 PDig%VSR % 1319 PriDigSRT Days %TS 483 PriDigSRT Days %TS 30 DAY V483 PriDig VOL MG 529 Trans %TS % 136 ELL PrTranFlo TGD 344 10/1 /2014 0.8289 0.7943 0.8110 70.35 45 273 52 , 7.568 1.72 10/2/2014 10/3/2014 0.7582%< 0.7673 0.7918 %; 0.7952 0.8101 0.8092 70.00* 70.27 45 %� 44 26 % 36 51 52 7.568 7.568 1.80* 1.85 88.4 2. 211.9 10/4/2014 0.7567 0.7882 0.8077 71.88 39 97 54 7.568 1.92 78.3 10/5/2014 0.8137 0.7870 0.8078 69.89 45 19 54 7.568 1.76 393.5 10/6/2014 0.8249 0.7910 0.8088 70.45 44 140 57 7.568 1.76 53.9 10/7/2014 0.8278 0.8049 0.8088 69.66 46 97 60 7.568 1.78 78.3 10/8/2014 0.8333 0.8115 0.8095 70.00 45 40 60 7.568 1.80 187.0 10/9/2014 0.8538 0.8112 69.71 46 193 65 7.568 1.75 39.2 10/10/2014 0.8515 0.8127 69.36 48 73 66 7.568 1.73 103.0 OM 1 /2014 0.8099 0.8125 69.66 47 56 67 7.568 1.78 134.7 10/12/2014 0.8299 0.8126 66 7.568 0.0 OM 312014 0.8202 0.8470 0.8130 67 7.568 0.0 10/14/2014 0.8208 0.8403 6.8138 70.11 46 32 67 7.568 1.74 238.3 10/15/2014 0.8397 0.8143 0.8148 69.83 47 24 66 7.568 1.79 314.3 10/16/2014 0.8226 0.8000 0.8150 70.33 46 31 66 7.568 1.82 247.4 10/17/2014 0.8227 0.8025 0.8158 69.95 47 30 64 7.568 1.83 254.3 OM 8/2014 0.8125 0.7991 0.8162 69.83 48 106 67 7.568 1.79 71.3 10/19/2014 0.8273 0.7971 0.8161 69.32 49 22 66 7.568 1.76 345.3 10/20/2014 0.8259 0.7905 0.8158 71.27 44 26 64 7.568 1.81 291.4 0.8156 0.7922 0.8153 70.22 47 25 64 7.568 1.78 301.4 0.8158 0.7913 0.8143 70.22 46 17 64 7.568 1.78 454.8 E 0.8286 0.7934 0.8138 69.19 49 191 69 7.568 1.72 39.6 0.8312 0.7857 0.8138 69.66 47 42 68 7.568 1.78 182.3 0.8303 0.7685 0.8134 70.95 44 29 68 7.568 1.79 264.1 10/26/2014 0.8785 6.7854 0.8142 69.61 48 66 68 7.568 1.81 114.9 10/27/2014 0.8649 0.7863 0.8145 70.69 45 24 67 7.568 1.74 314.0 10/28/2014 0.8266 0.7854 0.8137 70.45 45 24 67 7.568 1.76 315.7 10/29/2014 0.8524 0.7877 0.8133 69.66 47 91 66 7.568 1.78 83.2 10/30/2014 0.8304 0.7890 0.8129 70.86 44 22 66 7.568 1.75 342.7 10/31 /2014 0.8231 0.7813 0.8124 70.39 45 27 57 7.568 1.79 280.0 Total 25.5450 21.5009 25.1940 2,033.80 1,330 1,879 1,957 234.608 51.67 6,050.9 Samples 1 31 27 31 29 29 29 31 31 29 31 Averaae 0.8240 0.7963 0.8127 70.13 46 65 63 7.568 1.78 195.2 * Data qualified. 11/24/2014 11:13:32 AM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 10/112014 to 10/31/2014 Date 6ig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 Dig#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 10/1 /2014 98 96 97 96 96 96 10/2/2014 97 96 96 97 96 96 10/3/2014 97 96 96 99 97 98 10/4/2014 96 97 97 100 98 99 10/5/2014 96 99 99 99 98 99 10/6/2014 97 100 100 98 99 98 10/7/2014 99 99 99 98 98 98 10/8/2014 99 98 99 97 98 98 10/9/2014 99 98 98 97 98 98 TOM 0/ 0014 98 98 98 97 97 98 TOM 1/2014 98 97 98 97 97 98 TOM 2/ 0014 98 97 98 97 97 97 TOM 3/ 0014 97 97 97 96 97 97 10/14/2014 96 96 97 96 96 96 10/15/2014 95 95 97 98 96 95 10/16/2014 96 95 96 97 96 95 10/17/2014 97 97 97 97 98 97 10/18/2014 98 98 98 97 98 98 10/19/2014 98 97 98 99 98 97 10/20/2014 97 96 98 99 97 97 10/21 /2014 98 98 97 98 97 97 10/22/2014 97 97 98 97 98 98 10/23/2014 96 96 99 96 98 99 10/24/2014 96 96 99 96 98 99 10/25/2014 98 99 98 95 98 99 99 99 99 96 97 99 ' 014 99 99 98 99 98 99 LO/26/2014 014 98 98 98 99 99 98 014 98 98 99 100 98 99 014 99 98 98 99 98 98 10/31 /2014 101 98 98 98 98 98 Total 3,025 3,018 3,034 3,024 3,022 3,028 Samples 31 31 31 31 31 31 Averaae 98 97 98 98 97 98 Digester Temperature monthly average is 97°F. 12/11/201412:18:31 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 11 /1 /2014 11 /30/2014 11 21 Feed DTrVoFrac PDig%VSR PriDigSRT PriDigSRT PriDig Trans ELL VolFrac VolFrac Vol Frac VOL %TS PrTranFlo 30 day ratio ratio Mavg % % Days %TS Days %TS MG % TGD Date 683 684 1320 419 1319 483 30 DAY V483 529 136 344 11 /1 /2014 0.7991 0.7717 0.8129 68.97 49 28 57 , 7.568 1.74 275.1 11 /2/2014 0.8600 0.7787 0.8133 70.06 46 25 57 7.568 1.77 304.7 11/3/2614 0.8466 0.7876 0.8152 69.89 47 66 56 7.568 1.76 114.9 11 /4/2014 0.8553 0.7913 0.8157 70.27 47 34 56 7.568 1.85 221.9 11 /5/2014 0.8571 0.7864 0.8158 69.57 48 28 52 7.568 1.84 274.4 11/6/2014 0.8498 0.7847 0.8159 71.26 44 66 51 7.568 1.74 114.9 11l7/2014 0.8571 0.7800 0.8154 68.27 51 191 57 7.568 2.08 39.6 11 /8/2014 0.8551 0.7939 0.8140 1 69.90 47 33 51 7.568 1.96 229.9 11 /9/2014 0.8433 0.7897EO.8127 69.82 47 25 49 7.568 1.69 299.1 11/10/2014 0.8198 0.7928 70.52* 45 %: 38 49 7.568 1.73 197.0 11/11/2014 0.8269 0.7931 70.81 44 49 49 7.568 1.85 154.E 11/12/2014 0.8405 0.7919 69.95 46 14752 7.568 1.83 51.5 11 /13/2014 0.8277 0.7881 70.69 44 23 52 7.568 1.74 326.1 11 /14/2014 0.8230 0.7960 0.8100 71.26 42 28 52 7.568 1.74 11/15/2014 0.8342 0.7980 6.8102 70.18 45 43 52 7,568 1.71 174.1 174.2 11/16/2014 0.8447 0.8031 0.8105 71.01 43 28 52 7.568 1.69 266.9 11/17/2014 0.8329 0.7992 0.8109 71.35 42 33 50 7.568 1.71 228.7 Ti /18/2014 0.8200 0.8009 0.8109 70.59 44 23 50 7.568 1.70 330.1 11/19/2014 0.8539 0.8047 0.8117 71.26 42 55 51 7.568 1.67 138.0 11 /20/2014 0.8470 0.8088 0.8126 70.41 45 34 51 7.568 1.69 221.7 11/21/2014 0.8420 0.8135 0.8134 70.59 45 56 52 7.568 1.70 134.7 11 /22/2014 0.8348 0.8036 0.8138 71.26 43 18 47 7.568 1.67 411.9 11 /23/2014 0.8102 0.7984 68136 71.01 44 43 47 7.568 1.69 174.4 11 /24/2014 0.8127 0.7935 0.8139 71.26 43 28 47 7.568 1.67 273.7 11/25/2014 0.8401 0.7974 0.8135 70.29 46 52 46 7.568 1.75 146.E 11/26/2014 0.8351 0.7920 0.8132 70.24 46 21 46 7.668 1.68 356.2 11 /27/2014 0.8267 0.7922 0.8133 69.05 49 35 46 7.568 1.68 214.0 11/28/2014 0.8698 0.7833 0.8134 71.10 44 30 44 7.568 1.73 250.6 11/29/2014 0.8707 0.7840 0.8139 70.73 45 27 45 7.568 1.64 281.8 11 /30/2014 0.8671 0.7796 0.8145 71.18 44 50 45 7.568 1.70 152.5 Total 25.1431 23.7780 23 • 57b4 L04'L . 16 Samples 30 30 29 29 Average 0.8381 0.7926 0.8130 70.42 * Estimates. 151 1 1,500 I,DIU LLl.UYU G.YV 29 30 30 30 30 45 45 50 7.568 1.75 30 220.9 12/11/2014 12:18:28 PM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 1111/2014 to 11/30/2014 Dig#1Temp Dig#2Temp Dig#3Temp Dig#4Temp Dig#5Temp Dig#8Temp Date Deg F 382 Deg F 383 Deg F 384 Deg F 386 Deg F 386 Deg F 387 11/1/2014 11/2/2014 11 /3/2014 11/4/2014 11 /5/2 114 11/6/2014 11/7/2014 11 /8/2014 11/9/2014 11/10/2014 11/11/2014 11/12/2014 11/13/2014 11/14/2014 Ti/15/ 0014 11/16/2014 11 /17/2014 11/18/2014 11/19/2014 11/20/2014 11/21/2014 11/22/2014 11 /23/2014 11/24/2014 100 98 97 98 99 98 97 96 95 98 101 99 98 97 99 99 98 96 96 97 98 97 98 97 96 95 97 96 96 96 97 97 99 98 97 99 99 98 97 96 97 101 101 100 98 97 97 99 98 97 96 97 96 97 98 99 98 97 96 96 97 96 97 97 99 101 101 100 98 98 97 96 97 97 96 97 97 96 96 98 99 98 97 96 98 99 98 97 96 95 98 100 99 98 97 98 99 100 100 99 98 97 96 99 99 97 97 98 98 96 95 97 96 98 97 96 95 95 96 95 97 97 98 98 97 98 98 98 98 99 99 99 99 97 98 98 98 98 97 96 96 96 98 98 97 96 96 95 94 94 99 97 96 98 99 98 99 101 199 99 98 97 98 98 97 97 98 97 97 98 99 99 98 97 98 98 97 96 95 94 11/25/2014 11 /26/2014 11/27/2014 11/28/2014 11 /29/ 0014 11/30/2014 Tn+al 2.922 2,932 2,924 e,aza 4,a 1 Samples 30 30 30 3u °" Avarnna 97 98 97 97 97 98 Digester Temperature monthly average is 97°F• 01/14/2015 03:36:09 PM LAND APPLIED BIOSOLIDS ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 Page 4 12/1 /2014 12/31 /2014 11 VolFrac 21 VolFrac Feed Vol Frac DTrVoFrac PDig%VSR PriDigSRT PriDigSRT PriDig Trans ELL 30 day VOL %TS PrTranFlo ratio ratio Mavg % % Days %TS Days %TS MG % TGD Date 683 684 1320 419 1319 483 30 DAY V483 529 136 344 12/1 /2014 0.8280 0.7870 0.8153 71.08 44 64 46 7.568 1.66 118.2 12/2/2014 0.8520 0.7818 0.8162 71.34 _ 44 24 46 7.568 1.64 314.2 12/3/2014 0.8595 0.7950 0.8164 _ 11.59 43 _ 97 _ 47 7.568 1.76 78.3 12/4/2014 0.8742 0.7890 0.8168 71.51 44 74 _ 49 7.568 1.79 102.8 12/5/2014 68628 0.7956 0.8172 70.73 46 _ 44 49 7.568 1.64 170.4 12/6/2014 0.8754 0.7863 0.8173 70.81 46 _ 26 48 7.568 1.61 285.6 12/7/2014 0.8596 0.7890 0.8176 71.52 44 40 43 7.568 1.58 191.2 12/8/2014 0.8641 0.7845 0.8179 70.37 _ 47 27 _ 43 7.568 1.62 282.3 12/9/2014 0.8447 0.7958 0.8182 _ 70.00 24 _ _ - -43 7.568 1.60 314.0 12/10/2014 0.8581 0.7951 0.8189 71.07 _48 - 46 21 _ 42 7.568 _ 1.59 355.3 12/11 /2014 0.8409 0.7966 0.8192 70.63 47 22 41 7.568 1.60 347.8 12/12/2014 0.8469 0.7948 0.8192 71.25 45 _ 27 37 7.568 _ 1.60 276.7 12/13/2014 0.8667 0.7924 0.8198 70.89 46 29 37 7.568 1.58 260.4 12/14/2014 0.8607 0.7932 68203 _ 71.07 46 24 37 7.568 1.59 312.6 12/15/2014 0.8597 _0.7939 0.8206 _�_ 70.55 48 24 _ 37 7.568 _ 1.63 321.0 12/16/2014 0.8692 0.7991 0.8204 69.94 49 38 _ 37 7.568 1.63 200.6 12/17/2014 0.8692 0.8043 0.82 00 71.26 46 48 _ 37 7.568 1.67 159.0 12/18/2014 0.8654 0.8091 0.8218 72.35 _ 43 _ 67 39 7.568 1.70 112.6 12/19/2014 0.8547 0.8054 0.8218 71.17 4_6 80 _ 40 7.568 1.63 95.1 12/20/2014 0.8556 _ 0.7982 _ 0.8217 71.34 _ _- 4_6 26 40 7.568 1.64 293.0 12/21/2014 0.8658 0.8009 68218 70.37 48 24 38 7.568 1.62 314.7 12/22/2014 0.8559 0.7966 0.8219 70.37 49 31 39 7.568 1.62 245.3 12/23/2014 0.8424-,ye 0.7931X- 0.8223 - -- - 39 7.568 0.0 12/24/2014 0.8308 0.7895 0.8225 39 7.568 0.0 12/25/2014 0.8189 0.7981 1_0.8222 39 7.568 0.0 12/26/2014 0.8631 _ 0.8238 _ 69.4_6 4 51 _ __ 239 47 7.568 1.67 _ _ 31.7 12/27/2014 0.8771 0.8261 71.08 48 - 382 60 7.568 1.66 19.8 12/28/2014 0.8764 0.8279 70.12 51 382 73 7.568 1.64 19.8 12/29/2014 0.8444 _ 8286 0.34 _ 71. 49 _ 41 73 7.568 1.64 185.6 12/30/2014 0.8518 0.8084 0.8286 71.34 49 91 75 7.568 1.57 83.2 12/31 /2014 0.8350 0.8164 0.8292 69.14 54 _ 30 _ 73 7.568 1.75 253.4 4.2.66-Ytl U:-�-Mft, ocY,&:60 I,yu3.0V 1,314 2,045 1,434 234.608 45.93 5,744.6 Samples _ 3Q - . .26. 3 a ----- -Zg ---- 28 - 28 _- - 31 31 28 31 Average $ a��'%' _ , Q 0.8211 70_85 47 _- 73 - _ 46 7.568 1.64 185.3 = A�flnu5!► ��e�� was 5- rvdge- rid -ID f-Ae. oi�es�ers. 74-Ae,-�tt�Gs �o c��I�GS�Gc3 s/� l y� ramp��d� 71-A61'eAl'r. no res&I-1- CaA �e- calaolq&d for firer Pri/NGrq di5esferr qa VS,P . 01/16/2015 08:57:38AM LAND APPLIED BIOSOLIDS Page 2 ARCHIE ELLEDGE WASTEWATER TREATMENT PLANT Permit No. NCO037834 12/1 /2014 to 12/31 /2014 Date Dig#1Temp Deg F 382 Dig#2Temp Deg F 383 Dig#3Temp Deg F 384 619#4Temp Deg F 385 Dig#5Temp Deg F 386 Dig#8Temp Deg F 387 12/1 /2014 95 95 95 95 94 95 12/2/2014 96 95 97 96 95 97 12/3/2014 97 97 97 96 96 98 12/4/2014 98 98 98 97 98 97 12/5/2014 99 98 97 99 99 97 12/6/2014 98 99 99 98 98 97 12/7/2014 99 98 99 97 98 98 12/8/2014 98 97 99 97 98 100 12/9/2014 97 100 98 99 98 100 12/10/2014 100 99 98 98 97 99 12/11/2014 99 97 100 98 97 97 12/12/2014 1 98 98 99 98 97 97 12/13/2014 98 98 98 97 97 98 12/14/2014 97 98 97 97 98 99 12/15/2014 97 98 97 98 99 98 12/16/2014 97 98 97 97 99 98 12/17/2014 96 100 100 96 98 98 12/18/2014 1 97 101 100 96 97 99 12/19/2014 98 99 99 98 98 98 12/20/2014 98 99 99 98 97 98 12/21/2014 98 98 98 99 98 99 12/22/2014 97 98 98 98 98 98 12/23/2014 97 98 97 97 98 98 12/24/2014 97 97 98 97_ 98 97 12/26/2014 97 97 98 98 98 98 12/26/2014 98 98 98 100 98 99 12/27/2014 99 98 98 99 98 98 12/28/2014 98 97 98 99 99 98 12/29/2014 98 97 98 98 99 99 12/30/2014 98 98 97 96 98 97 12/31/2014 98 98 97 96 96 97 Total 3,027 3,036 3,038 3,022 3,026 3;036 Samples 31 31 31 31 31 31 Average — - 98 98 98 97 98 98 D i p,64&r Te m?,sr4,+ure, 1noro 4,k )q Be verag e, is q7,O F• MUDDY CREEK WWTP NPDES Permit # NCO050342 2014 Pathogen and Vector Attraction Reduction Summary and Operational Data Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Muddy Creek WWTP NPDES Permit # NC0050342 2014 Compliance Summary Pathogen Reduction PSRP Data for Class B Residuals Anaerobic Digester System Month * * Primary Digester SRT(days)* Monthly Average Temp. °F Monthly Average January 50 94 February 50 95 March 50 95 April 41 96 May 35 95 June 41 97 July 41 97 August 35 96 September 33 95 October 48 94 November 41 95 December 41 96 * SRT = Solids Retention Time; based on % Total Solids. ** Bi-monthly monitoring is required but is actually done on a monthly basis. Page 2 MUDDY CREEK WWTP Pathogen Reduction NPDES Permit # NC0050342 This plant normally operates three Primary Digesters (1, 2, and 3) and one Secondary Digester (4). The SRTs (or MCRTs) for the Muddy Creek WWTP are calculated daily and the summary on Page 1 uses the monthly average since daily values fluctuate so greatly from day to day. The formula below, using data from January 1, 2014, shows an example calculation. See attached monthly LAND APPLIED BIOSOLIDS REPORT, Page 4. Any estimated or qualified data is marked as such on these report pages. Any estimates are not included in the monthly average shown on the previous Page 1. Please find Digester Temperatures on this same report Page 4. Digester #4 is a Secondary Digester and its temperature is not included in determining the monthly average. Occasionally, this Digester's temperature does not get recorded and those instances are either notated or left blank in the data column for `Dig#4 Temp'. FORMULA: [Primary Digester Volume x 8.34 x Primary Digester Transfer %Total Solids] (Pounds of solids in Primary Digesters) [Transfer %Total Solids x 8.34 x Primary Transfer Flow] (Pounds of solids being transferred to Blending Tanks) = PriDigSRT (Days %TS) FROM ATTACHED DATA SHEETS for January 1, 2014: [[PriDigVOL (MG)] x 8.34 x [Trans%TS (%)]] [[Trans%TS (%)] x 8.34 x [PrTranFlo (TGD)/1000]] or 14.8880 x 8.34 x 0.00921 = 0.3750 = 33.19 or [0.0092 x 8.34 x (146.9/1000)] 0.0113 as shown on the report, 33 Days SRT EXAMPLE 02/25/2014 10:20:49 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 PriDig VOL MG Trans %TS % 3 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVOFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 Date PriDig SRT Days %TS 163 �4.8�880( 146.9 49.0 0.6813 0,7051 66.30 54.64 8 50 11,271 7,478 95 95 92 92 95 95 89 89 89 86 1!1/2014 1/2/2014 33 100 4.8880 .92 1.83 1.47 97.9 102.8 0.6992 0.6745 61.22 61.54 32 23 12,002 15,604 95 95 92 92 95 95 1/3/2014 50 4.8880 1/4/2014 48 4.8880 1.82 137.1 0.6658 61.15 21 15,893 95 93 95 8 1/5/2014 36 4.8880 1.39 0.0 205.6 137.1 97.9 0.6915 61.29 29 0 95 94 96 86 1 /6/2014 4.8880 1.24 0.7177 0.7284 0.7 0.7588 0.7738 0.6130 0.6811 0.7463 0.7664 0.7661 0.7387 0,8025 0.8034 0.8049 0.8014 62.41 61.65 61.84 61.27 61.11 62.12 58,70 60.26 60.94 62.12 60.77 61.60 61.29 62.14 61.27 61,54 61.64 61.64 62.69 61.42 60.92 , -74r 7r 35 40 48 54 1 23 57 54 45 60 62 66 63 66 70 68 70 71 72 70 70 1 spa 22,806 15,207 8,684 9,273 12,346 16,7111 28,175 10,187 18,820 0 14,554 19,114 15,314 4,561 10,859 15,656 9,923 19,480 20,870 13,679 3,114 28,414 391.916 95 95 95 96 96 96 96 96 95 95 95 95 95 95 95 95 95 95 95 95 95 95 2,952 92 92 92 93 93 93 93 93 92 92 92 93 92 92 92 92 93 93 93 93 91 92 2,865 94 95 94 95 95 95 96 96 96 96 96 96 95 96 96 96 95 95 95 95 95 95 2,955 87 88 84 87 88 89 87 89 89 87 88 89 89 87 87 87 88 89 88 88 89 87 84 2,715 24 4.8880 1.33 36 4.8880 1.33 E/8/2O14 504.8880 1.46 71 4.8880 1.52 68.5 1/11/2014 62 4.8880 1.42 78.3 1/12/ 0014 48 4.8880 1.44 102.8 1/13/ 0014 1/14/2014 32 4.8880 4,8880 1.32 551.8 0.0 1/15/2014 20 244.8 1/16/2014 62 78.3 1/17/2014 28 V 176.3 1/18/ 0014 1/19/2014 4.8880 0.0 0.0 1/20/2014 1 /21 /2014 37 28 4.8880 4.8880 1.32 1.30 132.2 176.3 1/22/2014 33 4.8880 1.25 146.9 0.8254 0.8108 1/23/2014 111 4.8880 1.24 44.1 1/24/2014 53 4.8880 1.40 93.0 0.8295 0.8390 0.8316 0.8408 0.8487 0.8590 0.8395 0.8406 ." 1/25/2014 37 4.8880 1.42 132.2 1 /26/2014 1/27/2014 59 33 4.8880 4.8880 1.43 1.59 83.2 146.9 1/28/2014 1 /29/2014 1/30/2014 1/31l2014 29 40 166 25 4.8880 4.8880 4.8880 4.8880 1.46 1.34 1.27 1.74 171.4 122.4 29.4 195.8 Total 1,349 151.5280 6y)Af `, •.,"' 28 31 31 31 31 31 Samples 27 31 28 31 31 28 Average 50 4.8880 1.41 108.0 0.7659 61.28 49 12,642 95 92 95 88 Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Muddy Creek WWTP NPDES Permit # NCO050342 2014 Compliance Summary Vector Attraction Reduction Requirements for Class B Residuals Compliance determination by Calculation of Volatile Solids Reduction across the Anaerobic Digesters as the treatment system. Calculated %VSR (38% Minimum) Monthly Average VAR Option 1 Prim Digester System January 49 65 r 61 56 55 June 52 ** Jul 53 Au st 54 September 57 October 57 November 59 December 56 * Bimonthly monitoring is required but is actually done on a monthly basis. ** Beginning in June, 2014, there is an offset of time factored in regarding digester solids retention time (or MCRT). A given month's %VSR is now calculated using the previous month's SRT average. See page 2 of this section for the formula used for the first five months of 2014, as well as the formula now used beginning in June of 2014. The equation used for calculating the above %VSRs is from the EPA White House Manual, Control of Pathogens and Vector Attraction in Sewage Sludge, Chapter 10 and Appendix C. Page 2 Muddv Creek WWTP Vector Attraction Reduction NPDES Permit # NCO050342 Data submitted in the chart on Page 1 of this summary shows that the calculated monthly average Volatile Solids Reduction meets the minimum of 38% VSR requirement over the Primary Digester System at the Muddy Creek WWTP for the year of 2014. Volatile Solids Reduction (VSR) is calculated by the Van Kleeck equation using the digester feed and digester stabilized transfer sludge volatile fractions. While there was previously no offset necessary for digester Solids Retention Times (or MCRTs) due to the consistency with which these digesters were operated, upon in-house review, the City began in June of 2014 calculating one month's %VSR using the previous month's SRT average. This more accurately reflects current digester operations. Any data qualified by the lab .is marked as such on data sheets. Also, in instances when a daily sample was not collected for %Volatile Solids analysis of the Transfer (`Trans') Sludge, an estimated value was used along with actual flows for that day in order to calculate treatment in the digesters. Any estimated daily values are marked as such on data sheets, but the monthly average values (shown on the previous Page 1) were calculated excluding this estimated data in order to certify compliance. The values for January 2; 2014 from the attached LAND APPLIED BIOSOLIDS report Page 4 are used in the example equation below. This is the formula -used for the period of Jan. — May, 2014. The heading `VolFrac 311+318' refers to the Volatile Fraction of the Digester feed samples and the heading `DTrVoFrac' refers to the Volatile Fraction of the stabilized Primary Digester transfer samples. The calculated Percent Volatile