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HomeMy WebLinkAboutWQ0028547_Residual Annual Report 2014_2015030651�11001- MAR 0 6 2015 DWR SECTION INFORMATION PROCESSING UNIT TOWN OF YANCEYVILLE 2014 ANNUAL LAND APPLICATION OF RESIDUAL BIO-SOLIDS REPORT CLASS B PROGRAM WQ0028547 Submitted by: Soil Plus 208 Williams Street Greenville, North Carolina 27858 February 25, 2015 sC')' .1?C -tk -S February 25, 2015 NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Re: 2014LAND APPLICATION ANNUAL REPORT Town of Yanceyville "Class B" Program NC Permit No.: WQ0028547 Soil Plus Project No. 201205.A10 Information Processing Unit: Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as specified in the above referenced permit for the Town of Yanceyville on behalf of Granville Farms, Inc. Soil Plus compiled this report using data gathered during the compliance year. This data includes (1) certification form, (2)' residual sampling, (3) field loading calculations, (4) pathogen and vector attraction reduction documentation, (5) standard soil fertility nutrient analysis. The Town of Yanceyville conducted application events on permitted fields in Caswell County during 2014. A total of 97.14 Dry Tons or 520,000 gallons from the Town's Water Treatment Plant and 30.64 Dry Tons or 227,500 gallons from the Town Wastewater Treatment Plant of permitted residual bio-solids were land applied to permitted fields. If there is any further information required or questions regarding this annual report please do not hesitate to contact me or the Town of Yanceyville (336) 694-1335 for further assistance. Respectfully, C. Scott Carpenter, L.S.S. North Carolina Nutrient Management Planner Brian Merritt, Envirolink, Inc. Jason Smith, Granville Farms 208 Williams Street Greenville, NC 27858 t (252) 917-4288 f (800) 755-7153 www.soilplus.net Town of Yanceyville 2014 Annual Land Application of Residual Bio-Solids Report WQ0028547 Yanceyville, NC I ANNUAL LAND APPLICATION CERTIFICATION FORM Field Loading & Source Summary ANNUAL RESIDUAL SAMPLING SUMMARY FORM Annual Analytical Data FIELD LOADING SUMMARY FORM NC-CS-81 ANNUAL PATHOGEN & VECTOR A'I"TRACTION REDUCTION FORM 4 Fecal Coliform Data 30-Day Scale Bench Test SOIL SAMPLES NC-CS-81 © Copyright APPENDIX I CERTIFICATION FORM SUMMARY FORM D Source Summary Report MI YanceyviHe VVIP 520,000 97.14 YanceyviHe VVVVTP 227,500 30.64 Total 747,500 127.79 Wednesday, February 25, 2015 Page 1 of 1 YEAR TO DATE FIELD LOADING SUMMARY CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES Acres Volume Crop 1 PAN Crop 2 PAN Crop 1 PAN 1 Crop 2 PAN 2 Field Used Applied Total DT lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used Site# NC-CS-81 4 11.97 58,500 10.93 5.71 Fescue Pasture 112 5.1% 5 15.43 240,500 44.93 18.20 Fescue Pasture 250 7.3% 6 5.77 45,500 8.50 9.21 Fescue Pasture 250 3.7% 7 15.73 227,500 30.64 62.98 Fescue Pasture 250 25.2% 8 8.38 175,500 32.79 24.45 Fescue Pasture 169 14.5% Total 747,500 Wednesday, February 25, 2015 Page 1 of 1 APPENDIX II RESIDUAL SAMPLING SUMMARY FORM FIELD LOADING CALCULATIONS ANALYTICAL &,- AGMAN FIELD LOADING ESTIMATES Facility Yanceyville WI P Sampling Date 6/19/2014 % Solids 4.48 Mineralization Rate 0.40 Gallons per DT 5,352.86 pH 6.81 Sodium Absorpotion 0.41 <5.0 Safe 5.0 -10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION NUTRIENT APPLICATION TKN (mg/Kg) 7,590 lbs./1,000 gal 2.84 Potassium lbs./1,000 gal 0.34 Ammonia Nitrogen (mg/Kg) 446.00 lbs./1,000 gal 0.17 Phosphorus lbs./1,000 gal 0.56 Nitrate -Nitrite (mg/Kg) 44.64 lbs./1,000 gal 0.02 Calcium lbs./1,000 gal 0.68 PLANT AVAILABLE NITROGEN SURFACE APPLIED Calcium lbs./1,000 gal 0.55 PAN (mg/Kg) 3,125 lbs./1,000 gal 1.17 Manganese lbs./1,000 gal 0.72 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal 3.33 PAN (mg/Kg) 3,348 lbs./1,000 gal 1.25 Molybdenum lbs./1,000 gal 0.00 j Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) HEAVY METAL CONCENTRATION HEAVY METAL LOADING 41 75 Arsenic (mg/Kg) 6.00 Arsenic lbs./1,000 gal 0.00 39 85 Cadmium (mg/Kg) 2.00 Cadmium