Solids Reduction is indicated by the heading `PriDig%VSRed (%)'. FORMULA January — May, 2014: [VolFrac 3l l + 318] - [DTrVoFrac/100] = PriDi VSR (%) (Feed) (Transfer) g [VolFrac 311+ 318] - [(VolFrac 311 + 318) x (DTrVoFrac/100)] (Feed) (Feed) (Transfer) FROM ATTACHED DATA SHEETS for January 2, 2014: 0.7051— 0.5464 = 0.1587 = 0.4962 or -as shown on the report, 50% VSR 0.7051 - (0.7051 x 0.5464) 0.3198 ----------------------------------------------------------------------------------------------------------------- See on the attached LAND APPLIED BIOSOLIDS report Page 4,, June 1, 2014, for the current method of calculating %VSR. The new heading of "Feed Vo1Fr 30 day mavg" is the Feed Volatile Fraction 30 day moving average. See monthly averages June — Dec., 2014, in the chart on the previous Page 1 of this summary and attached daily data. FORMULA June — December, 2014: [Feed Vol Frac 30 day mavg] - [DTrVoFrac/100] - PriDi VSR (Feed) (Transfer) g ( ) [Feed Vol Frac 30 day mavg] - [(Feed Vol Frac 30 day mavg) x (DTrVoFrac/100)] (Feed) (Feed) (Transfer) FROM ATTACHED DATA SHEETS for June 1, 2014: 0.8472 — 0.7193 = 0.1279 = 0.5378 or as shown on the report, 54% VSR 0.8472 — (0.8472 x 0.7193) 0.2378 Van Kleeck Equation used: %VS Reduction = 1%VS (Feed)1- f%VS (Stabilizedil [%VS (Feed)] - [%VS (Feed) x %VS (Stabilized)]. %VS (Feed) = Volatile fraction of raw and thickened sludges fed to primary digesters %VS (Transfer) = Volatile fraction of stabilized sludge transferred from primary digesters EXAMPLE 02/25/2014 10:20:49 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 p' #4 PriDig PriDig Trans PrTranFlo VolFrac DTr SRT VOL %TS Days %TS MG %u TGD 311+318 % 163 492 93 357 389 42 33 4.8880 0.92 146.9 0.6813 6E 100 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4,8880 4.8880 1.83 1.47 1.82 1.39 1.24 1.33 1.33 1.46 1.52 1.42 1.44 1.32 1.38 1.56 1.28 1.32 1.30 1.25 1.24 1.40 1.42 1.43 1.59 1.46 1.34 1.27 1.74 49.0 97.9 102.8 137.1 0.0 205.6 137.1 97.9 68.5 78.3 102.8 151.8 0.0 244.8 78.3 176.3 0.0 0.0 132.2 176.3 146.9 44.1 93.0 132.2 83.2 146.9 171.4 122.4 29.4 195.8 0,7051 06992 0.6658 0.6915 0.7177 0.7284 0.7582 0.7588 0.7738 0.6130 0.6811 0.7463 0.7664 0.7661 0.7387 0.8025 0.8034 0.8049 0.8014 0.8254 0.8108 0.8295 0.8390 0,8316 0,8408 0.8487 0.8590 0.8395 0.8406 5< 6 6' 6' 6; 6 6' 6 6 6 6 5 E E E E f f 01/7/2014 50 48 36 24 36 50 71 62 1 /8/2014 1l9/2014 1110/2014 1111/2014 1/12/2014 48 1/13/2014 32 1/14/2014 1/15/2014 1/16/2014 20 62 1/17/2014 1/18/2014 1/19/2014 1 /20/2014 1 /21 /2014 1 /22/2014 1 /23/2014 1 /24/2014 1/25/2014 1/26/2014 1/27/2014 1 /28/2014 1 /29/2014 1/30/2014 1 /31 /2014 28 37 28 33 111 53 37 59 33 29 40 166 25 _ e anc o 93 7411 1.7 Total 1,34V io,.ocov Samples 27 31 28 31 Average 50 4.8880 1.41 108.0 0.7659 VoFrac PriDig% Trans lb Dig #1 Dig #2 Tee#3 Teto rn VSRed %TS Temp Temp P p %, Ib %TS Deg F Deg F Deg F Deg F 2 751 741 775 776 777 778 ;.30 8 11,271 95 92 95 89 ,.64 50 7,478 95 92 95 89 .22 32 12,002 95 92 95 89 .54 23 15,604 95 92 95 88 1.15 21 15,893 95 93 95 86 1.29 29 0 95 94 96 86 ,.41 35 22,806 95 92 94 87 1.65 40 15,207 95 92 95 88 ).27 52 11,921 95 92 95 86 1.84 48 8,684 95 92 94 84 1.27 54 9,273 96 93 95 87 88 1.11 1 12,346 96 93 95 2.12 23 16,711 96 93 95 89 0 96 93 96 87 8.70 57 28,175 96 93 96 89 0.26 54 10,187 96 93 96 89 0.94 45 18,820 96 92 96 87 0 95 92 96 87 0 95 92 96 88 �95 92 96 892.12 60 14,554 96 89 i0.77 62 19,114 95 92 95 87 0.60 66 15,314 95 0.29 63 4,561 95 92 96 87 i2.14 66 10,859 95 92 96 87 31.27 70 15,656 95 92 96 88 i1.54 68 9,923 95 93 95 89 70 19,480 95 93 95 88 i1.64 93 95 88 31.64 71 20,870 95 32.69 72 13,679 95 93 95 89 31.42 70 3,114 95 91 95 87 80.92 70 28,414 84 95 92 95 15.75 1,378 391,916 2,952 2,865 2,955 2,715 28 28 31 31 31 31 31 95 88 61.28 49 12,642 95 92 2 751 741 775 776 777 778 ;.30 8 11,271 95 92 95 89 ,.64 50 7,478 95 92 95 89 .22 32 12,002 95 92 95 89 .54 23 15,604 95 92 95 88 1.15 21 15,893 95 93 95 86 1.29 29 0 95 94 96 86 ,.41 35 22,806 95 92 94 87 1.65 40 15,207 95 92 95 88 ).27 52 11,921 95 92 95 86 1.84 48 8,684 95 92 94 84 1.27 54 9,273 96 93 95 87 88 1.11 1 12,346 96 93 95 2.12 23 16,711 96 93 95 89 0 96 93 96 87 8.70 57 28,175 96 93 96 89 0.26 54 10,187 96 93 96 89 0.94 45 18,820 96 92 96 87 0 95 92 96 87 0 95 92 96 88 �95 92 96 892.12 60 14,554 96 89 i0.77 62 19,114 95 92 95 87 0.60 66 15,314 95 0.29 63 4,561 95 92 96 87 i2.14 66 10,859 95 92 96 87 31.27 70 15,656 95 92 96 88 i1.54 68 9,923 95 93 95 89 70 19,480 95 93 95 88 i1.64 93 95 88 31.64 71 20,870 95 32.69 72 13,679 95 93 95 89 31.42 70 3,114 95 91 95 87 80.92 70 28,414 84 95 92 95 15.75 1,378 391,916 2,952 2,865 2,955 2,715 28 28 31 31 31 31 31 95 88 61.28 49 12,642 95 92 EXAMPLE 07/17/2014 09:09:55 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 06/01/14 TO 06/30/14 PrTranFlo TGD 357 Feed VoIFr 30 day Mavg 921 DTrVOFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Tema Deg F 777 Dig #4 Temp Deg F 778 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 0.8472 0.8474 0.8473 71,93 73.83 72.22 72.64 72.03 72.22 72.73 �4 70.76 72.07 72.07 72.22 71.81 73.44 72.73 73.81 72.39 72.09 72.65 72.80 72.64 73.83 72.97 72.22 74.24 72.50 73.53 72.90 54 49 53 52 53 53 52�< _ 56 53 53 54 55 51 53 50 53 54 52 52 53 50 52 54 49 53 51 52 16,1 9 15,170 14,619 16,22298 15,716 4,2420 0 1,7460 18,526 23,458 16,774 15,080 28,208 14,550 19,799 17,213 15,568 18,655 4,703 20,714 6,347 11,547 4,360 23,287 18,847 13,941 6,261 11,083 97 97 97 98 98 98 98 99 99 98 98 98 98 97 99 98 98 98 98 98 99 99 98 97 98 99 99 95 95 9996 97 101 96 96 96 97 _ 99 96 96 96 95 96 95 96 96 97 96 97 96 97 97 99 95 96 97 97 97 97 974.8880 98 98 97 98 98 98_ 98 98 97 98 97 95 97 97 97 97 97 97 98 98 96 96 97 97 97 94 94 95 96 94 94 94 96 96 ` 96 96 96 97 - 97 97 97 97 96 97 97 97 - 97 97 96 97 97 97 96_... 172.9 170.0 4.8880 4.8880 1.14 1.07 ff 4.8880 1.08 1623 4.8880 1.06 183.5 0.8471 1.18 159.7 0.8465 6/6/2014 104 4,8880 1.08 47.1 0.8463 0.8465 0.8468 0.8473 0.8470 0.8465 0.8470 6/7/2014 6/8/2014 4.8880 4.8880 1.21 * 0.0 0.0 6/9/2014 283 %c 4.8880 17.3 6/10/2014 4.8880 0.0 6/11/2014 38 4.8880 1.71 _ 129.9 6/12/2014 19 4.8880 1.11 253.4 6/13/2014 27 4.8880 1.11 181.2 0.8469 6/14/2014 34 4.8880 1.26 143.5 0.8488 6/15/2014 6/16/2014 6/17/2014 22 36 25 4.8880 4.8880 4.8880 1.49 1.28 1.21 227.0 136.3 196.2 0.8495 0.8498 0.8492 6/18/0014 30 4.8880 1.26 163.8 0.8488 6/19/2014 35 4.8880 1.34 139.3 0.8485 6/20/2014 28 4.8880 1.29 173.4 0.8482 6/21 /2014 101 4.8880 1,17 48.2 0.8480 6/22/2014 25 4.8880 0.8484 6/23/2014 6/24/2014 68 38 4.8880 4.8880 M25198.7 71.8 129.4 0.8487 0.8485 6/25/2014 6/26/2014 104 25 4.8880 4.8880193.9 47.1 0.8483 0.8491 6/27/2014 29 4.8880 1.32 171.2 0.8491 6/28/2014 35 4.8880 1.20 139.3 0.8487 6/29/2014 66 4.8880 1.02 73.6 0.8489 0.84 00 6/30/2014 39 4.8880 1.07 124.2 i S2AR eF 1 2F,'� 2,897 2,915 2,882 -'-! �91 .329 2,942 Total I U / i 114b.b4uu ) I . w A,o:r..c. - - - - - - - 25 - 29 Samples 26 30 26 30 30 26 Average 41 4.8880 1.21 128.5 0.8480 72.64 52 _1 3 , 494 Primary Digester Temperature monthly average is 97°F. * Estimate. 30 30 30 30 98 97 97 96 02/24/2014 01:39:24 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temn Deg F 776 Dig #2 Temp Deg F 776 Dig #3 Temo Deg F 777 Dig #4 Temp Deg F 778 1/1/2014 33 4.8880 0.92 146.9 0.6813 66.30 8 11,271 95 92 95 89 1/2/2014 100 4.8880 1.83 49.0 0.7051 54.64 50 7,478 95 92 95 89 1/3/2014 50 4.8880 1.47 97.9 0.6992 61.22 32 12,002 95 92 95 89 1/4/2014 48 4.8880 1.82 102.8 0.6745 61.54 23 15,604 95 92 95 88 1/5/2014 1 36 4.8880 1.39 137.1 0.6658 61.15 21 15,893 95 93 95 86 1/6/2014 4.8880 1.24 0.0 0.6915 61.29 29 0 95 94 96 86 1R/2014 24 4.8880 1.33 205.6 0.7177 62.41 35 22,806 95 92 94 87 1/8/2014 36 4.8880 1.33 137.1 0.7284 61.65 40 15,207 95 92 95 88 1/9/2014 50 4.8880 1.46 97.9 0.7582 60.27 52 11,921 95 92 95 86 1/10/2014 71 4.8880 1.52 68.5 0.7588 61.84 48 8,684 95 92 94 84 1 /11 /2014 62 4.8880 1 1.42 78.3 0.7738 61.27 54 9,273 96 93 95 87 1/12/20 4 -48 4.8880 1.44 102.8 0.6130 61.11 1 12,346 96 93 95 88 1/13/2014 32 4.8880 1.32 151.8 0.6811 62.12 23 16,711 96 93 95 89 1 /14/2014 4.8880 0.0 0.7463 0 96 93 96 87 1/15/2014 20 4.8880 1.38 244.8 0.7664 58.70 57 28,175 96 93 96 89 1 /16/2014 62 4.8880 1.56 78.3 0.7661 60.26 54 10,187 96 93 96 89 1/17/ 0014 28 4.8880 1.28 176.3 0.7387 60.94 45 18,820 96 92 96 87 1 /18/2014 4.8880 0.0 0.8025 0 95 92 96 87 1 /19/2014 4.8880 0.0 0.8034 0 95 92 96 88 1/20/2014 37 4.8880 1,32 132.2 0.8049 62.12 60 14,554 95 92 96 89 1 /21 /2014 28 4.8880 1.30 176.3 0.8014 60.77 62 1 19,114 95 93 96 89 1/22/2014 33 4.8880 1.25 146.9 0.8254 61.60 66 1 15,314 95 92 95 87 1/23/2014 111 4.8880 1.24 44.1 0.8108 61.29 63 4,561 95 1 92 96 87 1/24/2014 53 4.8880 1.40 93.0 0.8295 62.14 66 10,859 95 92 96 87 1/25/2014 37 4.8880 1.42 132.2 0.8390 61.27 70 15,656 95 92 96 88 1/26/2014 59 4.8880 1.43 83.2 0.8316 61.54 68 9,923 95 93 95 89 1/27/2014 33 4.8880 1.59 146.9 0,8408 61.64 70 19,480 95 93 95 88 1/28/2014 29 4.8880 1.46 171.4 0.8487 61.64 71 20,870 95 93 95 88 1/29/2014 40 4.8880 1.34 122.4 0.8590 62.69 72 13,679 95 93 95 89 1 /30/2014 166 4.8880 1.27 29.4 0.8395 61.42 70 3,114 95 91 95 87 1/31/2014 25 4.8880 1.74 195.8 0.8406 60.92 70 28,414 95 92 95 84 Total 1,349 1bl.!)ZbU 39.4( 3,34tUJ Z3.14.3'1 1,/ 10./0 1,010 ow 1,V 10 4,vQ4 c,oUU G,JUU 4,1 io Samples 27 31 28 31 31 28 28 31 31 31 31 31 Average 50 4.8880 1.41 108.0 0.7659 61.28 49 12,642 95 92 95 88 Primary Digester Temperature monthly average is 94°F. 03/13/2014 04:22:59 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO060342 02/01/14 TO 02/28/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 761 Trans lb %TS lb %TS 741 Dig #1 Temo Deg F 776 Dig #2 Temp Deg F 776 Dig #3 Temn Deg F 777 Dig #4 Temp Deg F 778 2/1 /2014 36 4.8880 1.35 137.1 0.8448 62.96 69 16,436 95F92 95 88 2/2/2014 4.8880 0.0 0.8491 0 96 95 90 2/3/2014 37 4.8880 1.41 132.2 0.8358 63.12 66 15,546 96 95 85 2/4/2014 67 4.8880 1.32 73.4 0.8470 63.64 68 8,080 96 95 89 2/5/2014 55 4.8880 1.25 88.1 0.8635 64.00 72 9,184 96 96 91 2/6/2014 2/7/2014 33 42 4.8880 4.8880 1.45 1.26 146.9 117.5 0.8631 0.8648 63.45 64.29 72 72 17,765 12,347 95 95 92 92 95 95 91 89 2/8/2014 83 4.8880 1.33 58.8 0.8647 64.66 71 6,522 95 93 95 90 2/9/2014 32 4.8880 1.23 151.8 0.8620 65.85 69 15,572 95 93 95 91 2/10/2014 29 4.8880 1.22 166.5 0.7817 63.93 51 16,941 95 93 95 90 2/11/2014 77 4.8880 1.22 63.6 0.7733 63.93 48 6,471 95 93 96 91 2/12/2014 38 4.8880 1.24 127.3 0.8460 64.52 67 13,165 96 92 96 91 2/13/2014 38 4.8880 1.37 127.3 0.8575 63.50 71 1.4,545 96 92 96 91 2/14/2014 83 4.8886 1.22 58.8 0.8525 65.57 67 5,983 96 92 96 90 2/15/2 114 4.8880 0.0 0.8125 0 95 92 96 90 2/ 66/2 114 4.8880 0.0 0.8275 0 96 92 96 90 2/17 014 29 4.8880 1.28 168.0 0.8422 66.41 63 17,934 96 92 96 90 2/18/ 0014 2/19/2014 31 25 4.8880 4.8880 1.27 1.68 156.7 195.8 0.8423 0.8479 65.35 63.92 65 68 16,597 25,801 96 95 93 93 96 96 90 90 2/20/2014 51 4.8880 1.24 95.1 0.8540 65.32 68 9,835 96 93 96 91 2/21/2014 55 4.8880 1.19 88.1 0.8491 66.39 65 8,744 96 93 96 89 2/22/2014 42 4.8880 1.24 117.5 0.8298 65.32 61 12,151 96 93 96 91 2/23/2014 28 4.8880 1.58 172.7 0.8037 63.29 58 22,757 96 93 96 92 2/24/2014 90 4.8880 1.34 54.1 0.8174 64.18 60 6,046 97 93 96 92 2/25/2014 32 4.8880 1.49 154.8 0.8276 65.10 61 19,236 97 93 96 92 2/26/2014 106 4.8880 1.19 45.9 0.8395 64.71 65 4,555 96 93 96 92 2/27/2014 35 4.8880 1.52 138.2 0.8357 63.82 65 17,519 96 93 95 92 2/28/2014 62 4.8880 1.20 79.4 0.8477 65.83 65 7,946 96 92 95 91 Total 1,238 136.8640 32.99 2,915.6 23.4825 1,613.07 1,628 3Yb,bfb z,00-1 Z,aa4 c,oi 1 L,O4C7 Samples 25 28 25 28 28 25 25 28 28 28 28 28 Averaae 50 4.8880 1.32 104.1 0.8387 64.52 65 11,667 96 93 96 90 Primary Digester Temperature monthly average is 95°F- 04/16/2014 04:33:47 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 03/01/14 TO 03/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temo Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temu Deg F 777 Dig #4 Temp Deg F 778 3/1/2014 50 4.8880 1 1.33 97.9 0.8522 65.41 1 67 10,859 96 93 95 91 3/2/2014 34 4.8880 1.12 142.1 0.8525 64.29 69 13,273 96 93 96 90 3/3/2014 34 4.8880 1.20 143.1 0.8480 81.67 20 14,321 96 93 95 92 3/4/2014 113 4.8880 1.19 43.3 0.8277 67.23 57 4,297 95 92 95 91 3/5/2014 33 4.8880 1.16 146.3 0.8456 67.24 63 14,154 95 92 95 89 3/6/2014 48 4.8880 1.31 102.8 0.7899 67.18 46 11,231 95 92 95 88 3/7/2014 37 4.8880 1.39 132.8 0.8260 66.91 57 15,395 95 91 95 90 3/8/2014 37 4.8880 1.18 133.2 0.8104 67.80 51 13,108 95 91 95 88 3/9/2014 39 4.8880 1.24 124.8 0.8218 66.13 58 12,906 95 92 96 90 3/10/ 0014 29 4.8880 1.15 171.5 0.8283 66.96 58 16,449 96 93 96 92 3/11/2014 62 4.8880 1.15 79.2 0.8593 68.70 64 7,596 96 94 96 91 3/12/2014 44 4.8880 1.16 110.7 0.8610 68.10 66 10,710 96 94 96 91 3/13/2014 33 4.8880 1.18 148.3 0.8411 66.95 62 14,594 96 93 96 91 3/14/2014 44 4.8880 1.30 112.1 0.8531 67.69 64 12,154 96 92 96 91 3/15/2014 42 4.8880 1.24 115.1 0.8349 67.74 58 11,903 96 92 96 92 3/16/2014 100 4.8880 1.12 49.0 0.8618 67.86 66 4,577 96 92 96 90 3/17/ 0014 25 4.8880 1.25 193.7 0.8576 68.00 65 20,193 96 92 96 91 3/18/2014 30 4.8880 1.27 163.9 0.8337 1 67.72 58 17,360 96 92 96 1 91 3/19/2014 31 4.8880 1.32 156.7 0.8631 67.42 67 17,251 96 93 95 91 3/20/2014 49 4.8880 1.31 98.9 0.8591 67.94 65 10,805 96 97 95 91 3/21/2014 67 4.8880 1.10 73.4 0.8569 69.09 63 6,734 96 92 96 91 3/22/2014 27 4.8880 1.24 181.7 0.8557 67.74 65 18,791 96 92 96 92 3/23/2014 34 4.8880 1.30 142.0 0.8589 67.69 66 15,396 96 93 96 92 3/24/2014 137 4.8880 1.39 35.7 0.8649 66.91 68 4,139 1 96 93 96 92 3/25/2014 28 4.8880 1.31 175.5 0.8612 67.94 66 19,174 96 93 96 92 3/26/2014 31 4.8880 1.29 156.0 0.8625 67.44 67 16,783 95 92 96 91 3/27/2014 84 4.8880 1.20 57.9 0.8566 68.33 64 5,795 95 92 96 91 3/28/2014 45 4.8880 1.10 108.6 0.8442 69.09 59 9,963 95 92 95 89 3/29/2014 27 4.8880 1.30 178.7 0.8573 69.23 63 19,375 96 92 95 89 3/30/2014 107 4.8880 1.19 45.5 0.8493 69.75 59 4,516 96 92 95 90 3/31/2014 34 4.8880 1.50 144.E 0.8634 69.33 64 18,089 96 92 95 90 Total 1,536 151.5280 38.49 3,765.0 26.2577 2,111.47 1,883 391,891 z,967 z,bbd z,ub;j z,alu Samples 31 31 31 31 31 31 31 31 31 31 31 31 Average 50 4.8880 1.24 121.5 0.8470 68.11 61 12,642 96 93 96 91 Primary Digester Temperature monthly average is 95°F. 05/21/2014 02:13:10 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 04/01/14 TO 04/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temo Deg F 776 Dig #2 Temp Deg F 776 Dig #3 Temo Deg F 777 Dig #4 Temp Deg F 778 4/1/2014 34 4.8880 1.12 144.6 0.8624 69.64 63 13,507 96 93 95 92 4/2/2014 42 4.8880 1.22 116.8 0.8722 70.49 65 11,884 97 94 96 92 4/3/2014 60 4.8880 1.25 81.9 0.8621 68.80 65 8,538 93 96 95 91 4/4/2014 46 4.8880 1.13 107.1 0.8480 69.91 58 10,093 96 93 95 92 4/5/2014 41 4.8880 1.51 118.4 0.8474 70.86 56 14,911 95 94 96 92 4/6/2014 28 4.8880 1.53 176.4 0.8546 69.93 60 22,509 96 94 96 93 4/7/2014 27 4.8880 1.11 180.9 0.8405 70.27 55 16,747 95 93 96 93 4/8/2014 37 4.8880 1.15 132.1 0.8242 ` 71.30 47 %; 12,670 95 94 95 93 4/9/2014 37 4.8880 1.12 133.3 0.8590 71.43 59 12,451 95 94 97 93 4/10/2014 46 4.8880 1.11 105.5 0.8638 69.37 64 9,767 96 93 98 93 4/11/2014 29 4.8880 1.12 168.8 0.8489 69.64 59 15,767 95 93 99 93 4/12/2014 30 4.8880 1.09 1 162.6 0.8448 69.72 58 14,781 95 93 100 93 4/13/2014 78 4.8880 1.65 63.0 0.8552 70.30 60 8,669 96 94 101 92 4/14/2014 47 4.8880 1.04 103.9 0.8649 71.15 61 9,012 98 94 102 93 4/15/2014 29 4.8880 1.23 166.8 0.8094 69.92 45 17,111 98 94 104 94 4/16/2014 24 4.8880 1.56 206.0 0.7816 69.23 37 26,801 98 93 103 94 4/17/2014 40 4.8880 1.04 121.2 0.8395 70.19 55 10,512 97 93 102 94 4/18/2014 36 4.8880 1.27 137.3 0.8439 71.65 53 14,543 96 93 103 94 4/19/2014 39 4.8880 1.18 124.0 0.8397 69.49 57 12,203 96 93 103 94 4/20/2014 35 4.8880 1.13 140.9 0.8414 70.80 54 13,279 98 93 99 1 94 4/21/2014 47 4.8880 1.05 103.6 0.8483 71.43 55 9,072 98 94 99 94 4/22/2014 33 4.8880 1.20 147.0 0.8478 70.00 58 14,712 98 93 100 94 4/23/2014 34 4.8880 1.07 142.0 0.8498 71.03 57 12,672 98 93 98 94 4/24/2014 50 4.8880 1.04 97.6 0.8492 1 69.23 60 8,465 97 94 98 94 4/25/2014 30 4.8880 1.21 162.1 0.8395 71.07 53 16,358 96 94 97 94 4/26/2014 29 4.8880 1.16 1 168.7 0.8345 71.55 50 16,321 96 95 97 94 4/27/2014 113 4.8880 1.48 43.3 0.8372 70.27 54 5,345 96 1 95 97 94 4/28/2014 23 14.8880 1.09 209.1 0.8419 70.64 55 19,008 96 95 97 94 4/29/2014 62 4.8880 1.10 78.9 0.8490 71.82 55 7,238 96 94 96 95 4/30/2014 32 4.8880 1.10 151.3 0.8462 70.91 56 13,880 96 94 96 94 Total 1,238 146.6400 36.06 3,995.1 25.3468 2,112.08 1,686 398,826 2,888 2,812 2,950 2,800 Samples 30 30 30 30 30 30 30 30 30 30 30 30 Averaae 41 4.8880 1.20 133.2 0.8449 70.40 56 13,294 96 94 98 93 %, Data qualified by Lab. Primary Digester Temperature monthly average is 96°F. 06/12/2014 03:05:07 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 05/01/14 TO 05/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temn Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temn Deg F 777 Dig #4 Temp Deg F 778 5/1/2014 43 4.8880 1.11 114.1 0.8396 71.17 53 10,563 97 94 97 94 5/2/2014 40 4.8880 1.30 122.4 0.8500 70.77 57 13,271 96 95 96 94 5/3/2014 29 4.8880 1.12 168.3 0.8530 71.43 57 15,721 96 95 97 94 5/4/2014 30 4.8880 1.16 160.9 0.8468 67.24 63 15,566 95 95 97 94 5/5/2014 48 4.8880 1.13 102.7 0.8323 72.57 47 9,679 @ 95 94 94 5/6/2014 29 4.8880 1.12 168.9 0.8581 71.43 59 15,777 94 96 96 94 5/7/2014 59 4.8880 1.10 83.3 0.8509 70.91 57 7,642 94 96 96 94 5/8/2014 32 4.8880 1.13 152.9 0.8427 71.68 53 14,410 94 95 96 94 5/9/2 114 46 4.8880 1.20 105.3 0.8511 70.83 58 10,538 96 95 96 95 5/10/2014 33 4.8880 1.18 146.4 0.8472 72.03 54 14,408 95 96 96 94 6111 01014 45 4.8880 1.49 107.9 0.8527 71.81 56 13,408 96 95 97 94 5/12/2014 30 4.8880 1.23 161.6 0.8565 71.54 58 16,577 95 94 97 95 5/13/2014 31 4.8880 1.42 155.6 0.8326 71.13 50 18,427 96 95 97 95 5/14/2014 29 4.8880 1.31 170.5 0.8501 70.99 57 18,628 96 95 97 95 5/15/2014 57 4.8880 1.32 85.1 0.7876 70.45 36 9,368 96 95 97 95 5/16/2014 25 4.8880 1.16 194.3 0.8185 71.55 44 18,797 96 94 96 94 5/17/2014 29 4.8880 1.23 166.8 0.8368 71.54 51 17,111 96 93 96 94 5/18/2014 23 4.8880 1.30 210.0 1 0.8493 70.77 57 22,768 96 94 96 94 5/19/2014 24 4.8880 1.34 205.7 0.8641 71.64 60 22,988 96 93 97 94 5/20/2014 30 * 4.8880 1.30 162.9 0.8593 71.54 59 17,662 96 93 97 94 5/21/2014 39 4.8880 1.33 125.9 0.8608 71.43 60 13,965 96 93 97 94 5/22/2014 46 4.8880 1.40 105.8 0.8558 71.43 1 58 12,353 96 94 96 95 5/23/2014 29 4.8880 1.23 169.6 0.8444 71.54 54 17,398 94 96 96 94 5/24/2014 29 4.8880 1.26 168.2 0.8575 72.22 57 17,675 92 96 96 95 5/25/2014 27 4.8880 1.10 180.3 0.8620 72.73 57 16,541 96 96 96 94 5/26/2014 44 4.8880 1.40 111.4 0.8621 71.43 60 13,007 96 96 96 95 5/27/2014 54 4.8880 1.25 91.3 0.8338 72.80 47 9,518 96 96 96 96 5/28/2014 20 14.8880 1.12 242.1 0.8488 72.32 53 22,614 96 96 96 96 5/29/2014 26 4.8880 1.16 184.5 0.8596 72.41 57 17,849 98 99 97 96 5/30/2014 21 4.8880 1.21 228.4 0.8445 71.90 53 23,049 98 96 96 .95 5/31 /2014 40 4.8880 1 1.16 123.6 0.8492 1 71.55 55 1 11,958 97 96 1 96 96 Total 1,089 151.5280 38.27 4,676.7 26.2577 2,214.81 1,695 479,236 2,871 2,947 2,986 2,931 Samples 31 31 31 31 31 31 31 31 30 31 31 31 Average 35 4.8880 1.23 150.9 0.8470 71.45 55 15,459 96 95 96 95 Primary Digester Temperature * Data qualified by Lab. @ No Digester temperature due monthly average is 95°F• to maintenance on heat exchanger. 07/17/2014 09:09:55 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 06/01/14 TO 06/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 6/1/2014 28 4.8880 1.14 172.9 0.8472 71.93 54 16,439 97 95 97 94 6/2/2014 29 4.8880 1.07 170.0 0.8474 73.83 49 15,170 97 95 97 94 6/3/2014 30 4.8880 1.08 162.3 0.8473 72.22 53 14,619 97 99 96 95 6/4/2014 27 4.8880 1.06 183.5 0.8471 72.64 52 16,222 98 97 97 96 6/5/2014 31 4.8880 1.18 159.7 0.8465 72.03 53 15,716 98 101 98 96 6/6/2014 104 4.8880 1.08 47.1 0.8463 72.22 53 4,242 97 96 97 96 6/7/2014 4.8880 0.0 0.8465 0 98 96 98 94 6/8/2014 4.8880 1.21 0.0 0.8468 0 98 96 97 94 6/9/2014 283 4.8880 17.3 0.8473 72.73* 52* 1,746 99 96 98 94 6/10/2014 4.8880 0.0 0.8470 0 98 97 98 96 6/11/2014 38 4.8880 1.71 129.9 0.8465 70.76 56 18,526 99 99 98 96 6/12/2014 19 4.8880 1.11 253.4 0.8470 72.07 53 23,458 99 96 98 96 6/13/2014 27 4.8880 1.11 181.2 0.8469 72.07 53 16,774 98 96 98 96 6/14/2014 34 4.8880 1.26 143.5 0.8488 72.22 54 15,080 98 96 97 96 6/15/2014 22 4.8880 1.49 227.0 0.8495 71.81 55 28,208 98 95 98 97 6/16/2014 36 4.8880 1.28 136.3 0.8498 73.44 51 14,550 98 96 97 97 6/17/2014 25 4.8880 1.21 196.2 0.8492 72.73 53 19,799 97 95 95 97 6/18/2014 30 4.8880 1.26 163.8 0.8488 73.81 50 17,213 99 96 97 97 6/19/2014 35 4.8880 1.34 139.3 0.8485 72.39 53 15,568 98 96 97 97 6/20/2014 28 4.8880 1.29 173.4 0.8482 72.09 54 18,655 98 97 97 96 6/21/2014 101 4.8880 1.17 48.2 0.8480 72.65 52 4,703 98 96 97 97 6/22/2014 25 4.8880 1.25 198.7 0.8484 72.80 52 20,714 98 97 97 97 6/23/2014 68 4.8880 1.06 71.8 0.8487 72.64 53 6,347 98 96 97 97 6/24/2014 38 4.8880 1.07 129.4 0.8485 73.83 50 11,547 99 1 97 98 97 6/25/2014 104 4.8880 1.11 47.1 0.8483 72.97 52 4,360 99 97 98 97 6/26/2014 25 4.8880 1.44 193.9 0.8491 72.22 54 23,287 98 99 1 96 96 6/27/2014 29 4.8880 1 1.32 171.2 0.8491 74.24 49 18,847 97 95 96 97 6/28/2014 35 4.8880 1.20 139.3 0.8487 72.50 53 13,941 98 96 97 97 6/29/2014 66 4.8880 1.02 73.6 0.8489 1 73.53 51 6,261 99 97 97 97 6/30/2014 39 4.8880 1.07 124.2 0.8490 72.90 52 11,083 1 99 97 97 96 Total l U/ I .146.6400 51.30 Samples 26 30 26 Average 41 4.8880 1.21 3,854.2 25.4391 30 30 128.5 0.8480 1000-jb 15b3 5)1 5LJ 26 - 26 29 72.64 52 13,494 Primary Digester Temperature monthly average is 97°F. ;; Estimate. 2,942 2,897 2,915 2,882 30 30 30 30 98 97 97 96 i 08/12/2014 03:19:23 PM LAND APPLIED BIOSOLIDS MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 07/01/14 ' O 07/31/14 Page 4 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VblFr 30 day Mavg 921 DTrVoFrac 1% 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F -777 Dig #4 Temp Deg F 778 7/1/2014 27 4.8880 1.07 182.1 0.8494 73.83 50 16,250 99 97 98 97 7/2/2014 41 4.8880 1.06 119.3 0.8492 73.58 51 10,547 100 99 98 97 7/3/2014 35 4.8880 1.17 141.4 0.8490 71.79 55 13,798 100 98 99 97 7/4/2014 54 4.8880 1.02 89.7 0.8499 73.53 51 7,631 100 96 98 97 7/5/2014 45 4.8880 1.01 107.7 0.8507 73.27 52 9,072 99 96 98 96 7/6/2014 92 4.8880 1.18 53.1 0.8511 72.88 53 5,226 99 97 97 97 7/7/2014 25 4.8880 1.01 193.6 0.8514 73.27 52 16,308 99 97 98 97 7/8/2014 27 4.8880 1.02 180.1 0.8509 73.53 51 15,321 99 ' 98 98 96 719/2 114 48 4.8880 1.24 101.2 0.8505 72.58 53 10,466 99 97 97 97 7/10/ 0014 59 4.8880 1.20 83.4 0.8497 72.50 53 8,347 99 97 97 98 7/11/ 0014 32 4.8880 1.06 154.0 0.8499 72.64 53 13,614 98 96 97 97 7/12/2014 44 4.8880 1.10 112.1 0.8501 72.73 53 10,284 98 96 97 1 97 7/13/2014 28 4.8880 1.22 175.3 0.8504 72.13 54 17,836 99 97 97 97 7/14/2014 39 4.8880 1.19 126.5 0.8507 72.27 54 12,555 99 98 98 97 7/15/2014 45 4.8880 1.33 109.6 0.8509 3.68 51 12,157 99 97 98 98 7/16/2014 51 4.8880 1.37 96.5 0.8507 72.99 53 11,026 99 97 98 97 7/17/2014 98 4.8880 1.81 50.1 0.8509 71.82 55t7563 99 97 98 97 7/18/2014 24 4.8880 1.36 203.1 0.8506 72.79 53 98 97 97 98 7/19/2014 29 4.8880 1.20 170.6 0.8511 %3.33 52 99 97 97 97 7/20/2014 42 4.8880 1.46 116.8 0.8515 72.60 54 99 97 97 97 7/21/2014 41 4.8880 1.44 118.3 0.8517 70.83 58 99 97 97 97 7/22/2014 63 4.8880 1.05 77.3 0.8616 72.38 54 , 102 98 98 97 7/23/2014 27 4.8880 1.04 183.4 0.8516 13.08 53 15,907 100 _99 98 97 7/24/2014 26 4.8880 1.06 185.6 0.8519 72.64 54 16,408 99 97 98 98 7/25/2014 26 4.8880 1.34 186.6 0.8513 72.39 54 20,854 99 97 97 98 7/26/2014 33 4.8880 1.01 146.3 0.8512 73.27 52 12,323 100 98 97 98 7/27/2014 22 4.8880 1.02 223.6 0.8515 72.55 54 19,021 99 98 97 98 7/28/2014 27 4.8880 1.00 178.7 0.8515 73.00 53 14,904 99 99 97 98 7/29/2014 48 4.8880 1.02 102.1 0.8514 73.53 52 8,685 99 98 97 98 7/30/2014 37 4.8880 1.07 131.5 0.8517 73.83 51 11,735 98 96 97 98 7/31/2014 41 4.8880 1.09 119.4 0.8516 73.39 52 10,854 9 8 97 96 96 Total 1,275 151.52b 36.22 4,ZIU.0 Z6.3/00 Z,ZDZ5.00 1,04v 4u4,uuu J,u/L 0,u la u,vc I v,v 1- Samples 31 31 31 31 31 1 31 31 31 31 31 31 31 Average 41 4.8880 1.17 136.1 0.8508 12.86 53 13,032 99 97 97 97 frifnarq di'gesfe-r -t-er,p6ra.fure. /Y1on/f7�ly c��leraye q'7v 09/16/2014 10:24:01 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 08/01/14 TO 08/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 8/1/2014 34 4.8880 1.18 142.5 0.8517 73.73 51 14,024 99 96 97 96 8/2/2014 24 4.8880 1.21 202.3 0.8521 74.38 50 20,415 98 95 96 97 8/3/2014 45 4.8880 1.06 107.8 0.8522 73.58 52 9,530 98 95 96 94 8/4/2014 25 4.8880 1.04 197.7 0.8525 74.04 51 17,148 98 96 96 97 8/5/2014 32 4.8880 1.11 154.4 0.8525 72.97 53 14,293 97 95 95 96 8/6/2014 27 4.8880 1.31 178.5 0.8528 74.05 51 19,502 98 97 95 97 8/7/2014 58 4.8880 1.05 84.9 0.8533 73.33 53 7,435 98 98 97 97 8/8/2014 25 4.8880 1.13 193.2 0.8539 74.34 50 18,208 98 96 95 97 8/9/2014 27 4.8880 1.31 178.3 0.8551 74.81 50 19,480 98 95 95 97 8/10/2014 29 4.8880 1.15 165.7 0.8559 73.04 54 15,892 97 96 95 96 8/11/2014 24 4.8880 1.24 204.8 0.8564 73.39 54 21,180 97 96 95 95 8/12/2014 31 4.8880 1.23 160.2 0.8563 73.98 52 16,434 97 96 95 96 8/13/2014 24 4.8880 1.05 207.2 0.8566 75.24 49 18,145 97 96 95 96 8/14/2014 29 4.8880 1.10 169.9 0.8571 73.64 53 15,587 97 95 94 95 8/15/2014 27 4.8880 1.18 181.9 0.8581 73.73 54 17,901 97 95 94 93 8/16/2014 38 4.8880 1.05 128.7 0.8596 73.33 55 11,270 98 96 94 93 8/17/2014 45 4.8880 1.34 108.7 0.8606 72.39 58 12,148 96 96 94 95 8/18/2014 33 4.8880 1.26 149.1 0.8610 73.81 54 15,668 97 96 94 94 8/19/2014 43 4.8880 1.33 113.4 0.8606 73.68 55 12,579 97 97 95 96 8/20/2014 32 4.8880 1.04 153.1 0.8603 74.04 54 13,279 97 97 94 96 8/21/2014 23 4.8880 1.33 212.4 0.8610 1 72.93 57 23,560 97 97 95 97 8/22/2014 35 4.8880 0.96 140.2 0.8613 72.92 57 11,225 97 97 95 95 8/23/2014 32 4.8880 1.16 152.6 0.8617 74.14 54 14,763 97 97 95 96 8/24/2014 42 4.8880 1.03 116.4 0.8631 73.79 55 9,999 97 97 95 96 8/25/2014 59 4.8880 1.01 82.4 0.8638 74.26 55 6,941 97 97 95 96 8/26/2014 33 4.8880 1.02 147.9 0.8640 73.53 56 12,582 97 97 94 95 8/27/2014 26 4.8880 1.00 191.3 0.8647 73.00 58 15,954 97 96 95 1 96 8/28/2014 96 4.8880 1.13 50.9 0.8652 74.34 55 4,797 97 96 95 95 8/29/2014 40 4.8880 1.45 122.5 0.8654 72.41 59 14,814 97 96 96 95 8/30/2014 28 4.8880 1.12 173.E 1 0.8657 73.21 58 16,216 96 96 95 95 8/31/2014 1 30 14.8880 1.49 162.9 0.8664 73.15 58 20,243 97 96 96 96 Total 1,096 151.5280 36.07 4,735.4 2b.62Ub Z,263.lb l,b/3 4bl,Z"IZ a,u-ia L,au i L,y4/ Z,a09 Samples 31 31 31 31 31 31 31 . 31 31 31 31 31 Average 35 4.8880 1.16 152.8 0.8587 73.65 54 14,878 97 96 95 96 ;its-Iep 7e," �c urn G N'i.�ll n1/Fig /" �Gc' 10/15/2014 05:23:50 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 09/01/14 TO 09/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS Ib %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 911/2014 28 4.8880 1.13 176.9 0.8671 74.34 56 16,671 97 96 96 96 9/2/2014 48 4.8880 1.10 101.4 0.8676 72.73 59 9,302 97 97 95 96 9/3/2014 45 4.8880 1.27 109.3 0.8677 73.23 58 11,577 97 97 96 96 9/4/2014 27 4.8880 1.18 180.4 0.8679 72.88 59 17,754 97 96 95 96 9/5/2014 34 4.8880 1.01 144.1 0.8674 74.26 56 12,138 97 96 95 96 9/6/2014 64 4.8880 1 1.56 76.9 0.8671 75.00 54 10,005 97 96 95 96 917/2014 25 4.8880 1.36 193.2 0.8672 72.79 59 21,914 97 96 95 95 9/8/2014 27 4.8880 1.36 181.6 0.8673 72.79 59 20,598 96 95 95 95 9/9/2014 64 4.8880 0.92 75.9 0.8671 73.91 57 5,824 96 95 95 95 9/10/2014 38 4.8880 0.95 129.8 0.8669 73.68 57 10,284 97 96 95 96 9/11/2014 33 4.8880 1.33 1 150.0 0.8672 72.93 59 16,638 97 96 95 96 9/12/2014 47 4.8880 1.18 103.6 0.8670 72.88 59 10,195 97 96 94 96 9/13/2014 28 4.8880 1.11 176.3 0.8670 72.97 59 16,321 97 95 95 95 9/14/2014 32 4.8880 1.28 150.9 0.8668 73.44 57 16,109 94 95 94 95 9/15/2014 22 4.8880 1.12 219.2 0.8663 73.21 58 20,475 97 94 94 95 9/16/2014 31 4.8880 0.95 159.7 0.8660 73.68 57 12,653 96 95 94 95 9/17/2014 18 4.8880 0.94 268.9 0.8652 73.40 57 21,081 95 94 94 1 95 9/18/2014 23 4.8880 0.96 209.9 0.8647 73.96 56 16,805 96 95 94 95 9/19/2014 26 4.8880 0.99 190.4 0.8642 72.73 58 15,721 95 94 94 95 9/20/2014 25 4.8880 0.87 199.3 0.8635 72.41 59 14,461 96 95 95 95 9/21/2014 26 4.8880 1.09 191.4 0.8628 72.48 58 17,399 95 93 94 95 9/22/2014 26 4.8880 1.00 186.1 0.8619 73.00 57 15,521 96 94 95 95 9/23/2014 26 4.8880 0.67 188.7 0.8609 71.64 59 10,544 95 94 94 1 95 9/24/2014 28 4.8880 0.74 176.1 0.8600 72.97 56 10,868 95 1 94 94 94 9/25/2014 50 4.8880 1.27 98.4 0.8598 72.44 57 10,422 95 93 94 94 9/26/2014 31 4.8880 1 1.40 158.9 0.8592 72.14 58 18,553 95 93 94 94 9/27/2014 25 4.8880 1.07 192.6 0.8589 72.90 56 17,187 95 93 94 94 9/28/2014 31 4.8880 0.98 160.2 0.8588 73.47 54 13,093 95 93 93 93 9/29/2014 41 4.8880 1.03 119.1 0.8585 73.79 54 10,231 94 93 94 94 9/30/2014 27 4.8880 1.31 178.0 0.8578 73.28 55 19,447 94 92 93 94 Total 994 146.6400 33.13 4,847.2 2b.929b 2,'lyb.3b 1,114 43y,/yl Z,bfI Z,0141 Z,004 /,abi Samples 30 30 30 30 30 30 30 . 30 30 30 30 30 Averaoe 33 4.8880 1.10 161.6 0.8643 73.18 57 14,660 96 95 94 95 rar ud o1qjye,3�er %�'o,,11hl� 7 t'r'� u/� �';' �/S° m � ! 11/24/2014 11:16:28 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 10/01/14 TO 10/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed Vo1Fr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 10/1/2014 30 4.8880 1.14 164.8 0.8575 _ 0.85 11 0.8561 73.68 53 15,669 93 93 94 93 10/2/2014 25 * 4.8880 0.95 % 192.1 72.63* 56 % 15,220 94 92 93 93 10/3/2014 37 4.8880 0.98 131.5 73.47 53 10,748 94 92 95 94 10/4/2014 23 4.8880 1.60 209.8 0.8560 71.88 57 27,996 95 92 94 94 10/5/2014 24 4.8880 1.19 206.5 0.8567 73.95 53 20,494 94 95 94 93 10/6/2014 19 4.8880 1.17 252.8 0.8576 72.65 56 24,668 93 95 93 94 10/7/2014 28 4.8880 1.23 175.1 0.8574 72.36 56 17,962 94 92 92 94 10/8/2014 35 4.8880 0.88 140.5 0.8575 72.73 56 10,312 95 93 94 94 10/9/2014 145 4.8880 0.91 33.6 0.8576 72.53 56 2,550 95 93 94 94 10/10/2014 62 4.8880 0.87 78.6 0.8576 73.56 54 5,703 95 94 93 94 10/11/2014 27 4.8880 1.20 184.1 0.8574 73.33 54 18,425 95 98 94 93 10/12/2014 28 4.8880 1.38 174.2 0.8576 71.74 58 20,049 95 92 93 93 10/13/2014 77 4.8880 1.48 63.1 0.8578 73.65 54 7,789 95 92 93 93 10M4/2014 28 4.8880 1.14 176.4 0.8581 73.68 54 16,771 95 92 94 93 10/15/2014 41 4.8880 0.80 119.7 0.8580 72.50 56 7,986 96 94 94 94 10M6/2014 26 4.8880 1.07 186.3 0.8578 72.90 55 16,625 96 93 94 93 10/17/2014 109 4.8880 1.56 44.9 0.8583 73.72 54 5,842 96 92 94 93 10/18/2014 39 4.8880 0.90 124.4 0.8600 72.22 58 9,337 95 92 94 93 10/19/2014 20 4.8880 1.09 245.1 0.8613 77.06 46 22,281 96 94 94 91 10/20/2014 149 4.8880 0.90 32.7 0.8618 73.33 56 2,454. 96 92 94 91 10/21/2014 27 4.8880 0.91 180.2 0.8633 72.53 58 13,676 96 93 94 92 10/22/2014 84 4.8880 0.89 58.0 0.8649 71.91 60 4,305 96 93 94 91 10/23/2014 96 4.8880 0.88 50.9 0.8660 72.73 59 3,736 96 1 93 94 91 10/24/2014 34 4.8880 1.09 141.8 1 0.8671 71.56 61 12,890 96 92 93 90 10/25/2014 47 4.8880 0.65 104.4 0.8675 1 70.77 63 5,660 97 96 94 87 10/26/2014 4.8880 0.0 0.8685 0 96 93 94 91 10/27/2014 50 4.8880 0.73 97.9 0.8697. 69.86 65 5,960 96 92 94 89 10/28/2014 39 4.8880 0.92 125.2 0.8710 71.74 62 9,606 96 92 94 90 10/29/2014 38 4.8880 1.02 127.2 0.8726 71.57 63 10,821 96 93 94 88 10/30/2014 4.8880 0.0 0.8742 0 97 93 94 91 10/31 /2014 16 14.8880 1 0.84 302.5 1 1 0.8740 71.43 64 1 21,192 1 97 94 95 91 Total 1,406 1b1.b;ebU 3U.31 4,1Z4.3 Z0J'1/a Z,-Iui.ei I,00i 000,/G/ 4,a00 4,000 t,�Juo c,0oa Samples 29 31 29 31 31 29 29 31 31 31 31 31 Averaae 48 4.8880 1.05 133.0 0.8619 72.68 57 11,830 95 93 94 92 Primary Digester Temperature monthly average is 94°F. * Data qualified. 12/11/2014 12:19:33 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 11101 /14 TO 11130/14 PriDig SRT PriDig VOL Trans %TS PrTranFlo Feed VolFr DTrVoFrac PriDig %VSR Transfer lb %TS Dig #1 Temp Dig #2 Temp Dig #3 Temp Dig #4 Temp Days %TS MG % TGD 30 day %, % lb %TS Deg F Deg F Deg F Deg F Mavg Date 163 492 93 357 921 422 920 741 775 776 777 778 11 /1 /2014 11/2/2014 11/3/2014 11 /4/2014 11/5/2014 11/6/2014 11/7/2014 11/8/2014 11/9/2014 11/10/2014 11 /11/2014 11/12/2014 11/13J2014 11/14/2014 11/15/2014 83 22 98 130 ' 32 29 75 40 40 35 30 41 49 25 17 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880K1.06290.5 4.88807.3 4.88802.2 4.88808.5 4.88808.0 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 1.40 1.25 1.78 2.12 1.66 1.11 2.22 1.08 0.95 0.90 0.97 1.66 1.09 0.97 1.04 1.01 1.02 1.08 1.20 0.98 0.97 1.02 1.05 58.7 219.8 0.0 50.0 37.7 150.5 0.0 169.8 65.3 121.7 122.0 140.2 162.2 120.1 99.5 198.2 203.1 55.3 207.6 191.1 176.6 178.4 182.1 221.1 115.7 0.8732 0.8748 0.8762 0.8755 0.8759 0.8758 0.8753 0.8751 0.8754 0.8759% 0.8759 %� 0.8749 0.8724 0.8704 0.8685 0.8674 0.8658 0.8652 0.8647 0.8637 0.8622 0.8613 0.8607 0.8601 0.8592 0.8575 0.8563 0.8548 0.8535 0.8539 71.43 72.00 72.47 71.70 70.48 71.17 70.27 72.22 %< 72.63 %; 72.22 71.13 71.08 72.48 72.16 73.58 73.33 74.29 72.83 73.63 73.08 73.27 74.51 73.15 72.50 74.49 73.20 73.53 73.33 64 63 63 64 66 65 66 63%; 62 %; 63 64 63 60 60 57 57 55 `58 55 56 56 52 55 56 51 54 52 53 6,854 22,914 0 7,423 6,666 20,836 0 15,71.9 12,090 10,962 9,666 10,523 13,122 16,627 9,045 16,034 25,681 19,905 24,712 16,765 8,955 17,616 4,658 17,660 17,213 17,674 14,581 14,732 18,809 10,132 98 97 97 98 98 98 98 97 97 97 . 98 98 97 97 96 95 95 95 95 95 95 96 96 97 97 97 96 96 95 96 93 94 93 94 94 95 95 94 95 95 94 95 95 95 95 94 93 93 92 92 93 92 93 94 95 95 94 93 93 93 95 96 94 94 94 95 96 95 96 96 98 98 98 97 96 96 95 95 95 9594 95 95 95 96 97 96 96 96 95 96 92 91 91 88 90 86 87 92 93 92 88 93 90 92 90 87 89 93 90 89 92 92 90 91 94 93 94 91 94 11/16/2014 11/17/2014 11/18/2014 22 11/19/2014 17 11/20/2014 22 11121/2014 41 11/22/2014 24 11/23/2014 88 11/24/2014 24 11/25/2014 26 11/26/2014 28 11/27/2014 27 11/28/2014 27 11/29/2014 22 11J30l2014 42 �4 a(,07 1 RR7 q9 1 ;, [n An7 r,74 AQ7 9 815 2.871 2.728 Total 1,156 146.6400 33.52 4,366.2 - - - - Samples 28 30 28 30 28 _ 26-- 26 30 30 30 30 30 Average 41 4.8880 1.20 146.1 0.8668 72.59 S9 13,586 97 94 96 91 * Estimates. Primary Digester Temperature monthly average is 95°F. 01/14/2015 03:38:45 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 12/01/14 TO 12/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp. Deg F 778 12/1/2014 26 4.8880 1.01 185.5 0.8546 73.27 53 15,625 96 96 94 12/2/2014 25 4.8880 1.07 197.2 0.8533 72.90 54 17,598 96 96 93 12/3/2014 43 4.8880 0.94 112.8 0.8516 74.47 49 8,843 96 F95 96 96 12/4/2014 4.8880 0.0 0.8515 0 96 96 93 12/5/2014 29 4.8880 1.00 170.5 0.8503 73.00 52 14,220 97 96 93 12/6/2014 40 4.8880 1.05 122.9 0.8503 73.33 52 10,762 97 95 97 92 12/7/2014 41 4.8880 1.04 118.5 0.8509 73.08 52 10,278 97 95 97 92, 12/8/2014 26 4.8880 1.10 190.4 0.8514 73.64 51 17,467 97 95 96 92 12/9/2014 24 4.8880 1.18 203.9 0.8514 74.58 49 20,066 97 94 96 93 12/10/2014 28 4.8880 1.01 172.4 0.8514 74.26 50 14,522 97 94 96 94 12/11/2014 28 4.8880 1.04 174.8 0.8519 73.08 53 15,161 97 94 96 94 12/12/2014 36 4.8880 1.02 135.0 0.8529 74.51 50 11,484 1 97 93 96 94 12/13/2014 25 4.8880 0.99 194.8 0.8556 �72.73 55 16,084 97 94 97 93 12/14/2014 4.8880 0.0 0.8581 0 97 95 97 94 12/15/2014 35 4.8880 0.96 140.2 0.8600 72.92 56 11,225 97 95 97 93 12/16/2014 133 4.8880 0.90 36.7 0.8617 73.33 56 2,755 97 95 97 94 12/17/2014 43 4.8880 1 0.96 114.2 0.8632 72.92 57 9,143 97 95 97 94 12/18/2014 31 4.8880 1.00 159.9 0.8637 72.00 59 13,336 97 95 97 93 12/19/2014 44 4.8880 0.89 110.2 0.8638 73.03 57 8,180 97 95 96 93 12/20/2014 86 4.8880 1.04 57.0 0.8639 1 73.08 57 4,944 97 95 96 93 12/21/2014 43 4.8880 1.12 114.4 0.8646 74.11 55 10,686 1 97 95 96 92 12/22/2014 32 4.8880 1.04 1.03 )� 155.0 0.8652 74.04 1 56 13,444 97 95 96 92 12/23/2014 112--Y- 4.8880 43.8 0.8654* 73.79 56 3,763 97 94 96 92 12/24/2014 38 4.8880 1.02 128.1 0.8658 72.55 59 10,897 97 94 96 92 12/25/2014 47 4.8880 1.91 103.0 0.8658 71.73 61 16,407 97 94 96 94 12/26/2014 86 4.8880 1.00 57.1 0.8679 73.00 59 4,762 97 94 96 93 12/27/2014 34 4.8880 1.25 141.9 0.8682 72.00 61 14,793 97 93 96 94 12/28/2014 33 4.8880 1.49 147.8 0.8686 72.48 60 18,367 97 96 98 91 12/29/2014 26 4.8880 1.66 189.1 0.8686 71.69 62 26,180 98 95 98 93 12/30/2014 25 4.8880 1.23 198.5 0.8686 71.54 62 20,363 98 96 98 92 12/31/2014 43 14.8880 r1.03 1 114.3 1 0.8693 71.84 62 1 9,819 98 95 98 94 wiai 51 r .r I V I.000V -7 V. 7 Samples $ 31 a Average 4.8880 1.10 5 S f•; fAq+e- .].7nM y si 128.7 SS4,S _ '7356 PriMG,N d?v ster 6mperalure, MOy)AN aVcrace- iS :51-1,1 /4 6,uuti 2,9:32 2,992 2,886 31 31 31 31 31 11,973 97 95 97 93 MUDDY CREEK WWTP NPDES Permit # NC0050342 2014 Pathogen and Vector Attraction Reduction Summary and Operational Data Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Muddy Creek WWTP NPDES Permit # NC0050342 2014 Compliance Summary Pathogen Reduction