lbs./1,000 gal 0.00 1,500 4,300 Copper (mg/Kg) 41.00 Copper lbs./1,000 gal 0.02 300 840 Lead (mg/Kg) 24.00 Lead lbs./1,000 gal 0.01 17 57 Mercury (mg/Kg) 0.40 Mercury lbs./1,000 gal 0.00 420 420 Nickel (mg/Kg) 24.00 Nickel lbs./1,000 gal 0.01 100 100 Selenium (mg/Kg) 5.00 Selenium lbs./1,000 gal 0.00 2,800 7,500 Zinc (mg/Kg) 65.00 Zinc lbs./1,000 gal 0.02 RESIDUAL NITROGEN CALCULATION Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen TBN (mg/kg) (lbs/DT) (mg/Kg) PAN PAN Nitrogen Tffiv (mg/kg) (lbs/DT) (mg/Hg) Equations 1 st Year 7,590 3,125 6.25 4,465 7,590 3,348 6.70 4,242 1 st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Year 4,465 893 1.79 3,572 4,242 848 1.70 3,393 2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x W/2) I 3rd Year 3,572 357 0.71 3,215 3,393 339 0.68 3,054 3rd Yr PAN (mg/Kg) = 3rd Yr. TKN x (MR/4) 4th Year I 3,215 161 0.32 3,054 3,054 153 0.31 2,901 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Year 3,054 76 0.15 Z978 2,901 730.15 Z829 5th Yr PAN (mg/Kg)= 5th Yr. TKN x W116) total 4,612 9.22 Total 4,761 9.52 Page: i of 2 Report Number: 14-171-0202 v A &L Eastern Laboratories, Inc. Account Number: 04596 � � 7621 Whitepine Road Richmond, Virginia 2323T (804) 743-9401 'Fax (804) 271.6446 Submitted By: SCOTT CARPENTER wwwaleastem.com Send To: SOIL PLUS, LLC Project: YANCEYVILLE WTP SCOTT CARPENTER NC CERT#257 P.O. BOX 1396 OXFORD, NC 27565 REPORT OF ANALYSIS Date Sampled: 6/19/2014 12:30:00 Lab Number: 56032 Date Received: 06/20/2014 00:00 Sample Id : YWTP 061914 Date Reported: 06/26/2014 Total Solids * 4.48 44800 100.0 JM Moisture * 95.52 100.0 JM Total Kjeldahl Nitrogen 0.76 7590 10.0 JM Total Phosphorus 0.15 1510 100 KM Total Potassium 0.09 908 100 KM Total Sulfur 0.89 8910 100 KM Total Calcium 0.18 1810 100 KM Total Magnesium 0.15 1470 100 KM Total Sodium 0.05 465 100 KM Total Iron 33400 100 KM Total Aluminum 158000 100 KM Total Manganese 1940 5 KM Total Copper 41 5 KM Total Zinc 65 5 KM Ammonia Nitrogen 0.04 446 10.0 JM Organic N 0.72 7144 10.0 Nitrate+Nitrite-N <2.00 2.00 JM Total Cadmium <2.0 2.0 KM All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis 06/20/2014 13:34 06/20/2014 13:34 06/23/2014 08:50 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 10:20 06/23/2014 08:50 06/23/2014 08:50 06/23/2014 08:40 06/23/2014 10:20 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SM-254OG SM-254OG SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NH3C CALCULATION SM-450ONO3F SW 6010C Page: 2 of 2 Report Number: 14-171-0202 Account Number: 04596 Submitted By: SCOTT CARPENTER Send To: SOIL PLUS, LLC SCOTT CARPENTER P.O. BOX 1396 OXFORD, NC 27565 Lab Number: 56032 Sample Id: YWTP 061914 L A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237' (804) 743-9401 Fax (804) 2714446 wwwaleastern.com Project: YANCEYVILLE WTP NC CERT#257 REPORT OF ANALYSIS Total Chromium 92 5 KM Total Nickel 24 5 KM Total Lead 12 5 KM Total Arsenic 6.0 3.0 KM Total Mercury <0.4 0.4 KM Total Selenium <5.0 5.0 KM pH (Standard Units) ` 6.81 2.00 JM Total Molybdenum <5 5 KM Soluble Phosphorus <0.01 <100 100 JM Comments: WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. Date Sampled: 6/19/2014 12:30:00 Date Received: 06/20/2014 00:00 Date Reported: 06/26/2014 06/23/2014 10:20 SW 6010C 06/23/2014 10:20 SW 6010C 06/23/2014 10:20 SW 6010C 06/23/2014 10:20 SW 6010C 06/24/201412:00 SW-7471B 06/23/2014 10:20 SW 6010C 06/23/2014 08:50 SW-9045D 06/23/2014 1020 SW 6010C 06/24/2014 10:59 SOLUBLE P IN MANURE All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.-� Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt CERTIFICATE OF ANALYSIS SCOTT CARPENTER SOIL PLUS 208 WILLIAMS ST GREENVILLE NC 27858 USA SIDN Client Marks AA51757 Yanceyville WTP 061914 AA51757 Yanceyville WTP 061914 AA51757 Yanceyville WTP 061914 AA51757 Yanceyville WTP 061914 AA51757 Yanceyville WTP 061914 Comments: Microbac Laboratories, Inc. - Wilson Division 3809 Airport Drive NW Wilson, NC 27896 Tel: (252) 237-4175 Report Date: 2014/07/07 Quote: 23-20140328-14 Work Order: 2014-06-19-022 Matrix: WW Collection Date: 2014106/19 Sample Submission Date: 2014/06/19 Analysis Name Method Flash Point - LiquidsSubcontracted pH (Corrosivity) Subcontracted Reactive Cyanide Subcontracted Reactive Sulfide Subcontracted TCLP Full Metals V(Subcontracted Approved by: Kim Hesse Result Unit *See Attached *See Attached *See Attached *See Attached *See Attached For any feedback concerning our services, please contact James Nokes, Senior Vice President, at james.nokes@microbac.com or Trevor Boyce at president@microbac.com Environmental ® Agrochemical 9 Food s Pharmaceuticals Page 1 of 1 N: L14061480 k: 2041.016 ie: Wilson NC M EmllyYoak Certificate of Analvsis Analyte CAS # Result Qual RL MDL Reactivity, cyanide 57-12-5 U 9.98 9.98 U I Not detected at or above adjusted sample detection Gmit Analyte CAS # Result Qual R! MDL Reactivity, Sulfide 18496-25-8 U 100 10o U Not detected at or above adjusted sample detection limit Analyte CAS # -- Result Qual RL MDL Corrosivity pH 10-29-7 6.60 0.000 0.000 Temperature At Determination (C) 16.9 0.000 0.000 Analyte CAS # Result Qual RL MDL ' Ignitability I 65.0 > 0.000 0.000 I> I Result is greater than the associated numerical value. Page 2 of 3 Generated at Ad 3.2014 04:04 Page 14 L14061480 / Revision: 0 / 25 total pages Generated: 07/03/2014 09:06 :port#: L14061480 olect #: 2941.016 Name: Wilson NC ontacC EmltyYoak Analyte CAS # Result Qual RL MDL ReacCnrity, Cyanide 57-12-5 U 10.1 10.1 `U Not detected at or above adjusted sample detection limit Page 3 of 3 Generated at.7ul 3.2014 09:04 Page 15 L14061480 / Revision: 0 / 25 total pages Generated: 07/03/2014 09:06 _ Analyte Result Qua] RL _� MDL EPA HW# i Reg. Limit Arsenic, TCLP Barium, TCLP Cadmium, TCLP 0.0925 U J �U 1.00 ; 0.500 0.100 0.0500 i D.S00 I 0.0500 D004 —! 5 —_---� D005 _ j 100 D006 i 1 Chromium, TCLP U 0.200 010 D D007 i 5 Lead, TCLP U LOD j 0.500 D008 i 5 � Page 1 of 2 _ Generated at ]d 3, 2014 0"4 Page 16 L14061480 / Revision: 0 / 25 total pages Generated: 07/03/2014 09:06 L14061480 294LO16 wpson Nc EmgyYoak Certificate of Analvsis Analyte Result Qual RL MDL EPA HW# Reg. Limit Selenium, TCLP U 0.800 0.400 D010 1 Silver, TCLP U 0.100 0.0500 D011 5 1 J The analyte was positively identified, but the quantitation was below the RL U Not detected at or above adjusted sample detection limit Analyte Result Qual RL MDL EPA HW# Reg. Limit Mercury U 0.00200 0.60100 D009 0.2 U Not detected at or above adjusted sample detection limit Page 2 of 2 Generated at JUI a. 2014 09:64 Page 17 L14061480 / Revision: 0 125 total pages Generated: 07/03/2014 09:06 i ANNUAL RESIDUAL. SAMPLING SUMMARY FORM 4 fiQ Permit N1o, \UQ0028547 Facility Name Town of YancoyMc Source Permit.No: NC004001l Source Name Yanccyville l4'1V/' T Laboratriry'I Loboratory.2 Sample or CompositeDaw Parameter (mg/lCg) Class A Cliis B A&LEaetern Labe, Inc. 6/19/2014 'Aluminum N/A N/A 28,3 ap Am monia Nitrogen N/A N/A 99j0 Arsenic 41 75 4 Cadmium 39 85 2' Calcium N/A N/A- ]t,70t1 Copper 1,500 4,300 ;M Lead -300 840 37 Magnesium N/A' N/A 4,820 Mercuy '17- 57 0.4 Molybdenum N/A 75 G Nickel 420 420 35 iaate•NiirirrNiuogen N/A N/A ; 3 Percent Solids N/A N/A 3.23 pH (no units) N/A N/A. 7,44 Phosphorus N/A" N/A 16,3W) Potassium ,N/A. N/A 3,060 PAN,(inj,/Inc.) N/A N/A, m1,120 PAN (Surface) N/A N/A 16,165 Selenium . 100 100. 5 . Sodium N/A 'N/A 2;)5ti SAR 'N/A- . N/A 0.64 TKN N/A.. N/A 47,10tt - Zine . 2,800 7,500 7f 7, 511 certify, under penalty oflaw, that this document was prepared tinder friy, direction'or supervision in accordance'with a system designed to assure that qualified personnel properly gathered: anti evaluated, the infnnna'tinn submitted, '1am aware thattherc are signMeantpenalties for ' submitthig false info►mntion; including the possibility of fipes: and imprisonment for knowing violations:' , Si atureofPrcparer* — ?1)atc' *Preparer is'tleilned in 40 CPR-Parh503.9(r)'and 15A NCAC 2T,1102 (26) .'AGMAN FIELD LOADING ESTIMATES Facility Yanceyville WWI'P Sampling Date 6/19/2014 % Solids 3.23 Mineralization Rate 0.30* Gallons per DT 7,424.40 pH 