PSRP Data for Class B Residuals Anaerobic Digester System Month ** Primary Digester SRT(days)* Monthly Average Temp. °F Monthly Ave rage January 50 94 February 50 95 March 50 95 April 41 96 May 35 95 June 41 97 July 41 97 August 35 96 September 33 95 October 48 94 November 41 95 December 41 96 * SRT = Solids Retention Time; based on % Total Solids. ** Bi-monthly monitoring is required but is actually done on a monthly basis. Page 2 MUDDY CREEK WWTP Pathogen Reduction NPDES Permit # NC0050342 This plant normally operates three Primary Digesters (1, 2, and 3) and one Secondary Digester (4). The SRTs (or MCRTs) for the Muddy Creek WWTP are calculated daily and the summary on Page 1 uses the monthly average since daily values fluctuate so greatly from day to day. The formula below, using data from January I, 20I4, shows an example calculation. See attached monthly LAND APPLIED BIOSOLIDS REPORT, Page 4. Any estimated or qualified data is marked as such on these report pages. Any estimates are not included in the monthly average shown on the previous Page 1. Please find Digester Temperatures on this same report Page 4. Digester #4 is a Secondary Digester and its temperature is not included in determining .the monthly average. Occasionally, this Digester's temperature does not get recorded and those instances are either notated or left blank in the data column for `Dig#4 Temp'. FORMULA: [Primary Digester Volume x 8.34 x Primary Digester Transfer %Total Solids] (Pounds of solids in Primary Digesters) [Transfer %Total Solids x 8.34 x Primary Transfer Flow] (Pounds of solids being transferred to Blending Tanks) = PriDigSRT (Days %TS) FROM ATTACHED DATA SHEETS for January 1, 2014: [[PriDigVOL (MG)] x 8.34 x [Trans%TS (%)]] [[Trans%TS (%)] x 8.34 x [PrTranFlo (TGD)/1000]] or [4.8880 x 8.34 x 0,00921 = 0.3750 33.19 or [0.0092 x 8.34 x (146.9/1000)] 0.0113 as shown on the report, 33 Days SRT 02/25/2014 10:20:49 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans Ib %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 4.8880 4.8880 0.92 1.83 146.9 49.0 0.6813 0.7051 66.30 64.64 8 50 11,271 7,478 95 95 92 92 95 95 89 89 1/1/2014 33 100 1/2/2014 4.8880 4.8880 1.47 1.82 97.9 102.8 0.6992 0.6745 61.22 61.54 32 23 12,002 15,604 95 95 92 92 95 95 89 86 1/3/2014 50 48 1/4/2014 1.39 1.24 137.1 0.0 0.6658 0.6915 61.15 61.29 21 29 15,893 0 95 95 93 94 95 96 86 86 1/5/2014 36 4.8880 1/6/2014 4.8880 1.33 1.33 205.6 137.1 97.9 68.5 0.7177 0.7284 0.7582 0.7588 62.41 61.65 60.27 61.84 '35 40 52 48 22,806 15,207 11,921 8,684 95 95 95 95 92 92 92 92 94 95 95 94 87 88 86 84 1/7/2014 24 4.8880 1/8/2014 36 4.8880 1/9/2014 50 4.8880 1.46 1/10/2014 71 4.8880 1.52 78.3 102.8 0.7738 0.6130 0.6811 0.7463 0.7664 61.27 61.11 62.12 58.70 60.26 60.94 62.12 60.77 61.60 61.29 62.14 61.27 61.54 61.64 61.64 62.69 61.42 60,92 54 1 23 57 54 45 60 62 66 63 66 70 68 70 71 72 70 70 9,273 12,346 16,7111 0 28,175 10,187 18,8200 0 14,554 19,114 15,314 4,561 10,859 15,656 9,923 19,480 20,870 13,679 3,114 28,414 96 96 96 96 96 96 95 95 95 95 95 95 95 95 95 95 95 95 95 95 93 93 93 93 93 93 92 92 92 93 92 92 92 92 93 93 93 93 91 92 95 95 95 96 96 96 96 96 96 96 95 96 96 96 95 95 95 95 95 95 87 88 89 87 89 89 87 87 88 89 89 87 87 87 88 89 88 88 89 87 84 1/11/2014 62 4.8880 1.42 1/12/2014 48 4.8880 1.44 1/13/2014 32 4.8880 1.32 151.8 1/14/2014 4,8880 0.0 1/15/ 0014 20 4.8880 244.8 1 /16/2014 62 4.8880 6 78.30.7661 1/17/2014 28 4.8880 g1,38 8 176.3 0.7387 1/18/2014 4.8880 0.0 0.8025 1/19/ 0014 4.8880 0.0 0.8034 1/20/2014 37 4.8880 1.32 132.2 0.8049 1/21/2014 28 4.8880 1.30 176.3 0.8014 1/22/ 0014 33 4.8880 1.25 146.9 0.8254 1/23l2014 111 4.8880 1.24 44.1 0.8108 1/24/2014 53 4.8880 1.40 93.0 0.8295 1/25/2014 37 4.8880 1.42 132.2 0.8390 1/26/2014 59 4.8880 1.43 83.2 0.8316 0.8408 0.8487 0.8590 0.8395 0.8406 -4 1/27/2014 33 4.8880 1.59 146.9 1/28/2014 29 4.8880 1.46 171.4 1/29/2014 1/30/2014 1/31/2014 40 166 25 4.8880 4.8880 4.8880 1.34 1.27 1.74 122.4 29.4 195.8 a 71F75 1 -178 391.916 2,952 2,865 2,955 2,715 Total 1,349 151.52M 6y)Af Lam. 1. Samples 27 31 28 31 31 28 28 31 31 31 31 31 Average 50 4.8880 1.41 108.0 0,7669 61.28 49 12,642 95 92 95 88 Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Muddy Creek WWTP NPDES Permit # NCO050342 2014 Compliance Summary Vector Attraction Reduction Requirements for Class B Residuals Compliance determination by Calculation of Volatile Solids Reduction across the Anaerobic Digesters as the treatment system. Calculated %VSR (38% Minimum) Monthly Average VAR Option 1 Month * Primary Digester System Janua 49 FebruaryE 65 March 61 April 56 55 52 53 st P 54 mber 57 er 5mber 59 December, 56 * Bimonthly monitoring is required but is actually done on a monthly basis. ** Beginning in June, 2014, there is an offset of time factored in regarding digester solids retention time (or MCRT). A given month's %VSR is now calculated using the previous month's SRT average. See page 2 of this section for the formula used for the first five months of 2014, as well as the formula now used beginning in June of 2014. The equation used for calculating the above %VSRs is from the EPA White House Manual, Control of Pathogens and Vector Attraction in Sewage Sludge, Chapter 10 and Appendix C. Page 2 Muddy Creek WWTP Vector Attraction Reduction NPDES Permit # NC0050342 Data submitted in the chart on Page 1 of this summary shows that the calculated monthly average Volatile Solids Reduction meets the minimum of 38% VSR requirement over the Primary Digester System at the Muddy Creek WWTP for the year of 2014. Volatile Solids Reduction (VSR) is calculated by the Van Kleeck equation using the digester feed and digester stabilized transfer sludge volatile fractions. While there was previously no offset necessary for digester Solids Retention Times (or MCRTs) due to the consistency with which these digesters were operated, upon in-house review, the City began in June of 2014 calculating one month's %VSR using the previous month's SRT average. This more accurately reflects current digester operations. Any data qualified by the lab is marked as such on data sheets. Also, in instances when a daily sample was not collected for %Volatile Solids analysis of the Transfer (`Trans') Sludge, an estimated value was used along with actual flows for that day in order to calculate treatment in the digesters. Any estimated daily values are marked as such on data sheets, but the monthly average values (shown on the previous Page 1) were calculated excluding this estimated data in order to certify compliance. The values for January 2, 2014 from the attached LAND APPLIED BIOSOLIDS report Page 4 are used in the example equation below. This is the formula used for the period of Jan. — May, 2014. The heading `VolFrac 311+318' refers to the Volatile Fraction of the Digester feed samples and the heading `DTrVoFrac' refers to the Volatile Fraction of the stabilized Primary Digester transfer samples. The calculated Percent Volatile Solids Reduction is indicated by the heading `PriDig%VSRed (%)'. FORMULA January — May, 2014: [VolFrac 311 + 318] - [DTrVoFrac/100] = priDigVSR (%) (Feed) (Transfer) [VolFrac 311+ 3181 - [(VolFrac 3e11 + 318) x (DT (Transfer) 0)] d (Feed) ) FROM ATTACHED DATA SHEETS for January 2, 2014: 0.7051 — 0.5464 = 0.1587 = 0.4962 or as shown on the report, 50% VSR 0.7051 - (0.7051 x 0.5464) 0.3198 ----------------------------------------------------------- ------ ---------------- - IDS - report Page 4, June 1, 20I4, for the current method of calculating See on the attached LAND APPLIED BIOSOL %VSR. The new heading of "Feed Vo1Fr 30 day mavg" is the Feed Volatile Fraction 30 day moving average. See monthly averages June — Dec., 2014, in the chart on the previous Page 1 of this summary and attached daily data. FORMULA June — December, 2014: [Feed Vol Frac 30 day mavg] - [D (Transfer)100] = priDigVSR (%) (Feed) [Feed Vol Frac 30 day mavg] - [(Feed Vol Frac 30 day mavg) x (DTrVoFrac/l00)] (Feed) (Feed) (Transfer) FROM ATTACHED DATA SHEETS for June 1, 2014: 0.8472 — 0.7193 = 0.1279 = 0.5378 or as shown on the report, 54% VSR 0.8472 — (0.8472 x 0.7193) 0.2378 Van Kleeck Equation used: %VS Reduction = f%VS (Feed)l - f%VS (Stabilized)1 [%VS (Feed)] - [%VS (Feed) x %VS (Stabilized)]. %VS (Feed) = Volatile fraction of raw and thickened sludges fed to primary digesters %VS (Transfer) = Volatile fraction of stabilized sludge transferred from primary digesters 02/25/2014 10:20:49 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492. Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS Ib %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 0.92 146.9 49.0 97.9 0.6813 0.7051 0.6992 0.6745 0.6658 66.30 54.64 61.22 61.54 61.15 61.29 62.41 61.65 60.27 61.84 61.27 61.11 62.12 8 50 32 23 21 29 35 40 52 48 54 1 23 57 54 45 60 62 66 63 66 70 70 71 72 70 70 1,37 11,271 7,478 12,002 15,604 15,893 0 22,806 15,207 11,921 8,684 9,273 12,346 16,7111 28,175 10,187 20 18,820 0 14,554 19,114 15,314 4,561 10,856 9,923 19,480 13,679 13,679 3,114 28,414 95 95 95 95 95 95 95 95 95 95 96 96 96 96 96 95 95 95 9b 95 95 95 95 95 95 95 95 95 92 92 92 ' 92 93 94 92 92 92 92 93 93 93 93 93 92 92 92 93 92 92 993 2 93 93 93 91 92 5 95 95 95 95 95 96 94 95 95 94 95 95 96 96 96 96 96 96 96 95 96 96 95 95 95 95 95 95 2,955 89 89 89 86 8 86 87 88 86 84 87 88• 89 87 gg 89 87 87 88 89 89 87 87 87 88 89 88 88 89 87 84 2.715 1/1/2014 33 4.8880 1/2/2014 1/3/2014 100 50 4.8880 4.8880 1.83 1.47 1/4/2014 48 4;8880 132 102.8 1/5/2014 36 4,8880 1.39 137.1 1/6/2014 8 4.880 1.24 0.0 0.6915 1I7/2014 24 4.8880 1.33 205.6 0.7177 1/8/2014 36 4.8880 1.33 137.1 0.7284 1!9/2014 50 4.8880 1.46 97.9 0.7582 1/10/2014 71 4.8880 1.52 68.5 O'7588 1/11/2014 1 /12/2014 62 48 4.8880 4.8880 1.42 1.44 78.3 102.8 0.7738 0.6130 1/13/2014 32 4.8880 1.32 151.8 0:6811 1/14/2014 20 62 28 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 1.38 - 56 1.28 1.32 1.30 1.25 1.24 1.40 1.42 1.43 1.59 1.46 1.34 1.27 1.74 . , 0.0 244.8 78.3 176.3 0.0 0.0 132.2 176.3 146.9 44.1 93.0 132.2 83.2 1-46 9 171.4 122.4 29.4 195.8 a ua a 0.7463 0.7664 0.7661 0.7387 0.8025 0.8034 0.8049 0.8014 0,8254 0.8108 0.8295 683 661.27 0.8316 0,8408 0.8487 0.8590 0.8395 0.8406 73-7431 58.70 60.26 60.94 62.12 60.77 61.60 61.29 62.14 61.54 6,1.64 61.64 62.69 61.42 60,92 1,715.75 1 /15/2014 1/16/2014 1/17/2014 1/18/2014 1/19/2014 1/20/2014 37 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8886 4.8880 4.8880 4,8880 4.8880 1/21/2014 28 1/2 j 014 33 1/23l2014 111 1/24/20.14 53 1/25/2014 37 1/26/2014 59 1/27/2014 33 1/28/2014 29 1/29/2014 40 1/30/2014 166 1/31/2014 25 Total [,r+Zv 1:,1.:- - - 31 28 28 Samples 27 31 28 31 Average 50 4.8880 1.41 108.0 0.7659 61.28 49 31 12,64E vv - 88 07/17/2014 09:09:55 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO060342 06/01/14 TO 06/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VoIFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 95 95 99 97 101 96 96 96 96 97 99 96 96 96 95 96 95 96 96 97 96 97 96 97 97 99 95 96 97 97 97 97 96 97 98 97 98 97 98 98 98 98 98 97 98 97 95 97 97 97 97 97 97 98 96 96 96 97 97 97 94 94 95 96 96 96 94 94 94 96 ^96 96 96 96 97 97 97 97 97 96 97 97 97 97 97 96 97 97 97 96 97 97 97 98 98 97 98 98 99 98 99 99 98 98 98 98 97 99 98 98 98 98 98 99 99 98 97 98 99 99 6/1/2014 6/2/2014 28 29 4.8880 4.8880 1.14 1.07 1.08 1.06 172.9 170.0 162.3 183.5 159.7 47.1 0.0 0.0 17.3 0.0 0.8472 0.8474 0.8473 0.8471 0.8465 0.8463 0.8465 0.8468 0.8473 0.8470 0.8465 0.8470 0.8469 0.8488 0.8495 0.8498 0.8492 0.8488 71.93 73.83 72.22 72.64 72.03 72.22 72.73 * 70.76 72.07 72.07 72.22 71.81 73.44 72.73 73.81 72.39 72.09 72.65 72.80 72.64 73.83 72.97 72.22 74.24 72.50 73.53 72.90 54 49 53 52 53 53 52* 56 53 53 54 55 51 53 50 53 54 52 52 53 50 52 54• 49 53 51 52 16,439 15,170 14,619 16,222 15,716 4,242 0 0 1,746 0 18,526 23,458 16,774 15,080 28,208 14,550 19,799 17,213 15,568 18,655 4,703 20,714 6,347 11,547 4,360 23,287 18,847 13,941 ,261 11,083 6/3/2014 30 4.8880 6/4/2014 27 4.8880 6/5/2014 31 4.8880 1.18 6/6/2014 104 4.8880 4.8880 1.08 6/7/2014 6/8/2014 4.8880 1.21" 6/9/2014 283 :: 4.8880 ;6/10/2014 4.8880 6/11/2014 38 4.8880 1. 71 129.9 6/12/2014 19 4.8880 1.11 253.4 6/13/2014 27 4.8880 1.11 181.2 6/14/2014 34 4.8880 1.26 143.5 6/15/2014 22 4.8880 1.49 227.0 6/16/2014 36 4.8880 1.28 136.3 6/17/2014 25 4.8880 1.21 196.2 6/1/2014 30 4.8880 1.26 163.8 6/19/2014225 4.8880 1.34 139.3 0.8485 0.8482 0.8480 6/20/2014 4.8880 1.29 173.4 6/21/2014 4.8880 1.17 48.2 6/22/2014 4.8880 1.25 198.7 0.8484 0.8487 6/23/2014 4.8880 1.06 71.6 6/24/2014 38 4.8880 1.07 129A 0.8485 6/25/2014 6/26/2014 104 25 4.8880 4.8880 1.11 1.44 47.1 193.9 0.8483 0.8491 6/27/2014 29 4.8880 1.32 171.2 0.8491 6/28/2014 35 4.8880 1.20 139.3 0.8487 0.8489 0.8490 6/29/2014 66 4.8880 1.02 73.6 6/30/2014 39 4.8880 1.07 124.2 QQA cr, 1 2F,� 21897 2,915 2,882 I91 _ 329 2.942 Total i v / i 140.04uv -� I . �" .- -- - 30 30 30 3U Samples 26 30 26 30 30 26 26 �9 97 97 96 Average 41 4.8880 1.21 128.5 0.8480 72.64 52 _1 3 , 494 98 Primary Digester Temperature monthly average is 97°F• Estimate. 02/24/2014 01:39:24 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS Ib %TS 741 Dig #1 Temn Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Terno Deg F 777 Dig #4 Temp Deg F 778 1/1/2014 33 4.8880 0.92 146.9 0.6813 66.30 8 11,271 95 92 95 89 1/2/2014 100 4.8880 1.83 49.0 0.7051 54.64 50 7,478 95 92 95 89 1/3/2014 50 4.8880 1.47 97.9 0.6992 61.22 32 12,002 95 92 95 89 1/4/2014 48 4.8880 1.82 102.8 0.6745 61.54 23 15,604 95 92 95 88 1/5/2014 36 4.8880 1.39 137.1 0.6658 61.15 21 15,893 95 93 95 86 1 /6/2014 4.8880 1.24 0.0 0.6915 61.29 29 0 95 94 96 86 1/7/2014 24 4.8880 1.33 205.6 0.7177 62.41 35 22,806 95 92 94 87 1/8/2014 36 4.8880 1.33 137.1 0.7284 61.65 40 15,207 95 92 95 88 1/9/2014 50 4.8880 1.46 97.9 0.7582 60.27 52 11,921 95 92 95 86 1/10/2014 71 4.8880 1.52 68.5 0.7588 61.84 48 8,684 95 92 94 84 1 /11 /2014 62 4.8880 1.42 78.3 0.7738 61.27 54 9,273 96 1 93 95 87 1/12/ 0014 48 4.8880 1.44 102.8 0.6130 61.11 1 12,346 96 93 95 88 1/13/2014 32 4.8880 1.32 151.8 0.6811 62.12 23 16,711 96 93 95 89 1/14/2014 4.8880 0.0 0.7463 0 96 93 96 87 1/15/2014 20 4.8880 1.38 244.8 0.7664 58.70 57 28,175 96 93 96 89 1/16/2014 62 4.8880 1.56 78.3 0.7661 60.26 54 10,187 96 93 96 89 1/17/2014 28 4.8880 1.28 176.3 0.7387 60.94 45 18,820 96 92 96 87 1 /18/2014 4.8880 0.0 0.8025 0 95 92 96 87 1 /19/2014 4.8880 0.0 0.8034 0 95 92 96 88 1/20/2014 37 4.8880 1.32 132.2 0.8049 62.12 60 14,554 95 92 96 89 1/21/2014 28 4.8880 1.30 176.3 0.8014 60.77 62 19,114 95 93 96 89 1/22/2014 33 4.8880 1.25 146.9 0.8254 61.60 66 15,314 95 92 95 87 1/23/2014 111 4.8880 1.24 44.1 0.8108 61.29 63 4,561 95 92 96 87 1/24/2014 53 4.8880 1.40 93.0 0.8295 62.14 66 10,859 95 92 96 87 1/25/2014 37 4.8880 1.42 132.2 0.8390 61.27 70 15,656 95 92 96 88 1/26/2014 59 4.8880 1.43 83.2 0.8316 61.54 68 9,923 95 93 95 89 1/27/2014 33 4.8880 1.59 146.9 0.8408 61.64 70 19,480 95 93 95 88 1/28/2014 29 4.8880 1.46 171.4 0.8487 61.64 71 20,870 95 93 95 88 1/29/2014 40 4.8880 1.34 122.4 0.8590 62.69 72 13,679 95 93 95 89 1/30/2014 166 4,8880 1.27 29.4 0.8395 61.42 70 3,114 95 91 95 87 1 /31 /2014 25 4.8880 1.74 195.8 0.8406 60.92 70 28,414 95 92 95 84 Total 1,349 151.5280 39.47 3,348.9 23.7431 1,715.75 1,378 391,916 2,952 2,bbb 2,955 2,/15 Samples 27 31 28 31 31 28 28 31 31 31 31 31 Averaqe 50 4.8880 1.41 108.0 0.7659 61.28 49 12,642 95 92 95 88 Primary Digester Temperature monthly average is 94°F. 03/13/2014 04:22:59 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO060342 02/01/14 TO 02/28/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temo Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temo Deg F 777 Dig #4 Temp Deg F 778 2/1/2014 36 4.8880 1.35 137.1 0.8448 62.96 69 15,436 95 92 95 88 2/2/2014 4.8880 0.0 0.8491 0 96 92 95 90 2/3/2014 37 4.8880 1.41 132.2 0.8358 63.12 66 15,546 96 92 95 85 2/4/2014 67 4.8880 1.32 73.4 0.8470 63.64 68 8,080 96 93 95 89 2/5/2014 55 4.8880 1.25 88.1 0.8635 64.00 72 9,184 96 93 96 91 2/6/2014 33 4.8880 1.45 146.9 0.8631 63.45 72 17,765 95 92 95 91 2/7/2014 42 4.8880 1.26 117.5 0,8648 64.29 72 12,347 95 92 95 89 2/8/2014 83, 4.8880 1.33 58.8 0.8647 1 64.66 71 6,522 95 93 95 90 2/9/2014 32 4.8880 1.23 151.8 0.8620 65.85 69 15,572 95 93 95 91 2/10/2014 29 4.8880 1.22 166.5 0.7817 63.93 51 16,941 95 93 95 90 2/11/2014 77 4.8880 1.22 63.6 0.7733 63.93 48 6,471 95 93 96 91 2/12/2014 38 4.8880 1.24 127.3 0.8460 64.52 67 13,165 96 92 96 91 2/13/0014 38 4.8880 1.37 127.3 0.8575 63.50 71 1.4,545 96 92 96 91 2/14/2014 83 4.8880 1.22 58.8 0.8525 65.57 67 5,983 96 92 96 90 2/15/2014 4.8880 0.0 0.8125 0 95 92 96 90 2/16/2014 4.8880 0.0 0.8275 0 96 92 96 90 2/17/2014 29 4.8880 1.28 168.0 0.8422 66.41 63 17,934 96 92 96 _ 90 2/18/2014 31 4.8880 1.27 156.7 0.8423 65.35 65 16,597 96 93 96 90 2/19/2014 25 4.8880 1.58 195.8 0.8479 63.92 68 25,801 95 93 96 90 2/20/2014 51 4.8880 1.24 95.1 0.8540 65.32 68 9,835 96 93 96 91 2/21/2014 55 4.8880 1.19 88.1 0.8491 66.39 65 8,744 96 93 96 89 2/22/2014 42 4.8880 1.24 117.5 0.8298 65.32 61 12,151 96 93 96 91 2/23/2014 28 4.8880 1.58 172.7 0.8037 63.29 58 22,757 96 1 93 96 92 2/24/2014 90 4.8880 1.34 54.1 0.8174 64.18 60 6,046 97 93 96 92 2/25/2014 32 4.8880 1.49 154.8 0.8276 65.10 61 19,236 97 93 96 92 2/26/2014 106 4.8880 1.19 1 45.9 0.8395 64.71 65 4,555 96 93 96 92 2/27/2014 35 4.8880 1.52 138.2 0.8357 63.82 65 17,519 96 93 95 92 2/28/2014 62 4.8880 1.20 79.4 0.8477 65.83 65 7,946 96 92 95 91 Total 1,238 136.8640 32.99 2,915.6 23.4825 1,613.07 1,628 326,678 z,bt$l Z,wlz z,0ii z,9za Samples 25 28 25 28 28 25 25 28 28 28 28 28 Averaoe 50 4.8880 1.32 104.1 0.8387 64.52 65 11,667 96 93 96 90 Primary DigRster Temperature monthly average is 95°F• 04/16/2014 04:33:47 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 03/01/14 TO 03/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS Ib %TS 741 Dig #1 Tema Deg F 776 Dig #2 Temp Deg F 776 Dig #3 Tema Deg F 777 Dig #4 Temp Deg F 778 3/1/2014 50 4.8880 1.33 97.9 0.8522 65.41 1 67 10,859 96 93 95 91 3/2/2014 34 4.8880 1.12 142.1 0.8525 64.29 69 13,273 96 93 96 90 3/3/2014 34 4.8880 1.20 143.1 0.8480 81.67 20 14,321 96 93 95 92 3/4/2014 113 4.8880 1.19 43.3 0.8277 67.23 57 4,297 95 92 95 91 3/5/2014 33 4.8880 1.16 146.3 0.8456 67.24 63 14,154 95 92 95 89 3/6/2014 48 4.8880 1.31 102.8 0.7899 67.18 46 11,231 95 92 95 88 3r7/2014 37 4.8880 1.39 132.8 0.8260 66.91 57 15,395 95 91 95 90 3/8/2014 37 4.8880 1.18 133.2 0.8104 67.80 51 13,108 95 91 95 88 3/9/2014 39 4.8880 1.24 124.8 0.8218 66.13 1 58 12,906 95 92 96 90 3/10/2014 29 4.8880 1.15 171.5 0.8283 66.96 58 16,449 96 93 96 92 3/11/2014 1 62 4.8880 1.15 79.2 0.8593 68.70 64 7,596 96 94 96 91 3/12/2014 44 4.8880 1.16 110.7 0.8610 68.10 66 10,710 96 94 96 91 3/13/2014 33 4.8880 1.18 148.3 0.8411 66.95 62 14,594 96 93 96 91 3/14/2014 44 4.8880 1.30 112.1 0.8531 67.69 64 12,154 96 92 96 91 3/15/2014 42 4.8880 1.24 115.1 0.8349 67.74 58 11,903 96 92 96 92 3/16/2014 100 4.8880 1.12 49.0 0.8618 67.86 66 4,577 96 92 96 90 3/17/2014 25 4.8880 1.25 193.7 0.8576 68.00 65 20,193 96 92 96 91 3/18/2014 30 4.8880 1.27 163.9 0.8337 67.72 58 17,360 96 92 96 91 3/19/2014 31 4.8880 1.32 156.7 0.8631 67.42 67 17,251 96 93 95 91 3/20/2014 49 4.8880 1.31 98.9 0.8591 67.94 65 10,805 96 97 95 91 3/21/2014 67 4.8880 1.10 73.4 0.8569 69.09 63 6,734 96 92 96 91 3/22/2014 27 4.8880 1.24 181.7 0.8557 67.74 65 18,791 96 92 96 92 3/23/2014 34 4.8880 1.30 142.0 0.8589 67.69 66 15,396 96 93 96 92 3/24/2014 137 4.8880 1.39 35.7 0.8649 66.91 68 4,139 96 93 96 92 3/25/2014 28 4.8880 1.31 175.5 0.8612 67.94 66 19,174 96 93 96 92 3/26/2014 31 4.8880 1.29 156.0 0.8625 67.44 67 16,783 95 92 96 91 3/27/2014 84 4.8880 1.20 5T9 0.8566 68.33 64 5,795 95 92 96 91 3/28/2014 45 4.8880 1.10 108.6 0.8442 69.09 1 59 1 9,963 95 92 95 89 3/29/2014 27 4.8880 1.30 178.7 0.8573 69.23 63 19,375 96 92 95 1 89 3/30/2014 107 4.8880 1.19 45.5 0.8493 69.75 59 4,516 96 92 95 90 3/31/2014 34 4.8880 1.50 144.6 1 0.8634 69.33 64 18,089 96 92 95 90 Total 1,536 151.5280 38.49 3,765.0 26.2577 2,111.47 1,883 391,891 2,967 2,868 2,963 2,810 Samples 31 31 31 31 31 31 31 31 31 31 31 31 Average 50 4.8880 1.24 121.5 0.8470 68.11 61 12,642 96 93 96 91 Primary Digester Temperature monthly average is 95°F. 05/21/2014 02:13:10 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 04/01/14 TO 04/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS Ib %TS 741 Dig #1 Temo Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temo Deg F 777 Dig #4 Temp Deg F 778 4/1/2014 34 4.8880 1.12 144.6 0.8624 69.64 63 13,507 96 93 95 92 4/2/2014 42 4.8880 1.22 116.8 0.8722 70.49 65 11,884 97 94 96 92 4/3/2014 60 4.8880 1.25 81.9 0.8621 68.80 65 8,538 93 96 95 91 4/4/2014 46 4.8880 1.13 107.1 0.8480 69.91 58 10,093 96 93 95 92 4/5/2014 41 4.8880 1.51 118.4 0.8474 70.86 56 14,911 95 94 96 92 4/6/2014 28 4.8880 1.53 176.4 0.8546 69.93 60 22,509 96 94 96 93 4/7/2014 27 4.8880 1.11 180.9 0.8405 70.27 55 16,747 95 93 96 93 4/8/2014 37 4.8880 1.15 132.1 0.8242 11 71.30 47 %< 12,670 95 94 95 93 4/9/2014 37 4.8880 1.12 133.3 0.8590 71.43 59 12,451 95 94 97 93 4/10/2014 46 4.8880 1.11 105.5 0.8638 69.37 64 9,767 96 93 98 93 4/11/2014 29 4.8880 1.12 168.8 0.8489 69.64 59 15,767 95 1 93 99 93 4/12/2014 30 4.8880 1.09 162.6 0.8448 69.72 58 14,781 95 93 100 93 4/13/2014 78 4.8880 1.65 63.0 0.8552 70.30 60 8,669 96 94 101 92 4/14/2014 47 4.8880 1.04 103.9 0.8649 71.15 1 61 91012 98 94 102 93 4/15/2014 29 4.8880 1.23 166.8 0.8094 69.92 45 17,111 98 94 104 94 4/16/2014 24 4.8880 1.56 206.0 0.7816 69.23 37 26,801 98 93 103 94 4/17/2014 40 4.8880 1 1.04 121.2 0.8395 70.19 55 10,512 97 93 102 94 4/18/2014 36 4.8880 1.27 137.3 0.8439 71.65 53 14,543 96 93 103 94 4/19/2014 39 4.8880 1.18 124.0 0.8397 69.49 57 12,203 96 93 103 94 4/20/2014 35 4.8880 1.13 140.9 0.8414 70.80 1 54 13,279 98 93 99 94 4/21/2014 47 4.8880 1.05 103.6 0.8483 71.43 55 9,072 98 94 99 94 4/22/2014 33 4.8880 1.20 147.0 0.8478 70.00 58 14,712 98 93 100 94 4/23/2014 34 4.8880 1.07 142.0 0.8498 71.03 57 12,672 98 93 98 94 4/24/2014 50 4.8880 1.04 97.6 1 0.8492 69.23 60 8,465 97 94 98 94 4/25/2014 30 4.8880 1.21 162.1 0.8395 71.07 53 16,358 96 94 97 94 4/26/2014 29 4.8880 1.16 168.7 0.8345 71.55 50 16,321 96 95 97 94 4/27/2014 113 4.8880 1.48 43.3 0.8372 70.27 54 5,345 96 95 97 94 4/28/2014 23 4.8880 1.09 209.1 0.8419 70.64 55 19,008 96 95 97 94 62 4.8880 1.10 78.9 0.8490 71.82 55 7,238 96 94 96 95 E32 32 4.8880 1.10 1 151.3 0.8462 70.91 56 13,880 96 1 94 96 94 total 1,238 146.6400 36.06 3,995.1 25.3468 2,112.08 1,686 398,826 2,888 2,812 2,950 2,800 Samples 30 30 30 30 30 30 30 30 30 30 30 30 _ Average 41 4.8880 1.20 133.2 0.8449 70.40 56 13,294 96 94 98 93 * Data qualified by Lab. Primary Digester Temperature monthly average is 96°F. 06/12/2014 03:05:07 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 05/01 /14 TO 05/31 /14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 TemD Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 5/1/2014 43 4.8880 1.11 114.1 0.8396 71.17 53 10,563 97 94 97 94 5/2/2014 40 4.8880 1.30 122.4 0.8500 1 70.77 57 13,271 96 95 96 94 5/3/2014 29 4.8880 1.12 168.3 0.8530 71.43 57 15,721 96 95 97 94 5/4/2014 30 4.8880 1.16 160.9 0.8468 67.24 63 15,566 95 95 97 94 5/5/2014 48 4.8880 1.13 102.7 0.8323 72.57 47 9,679 @ 95 94 94 5/6/2014 29 4.8880 1.12 168.9 0.8581 71.43 59 15,777 94 96 96 94 5!7/2014 59 4.8880 1.10 83.3 0.8509 70.91 57 7,642 94 96 96 94 5/8/2014 32 4.8880 1.13 1 152.9 0.8427 71.68 53 14,410 94 95 96 94 5/9/2014 46 4.8880 1.20 105.3 0.8511 70.83 58 10,538 96 95 96 95 5/10/2014 33 4.8880 1.18 146.4 0.8472 72.03 54 14,408 95 96 96 94 5/11/2014 45 4.8880 1.49 107.9 0.8527 1 71.81 56 13,408 96 95 97 94 5/12/2014 1 30 4.8880 1.23 161.6 0.8565 71.54 58 16,577 95 94 97 95 5/13/2014 31 4.8880 1.42 155.6 0.8326 71.13 50 18,427 96 95 97 95 5/14/2014 29 4.8880 1 1.31 170.5 0.8501 70.99 57 18,628 96 95 97 95 5/15/2014 57 4.8880 1.32 85.1 0.7876 70.45 36 9,368 96 95 97 95 5/16/2014 25 4.8880 1,16 194.3 0.8185 71.55 44 18,797 96 94 96 94 5/17/2014 29 4.8880 1.23 166.8 0.8368 71.54 51 17,111 96 93 96 94 5/18/2014 23 4.8880 1.30 210.0 0.8493 70.77 57 22,768 96 94 96 94 5/19/2014 24 4.8880 1.34 205.7 0.8641 71.64 60 22,988 96 93 97 94 5/20/2014 30 % 4.8880 1.30 ' 162.9 0.8593 % 71.54 59 % 17,662 96 93 97 94 5/21/2014 39 4.8880 1.33 125.9 0.8608 71.43 60 13,965 96 93 97 94 5/22/2014 46 4.8880 1.40 105.8 0.8558 71.43 58 12,353 96 94 96 95 5/23/2014 29 4.8880 1.23 169.6 0.8444 71.54 54 17,398 94 96 96 1 94 5/24/2014 29 4.8880 1.26 168.2 0.8575 72.22 57 17,675 92 96 96 95 5/25/2014 27 4.8880 1.10 180.3 0.8620 72.73 57 16,541 96 96 96 94 5/26/2014 44 4.8880 1.40 111.4 0.8621 71.43 60 13,007 96 96 96 95 5/27/2014 54 4.8880 1.25 91.3 0.8338 72.80 47 9,518 96 96 96 96 5/28/2014 20 4.8880 1.12 242.1 0.8488 72.32 53 22,614 96 96 96 96 5/29/2014 26 4.8880 1.16 184.5 0.8596 1 72.41 57 17,849 98 99 97 96 5/30/2014 21 4.8880 1.21 228.4 0.8445 71.90 53 23,049 98 96 96 .95 5/31 /2014 40 14.8880 1.16 123.6 0.8492 71.55 55 1 11,958 1 97 1 96 96 1 96 Total 1,089 151.5280 38.27 4,676.7 26.2577 2,214.81 1,695 479,236 2,871 2,947 2,986 2,931 Samples 31 31 31 31 31 31 31 31 30 31 31 31 Average 35 4.8880 1.23 150.9 0.8470 71.45 55 15,459 96 95 96 95 Primary Digester Temperature monthly average is 95°F. * Data qualified by Lab. @ No Digester temperature due to maintenance on heat exchanger. 07/17/2014 09:09:55 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 06/01/14 TO 06/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VoIFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 6/1/2014 28 4.8880 1.14 172.9 0.8472 71.93 54 16,439 97 95 97 94 6/2/2014 29 4.8880 1.07 170.0 0.8474 73.83 49 15,170 97 95 97 94 6/3/2014 30 4.8880 1.08 162.3 0.8473 72.22 53 14,619 97 99 96 95 6/4/2014 27 4.8880 1.06 183.5 0.8471 72.64 52 16,222 98 97 97 96 6/5/2014 31 4.8880 1.18 159.7 0.8465 72.03 53 15,716 98 101 98 96 6/6/2014 104 4.8880 1.08 47.1 0,8463 72.22 53 4,242 97 96 97 96 6/7/2014 4.8880 0.0 0.8465 0 98 96 98 94 6/8/2014 4.8880 1.21'` 0.0 0.8468 0 98 96 97 94 6/9/2014 283 4.8880 17.3 0.8473 72.73* 52* 1,746 99 96 98 94 6/10/2014 4.8880 0.0 0.8470 0 98 97 98 96 6/11/2014 38 4.8880 1.71 129.9 0.8465 70.76 56 18,526 99 99 98 96 6/12/2014 19 4.8880 1.11 253.4 0.8470 72.07 53 23,458 99 96 98 96 6/13/2014 27 4.8880 1.11 181.2 0.8469 72.07 53 16,774 98 96 98 96 6/14/2014 34 4.8880 1.26 143.5 0.8488 72.22 54 15,080 98 96 97 96 6/15/2014 22 4.8880 1.49 227.0 0.8495 71.81 55 28,208 98 95 98 97 6/16/2014 36 4.8880 1.28 136.3 0.8498 73.44 51 14,550 98 96 97 97 6/17/2014 25 4.8880 1.21 196.2 0.8492 72.73 53 19,799 97 1 95 95 97 6/18/2014 30 4.8880 1.26 163.8 0.8488 73.81 50 17,213 99 96 _ 97 97 6/19/2014 35 4.8880 1.34 139.3 0.8485 72.39 53 15,568 98 96 97 97 6/20/2014 28 4.8880 1.29 173.4 0.8482 72.09 54 18,655 98 97 97 96 6/21/2014 101 4.8880 1.17 48.2 0.8480 72.65 52 4,703 98 96 97 97 6/22/2014 25 4.8880 1.25 198.7 0.8484 72.80 52 20,714 98 97 97 97 6/23/2014 68 4.8880 1.06 71.8 0.8487 72.64 53 6,347 98 96 97 97 6/24/2014 38 4.8880 1.07 129.4 0.8485 73.83 50 11,547 99 97 98 97 6/25/2014 104 4.8880 1.11 47.1 0.8483 72.97 52 4,360 99 97 98 97 6/26/2014 25 4.8880 1.44 193.9 0.8491 72.22 54 23,287 98 99 96 96 6/27/2014 29 4.8880 1.32 171.2 0.8491 74.24 49 18,847 97 95 96 1 97 6/28/2014 35 4.8880 1.20 139.3 0.8487 72.50 53 13,941 98 96 97 97 6/29/2014 66 4.8880 1 1.02 73.6 0.8489 1 73.53 51 6,261 99 97 97 97 6/30/2014 39 4.8880 1.07 124.2 0.8490 72.90 52 11,083 99 97 97 96 888. 56 1 363 '391 Total 1071 146.6400 31 . 38 3.854.2 25.4391 1 _ 329 9 q49 9 Rg7 9g1F 7 RR7 Samples 26 30 26 30 30 26 26 29 Average 41 4.8880 1.21 128.5 0.8480 72.64 52 13 , 494 Primary Digester Temperature monthly average is 97°F. .; Estimate. 30 30 30 30 98 97 97 96 08/12/2014 03:19:23 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 07/01/14 TO 07/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer Ib %TS Ib %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 7/1/2014 27 4.8880 1.07 182.1 0.8494 73.83 50 16,250 99 97 98 97 7/2/2014 41 4.8880 1.06 119.3 0.8492 73.58 51 10,547 100 _ 99 98 97 7/3/2014 35 4.8880 1.17 141.4 0.8490 71.79 55 13,798 100 98 99 97 7/4/2014 54 4.8880 1.02 89.7 0.8499 73.53 51 7,631 100 96 _ 98 97 7/5/2014 45 4.8880 1.01 107.7 0.8507 73.27 52 9,072 99 96 98 96 7/6/2014 92 4.8880 1.18 53.1 0.8511 72.88 53 99 97 97_ 97 7/7/2014 1 25 4.8880 1.01 193.6 0.8514 73.27 52 _5,226 16,308 99 97 98 97 7/8/2014 27 4.8880 _ 1.02 180.1 0.8509 73.53 51 15,321 99 98 98 96 7/9/2014 48 4.8880 1.24 101.2 0.8505 72.58 _ 53 10,466 99 97 97 97 7/10/2014 59 4.8880 1.20 83.4 0.8497^ 72.50 53 8,347 99 97 97 98 7/11/2014 32 4.8880 1 1.06 154.0 0.8499 72.64 53 13,614 98 96 97 97 7/12/2014 44 4.8880 1.10 112.1 0.8501 72.73 53 10,284 ^_ 98 96 _ 97 97 7/13/2014 28 4.8880 1.22 175.3 0.8504 72.13 54 _ 17,836 99 97 97 97 7/14/2014 39 4.8880 1.19 126.5 0.8507 72.27 54 12,556 99 98 98 97 7/15/2014 45 4.8880 1.33 109.6 0.8509 73.68 51 12,157 99 97 98 98 7/16/2014 51 4.8880 1.37 96.5 0.8507 1 72.99 53 11,026 99 97 98 97 7/17/2014 98 4.8880 1.81 50.1 0.8509 71.82 55 7,563 99 97 98 97 7/18/2014 24 4.8880 1.36 203.1 0.8506 72.79 53 23,036 98 97 _ 97 98 7/19/2014 29 4.8880 1.20 170.6 0.8511 73.33 52 17,074 99 97 97 97 7/20/2014 42 4.8880 1.46 116.8 0.8515 72.60 54 14,222 99 97 97 97 7/21/2014 41 4.8880 1.44 118.3 0.8517 70.83 58 14,207 99 97 97 97 7/22/2014 63 4.8880 _ 1.05 77.3 0.8516 1 72.38 54 6,769 102 98 98 97 7/23/2014 27 4.8880 1.04 183.4 0.8516 73.08 53 15,907 100� 99 98 97 7/24/2014 26 4.8880 1.06 185.6 0.8519 72.64 54 16,408 99 97 98--- __ 98 7/25/2014 26 4.8880 1.34 186.6 0.8513 72.39 54 20,854 99 _ 97 97 98 7/26/2014 33 4.8880 1.01 146.3 0.8512 73.27 52 12,323 100 98 97 98 7/27/2014 22 4.8880 1.02 223.6 0.8515 72.55 54 19,021 99 98 97 98 _ 7/28/2014 27 14.8880 1.00 178.7 0.8515 1 73.00 53 14,904 99 99 97 98 7/29/2014 48 4.8880 1.02 102.1 0.8514 73.53 52 8,685 99 98 97 98 7/30/2014 37 4.8880 1.07 131.5 0.8517 73.83 51 11,735 98 96 _ 97 98 7/31/2014 41 4.8880 1.09 119.4 0.8516 73.39 52 10,854 98 97 96 96 Total 1,275 151.6280 36.22 4,219.0 26.3756 2,258.66 1,640 404,000 3,072 3,015 3,021 3,014 Samples 31 31 31 31 31 i 31 31 31 31 31 31 31 Averaoe 41 4.8880 1.17 136.1 0.8508 72.86 53 13,032 99 97 97 97 Prrrlarq di'gesf�r f�,K�GrctfU�2� /Y1o�f1�/y C(t/2r4yQ� ����F 09/16/2014 10:24:01 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 08/01/14 TO 08/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 8/1/2014 34 4.8880 1.18 142.5 0.8517 73.73 51 14,024 99 96 97 96 8/2/2014 24 4.8880 1.21 202.3 0.8521 74.38 50 20,415 98 95 96 97 8/3/2014 45 4.8880 1.06 107.8 0.8522 73.58 52 9,530 98 95 96 94 8/4/2014 25 4.8880 1.04 197.7 0.8525 74.04 51 17,148 98 96 96 97 8/5/2014 32 4.8880 1.11 154.4 0.8525 72.97 53 14,293 97 95 95 96 8/6/2014 1 27 4.8880 1.31 178.5 0.8528 74.05 51 19,502 98 97 95 97 8/7/2014 58 4.8880 1.05 84.9 0.8533 73.33 53 7,435 98 98 97 97 8/8/2014 25 4,8880 1.13 193.2 0.8539 74.34 50 18,208 98 96 95 97 8/9/2014 27 4.8880 1.31 178.3 0.8551 74.81 50 19,480 98 95 95 97 8/10/2014 29 4.8880 1.15 165.7 0.8559 73.04 54 15,892 97 96 95 96 8/11 /2014 24 4.8880 1.24 204.8 0.8564 73.39 54 21,180 97 96 95 95 8/12/2014 31 4.8880 1.23 160.2 0.8563 73.98 52 16,434 97 96 95 96 8/13/2014 24 4.8880 1.05 207.2 0.8566 75.24 49 18,145 97 96 95 96 8/14/2014 29 4.8880 1.10 169.9 0.8571 73.64 53 15,587 97 95 94 95 8/15/2014 27 4.8880 1.18 181.9 0.8581 73.73 54 17,901 97 95 94 93 8/16/2014 38 4.8880 1.05 128.7 0.8596 1 73.33 55 11,270 98 96 94 93 8/17/2014 45 4.8880 1.34 108.7 0.8606 72.39 58 12,148 96 96 94 95 8/18/2014 1 33 4.8880 1.26 149.1 0.8610 73.81 54 15,668 97 96 94 94 8/19/2014 43 4.8880 1.33 113.4 0.8606 73.68 55 12,579 97 97 95 96 8/20/2014 32 4.8880 1.04 153.1 0.8603 74.04 54 13,279 97 97 94 96 8/21/2014 23 4,8880 1.33 212.4 0.8610 72.93 57 23,560 97 97 95 97 8/22/2014 35 4.8880 0.96 140.2 0.8613 72.92 57 11,225 97 97 95 95 8/23/2014 32 4.8880 1 1.16 152.6 0.8617 74.14 54 14,763 97 97 95 96 8/24/2014 42 4.8880 1.03 116.4 0.8631 73.79 55 9,999 97 97 95 96 8/25/2014 59 4.8880 1.01 82.4 0.8638 74.26 55 6,941 97 97 95 96 8/26/2014 33 4.8880 1.02 147.9 0.8640 73.53 56 12,582 97 97 94 95 8/27/2014 26 4.8880 1.00 191.3 0.8647 73.00 58 15,954 97 96 95 96 8/28/2014 96 4.8880 1.13 50.9 0.8652 74.34 55 4,797 97 96 95 95 8/29/2014 40 4.8880 1.45 122.5 0.8654 72.41 59 14,814 97 96 96 95 8/30/2014 28 4.8880 1.12 173.E 0.8657 73.21 58 16,216 96 96 95 95 8/31/2014 30 4.8880 1.49 1 162.9 0.8664 1 73.15 1 58 20,243 97 96 96 96 Total 1,096 151.5280 36.07 4,735.4 26.6208 2,283.18 1,6I3 4b1,YlY 3,U"10 G,ytS I L,y-+/ t,yoo Samples 31 31 31 31 31 31 31 • 31 31 31 31 31 Averaqe 35 4,8880 1.16 152.8 0.8587 73.65 54 14,878 97 96 95 96 pr,.r,G). i ArcesdeP %empercdurC./"b'j-F 10/15/2014 05:23:50 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 09/01/14 TO 09/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 9/1/2014 28 4.8880 1.13 176.9 0.8671 74.34 56 16,671 97 96 96 96 9/2/2014 48 4.8880 1.10 101.4 0.8676 72.73 59 9,302 97 97 95 96 9/3/2014 45 4.8880 1.27 109.3 0.8677 73.23 58 11,577 97 97 96 96 9/4/2014 27 4.8880 1.18 180.4 0.8679 72.88 59 17,754 97 96 95 96 9/5/2014 34 4.8880 1.01 144.1 0.8674 74.26 56 12,138 97 96 95 96 9/6/2014 64 4.8880 1.56 76.9 0.8671 75.00 54 10,005 97 96 95 96 9/7/2014 25 4.8880 1 1.36 193.2 0.8672 72.79 59 21,914 97 96 95 95 9/8/2014 27 4.8880 1.36 181.6 0.8673 72.79 59 20,598 96 95 95 95 9/9/2014 64 4.8880 0.92 75.9 0.8671 73.91 57 5,824 96 95 95 95 9/10/2014 38 4.8880 0.95 1 129.8 0.8669 73.68 57 10,284 97 96 95 96 9/11/2014 33 4.8880 1.33 150.0 0.8672 72.93 59 16,638 97 96 95 96 9/12/2014 47 4.8880 1.18 103.6 0.8670 72.88 59 10,195 97 1 96 94 1 96 9/13/2014 28 4.8880 1.11 176.3 0.8670 72.97 59 16,321 97 95 95 95 9/14/2014 32 4.8880 1.28 150.9 0.8668 73.44 57 16,109 94 95 94 95 9/15/2014 22 4.8880 1.12 219.2 0.8663 1 73.21 58 20,475 97 94 94 95 9/16/2014 31 4.8880 0.95 159.7 0.8660 73.68 57 12,653 96 95 94 95 9/17/2014 18 4.8880 0.94 268.9 0.8652 73.40 57 21,081 95 94 94 95 9/18/2014 23 4.8880 0.96 209.9 0.8647 73.96 56 16,805 96 1 95 94 1 95 9/19/2014 26 4.8880 0.99 190.4 0.8642 72.73 58 15,721 95 94 94 95 9/20/2014 25 4.8880 0.87 199.3 0.8635 72.41 59 14,461 96 95 95 95 9/21/2014 26 4.8880 1 1.09 191.4 0.8628 1 72.48 58 17,399 95 93 94 95 9/22/2014 26 4.8880 1.00 186.1 0.8619 73.00 57 15,521 96 94 95 95 9/23/2014 26 4.8880 0.67 188.7 0.8609 71.64 59 10,544 95 94 94 95 9/24/2014 28 4.8880 0.74 176.1 0.8600 72.97 56 10,868 95 94 94 94 9/25/2014 50 4.8880 1.27 98.4 0.8598 72.44 57 10,422 95 93 94 94 9/26/2014 31 4.8880 1.40 158.9 0.8592 72.14 58 18,553 95 93 94 94 9/27/2014 25 4.8880 1.07 192.6 0.8589 1 72.90 56 17,187 95 93 94 94 9/28/2014 31 14,8880 0.98 160.2 0.8588 73.47 54 13,093 95 93 93 93 9/29/2014 41 4.8880 1.03 119.1 0.8585 73.79 54 10,231 94 93 94 94 9/30/2014 27 4.8880 1.31 178.0 0.8578 73.28 55 19,447 94 92 93 94 ioiai yy4 14b.64UU 33.13 4,647.2 25.9295 2,195.35 1,714 439,791 2,877 2,841 2,834 2,851 Samples 30 30 30 30 30 30 30 • 30 30 30 30 30 Average 33 4.8880 1.10 161.6 0.8643 73.18 57 14,660 96 95 94 95 /I ve -<. y c�, f " I o G., q D ; j t, 5 � c /- A 0 1,11A /K 7-elli l-,-,d ur e- 1, s. q S `, ' 11/24/2014 11:16:28AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 10/01/14 TO 10/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 367 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 10/1/2014 30 4.8880 1.14 164.8 0.8575 0.8571 0.8561 73.68 53 15,669 93 93 94 93 10/2/2014 25%; 4.8880 0.95 % 192.1 72.63 56 % 15,220 94 92 93 93 10/3/2014 37 4.8880 0.98 131.5 73.47 53 10,748 94 92 95 94 10/4/2014 23 4.8880 1.60 209.8 0.8560 71.88 57 27,996 95 92 94 94 10/5/2014 24 4.8880 1.19 206.5 0.8567 73.95 53 20,494 94 95 94 93 10/6/2014 19 4.8880 1.17 252.8 0.8576 72.65 56 24,668 93 95 _ 93 94 10/7/2014 28 4.8880 1.23 175.1 0.8574 72.36 56 17,962 94 92 92 94 10/8/2014 35 4.8880 0.88 140.5 0.8575 72.73 56 10,312 95 93 94 94 10/9/2014 145 4.8880 0.91 33.6 0.8576 72.53 56 2,550 95 93 94 94 10/10/2014 62 4.8880 0.87 78.6 0.8576 73.56 54 5,703 95 94 93 94 10/11/2014 27 4.8880 1.20 184.1 0.8574 1 73.33 54 18,425 95 1 98 94 93 10/12/2014 28 4.8880 1.38 174.2 0.8576 71.74 58 20,049 95 92 93 1 93 10/13/2014 77 4.8880 1.48 63.1 0.8578 73.65 54 7,789 95 92 93 93 10/14/2014 28 4.8880 1.14 176.4 0.8581 73.68 54 16,771 95 92 94 93 10/15/2014 41 4.8880 0.80 119.7 0.8580 72.50 56 7,986 96 94 94 94 10/16/2014 26 4.8880 1.07 186.3 0.8578 72.90 55 16,625 96 93 94 93 10/17/2014 109 4.8880 1.56 44.9 0.8583 73.72 54 5,842 96 92 94 93 10/18/2014 39 4.8880 0.90 124.4 0.8600 72.22 58 9,337 95 92 94 _ 93 10/19/2014 20 4.8880 1.09 245.1 0.8613 77.06 46 22,281 96 94 94 91 10/20/2014 149 4.8880 0.90 32.7 0.8618 73.33 56 2,454. 