7.44 Sodium Absorpotion 0.64 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION NUTRIENT APPLICATION TKN (mg/Kg) 47,100 lbs./1,000 gal 12.69 Ammonia Nitrogen (mg/Kg) 9,910.00 lbs./1,000 gal 2.67 Nitrate -Nitrite (mg/Kg) 52.60 lbs./1,000 gal 0.01 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 16,165 lbs./1,000 gal 4.35 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 21,120 lbs./1,000 gal 5.69 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class'A Ceiling Limits (mg/Kg) Class B Ceiling Limits (mg/Kg) Potassium lbs./1,000 gal 0.82 Phosphorus lbs./1,000 gal 4.39 Calcium lbs./1,000 gal 4.50 Caicium lbs./1,000 gal 1.30 Manganese lbs./1,000 gal 0.12 Sulfur lbs./1,000 gal 3.77 Molybdenum lbs./1,000 gal 0.00 HEAVY METAL CONCENTRATION HEAVY METAL LOADING 41 75 Arsenic (mg/Kg) 4.00 Arsenic lbs./1,000 gal 0.00 39 85 Cadmium (mg/Kg) 2.00 Cadmium lbs./1,000 gal 0.00 1,500 4,300 Copper (mg/Kg) 381.00 Copper lbs./1,000 gal 0.10 300 840 Lead (mg/Kg) 37.00 Lead lbs./1,000 gal 0.01 17 57 Mercury (mg/Kg) 0.40 Mercury lbs./1,000 gal 0.00 420 420 Nickel (mg/Kg) 35.00 Nickel lbs./1,000 gal 0.01 100 100 Selenium (mg/Kg) 5.00 Selenium lbs./1,000 gal 0.00 2,800 7,500 Zinc (mg/Kg) 767.00 . Zinc lbs./1,000 gal 0.21 RESIDUAL NITROGEN CALCULATION i 1st Year 2nd Year j 3rd Year Fi 4th Year 5th Year I Surface Application Injection/Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (.g/kg) (lbs/DT) (-g/Kg) Tl (-g/kg) (lbs/DT) (-g/Kg) 47,100 16,165 32.33 30,935 47,100 21,120 4224 25,980 30,935 4,640 9.28 26,295 25,980 3,897 7.79 22,083 26,295 1,972 3.94 24,323 22,083 1,656 3.31 20,427 24,323 912 1.82 23,411 20,427 766 1.53 19,661 23,411 439 0.88 22,972 19,661 369 0.74 19,292 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Total 24,128 48.26 Total 27,808 55.62 L J Page: 1 of 2 Report Number: 14-171-0201 Account Number: 04596 Submitted By: SCOTT CARPENTER Send To: SOIL PLUS, LLC SCOTT CARPENTER P.O. BOX 1396 OXFORD, NC 27565 Lab Number: 56031 Sample Id: YWWTP 061914 q � A&L Eastem Laboratories, Inc. 7621 Whitepihe Road Richmohd, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www.aleastern.com Project: YANCEYVILLE WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/19/2014 11:30:00 Date Received: 06/20/2014 00:00 Date Reported: 06/26/2014 Total Solids * 3.23 32300 100.0 JM 06/20/2014 13:34 SM-254OG Moisture * 96.77 100.0 JM 06/20/2014 13:34 SM-2540G Total Kjeldahl Nitrogen 4.71 47100 10.0 JM 06/23/2014 08:50 SM-4500-NH3C-TKN Total Phosphorus 1.63 16300 100 KM 06/23/2014 10:20 SW 6010C Total Potassium 0.31 3060 100 KM 06/23/2014 10:20 SW 6010C Total Sulfur 1.40 14000 100 KM 06/23/2014 10:20 SW 6010C Total Calcium 1.67 16700 100 KM 06/23/2014 10:20 SW 6010C Total Magnesium 0.48 4820 100 KM 06/23/2014 10:20 SW 6010C Total Sodium 0.21 2050 100 KM 06/23/2014 10:20 SW 6010C Total Iron 24000 100 KM 06/23/2014 10:20 SW 6010C Total Aluminum 28300 100 KM 06/23/2014 10:20 SW 6010C Total Manganese 428 5 KM 06/23/2014 10:20 SW 6010C Total Copper 381 5 KM 06/23/2014 10:20 SW 6010C Total Zinc 767 5- KM 06/23/2014 10:20 SW 6010C Ammonia Nitrogen 0.99 9910 10.0 JM 06/23/2014 08:50 SM-4500-NH3C Organic N 3.72 37190 10.0 06/23/2014 08:50 CALCULATION Nitrate+ N itrite-N 52.6 2.00 JM 06/23/2014 08:40 SM-450ONO3F Total Cadmium 2.0 2.0 KM 06/23/2014 10:20 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-171-0201 Account Number: 04596 Submitted By: SCOTT CARPENTER Send To: SOIL PLUS, LLC SCOTT CARPENTER P.O. BOX 1396 OXFORD, NC 27565 Lab Number: 56031 Sample Id : YWWTP 061914 A&L Eastern Laboratories, Inc. 7621 Whttepine Road Richmond, Wginia 23237' (804) 743-9401 Fax (804) 271.6446 wwwaleasternmin Project: YANCEYVILLE WWTP NC CERT#257 REPORT OF ANALYSIS Total Chromium 58 5 KM Total Nickel 35 5 KM Total Lead 37 5 KM Total Arsenic 4.0 3.0 KM Total Mercury 0.4 0.4 KM Total Selenium <5.0 5.0 KM pH (Standard Units) * 7.44 2.00 JM Total Molybdenum 6 5 KM Soluble Phosphorus 0.12 1200 100 JM Comments: WATER SOLUBLE P, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. Date Sampled: 6/19/2014 11:30:00 Date Received: 06/20/2014 00:00 Date Reported: 06/26/2014 06/23/2014 10:20 SW 6010C 06/23/2014 10:20 SW 6010C 06/23/2014 10:20 SW 6010C 06/23/2014 10:20 SW 6010C 06/24/2014 12:00 SW-7471 B 06/23/2014 10:20 SW 6010C 06/23/2014 08:50 SW-9045D 06/23/2014 10:20 SW 6010C 06/24/2014 10:59 SOLUBLE P IN MANURE All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt �M CR* 0B;�c° CERTIFICATE OF ANALYSIS SCOTT CARPENTER SOIL PLUS 208 WILLIAMS ST. GREENVILLE NC 27858 USA Microbac Laboratories, Inc. - Wilson Division 3809 Airport Drive NW Wilson, NC 27896 Tel: (252) 237-4175 Report Date: 2014/07/07 Quote: 23=20140328-14 Work Order: 2014-06-19-022 Matrix: WW Collection Date: 2014/06119 Sample Submission Date: 2014/06/19 SIDN Client Marks Analysis -Name Method Result Unit AA51756 Yanceyville WWTP 061914 Flash Point - LiquidsSubcontracted *See Attached AA51756 Yanceyville WWTP 061914 pH (Corrosivity) Subcontracted *See Attached AA51756 Yanceyville WWTP 061914 Reactive Cyanide Subcontracted *See Attached AA51756 Yanceyville WWTP 061914 Reactive Sulfide Subcontracted *See Attached AA51756 Yanceyville WWTP 061914 TCLP Full Metals V(Subcontracted *See Attached Comments: Approved by: 14 Kim Hesse! f For any feedback concerning our services, please contact James Nokes, Senior Vice President, at James.nokes@microbac.com or Trevor Boyce at president@microbac.com Environmental • Agrochemical 9 Food • Pharmaceuticals Page 1 of 1 N: 1-14061480 H: 294L016 im Wilson NC at: EmllyYoak Analyte CAS # Result Qua) RL MDL Reactivity, Sulfide 18496-25-8 U 100 100 U Not detected at or above adjusted sample detection limit Analyte CAS # Result Qual RL MDL Corrosivity pH 10-29-7 6.70 I 0.000 0.000 Temperature At Determination (C) 18.3 0.000 0.000 Analyte CAS # Result Qual RL MDL Ignitability, 64.0 > 0.000 0.000 > Result Is greater than the associated numerical value. J Page 1 of 3 Generated at Jul 3, 2014 09:04 Page 13 L14061480 / Revision: 0 125 total pages Generated: 07/03/2014 09:06 Lob Report d: L14061480 .Lab Project g: 294L015 Project Name: WUsonNC Lob Contact: EmBy Ybak 4"L- -PE-1 CP2-' Analyte Result Qual RL MDL EPA HW# Reg. Limit Arsenic, TCLP U im 0.500 D004 5 Barium, TCLP u U 0.100 0.0500 I D005 100 Cadmium, TCLP Chroryfium, TCLP U-.-T-. U 0.100 -T-�0500 0.200 0.100 D006 0007 5 Lead, TCLP T U 1 1.00 0.500 DOOB 5 Selenium, TCLP r yT^ U 0.800 0.400 D010 1 Silver, TCLP 1 U 0.100 0.0500 DOIj r 5 :U Not detected at or above adjusted sample detection limit Result Qual RL MDL EPAHW# }—Reg. Limit Analyte - — - ------- U 0.00200 0.00100 1 D009 Mercury 0.2 U I Not detected at or above adjusted sample detection limit '6 - APPENDIX III FIELD LOADING SUMMARY FORM PermitNumber WQ0028547 Facility Name Town of Yanceyville LandOwner Vernon H. Williamson Operator Vernon H. Williamson ANNUAL LAND APPLICATION FIELD SUMMARY FORM Site# NC-CS-81 County Caswell Crop I Fescue Pasture Field Name 4 SoilSeries Iredell Crop I Pan 112 Acres Permited 11.97 Soil Abbreviation: 250B Crop 2 Crop 2 Pan Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN 08/27/2014 Gallons 58,500 4.48 11.97 0.91 10.93 Yanceyville WTP Dry 0 Surface 2.76 0.50 0.40 7,590 446.00 44.64 5.71 Total Volume Applied 58,500 Reported in Gallons Arsenic Cadmium Current Year 0.011 0.004 Prior Year 0.026 0.013 Cumulative Total 0.037 0.017 Permitted CPLR 36 34 Total Dry Tons 10.93 Copper Chromium Lead 0.075 0.168 0.044 2.592 0.582 0.292 2.666 0.750 0.336 1338 267 Crop Crop l Sum Total P 2.76 Total 5.71 Total Mercury Molvbdenum Nickel Selenium "Line Crop 1 Crop 2 PAN PAN 0.001 0.009 0.044 0.009 0.119 (lbs./Ac) Lime (T/Ac.) Date (lbs./Ac.) 0.010 0.044 0.260 0.021 4.520 0.010 0.053 0.304 0.030 4.638 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN _ Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, • **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 2-25-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0028547 Site# NC-CS-81 County Caswell Crop 1 Fescue Pasture Facility Name Town of Yanceyville Field Name 5 SoilSeries Orange Crop I Pan 250 LandOwner Vernon H. Williamson