96 92 94 91 10/21/2014 27 4.8880 0.91 180.2 0.8633 72.53 58 13,676 96 93 94 92 10/22/2014 84 4.8880 0.89 58.0 0.8649 71.91 60 4,305 96 93 94 91 10/23/2014 96 4.8880 1 0.88 50.9, 0.8660 72.73 59 3,736 96 93 94 91 10/24/2014 34 4.8880 1.09 141.8 0.8671 71.56 61 12,890 96 1 92 93 90 10/25/2014 47 4.8880 0.65 104.4 0.8675 70.77 63 5,660 97 96 94 87 10/26/2014 4.8880 0.0 0.8685 0 96 93 94 91 10/27/2014 50 4.8880 0.73 97.9 0.8697 69.86 65 5,960 96 92 94 89 10/28/2014 39 4.8880 0.92 125.2 0.8710 71.74 62 9,606 96 92 94 90 10/29/2014 38 4.8880 1 1.02 127.2 0.8726 71.57 63 10,821 96 93 94 88 10/30/2014 4.8880 0.0 1 0.8742 0 97 93 94 1 91 110/31/20141 16 4.8880 0.84 1 302.5 1 0.8740 1 71.43 64 21,192 97 1 94 95 91 Total 1,406 151.5280 30.37 4,124.3 26.7179 2,107.67 1,651 366,727 2,956 2,886 2,908 2,855 Samples 29 31 29 31 31 29 29 31 31 31 31 31 Average 48 4.8880 1.05 133.0 0.8619 72.68 57 11,830 95 93 94 92^� Primary Digester Temperature monthly average is 94°F. * Data qualified. 12/11/2014 12:19:33 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO060342 11101 /14 TO 11 /30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VoIFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS Ib %TS 741 Dig #1 Temp Deg F 776 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 11/1/2014 83 4.8880 1.40 58.7 0.8732 71.43 64 6,854 98 93 95 92 11/2/2014 22 4.8880 1.25 219.8 0.8748 72.00 63 22,914 97 94 96 91 11/3/2014 4.8880 0.0 0.8762 0 97 93 94 91 11/4/2014 98 4.8880 1.78 50.0 0.8755 72.47 63 7,423 98 94 94 88 11/5/2014 130 4.8880 2.12 37.7 0.8759 71.70 64 6,666 98 94 94 90 11/6/2014 32 4.8880 1,66 150.5 0.8758 70.48 66 20,836 98 95 95 86 11/7/2014 4.8880 0.0 0.8753 0 98 95 96 87 11/8/2014 29 4.8880 1.11 169.8 0.8751 71.17 65 15,71.9 97 94 95 92 11/9/2014 75 4.8880 2.22 65.3 0.8754 70.27 66 12,090 97 95 96 93 11/10/2014 40 4.8880 1.08 121.7 0.8759k 72.22 * 63%; 10,962 97 95 96 92 11/11/2014 40 4.8880 0.95 122.0 0.8759 %; 72.63 %; 62 x 9,666 98 94 98 88 11/12/20141 35 4.8880 1 0.90 140.2 0.8749 72.22 1 63 10,523 98 95 98 93 11 /13/2014 30 4.8880 0.97 162.2 0.8724 71.13 64 13,122 97 95 98 90 11/14/2014 41 4.8880 1.66 120.1 0.8704 71.08 63 16,627 97 95 97 92 11/15/2014 49 4.8880 1.09 99.5 0.8685 72.48 60 9,045 96 95 96 90 11/16/2014 25 4.8880 0.97 198.2 0.8674 72.16 60 16,034 95 94 96 87 11/17/2014 17 4.8880 1.06 290.5 0.8658 73.58 57 25,681 95 93 95 89 11118/20141 22 4.8880 1.05 227.3 0.8652 73.33 57 19,905 95 93 95 93 11/19/2014 17 4.8880 1.05 282.2 0.8647 74.29 55 24,712 95 92 95 90 11/20/2014 22 4.8880 0.92 218.5 0.8637 72.83 158 16,765 95 92 95 94 11 /21 /2014 41 4.8880 0.91 118.0 0.8622 73.63 55 8,955 95 93 95 89 11/22/2014 24 4.8880 1.04 203.1 0.8613 73.08 56 17,616 96 92 95 92 11/23/2014 88 4.8880 1.01 55.3 0.8607 73.27 56 4,658 96 93 95 92 11/24/2014 24 4.8880 1.02 207.6 0.8601 74.51 52 17,660 97 94 96 90 11/25/2014 26 4.8880 1.08 191.1 0.8592 73.15 55 17,213 97 95 97 91 11/26/2014 28 4.8880 1.20 176.6 0.8575 72.50 56 17,674 97 95 96 94 11/27/2014 27 4.8880 0.98 178.4 0.8563 74.49 51 14,581 96 94 96 93 11/28/2014 27 4.8880 0.97 182.1 0.8548 73.20 54 14,732 96 93 96 94 11/29/2014 22 4.8880 1.02 221.1 0.8535 73.53 52 18,809 95 93 95 91 11 /30/2014 42 4.8880 1.05 115.7 0.8539 73.33 53 10,132 96 93 96 94 Total 1,156 146.6400 33.52 4,383.2 1uu1.�c I 407,574 z,aai 4,010 4,011 4,1 Gu Samples 28 30 28 30 28 26 26 30 30 30 30 30 Average 41 4.8880 1.20 146.1 0.8668 72 59 59 13,586 97 94 96 91 - Estimates. Primary Digester Temperature monthly average is 95°F. 01/14/2015 03:38:45 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 12/01/14 TO 12/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 - PrTranFlo TGD 357 -T-_ Feed Vb1Fr 30 day Mavg __ 921 DTrVoFrac % 422 PriDig %VSR ° /o 920 Transfer lb %TS lb ° %TS 741 Dig #1 Temp Deg F 776 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 - 12/1/2014 26 4.8880 1.01 185.5 0.8546 73.27 53 96_ 94 12/2/2014 25 4.8880 1.07 1972 0.8533 72.90 54 _15,625 17,598 96 96 93 12/3/2014 43 4.88800.941128 0.8516 7447 49 8,843 96 q9496 96 96 12/4/2014 4.8880 0.0 0.8515 96 96 9312/5/201429 4.8880 1.00 170.5 0.8503 _0 73.00 52 14,220 97 93 12/6/2014 40 _4.8880 1.05 -_122._9 0.8503 73.33 52 10,762 97 95 _96_ 97 _ 92 12/7/2014 41 4.8880 1.04^ 118.5- 0.8509 73.08 52 10,278 97 _ 95__ 97 _ 92 12/8/2014 26 _ 4.8880 _ _1_.10_ 190.4_ - 0.8514 73.64_ 51 17,467 97 95 96 92 12/9/2014 24 4.8880 1.18 203.9 0.8514 74.58 49 20,066 97 94 96 93 12/10/2014 28 4.8880 1.01 172.4_ _ 0.8514_ 50 14,522 _ 97 94 96 9_4_ 12/11 /2014 28 4.8880 1.04 174.8 0.8519 ^_ _74.2_6 73.08 _ _ 53 15,161 97 96 __ 94 12/12/2014 36 4.8880135.0_ 0.8_529 74.51 50_ 11,484 97 _94 _ 93 96 94 12/13/2014 25 4.8880 0.99 194.8 _ 0.8556 - 72.7 _ 55 16,084 97 94 97 12/14/2014 4.8880 0.0 0.8581 0 97 95-- 97 _93 94 12/15/2014 35 4.8880 _ 0.96 140.2 0.8600 56 11,225_ 97 95 97 93 12/16/2014 133 _ 4.8880- - 0.90 36.7 _ 0.8617 _72.92_ 73.33 56 2,755 97 95 97 94 12/17/2014 43 4.8880 0.96 114.2_ 0.8632 72.92 57 9,143 97 95 97 94 12/18/2014 31 4.8880 _ 1.00 159.9 �110.2 0.8637 72.00 59 13,336 97 95 97 93 12/19/2014 44 _4.8880 0.89 0.8638 73.03 57 8,180 97 95 96 93 12/20/2014 86 4.8880 T 04 57.0 68639 73.08 57 4,944 ^_ 97 95 96 _ 93 12/21 /2014 43 4.8880 1.12 114.4 0.8646 74.11 55 10,686 97 95 ! 96 92 12/22l2014 32 4.8880 1.04 1.03 155.0 0.8652 _ _ 74.04 _ 56 13,444 97 95 96 92 12/23/2014 112 4.8880 43.8 0.8654 73.79 56 3,763 97_ 94 96 92 12/24/2014 38 4.8880 1.62 128.1 0.8658 72.55 59 10,897 97 94 _ 96 _ _ 92 12/25/2014 47 4.8880 1.91 103.0 0.8658 71.73 61 16,407 94u 96 _ 94 T 12/26/2014 86 4.8880 1.00 57.1- 0.8679 73.00 59 4,762 _97 97 94 96 _ 93 12/27/2014 34 4.8880 1.25 141.9 _0.8682 72.00 61 14,793 97 93 96 ^ 94 12/28/2014 33 4.8886 1.49 147.8 0.8686 T 72.48 60 18,367 97 96 98 91 12/29l2014 26 4.8880 1.66 189.1 0.8686 -71.69 62 26,180 98 95 �98 93 12/30/20141 _ 25 4.8880 198.5 0.8686 71.54 62 20,363 _ 98 96 98 92 12/31l2014 T ♦., I 43 I U O 4.8880L:�1L03--TI-4.3-0.8693-- 7 n n r ---T 71_.84 62 - 9,819 _ 98 95 98 94 I lllGll L7� a,aua.a _��;°X-W .410 qS-Qfj 1,55q_, 371,174 3,006 2,932 2,992 2,886 Samples _ g _ 31 a $ _T 31 30 S _ a g - 31 31 31 31 31 _ Average _ 4/� 4.8880 1.10 128.7 SS4 - 73•o 56 11,973 97 95 97^ 93 E sf; Mgfe. Prirn12r4 JiceSter e-mpera4ure- MONA)q average- fS MUDDY CREEK WWTP NPDES Permit # NC0050342 2014 Pathogen and Vector Attraction Reduction Summary and Operational Data Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Muddy Creek WWTP NPDES Permit # NC0050342 2014 Compliance Summary Pathogen Reduction PSRP Data for Class B Residuals Anaerobic Digester System Month * * PrimaryDi ester SRT(days)* Monthly Average Temp..°F Monthly Average January 50 94 February 50. 95 March 50 95 April 41 96 May 35 95 June 41 97 July 41 97 August 35 96 September 33 95 October 48 94 November 41 95 December 41 96 * SRT = Solids Retention Time; based on % Total Solids. ** Bi-monthly monitoring is required but is actually done on a monthly basis. Page 2 MUDDY CREEK WWTP Pathogen Reduction NPDES Permit # NC0050342 This plant normally operates three Primary Digesters (1, 2, and 3) and one Secondary Digester (4). The SRTs (or MCRTs) for the Muddy Creek WWTP are calculated daily and the summary on Page 1 uses the monthly average since daily values fluctuate so greatly from day to day. The formula below, using data from January 1, 2014, shows an example calculation. See attached monthly LAND APPLIED BIOSOLIDS REPORT, Page 4. Any estimated or qualified data is marked as such on these report pages. Any estimates are not included in the monthly average shown on the previous Page 1. Please find Digester Temperatures on this same report Page 4. Digester #4 is a Secondary Digester and its temperature is not included in determining the monthly average. Occasionally, this Digester's temperature does not get recorded and those instances are either notated or left blank in the data column for `Dig#4 Temp'. FORMULA: [Primary Digester Volume x 8.34 x Primary Digester Transfer %Total Solids] (Pounds of solids in Primary Digesters) [Transfer %Total Solids x 8.34 x Primary Transfer Flow] (Pounds of solids being transferred to Blending Tanks) = PriDigSRT (Days %TS) FROM ATTACHED DATA SHEETS for January 1, 2014: [[PriDigVOL (MG)] x 8.34 x [Trans%TS (%)]] [[Trans%TS (%)].x 8.34 x [PrTranflo (TGD)/1000]] or [4.8880 x 8.34 x 0.06921 = 0.3750 = 33.19 or [0.0092 x 8.34 x (146.9/1000)] 0.0113 as shown on the report, 33 Days SRT 02/25/2014 10:20:49 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO060342 01/01/14 TO 01/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS Ib %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 4.8880 4.8880 4.8880 0.92 1.83 1.47 1.82 1.39 146.9 49.0 97.9 102.8 137.1 0.0 0.6813 0.7051 0.6992 0.6745 0.6658 0.6915 66.30 54.64 61.22 61.54 61.15 61.29 8 50 32 23 21 29 11,271 7,478 12,002 15,604 15,893 0 95 95 95 95 95 95 92 92 92 92 93 94 95 95 95 95 95 96 89 89 89 88 86 86 l/l/2014 1!2/2014 1/3/2014 33 100 50 1/4/2014 48 4.8880 1/5/2014 36 4.8880 1/6/2014 4.8880 1.24 205.6 137.1 0.7177 0.7284 0,7582 0,7588 0,7738 0,6130 0.6811 0.7463 62.41 61.65 60.27 61.84 61.27 61.11 62.12 58.70 60.26 60.94 62.12 60.77 61.60 61.29 62.14 61.27 61.54 61.64 61.64 62.69 61,42 60.92 35 40 52 48 54. 1 23 57 54 45 60 62 66 63 66 70 68 70 71 72 70 70 22,806 15,207 11,921 8,684 9,273 12,346 16,7110 28,175 10,187 18,8200 0 14,554 19,114 15,314 4,561 10,859 15,656 9,923 19,480 20,870 13,679 3,114 28,414 95 95 95 95 96 96 96 96 96 95 95 95 95 95 95 95 95 95 95 95 95 95 95 92 92 92 92 93 93 93 93 93 92 92 92 93 92 92 92 92 93 93 93 93 91 92 94 95 95 94 95 95 96 96 96 96 96 96 96 95 96 96 96 95 95 95 95 95 95 87 88 86 84 87 88 887 89 89 87 88 89 89 87 87 87 88 89 88 88 89 87 84 1/7/2014 24 4.8880 1.33 1/8/2014 36 4.8880 1.33 1/9/2014 50 4.8880 1.46 97.9 1/10/2014 71 4.8880 1.52 68.5 111/ 0014 62 4.8880 1.42 78.3 1l12/2014 48 4.8880 1.44 102.8 1/l 3/2014 32 4.8880 1.32 151.8 1 /14/2014 4.8880 0.0 1/15/ 0014 20 4.8880 1.38 244.8 0.7664 1/16/2014 62 4,8880 1.56 78.3 0.7661 1/17/ 0014 28 4.8880 1.28 176.3 0.7387 1/18l2014 4.8880 0.0 0.8025 1 /19/ 0014 4.8880 0.0 0.8034 1/20/2014 37 4.8880 1.32 132.2 0,8049 1 l21 /2014 28 4.8880 1.30 176.3 0.8014 1/22/2014 33 4.8880 1.25 146.9 0.8254 1123/2014 111 4.8880 1.24 44.1 0.8108 1/24/2014 53 4.8880 1.40 93.0 0.8295 1/25/2014 37 4.8880 1.42 132.2 0.8390 1/26/2014 59 4.8880 1.43 83.2 0.8316 1 /27/2014 33 4.8880 1.59 146.9 0.8408 1128/2014 29 4.8880 1.46 171.4 0.8487 1/29/2014 40 4.8880 1.34 122.4 0.8590 1 /30/2014 666 4.8880 1.27 29.4 0.8395 1/31/2014 25 4.8880 1.74 195,8 0.8406 17A 1 715 75 1 378 391,916 2,952 2,865 2,955 2,715 Total 1,349 151.5280 39.47 3,348.9 23. Samples 27 31 28 31 31 28 28 31 31 31 31 31 Average 50 4.8880 1.41 108.0 0.7659 61.28 49 12,642 95 92 95 88 Page 1 CITY OF WINSTON-SALEM 2014 Annual Monitoring Report for WWTP Residuals Muddy Creek WWTP NPDES Permit # NCO050342 2014 Compliance Summary Vector Attraction Reduction Requirements for Class B Residuals Compliance determination by Calculation of Volatile Solids Reduction across the Anaerobic Digesters as the treatment system. Calculated %VSR (380,/o Minimum) -Monthly Average VAR Option 1 Month * Primary Digester System_ January 49 February 65 March 61 56 55 June 52 ** 53 54 September 57 October 57 November 59. December 56 * Bimonthly monitoring is required but is actually done on a monthly basis. ** Beginning in June, 2014, there is an offset of time factored in regarding digester solids retention time (or MCRT). A given month's'%VSR is now calculated using the previous month's SRT average. See page 2 of this section for the formula used for the first five months of 2014, as well as the formula now used beginning in June of 2014. The equation used for calculating the above %VSRs is from the EPA White House Manual, Control of Pathogens and Vector Attraction in Sewage Sludge, Chapter 10 and Appendix C. Page 2 Muddy Creek WWTP Vector Attraction Reduction NPDES Permit # NCO050342 Data submitted in the chart on Page 1 of this summary shows that the calculated monthly average Volatile Solids Reduction meets the minimum of 38% VSR requirement over the Primary Digester System at the Muddy Creek WWTP for the year of 2014,. Volatile Solids Reduction (VSR) is calculated by the Van Kleeck equation using the digester feed and digester stabilized transfer sludge volatile fractions. While there was previously no offset necessary for digester Solids Retention Times (or MCRTs) due to the consistency with which these digesters were operated, upon in-house review, the City began in June of 2014 calculating one month's %VSR using the previous month's SRT average. This more accurately reflects current digester operations. Any data qualified by the lab is marked as such on data sheets. Also, in instances when a daily sample was not collected for %Volatile Solids analysis of the Transfer (`Trans') Sludge, an estimated value was used along with actual flows for that day in order to calculate treatment in the digesters. Any estimated daily values are marked as such on data sheets, but the monthly average values (shown on the previous Page 1) were calculated excluding this estimated data in order to certify compliance. The values for January 2, 2014 from the attached LAND APPLIED BIOSOLIDS report Page 4 are used in the example equation below. This is the formula used for the period of Jan. — May, 2014. The heading `VolFrac 311+318' refers to the Volatile Fraction of the Digester feed samples and the heading `DTrVoFrac' refers to the Volatile Fraction of the stabilized Primary Digester transfer samples. The calculated Percent Volatile Solids Reduction is indicated by the heading `PriDig%VSRed (%)'. VolFrac 3l l + 318 TrVoFrac/100] FORMULA January —May, 2014: [ ] - � = PriDi VSR (%) (Feed) (Transfer) g [VolFrac 311+ 318] - [(VolFrac 311 + 318) x .(DTrVoFrac/100)] (Feed) (Feed) (Transfer) FROM ATTACHED DATA SHEETS for January 2, 2014: 0.7051— 0.5464 = 0.1587 = 0.4962 or as shown on the report, 50% VSR 0.7051 - (0.7051 x 0.5464) 0.3198 --------------------------------------------------------------------------------------------=------------------------ - See on the attached LAND APPLIED BIOSOLIDS report Page 4, June 1, 2014, for the current method of calculating %VSR. The new heading of "Feed VolFr 30 day mavg" is the Feed Volatile Fraction 30 day moving average. See monthly averages June — Dec., 2014, in the chart on the previous Page 1 of this summary and attached daily data. FORMULA June — December, 2014: [Feed Vol Frac 30 day mavg] - [D r ooF f =/)100] Fee = priDigVSR:(%) (d) [Feed Vol Frac 30 day mavg] - [(Feed Vol Frac 30 day mavg) x (DTrVoFrac/100)] (Feed) (Feed) (Transfer) FROM ATTACHED DATA SHEETS for June 1, 2014: 0.8472 — 0.7193 = 0.1279 = 0.5378 or as shown on the report, 54% VSR 0.8472 — (0.8472 x 0.7193) 0.2378 Van Kleeck-Equation used: %VS Reduction = r%VS (Feed)l - f%VS (S1abilized)1 [%VS (Feed)] -,[%VS (Feed) x %VS (Stabilized)] %VS (Feed) = Volatile fraction of raw and thickened sludges fed to primary digesters %VS (Transfer) = Volatile fraction of stabilized sludge transferred from primary digesters 02/25/2014 10:20:49 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 PriDig SRT PriDig VOL Trans %TS PrTranFlo VolFrac DTrVoFrac PriDig% VSRed Trans lb %TS Dig #1 Temp Dig #2 Temp Dig #3 Temp. Dig #4 Temp Days %TS MG % TGD 311+318 % % lb %TS Deg F Deg F Deg F Deg F Date 163 492 • 93 357 389 422 751 741 775 776 777 778 0.6813 66.30 54.64 8 50 32 23 21 29 35 40 52 48 1 23 57 45 60 62 66 63 66 68 70 71 72 70 70 1,378 11,271 7,478 12,002 15,604 15,893 - 0 22,806 15,207 11,921 9,273 12 346 16,710 28,175 10,187 18,820 0 0 14,554 19,114 1�,56� 85 10,9 1g 923 19,480 20,870 13i614 28,414 391,916 95 95 95 95 95 95 95 95 96 96 96 96 96 96 95 95 95 95 95 95 95 95 95 95 95 95 95 2,962 92 92 92' 92 94 92 92 g2 93 93 93 93 93 93 92 92 92 92 93 92 92 92 92 93 93 93 93 91 92 2,865 95 95 95 95 95 96 95 94 95 95 95 96 96 96 96 96 96 gg 96 95 96 96 96 95 95 95 95 95 95 2,955' 89 89 88 86 86 87 88 87 88' 89 87 89 89 87 87 88 89 89 87 87 87 88 89 88 88 89 87- 2,715 1/1/2014 33 4.8880 0.92 146.9 1/2/2014 100 4.8880 1.83 49.0 0.7051 1/3/2014 50 4.8880 1.47 97.9 0,6992 61.22 61.54 61.15 61.29 62.41 61.65 60.27 61.84 61.27 62,11 62.12 58.70 60.26 60 62.12 60.77 61.60 61.29 62.14 61,27 61., 61 62 84 62.69 61.42 60,92 1.715.75 1!4/2014 48 44.8880 1.82 102.8 0.6745 1!5/2014 36 4.8880 1.39 137.1 0.6658 1Y6/2014 4:8880 1,24 0.0 0.6915 1(7/2014 1/8/2014 '1/9/2014 24 36 50 71 62 48 32 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 1.33 1.33 1,46 1.52 1.42 1.44 1,32 1.38 1.56 1.28 1,32 1.30 1.25 1.24 1.40 1.42 1.43 1.59 1.46 1.34 1.27 1.74. 205.6 137.1 97.9 68.5 78.3 102.8 151.8 0.0 244.8 78.3 176.3 0.0 0.0 132.2 176.3 146.9 44.1 93.0 132.2 83.2 146.9 171.4 122.4 29,4 195.8 OAa o 0.7177 0.7284 0,7582 0.7588 OJ738 0.6811 0.6811 0.7463 0.7664 0.7661 0.7387 0,8025 0.8034 0.8049 0.8014 0.8254 0,8108 0.8295 0.8390 0.8316 0.8408 0.8590 0.8590 0.8395 0.8406 �s 7431 1/10/2014 1111/2014 1/12/2014 1/13/2014 1/14/2014 1115/2014 20 1/16/2014 1117/2014 1/18/2014 1/19/ 0014 1l20/2014 1/21/2014 1/22/2014 1/23/2014 1/24/2014 1/25/2014 1/26/2014 1l27l2014 1 /28/2014 1/29/2014 1/30/2014 1 /31 /2014 62 28 37 28 33 111 53 37 59 33 29 40 666 25 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4,8880 4.8880 Total 1,34y 31 28 28 31 o i _ . Samples 27 31 28 31 .41 108.0 0.7659 6128 49 12,642 95 92 Average 60 4,8880 195 88 07/17/2014 09:09:55 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 06/01/14 TO 06/30/14 PriDig VOL Trans %TS PrTranFlo Feed VolFr DTrVoFrac PriDig %VSR Transfer lb %TS Dig #1 Temp Dig #2 Temp Dig Temp Dig Temp PriDig SRT Days %TS MG % TGD 30 day % % lb %TS Deg F Deg F Deg F Deg F Mavg Date 163 492 93 357 921 422 920 741 776 776 777 778 172.9 0.8472 71.93 73.83 72.22 72.64 72.03 72.22 72.73 �4 70.76 72.07 72.07 72.22 71.81 73.44 72.73 73.81 72.39 72.09 72.65 72.80 72.64 73.83 72.22 72.22 74.24 72.50 73.53 72.90 1 RRR _ S6 54 49 53 52 53 53 52* 56 53 53 54 55 51 53 50 53 54 52 52 53 50 52 54, 49 53 51 52 1363 16,439 15,170 14,619 16,222 15,716 4,2422 0 1,746 0 18,526 23,458 16,774 15,080 28,208 14,550 19,799 17,213 15,568 18,653 4.70 20,714 6,347 11,547 4,360 23,2877 18,847 13,941 6,261 11,083 391 , 329 97 97 97 98 98 97 98 99 98 99 99 98 98 98 98 97 99 98 98 98 98 98 99 99 98 97 98 99 99 95 95 99 97 101 96 96 96 97 99 96 96 95 95 95 95 96 96 97 96 97 96 97 97 99 95 96 97 97 97 97 96 97 98 9796 8 97 98 98 98 98 . 