Acres Permited 15.43 Soil Abbrevation: OrB Crop 2 Operator Vernon H. Williamson Crop 2 Pan Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 08/28/2014 Gallons 19,500 4.48 15.43 0.24 3.64 Yanceyville WTP Dry 0 Surface 0.71 0.50 0.40 7,590 446.00 44.64 1.48 Crop 1 08/29/2014 Gallons 58,500 4.48 15.43 0.71 10.93 Yanceyville WTP Dry 0 Surface 2.14 0.50 0.40 7,590 446.00 44.64 4.43 Crop 1 09/02/2014 Gallons 39,000 4.48 15.43 0.47 7.29 Yanceyville WTP Dry 0 Surface 1.43 0.50 0.40 7,590 446.00 44.64 2.95 Crop 1 09/04/2014 Gallons 19,500 4.48 15.43 0.24 3.64 Yanceyville WTP Dry 0 Surface 0.71 0.50 0.40 7,590 446.00 44.64 1.48 Crop 1 09/06/2014 Gallons 19,500 4.48 15.43 0.24 3.64 Yanceyville WTP Dry 0 Surface 0.71 0.50 0.40 7,590 446.00 44.64 1.48 Crop 1 09/19/2014 Gallons 84,500 4.48 15.43 1.02 15.79 Yanceyville WTP Dry 0 Surface 3.09 0.50 0.40 7,590 446.00 44.64 6.39 Crop 1 Total Volume Applied 240,500 Total Dry Tons 44.93 Sum Total P 8.79 Total 18.20 Total Reported in Gallons arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.035 0.012 0.239 0.536 0.140 0.002 0.029 0.140 0.029 0.379 (ibs./Ac.) (lbs./Ac.) Lime T/Ac. Date Prior Year 0.034 0.016 2.997 0.711 0.340 0.012 0.054 0.308 0.029 5.210 Cumulative Total 0.068 0.028 3.236 1.247 0.480 0.014 0.083 0.448 0.059 5.589 Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, `� +'�. **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 S�L 2-25-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PemtitNumber WQ0028547 Site# NC-CS-81 County Caswell Crop I Fescue Pasture Facility Name Town of Yanceyville Field Name 6 SoilSeries Helena Crop 1 Pan 250 LandOwner Vernon H. Williamson Acres Permited 5.77 Soil Abbrevation: Hell Crop 2 Operator Vernon H. Williamson Crop 2 Pan Volume Acres Dry Date M. , urement Applied % Solids Used DT/Ac. Tons 08/25/2014 Gallons 45,500 4.48 5.77 1.47 8.50 Source Yanceyville WTP Soil Application Condition Precip Method Dry 0 Surface Total P 4.45 Nitrate- Crop 1 Volatilization Mineralization TKN Ammonia Nitrite PAN 0.50 0.40 7,590 446.00 44.64 9.21 Crop 2 PAN Crop Crop 1 Total Volume Applied 45,500 Total Dry Tons 8.50 Sum Total P 4.45 Total 9.21 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.018 0.006 0.121 0.271 0.071 0.001 0.015 0.071 0.015 0.192 Lime (T/Ac.) Date (lbs./Ac.) (lbs./Ac.) Prior Year 0.042 0.021 3.842 0.905 0.436 0.015 0.069 0.394 0.037 6.683 Cumulative Total 0.060 0.027 3.963 1.176 0.507 0.016 0.083 0.465 0.052 6.874 Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 2-25-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0028547 Site# NC-CS-81 County Caswell Crop I Fescue Pasture Facility Name Town of Yanceyville Field Name 7 SoilSeries Iredell Crop 1 Pan 250 LandOwner Vernon H. Williamson Acres Permited 15.73 Soil Abbrevation: 250B Crop 2 Operator Vernon H. Williamson Crop 2 Pan Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 10/07/2014 Gallons 91,000 3.23 15.73 0.78 12.26 Yanceyville WWTP Dry 0 Surface 25.40 0.50 0.30 47,100 9,910.00 32.60 25.19 Crop 1 10/08/2014 Gallons 136,500 3.23 15.73 1.17 18.39 Yanceyville WWTP Dry 0 Surface 38.10 0.50 0.30 47,100 9,910.00 52.60 37.79 Crop 1 Total Volume Applied 227,500 Total Dry Tons 30.64 Sum Total P 63.51 Total 62.98 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium Zinc Crop 1 Crop 2 PAN PAN Current Year 0.016 0.008 1.484 0.226 0.144 0.002 0.023 0.136 0.019 2.988 (lbs./Ac.) (lbs./Ac.) Lime (T/Ac.) Date Prior Year 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Cumulative Total 0.016 0.008 1.484 0.144 0.002 0.023 0.136 0.019 2.988 Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, taw sludge -0.4 2-25-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PermitNumber WQ0028547 Site# NC-CS-81 County Caswell Crop 1 Fescue Pasture Facility Name Town of Yanceyville Field Name 8 SoilSeries Helena Crop 1 Pan 169 LandOwner VemonH. Williamson Acres Permited 8.38 SoilAbbrevation: HeB Crop 2 Operator Vernon H. Williamson Crop 2 Pan Volume Acres Dry Soil Application Total Nitrate- Crop 1 Crop 2 Date Measurement Applied % Solids Used DT/Ac. Tons Source Condition Precip Method P Volatilization Mineralization TKN Ammonia Nitrite PAN PAN Crop 08/26/2014 Gallons 104,000 4.48 8.38 2.32 19.43 Yanceyville VrIT Dry 0 Surface 7.00 0.50 0.40 7,590 446.00 44.64 14.49 Crop 1 08/27/2014 Gallons 19,500 4.48 8.38 0.43 3.64 Yanceyville WTP Dry 0 Surface 1.31 0.50 0.40 7,590 446.00 44.64 2.72 Crop 1 08/28/2014 Gallons 52,000 4.48 8.38 1.16 9.71 Yanceyville WTP Dry 0 Surface 3.50 0.50 0.40 7,590 446.00 44.64 7.25 Crop 1 Total Volume Applied 175,500 Total Dry Tons 32.79 Sum Total P 11.82 Total 24.45 Total Reported in Gallons Arsenic Cadmium Copper Chromium Lead Mercury Molybdenum Nickel Selenium "Zinc Crop 1 Crop 2 PAN PAN Current Year 0.047 0.016 0.321 0.720 0.188 0.003 0.039 0.188 0.039 0.509 Lime (T/Ac.) Date (lbs./Ac.) (lbs./Ac.) Prior Year 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Cumulative Total 0.047 0.016 0.321 0.188 0.003 0.039 0.188 0.039 0.509 Permitted CPLR 36 34 1338 267 15 374 89 2498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4 t'dwx S��_ _ _ _ _ _ _ ****C.P.L.R.: Cumulative Pollutant Loading Rate Signature of Land Applier Date APPENDIX IV PATHOGEN AND VECTOR VERIFICATION 11 "Class V' Alter ia.tive: Not Applicable If applicable to alternative performed ("Class Ai only) indicate "Process to" Further Reduce Paihogcns" ;" B'eta,RaT+ "Class B"'Alternative: Aitcrriative 1 If Foplicalilc to alternative perforated ("Class B" only) indicate "Process to Further Reduee-Pathoac s":: Nor Applicable " Fecal Coliforrn, Minimutn' Geo. Mean Maidinum #-of Exce,edences Fregtiency Sample Type . Colonies -Per Grim of . Total Solids(Dry 4068.94 5,543, 7SE307 0 ' 1 Grab Sattiples Weight) . Analytical Technique,. SN 9221'E.' VeciorAttraction Reduction'Perfomied (15ANCAC 02T.1107)t iVo alteniatives petfonned "I testify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1105 and the vector attraction reduction requirement in 1SA NCAC 02T .1107 have been met. " "1 cerdfy, under penalty of law, that the patbogen.requirements in 15A 14CAC 02T JA06 anti the vectof attraction reduction requirement in-15A NCAC 02T .1107-have not been met 2' (Please note if you check this statement attach nit explanation whg you have-not met one or 'both of the requirements.) "This determinau'On.has.been made under -my direction and supervision in accordance with -the system'desigiied to ensure that quatified personnelproperlygathec and evaluate -the -information used to determine that the pathogen andvectonattraction teductionrequitements,havc been met. ,I am aware that there -ate significant penalties for false certification indudin_ g fine.and -imprisonments• Jason Stnitb VP iTt Coin �,{t7PXti2t-i' o V. Preparer Name and Title {t}Te or print) Land Applier Name and:Titie (if applicable)(type or puns). ;AM. 02-25-2015 3 ft5 ignature"of Preparer* Date Signature of Land Applier (if applicable Date. *Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26) Wednesday,.Febr iary 251.2015 - ®---�- CLIENT \4M9 AMAtE <. ',SAMPLE -.DATE,: ' m` ■. . %#tYSfS"' —_/ , e miffe- ■ - r AN&!METHODMITIORI ^Class A" Alternative: Not,Applicable . to alternative performed -("Class A" only) indicate "Process to Further Reduce Fathom ns`": Not Applicable - If applicable . "Class R" Alternative: lremative 1 1£applicable io.altemative performed fflass]3" only) indicate "Process to'Further Reduce l'athogegs": Not 'Applicable-; ; Fecal Coliform• -Minimurn. ,Geo. Mean Maximum # of Fwceedences, Frequency, SampleType Colonies')P'er. Grath of , Total 5olids(Dry. ' 184306.16 198,125 216981.84 1 Grab S•aiupks Weight) Analytical Technique . SM,922I E' . Vector Attraction Reduction Perfotsned (15ANCAC 02T .1107). Ak 3 (30-day bench) "I certify; under penalty of lave, that the patho„sen requirements in 15A NCAC 42 i .11U6 and.tff2e vector attraction reduction- ` requirement in 15ANCAC:02T :1107 have been,met2' "I certify, under penalty of iaw,.that tlie�patitogen requirements in 15A NCAC 02T .110E and the vector attraction reduction Q requirement,in 15A,NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation vehy. , you have not met.one ,or both of the regiurernents "'Phis deterntinatiort has been mane under -my direction andsupervisioti in accordance,with the system designed to en' iurc that qualified personnel properly-gathei and.evaluate the information used- to determine -that the Pathogen and vector attraction `reduction requirements liave been met. I am aware that theie'are significant penalties for false certification'including fine and imprisonment.'