98 97 98 97 95 97 97 97 97 97 97 98 98 96 96 97 97 97 2,915 94 94 95 96 96 94 94 94 96 _96 _ 96 96 96 97 97 97 97 97 96 97 97 97 97 97 96 97 97 97 96__ 2,882 6/1 /2014 28 4.8880 1.14 6/2/2014 29 4.8880 1.07 170.0 0.8474 0.8473 0.8471 0.8465 0.8463 0.8465 0.84 68 0.8473 0.8470 0.8465 6/3/2014 30 4.8880 1.08 162.3 6/4/2014 27 4,8880 1.06 183.5 6/5/2014 31 4.8880 1.18 159.7 6/6/2014 104 4.8880 1.08 47.1 6/7/2014 4.8880 0.0 6/8/2014 4.8880 1.21 J` 0.0 6/9/2014 283 :: 4.8880 17.3 0.0 6/10/2014 4.8880 6/11/2014 38 4.8880 1.71 129.9 6/12/2014 19 4.8880 1.11 253.4 0.8470 6/13/2014 6/14/2014 6/15/2014 6/16/2014 6/17/ 0014 6/18/2014 6/19/2014 6/20/2014 6/21/2014 6/22/2014 6/23/2014 6/24/2014 6/25/2014 6/26/2014 6/27/2014 6/28/2014 6/29/2014 6/30/2014 27 34 22 36 25 30 35 28 101 25 68 38 104 25 29 35 66 39 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 1.11 1.26 1.49 1.28 1.21 1.26 1.34 1.29 1.17 1.25 1.06 1.07 1.11 1.44 1.32 1.20 1.02 1.07 181.2 143:5 227.0 136.3 196.2 163.8 139.3 173.4 48.2 198.7 71.8 129.4 47.1 193.9 171.2 139.3 73.6 124.2 0.8469 0.8488 0.8495 0.8498 0.8492 0.8488 0.8485 0.8482 0.8480 0.8484 0.8487 0.8485 0.8483 0.8491 0.8491 0.8487 0.8489 0.8490 o nc �aoa 2,942 2,897 Total IV i I , , . 26 - 26 Samples 26 30 26 30 30 Average 41 4.8880 1.21 128.5 0.8480 72.64 52 Primary Digester Temperature monthly average is 97°F• Estimate. 29 30 Su ")v 11 3 , 494 98 97 97 96 02/24/2014 01:39:24 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 01/01/14 TO 01/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans Ib %TS lb %TS 741 Dig #1 Temo Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temn Deg F 777 Dig #4 Temp Deg F 778 1/1/2014 33 4.8880 0.92 146.9 0.6813 1 66.30 8 11,271 95 92 95 89 1/2/2014 100 4.8880 1.83 49.0 0.7051 54.64 50 7,478 95 92 95 1 89 1/3/2014 50 4.8880 1.47 97.9 0.6992 61.22 32 12,002 95 92 95 89 1/4/2014 48 4.8880 1.82 102.8 0.6745 61.54 23 15,604 95 92 95 88 1/5/2014 36 4.8880 1.39 137.1 0.6658 61.15 21 15,893 95 93 95 86 1 /6/2014 4.8880 1.24 0.0 0.6915 61.29 29 0 95 94 96 86 1/7/2014 24 4.8880 1.33 205.6 0.7177 1 62.41 35 22,806 95 92 94 87 1/8/2014 36 4.8880 1.33 137.1 0.7284 61.65 40 15,207 95 92 95 88 1/9/2014 50 4.8880 1.46 97.9 0.7582 60.27 52 11,921 95 92 95 86 1/10/2014 71 4.8880 1.52 68.5 0.7588 61.84 48 8,684 95 92 94 84 1 /11 /2014 62 4.8880 1.42 78.3 0.7738 61.27 54 9,273 96 93 95 87 1/12/2014 48 4.8880 1.44 102.8 0.6130 61.11 1 12,346 96 93 95 88 1/13/2014 32 4.8880 1.32 151.8 0.6811 62.12 23 16,711 96 93 95 89 1/14/2014 4.8880 0.0 0.7463 0 96 93 96 87 1 /15/2014 20 4.8880 1.38 244.8 0.7664 58.70 57 28,175 96 93 96 89 1/16/2014 62 80 1.56 78.3 0.7661 60.26 54 10,187 96 93 96 89 1/17/ 0014 28 80 1.28 176.3 0.7387 60.94 45 18,820 96 92 96 87 1 /18/2014 80 [4.8880 0.0 0.8025 0 95 92 96 87 1/19/2014 0.0 0.8034 0 95 92 96 88 1/20/2014 37 80 1.32 132.2 0.8049 62.12 60 14,554 95 92 96 89 1 /21 /2014 28 4.8880 1.30 176.3 0.8014 1 60.77 62 19,114 95 93 96 89 1/22/2014 33 4.8880 1 1.25 146.9 0.8254 1 61.60 66 15,314 95 92 95 87 1/23/2014 111 4.8880 1.24 44.1 0.8108 61.29 63 4,561 95 92 96 87 1/24/2014 53 4.8880 1.40 93.0 0.8295 62.14 66 10,859 95 92 96 87 1/25/2014 37 4.8880 1.42 132.2 0.8390 61.27 70 15,656 95 92 96 88 1/26/2014 59 4.8880 1.43 83.2 0.8316 61.54 68 9,923 95 93 95 89 1/27/2014 33 4.8880 1.59 146.9 0,8408 61.64 70 19,480 95 93 95 88 1/28/2014 29 4.8880 1.46 171.4 0.8487 61.64 71 20,870 95 93 95 88 1/29/2014 40 4.8880 1.34 122.4 0.8590 62.69 72 13,679 95 93 95 89 1/30/2014 166 4.8880 1.27 29.4 0.8395 61.42 70 3,114 95 91 95 87 1/31/2014 25 4.8880 1.74 195.8 0.8406 60.92 70 28,414 95 92 95 84 Total 1,349 151.5280 39.47 3,348.9 23.7431 1,715.75 1,378 391,91b [,U01 L,bt)O Z,U00 Z,i 10 Samples 27 31 28 31 31 28 28 31 31 31 31 31 Averaoe 50 4.8880 1.41 108.0 0.7659 61.28 49 12,642 95 92 95 88 Primary Digester Temperature monthly average is 94°F. 03/13/2014 04:22:59 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 02/01 /14 TO 02/28/14 PriDig PriDig Trans PrTranFlo VolFrac DTrVoFrac PriDig% Trans lb Dig Dig #2 Dig Dig #4 SRT VOL %TS VSRed %TS #1 Temp #3 Temp Temo Temo Days %TS MG % TGD 311+318 % % lb %TS Deg F Deg F Deg F Deg F Date 163 492 93 367 389 422 751 741 775 776 777 778 2/1/2014 36 4.8880 1.35 137.1 0.8448 62.96 69 15,436 95 92 95 88 2/2/2014 4.8880 0.0 0.8491 0 96 92 95 90 2/3/2014 37 4.8880 1.41 132.2 0.8358 63.12 66 15,546 96 92 95 85 2/4/2014 67 4.8880 1.32 73.4 0.8470 63.64 68 8,080 96 93 95 89 2/5/2014 55 4.8880 1.25 88.1 0.8635 64.00 72 9,184 96 93 96 91 216/2 114 33 4.8880 1.45 146.9 0.8631 63.45 72 17,765 95 92 95 91 2/7/2014 42 4.8880 1.26 117.5 0.8648 64.29 72 12,347 95 92 95 89 2/8/2014 83 4.8880 1.33 58.8 0.8647 64.66 71 6,522 95 93 95 90 2/9/2014 32 4.8880 1.23 151.8 0.8620 65.85 69 15,572 95 93 95 91 2/10/2014 29 4.8880 1.22 166.5 0.7817 63.93 51 16,941 95 93 95 90 2/11/ 0014 77 4.8880 1.22 63.6 0.7733 63.93 48 6,471 95 93 96 91 2/12/2014 38 4.8880 1.24 127.3 0.8460 64.52 67 13,165 96 92 96 91 2/13/2014 38 4.8880 1.37 127.3 0.8575 63.50 71 1.4,545 96 92 96 91 2/14/2014 83 4.8880 1.22 58.8 0.8525 65.57 67 5,983 96 92 96 90 2/15/2014 4.8880 0.0 0.8125 0 95 92 96 90 2/16/2014 4.8880 0.0 0.8275 0 96 92 96 90 2/17/2 114 29 4.8880 1.28 168.0 0.8422 66.41 63 17,934 96 92 96 90 2/18/2014 31 4.8880 1.27 156.7 0.8423 65.35 65 16,597 95 93 96 90 2/19/2014 25 4.8880 1.58 195.8 0.8479 63.92 68 25,801 95 93 96 90 2/20/2014 51 4.8880 1.24 95.1 0.8540 65.32 68 9,835 96 93 96 91 2/21/2014 55 4.8880 1.19 88.1 0.8491 66.39 65 8,744 96 93 96 89 2/22/2014 42 4.8880 1.24 117.5 0.8298 65.32 61 12,151 96 93 96 91 2/23/2014 28 4.8880 1.58 172.7 68037 63.29 58 22,757 96 93 96 92 2/24/2014 90 4.8880 1.34 54.1 0.8174 64.18 60 6,046 97 93 96 92 2/25/2014 32 4.8880 1.49 154.8 0.8276 65.10 61 19,236 97 93 96 92 2/26/2014 106 5880 1.19 45.9 0.8395 64.71 65 4,555 96 93 96 92 2/27/2014 35 4.8880 1.52 138.2 0.8357 63.82 65 17,519 96 93 95 92 2/28/2014 62 4.8880 1.20 79.4 0.8477 65.83 65 7,946 96 92 95 91 1) ego o a77 Total 1,238 13t).t5b4V 3Y.`.1`9 G,y 10.0 LJ.'40G 7 i,v I. -- - - -- • - --- - - Samples 25 28 25 28 28 25 25 28 28 28 28 28 Averaae 50 4.8880 1.32 104.1 0.8387 64.52 65 11,667 96 93 96 90 Primary Digester Temperature monthly average is 95°F. 04/16/2014 04:33:47 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 03/01/14 TO 03/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temo Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temn Deg F 777 Dig #4 Temp Deg F 778 3/1/2014 50 4.8880 1.33 97.9 0.8522 65.41 67 10,859 96 93 95 91 3/2/2014 34 4.8880 1.12 142.1 0.8525 64.29 69 13,273 96 93 96 90 3/3/2014 34 4.8880 1.20 143.1 0.8480 81.67 20 14,321 96 93 95 92 3/4/2014 113 4.8880 1.19 43.3 0.8277 67.23 57 4,297 95 92 95 91 3/5/2014 33 4.8880 1.16 146.3 0.8456 67.24 63 14,154 95 92 95 89 3/6/2014 48 4.8880 1.31 102.8 0.7899 67.18 46 11,231 95 92 95 88 3/7/2014 37 4.8880 1.39 132.8 0.8260 66.91 57 15,395 95 91 95 90 3/8/2014 37 4.8880 1.18 133.2 0.8104 67.80 51 13,108 95 91 95 88 3/9/2014 39 4.8880 1.24 124.8 0.8218 66.13 58 12,906 95 92 96 90 3/10/2014 29 4.8880 1.15 171.5 0.8283 66.96 58 16,449 96 93 96 92 3/11/2014 62 4.8880 1.15 1 79.2 0.8593 68.70 64 7,596 96 94 96 91 3/12/2014 44 4.8880 1.16 110.7 0.8610 68.10 66 10,710 96 94 96 91 3/13/2014 33 4.8880 1.18 148.3 0.8411 1 66.95 62 14,594 96 93 96 91 3/14/2014 44 4.8880 1.30 112.1 0.8531 67.69 64 12,154 96 92 96 91 3/15/2014 42 4.8880 1.24 115.1 0.8349 67.74 58 11,903 96 92 96 92 3/16/2014 100 4.8880 1.12 49.0 0.8618 67.86 66 4,577 96 92 96 90 3/17/2014 25 4.8880 1.25 193.7 0.8576 68.00 65 20,193 96 92 96 91 3/18/2014 30 4.8880 1.27 163.9 0.8337 67.72 58 17,360 96 92 96 91 3/19/2014 31 4,8880 1.32 156.7 0.8631 67.42 67 17,251 96 93 95 91 3/20/2014 49 4.8880 1.31 98.9 0.8591 67.94 65 10,805 96 97 95 91 3/21/2014 67 4.8880 1.10 73.4 0.8569 69.09 63 6,734 96 92 96 91 3/22/2014 27 4.8880 1.24 181.7 0.8557 67.74 65 18,791 96 92 96 92 3/23/2014 34 4.8880 1.30 142.0 0.8589 67.69 66 15,396 96 93 96 92 3/24/2014 137 4.8880 1 1.39 35.7 0.8649 66.91 68 4,139 96 93 96 92 3/25/2014 28 4.8880 1.31 175.5 0.8612 67.94 66 19,174 96 93 96 92 3/26/2014 31 4.8880 1.29 156.0 0.8625 67.44 67 16,783 95 92 96 91 3/27/2014 84 4.8880 1.20 57.9 0.8566 68.33 64 5,795 95 92 96 91 3/28/2014 45 4.8880 1.10 108.6 0.8442 69.09 59 9,963 95 92 95 89 3/29/2014 27 4.8880 1.30 178.7 0.8573 69.23 63 19,375 96 92 95 89 3/30/2014 107 4.8880 1.19 45.5 0.8493 69.76 59 4,516 96 92 95 90 3/31/2014 34 14.8880, 1 1.50 144.6 0.8634 69.33 64 1 18,089 96 92 1 95 90 Total 1,536 151.5280 38.49 3,765.0 26.2577 2.111.47 1,883 391,891 2,967 2,868 2,963 2,810 Samples 31 31 31 31 31 31 31 31 31 31 31 31 Averaae 50 4.8880 1.24 121.5 0,8470 68.11 61 12,642 96 93 96 91 .Primary Digester Temperature monthly average is 95°F. 05/21/2014 02:13:10 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 04/01/14 TO 04/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans lb %TS lb %TS 741 Dig #1 Temo Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temo Deg F 777 Dig #4 Temp Deg F 778 4/1/2014 34 4.8880 1.12 144.6 0.8624 69.64 63 13,507 96 93 95 92 4/2/2014 42 4.8880 1.22 116.8 0.8722 70.49 65 11,884 97 94 96 92 4/3/2014 60 4.8880 1.25 81.9 0.8621 68.80 65 8,538 93 96 95 91 4/4/2014 46 4.8880 1.13 107.1 0.8480 69.91 58 10,093 96 93 95 92 4/5/2014 41 4.8880 1.51 118.4 0.8474 70.86 56 14,911 95 94 96 92 4/6/2014 28 4.8880 1.53 176.4 0.8546 69.93 60 22,509 96 94 96 93 4/7/2014 27 4.8880 1.11 180.9 0.8405 70.27 55 16,747 95 93 96 93 4/8/2014 37 4.8880 1.15 132.1 0.8242 ` 71.30 47 12,670 95 94 95 93 4/9/2014 37 4.8880 1.12 133.3 0.8590 71.43 59 12,451 95 94 97 93 4/10/2014 46 4.8880 1.11 105.5 0.8638 69.37 64 9,767 96 93 98 93 4/11/2014 29 4.8880 1.12 168.8 0.8489 69.64 59 15,767 95 93 99 93 4/12/2014 30 4.8880 1 1.09 162.6 0.8448 69.72 58 14,781 95 93 100 93 4/13/2014 78 4.8880 1.65 63.0 0.8552 70.30 60 8,669 96 94 101 92 4/14/2014 47 4.8880 1.04 103.9 OB649 71.15 • 61 9,012 98 94 102 93 4/15/2014 29 4.8880 1.23 166.8 0.8094 69.92 45 17,111 98 94 104 94 4/16/2014 24 4.8880 1.56 206.0 0.7816 69.23 37 26,801 98 93 103 94 4/17/2014 40 4.8880 1.04 121.2 0.8395 70.19 55 10,512 97 93 102 94 4/18/2014 36 4.8880 1 1.27 137.3 0.8439 71.65 53 14,543 96 93 103 94 4/19/2014 39 4.8880 1.18 124.0 0.8397 69.49 57 12,203 96 93 103 94 4/20/2014 35 4.8880 1.13 140.9 0.8414 70.80 54 13,279 98 93 99 94 4/21/2014 47 4.8880 1.05 103.6 0.8483 71.43 55 9,072 98 94 99 94 4/22/2014 33 4.8880 1.20 147.0 0.8478 70.00 58 14,712 98 93 100 94 4/23/2014 34 4.8880 1.07 142.0 0.8498 71.03 57 12,672 98 93 98 94 4/24/2014 50 4.8880 1.04 97.6 0.8492 69.23 60 8,465 97 94 98 94 4/25/2014 30 4.8880 1.21 162.1 0.8395 71.07 53 16,358 96 94 97 94 4/26/2014 29 4.8880 1.16 168.7 0.8345 71.55 50 16,321 96 95 97 94 4/27/2014 113 4.8880 1.48 43.3 0.8372 70.27 54 5,345 96 95 97 94 4/28/2014 23 4.8880 1.09 209.1 0.8419 70.64 55 19,008 96 95 97 94 4/29/2014 62 4.8880 1.10 78.9 0.8490 71.82 55 7,238 96 94 96 95 4/30/2014 32 4.8880 1.10 151.3 0.8462 70.91 56 13,880 1 96 94 96 94 Total 1,238 146.6400 36.06 3,995.1 25.3468 2,112.08 1,686 398,826 2,888 2,812 2,950 2,800 Samples 30 30 30 30 30 30 30 30 30 30 30 30 Averaae 41 4.8880 1.20 133.2 0.8449 70.40 56 13,294 96 94 98 93 * Data qualified by Lab. Primary Digester Temperature monthly average is 96°F. 06/12/2014 03:05:07 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 05/01/14 TO 05/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 VolFrac 311+318 389 DTrVoFrac % 422 PriDig% VSRed % 751 Trans Ib %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 5/1/2014 43 4.8880 1.11 114.1 0.8396 71.17 53 10,563 97 94 97 94 5/2/2014 40 4.8880 1.30 122.4 0.8500 70.77 57 13,271 96 95 96 94 5/3/2014 29 4.8880 1.12 168.3 0.8530 71.43 57 15,721 96 95 97 94 5/4/2014 30 4.8880 1.16 160.9 0.8468 67.24 63 15,566 95 95 97 94 5/5/2014 48 4.8880 1.13 102.7 0.8323 72.57 47 9,679 @ 95 94 94 5/6/2014 29 4.8880 1.12 168.9 0.8581 71.43 59 15,777 94 96 96 94 5/7/2014 59 4.8880 1.10 83.3 0.8509 70.91 57 7,642 94 96 96 94 5/8/2014 32 4.8880 1.13 152.9 0.8427 71.68 53 14,410 94 95 96 94 5/9/2014 46 4.8880 1.20 105.3 0.8511 70.83 58 10,538 96 95 96 95 5/10/2014 33 4.8880 1.18 146.4 0.8472 72.03 54 14,408 95 96 96 94 5/11/2014 45 4.8880 1 1.49 107.9 0.8527 71.81 56 13,408 96 1 95 97 94 5/12/2014 30 4.8880 1.23 161.6 0.8568 71.54 58 16,577 95 94 97 95 5/13/2014 31 4.8880 1.42 155.6 0.8326 71.13 50 18,427 96 95 97 95 5/14/2014 29 4.8880 1.31 170.5 0.8501 70.99 57 18,628 96 95 97 1 95 5/15/2014 57 4.8880 1.32 85.1 0.7876 70.45 36 9,368 96 95 97 95 5/16/2014 25 4.8880 1.16 194.3 0.8185 71.55 44 18,797 96 94 96 94 5/17/2014 29 4,8880 1.23 166.8 0.8368 71.54 51 17,111 96 93 96 94 5/18/2014 23 4.8880 1.30 210.0 0.8493 70.77 57 22,768 96 94 96 94 5/19/2014 24 4.8880 1 1.34 205.7 0.8641 71.64 1 60 22,988 96 93 97 94 5/20/2014 30 4.8880 1.30 162.9 0.8593 71.54 59 17,662 96 93 97 94 5/21/2014 39 4.8880 1.33 125.9 0.8608 71.43 60 13,965 96 93 97 94 5/22/2014 46 4.8880 1.40 105.8 0.8558 71.43 58 12,353 96 94 96 95 5/23/2014 29 4.8880 1.23 169.6 0.8444 71.54 54 17,398 94 96 96 94 5/24/2014 29 4.8880 1.26 168.2 0.8575 72.22 57 17,675 92 96 96 95 5/25/2014 27 4.8880 1.10 180.3 0.8620 72.73 57 16,541 96 96 96 94 5/26/2014 44 4.8880 1.40 111.4 0.8621 71.43 60 13,007 96 96 96 95 5/27/2014 54 4.8880 1.25 91.3 0.8338 72.80 47 9,518 96 96 96 96 5/28/2014 20 4.8880 1.12 242.1 0.8488 72.32 53 22,614 96 96 96 96 5/29/2014 26 4.8880 1.16 184.5 0.8596 72.41 57 17,849 98 99 97 96 5/30/2014 21 4.8880 1.21 1 228.4 1 0.8445 71.90 53 23,049 98 96 96 .95 5/31/2014 40 4.8880 1.16 123.E 0.8492 71.55 55 11,958 97 96 96 96 Total 1,089 151.6280 38.27 4,676.7 26.2577 2,214.81 1,695 419,23b 2,bll 2,y41 2,aab z,ysi Samples 31 31 31 31 31 31 31 31 30 31 31 31 Averaqe 35 4.8880 1.23 150.9 0.8470 71.45 55 15,459 96 95 96 95 Primary Digester Temperature monthly average is 95°F. * Data qualified by Lab. @ No Digester temperature due to maintenance on heat exchanger. 07/17/2014 09:09:55 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 06/01 /14 TO 06/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 6/1/2014 28 4.8880 1.14 172.9 0.8472 71.93 54 16,439 97 95 97 94 6/2/2014 29 4.8880 1.07 170.0 0.8474 73.83 49 15,170 97 95 97 94 6/3/2014 30 4.8880 1.08 162.3 0.8473 72.22 53 14,619 97 99 96 95 6/4/2014 27 4.8880 1.06 183.5 0.8471 72.64 52 16,222 98 97 97 96 6/5/2014 31 4.8880 1.18 159.7 0.8465 72.03 53 15,716 98 101 98 96 6/6/2014 104 4.8880 1.08 47.1 0.8463 72.22 53 4,242 97 96 97 96 6/7/2014 4.8880 0.0 0.8465 0 98 96 98 94 6/8/2014 4.8880 1.21* 0.0 0.8468 0 98 96 97 94 6/9/2014 283 % 4.8880 17.3 0.8473 72.73/, 52* 1,746 99 96 98 94 6/10/2014 4.8880 0.0 0,8470 0 98 97 98 96 6/11/2014 38 4.8880 1.71 129.9 0.8465 70.76 56 18,526 99 99 98 96 6/12/2014 19 4.8880 1 1.11 253.4 0.8470 72.07 53 23,458 99 1 96 98 96 6/13/2014 27 4.8880 1.11 181.2 0.8469 72.07 53 16,774 98 96 98 96 6/14/2014 34 4.8880 1.26 143.5 0.8488 72.22 54 15,080 98 96 97 96 6/15/2014 22 4.8880 1.49 227.0 0.8495 71.81 55 28,208 98 95 98 97 6/16/2014 36 4.8880 1.28 136.3 0.8498 73.44 51 14,550 98 96 97 97 6/17/2014 25 4.8880 1.21 196.2 0.8492 72.73 53 19,799 97 95 95 97 6/18/2014 30 4.8880 1 1.26 163.8 0.8488 73.81 50 17,213 99 96 97 97 6/19/2014 35 4.8880 1.34 139.3 0.8485 72.39 53 15,568 98 96 97 97 6/20/2014 28 4.8880 1.29 173.4 0.8482 72.09 54 18,655 98 97 97 96 6/21/2014 101 4.8880 1.17 48.2 0.8480 72.65 52 4,703 98 96 97 97 6/22/2014 25 4.8880 1.25 198.7 0.8484 72.80 52 20,714 98 97 97 97 6/23/2014 68 4.8880 1.06 71.8 0.8487 1 72.64 53 6,347 98 96 97 97 6/24/2014 38 4.8880 1 1.07 129.4 0.8485 73.83 50 11,547 99 97 98 97 6/25/2014 104 4.8880 1.11 47.1 0.8483 72.97 52 4,360 99 97 98 _ 97 6/26/2014 25 4.8880 1.44 193.9 0.8491 72.22 54 23,287 98 99 96 96 6/27/2014 29 4.8880 1.32 171.2 0.8491 74.24 49 18,847 97 95 96 97 6/28/2014 35 4.8880 1.20 139.3 0.8487 72.50 53 13,941 98 96 97 97 6/29/2014 66 4.8880 1.02 73.6 0.8489 73.53 1 51 6,261 99 97 97 97 6/30/2014 39 4.8880 1.07 124.2 1 0.8490 1 72.90 52 11,083 99 97 97 96 1888.56 _ 1363 '391.329 Tnfn1 1071 146640n 11.18 38547 2.94391 2.942 2.897 2.915 2.882 Samples 26 30 26 30 30 26 26 .29 Average 41 4.8880 1.21 128.5 0.8480 72.64 52 13,494 Primary Digester Temperature monthly average is 97°F. ;; Estimate. 30 30 30 30 98 97 97 96 08/12/2014 03:19:23 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 07/01/14 TO 07/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac '% 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 7/l/2014 27 4.8880 1.07 182.1 0.8494 73.83 50 16,250 99 97 98 97 7/2/2014 41 4.8880 1.06 119.3 0.8492 73.58 51 10,547 100 99 98 97 7/3/2014 35 4.8880 1.17 141.4 0.8490 71.79 55 13,798 100 98 99 97 7/4/2014 54 4.8880 1.02 89.7 0.8499 73.53 51 7,631 100 96 98 97 7/5/2014 1 45 4.8880 1.01 107.7 0.8507 73.27 52 9,072 99 96 98 _96 7/6/2014 92 _ 4.8880 1.18 53.1 0.8511 72.88 53 5,226 99 97 97 97 7/7/2014 25 4.8880 1.01 193.6 0.8514 73.27 52 16,308 99 _ 97 98 97 7/8/2014 _ 27 4.8880 _ 1.02 180.1 0.8509 51 15,321 99 98 98 96 _ 7/9/2014 48 4.8880 _ 1.24 101.2 0.8505 _73.53� 72.58 53 _10,466 99 97 97 97 7/10/2014 59 4.8880 1 1.20 83.4 0.8497 72.50 53 8,347 99 97 97 98 7/11/2014 32 4.8880 1.06 154.0 0.8499 72.64 53 13,614 98 96 97 97 7/12/2014 44 4.8880 1.10 112.1 _ 0.8501 72.73 53 10,284 98 96 97 97 7/13/2014 28 4.8880 1.22 175.3 0.8504 �2.13 54 17,836 99 97 _ 97 97 7/14/2014 39 4.8880 1.19 126.5 0.8507 72.27 54 12,555 99 98 98 97 7/15/2014 45 4.8880 1.33 109.6 0.8509 73.68 51 12,157 99 97 98 98 7/16/2014 51_ 4.8880 1.37 96.5 0.8507 72.99 53 11,026 99 97 98 97 7/17/2014 98 4.8880 1.81 50.1 0.8509 71.82 55 7,563 99 97 _ 98 97 7/18/2014 24 4.8880 1.36 203.1 0.8506 72.79 53 23,036 98 97 97 98 7/19/2014 29 4.8880 1.20 170.6 0.8511 73.33 52 17,074 99 97 97 97 7/20/2014 _ 42 4.8880 _ 1.46 116.8 0.8515 72.60 54 14,222 99 97 97 97 _ 7/21/2014 41 4.8880 1.44 118.3 0.8517 70.83 58 14,207 99 97 97 _97 7/22/2014 63 4.8880 1.05 77.3 0.8516 72.38 54 6,769 102 98 98 97 7/23/2014 27 4.8880 1.04 183.4 0.8516 73.08 53 15,907 100 99 98 97 7/24/2014 26 4.8880 1.06 185.6 0.8519 72.64 54 16,408 99 97-- 98 __ 98 7/25/2014 26 4.8880 1.34 186.6 0.8513 72.39 54 20,854 99 97 97 98 7/26/ 0014 33 4.8880 1.01 146.3 0.8512 73.27 52 12,323 100 98 97 98 7/27/2014 22 4.8880 1.02 223.6 0.8515 72.55 54 19,021 99 98 97 98 7/28/2014 27 4.8880 1.00 178.7 0.8515 73.00 53 14,904 99 99 _ 97 98 7/29/2014 48 4.8880 1.02 102.1 0.8514 73.53 52 8,685 99 98 97 --"E98 98 7/30/2014 37 4.8880 1.07 131.5 0.8517 73.83 51 11,735 98 96 97 7/31/2014 41 4.8880 1.09 119.4 0.8516 73.39 52 10,854 98 97 96 96 Total 1,275 151.5280 36.22 4,219.0 26.3756 2,268.66 1,640 404,000 3,072 3,015 3,021 3,014 Samples 31 31 31 31 31 j 31 31 31 31 31 31 31 Averaoe 41 4.8880 1.17 136.1 0.8508 12.86 53 13,032 99 97 _ 9797 r Pf,ffnccr q C�i'�est�f /Y1a.�f7�/y C7i/sr4 e = q 7 F 09/16/2014 10:24:01 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 08/01/14 TO 08/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 8/1/2014 34 4.8880 1.18 142.5 0.8517 73.73 51 14,024 99 96 97 96 8/2/2014 24 4.8880 1.21 202.3 0.8521 74.38 50 20,415 98 95 96 97 8/3/2014 45 4.8880 1.06 107.8 0.8522 73.58 52 9,530 98 95 96 94 8/4/2014 25 4.8880 1.04 197.7 0.8525 74.04 51 17,148 98 96 96 97 8/5/2014 32 4.8880 1.11 154.4 0.8525 72.97 53 14,293 97 95 95 96 8/6/2014 1 27 4.8880 1.31 178.5 0:8528 74.05 51 19,502 98 97 95 97 8/7l2014 58 4.8880 1 1.05 84.9 0.8533 73.33 53 7,435 98 98 97 97 8/8/2014 25 4.8880 1.13 193.2 0.8539 74.34 50 18,208 98 96 95 97 8/9/2014 27 4.8880 1.31 178.3 0.8551 74.81 50 19,480 98 95 95 97 8/10/2014 29 4.8880 1.15 165.7 0.8559 73.04 54 15,892 97 96 95 96 8/11/2014 24 4.8880 1.24 204.8 0.8564 73.39 54 21,180 97 96 95 95 8/12/2014 31 4.8880 1.23 160.2 0.8563 73.98 52 16,434 97 96 95 96 8/13/2014 24 4.8880 1.05 207.2 0.8566 75.24 49 18,145 97 96 95 96 8/14/2014 29 4.8880 1.10 169.9 0.8571 73.64 53 15,587 97 95 94 95 8/15/2014 27 4.8880 1.18 181.9 0.8581 73.73 54 17,901 97 95 94 83 8/16/2014 38 4.8880 1.05 128.7 0.8596 73.33 55 11,270 98 96 94 93 8/17l2014 45 4.8880 1.34 108.7 0.8606 72.39 58 12,148 96 96 94 95 8/18/2014 33 4.8880 1.26 149.1 0.8610 73.81 54 15,668 97 96 94 94 8/19/2014 43 4.8880 1.33 113.4 0.8606 73.68 55 12,579 97 97 95 96 8/20/2014 32 4.8880 1.04 153.1 0.8603 74.04 54 13,279 97 97 94 96 8/21/2014 23 4.8880 1.33 212A 0.8610 72.93 57 23,560 97 97 95 97 8/22/2014 35 4.8880 0.96 140.2 0.8613 72.92 57 11,225 97 97 95 95 8/23/2014 32 4.8880 1.16 152.E 68617 74.14 54 14,763 97 97 95 96 8/24/2014 42 4.8880 1.03 116.4 0.8631 73.79 55 9,999 97 97 95 96 8/25/2014 59 4.8880 1.01 82.4 0.8638 74.26 55 6,941 97 97 95 96 8/26/2014 33 4.8880 1.02 147.9 0.8640 73.53 56 12,582 97 97 94 95 8/27/2014 26 4.8880 1.00 191.3 0.8647. 73.00 58 15,954 97 96 95 96 8/28/2014 96 4.8880 1.13 50.9 0.8652 74.34 55 4,797 97 96 95 95 8/29/2014 40 4.8880 1.45 122.5 0.8654 72.41 59 14,814 97 96 96 95 8/30/2014 28 4.8880 1.12 173.6 0.8657 73.21 58 16,216 96 96 95 95 8/31/2014 30 4.8880 1.49 162.9 0.8664 73.15 58 20,243 97 96 n n04 96 n nA7 96 O ORS iota) l,Uvb IOI.ozou 00.U/ 9,/JO.4 GV.vcuu •- - - E- - - Samples 31 31 31 31 31 31 31 31 31 31 31 31 Averaqe 35 4.8880 1.16 152.8 0.8587 73.65 54 14,878 97 96 95 96 / c, DjGtsje2 %+°MpPr4 urn/ 10/15/2014 05:23:50 PM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 09/01/14 TO 09/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 9/l/2014 28 4.8880 1.13 176.9 0.8671 74.34 56 16,671 97 96 96 96 9/2/2014 48 4.8880 1.10 101.4 0.8676 72.73 59 9,302 97 97 95 96 9/3/2014 45 4.8880 1.27 109.3 0.8677 73.23 58 11,577 97 97 96 96 9/4/2014 27 4.8880 1.18 180.4 0.8679 72.88 59 17,754 97 96 95 96 9/5/2014 34 4.8880 1.01 144.1 0.8674 74.26 56 12,138 97 96 95 96 9/6/2014 64 4.8880 1.56 76.9 0.8671 75.00 54 10,005 97 96 95 96 9/7/2014 25 4.8880 1.36 193.2 0.8672 72.79 59 21,914 97 96 95 95 9/8/2014 27 4.8880 1.36 181.6 0.8673 72.79 59 20,598 96 95 95 95 9/9/2014 64 4.8880 0.92 75.9 0.8671 73.91 57 5,824 96 95 95 95 9/10/2014 38 4.8880 0.95 129.8 0.8669 73.68 57 10,284 97 96 95 96 9/11/2014 33 4.8880 1.33 150.0 0.8672 72.93 59 16,638 97 1 96 95 1 96 9/12/2014 47 4.8880 1.18 103.6 0.8670 72.88 59 10,195 97 96 94 96 9/13/2014 28 4.8880 1.11 176.3 0.8670 72.97 59 16,321 97 95 95 95 9/14/2014 32 4.8880 1.28 150.9 0.8668 73.44 57 16,109 94 95 94 95 9/15/2014 22 4.8880 1.12 219.2 0.8663 73.21 58 20,475 97 94 94 95 9/16/2014 31 4.8880 0.95 159.7 0.8660 73.68 57 12,653 96 95 94 95 9/17/2014 18 4.8880 0.94 268.9 0.8652 73.40 57 21,081 95 1 94 94 95 9/18/2014 23 4.8880 0.96 209.9 0.8647 73.96 56 16,805 96 95 94 95 9/19/2014 26 4.8880 0.99 1 190.4 0.8642 72.73 58 15,721 95 94 1 94 95 9/20/2014 25 4.8880 0.87 199.3 0.8635 72.41 59 14,461 96 95 95 95 9/21/2014 26 4.8880 1.09 191.4 0.8628 72.48 58 17,399 95 93 94 95 9/22/2014 26 4.8880 1.00 186.1 0.8619 73.00 57 15,521 96 94 95 95 9/23/2014 26 4.8880 0.67 188.7 _ 0.8609 71.64 59 10,544 95 94 94 95 9/24/2014 28 4.8880 0.74 176.1 0.8600 72.97 56 10,868 95 94 94 94 9/25/2014 50 4.8880 1.27 98.4 0.8598 72.44 57 10,422 95 93 94 94 9/26/2014 31 4.8880 1.40 158.9 0.8592 1 72.14 58 18,553 95 93 94 94 9/27/2014 25 4.8880 1.07 192.6 0.8589 1 72.90 56 17,187 95 93 94 94 9/28/2014 31 4.8880 0.98 160.2 0.8588 73.47 54 13,093 95 93 93 93 9/29/2014 41 4.8880 1.03 119.1 0.8585 73.79 54 10,231 94 93 94 94 9/30/2014 27 4.8880 1.31 178.0 0.8578 73.28 55 19,447 94 92 93 94 Total 994 146.640 33.13 4,841.2 2b.929b 2,1Vb.3b I,n4 43y,/y"I 4,0f1 L,041 L,6J4 4,0DI Samples 30 30 30 30 30 30 30 30 30 30 30 30 Averaae 33 4.8880 1.10 161.6 0.8643 73.18 57 14,660 96 95 94 95 11/24/2014 11:16:28 AM LAND APPLIED BIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO060342 10/01 /14 TO 10/31/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed Vb1Fr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 10/1/2014 30 4.8880 1.14 164.8 0.8575 0.8571 0.8561 73.68 53 15,669 93 93 94 93 10/2/2014 25 * 4.8880 0.95 192.1 72.63* 56 15,220 94 92 93 93 10/3/2014 37 4.8880 0.98 131.5 73.47 53 10,748 94 92 95 94 10/4/2014 23 4.8880 1.60 209.8 0.8560 71.88 57 27,996 95 92 94 94 10/5/2014 24 4.8880 1.19 206.5 0.8567 73.95 53 20,494 94 95 94 93 10/6/2014 1 19 4.8880 1.17 252.8 0.8576 72.65 56 24,668 93 95 93 94 10/7/2014 28 4.8880 1.23 175.1 0.8574 72.36 56 17,962 94 92 92 94 10/8/2014 35 4.8880 0.88 140.5 0,8575 72.73 56 10,312 95 93 94 94 10/9/2014 145 4.8880 0.91 33.6 0.8576 72.53 56 2,550 95 93 94 94 10/10/2014 62 4.8880 0.87 78.6 0.8576 73.56 54 5,703 95 94 93 1 94 10/11/2014 27 4.8880 1.20 184.1 0.8574 73.33 54 18,425 95 98 94 93 TOM -2/20141 28 4.8880 1.38 174.2 0.8576 71.74 58 20,049 95 92 93 93 10/13/2014 77 4.8880 1.48 63.1 0.8578 73.65 54 7,789 95 92 93 93 10/14/2014 28 4.8880 1.14 176.4 0.8581 73.68 54 16,771 95 92 94 93 10/15/2014 41 4.8880 0.80 119.7 0.8580 72.50 56 7,986 96 94 94 94 10/16/2014 26 4.8880 1 1.07 186.3 0.8578 72.90 55 16,625 96 93 94 93 10/17/2014 109 4.8880 1.56 44.9 0.8583 73.72 54 5,842 96 92 94 93 10/18/2014 39 4.8880 0.90 124.4 0.8600 72.22 58 9,337 95 92 94 93 10/19/2014 20 4.8880 1.09 245.1 0.8613 77.06 46 22,281 96 94 94 91 10/20/2014 149 4.8880 0.90 32.7 0.8618 73.33 56 2,454, 96 92 94 91 10/21/2014 27 4.8880 0.91 180.2 0.8633 72.53 58 13,676 96 93 94 92 10/22/2014 84 4.8880 0.89 58.0 0.8649 1 71.91 60 4,305 96 93 94 91 10/23/2014 96 4.8880 0.88 50.9 0.8660 72.73 59 3,736 96 93 94 _ 91 10/24/2014 34 4.8880 1.09 141.8 0.8671 71.56 61 12,890 96 92 93 90�� 10/25/2014 47 4.8880 0.65 104.4 0.8675 70.77 63 5,660 _ 97 96 94 87 10/26/2014 4.8880 0.0 0.8685 0 96 93 94 91 10/27/2014 50 4.8880 0.73 97.9 0.8697 69.86 65 5,960 96 92 94 89 10/28/2014 39 4.8880 0.92 125.2 0.8710 71.74 62 9,606 96 92 _ 94 90 10/29/2014 38 4.8880 1.02 127.2 0.8726 71.57 63 10;821 96 93 94 88 10/30/2014 4.8880 0.0 0.8742 0 97 1 93 94 91 10/31 /2014 16 4.8880 0.84 302.5 0.8740 71.43 64 21,192 97 1 94 95 91 Total 1,406 151.5280 30.37 4,124.3 26.7179 2,107.67 1,651 366,727 2,956 2,886 2,908 2,855 Samples 29 31 29 31 31 29 29 31 31 31 31 31 Average 48 4.8880 1.05 133.0 0.8619 72.68 57 11,830 95 93 94 92 Primary Digester Temperature monthly average is 94°F. * Data qualified. 12/11/2014 12:19:33 PM LAND APPLIED SIOSOLIDS Page 4 MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 11101/14 TO 11/30/14 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VolFr 30 day Mavg 921 DTrVoFrac %, 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 11/1/2014 83 4.8880 1.40 58.7 0.8732 71.43 64 6,854 98 93 95 92 11/2/2014 11/3/2014 11/4/2014 11/5/2014 11/6/2014 11 /7/2014 11/8/2014 11/9/2014 11 /10/2014 11 /11 /2014 22 98 130 32 29 75 40 40 35 30 41 49 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 4.8880 1.25 1.78 2.12 1.66 1.11 2.22 1.08 0.95 0.90 0.97 1.66 1.09 0.97 1.06 1.05 1.05 0.92 0.91 219.8 0.0 50.0 37.7 150.5 0.0 169.8 65.3 121.7 122.0 140.2 162.2 120.1 99.5 198.2 290.5 227.3 282.2 218.5 118.0 203.1 55.3 207.6 191.1 176.6 178.4 182.1 221.1 115.7 0.8748 6.8762 0.8755 0.8759 0.8758 0:8753 0.8751 0.8754 0.8759* 0.8759 %; 0.8749 0.8724 0.8704 0.8685 0.8674 0.8658 0.8652 0.8647 0.8637 0.8622 0.8613 0.8607 0.8601 0.8592 6.85 55 0.8563 0,8548 0.8535 0.8539 72.00 72.47 71.70 70.48 71.17 70.27 72.22 72.63 %; 72.22' 71.13 71.08 72.48 72.16 73.58 73.33 74.29 72.83 73.63 73.08 73.27 74.51 73.15 72.50 74.49 73.20 73.53 73.33 63 63 64 66 65 66 63* 62 ` 63 64 63 60 60 57 57 55 '58 55 56 56 52 55 56 51 54 52 53 22,914 0 7,423 6,666 20,836 0 15,71.9 12,090 10,962 9,666 10,523 13,122 16,627 9,045 16,034 25,681 19,905 24,712 16,765 8,955 17,616 4,658 17,660 17,213 17,674 14,581 14,732 18,809 10,132 97 97 98 98 98 98 97 97 97 98 98 97 97 96 95 95 95 95 95 95 96 96 97 97 97 96 96 95 96 94 93 94 94 95 95 94 95 95 94 95 95 95 95 94 93 93 92 92 93 92 93 94 95 95 94 93 93 93 96 94 94 94 95 96 95 96 96 98 98 98 97 96 96 95 95 95 95 95 95 95 96 97 96 96 96 95 96 91 91 88 90 86 87 92 93 92 88 93 90 92 90 87 89 93 90 94 89 92 92 90 91 94 93 94 91 94 11/12/2014 11 /13/2014 11/14/2014 11/15/2014 11/16/2014 25 11/17/2014 17 4.8880 4.8880 4.8880 11 8/8/2014 22 11/19/ 0014 17 11/20/2014 22 4.8880 11 /21 /2014 41 4.8880 11/22/2014 24 4:8880 1.04 11/23/2014 88 4.8880 1.01 11/24/2014 24 4.8880 1.02 11/25/2014 26 4.8880 1.08 11/26/2014 28 4.8880 1.20 11/27/2014 27 4.8880 0.98 0.97 1.02 1.05 11/28/2014 27 4.8880 11/29/2014 22 4.8880 11/30/2014 42 4.8880 Alt ��Q7 1 RR7 22 1 F�nl nn7 r7:i 9 AW 2.815 2.871 2,728 Total 1,156 146.6400 33.52 a,�tss.z ` • `- -- ' - - -- Samples 28 30 28 30 28 _ 26 26 30 30 30 30 30 Average 41 4.8880 1.20 146.1 0.8668 72.59 59 13,586 97 94 96 91 - Estimates. Primary Digester Temperature monthly average is 95°F. 01/14/2015 03:38:45 PM LAND APPLIED BIOSOLIDS MUDDY CREEK WASTEWATER TREATMENT PLANT Permit No. NCO050342 12/01/14 TO 12/31/14 Page 4 Date PriDig SRT Days %TS 163 PriDig VOL MG 492 Trans %TS % 93 PrTranFlo TGD 357 Feed VblFr 30 day Mavg 921 DTrVoFrac % 422 PriDig %VSR % 920 Transfer lb %TS lb %TS 741 Dig #1 Temp Deg F 775 Dig #2 Temp Deg F 776 Dig #3 Temp Deg F 777 Dig #4 Temp Deg F 778 12/1/2014 26 4.8880 1.01 185.5 0.8546 73.27 53 15,625 96 94 96 94 12/2/2014 25 4.8880 1.07 197.2 0.8533 72.90 54 17,598 96 94 96 93 12/3/2014 43 4.8880 0.94 112.8 0.8516 74.47 49 8,843 96 94 96 96 12/4/2014 4.8880 0.0 0.8515 0 96 95 96 93 12/5/2014 29 4.8880 1.60 170.5_ 0.8503_ 52 14,220 97 95 96 93 12/6/2014 40 4.8880 _ _1 . 0 5 ^ _122.9 _ 0.8503 _73.00 73.33 _ 10,762 97 95 97 _ 92 12/7/2014 41 _4.8880 1.04 118.5 0.8509 73.08 _52 52 10,278 97 95 97 ~ 92 12/8l2014 _26 _ 4.8880 1.10 190.4 0.8514 73.64 51 17,467 97 95 96 92 12/9/2014 24 4.8880 1.18 203.9 0.8514 74.58 _ 49 20,066 _ 94 96 93 12/10/2014 28 4.8880 1.01 ^ 172.4 0.8514 _ 74.26 _ 50 _ 14,522 _97 97 94 96__ 9_4_ 12/11 /2014 28 4.8880 1.04 174.8 0.8519 _ 73.08 53 15,161 97 94 96 94 12/12/2014 36 4.8880 1.02 135.0 0.8529 74.51 50 11,484_ _ 93 _ 96 94 12/13/2014 25 4.8880 0.99 194.8 0.8556 T 72.73 _ 55 16,084 _97 97 94 93 12/14/2014 4.8880 0.0 0.8581 0 97 95 _97 -97 _ 94 12/15/2014 35 4.8880 0.96 140.2 _ 0.8600 72.92 56 11,225 97 95 97 93 12/16/2014 133 4.8880 0.90 36.7 0.8617T 73.33 56 2,755 97 95 97 94 12/17/2014 43 4.8880 0.96 114.2 0.8632 72.92 57 97 _ 95 97 94 12/18/2014 31 4.8880 1.00 ^ 159.9 0.8637 72.00 59 _9,143 13,336 97 95 97 93_ 12/19/2014 44 4.8880 689 110.2 0.8638 73.03 57 8,180 97 95 96 93 12/20/2014 86 4.8880 1.04 57.0 0.8639 73.08 57 4,944_ ^ 97 95 96 93 12/21/2014 43 4.8880 1.12 114.4 _ 0,8646 74.11 55 10,686 97 95 _ 96 92 12/22/2014 32 4.8880 1.04 1.03 -1.02 15_5.0 0.8652 _ 74.04 56 13,444 97 95_ 96 92 12/23l2014 112..,Y! 4.8880 43.8 0.8654-.iK- 73.79 56 3,763 97 9_6_ _ 92 12/24/2014 38 4.8880 128.1 0.8658 72.55 59 10,897 �97 _94 94 96 92 12/25/2014 47 4.8880 1.91 103.0 0.8658 71.73 61 16,407 97 94 _ 94 12/26/2014 86 4.8880 _1.00 _ 57.1 0.8679 73.00 59 97 94 _96 96 93 12/27/2014 34 4.8880 1.25 141.9 0.8682 72.00 61 _4,762 14,793 97 93 96 94 12/28/2014 33 4.8880 1.49 147.8 0.8686 72.48 _ 60 18,367 97 96 98 91 12/29/2014 26 4.8880 1.66 T 189.1 _ 0.8686 62 26,180 98 95 98 93 12/30/2014 25 4.8880 1.23 198.5 0.8686 _71.69 71.54 62 20,363 98 96 98 92 12/31/2014 43 4.8880 1.03 114.3 0.8693 71.84 62 9,819 98 95 98 94 IOtal ;l 7 -1 Samples g Average 151.5Z8U 31 4.8880 Tr- E5f;1vafe- 50.75 3,989.9 a5 r-Sy �,D�lSAB b553- 371,174 3,006 2,932 2,992 2,886 30 _ 019 ab T 31 31 31 31 31 1.10 _ 128.7 � - SS45 _ 73 •Q 11_ ` 56 11,973 97 95 97 93 PHVIOr4 J)Cesler e-mPer-a�ure- MorVAN average- iS 96,r'• City of Winston-Salem 2014 Class B Biosolids Monitoring. Report Section 11. City of Winston-Salem Class B cover letter; DENR FORM ACF Winston-Salem a Forsyth County C /CountyI�ties Water t Sewer, Solid Waste Disposal Manson Meads Complex City of Winston-Salem 27 99 Griffith Road Winsmn-Salem, NC 27103 CityLink 311 (336.727.8000) Fax 336.659.4320 mm dipfms org February 6, 2015 NC Department of Environment & Natural Resources Division of Water Resources Aquifer Protection Section Land Application Unit 1636 Mail Service Center Raleigh, NC 27699-1636 Please find attached the Annual Land Application Certification Form (DENR FORM ACF) for 2014 for the Winston-Salem/Forsyth County Utilities Commission Class B Biosolids program. The Utilities Commission oversees two Wastewater Treatment Plants (WWTPs), the Archie Elledge WWTP (NPDES # NC0037834) and the Muddy Creek WWTP (NPDES # NC0050342). Although the NCDWQ Non -Discharge Permit WQ0000094 covers the land application of the Class B Biosolids from these two plants, there was no Class B land application during 2014. Stabilized Digested Sludges from the two WWTPs were blended in the Blending Tanks at the Archie Elledge WWTP before being dewatered to produce a Class A dried pelletized product. Pathogen and Vector Attraction Reduction Certifications (FORM RF) and operational data for both WWTPs have been included in the City's annual monitoring report for Class A Biosolids,-since those documents support compliance requirements for a Class A product. Various Class B Biosolids products were analyzed for TCLP parameters, but since there was no land application of Class B Biosolids during 2014, the TCLP information is not included here. It is available for review if so desired. If you should need further information, please call me at (336)397-7662 or you may call Ron Hargrove at (336)397-7312. Sincerely, ,&Z?-� or. OT Bruce M. Casey Utility Plant Supervisor (Biosolids) City Coonal: Mawr Allen Joines; Vivian H. Burke, Mayor Pm Tempore, Northeast Ward; Denise D. Adams, Narth Ward; Dan Besse, Sou hwsar Ward; Robert C. Clark, Wcsr Ward; Molly l.xighr, South Wand; Jeff Macintosh, Northwest Ward; Derwin 'L Montgomery, Past Ward; JamcsTaylor, r., Southeast Ward; City Manager: Lee D. Garrity Forsyth Conmy Commlssimu= David R. Plyle. , Chairman; Don Martin, V foe Chair; Ted Kaplan; Richard V. I.invillr, Walter Marshall; Gloria D. Whisenhum; Everette Witherspoon; Call311 or336-727-8000 eotmyManagerDudley warns']` Cl}��li nk CI Of1NS.Or City/County Utility Comm;ss on Daaid Neill, Chairman;" Randall S. Tunic, Vice -chair, Wesley Curtis, Jc; Harold E Day, Tom Griffin; Harold R. Holmes: Charles D. Jewell,11; `Y 9 Paul S. McGill; Chris faker; Al H. Seymour, J. Hill'Smckton January 7, 2013 �instonsaiem Mr. Charles Wakild Office of the Director of Water Quality Division city Manager NCDENR-DWQ' Oro, y M. Turner, P.E. 1.636 Mail Service Center Akststaat Gry Ma.mayu Raleigh, NC 27699-1636 OLY or\Vinton-Salem 'P.O.. Box 251 t Subject: Dele ation of Signature Authori ,, stop -Salem, NC 27102 - g Tel 336.747.486E Winton—aSalemi Forsyth County Utility, Coif mission lQax 336.748.3060 ' g-vo<inwhvi-ort Dear Mr. Wakild: wtt"tt�,yajt�r.•>g By notice of this letter, I hereby delegate signatory authority to the position of Utilities Director for the City of Winston Salem as the Owners Representative for all permit applications.' discharge monitoring reports, and other information relating to the Commissions Facilities listed below as required by all applicable federal, state, and local environmental agencies .specifically with the requirements for signatory authority as specified in 15A NCAC 2B.0506. NPDES PERMITS NCO037834 City of WS Archie Elled a WWTP NCO050342 City of WS Muddy Creek WWTP NC0079821 'City of WS Thomas WTP NCO086011 City of WS Neilson WTP NCO086762 I City of WS Swann WTP LAND APPLICATION / DISTRIBUTION PERMITS WQ0000094 City of WS Residuals Program WQ0029804 City of WS Thermal Biosolids Facility WQ0031314 City of WS Swann WTP If you have any questions, please feel free to contact Ron Hargrove (Acting Utilities Director) at (336) 747-73.12. Sin4gory. e_urner, PE Assistant City Manager cc: Winston-Salem'Regional Office Chy COMA Mayor Allen Joiner: Vivian H. Burke. Mayor l'ro'I'cmpom,,\orthrast Wand; Denise D. Adams, worth Want; Dan Bcue, Seuthwat Wand; Rohcrt d Clark. War Ward; Molly Wot. South Ward: Wanda Merxhel. Northmn Ward: llcnvin L Montgomery„Ean Ward; James'tayhx. Jr., Southeut Ward; Gry Manager. l.ee U. Garrity 'Cali 3`11. or 336=729=8000 citvlink@.citvofws:org ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0000094 County: Forsyth Year: 2014 Facility Name (as shown on permit): City of Winston-Salem Residuals Land Application Program Land Application Operator: Bruce M. Casey Phone: 336-397-7662 Land application of residual solids as allowed by the permit occurred during the past calendar year? ❑ Yes 0 No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Part B: Facility was compliant during calendar year with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Resources:❑ Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1.Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). r `'8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for k='violations." Ron Hargrove, Utilities Director Permittee Name and Title (type or print) ignature f Permittee Date Signature of Preparer* (if different from Permittee) * Preparer is defined in 40 CFR Part 503.9 (r) Date Signature of Land Applier Date (if different from Permittee and Preparer) DENR FORM ACF (5/2003)