! I3ratt111crtitt ORC Jason Stnith XT Prepaxer Name. and Title, (type or print) Land Applier'Name and Title: (if applicable)(type.or pint) •, . 02-25:72015' Si,*nature -Preparers . Dare Signattue ofLand Applies (if applicable . Date *Pieparer is defined inAO CFR Part 503:9(r) and 15A NCAC 2T .1102 (26) Wednesday, February 25, 2015 . . ' P.O.- Box 411483 e Charlotte; NC 2824I-1483 Phone: (704) 588-8333 , Fax: (704) 588-8335 y f I 4E STTART DATE. I • ND-04 •F.-xv,•'..rw+n.M..ly Ysw2n wYR YM4v4',1 Y. ,1 utieM�W+' i i . �. Sfart: . End: TS . ° 0.21,16 ; ::. 0.2083 TS°/a' 1,63°l0 _ '- 1-,63% VS 0.1185 :- ' .. 0:1'11.2 VS%:, . ; ,56.00%0- .. ,_`_ ,53,:38% OUT = 0:00279858 FSVR-(Mass Balance) -. - 6.15% FSVR (Van Kleeck) -1a OT% FSVR M ss.Balance)'<.15% _ "YES ` FSVR (Van Kleeck) --15°l0, ... YES• .° „_ ZANNE ICE . AMPL.1 DAM A I BEE 11 ANALYS!§_METff0D- Ww"', mj I C, I �mm 1111011 E '�Tyv onto n"- - - - - - - - - - - - - - - - ----- - 500 -myv�§' Q� WAS!, 14 A Qq-v�- _1- ­J.� WAS, '3� a 0 of tattoo "M Wmah-Yl 75-o c B45' _7 1" TO Q '72%6` 041 4 W-0 hT I MO its. W. I 1 MOT a, 9-1: EMT 1 1 hs, "awas "Promwo NSA T4 k__ 4 bl", I jK Qi, to W .7 ICA) j . WAR �07, 7 7- I X nm Now OW Qfy on ny­ "it Encessiot W323 LON MOO " HOME= - - SMAM— A WANN" own; ; , t�' ": -,, ­, -mot '2 MAMMA Mass; v" PSI nW—�j i-0,7Lq� -05_, NOW - Man an x", Vv AMS yTQ_"QfQ "too -_ __QWm-" V-, C, 01""Of K, Am 4�, Q&TY94 Q By", j#Q -, ANY A� W, W"m Also, 9=5 —TOM ANN 400 too W 51; y A WMW�"Gm n_m �"041 _K son ap A py-- g low A &I AW TM �W on &Mao owl Do- Vol a 1 TAW OW solo No guy VIC lyt,f Ampylim "00-:00 0005 Wavy , '_'. !,- _ , mkoy Oyu a_ CO AV A� APPENDIX V SOIL SAMPLES Page 1 of 1 Report Number: 14-356-0758 Account Number: 04596 Send To: SOIL PLUS, LLC SCOTT CARPENTER P.O. BOX 1396 OXFORD NC 27565 Date Received: 12/2212014 9� A&L Eastern Laboratories - Carolinas 2850 Daisy Lane Wilson, North Carolina 27896 (252) 206.1721 Fax (252) 206- 9973 www.aleastern.com Grower: Submitted By: SCOTT CARPENTER GRANVILLE FARMS Farm ID: NC-CS-81 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Analysis: 12/23/2014 Date Of Report: 12/23/2014 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity` : C.E.0 Sample ID; Lab ENR ` Metilichs Reserve M°`� g Ca Na Soil Buffer" H` Field ID „ Number % Rate Ibs/A ppm. Rate ,,ppm , Rate .ppm .. Rate ppm, ' Rate -ppm Rate „ppm . Rate pH Index me0/100g meq/100g, 4 15090 0.1 VL 39 37 M 66 L 316 VH 1225 M 25 VL 6.8 0.3 9.3 INC=31 NC=34 5 15091 0.4 VL 47 172 H 283 VH 1270 VH 893 M 123 VL 6.6 0.5 8.0 NC = 60 NC = 145 6 15092 0.9 VL 59 95 H 127 H 1198 VH 779 M 121 VL 6.6 0.4 6.3 NC=79 NC=65 8 15093 0.1 VL 38 72 H 290 VH �375 VH 1053 M �26 VL 6.6 0.6 9.8 NC=60 NC=148 percent Base Saturation' Nitrate Sulfur Zinc ° Manganese .. ` iron Copper Boron soluble salts. .' Chloride Aluminum S ample ID. 17161 13 .. K .. Mg °, Ca Na" -.H NON 3 S Zn Min Fe Cu B' SS - Cl,AI,,, . , % . % 0/o % % ppm Rate. ppm Rate ppm Rate ppm Rate ppm, Rate ppm Rate ppm Rate mslcm . Rate ppm Rate ppm 4 32 H 2.2 L 50 H 110 VH 1.9 H 0.3 VL 1.8 28.3 65.9 1.2 2.9 NC=67 NC=55.0 NC=313 1 NC=95.0 5 H M 51 VH VH 1.4 M 0.3 VL 9.1 28.1 55.8 1.3 5.9 �32 13.1 �1170 . NC=67 INC=77.5 NC=319 NC=70.0 6 ' M 3.5 H 93 VH VH 1.4 M 0.4 L 5.2 26.2 61.8 1.4 6,0 NC=42 r NC=87.5 IN 81 �235 NC=70.0 8 VH 2.9 M VH VH 2.0 H 0.4 L 7.6 31.9 53.7 1.2 5.9 �48 NC=100 NC=72.5 180 NC=500 �138 NC=100.0- Values on this report represent the plant available nutrients In the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ppylia H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary