NCG030556_COMPLETE FILE - HISTORICAL_20161129

STORMWATER DIVISION CODING SHEET
' NCG PERMITS
PERMIT NO.
DOC TYPE
-P� HISTORICAL FILE
O MONITORING REPORTS
DOC DATE
❑ ��/. I I a �1
YYYYMMDD

I
aceAnalytical •
WwwParatabscom
December 09, 2016
Mr. Gary Harries
American Truetzschler, Inc.
12300 Moores Chapel Rd.
Charlotte, NC 28214
RE: Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 900
Huntersville, NC 28078
[phone]
„IG� p36ssb
I°
RECEIVED
DEC 16 2016
CENTRAL FILES
�WR SECTION
Dear Mr. Hames:
Enclosed are the analytical results for sample(s) received by the laboratory on November 29, 2016_
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
a- 4�1-
Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 1 of 34

CeAnalytical
rrrpeoetab&=n
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Pace Analyttcal Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
FloridalNELAP Certification #: E87627
Kentucky LIST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 34

. CeAr�alytical
wwrpmxftba.aam
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Lab ID Sample ID
92321149001 Al
92321149002 A2
Pate AnaEytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )875-9092
SAMPLE ANALYTE COUNT
Method
Analysts
Analysts
Reported
Laboratory
EPA 1664E
JMS
1
PASI-C
EPA200.7
SH1
12
PASI-A
EPA 245.1
SER
1
PASI-A
EPA 625
BPJ
58
PASI-C
EPA 624
GAW
38
PASI-C
SM 2540D
MJ51
1
PASI-A
SM 4500-S2D
EWS
1
PASI-A
EPA 9040
ALC
1
PASI-A
EPA 300.0
AES2
1
PASI-A
EPA420A
DMN
1
PASI-A
SM 4500-CN-E
DMN
1
PASI-A
EPA 1664E
JMS
1
PASI-C
EPA200.7
SH1
12
PASI-A
EPA245.1
SER
1
PASI-A
EPA 625
BPJ
58
PASI-C
EPA 624
GAW
38
PASI-C
SM 2540D
MJS1
1
PASI-A
SM 4500-S2D
EWS
1
PASI-A
EPA 9040
ALC
1
PASI-A
EPA 300.0
AES2
1
PASI-A
EPA420A
DMN
1
PASI-A
SM 4500-CN-E
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyticat Services, LLC. Page 3 of 34

CeAnalytrcal
www.pacebbKoom
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Sample: Al
Parameters
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92321149001 Collected: 11/29/16 12:15 Received: 11/29/16 14:16 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND
mg1L
5.0
1
12/08/16 08:03
200.7 MET ICP
Analytical Method: EPA200.7
Preparation Method: EPA200.7
Antimony
ND
ug/L
5.0
1
12/02/16 22:40
12/06/16 03:11
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/02/16 22:40
12/06/16 03:11
7440-38-2
Beryllium
ND
ug/L
1.0
1
12/02/16 22:40
12/06/16 03:11
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/02/16 22:40
12/06/16 03,11
7440-43-9
Chromium
5.1
ug/L
5.0
1
12/02/16 22:40
12/06/16 03:11
7440-47-3
Copper
11.1
ug/L
5.0
1
12/02/16 22:40
12/06/16 03:11
7440-50-8
Lead
ND
ug/L
5.0
1
12/02/16 22:40
12/06/16 18:20
7439-92-1
Nickel
5.4
ug/L
5.0
1
12/02/16 22:40
12/06/16 03:11
7440-02-0
Selenium
ND
ug/L
10A
1
12/02/16 22:40
12/06/16 03:11
7782-49-2
Silver
ND
ug/L
5.0
1
12/02/16 22:40
12/06/15 03:11
7440-22-4
Thallium
ND
ug/L
10.0
1
12/02/16 22:40
12/06/16 18:20
7440-28-0
Zinc
120
ug/L
10.0
1
12/02/16 22:40
12/06/16 18:20
7440-66-6
245.1 Mercury
Analytical Method: EPA245.1
Preparation Method: EPA245.1
Mercury
ND
ug/L
0.20
1
12/02/16 11:15
12/07/16 03:26
7439-97-6
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthylene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
208-96-8
Anthracene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
120-12-7
Benzidine
ND
ug/L
50.0
1
11/29/16 16:40
12101/16 01:09
92-87-5
Benzo(a)anthracene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
50-32-8
Benza(b)fluoranthene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
191-24-2
Benzo(k)fluoranthene
ND
ug1L
5.0
1
11/29116 16:40
12/01/16 01:09
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
11/29116 16:40
12/01/16 01:09
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
11/29/16 16:40
12/01/16 01:09
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
111 44 4
2-Chloronaphthalene
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:09
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
11/29/16 16:40
12/01/15 01:09
7005-72-3
Chrysene
ND
ug/L
5.0
1
11/29/15 15:40
12/01/16 01:09
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
11/29/16 16:40
12/01/16 01:09
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
11/29/16 16A0
12JO1116 01:09
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
11/29/16 16:40
1210106 01:09
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
11/29/16 16:40
12/01/16 01:09
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
11/29/16 16:40
12/01/16 01:09
51-28-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in tuff.
Date: 12/09/2016 02:21 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 34

CeArralytical
kft psrel ac m
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Sample: Al
Parameters
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92321149001 Collected: 11/29/16 12:15 Received: 11/29/16 14:16 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
625 MSSV Analytical Method: EPA625 Preparation Method: EPA625
2,4-Dinitrotoluene
ND
ug/L
5.0
1
11/29/16 16:40
1210111601:09
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
11/2911616:40
1210111601:09
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
117-84-0
1,2-Diphenylhydrazine
ND
ug/L
5.0
1
11/29/16 16:40
1210111601:09
122-56-7
bis(2-Ethylhexyl)phthalate
ND
uglL
5.0
1
11/29/16 16:40
12/01/16 01:09
117-81-7
Fluoranthene
ND
ug/L
5.0
1
11/29/16 16:40
12/0111601:09
206-44-0
Fluorene
NO
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
W73-7
Hexachloro-1,3-butadiene
ND
ug1L
5.0
1
11/2911616:40
1210111601:09
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
11/29/16 16740
12/01/16 01:09
77-47-4
HexachEoroethane
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
11/29/16 16:40
1210111601:09
193-39-5
Isophorone
ND
ug/L
10.0
1
11/29/16 16:40
12/01/16 01:09
78-59-1
Naphthalene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
91-20-3
Nitrobenzene
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:09
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
11/29/16 16:40
12/01/16 01:09
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
11/29/16 16A0
12/01/16 01:09
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
11/29/16 16:40
12101/15 0 1! 09
86-30-6
Pentachlorophenol
ND
ug/L
10.0
1
11/29/16 16:40
12/01/16 01:09
87-86-5
Phenanthrene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:09
85-01-8
Phenol
ND
ug/L
5.0
1
11/29/16 16:40
12101/16 01:09
Pyrene
ND
ug/L
5.0
1
11/29/16 16A0
12JO1116 01:09
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
1112911616:40
12101/1601:09
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
11/29/16 16:40
12/01/16 01:09
88-06-2
Surrogates
Nitrobenzene-d5 (S)
31
%
10-120
1
11/29/16 16:40
12/01/16 01:09
4165-60-0
2-Fluorobiphenyl (S)
36
%
15-120
1
11/29/16 16:40
12/01/16 01:09
321-60-8
Terphenyl-d14 (S)
43
%
11-131
t
11/29/16 16740
12/01/16 01:09
1718-51-0
Phenol-d6 (S)
14
%
10-120
1
11/29/16 16:40
12/01/16 01:09
13127-88-3
2-Fluorophenol(S)
19
%
10-120
1
11/29/16 16:40
12/01/16 01:09
367-12-4
2,4,6-Tribromophenol (S)
44
%
10-137
1
11/29/16 16:40
12/01/16 01:09
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
ND
ug/L
5.0
1
12/01/1619:51
107-02-8
Acrylonitrile
ND
ug/L
50.0
1
12/0111619:51
107-13-1
Benzene
ND
ug/L
2.0
1
12/01/1619:51
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
1210111619:51
75-27-4
Bromoform
ND
ug/L
2.0
1
1210111619:51
75-25-2
Bromomethane
ND
ug/L
2.0
1
1210111619:51
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
12/01/16 19:51
56-23-5
Chlorobenzene
ND
ug/L
2.0
1
1210111619:51
108-90-7
Chloroethane
ND
ug/L
2.0
1
12/0111619:51
75-00-3
2-Chloroethylvinyl ether
ND
ug/L
5.0
1
12/01/16 19:51
110-75-8
Chloroform
ND
ug/L
2.0
1
12101/1619:51
67-66-3
Chloromethane
ND
ug/L
2.0
1
12101/1619:51
74-87-3
REPORT OF LABORATORY ANALYSIS
c2
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 34

IC, o a f
wwwpeoelabacam
ANALYTICAL RESULTS
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Pace Analytical Services, LLG
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Al
Parameters
Lab ID: 92321149001 Collected: 11/29/16 12:15 Received:
Results Units Report Limit DF Prepared
11/29/16 14:16 Matrix: Water
Analyzed CAS No. Qual
624 Volatile Organics
Analytical Method: EPA624
Dibromochloromethane
NO uglL
2.0
1
12101/1619:51
124-48-1
1,2-Dichiorobenzene
ND uglL
2.0
1
12/01/1619:51
95-50-1
1,3-Dichlorobenzene
NO uglL
2.0
1
12/01/1619:51
541-73-1
1,4-Dichlorobenzene
NO ug1L
2.0
1
12/01/1619:51
106-46-7
1,1-Dichloroethane
NO ug1L
2.0
1
12101/1619:51
75-34-3
1,2-Dichloroethane
NO ug1L
2.0
1
12/01/1619:51
107-06-2
1,1-Dichloroethene
NO ug1L
2.0
1
12/0111619:51
75-35-4
cis-1,2-Dichloroethene
NO uglL
2.0
1
1210111619:51
156-59-2
trans-1,2-Dichloroethene
NO uglL
2.0
1
1210111619:51
156-60-5
1,2-Dichloropropane
NO uglL
2.0
1
1210111619:51
78-87-5
cis-1,3-Dichloropropene
ND ug1L
2.0
1
12/0111619:51
10061-01-5
trans-1,3-Dichloropropene
ND uglL
2.0
1
1210111619:51
10061-02-6
Ethylbenzene
NO uglL
2.0
1
12/0111619:51
100-41-4
Hexachloro-1,3-butadiene
NO uglL
5.0
1
12/0111619:51
87-68-3
Methylene Chloride
NO ug1L
2.0
1
12/01/16 19:51
75-09-2
Naphthalene
NO ugll-
5.0
1
12/01/1619:51
91-20-3
1,1,2,2-Tetrachloroethane
ND uglL
2.0
1
1210111619:51
79-34-5
Tetrachloroethene
ND uglL
2.0
1
12101/1619:51
127-18-4
Toluene
NO ug1L
2,0
1
12101/1619:51
108-88-3
1, 1, 1 -Trichloroethane
ND uglL
2.0
1
12/01/1619:51
71-55-6
1,1,2-Trichloroethane
NO uglL
2.0
1
1210111619:51
79-00-5
Trichloroethene
ND uglL
2.0
1
12101/16 19:51
79-01-6
Vinyl chloride
ND uglL
2.0
1
1210i116 19:51
75-01-4
Surrogates
4-Bromofluorobenzene (S)
102 %
70-130
1
12/01116 19:51
460-00-4
Toluene-d8 (S)
105 %
70-130
1
12/01/16 19:51
2037-26-5
1,2-Dichloroethane-d4 (S)
93 %
70-130
1
12/01/16 19:51
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
$5.5 mglL
12.5
1
11/30/16 18:08
4500S21) Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
NO mglL
0.10
1
1210111614:00
18496-25-8 M1
9040 pH
Analytical Method: EPA 9040
pH
5.9 Std. Units
0.10
1
11/30/16 12:03
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
2.3 mg1L
2.0
1
12/0711618:39
14808-79-8
420.4 Phenolics, Total
Analytical Method: EPA420.4
Phenol
0.014 mg1L
0.010
1
1210811615:14
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E
Cyanide
NO mg1L
0.0080
1
12/0111614:56
57-12-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 34

Pace Analytical Services, LLC
' Q dn� /+��
e ceA fQ1��ru►
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wwrpeodabs.com
1(
[phone]
ANALYTICAL RESULTS
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Sample: A2
Lab ID: 92321149002 Collected: 11/29/16 12:30
Received: 11/29/16 14:16 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. 4ual
ITEM, Oil and Grease
Analytical Method: EPA 16646
Oil and Grease
ND
mg/L
5.0
1
12/08/16 08:11
200.7 MET ICP
Analytical Method: EPA200.7
Preparation Method: EPA200.7
Antimony
ND
ug/L
5.0
1
12/02/16 22:40
12/06/16 03:14
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/02/16 22:40
12/06/16 03:14
7440-38-2
Beryllium
ND
ug/L
1.0
1
12/02/16 22:40
12/06/16 03:14
7440-41-7
Cadmium
ND
ug/L
1.0
1
12102/16 22A0
12/06/16 03:14
7440-43-9
Chromium
17.1
ug/L
5.0
1
12f02/16 22:40
12/06/16 03:14
7440-47-3
Copper
18.5
ug/L
5.0
1
12102/16 22:40
12/06/16 03:14
7440-50-8
Lead
9.8
ug/L
5.0
1
12/02/16 22AG
12/06/16 18:33
7439-92-1
Nickel
8.3
ug/L
5.0
1
12/02/16 22:40
12/06/16 03:14
7440-02-0
Selenium
ND
ug/L
10.0
1
12/02/16 22A0
12/06/16 03:14
7782-49-2
Silver
ND
ug/L
5.0
1
12f02116 22:40
12/06/16 03:14
7440-22-4
Thallium
ND
ug/L
10.0
1
12/02/16 22:40
12/06/16 18:33
7440-28-0
Zinc
89.9
ug/L
10.0
1
12/02/1622A0
12106/1618:33
7440-66-6
245.1 Mercury
Analytical Method: EPA245.1
Preparation Method: EPA245.1
Mercury
ND
ug/L
0.20
1
12/02/16 11:15
12/07/16 03:29
7439-97-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthylene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
208-96-8
Anthracene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
120-12-7
Benzidine
NO
ug/L
50.0
1
11/29/16 16:40
12/01/16 01:38
92-87-5
Benzo(a)anthracene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
55-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
1112911616:40
12101/1601:38
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
11MI1616:40
1210111601:38
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
11/29/1616740
1210111601:38
207-08-9
4-Bromophenylphenylether
ND
ug/L
5.0
1
il/2911616:40
1210111601:38
101-55-3
Butylbenzylphthalale
ND
ug/L
5.0
1
11/2911616:40
12JOl 116 01:38
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
11/29/16 16:40
12/01/16 01:38
111-91-1
bis(2-Chloroelhyl) ether
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
91-58-7
2-Chlorophenol
ND
ug1L
5.0
1
11/29/16 16:40
12101/16 01:38
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
7005-72-3
Chrysene
ND
ug/L
5.0
1
11129/1616:40
12101/1601:38
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
11/29/16 16A0
12/01/16 01:38
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
1112911616:40
12101/1601:38
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
120-83-2
Diethylphthalate
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
11/29/16 16:40
12/01/16 01:38
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
11129/16 16:40
12JO1116 01:38
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
11/29/16 16:40
12/01/16 01:38
534-52-1
2,4-Dinitrophenol
ND
ug1L
50.0
1
1112911616:40
12JO1/1601:38
51-28-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 34

Ce/4nWca
WWWpeoetabscarn
ANALYTICAL. RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
(704)875r9092
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Sample: A2
Lab ID: 92321149002
Collected: 11129/16 12:30
Received: 11/29/16 14:16 Matrix:
Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Qual
625 MSSV
Analytical Method: EPA625
Preparation Method: EPA625
2,4-Dinitrotoluene
NO
uglL
5.0
1
11/29/16 16:40
12/0111601:38
121-14-2
2,6-Dinitrotoluene
ND
uglL
5.0
1
11/29/16 16:40
12/01/16 01:38
606-20-2
Di-n-octylphthaiate
ND
uglL
5.0
1
11/29/16 16A0
12/01/16 01:38
117-84-0
1,2-Diphenylhydrazine
NO
uglL
5.0
1
11/29/16 16A0
12/01/16 01:38
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
117-81-7
Fluoranthene
ND
uglL
5.0
1
11/29/16 16:40
12101/16 01:38
206-44-0
Fluorene
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
86-73-7
Hexachloro-1,3-butadiene
ND
ug1L
5.0
1
11129M6 16:40
12/01/16 01:38
87-68-3
Hexachlorobenzene
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
118-74-1
Hexachlorocyclopentadiene
ND
ug1L
10.0
1
11/29/16 16:40
12101MIS 01:38
77-47A
Hexachloroethane
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
67-72-1
Indeno(1,2,3-cd)pyrene
NO
ug1L
5.0
1
11f29116 16:40
12/01/16 01:38
193-39-5
Isophorone
NO
uglL
10.0
1
11/29/16 16:40
12/01/16 01:38
78-59-1
Naphthalene
ND
uglL
5.0
1
11/29/16 16:40
12/01/16 01:38
91-20-3
Nitrobenzene
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
98-95-3
2-Nitrophenol
NO
ug1L
5.0
1
11/29/16 16AO
12/01/16 01:38
88-75-5
4-Nitrophenol
NO
ug1L
50.0
1
11/29/16 16:40
12/01/16 01:38
100-02-7
N-Nitrosodimethylamine
NO
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
62-75-9
N-Nitroso-di-n-propylamine
NO
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
621-64-7
N-Nitrosodiphenylamine
ND
ug1L
10.0
1
11/29/16 16:40
12/01/16 01:38
86-30-6
Pentachlorophenol
NO
uglL
10.0
1
11/29/16 16:40
12101f16 01:38
87-86-5
Phenanthrene
NO
uglL
5.0
1
11129/1616:40
1210111601:38
85-01-8
Phenol
NO
ug/L
5.0
1
11/29/16 16:40
12/01/16 01:38
Pyrene
ND
ug1L
5.0
1
11/29/16 16:40
12/01/16 01:38
129-00-0
12,4-Trichlorobenzene
ND
uglL
5.0
1
11129/1616:40
1210111601:38
120-82-1
2,4,6-Trichlorophenol
ND
ug1L
10.0
1
11/29/16 16:40
12/01/16 01:38
88-06-2
Surrogates
Nitrobenzene-d5 (S)
23
%
10-120
1
11/29/16 16:40
12101f16 01:38
4165-60-0
2-Fluorobiphenyt (S)
27
%
15-120
1
11/29/16 16:40
12/01/16 01:38
321-60-8
Terphenyl-d14 (S)
43
%
11-131
1
11/29/16 16:40
12/01/16 01:38
1718-51-0
Phenol-d6 (S)
10
%
10-120
1
11/29/16 16:40
12/01/16 01:38
13127-88-3
2-Fluorophenol (S)
14
%
10-120
1
11/29/16 16:40
12101M6 01:38
367-12-4
2,4,6-Tribromophen0l (S)
42
%
10-137
1
11/29/16 16:40
12/01/16 01:38
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
ND
uglL
5.0
1
12/01/16 20:08
107-02-8
Acrylonitrile
ND
ug1L
50.0
1
12/01/16 20:08
107-13-1
Benzene
ND
ug1L
2.0
1
12/01/16 20:08
7143-2
Bromodichloromethane
NO
ug1L
2.0
1
12/01/16 20:08
75-27-4
Bromoform
NO
ug1L
2.0
1
12/01/16 20:08
75-25-2
Bromomethane
NO
ug1L
2.0
1
12/01/16 20:08
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
12/01/16 20:08
56-23-5
Chlorobenzene
NO
ug1L
2.0
1
12101/16 20:08
108-90-7
Chloroethane
ND
ug1L
2.0
1
12/01/16 20:08
75-00-3
2-Chloroethylvinyl ether
NO
ug1L
5.0
1
i210i/16 20:08
110-75-8 c2
Chloroform
ND
ug1L
2.0
1
12101/16 20:08
67-66-3
Chloromethane
ND
ug1L
2.0
1
12/01/16 20:08
74-87-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: I M912016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 34

cemaly�ilcal
W"peoMa6a.cvm
ANALYTICAL RESULTS
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntersWle, NC 28078
[phone]
Sample: A2
Parameters
Lab ID: 92321149002 Colleoted: 11/29/16 12:30 Received:
Results Units Report Limit DF Prepared
11/29116 14:16 Matrix: Water
Analyzed CAS No, Qual
624 Volatile Organics
Analytical Method: EPA624
Dibromochloromethane
ND uglL
2.0
1
12/01/16 20:08
124-48-1
1,2-Dichlorobenzene
ND ug1L
2.0
1
12/01/16 20:08
95-50-1
1,3-Dichlorobenzene
ND ug1L
2.0
1
12/01/16 20:08
541-73-1
1,4-Dichlorobenzene
ND ug1L
2.0
1
12/01/16 20:08
106-46-7
1,1-DlGhloroethane
ND ugll-
2.0
1
12/0111620:08
75-34-3
1,2-Dichloroethane
ND uglL
2.0
1
12101/1620:08
107-06-2
1,1-Dichloroethene
ND ug1L
2.0
1
12/01/16 20:08
75-35-4
cis-1,2-Dichloroethene
ND ug1L
2.0
1
12/01/16 20:08
156-59-2
trans-1,2-Dichloroethene
ND uglL
2.0
1
12/01/16 20:08
156-60-5
1,2-Dichloropropane
ND uglL
2.0
1
12/0111620:08
78-87-5
cis- 1,3-Dichloropropene
ND uglL
2.0
1
12/01/16 20:08
10061-01-5
trans- 1,3-Dichloropropene
ND ug1L
2.0
1
12/01/16 20:08
10061-02-6
Ethyibenzene
ND ug1L
2.0
1
12/01/16 20:08
100-41-4
Hexachloro-1,3-butadiene
ND ug/L
5.0
1
12/0111620:08
87-68-3
Methylene Chloride
ND ug1L
2.0
1
12/01/16 20:08
75-09-2
Naphthalene
ND ug1L
5.4
1
12/01/16 20.08
91-20-3
1,1,2,2-Tetrachloroethane
ND uglL
2.0
1
12101/1520:08
79-34-5
Tetrachloroethene
ND ug1L
2.0
1
12/01/16 20:08
127-18-4
Toluene
ND ug1L
2.0
1
12/01/16 20:08
108-88-3
1,1.1-Trichloroethane
ND uglL
2.0
1
12101/1620:08
71-55-6
1,1,2-Tdchloroethane
ND ug1L
2.0
1
12101/1620:08
79-00-5
Trichloroethene
NO ug1L
2.0
1
12/01/16 20:08
79-0143
Vinyl chloride
ND uglL
2.0
1
12/01/16 20:08
75-01-4
Surrogates
4-Bromofluorobenzene (S)
101 %
70-130
1
12/01/16 20:08
460-00-4
Toluene-d8 (S)
105 %
70-130
1
12/01/16 20i08
2037-26-5
1,2-Dichloroethane-d4 (S)
98 %
70-130
1
12/01/16 20:08
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
214 mg1L
50.0
1
11/30/16 18:09
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mglL
0.10
1
12/01/1614:00
18496-25-8
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std. Units
0.10
1
11/30/16 12:03
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
2.1 mg1L
2.0
1
12/07/1618:48
14808-79-8
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
0.011 mglL
0.010
1
12108/1615:15
450OCNE Cyanide, Total
Analytical Method: SM 4500-CN-E
Cyanide
ND mglL
0,0080
1
12/0111614:56
57-12-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 12109/2016 02:21 PM
without the written consent of Pace
Analytical Services, LLC.
Page 9 of 34

s
aceARalytical
wwwpeoelabs.oam
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 339918
QC Batch Method: EPA 1664B
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK: 1885370
Associated Lab Samples: 92321149001, 92321149002
Parameter Units
Oil and Grease mg1L
LABORATORY CONTROL SAMPLE: 1885371
Parameter Units
Oil and Grease mglL
Pace Analytical Services, LLC
9B00 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 12JO8116 07:56
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 36.9 92 78-114
MATRIX SPIKE SAMPLE: 1885372
92321859001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L ND 40 36.0 90 78-114
Results presented on this page are in the units indicated by the "Units- column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 34

to
CeAnalyfical
www.pacataDs com
Project: SAMPLING 11I29I16
Pace Project No.: 92321149
QC Batch: 339045
QC Batch Method: EPA 245.1
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK: 1880183
Associated Lab Samples: 92321149001, 92321149002
Parameter Units
Mercury ug/L
LABORATORY CONTROL SAMPLE: 1880184
Parameter Units
Mercury uglL
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA245.1
Analysis Description: 245.1 Mercury
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0,20 12107/16 02:33
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.7 110 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1880185 1880186
MS MSD
92321226011 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Mercury ug1L ND 2.5 2.5 2.7 2.6 106 104 70-130 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1880187 1880188
MS MSD
92321141001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury uglL ND 2.5 2.5 1.7 1.5 65 59 70-130 9 M1
Resurts presented on this page are in the units indicated by the "Units" coturnn except where an attertute unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 34

IeAnalytical.
nwrpscelabaoorn
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 339077
QC Batch Method: EPA 200.7
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK: 1880248
Associated Lab Samples: 92321149001, 92321149002
Parameter
Units
Antimony
ug1L
Arsenic
ug1L
Beryllium
ug1L
Cadmium
ug/L
Chromium
ug/L
Copper
ug/L
Lead
ug/L
Nickel
ug1L
Selenium
ug/L
Silver
ug/L
Thallium
uglL
Zinc
ug/L
LABORATORY CONTROL SAMPLE:
1880249
Parameter
Units
Antimony
ug1L
Arsenic
ug/L
Beryllium
ug/L
Cadmium
ug1L
Chromium
ug1L
Copper
ug1L
Lead
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Thallium
ug1L
Zinc
ug1L
QUALITY CONTROL DATA
Analysis Method: EPA 200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank
Result
Spike
Conc.
500
500
500
500
500
500
500
500
500
250
500
500
NO
ND
ND
ND
NO
ND
ND
ND
NO
NO
NO
NO
Reporting
Limit Analyzed
5.0
12106/1601:45
10.0
12/06/16 01:45
1.0
12/06/16 01:45
1.0
12/06/16 01:45
5.0
12/06/16 01:45
5.0
12/0611601:45
5.0
12/06/16 17:12
5.0
12/0611601:45
10.0
12106/1601:45
5.0
1210611601:45
10.0
12/06/16 17:12
10.0
12/06/16 17:12
LCS
Result
479
460
486
480
493
490
507
476
482
243
517
513
LCS
% Rec
96
92
97
96
99
98
101
95
96
97
103
103
% Rec
Limits
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1880260
1880251
MS
MSD
92321569008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
NO
500
500
479
482
96
96
70-130
1
Arsenic
ug/L
ND
500
500
463
464
93
93
70-130
0
Beryllium
ug/L
0.071J
500
500
488
489
98
98
70-130
0
Cadmium
ug/L
ND
500
500
483
484
97
97
70-130
0
Chromium
ug/L
ND
500
500
489
490
98
98
70-130
0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC, Page 12 of 34

e
ICBAIIr?lyt a
rtrw.pacalrbx000r
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
J
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1880250
1880251
M5
MSD
92321569008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Copper
ug1L
ND
500
500
491
494
98
99
70-130
0
Lead
ug1L
ND
500
500
507
505
101
101
70-130
0
Nickel
ug1L
ND
500
500
475
475
95
95
70-130
0
Selenium
ug1L
ND
500
500
480
482
96
96
70-130
0
Silver
ug1L
ND
250
250
243
244
97
98
70-130
0
Thallium
ug1L
ND
500
500
468
475
93
95
70-130
2
Zinc
ug1L
14.2
500
500
492
494
96
96
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1880252
1880253
MS
MSD
92321092003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc,
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug1L
ND
500
500
476
470
95
94
70-130
1
Arsenic
ug1L
ND
500
500
458
453
91
90
70-130
1
Beryllium
ug1L
ND
500
500
487
482
97
96
70-130
1
Cadmium
ug1L
ND
500
500
480
474
96
95
70-130
1
Chromium
ug1L
ND
500
500
490
486
98
97
70-130
1
Copper
ug1L
63.8
500
500
562
551
100
97
70-130
2
Lead
ug1L
ND
500
500
468
464
93
92
70-130
1
Nickel
ug1L
ND
500
500
472
465
94
93
70-130
2
Selenium
ug1L
ND
500
500
480
474
96
95
70-130
1
Silver
ug/L
ND
250
250
243
241
97
96
70-130
1
Thallium
ug/L
ND
500
500
456
448
91
89
70-130
2
Zinc
ug1L
46.4
500
500
565
558
104
102
70-130
1
Results presented on this page are in the units indicated by the " Untts" column except where an alternate unit is presented to the right of the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the wntten consent of Pace Analytical Services, LLC. Page 13 of 34

CBAfk?Iy�ICd1
wrw peontabaoom
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 338976 Analysis Method: EPA 624
QC Batch Method: EPA624 Analysis Description: 624 MSV
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK 1879658
Associated Lab Samples: 92321149001, 92321149002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
12/01/1513:22
1,1,2,2-Tetrachloroethane
ug/L
ND
2.A
12101/1613:22
1,1,2-Trichtoroethane
ug/L
ND
2.0
12/0111613:22
1,1-Dichloroethane
ug/L
ND
2.0
12101/1613:22
11-Dichloroethene
ug/L
ND
2.0
12/0111613:22
1,2-Dichlorobenzene
ug/L
ND
2.0
1210111613:22
1,2-Dichloroethane
ug/L
ND
2.0
12101/1613:22
1,2-Dichloropropane
uglL
ND
2.0
12101/1613:22
1,3-Dichiorobenzene
ug/L
ND
2.0
12101/1613:22
1,4-Dichlorobenzene
ug/L
ND
2.0
12/0111613:22
2-Chloroethylvinyl ether
ug1L
ND
5.0
12/01/16 13:22
Acrolein
ug/L
ND
5.0
1210111613:22
Acrylonitrile
ug/L
ND
50.0
1210111613:22
Benzene
ug/L
ND
2.0
12/01/1513:22
Bromodichloromethane
ug1L
ND
2.0
12/01/16 13:22
Bromoform
ug/L
ND
2.0
12/01/16 13:22
Bromomethane
ug/L
ND
2.0
12/01/16 13:22
Carbon tetrachloride
ug/L
ND
2.0
12/01/16 13:22
Chlorobenzene
uglL
ND
2.0
12101/1513:22
Chloroethane
ug/L
ND
2.0
12/01/1613:22
Chloroform
ug/L
ND
2.0
1210111613:22
Chloromethane
ug/L
ND
2.0
12101/1613:22
cis-1,2-Dichloroelhene
ug/L
ND
2.0
12/0111613:22
cis-1,3-Dichloropropene
ug/L
ND
2.0
1210111613:22
Dibromochloromethane
ug/L
ND
2.0
1210111613:22
Ethylberizene
ug/L
ND
2.0
12101/1513:22
Hexachioro-1,3-butadiene
ug/L
ND
5.0
1210111613:22
Methylene Chloride
ug/L
ND
2.0
12JO1116 13:22
Naphthalene
ug/L
ND
5.0
12101/1613:22
Tetrachloroethene
ug/L
ND
2.0
12101/1613:22
Toluene
ug/L
ND
2.0
12/01/16 13:22
trans-1,2-Dichloroethene
ug/L
ND
2.0
12101/1613:22
trans- 1,3-Dichloropropene
ug/L
ND
2.0
12101/1613:22
Trichloroethene
ug/L
ND
2.0
12/01/16 13:22
Vinyl chloride
ug/L
ND
2.0
12/01/16 13:22
1,2-Dichloroethane-d4 (S)
%
93
70-130
12/01/16 13:22
4-Bromofluorobenzene (S)
%
99
70-130
12/01/16 13:22
Toluene-d8 (S)
%
106
70-130
12/01/16 13:22
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28079
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 34

e
CeAtiaocal
rnm4e08bb3,ccm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
99o0 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
LABORATORY CONTROL SAMPLE:
1879659
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,1-Trichloroethene
ug/L
20
19.7
98
52-162
1,1,2,2-Tetrachloroelhane
ug/L
20
18.6
93
46-157
1,1,2-Trichloroethane
ug1L
20
19.1
95
52-150
1,1-Dichloroelhane
ug1L
20
17.8
89
59-155
1,1-Dichloroethene
ug1L
20
19.5
97
1-234
1,2-Dichlorobenzene
ug1L
20
19.0
95
18-190
1,2-Dichloroethane
ug1L
20
19.4
97
49-155
1,2-Dichloropropane
ug/L
20
17.5
88
1-210
1,3-Dichlorobenzene
ug/L
20
18.7
93
59-156
1,4-Dichlorobenzene
ug/L
20
18.6
93
18-190
2-Chloroethylvinyl ether
ug1L
40
38.6
96
1-305
Acrolein
ug1L
100
133
133
15-152
AMIonitrile
ug1L
100
99.0
99
75-132
Benzene
ug1L
20
19.6
98
37-151
Bromodichloromethane
ug1L
20
19.7
99
35-155
Bromoform
ug1L
20
18.1
91
45-169
Bromomethane
ug1L
20
16.6
83
1-242
Carbon tetrachloride
ug/L
20
21.9
109
70-140
Chlorobenzene
uglL
20
18.0
90
37-160
Chloroethane
uglL
20
17.6
88
14-230
Chloroform
ug/L
20
19.8
99
51-138
Chloromethane
uglL
20
14.1
70
1-273
Cis-1,2-Dichloroethene
ug/L
20
18.4
92
68-146
cis-1,3-Dichloropropene
ug/L
20
18.6
93
1-227
Dibromochloromethane
ug/L
20
19.9
99
53-149
Ethylbenzene
ug/L
20
18.4
92
37-162
Hexachloro-1,3-butadiene
ug/L
20
19.8
99
70-130
Methylene Chloride
ug/L
20
17.9
90
1-221
Naphthalene
ug1L
20
17.9
89
70-130
Tetrachloroethene
ug1L
20
17.5
87
64-148
Toluene
ug1L
20
19.0
95
47-150
trans-1,2-Dichloroethene
ug1L
20
18.8
94
54-156
trans-1,3-Dichloropropene
ug/L
20
18.5
93
17-183
Trichloroethene
ug1L
20
19.7
99
71-157
Vinyl chloride
ug/L
20
16.5
83
1-251
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromotluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
1879661
923211369001 Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1, 1, 1 -Trichloroethane
ug/L
ND 20
23.3
116
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND 20
19.9
99
73-159
1,12-Trichloroethane
ug/L
ND 20
21.4
107
64-152
Results presented on this page are in the units indicated by the "Untts' column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 34

CeAnalytiCal
wwar.Pacelaba.00m
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Pace Analytical Services, LLC
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1879661
Units
92321369001
Result
Spike
Conc.
M5
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethane
ug1L
NO
20
20.2
101
43-172
1,1-Dichloroethene
ug1L
NO
20
23.0
115
48-189
1,2-Dichlorobenzene
uglL
NO
20
19.7
99
54-154
1,2-Dichloroethane
uglL
NO
20
21.7
108
42-171
1,2-Dichloropropane
uglL
NO
20
19.3
97
55-157
1,3-Dichlorobenzene
ug1L
ND
20
19.4
97
57-148
1,4-Dichlorobenzene
ug1L
NO
20
19.6
98
58-149
2-ChloroethyMnyl ether
ug1L
ND
40
NO
0
70-130 M1,c2
Acrolein
ug1L
ND
100
139
139
70-130 Mi
Acrylonilrile
ug1L
NO
100
1 D4
104
70-130
Benzene
ug1L
ND
20
22.9
114
54-163
Bromodichloromethane
ug/L
NO
20
22.3
112
W152
Bromoform
ug1L
ND
20
17.9
89
53-151
Bromomethane
ug1L
ND
20
21.2
106
10-200
Carbon tetrachloride
ug1L
ND
20
26.2
131
41-175
Chlorobenzene
uglL
NO
20
20.8
1D4
67-152
Chloroethane
ug1L
ND
20
21.8
109
23-200
Chloroform
ug1L
NO
20
22.5
113
51-166
Chloromethane
ug1L
NO
20
17.9
90
4D-175
cis-1,2-Dichloroethene
ug1L
NO
20
20.8
104
45-174
cis-13-Dichloropropene
ug1L
ND
20
20.9
104
38-146
Dibromochloromethane
ug1L
NO
20
20.2
101
65-144
Ethylbenzene
ug1L
NO
20
21A
105
57-152
Hexachloro-1,3-butadiene
ug1L
NO
20
19.8
99
70-130
Methylene Chloride
ug/L
ND
20
17.9
90
40-167
Naphthalene
ug1L
ND
20
17A
87
70-130
Tetrachloroethene
ug1L
ND
20
19.7
98
59-155
Toluene
ugll-
NO
20
23.0
115
47-162
trans-1,2-Dichloroethene
ug1L
ND
20
21.8
109
47-178
trans-1,3-Dichloropropene
uglL
ND
20
20.0
100
39-14B
Trichloroethene
ug1L
NO
20
23.9
120
60-153
Vinyl chloride
ug1L
NO
20
20.3
102
46-176
1,2-Dichloroethane-64 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
100
7D-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 1879660
92321318001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1-Trichloroethane
ug1L
NO
NO
1,1,2,2-Tetrachioroethane
ug1L
ND
NO
1,1,2-Trichloroethane
ug1L
ND
ND
1,1-Dichloroethane
ug1L
NO
NO
i,1-Dichloroethene
uglL
NO
NO
1.2-Dichlorobenzene
ug1L
NO
NO
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12l0912016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 34

•
CeAnalyti�cal
wwwpecataba.oam
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
SAMPLE DUPLICATE: 1879660
92321318001
Dup
Parameter
Units
Result
Result RPD
1,2-Dichloroethane
ug1L
NO
ND
1,2-Dichloropropane
ug1L
NO
ND
1,3-Dichlorobenzene
ug1L
NO
ND
1,4-Dichlorobenzene
ug1L
NO
ND
2-Chloroethylvinyl ether
ug1L
NO
ND
Acrolein
ug1L
NO
ND
Acrylonitrile
ug1L
NO
ND
Benzene
ug1L
NO
ND
Bromodichloromethane
uglL
NO
NO
Bromoform
ug/L
NO
NO
Bromomethane
uglL
NO
NO
Carbon tetrachloride
ug1L
NO
ND
Chlorobenzene
Ug/L
NO
NO
Chloroethane
ug1L
NO
NO
Chloroform
ug1L
ND
NO
Chloromethane
ug1L
NO
NO
cis- 1, 2-Dichloroethene
ug1L
ND
ND
cis- 1,3-Dichloropropene
ug1L
NO
NO
Dibromochloromethane
ug1L
NO
NO
Ethylbenzene
ug1L
NO
NO
Hexachloro-1,3-butadiene
ug1L
ND
NO
Methylene Chloride
ug1L
NO
NO
Naphthalene
ug1L
NO
NO
Tetrachloroethene
ug1L
NO
NO
Toluene
ug1L
ND
NO
trans-1,2-Dichloroethene
ug1L
NO
NO
trans-1,3-Dichloropropene
uglL
NO
ND
Trichloroethene
uglL
ND
ND
Vinyl chloride
uglL
ND
NO
1,2-Dichlotoethane-d4 (S)
%
98
96 3
4-Bromofluorobenzene (S)
%
102
100 2
Toluene-d8 (S)
%
105
102 3
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1210912016 02:21 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 34

ceARalytical
wrwpacah"tom
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 338743
QC Batch Method: EPA625
Associated Lab Samples: 92321149001. 92321149002
Analysis Method:
Analysis Description:
EPA625
625 MSS
METHOD BLANK: 1878200
Matrix: Water
Associated Lab Samples: 92321149001, 92321149002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
NO
5.0
11/30/16 20:57
1,2-Diphenylhydrazine
ug/L
NO
5.0
11/30/16 20:57
2,4,6-Trichlorophenol
ug/L
ND
10.0
11/30/16 20:57
2,4-Dichlorophenol
ug/L
NO
5.0
11/30/16 20:57
2,4-Dimethylphenol
ug/L
NO
10.0
11/30/16 20:57
2,4-Dinitrophenol
ug/L
NO
50.0
11/30/16 20:57
2,4-Dinitrotoluene
ug/L
NO
5.0
11/30/16 20:57
2,6-Dinitrotoluene
ug/L
NO
5.0
11/30/16 20:57
2-Chloronaphthatene
ug/L
NO
5.0
11/30/16 20:57
2-Chlorophenoi
ug/L
ND
5.0
11130/16 20:57
2-Nitrophenol
ug/L
ND
5.0
11/30/16 20:57
3,3'-Dichlorobenzidine
ug/L
ND
25.0
11/30/16 20:57
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
11/30/16 20:57
4-Bromophenylphenyl ether
ug/L
NO
5.0
11/30/16 20:57
4-Chloro-3-methylphenol
ug/L
NO
5.0
11/30/16 20:57
4-Chlorophenylphenyl ether
ug/L
NO
5.0
11/30/16 20:57
4-Nitrophenol
ug/L
NO
50.0
11/30/16 20:57
Acenaphthylene
ug/L
NO
5.0
11/30/16 20:57
Anthracene
ug/L
NO
5.0
11/30/16 20:57
Senzidine
ug/L
NO
50.0
11/30/16 20:57
Benzo(a)anthracene
ug/L
NO
5.0
11/30/16 20:57
Senzo(a)pyrene
ug/L
NO
5.0
11/30/16 20:57
Benzo(b)fluoranthene
ug/L
NO
5.0
11/30/16 20:57
Senzo(g,h,i)perylene
ug/L
NO
5.0
11/30/16 20:57
Benzo(k)fluoranthene
ug/L
NO
5.0
11/30/16 20:57
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
11/30/16 20:57
bis(2-Chloroethyl) ether
ug/L
NO
5.0
11/30/16 20:57
bis(2-Ethylhexyl)phthalate
ug/L
NO
5.0
11/3011620:57
Butylbenzylphthalate
ug/L
NO
5.0
11/30/16 20:57
Chrysene
ug/L
NO
5.0
11/30/16 20:57
Di-n-butylphthalate
ug/L
NO
5.0
11/30/16 20:57
Di-n-octylphthalate
ug/L
ND
5.0
11/30/16 20:57
Dibenz(a,h)anthracene
ug/L
ND
5.0
11/30/16 20:57
Diethylphthalate
ug/L
ND
5.0
11/30/16 20:57
Dimethylphthalate
ug1L
ND
5.0
11/30/16 20:57
Fluoranthene
ug/L
ND
5.0
11/30/16 20:57
Fluorene
ug/L
ND
5.0
11/3011620:57
Hexachloro-1,3-butadiene
ug/L
NO
5.0
11/30116 20:57
Hexachlorobenzene
ug/L
NO
5.0
11/30/16 20:57
Hexachlorocyclopentadiene
ug/L
NO
10.0
11/30/16 20:57
Hexachloroethane
ug/L
NO
5.0
11/30/16 20:57
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Ftesutts presented on this page are in the units indicated by the "Unks" column except where an alternate unit Is presented to the right of the resutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 34

ceAnalytical
wwrpacdab&=n
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
METHOD BLANK: 1878200
Associated Lab Samples: 92321149001, 92321149002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
11/30/16 20:57
Isophorone
ug/L
ND
10.0
11/30/16 20:57
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
11/30/16 20:57
N-Nitrosodimethylamine
ug/L
ND
5.0
11/30/16 20:57
N-Nitrosodiphenylamine
ug/L
ND
10.0
11/30/16 20:57
Naphthalene
ug/L
ND
5.0
11/30/16 20:57
Nitrobenzene
ug1L
ND
5.0
11/30/16 20:57
Pentachlorophenol
ug1L
ND
10.0
11/30/16 20:57
Phenanthrene
ug/L
ND
5.0
11/30/16 20:57
Phenol
ug/L
ND
5.0
11/30/15 20:57
Pyrene
ug/L
ND
5.0
11/30/16 20:57
2,4,6-Tribromophenol (S)
%
79
10-137
11/30/16 20:57
2-Fluorobiphenyl (S)
%
83
15-120
11/30/16 20:57
2-Fluorophenol (S)
%
42
10-120
11/30/16 20:57
Nitrobenzene-d5 (S)
%
70
10-120
11/30/16 20:57
Phenol-d6 (S)
%
32
10.120
11/30/16 20:57
TerphenyIA14 (S)
%
85
11-131
1113011620:57
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1878201
Units
Spike
Conc.
LCS
Result
LCS
% Rec
°% Rec
Limits
1,2,4-Tdchlorobenzene
ug/L
50
28.8
58
44-142
1,2-Diphenyihydrazine
ug/L
50
39.2
78
25-150
2,4,6-Tdchlorophenol
ug/L
50
46.4
93
37-144
2,4-Dichlorophenol
ug/L
50
38.9
78
1-191
2,4-Dimethylphenol
ug/L
50
36.4
73
32-119
2,4-Dinitrophenol
ug/L
250
125
50
1-181
2,4-Dinitrotoluene
ug/L
50
42.9
86
39-139
2,6-Dinitrotoluene
ug/L
50
43.2
86
50-158
2-Chloronaphihalene
ug/L
50
39.9
80
60-118
2-Chlorophenol
ug/L
50
35.7
71
23-134
2-Nitrophenol
ug/L
50
34A
69
29-182
3,3'-Dichlorobenzidine
ug/L
100
74.2
74
1-262
4,6-Dinitro-2-methyiphenol
ug/L
100
70.8
71
1-181
4-Bromophenylphenyl ether
ugJL
50
36.0
72
53-127
4-Chloro-3-methylphenol
ug/L
100
75.8
76
22-147
4-Chlorophenylphenyl ether
ug/L
50
41.4
83
25-158
4-Nitrophenol
ug/L
250
105
42
1-132
Acenaphthylene
ug/L
50
41.0
82
33-145
Anthracene
ug/L
50
37.1
74
1-166
Benzidine
ug/L
100
36J
36
25-150
Benzo(a)anthracene
ug/L
50
37.3
75
33-143
Benzo(a)pyrene
ug/L
50
39.3
79
17-163
Benzo(t))fluoranthene
ug/L
50
39.2
78
24-159
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
tiuntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units- column except where an alternate unit Is presented to the right of the result -
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 34

e
CeArWcal
wwwpeodabaoam
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
LABORATORY CONTROL SAMPLE: 1878201
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(g,h,i)perylene
ug/L
50
38.7
77
1-219
Benzo(k)fluoranthene
ug/L
50
40.2
80
11-162
bis(2-Chloroethoxy)methane
ug/L
50
34.0
68
33-184
bis(2-Chloroethyl) ether
ug/L
50
33.8
68
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
34.9
70
8-158
Butylbenzylphthalate
ug/L
50
36.5
73
1-152
Chrysene
ug/L
50
38.0
76
17-168
Di-n-butylphthalate
ug./L
50
40.8
82
1-118
Di-n-octylphthalate
ug/L
50
37.0
74
4-146
Dibenz(a,h)anthracene
ug/L
50
40.5
81
1-227
Diethylphthalate
ug/L
50
47A
95
1-114
Dimethylphthalate
ug/L
50
45.1
90
1-112
Fluoranthene
ug/L
50
39.9
80
26-137
Fluorene
ug/L
50
42.3
85
59-121
Hexachloro-1,3-butadiene
ug/L
50
25.1
50
24-116
Hexachlorobenzene
ug/L
50
38.1
76
1-152
Hexachlorocyclopentadiene
ug/L
50
26.4
53
25-150
Hexachloroethane
ug/L
50
24.3
49
40-113
indeno(1,2,3-cd)pyrene
ug/L
50
39.9
80
1-171
Isophorone
ug/L
50
35.7
71
21-196
N-Nitroso-di-n-propylamine
ug/L
50
40.8
82
1-230
N-Nitrosodimethylamine
ug/L
50
22.4
45
25-150
N-Nitrosodiphenylamine
ug/L
50
39.6
79
25-150
Naphthalene
ug/L
50
30.7
fit
21-133
Nitrobenzene
ug/L
50
33A
66
35-180
Pentachlorophenol
ug/L
100
81 A
81
14-176
Phenanthrene
ug/L
50
37.2
74
54-120
Phenol
ug/L
50
18.3
37
5-112
Pyrene
ug1L
50
35.2
70
52-115
2,4,6-Tribromophenol (S)
%
79
10-137
2-Fluorobiphenyl (S)
%
82
15-120
2-Fluorophenol (S)
%
43
10-120
Nitrobenzene-d5 (S)
%
69
10-120
Phenol-d6 (S)
%
33
10-120
Terphenyl-dl4 (S)
%
76
11-131
MATRIX SPIKE SAMPLE:
1878202
92321165002 Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
12,4-Trichlorobenzene
ug/L
ND 50
17.9
36
44-142 M1
1,2-Diphenylhydrazine
ug/L
ND 50
25.0
50
25-150
2,4,6-Trichlorophenol
ug/L
ND 50
26.4
53
37-144
2,4-Dichlorophenol
ug1L
ND 50
22.4
45
1-191
2,4-Dimethylphenol
ug/L
ND 50
22.6
45
32-119
2,4-Dinitrophenol
ug1L
ND 250
85.2
34
1-181
Results presented on this page are in the units indicated by the "Units" column except wherean alternate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 34

e
ceArialytical
wwwpacekn6acom
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9B00 Kincey Ave. Suite 100
Huntersville, NC 2a078
[phone]
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
MATRIX SPIKE SAMPLE: 1878202
92321165002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
NO
50
26.5
53
39-139
2,6-Dinitrotoluene
ug/L
NO
50
26.0
52
50-158
2-Chloronaphthalene
ug/L
NO
50
24.0
48
60-118 M1
2-Chlorophenol
ug/L
ND
50
22.1
44
23-134
2-Nitrophenol
uglL
NO
50
20.5
41
29-182
3,3'-Dichlorobenzidine
uglL
ND
100
36.9
37
1-262
4,6-Dinitro-2-melhylphenol
ug/L
ND
100
48.0
48
1-181
4-Bromophenylphenyl ether
ug/L
ND
50
22.6
45
53-127 M1
4-Chloro-3-methylphenol
ug/L
NO
100
46.9
47
22-147
4-Chlorophenylphenyl ether
ug/L
NO
50
24.7
49
25-158
4-Nitrophenol
ug/L
NO
250
70.2
28
1-132
Acenaphthylene
uglL
ND
50
24.8
50
33-145
Anthracene
ug1L
NO
50
24.9
50
1-166
Benzidine
ug/L
ND
100
NO
2
25-150 M1
Benzo(a)anthracene
ug/L
NO
50
24.5
49
33-143
Benzo(a)pyrene
ug/L
ND
50
25.4
51
17-163
Benzo(b)fluoranthene
ug/L
ND
50
24.8
50
24-159
Benzo(g,h,i)perylene
ug/L
NO
50
24.6
49
1-219
Benzo(k)fluoranthene
uglL
NO
50
26.2
52
11-162
bis(2-Chloroethoxy)methane
ug/L
NO
50
19.8
40
33-184
bis(2-Chloroethyl) ether
ug/L
ND
50
20.9
42
12-158
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
22.4
45
8-158
Butylbenzylphthalate
ug/L
ND
50
23.5
47
1-152
Chrysene
ug/L
ND
50
25.4
51
17-168
Di-n-butylphthalate
ug/L
NO
50
27.0
54
1-118
Di-n-octylphthalate
ug/L
ND
50
23.4
47
4-146
Dibenz(a,h)anthrarene
ug/L
ND
50
26.0
52
1-227
Diethylphthalate
ug/L
NO
50
29.9
60
1-114
Dimethylphthalate
ug/L
NO
50
27.5
55
1-112
Fluoranthene
ug/L
NO
50
26.4
53
26-137
Fluorene
uglL
NO
50
25.6
51
59-121 MI
Hexachloro-1,3-butadiene
ug/L
ND
50
16.0
32
24-116
Hexachlorobenzene
ug/L
ND
50
25.6
51
1-152
Hexachlorocyclopentadiene
ug/L
ND
50
17.0
34
25-150
Hexachloroethane
ug/L
ND
50
15.2
30
40-113 M1
Indeno(1,2,3-cd)pyrene
ug/L
NO
50
25.9
52
1-171
Isophorone
ug/L
ND
50
20.7
41
21-196
N-Nitroso-di-n-propylamine
ug/L
ND
50
26.3
53
1-230
N-Nitrosodimethylamine
ug/L
ND
50
14.2
28
25-150
N-Nitrosodiphenylamine
ug/L
ND
50
26.2
52
25-150
Naphthalene
ug/L
ND
50
19.5
39
21-133
Nitrobenzene
u911-
NO
50
20.2
40
35-180
Pentachlorophenol
ug/L
NO
100
52.7
53
14-176
Phenanthrene
ug/L
NO
50
25.4
51
54-120 MI
Phenol
ug/L
NO
50
11.7
23
5-112
Pyrene
ug/L
NO
50
22.8
46
52-115 M1
2,4,6-Tribromophenol (S)
%
50
10A37
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the reautL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduoed, except in full,
Date: 1210912016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 34

IC,
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wWwpecalabscom
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
MATRIX SPIKE SAMPLE:
1878202
92321165002 Spike
Parameter
Units Result Conc.
2-Fluorobiphenyt (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
SAMPLE DUPLICATE: 1878203
Parameter
Units
92321165003
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/L
NO
NO
1,2-Diphenylhydrazine
ug/L
NO
NO
2,4,6-Trichlorophenol
ug/L
NO
NO
2,4-Dichlorophenol
ug/L
NO
NO
2,4-Dimethylphenol
ug/L
NO
NO
2,4-Dinitrophenol
ug/L
NO
NO
2,4-Dinitrotoluene
ug/L
NO
NO
2,6-Dinitrotoluene
ug/L
NO
NO
2-Chloronaphthatene
ug/L
NO
NO
2-Chlorophenol
ug/L
NO
NO
2-Nitrophenol
ug/L
NO
NO
3,3'-Dichlorobenzidine
ug/L
NO
NO
4,6-Dinitro-2-methylphenol
ug/L
NO
NO
4-Bromophenylphenyl ether
ug1L
NO
ND
4-Chloro-3-methylphenol
ug/L
NO
NO
4-Chlorophenylphenyl ether
ug1L
NO
NO
4-Nitrophenol
ug1L
NO
NO
Acenaphthylene
ug/L
NO
NO
Anthracene
uglL
NO
NO
Benzidine
ug/L
NO
NO
Benzo(a)anthracene
ug/L
NO
NO
Benzo(a)pyrene
ug/L
NO
NO
Benzo(b)fluoranthene
ug1L
NO
NO
Benzo(g,h,i)perylene
ug/L
NO
NO
Benzo(k)ftuoranthene
ug/L
NO
NO
bis(2-Chloroethoxy)methane
ug/L
ND
NO
bis(2-Chloroethyl) ether
ug/L
NO
NO
bis(2-Ethylhexyl)phthalate
ug/L
NO
NO
Butylbenzylphthalate
ug/L
NO
NO
Chrysene
ug/L
NO
NO
Di-n-butylphthalate
ug/L
NO
ND
Di-n-octylphthalate
ug/L
NO
NO
Dibenz(a,h)anlhracene
ug/L
NO
NO
Diethylphthalate
ug/L
NO
NO
Dimethylphthalate
ug/L
NO
NO
Fluoranthene
ug/L
NO
NO
MS
Result
RPD
MS
% Rec
49
26
40
21
47
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
15-120
10-120
10-120
10-120
11-131
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 34

CBAnalytical
www.pacafsb&coM
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
SAMPLE DUPLICATE: 1878203
Parameter
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-ed)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitresodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
Units
92321165003
Result
Dup
Result
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
%
46
50
%
42
51
%
21
25
%
35
44
%
14
18
%
51
47
RPD Qualifiers
9
19
21
24
23
9
Pace Analytical Services, LLC
9800 Kinrey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the -Units' column except where an attemate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 1210912016 02:21 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 34

ceAnal'O al
wwwpecab6s.rnm
QUALITY CONTROL DATA
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 338855 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK: 1879024 Matrix: Water
Associated Lab Samples: 92321149001, 92321149002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 11/30/16 18:03
Pace Anatytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1879025
Spike LCS LCS % Rec
Parameter Units Cont. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 228 91 90-110
SAMPLE DUPLICATE: 1879026
92321256001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
350
283 21 D6
SAMPLE DUPLICATE: 1879027
92321149001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg1L
55.5
56.0 1
Results presented on this page are In the units indicated by the "Units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 34

ceAr�lytical
www.pacetw.com
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 338921
QC Batch Method: SM 45MS2D
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK: 1879261
Associated Lab Samples: 92321149001, 92321149002
Parameter Units
Sulfide mg/L
LABORATORY CONTROL SAMPLE: 1879262
Parameter Units
Sulfide mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvdle, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 4500-S20
Analysis Description: 4500S2D Sulfide Water
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 12/01/16 14:00
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.5 0.45 90 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1879263 1879264
MS MSD
92321149001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/L ND .5 .5 0.39 0.38 60 59 80-120 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1879265 1879266
MS MSD
92321226009 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfide mg1L ND .5 .5 0.47 0.47 95 94 80-120 0
Results presented on this page are In the units Indicated by the "Units" column except where an attemate unit is presented to the right of the neWIL
REPORT OF LABORATORY ANALYSIS
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Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 34

aceAnal.0 al
wwtvpe=4bs.cwn
QUALITY CONTROL DATA
Project: SAMPLING 11/29116
Pace Project No.: 92321149
QC Batch: 338719 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92321149001, 92321149002
SAMPLE DUPLICATE: 1878033
Parameter
pH
SAMPLE DUPLICATE: 1878034
Parameter
pH
92321071001 Dup
Units Result Result
Std. Units 6.4 6.5
92321114001 Dup
Units Result Result
Std. Units 7.3 7.3
RPD Qualifiers
0 H6
RPD Qualifiers
0 H6
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)87$-9092
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right at the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 34

Iei�a o
WWW..pacetabsmen
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 339761
QC Batch Method: EPA 300.0
Associated Lab Samples: 92321149001. 92321149002
METHOD BLANK: 1884270
Associated Lab Samples: 92321-149001, 92321149002
Parameter Units
Sulfate mglL
LABORATORY CONTROL SAMPLE: 1884271
Parameter Units
Sulfate mg1L
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 12/07/16 14:36
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
20 19.2 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1884272 1884273
MS MSD
92321623018 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg1L 12.0 20 20 32.2 32.0 101 100 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1884274 1884275
MS MSD
92321623029 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfate mg1L 6.0 20 20 25.3 25.3 96 96 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 34

2 6', afy[ical
wwwpamlaba.com
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 339981
QC Batch Method: EPA 420A
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK: 1885597
Associated Lab Samples: 92321149001. 92321149002
Parameter Units
Phenol mg1L
QUALITY CONTROL DATA
Analysis Method: EPA420A
Analysis Description: 420.4 Phenolics
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0,010 12/08/16 14:51
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1885598
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phenol mg1L .05 0.047 94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1885599 1885600
MS MSD
92321130001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenol mg1L ND .05 .05 0.047 0.047 81 81 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1885601 1885602
MS MSD
92321113001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenol mg1L 0.030 .05 .05 0.075 0.074 90 89 90-110 1 M1
Results presented on this page are in the units indicated by the "Units' column except wavers an ahemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the wntten consent of Pace AnalOcal Services, LLC.
Page 28 o134

ceAnalytical'
wrw.pacealm cam
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
QC Batch: 338760
QC Batch Method: SM 4500-CN-E
Associated Lab Samples: 92321149001, 92321149002
METHOD BLANK: 1878393
Associated Lab Samples: 92321149001, 92321149002
Parameter Units
Cyanide mg1L
LABORATORY CONTROL SAMPLE: 1878394
Parameter Units
Cyanide mg1L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 4500-CN-E
Analysis Description: 450OCNE Cyanide, Total
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0080 12/01/1614:46
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.1 0,096 96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1878395 1878396
MS MSD
92320983001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Cyanide mg/L ND .1 .1 0.095 0.099 95 99 75-125 4
Results presented an this page are In the units indicated by the "Units" column except where an alternate unit is pfesented to the right of the resutL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12109/2016 02:21 PM without the written consent of Pace Analytical Services, L.L.C.
Page 29 of 34

o
CeAtialygcal
wrw.paadaCs mm
QUALIFIERS
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anatyle is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethyivinyl ether.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 34

CeAnalytical
wwwpacelahs com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SAMPLING 11/29/16
Pace Project No.: 92321149
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
(704)B75-9U92
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92321149001
Al
EPA1664B
339918
92321149002
A2
EPA 1664B
339918
92321149001
Al
EPA200.7
339077
EPA200.7
339243
92321149002
A2
EPA200.7
339077
EPA200.7
339243
92321149001
Al
EPA245.1
339045
EPA245.1
339228
92321149002
A2
EPA 245.1
339045
EPA 245.1
339228
92321149001
At
EPA 625
338743
EPA 625
338907
92321149002
A2
EPA 625
338743
EPA 625
338907
92321149001
Al
EPA 624
338976
92321149002
A2
EPA 624
338976
92321149001
Al
SM 2540D
338855
92321149002
A2
SM 2540D
338855
92321149001
Al
SM 4500-S2D
338921
92321149002
A2
SM 4500-S2D
338921
92321149001
Al
EPA 9040
338719
92321149002
A2
EPA 9040
338719
92321149001
Al
EPA 300.0
339761
92321149002
A2
EPA 300.0
339761
92321149001
Al
EPA 420A
339981
92321149002
A2
EPA 420.4
339981
92321149001
Al
SM 4500-CN-E
338760
92321149002
A2
SM 4500-CN-E
338760
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/09/2016 02:21 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 34

Document Name: Document Revised: Sept. 21, 2016
I�WEr naljdibal • —Sample Condition U on Rece1 SOUR) Pa e 1 of 2
cy` Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality office
Laboratory receiving samples:
Asheville ❑ Eden[:] Greenwood ❑ Huntersville [�� Raleigh❑ Mechanicsville❑
Sample• • • Client Name: wog : 92321149
• Project #�:
Courier: ❑Fed Ex ❑ UP5 ❑USPS ❑Client
❑ Commercial QPace / ❑Other: 92321249 111r l 1 1
Custody Seal Present? ❑Yes [�f3O Seats Intact? ❑Yes �~
Date/Initials Person Examining contenu: J
Packing Material: ❑Bubble Wrap ubble Bags ❑None []Other:
Thermometer et ❑Blue []Noneampler on ice, cooling process has begun
Gun ID: Type of ioe:
Correction Factor: Cooler Temp Corrected (*CI: f 7-7 Biological Tissue Frozen? ❑Yes ®iVo ❑N/A
Temp should be above ire ng to 6'C
USDA Regulate oil ( N/A, water sample)
Did samples ginate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (IntemplC119wly,
Dyes FNo including Hawaii and Puerto Rico)? (]Yes FIND
Chain of Custody Present?
yes
No
N/A
1.
Sa mples Arrived within Hold Time?
es
Na
NIA
2.
Short Hold Time Ana Q2 hr.)?
es
No
N/A
3.
Rush Turn Around Time Requested?
Elyes
RK.
EINLA
4.
Sufficient Volume?'
_Eres
nNo
N/A
S.
Correct Containers Used?
TY�
[IN.
❑N/A
6.
-Pace Containers Used?
PfC
ONa
QNIA
-ontainers Intact?
es
ON.
N A
7.
*am les Field Filtered?
OYes
QNo
A
S. Note if sediment is visible in the dissolved container .
;ample Labels Match COC?
es
ON.
❑N/A
9.
W
-Includes Date/iime/iD/Analysts Matrix:
lea dspace In VOA Vials (a5-6mm)?
❑yes
No
NIA
10.
Yip Blank Present?
❑Yes
[]No
/A
11,
rip Blank Custody Seals Present?
OY.
QN,
A
CLIENT NOTIFICATION/RESOLLMON
_ Field Data Required? ❑Yes ❑No
Person Contacted:
Date/Time:
Comments/Sample �t 'O ,, (�
Discrepancy: MXY 4, PQ C
OD3
�4_t�P�
r
Qil� ' 0—Vel10— LUD
w�f
Project Manager SCURF Review: W
:,•
Project Manager SRF Review: bate:
)te: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be seM to the North Carolina DEHNR Certification Office (i.e.
it of hold, Incorrect preservative, out of temp, incorrect containers)
Page 32 of 34

�aceAnalAcal e
Document Name:
Condition Upon Recei;
Document No.:
F-CAR-CS-033-Rev.01
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
"Bottom half of box is to list number of bottles q. y
Document Revised: Sept. 21, 2016
Page 2 of 2
Issuing Authority:
Pace Quality Office
Project # , WO# : 92321149
PH; AMB Due Date: 12/13/16
CLIENT: 9241m Truata
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pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
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Page 33 of 34

/vPa eAnalytical"
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CHAIN -OF -CUSTODY I Analytical Request Document A
The Chairnaf-Custody is a LEGAL DOCUMENT. All felnvant holds must be completed accurately. do�}
c'f
Page:
of
Section A
Section B
Section C
IL
Required Giant Information:
Required Project Information:
Invoice Information:
^ �+ A
Company:
Report To;
ARnntlon:
1
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Addroee:
Copy To:
Company Namo:
REGULATORY AGENCY
Ina M �
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Address:
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UST
GROUND
RCRA
WATER
F DRINKING WATER
f OTHER
Email To:
Purdlaw Order No.:
Pepe Qrola
w w ran
Rntarm ce:
Phono: Fax:
O - cIS
Project Name:
Powpmiocl
Marlaya:
SltaLocatlon
Requested Duo DatarTAT;
Project Number:
Paco Prork e:
STA TE:
Requested Analysis Filtered (YIN)
Section o
Matrix C
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RequlrodChorif Womvruon
M1ATR1%
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COLLECTED
Preservatives
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co�RT c � s: v
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SL
SAMPLE ID
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DATE TIME DATE TIME
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ADDITIONAL COMMENTS
BY 1 AFFILIA110N
DATE
TIME
BY r AFFILIATION
DATE
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SAMPLE CONDITIONS
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ORIGINAL
SAMPLER NAME AND SIGNATURE
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h\
i
SWPPP Form 3: Rain Event Data
This form will be used to document any rainfall data starting at least 72 hours before the
expected representative storm event.
Personnel
6��y Agme-s
Date/Time/Rainfall
f tjZ41 j� /T3o p,(,. D . of
Date/Time/Rainfall
Date/Time/Rainfall
Z Au 15-
Date/Time/Rainfall
(Z( Z71 1 S 3�'j pw,/0-
DatelTimel Rainfall
7 l �: 3a p 0 . bJ
Date/Time/RainfallO-D
Date/Time/Rainfall
2f3a I ID, 2 0
Stormwater Pollution Prevention Plan
Appendices

:+
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfilling out this farm, please visit: h rt l.ncdenr or web wq Jws su n dessw#t b-4
Permit No.: N/J61 QJQ//Q/s21n/ or Certificate of Coverage No.:
Facility Name: AM ccAn i.rue,+z,-zc�n1 e g Z ✓N c -
County: J§b= fypr-1F.l,Abuf 7 Phone No. -LS
Inspector: Geau
Date of Inspection: NOV. -50 oA01
Time of Inspection: '
Total Event Precipitation (inches): - olD
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
N Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
i prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
t interval is representative for local storm events during the sampling period, and the permittee
# obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
—J�� vy I
of Permittee or Designee)
Pagel of 2

01
OutfallI �} ascription: (p p O A �� i f
utfall No. Structure (pipe, ditch, etc.) ,dj
Receiving Stream:
DDAscribe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge usin� basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: 1o(Z)e� n Prit,.3",
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): _ A10 1'jQ
Aft
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 Q 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 CZ) 3 4 5
5. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
a) 2 3 4 5
7. is there any foam in the stormwater discharge? Yes No
( 8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes oNo
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2

�.I►�.rrwr.
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisform, please visit: hM:/Iportal.ncdenr.org/web/wq/ws/su/nndessw#tab-4
Permit No.: N/Ulr /��gL/n—/t?A2/ or Certificate of Coverage No.:_/
Facility Name: `
County: Phone No. `Mq - 3; q -
Inspector: CAju+M
Date of Inspection: NoU --Z.c� . ;2a 15 _
Time of Inspection: q= IS Ar+n
Total Event Precipitation (inches): . r,D
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
rV Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By thin signature, I certify that this report is accurate and complete to the best of my knowledge:
(SignALi of Permittee or Designee)
Page 1 of 2

H
1. Outfall Description:
Outfall No. A ). Structure ipe, ditch, etc.) P. PC
Receiving Stream: bQa:.� _ �'y�t
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 �2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
( 1/ 2 3 4 5
7. Is there any foam in the stormwater discharge?
8. Is there an oil sheen in the stormwater discharge?
Yes
Yes
9. Is there evidence of erosion or deposition at the outfall?
10. Other Obvious indicators of Stormwater Pollution:
List and describe
No
No
Yes ONo
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2

ceA►Wcal"
wto pacoWmcam
I
December 14, 2015
Mr. Gary Hames
American Truetzschler, Inc.
12300 Moores Chapel Rd.
Charlotte, NC 28214
RE: Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Dear Mr. Hames:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28070
(704)B75-9092
Enclosed are the analytical results for sample(s) received by the laboratory on November 30, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Liamm Harrison
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 31

r
ceAnalytical
rrrpetehDsmrn
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification lDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006DOI
CERTIFICATIONS
FloddalNELAP Certification #: E87527
Kentucky UST Certification #: 84
West Virginia Certification #: 357
VirginialVELAP Certification #: 460221
Asheville Certification Ws
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 31

ceArWcal e
rWW,0Walab&=n
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Lab ID Sample ID
92277769001 Al
92277769002 A2
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 1664B
JMS
1
PASI-C
EPA 200.7
CDF
12
PASI-A
EPA245.1
SH1
1
PASI-A
EPA 625
Bpi
59
PASI-C
EPA 624
GAW
38
PASI-C
SM 2540D
MJP
1
PASI-A
SM 4500-S2D
MJP
1
PASI-A
EPA9040
MLS
1
PASI-A
EPA300.0
MDW
1
PASI-A
EPA 420.4
DMN
1
PASI-A
SM 4500-CN-E
SER
1
PASI-A
EPA 1664B
JMS
1
PASI-C
EPA 200.7
CDF
12
PASI-A
EPA245.1
SH1
1
PASI-A
EPA 625
Bpi
59
PASI-C
EPA 624
GAW
38
PASI-C
SM 2540D
MJP
1
PASI-A
SM 4500-S2D
MJP
1
PASI-A
EPA9040
MLS
1
PASI-A
EPA300.0
MDW
1
PASI-A
EPA420.4
IJMN
1
PASI-A
SM 4500-CN-E
SER
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 31

. CeARaiy cal
wwwpeoswcom
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Sample: Al Lab ID: 92277769001 Collected: 11/30/15 04:00 Received: 11/30/15 14:40 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qua[
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND
mg/L
5.0
1
12/08/15 05:02
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 2003
Antimony
ND
ug1L
5.0
1
12/01/15 19:00
12/05/15 0130
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/01/15 19.00
12/05/15 01:30
7440-38-2
Beryllium
ND
ug/L
1'0
1
12/01/15 19:00
12/05/15 01:30
7440-41-7
Cadmium
ND
ug/L
1.0
1
12JO1115 19:00
12/05/15 01:30
7440-43-9
Chromium
ND
ug/L
5.0
1
12/01/15 19:00
12IM15 01:30
7440-47-3
Copper
ND
ug/L
5.0
1
12/01/16 19:00
12/05/15 01:30
7440-50-8
Lead
ND
ug/L
5.0
1
12/01/15 19:00
12IM15 01:30
7439-92-1
Nickel
ND
ug/L
5.0
1
12/01/15 19:00
12/05/15 01:30
7440-02-0
Selenium
ND
ug/L
10.0
1
12/01/15 19:00
12/05/15 01:30
7782-49-2
Silver
ND
ug/L
5.0
1
12/01/15 19:00
12/05/15 01:30
7440-22-4
Thallium
ND
ug/L
10.0
1
12/01/15 19:00
12/05/15 01:30
7440-28-0
Zinc
11.3
ug/L
10.0
1
12/01/15 19:00
12/05/15 01:30
7440-6"
245.1 Mercury
Analytical Method: EPA 245.1 Preparation Method: EPA 245.1
Mercury
ND
ug/L
0.20
1
1210411516:30
12/0711512:41
7439-97-6
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthylene
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
208-96-8
Anthracene
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
120-12-7
Benzidine
ND
ug/L
50.0
1
12/01/15 16:40
12/04/15 04:29
92-87-5 L2
Benzo(a)anthracene
ND
ug/L
5.0
1
12JO1115 16:40
12/04/15 04:29
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
12101/1516:40
12/0411504:29
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
1210111516:40
1210411504:29
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
207-08-9
4-Bromophenylphenylether
ND
ug/L
5.0
1
1210111516:40
1210411504:29
101-55-3
Butylbenzylphthaiate
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 04:29
85-68-7
4-Chioro-3-methylphenol
ND
ug/L
5.0
1
121011151&40
1210411504:29
59-50-7
bis(2-Chloroethoxy)methane
N❑
ug1L
10.0
1
1210111516:40
1210411504:29
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
Ill 44 4
bis(2-Chloroisapropyl) ether
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
108-60-1
2-Chloronaphlhalene
ND
ug/L
5.0
1
1210111516:40
1210411504:29
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
121O1/15 16:40
12/04/15 04:29
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
12/0Ill 5 16:40
12/04/15 04:29
7005-72-3
Chrysene
ND
ug/L
5.0
1
12JO1115 16:40
12/04/15 04:29
21"1-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
12JO1115 16:40
12/04/15 04:29
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
12t0l/15 16:40
12/04/15 04:29
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
12/01/15 16:40
12JO4115 04:29
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
12101/15 16:40
12/04/15 04:29
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
12IOIll 5 16:40
12/04/15 04:29
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
12JO1115 16:40
12/04/15 04:29
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
1210111516:40
1210411504:29
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
12/OIll 5 16:40
12/04/15 04:29
534-52-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, inc.. Page 4 of 31

Pace Analytical Services, Inc.
C� /+�1 9800 Kinsey Ave. Suite loo
�+O A+/}� K+�au Huntersville, NC 28078
"'wwxcom [phone]
ANALYTICAL RESULTS
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Sample: Al Lab ID: 92277769001 Collected: 11/30/15 04:00 Received: 11/30/15 14:40 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
625 MSSV
Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrophenol
NO
ug/L
50.0
1
12/01/15 16:40
12/04/15 04:29
51-28-5
2,4-Dinitrotoluene
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.D
1
12/01/15 16:40
12/04/15 04:29
606-20-2
Di-n-octytphthalate
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
117-84-0
1,2-Diphenylhydrazine
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
122-06-7
bis(2-Ethylhexyl)phthalate
ND
ug/L
5.0
1
1VO1115 16:40
12/04/15 04:29
117-81-7
Fluoranthene
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 04:29
206- 4-0
Fluorene
NO
ug/L
5.0
1
12JO1/15 16:40
12/04/15 04:29
86-73-7
Hexachloro-1,3-butadierie
NO
ug/L
5.0
1
1210111516:40
1210411504:29
87-68-3
Hexachlorobenzene
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
118-74-1
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
12/01/15 16:40
12/04/15 04:29
77-47-4
L2
Hexachloroethane
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
67-72-1
L2
Indeno(1,2,3-cd)pyrene
NO
ug1L
5.0
1
12/01/15 16:40
12/0411504:29
193-39-5
Isophorone
NO
ug/L
10.0
1
12101/15 16:40
12/04/15 D4:29
78-59-1
Naphthalene
N❑
ug/L
5.0
1
12/01/15 16:40
12104/15 04:29
91-20-3
Nitrobenzene
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
98-95-3
2-Nilrophenol
NO
ug/L
5.0
1
12/01/15 16AO
12104115 04:29
88-75-5
4-Nilrophenol
ND
ug/L
50.0
1
12/01/15 16:40
12/04/15 04:29
100-02-7
N-Nitrosodimethylamine
NO
ug/L
5.0
1
12/01115 16AO
12/04/15 04:29
62-75-9
N-Nitroso-di-n-propylamine
NO
ug1L
5.0
1
12/01/15 16:40
12/04/15 04:29
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
12/01/15 16:40
12/04/15 04:29
86-30-6
Pentachlorophenot
NO
ug/L
10.0
1
12/01/15 16:40
12/04/15 04:29
87-86-5
Phenanlhrene
NO
uglL
5.0
1
12/01/15 16:40
12/04/15 04:29
85-01-8
Phenol
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
108-95-2
Pyrene
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
129-00-0
1,2,4-Trichlorobenzene
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 04:29
120-82-1
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
12/01/15 16:40
12/04/15 04:29
88-06-2
Surrogates
Nitrobenzene-d5 (S)
19
%
10-120
1
12/01/15 16:40
12/04/15 04:29
4165-60-0
P2
2-Fluorobiphenyl (S)
20
%
15-120
1
12/01/15 16:40
12/04/15 04:29
321-6"
Terphenyl-d14(S)
28
%
it-131
1
12O111516:40
1210411504:29
1718-51-0
Phenol-d6 (S)
4
%
10-120
1
12/01/15 16:40
12/04/15 D4:29
13127-88-3
SO
2-Fluorophenol (S)
4
%
10-120
1
12/01/15 16:40
12/04/15 04:29
367-12-4
SO
2,4,6-Tribromophenol (S)
10
%
10-137
1
12/01/15 16:40
12/04/15 04:29
118-79-6
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
NO
ug/L
5.0
1
12/13/15 02:40
107-02-8
Acrylonitrile
NO
ug/L
50.0
1
12/13/15 02:40
107-13-1
Benzene
NO
ug/L
2.0
1
12/13/15 02:40
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
12/13/15 02:40
75-27-4
Bromoform
NO
ug/L
2.0
1
12/13/15 02:40
75-25-2
Bromomethane
NO
ug/L
2.0
1
12/13/15 02:40
74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
12/13/15 02:40
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
12/13/15 02:40
108-90-7
Chloroethane
NO
ug/L
2.0
1
12/13/15 02:40
75-DD-3
2-Chloroethylvinyl ether
NO
ug/L
5.0
1
12/13/15 02:40
110-75-8
c2
Chloroform
NO
uglL
2.0
1
12/13/15 02:40
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in cull,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 31

I e
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rww ="
ANALYTICAL RESULTS
Pace Anatytkal Servicea, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Sample: Al
Lab ID: 92277769001 Collected: 11/30/15 04:00 Received:
11/30/15 14:40 Matrix: Water
Parameters
Results Units Report Limit
DF Prepared
Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA624
Chloromethane
ND ug1L
2.0
1
12/13/15 02:40
74-87-3
Dibromochloromethane
ND ug/L
2.0
1
12/13/15 02:40
124-48-1
1,2-Dichlorobenzene
ND ug/L
2.0
1
12/13/15 02:40
95-50-1
1,3-Dlchlorobenzene
ND ug/L
2.0
1
12/1311502:40
541-73-1
1,4-Dichlorobenzene
ND ug/L
2.0
1
12/13/15 02:40
106-4fr7
1,1-Dichloroethane
ND ug/L
2.0
1
12/13/15 02:40
75-34-3
1,2-Dichloroetharte
ND ug/L
2.0
1
12/13/15 02:40
107406-2
1,1-Dichloroethene
ND ug/L
2.0
1
12/13/15 02:40
75-35-4
cis-1,2-Dichloroethene
ND ug/L
2.0
1
12/13/15 02:40
156-59-2
trans-1,2-Dichloroethene
ND ug1L
2.0
1
12/13/15 02:40
156-60-5
1,2-Dichloropropane
ND ug1L
2.0
1
12/13/15 02:40
78-87-5
cis-1,3-Dichloropropene
ND ug/L
2.0
1
12/1311502:40
10061-01-5
trans-1,3-Dichloropropene
ND ug1L
2.0
1
12/13/15 02:40
10061-02-6
Ethylbenzene
ND ug/L
2.0
1
12/13115 02A0
100-414
Hexachloro-1,3-butadiene
ND ug/L
5.0
1
12113/15 02A0
87-68-3
Methylene Chloride
ND ug1L
2.0
1
12113/15 02.40
75-09-2
Naphthalene
ND ug/L
5.0
1
12/13/15 02:40
91-20-3
1,1,2,2-Tetrachloroethane
ND ug/L
2.0
1
12/13/15 02:40
79-34-5
Tetrachloroethene
ND ug/L
2.0
1
12/13/15 02:40
127-18-4
Toluene
ND ug/L
2.0
1
12/13115 02:40
108-88-3
1, 1, 1 -Trichloroethane
ND ug/L
2.0
1
12/13/15 02:40
71-55-6
1,1,2-Trichloroethane
ND ug/L
2.0
1
17J13115 02AO
79-00-5
Tdchloroethene
ND ug1L
2.0
1
12/13/15 02:40
79-01-6
Vinyl chloride
ND ug/L
2.0
1
12/13/15 02:40
75-01-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
12/13/15 02:40
460-00-4
Toluene-d8 (S)
103 %
70-130
1
12/13/15 02:40
2037-26-5
1,2-Dichloroethane-d4 (S)
96 %
70-130
1
12/13/15 02:40
17060-07-0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
5.1 mg/L
2.5
1
12/01/15 21:41
4500S20 Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
ND mg/L
0.10
1
1210411516:00
18496-25-8
9040 pH
Analytical Method: EPA 9040
pH
6.3 Sid. Units
0A0
1
12/0111514:35
H6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
ND mg/L
2.0
1
1210111516:59
14808-79-8
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
ND mg1L
0.010
1
1210311519:01
108-95-2
45000NE Cyanide, Total
Analytical Method: SM 4500-CN-E
Cyanide
ND mg/L
0.0080
1
12/02/15 05:35
57-12-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/14/2015 02:07 PM
without the written consent of
Pace Analytical Services, Inc..
Page 6 of 31

CeArWcal"
vwrzpaoelatutcom
ANALYTICAL RESULTS
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pate Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: A2
Parameters
Lab ID: 92277769002 Collected: 11/30/15 04:15
Results Units Report Limit OF
Received: 11/30/15 14:40 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND
mg1L
5.0
1
12/08/15 05:03
200.7 MET ICP
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
Antimony
ND
ug1L
5.0
1
12/01/15 19:00
12/05/15 01:33 7440-36-0
Arsenic
ND
ug/L
10.0
1
12/01/15 19:00
12/05/15 01:33 7440-38-2
Beryllium
ND
ug/L
1.0
1
12/01/15 19:00
12/05/15 01:33 7440-41-7
Cadmium
ND
ug/L
1.0
1
12/01/15 19:00
12/05115 01-33 7440-43-9
Chromium
ND
ug/L
5.0
1
12/01/15 19:00
1210 /15 01:33 7440-47-3
Copper
5.6
ug/L
5.0
1
12/01/15 19:00
12/05/15 01:33 7440-50-8
Lead
ND
ug/L
5.0
1
12/01/15 19:00
12/05/15 01:33 7439-92-1
Nickel
NO
ug/L
5.0
1
12/01/15 19:00
12/05/15 01:33 7440-02-0
Selenium
ND
ug/L
10.0
1
12JO1115 19:00
12/05/15 01:33 7782-49-2
Silver
NO
ug/L
5.0
1
12/01/15 19700
12/05/15 01:33 7440-22-4
Thallium
NO
ug1L
10.0
1
12/01/15 19:00
12/05/15 01:33 7440-28-0
Zinc
21.6
ug/L
10.0
1
12/01/15 19:00
12/05/15 01:33 7440-66-6
245.1 Mercury
Analytical Method: EPA 245.1
Preparation Method: EPA 245.1
Mercury
ND
uglL
0.20
1
12104/1516:30
12/07/1512:43 7430,97-6
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthylene
NO
ug1L
5.0
1
12/01/15 16:40
12/04/15 09:29 208-96-8
Anthracene
NO
ug./L
5.0
1
12/01/15 16740
12/04/15 09:29 120-12-7
Benzidine
NO
ug/L
50.0
1
12/01/15 16:40
12/04/15 09:29 92-87-5 L2
Benzo(a)anthraoene
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 56-55 3
Benzo(a)pyrene
NO
ug1L
5.0
1
12/01/15 16:40
12/04/16 09:29 50-32-8
Benzo(b)fluoranthene
NO
ug/L
5.0
1
12/01/15 15:40
12/04/15 09:29 205-99-2
Benzo(g,h,i)perylene
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 207.08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 85-68-7
4-Chloro-3-methylphenol
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 59-50-7
bis(2-Chlorcethaxy)methane
ND
ug/L
10.0
1
12/01/15 16:40
12/04/15 09:29 111-91-1
bis(2-Chloroethyi) ether
ND
ug1L
5.0
1
12/01/15 16:40
12/04115 09:29 111 44-4
bis(2-Chloroisopropyl) ether
ND
ug/L
5.0
1
12/01/15 16A0
12/04/15 09:29 108-60-1
2-Chloronaphthalene
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 91-58-7
2-Chlorophenol
NO
ug/L
5.0
1
1210Ill 5 16:40
12/04/15 09:29 95-57-8
4-Chlarophenylphenyl ether
NO
ug/L
5.0
1
12101/15 16:40
12/04/15 09:29 7005-72-3
Chrysene
ND
ug/L
5.0
1
12JO1115 16:40
12/04/15 09:29 218-01-9
Dibenz(a,h)anthracene
NO
ug/L
5.0
1
12JO1115 16:40
1210411509:29 53-70-3
3,3'-Dichlorobenzidine
ND
ug1L
25.0
1
12JO1115 16:40
1210411509:29 9i-94-1
2,4-Dichlorophenol
NO
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 120-83-2
Diethylphthalate
NO
ug/L
5.0
1
12/01/15 16A0
12/04/15 09:29 84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
12/01/15 16:40
12/04/15 09:29 105-67-9
Dimethylphthalate
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 09:29 131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29 84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
12/01/15 16:40
12/04/15 09:29 534-52-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1211412015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 31

aceAr�alytical'
www.pacakbamm
ANALYTICAL RESULTS
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 26078
[phone]
Sample: A2 Lab ID: 92277769002 Collected: 11/30/15 04:15 Received: 11/30/15 14:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrototuene
Di-n-octylphthalate
1,2-Diphertylhydrazine
bis(2-Ethythexyl)phthalate
Fluoranthene
Fluorene
Hexachloro- 1, 3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
Naphthalene
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N- NitrosDd imethylamine
N-Nitroso-di-n-propylamine
N- Nitrosod iphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
12,4-Trichlorobenzene
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyt (S)
Terphenyl-cl14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Analytical Method: EPA625 Preparation Method: EPA625
ND
ug[L
50.0
1
12101/1516A0
12104/150929
51-28-5
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29
121-14-2
ND
ug/L
5.0
1
12/01/15 16A0
12/04/15 0929
606-20-2
ND
ug/L
5.0
1
12101/1516:40
1210411509:29
117-84-0
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29
122-66-7
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 09:29
117-81-7
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 09:29
206-44-0
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29
136-73-7
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29
87-68-3
ND
ug/L
5.0
1
12/01/15 16A0
12/04/15 09:29
118-74-1
ND
ug/L
10.0
1
12/01/15 16:40
12/04/15 09:29
77-47-4 L2
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 09:29
67-72-1 L2
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29
193-39-5
ND
ugfL
10.0
1
12/01/15 16:40
12/04/15 09:29
78-59-1
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29
91-20-3
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 09:29
98-95-3
ND
ug/L
5.0
1
12/01/15 16A0
12/04/15 09:29
W75-5
ND
ug/L
50.0
1
12/01/15 16:40
12/04/15 09:29
100-02-7
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 0919
62-75-9
ND
ug1L
5.0
1
12/01/15 16:40
12/04/15 09:29
621-64-7
ND
ug/L
10.0
1
12/01/15 16:40
12/04/15 09:29
86-3D-6
ND
ug/L
10.0
1
12/01/15 16:40
12/04/15 0929
87-86-5
ND
ug/L
5.0
1
12101/1516:40
1210411509:29
85-01-8
ND
ug1L
5.0
1
12/01/15 16:40
12/04115 0919
108-95-2
ND
ug/L
5.0
1
1210111516:40
1210411509:29
129-00-0
ND
ug/L
5.0
1
12/01/15 16:40
12/04/15 09:29
120-82-1
ND
ug/L
10.0
1
12101/1516:40
1210411509:29
88-06-2
40
%
10-120
1
12101/1516:40
1210411509:29
4165-60-0
42
%
15-120
1
12101/1516:40
1210411509:29
321-60-8
49
%
11-131
1
12)01/1516:40
12l0411509:29
1718-51-0
12
%
10-120
1
12/01/15 16A0
12/04/15 09:29
13127-88-3
19
%
10-120
1
12/01/15 16:40
12/04/15 09:29
367-12-4
49
%
10-137
1
12/01/15 16:40
12/04/15 09:29
118-79-6
624 Volatile Organics Analytical Method: EPA 624
Acroiein
ND
ug/L
5.0
1
12/13/15 02:57 107-02-8
Acrylonitrile
ND
ug/L
50.0
1
12/13/15 02:57 107-13-1
Benzene
ND
ug/L
2.0
1
12/13/15 02:57 71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
12/13/15 02:57 75-27-4
Bromotorm
ND
ug/L
2.0
1
12/13/15 02:57 75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/15 02:57 74-83-9
Carbon tetrachloride
ND
ug/L
2.0
1
12/13/15 02:57 56-23-5
Chlorobenzene
ND
uglL
2.0
1
12/13/15 02:57 108-90-7
Chloroethane
ND
uglL
2.0
1
12/13/15 02:57 75-00-3
2-Chloroethylvinyf ether
ND
ug/L
5.0
1
12/13/15 02:57 110-75-8
Chloroform
ND
ug/L
2.0
1
12/13/15 02:57 67-66-3
REPORT OF LABORATORY ANALYSIS
5a
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 31

Ce'il a*
tinrw.pecelabspom
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Sample: A2 Lab ID: 92277769002 Collected: 11/30/15 04:15 Received: 11/30/15 14:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
624 Volatile Organics Analytical Method: EPA 624
Chloromethane
NO
ug/L
2.0
1
12/13/15 02:57
74-87-3
Dibromochloromethane
NO
uglL
2.0
1
12/13/15 02:57
124-48-1
1,2-Dichlorobenzene
NO
ug/L
2.0
1
12113/1502:57
95-50-1
1,3-Dichlorobenzene
ND
ug/L
2.0
1
12/13/15 02:57
541-73-1
1,4-Dichlorobenzene
NO
ug/L
2.0
1
12JI3115 02:57
106-46-7
1,1-Dichloroethane
NO
ug1L
2.0
1
12/13/15 02:57
75-34-3
i,2-Dichlorcelhane
NO
ug/L
2.0
1
12/13/15 02:57
107-06-2
1,1-Dichloroelhene
NO
ug/L
2.0
1
12/13/15 02:57
75-35-4
ds-1,2-Dichlorcethene
ND
ug/L
2.0
1
12/13/15 02:57
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
2.0
1
12/13/15 02:57
156-00-5
1,2-Dichloropropane
ND
ug/L
2.0
1
1211311502:57
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
2.0
1
12/13/15 02:57
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1
1211311502:57
10061-02-6
Ethyibenzene
NO
ug/L
2.0
1
12/13/15 02:57
100414
HexacNoro-1 ,3-butadiene
ND
ug/L
5.0
1
12/13/15 02:57
87-68-3
Methylene Chloride
ND
ug1L
2.0
1
12/13/15 02:57
75-09-2
Naphthalene
ND
ug/L
5.0
1
12/13/15 02:57
91-20-3
1,1,2,2-Tetrachloroethane
ND
ug/L
2.0
1
1211311502:57
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1
12/13/15 02:57
127-184
Toluene
ND
ug/L
2.0
1
12/13/15 02:57
108-88-3
1,1,1-Trichloroethane
ND
uglL
2.0
1
12/13/15 02:57
71-55-6
1,1,2-Trichloroethane
NO
ug/L
2.0
1
12/13tl 5 02:57
79-00-5
Trichloroethene
ND
ug/L
2.0
1
12/13/15 02:57
79-01-6
Vinyl chloride
ND
ug/L
2.0
1
12/13/15 02:57
75-01-4
Surrogafes
4-Bromofluorobenzene (S)
101
%
70-130
1
12/13/15 02:57
460-00-4
Toluene-d8 (S)
109
%
70-130
1
12/13/15 02:57
2037-26-5
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/13/15 02:57
17060-07-0
2540D Total Suspended Solids
Analytical Method:
SM 2540D
Total Suspended Solids
4.8
mg/L
2.5
1
12/01/15 21:41
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
NO
mg/L
0.10
1
12/0411516:00
18496-25-8
9040 pH
Analytical Method: EPA 9040
pH
6.3
Std. Units
0,10
1
12/01/15 14:35
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
ND
mg1L
2.0
1
12/0111516:59
14808-79-8
420.4 Phenolics, Total
Analytical Method: EPA420.4
Phenol ND mg1L 0.010 1 12/0311519:01 108-95-2
45ODCNE Cyanide, Total Analytical Method: SM 4500-CN-E
Cyanide ND mg/L 0.0080 1 12/02/15 05:36 57-12-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc..
H6
Page 9 of 31

CBARa4dcal
��eoelabsopn
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: GCSV23460 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92277769001, 92277769002
METHOD BLANK: 1622023 Matrix: Water
Associated Lab Samples: 92277769001, 92277769002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mgfL ND 5.0 12108I15 04:56
Pace analytical services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2807B
[phone]
LABORATORY CONTROL SAMPLE: 1622024
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Oil and Grease mg/L 40 36.3 91 78-114
MATRIX SPIKE SAMPLE: 1622025
92278186001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L ND 40 35.5 89 78-114
Results presented on this page are In the units Indicated by the "Units" column except where an afternate unit is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 31

ceAna6 tical.
wr�w.pecefa6soom
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: MERP18722 Analysis Method: EPA 245.1
QC Batch Method: EPA 245.1 Analysis Description: 245.1 Mercury
Associated Lab Samples: 92277769001, 92277769002
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
METHOD BLANK: 1619737 Matrix: water
Associated Lab Samples: 92277769001, 92277769002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 12 O7115 12:05
LABORATORY CONTROL SAMPLE: 1619738
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.5 100 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1619739 1619740
MS MSD
92276293001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug1L ND 2.5 2.5 2.7 2.7 106 106 70-130 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1619741 1619742
MS MSD
92277799001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug1L ND 2.5 2.5 2.6 2.6 101 102 7D-130 0
Results presented on this page are In the units indicaW by the "UrdW calumn except where an alternate Lm t Is preserded to the right of the fe5u1L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 31

ceAnalyfical'
www.pscawacom
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: MPRP/20146 Analysis Method: EPA 200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92277769001, 92277769002
METHOD BLANK: 1617573
Associated Lab Samples:
92277769001, 92277769002
Parameter
Units
Antimony
ug/L
Arsenic
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Copper
ug/L
Lead
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Thallium
ug/L
Zinc
ug/L
LABORATORY CONTROL SAMPLE:
1617574
Parameter
Units
Antimony
ug/L
Arsenic
ug1L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Copper
ug/L
Lead
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Thallium
ug/L
Zinc
ug/L
Matrix: Water
Blank
Result
Spike
Conc.
500
500
500
500
500
500
500
500
500
250
500
500
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Analyzed
Qualifiers
5.0
12/05/15 00:28
10.0
1210511500:28
1.0
12/05/15 00:28
1.0
12/05/15 00:28
5.0
12/05/15 00:28
5.0
12/05/15 00:28
5.0
12/05115 0028
5.0
12/05/15 00:28
10.0
12/05/15 0028
5.0
12/05/15 00:28
10.0
12/05/15 00:28
10.0
12/05/16 00:28
LCS
Result
458
436
426
443
430
445
440
441
439
219
446
439
LCS
% Rec
92
87
85
89
86
89
88
88
88
88
89
88
% Rec
Limits
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
85-115
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilte, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1617575
1617576
MS
MSD
92277577002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
413
451
82
90
70-130
9
Arsenic
ug/L
8•6
500
500
398
431
78
85
70-130
8
Beryllium
ug/L
ND
500
500
474
512
95
102
70-130
8
Cadmium
ug/L
ND
500
500
424
459
85
92
70-130
8
Chromium
ug/L
ND
500
500
448
486
89
97
70-130
8
Results presented on this page are in the units indicated by the "UntW column except where an alternate unit Is presented to the right of the resalL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 12 o131

CeAIk?IyhCc�
Wr�w.paoetabamm
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2807B
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1617575
MS
92277577002 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
1617576
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Copper
ug/L
ND
500
500
442
477
88
95
70-130
8
Lead
ug/L
ND
500
500
405
439
81
87
70-130
8
Nickel
ug/L
ND
500
500
421
457
84
91
70-130
8
Selenium
ug/L
ND
500
500
400
429
80
85
70-130
7
Silver
ug/L
ND
250
250
217
234
87
94
70-130
8
Thallium
ug/L
ND
500
500
410
460
82
92
70-130
11
Zinc
ug/L
49.7
500
500
446
481
79
86
70-130
8
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1617577
1617578
MS
MSD
92277707006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cane.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
459
465
92
93
70-130
1
Arsenic
u91L
ND
5D0
500
442
443
88
88
70-130
0
Beryllium
ug/L
ND
500
500
516
522
103
104
70-130
1
Cadmium
ug1L
ND
500
500
468
474
94
95
70-130
1
Chromium
ug/L
ND
500
500
492
500
98
99
70-130
2
Copper
ug/L
6.8
500
500
493
500
97
99
70-130
1
Lead
ug/L
ND
500
500
449
454
90
91
70-130
1
Nickel
ug/L
7.8
500
500
468
473
92
93
70-130
1
Selenium
ug/L
ND
500
500
442
448
88
90
70-130
1
Silver
ug/L
ND
250
250
237
242
94
96
70-130
2
Thallium
ug/L
ND
500
500
452
467
90
93
70-130
3
Zinc
ug/L
31.8
500
500
478
482
89
90
70-130
1
Results presented on this page are In We unks indicated by the 9tnIN' column except where an aftenu to unit is presented to the rlgbt of the remIL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 31

CeARalyticale
www.paaelebacom
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: MSV/34667
Analysis Method: EPA 624
QC Batch Method: EPA 624
Analysis Description: 624 MSV
Associated Lab Samples: 92277769001, 92277769002
METHOD BLANK: 1627867
Matrix:
Water
Associated Lab Samples: 92277769001, 92277769002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
ND
2.0
12/12/1513:19
1,1,2,2-Tetrachioroethane
ug1L
ND
2.0
1211211513:19
1,1,2-Trichloroethane
ug/L
ND
2.0
1211211513:19
1,1-Dichloroethane
ug/L
ND
2.0
1211211513:19
1,1-Dichloroethene
ug1L
ND
2.0
1211211513:19
1,2-Dichlorobenzene
ug1L
ND
2.0
12/12/15 13:19
1,2-Dichloroethane
ug/L
ND
2.0
12MV1513:19
1,2-Dichloropropane
uglL
ND
2.0
12112/1513:19
1.3-Dichlorobenzene
ug/L
ND
2.0
1211211513:19
1,4-Dichlorobenzene
uglL
ND
2.0
1211211513:19
2-Chloroethylvinyl ether
ug/L
ND
5.0
12112/15 13:19
Acrolein
ug/L
ND
5.0
12/12/15 13:19
Acrylonitrile
ug/L
ND
50.0
12112/1513:19
Benzene
ug1L
ND
2.0
12/12/15 13:19
Bromodichloromethane
ug/L
ND
2.0
12/12/15 13:19
Bromoform
ug/L
ND
2.0
12/12/15 13:19
Bromomethane
ug1L
ND
2.0
12/12/1513:19
Carbon tetrachloride
ug/L
ND
2.0
12/12/15 13:19
Chlorobenzene
ug/L
ND
2.0
12112/1513:19
Chloroethane
ug/L
ND
2.0
1211211513:19
Chloroform
ug/L
ND
2.0
12/12/1513:19
Chloromethane
ug/L
ND
2.0
12/1211513:19
cis-1,2-Dichloroethene
ug/L
ND
2.0
12/12/15 13:19
cis-1,3-Dichloropropene
ug/L
ND
2.0
12/12/1513:19
Dibromochloromethane
ug/L
ND
2.0
12/1211513:19
Ethylbenzene
ug/L
ND
2.0
112/12M513:19
Hexachloro-1,3-butadiene
ug/L
ND
5.0
12/12115 13:19
Methylene Chloride
ug/L
ND
2.0
12/12/15 13719
Naphthalene
ug/L
ND
5.0
1211211513:19
Tetrachloroethene
ug/L
ND
2.0
1211211513:19
Toluene
ug/L
ND
2.0
1211211513:19
trans-1,2-Dichloroethene
ug/L
ND
2.0
1211211513:19
trans-1,3-Dichloropropene
ug/L
ND
2.0
1211211513:19
Trichforoethene
ug/L
ND
2.0
1211211513:19
Vinyl chloride
ug1L
ND
2.0
12/12/15 13:19
1,2-Dichloroethane-d4 (S)
%
92
70-130
12/12/15 13:19
4-Bromofluorobenzene (S)
%
102
70-130
12/12/15 13:19
Toluene-d8 (S)
%
103
70-130
12/12/15 13:19
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
(7(34)875-9092
Results presented on trds page are in the units Indicated by the "Units" column except where an alternate unit is presented to am rkgM of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 31

ceAna&tica1
www.pataiab.=Corn
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
LABORATORY CONTROL SAMPLE: 16227868
Parameter
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
1, 1, 1 -Trichloroethane
ug1L
20
17.7
88
52-162
1,1,2,2-Tetrachloroetharte
ug1L
20
18.2
91
46-157
1,1,2-Trichloroethane
ug/L
20
16.7
84
52-150
1,1-Dichloroethane
ug1L
20
16.6
83
59-155
1,1-Dichloroethene
ug1L
20
17.7
89
1-234
1,2-Dichlorobenzene
uglL
20
19.0
95
18-190
1,2-Dichloroethane
ug/L
20
16.2
81
49-155
1,2-Dichloropropane
ug/L
20
17.5
88
1-210
1,3-Dichlorobenzene
ug/L
20
19.2
96
59-156
1,4-Dichlorobenzene
ug/L
20
18.4
92
18-190
2-Chloroethyivinyt ether
ug/L
40
36.0
90
1-305
Acrolein
ug/L
100
89.6
90
15-152
Acrylonitrile
ug/L
100
88.8
89
75-132
Benzene
ug/L
20
18.6
93
37-151
Bromodichloromethane
ug/L
20
17.7
89
35-155
Bromoform
ug/L
20
13.5
67
45-169
Brornomethane
ug/L
20
9.9
49
1-242
Carbon tetrachloride
ug/L
20
18.1
90
70-140
Chlorobenzene
ug1L
20
18.7
93
37-160
Chloroethane
ug1L
20
12.6
63
14-230
Chloroform
ug/L
20
18.2
91
51-138
Chloromethane
ug1L
20
14.1
70
1-273
cis-1,2-Dichloroethene
ug/L
20
17.7
88
68-146
cis-1,3-Dichloropropene
uglL
20
17.3
86
1-227
Dibromochloromethane
ug/L
20
16.1
80
53-149
Ethylbenzene
ug1L
20
18.3
92
37-162
Hexachloro-1,3-butadiene
ug/L
20
19.5
97
70-130
Methylene Chloride
ug/L
20
15.4
77
1-221
Naphthalene
ug/L
20
18.6
93
70-130
Tetrachloroethene
ug1L
20
18.0
90
64-148
Toluene
ug/L
20
17.9
90
47-150
trans- 1, 2-Dichloroethene
ug/L
20
17.9
90
54-156
trans-1,3-Dichloropropene
ug1L
20
16.1
81
17-183
Trichloroethene
ug1L
20
18.4
92
71-157
Vinyl chloride
ug/L
20
18.7
93
1-251
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
98
7D-130
Toluene-d8 (S)
%
102
70-130
Pace Ana"cal Services, Inc.
9800 ICincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are In the units Indicated by the 91nIts- column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in futi,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 31

ceArWbal e
�vw.pecefab:�om
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: OEXT139417
QC Batch Method: EPA625
Associated Lab Samples: 92277769001, 92277769002
Analysis Method:
Analysis Description:
EPA 625
625 MSS
METHOD BLANK: 1618490
Matrix: Water
Associated Lab Samples: 92277769001, 92277769002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/L
NO
5.0
12/03/1522:04
1,2-Diphenylhydrazine
ug1L
NO
5.0
12/03/15 22:04
2AG-Trichlorophenol
ug/L
ND
10.0
12/03/15 22:04
2,4-Dichlorophenot
ug/L
NO
5.0
12/03/15 22:04
2,4-Dimethylphenol
ug/L
NO
%0
12/03/15 22:04
2,4-Dinitrophenol
ug1L
NO
50.0
12/03/15 22:04
2,4-Dinitrotoluene
ug1L
NO
5.0
12/03/15 22:04
2,6-Dinitrotoluene
ug1L
NO
5.0
12/03/15 22:04
2-Chloronaphthaiene
uglL
NO
5.0
12/03/15 22:04
2-Chlorophenol
ug1L
ND
5.0
12/03/15 22:04
2-Nilrophenol
ug/L
NO
5.0
12/03/15 22:04
3,3'-Dichlorobenzidine
ug/L
ND
25.0
12/0311522:04
4,6-Dinitro-2-methylphenol
ug/L
ND
20.0
12/0311522:04
4-Bromophenylphenyi ether
ug1L
NO
5.0
12103/15 22:04
4-Chloro-3-methylphenol
ug/L
ND
5.0
12/03/15 22:04
4-Chlorophenylphenyt ether
ug1L
ND
5.0
12/03/15 22:04
4-Nitrophenol
ug1L
ND
50.0
12/03/15 22:04
Acenaphthylene
ug1L
ND
5.0
12/03/15 22:04
Anthracene
uglL
NO
5.0
12/03/15 22:04
Benzidine
ug/L
NO
50.0
12103/1522:04
Benzo(a)anthracene
ug/L
ND
5.0
12/03/15 22:04
Benzo(a)pyrene
ug/L
ND
5.0
12103/15 22:04
Benzo(b)fluoranthene
ug1L
ND
5.0
12/03/15 22:04
Benzo(g,h,i)perylene
ug/L
NO
5.0
12/03/15 22:04
Benzo(b)fluoranthene
ug/L
NO
5.0
12/03/15 22:04
bis(2-Chloroethoxy)methane
ug1L
ND
10.0
12/03/15 22:04
bis(2-Chloroethyl) ether
ug/L
ND
5.0
12/03/15 22:04
bis(2-Chlorotsopropyl) ether
ug1L
ND
5.0
12/03/15 22:04
bis(2-Ethylhexyl)phthalate
ug1L
ND
5.0
12/0311522:04
Butylbenzylphthalale
ug/L
ND
5.0
12/03/15 22:04
Chrysene
ug/L
ND
5.0
12/03/15 22:04
Di-n-butylphthalate
ug1L
NO
5.0
12/03/15 22:04
Di-n-octytphthalate
ug/L
ND
5.0
12/03/15 22:04
Dibenz(a,h)anthracene
ug/L
ND
5.0
12/03115 22:04
Diethylphthalate
ug1L
NO
5.0
12/03/15 22:04
Dimethylphthalate
ug/L
NO
5.0
12/03/15 22:04
Fluoranthene
ug/L
NO
5.0
12/03/15 22:04
Fluorene
ug/L
NO
5.0
12/03/15 22:04
Hexachloro-1,3-butadiene
uglL
NO
5.0
12/03/1522:04
Hexachlorobenzene
ug/L
NO
5.0
12/03/15 22:04
Hexachlorocyclopentadiene
ug/L
NO
10.0
12/03115 22:04
Results presented on this page are in the units indicated by the "UNts" column except where an attemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 31

CeAnalyffcal
wrrv.pasadabsmrrt
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace Analytical Services, Inc.
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1618490
Matrix: Water
Associated Lab Samples: 92277769001, 92277769002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Hexachloroethane
ug1L
ND
5.0
12/03/15 22:04
Indeno(1,2,3-cd)pyrene
ug1L
ND
5.0
12/03/15 22:04
Isophorone
ug1L
ND
10.0
12/03/15 22:04
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
12/03/15 22:04
N-Nitrosodimethyiamine
ug1L
ND
5.0
12/03/15 22:04
N-Nitrosodiphenylamine
ug1L
ND
10.0
12/03/15 22:04
Naphthalene
ug/L
ND
5.0
12/03/15 22:04
Nitrobenzene
uglL
ND
5.0
12 O3115 22:04
Pentachlorophenol
ug1L
ND
10.0
12/03/15 22:04
Phenanthrene
ug/L
ND
5.0
12/03/15 22:04
Phenol
uglL
ND
5.0
12/03/15 22:04
Pyrene
ug1L
ND
5.0
12 O3115 22:04
2,4,6-Tribromophenol (S)
%
61
10-137
12/03/15 22:04
2-Fluorobiphenyl (S)
%
44
15-120
12/03/15 22:04
2-Fluorophenol(S)
%
23
10-120
12/03/15 22:04
Nitrobenzene-d5 (S)
%
48
10-120
12/03/15 22.04
Phenol-d6 (S)
%
17
10-120
12/03/15 22:04
Terphenyl-d14 (S)
%
74
11-131
12/03/15 22:04
LABORATORY CONTROL SAMPLE:
1618491
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result % Rec Limits
Qualifiers
1,24-Trichlorobenzene
ug1L
50
23.1
46
44-142
1,2-Diphenythydrazine
ug1L
50
34.6
59
25-150
2,4,6-Trichlorophenol
ug1L
50
32.8
66
37-144
2,4-Dichlorophenol
ug1L
50
28.4
57
1-191
2,4-Dimethylphenol
ug1L
50
25.1
50
32-119
2,4-Dinitrophenol
ug1L
250
42.BJ
17
1-181
2,4-Dinitrotoluene
ug/L
50
35.0
70
39-139
2,6-Dinitrotoluene
ug1L
50
34.2
68
50-158
2-Chloronaphthalene
ug/L
50
31.0
fit
60-118
2-Chlorophenol
ug/L
50
27.0
54
23-134
2-Nitrophenol
ug1L
50
25.4
51
29-182
3,3'-Dichlorobenzidine
ug1L
100
72.9
73
1-262
4,6-Dinitro-2-methytphenol
ug1L
100
22.5
23
1-181
4-Bromophenylphenyl ether
ug1L
50
33.7
67
53-127
4-Chloro-3-methylphenol
ugfL
100
56.4
56
22-147
4-Chlorophenylphenyl ether
ug1L
50
30.6
61
25-158
4-Nitrophenol
ug1L
250
75.6
30
1-132
Acenaphthylene
ug/L
50
35A
71
33-145
Anthracene
ug/L
50
40.4
81
1-166
Benzidine
ug/L
100
6.6.1
7
25-150 LO
Benzo(a)anthracene
ug1L
50
39.5
79
33-143
Benzo(a)pyrene
ug1L
50
39.5
79
17-163
Results presented on this page are In the units Indicated by the "Units' column except where an alienate unit IS presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 31

Cieil`1rWcal e
WWW'Pacelab&own
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
LABORATORY CONTROL SAMPLE: 1618491
Pace Analytical Services, Inc.
9800 Kincey Ave. Sufte 100
Huntersville, NC 28078
(704)875r9092
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(b)fluoranthene
ug/L
50
37.1
74
24-159
Senzo(g,h,i)perylene
ug/L
50
34.8
70
1-219
Benzo(k)fluoranthene
ug/L
50
48.2
96
11-162
bis(2-Chloroethoxy)melhane
ug/L
50
24.2
48
33-184
bis(2-Chloroethyl) ether
ug/L
50
25.6
51
12-158
bis(2-Chloroisopropyl) ether
ug/L
50
21.5
43
36-166
bis(2-Ethylhexyl)phthaiate
ug/L
50
48.5
97
8-158
Butylbenzylphthalate
ug/L
50
50.0
100
1-152
Chrysene
uglL
50
39.6
79
17-168
Di-n-butylphthalate
ug/L
50
45.0
90
1-118
Di-n-octylphthalate
ug1L
50
46.3
93
4-146
Dibenz(a,h)anthracene
ug/L
50
35.0
70
1-227
Diethylphthalate
uglL
50
38.2
76
1-114
Dimethylphthalate
ug/L
50
36.2
72
1-112
Fluoranthene
uglL
50
41.1
82
26-137
Fluorene
uglL
50
36.9
74
59-121
Hexachloro-1,3-butadiene
uglL
50
22.0
44
24-116
Hexachlorobenzene
ug/L
50
39A
78
1-152
Hexachlorocyclopentadiene
ug/L
50
5.61
11
25-150 LO
Hexachloroethane
ug/L
50
19.3
39
40-113 LO
Indeno(1,2,3-cd)pyrene
ug/L
50
34.9
70
1-171
Isophorone
ug/L
50
26.9
54
21-196
N-Nitroso-di-n-propylamine
ug/L
50
28.1
56
1-230
N-Nitrosodimethylamine
ug/L
50
15.9
32
25-150
N-Nitrosodiphenylamine
ug/L
50
35.7
71
25-150
Naphthalene
ug/L
50
24.9
50
21-133
Nitrobenzene
ug/L
50
24.8
50
35-180
Pentachlorophenol
ug/L
100
62.4
62
14-176
Phenanthrene
ug/L
50
36.7
73
54-120
Phenol
ug/L
50
12A
25
5-112
Pyrene
ug/L
50
43.3
87
52-115
2,4,6-Tribromophenol (S)
%
76
10-137
2-Fluorobiphenyl (S)
%
60
15-120
2-Fluorophenol(S)
%
33
10-120
Nitrobenzene-d5 (S)
%
52
10-120
Phenol-d6 (S)
%
22
10-120
Terphenyl-dl4 (S)
%
78
11-131
MATRIX SPIKE SAMPLE:
1618492
^
92277684002 Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND 50
27.7
55
44-142
1,2-Diphenylhydrazine
ug/L
ND 50
33.1
66
25-150
2,4,6-Trichlorophenol
ug/L
ND 50
31.9
64
37-144
2,4-Dichlorophenol
ug/L
ND 50
28.8
58
1-191
Results presented on this page are in the units indicated by the "Unit:" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 31

CeAnalybcal
Mnrw.pa�abs.mm
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace Analytical Services, Inc.
9800 K incey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1618492
Units
92277684002
Result
Spike
Conc.
MS
Result
M5
% Rec
% Rec
Limits Qualifiers
2,4-Dimethylphenol
uglL
ND
50
4.8J
4
32-119 M1
2,4-Dinitrophenol
ugfL
NO
250
82.8
33
1-181
2,4-Dinitrotoluene
ug/L
NO
50
37.4
75
39-139
2,6-Dinitrotoluene
ug/L
NO
50
36.0
72
50-158
2-Chloronaphthalene
ug/L
ND
50
32.8
66
60-118
2-Chlorophenol
ugfL
ND
50
27.7
55
23-134
2-Nitrophenol
ug/L
NO
50
30.0
60
29-182
3,3'-Dichlorobenzidine
ugfL
NO
100
ND
0
1-262 M1
4,6-Dinitro-2-me#g1phenol
ug/L
NO
100
36.5
35
1-181
4-Bromophenylphenyl ether
ugfL
NO
50
33.0
66
53-127
4-Chloro-3-methylphenol
ug/L
ND
100
52.8
53
22-147
4-Chlorophenylphenyl ether
ug/L
ND
50
31.2
62
25-158
4-Nitrophenol
ug/L
ND
250
103
41
1-132
Acenaphthylene
ug/L
NO
50
32.4
65
33-145
Anlhracene
ug/L
NO
50
29A
59
1-166
Benzidine
ug/L
NO
100
NO
0
25-150 MO
Benzo(a)anthracene
ug/L
NO
50
37.4
75
33-143
Benzo(a)pyrene
ug/L
NO
50
25.1
50
17-163
Benzo(b)fluoranthene
ugfL
NO
50
39.5
79
24-159
Benzo(g,h,i)peg1ene
ug/L
NO
50
35.2
70
1-219
Benzo(k)fluoranthene
ug/L
NO
50
51.3
103
11-162
bis(2-Chloroethoxy)methane
ug/L
ND
50
27.8
56
33-184
bis(2-Chloroethyl) ether
ug/L
ND
50
25.7
51
12-158
bis(2-Chlorcisopropyl) ether
ug1L
ND
50
23.0
46
36-166
bis(2-Ethylhexyl)phthalate
ugfL
ND
50
45.4
91
8-158
Butylbenzylphthalate
ug/L
NO
50
46.7
93
1-152
Chrysene
ug/L
ND
50
39.7
79
17-168
Di-n-butylphthalate
ug/L
NO
50
46.5
93
1-118
Di-n-octylphthalate
ug/L
NO
50
45.6
91
4-146
Dibenz(a,h)anthracene
ug/L
NO
50
36.8
74
1-227
Diethylphthalate
ugfL
NO
50
37.5
75
1-114
Dimethylphthalate
ug/L
NO
50
35.3
71
1-112
Fluoranthene
ug/L
NO
50
46.2
92
26-137
Fluorene
ugfL
NO
50
38.0
76
59-121
Hexachloro-1,3-butadiene
ug/L
NO
50
27.8
56
24-116
Hexachlorobenzene
ug/L
ND
50
38.2
76
1-152
Hexachlorocyclopentadiene
ug/L
ND
50
12.7
25
25-150
Hexachloroethane
ug/L
ND
50
31.7
63
40-113
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
36.5
73
1-171
Isophorone
ug/L
ND
50
26.1
52
21-196
N-Nitroso-di-n-prapylamine
ugfL
ND
50
27.6
55
1-230
N-Nitrosodimethylamine
ug1L
ND
50
18.0
35
25-150
N-Nitrosodiphenylamine
ug/L
ND
50
28.8
58
25-150
Naphthalene
ug/L
39.0
50
64.3
51
21-133
Nitrobenzene
ug/L
ND
50
54.4
109
35-180
Pentachlorophenol
ug/L
ND
100
68.9
69
14-176
Phenanthrene
ug/L
ND
50
37.2
74
54-120
Results presented on this page are in the units indicated by the "Units- column except where an alternate unit Is presented to the right or the resulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 31

ceArWcal
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Project: 3rd Floor Men's Room
Pace Project No.: 92277769
MATRIX SPIKE SAMPLE: 1618492
Parameter
Units
Phenol
uglL
Pyrene
ug/L
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol(S)
%
Nitrobenzene-d5 (S)
%
Phenoi-d6 (S)
%
Terphenyl-d14 (S)
%
QUALITY CONTROL DATA
92277684002 Spike MS MS
Result Conc. Result % Rec
NO 50 13.2
NO 50 39.6
SAMPLE DUPLICATE: 1618493
Parameter
Units
92277685002
Result
1,2,4-Trichlorobenzene
ug/L
<0.98
1,2-Diphenylhydrazine
ug/L
<0.90
2,445-Trichlorophenol
ug/L
<1.3
2,4-Dichlorophenol
uglL
<i.7
2,4-Dimethylphenol
ug/L
<i.2
2,4-Dinitrophenol
ug/L
<9.0
2,4-Dinitrotoluene
ug/L
<0.90
2,6-Dinitrotoluene
ug1L
<0.98
2-Chloronaphthalene
ug/L
<0.98
2-Chlorophenol
ug/L
<1.3
2-Nitrophenol
ug/L
<0.91
3,3'-Dichlorobenzidine
ug/L
<2.1
4,6-Dinitro-2-methylphenol
ug/L
<2.6
4-Bromophenylphenyl ether
ug/L
<0.82
4-Chloro-3-methylphenol
ug/L
<3.7
4-Chlarophenyiphenyl ether
ug/L
<0.87
4-Nitrophenol
ug/L
<4.1
Acenaphthylene
ug/L
<0.21
Anthracene
ug/L
<0.14
Benzidine
ug/L
<5.1
Benzo(a)anthracene
ug/L
<0.33
Benzo(a)pyrene
ug/L
<0.30
Benzo(b)fluoranthene
ug/L
<0.28
Benzo(g,h,i)perylene
ug1L
<0.38
Benzo(k)fluoranthene
ug/L
<0.43
bis(2-Chloroethoxy)methane
ug/L
<0.92
bis(2-Chloroethyl) ether
ug/L
<1.0
bis(2-Chloroisopropyl) ether
ug/L
<0.95
bis(2-Ethylhexyl)phthalate
ug/L
1.51
Butylbenzylphthalate
ug/L
<0.79
Chrysene
ug/L
<0.21
Di-n-butylphthalate
ug/L
<0.75
Di-n-octylphthalate
ug/L
<0.66
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
26
5-112
79
52-115
70
10-137
61
15-120
33
10-120
54
10-120
23
10-120
58
11-131
Dup
Result RPD Qualifiers
NO
NO
NO
ND
NO
NO
NO
NO
ND
ND
NO
NO
ND
ND
N❑
ND
NO
ND
ND
ND
ND
ND
NO
NO
NO
ND
NO
NO
4J
NO
ND
NO
NO
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This repon shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 31

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QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
SAMPLE DUPLICATE: 1618493
Parameter
Units
92277685002
Result
Dup
Result
Dibenz(a,h)anthracene
uglL
<0.55
ND
Diethylphthalate
ug/L
<0.58
ND
Dimethylphthalate
uglL
<0.76
ND
Fluoranthene
uglL
<0.21
ND
Fluorene
uglL
<0.21
ND
Hexachloro-1,3-butadiene
ug/L
<0.94
ND
Hexachlorobenzene
ug/L
<0.72
ND
Hexachlorocyclopentadiene
ugfL
<0.88
ND
Hexachloroethane
ug/L
<1.1
ND
Indeno(1,2,3-cd)pyrene
ug/L
<0.29
ND
Isophorone
ug/L
<0.89
ND
N-Nitroso-di-n-propylamine
ug/L
<0.99
ND
N-Nitrosodimethylamine
ug/L
<0.91
ND
N-Nitrosodiphenylamine,
ug/L
<1.0
ND
Naphthalene
ug/L
<0.34
ND
Nitrobenzene
uglL
<1.1
ND
Pentachlorophenol
ug/L
<4.6
ND
Phenanthrene
ug/L
<0.22
ND
Phenol
ug/L
<1.9
ND
Pyrene
ug/L
<0.19
ND
2,4,6-Tribromophenol (S)
%
85
90
2-Fluorobiphenyt (S)
%
64
79
2-Fiuorophenol (S)
%
30
37
Nitrobenzene-d5 (S)
%
64
74
Phenol-d6 (S)
%
20
24
Terphenyl-dl4 (S)
%
90
93
RPD Qualifiers
5
22
22
14
18
2
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on tlrrs page are in the units Indicated by the "Untis" column except where an alternate unit Is Presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduoed, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc..
Page 21 of 31

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wrxpsoelabsCam
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: WET/41681
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92277769001, 92277769002
METHOD BLANK: 1617684
Matrix: Water
Associated Lab Samples: 92277769001,
92277769002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 12/01/15 21:37
LABORATORY CONTROL SAMPLE:
1617685
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 246
98 90-110
SAMPLE DUPLICATE: 1617686
92277758001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND ND
SAMPLE DUPLICATE: 1617687
92277791001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L ND ND
Results presented on this page are In the units indicated by the "Units" cdumn except where an altematp unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 22 of 31

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wwwpacetaba mm
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: WET/41752
QC Batch Method: SM 4500-S2D
Associated Lab Samples: 92277769001, 92277769002
METHOD BLANK: 1620479
Associated Lab Samples: 92277769001, 92277769002
Parameter Units
Sulfide mg/L
LABORATORY CONTROL SAMPLE: 162MO
Parameter Units
Sulfide rng/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 14D
Huntersville, NC 28078
(704)8759092
QUALITY CONTROL DATA
Analysis Method: SM 4500-S2D
Analysis Description: 4500S2D Sulfide Water
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 17/0411516:00
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.5 0.49 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1620481 1620482
MS MSD
92277769001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/L ND .5 .5 0.48 0.48 96 96 90-110 0
Results presented on this page are in the units Indicated by the'UnW colurnn except where an a ftenu a unit is presented to the ngtn of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12J14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc..
Page 23 of 31

ceAnalyftal
rr�tvw.pacsfabi.can
QUALITY CONTROL DATA
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: WETI41665 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH
Associated Lab Samples: 92277769001, 92277769002
SAMPLE DUPLICATE: 1616856
92277222002
Dup
Parameter
Units
Result
Result RPD Qualifiers
PH
Std. Units
8.0
8.0 0 H6
SAMPLE DUPLICATE: 1616858
92277769002
Dup
Parameter
Units
Result
Result RPD Qualifiers
pH
Std. Units
6.3
6.3 0 H6
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the untla Indicated by the "Units" column except where an aftervte unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Date: 12l1412015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 24 of 31

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QUALITY CONTROL DATA
Project: 3rd Floor Meri s Room
Pace Project No.: 92277769
QC Balch: WETA125593 Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92277769001, 92277769002
Pace Anaiylical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1617400
Matrix: Water
Associated Lab Samples: 92277769001. 92277769002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Sulfate
mglL
ND 2.0
1210111515:59
LABORATORY CONTROL SAMPLE:
1617401
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Sulfate
mg1L
20 20.6
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1617402 1617403
MS MSD
92277478001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Sulfate mglL ND 20 20 20A 20.0 98 98 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1617404 1617405
MS MSD
92277478002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Quat
Sulfate mg/L 5.2 20 20 25.4 25.9 101 103 90-110 2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result_
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc..
Page 25 of 31

CB�i� e
www.pacde6a com
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: WETA125614
QC Batch Method: EPA420.4
Associated Lab Samples: 92277769001. 92277769002
METHOD BLANK: 1618673
Associated Lab Samples: 92277769001, 92277769002
Parameter Units
Phenol mg/L
LABORATORY CONTROL SAMPLE: 1618674
Parameter Units
Phenol mg1L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
QUALITY CONTROL DATA
Analysis Method: EPA 420A
Analysis Description: 420.4 Phenolics
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.010 12/03/15 18:30
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
.05 0.049 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1618675
MS
92277023003 Spike
Parameter Units Result Conc.
Phenol mglL ND .05
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1618677
MS
92277023004 Spike
Parameter Units Result Cone.
Phenol mg1L ND .05
1618676
MSD
Spike MS MSD MS MSD % Rec
Cone. Result Result % Rec % Rec Limits RPD
.05 0.055 0.055 91 91 90-110 1
1618678
MSD
Spike MS MSD MS MSD % Rec
Cone, Result Result % Rec % Rec Limits RPD
.05 0.055 0.055 94 93 90-110 1
Results presented on this page are in the units indicated by the "units" column except where an alurnate unit is presented to the right of the reault.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 26 of 31

ceAirWca!s
uww.pacpfe6amm
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
QC Batch: WETA125591
QC Batch Method: SM 4500-CN-E
Associated Lab Samples: 92277769001, 92277769002
METHOD BLANK: 1617390
Associated Lab Samples: 92277769001, 92277769002
Parameter Units
Cyanide mg/L
LABORATORY CONTROL SAMPLE: 1617391
Parameter Units
Cyanide mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 4500-CN-E
Analysis Description: 450OCNE Cyanide, Total
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0080 12IO2I15 05:25
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
.1 0.089 89 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1617392 1617393
MS MSD
92277623001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD Qual
Cyanide mg/L ND .1 .1 0.068 0.077 65 74 75-125 13 M1,R1
Results presented on this page are In the units Indicated by the "Units' column except where an aRernate unit is pm"rrted to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1211412015 02:07 PM without the written consent of Pace Analytical Services, Inc..
Page 27 of 31

Pace Analytical Services, Inc.
cepA/}'� /+'l� 9800KinceyAve. Suite100
tl rs+l�[1G� Huntersville, NC 2B078
W's'p°0aIbbe com [phone]
QUALIFIERS
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated Concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anatytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
L0 Anatyte recovery in the laboratory control sample (LCS) was outside QC limits.
L2 Anatyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P2 Re -extraction or re -analysis Could not be performed due to insufficient sample amount.
R1 RPD value was outside control limits.
So Surrogate recovery outside laboratory control limits.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyf ether.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/14/2015 02:07 PM without the written consent of Pace Analytical Services, Inc.. Page 28 of 31

ceA�alytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 3rd Floor Men's Room
Pace Project No.: 92277769
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92277769001
Al
EPA 1664E
GCSV/23460
92277769002
A2
EPA 1664E
GCSV/23460
92277769001
Al
EPA 2007
MPRPI20146
EPA 200.7
92277769002
A2
EPA 200.7
MPRP120146
EPA 200.7
92277769001
Al
EPA 245.1
MERP18722
EPA 245A
92277769002
A2
EPA 245.1
MERPI8722
EPA 245.1
92277769001
Al
EPA 625
0EXT/39417
EPA 625
92277769002
A2
EPA 625
0EXT/39417
EPA 625
922TT769001
Al
EPA 624
MSVI34667
92277769002
A2
EPA 624
MSVI34667
922T7769001
Al
SM 2540D
WET/41681
92277769002
A2
SM 2540D
WET/41681
92277769001
Al
SM 4500-S2D
WET/41752
92277769002
A2
SM 4500-S2D
WET/41752
92277769001
Al
EPA 9040
WET/41665
92277769002
A2
EPA 9040
WET141665
92277769001
Al
EPA 300.0
WETAJ25593
92277769002
A2
EPA 300.0
WETAJ25593
92277769001
Al
EPA420.4
WETA/25614
M77769002
A2
EPA420.4
WETA/25614
92277769001
Al
SM 4500-CN-E
WETA125591
97277769002
A2
SM 4500-CN-E
WETA/25591
Date: 12/14/2015 02:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/18174
ICP/18174
MERC/8383
MERC/8383
MSSV/11595
MSSV/11596
Page 29 of 31

MkaVkal
f
uocumenc tvame:
Condition upon Receil
Document Number:
F-C HR-CS-003-rev.16
LJUUUI I ICI II T%VV I1CU. I9Iay Iu,
Page 1 of 2"
Issuing Authority:
Pace Huntersville Quality Office
Client Name: 1 , r ,tom. t. i17. �L(;, k a , I �,-� c ' Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed E)o UPC] USP❑ Clieri� CommerdaC] Pace Other O tional'.• i' •. = fi
Custody Seal on CoolerBox Present: ❑ es (o ` Seals intact: y ❑ ProJ'Dtie, ate
Y ❑ ,� ❑ es no
�!
Packing Material: ❑Bubble Wrap ❑ (Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1402 Type of Ice: 6()\t Blue None Samples on ice, cooling process has begun
TemD Correction Factor T1402 No Correction
Corrected Cooler Temp.: �"? •C
Temp should be above freezing to 61C
Biological Tissue Is Frozen: Yes No W�A
Comments:
Date and Initials gf person examining
contents: i H 11,1 ,rA_
Chain of Custody Present:
es.❑No
❑wA
1.
Chain of Custody Filled Out;
94 ON,
❑wA
2.
Chain of Custody Relinquished:
YW ONO
❑wA
3.
Sampler Name & Signature on COG:
❑No
❑wA
4.
Samples Arrived within Hold Time:
❑No
DMA
5.
Short Hold Time Analysis 472h ;
es ONO /©wA
6.
Rush Turn Around Time Requested:
❑Ye; 0 0
❑wA
7.
Sufficient Volume:
es ONO
❑wA
8.
Correct Containers Used:
-Pace Containers Used:
IY ONO
ONO
❑wA
❑wA
9.
Containers Intact:
Yea ON,
❑N X
10.
Filtered volume received for Dissolved tests
❑Y No
CINZA
I 11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
M4es ONO
L�
❑NJA
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
excepitons: VOA, cotlrorm, MC, O&G, W-DRO (water}
EI'Ye3 ONO
Y. ❑No
Y i_3No
❑wA
❑NrA
13,
Samples checked for dechlorination:
Yes ONO
❑wA.
14.
Heads ace in VOA Vials >6mm :
❑Yes ❑No
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (ifpurchased):
❑Yes ONO
❑Yes ONO
w
NIA
16.
Client Notification/ Resolution: Field data Required? Y 1 N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: E—LtE date:
SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
WON:92277769
111111111111111111111
Page 30 of 31

,0--/
PaceAnalytical'
MM.Pacata6s.csm
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody Is a LEGAL. DOCUMENT. All relevant fields must be completed accurately.
M
Section A Section S Section C
Pogo: of CM
Required Ckont Inlonnalion: Required Prejoct Inromutionl Inmru Informalion:
a
Report To, Allention:
Company:—,
18997 9 5
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Copy To:
Company Nama:
REGULATORY AGENCY
Address:
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Project Name:
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STATE:
Requested Due DatorTAT:
Project Number:
Proli10 a'
Requested
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STORMWATER DISCHARGE OUTFALL (SDO)
�` � � � MONITORING REPORT
GENERAL PERMIT NO. NCG030000 �lJ SAMPLES COLLECTED DURING CALENDAR YEAR: 0Z0 j S
CERTIFICATE OF COVERAGE NO. NCG03Q OpS (This monitoring report is due at the Division no later than 30 days from
FACILITY NAME__ csal'i'fUe-Sc�..i QQ I^ C
PERSON COLLECTING SAMPLES
CERTIFIED LABORATORY Lab #
Lab #
Part A: Specific Monitoring Requirements
the date the facility receives the sampling results from the laboratory.)
COUNTY MeGL,1. n)ny c'� — RECEIVED PHONE NO. (20-q -4
DEC 2 8 Z015 PLEASE SIGN ON THE REVERSE -)
CENTRAL. FILES
mthin ear rinhi
O+tfall
I.r
iii$te It
Sample CoUtto
C.Ik
tittllddl r'
4: �yb IA,yF4X f: 1
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".1 �l`. i;'� r
00400 t
11
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Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier l or Tier 2 responses.
See General Permit text.
Did this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ^ yes )�no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity .. onitorina Requirements
Ontfall
' No:
r„1 Date ,i. ;' a Y
..
Sari le C811eeted
P ,u , pr,l�w ;i a
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is
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-4 1 {:Zal v t1 x.
' f00 k .�
,e'ii�l --
:G.w:; Or
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses.
See General Permit text.
STORM EVENT CHARACTERISTICS:
Date 11 30 11S(first event sampled)
Total Event Precipitation (inches): ,r.10 ,T
Date (list each additional event sampled this reporting period, and rainfall amount)
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
Attn: DWQ Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
S WU-245-102107
® Page 1 of 2

1 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or
manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject
to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for
electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31).
Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may request that DWQ waive monitoring of total toxic organics. The solvent
management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities allowed such a waiver, the
discharger shall sign the following certification statement:
"Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I
certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater
runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management
plan included in the Stormwater Pollution Prevention Plan."
�ZA2 f'1\ . ko crt-QS ^ �_
Name (Print name)
�C n lwLC
Title (Print title)
Y1n 2 3
(S i e) (Date)
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted. Based on my inquiry of the person or persons who manage the system, or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations."
2L23) I-S-
jSig6kdre of Permittee) (Date)
SWIla45.10in7

A�
�w �
NCDENR
North Carolina Department of Environment and Natural Resources
Beverly Eaves Perdue
Governor
Gary Hames
American Truetzschler Inc
12300 Moores Chapel Rd
Charlotte, NC 28214
Dear Permittee:
Division of Water Quality
Charles Wakild, P. E.
Director
December 4, 2012
Dee Freeman
Secretary
Subject: NPDES Stormwater Permit Coverage Renewal
American Truetzschler
COC Number NCG030556
Mecklenburg County
In response to your renewal application for continued coverage under stormwater General Permit NCG030000
the Division of Water Quality (DWQ) is forwarding herewith the reissued General Permit. This permit is
reissued pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of
Agreement between the state of North Carolina and the U.S. Environmental Protection Agency, dated October
15, 2007 (or as subsequently amended).
The following information is included with your permit package:
• A new Certificate of Coverage (COC)
• A copy of General Permit NCG030000
• A copy of the Technical Bulletin for the General Permit
• Two copies of the Discharge Monitoring Report (DMR) Form
• Two copies of the Qualitative Monitoring Report Form
The General Permit authorizes discharges of stormwater, and it specifies your obligations for discharge
controls, management, monitoring, and record keeping. Please review the new permit to familiarize yourself
with all the changes in the reissued permit. Your facility has six (6) months from the time of receipt of the
permit to update your current SPPP to reflect all new permit requirements.
The first sample period of your permit begins January 1, 2013. Your facility must sample a "measureable
storm event" beginning during the periods beginning January 1 and July 1 of every year (or, if applicable,
report "No Flow," as outlined in Part III, Section E). Also, please note that Tier 3 Actions in Part II of your
permit are triggered by benchmark exceedances on four occasions beginning on the effective date of this
permit and do not count prior exceedances.
The more significant changes in the General Permit since your last COC was issued are noted either in the
Draft Permit Fact Sheet that accompanied the public notice (http://portal.ncdenr.orgLwebZwq/ws/su/current-
notices), or in the Response to Comments / Summary of Changes and Technical Bulletin documents that are
posted on the Stormwater Permitting Unit's website with the new General Permit. Please visit
http://portal.ncdenr.org/web/wq/ws/su/npdessw (click on 'General Permits' tab) to review that information
for your specific General Permit carefully.
1617 Mail Service Center, Ralegh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone:[phone]%, FAX:[phone]
lntemet: www.ncwi rzrguality.ong
or 1thCarolina
An Equal Opportunit. gfi.^.nativvt Action Employer

Gary Hames
December 4, 2012
Page 2 of 2
Some of the changes include:
Part II:
• Section A: The Stormwater Pollution Prevention Plan (SPPP) section, if applicable, has been updated
to the most current language of our permits. Additional conditions for specific industry sectors have
been added to the SPPP requirements in some cases.
• Sections B, C: Failure to perform analytical stormwater monitoring may result in the Division requiring
that the permittee begin a monthly sampling scheme.
• Sections B, C: A lower TSS benchmark of 50 mg/1 for HQW, ORW, PNA and Tr Waters applies to these
more sensitive waters.
• Sections B, C.- The monitoring parameter Oil & Grease (O&G) has been replaced by the parameter
Total Petroleum Hydrocarbons (TPH) for vehicle maintenance areas, and in some cases, other
analytical monitoring requirements.
• Sections B, C, D: Inability to sample due to adverse weather must be recorded in the SPPP, or in
separate on -site records if your General Permit does not require an SPPP. Adverse weather is defined
in the "Definitions" section of the permit.
• Sections B, C. The term "Representative Storm Event" has been replaced by "Measurable Storm
Event." A measurable storm event is defined in the permit.
• Section D: If the permittee fails to respond effectively to problems identified by qualitative
monitoring, DWQ may require the permittee to perform corrective action.
Please review Parts III and IV to understand the Standard Conditions of your new NPDES General Permit,
including Compliance and Liability, Reporting, Monitoring and Records requirements; Operation and
Maintenance obligations; and Definitions. Please note that all samples analyzed in accordance with the terms
of this permit must be submitted to the Division on Discharge Monitoring Report (DMR) forms available on
the Stormwater Permitting Unit's website above. DMR forms must be delivered to the Division no later than
30 days from the date the facility receives the sampling results from the laboratory. Also note that existing
permittees do not need to submit _a renewal request prior to expiration unless directed by the Division.
Your coverage under the General Permit is transferable only through the specific action of DWQ. This permit
does not affect the legal requirements to obtain other permits which may be required by DENR, nor does it
relieve the permittee from responsibility for compliance with any other applicable federal, state, or local law,
rule, standard, ordinance, order, judgment, or decree. If you have any questions regarding this permit
package, please contact the Division's Stormwater Permitting Unit at [phone].
Sincerely,
for Charles Wakild, P.E.
cc: DWQ Central Files
Stormwater Permitting Unit Files
Mooresville Regional Office

F I
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030556
STORM WATER
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
American Truetzschler Inc
is hereby authorized to discharge stormwater from a facility located at:
American Truetzschler
12300 Moores Chapel Rd
Charlotte
Mecklenburg County
to receiving waters designated as CATAWBA RIVER (Lake Wylie below elevation S70) North
Carolina portion, a class WS-V,B waterbody in the Catawba River Basin in accordance with the
effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, II, Ill,
and IV of General Permit No. NCG030000 as attached.
This certificate of coverage shall become effective December 4, 2012.
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this 4t" day of December, 2012.
for Charles Wakild, P.E., Director
Division of Water Quality
By Authority of the Environmental Management Commission

NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freernan
Govemor Director Secretary
March 18, 2009
Mr. Mark Smith, Plant Manager
American Truetzschler, Inc.
12300 Moores Chapel Road
Charlotte, NC 28214
Subject: Compliance Evaluation Inspection
American Truetzschler, Inc.
Stormwater Permit Number COC NCG030556
Mecklenburg County, NC
Dear Mr. Smith:
Enclosed is a copy of the Compliance Evaluation Inspection (CEI) report for the
inspection conducted at the subject facility on February 24, 2009, by Mr. Ron Eubanks and Mr.
Craig Miller of Charlotte -Mecklenburg Storm Water Services (CMSWS). This inspection was
conducted as part of a cooperative working agreement between Mecklenburg County and the
Division of Water Quality. Thank you for your assistance and cooperation during the inspection.
Overall, the facility's Stormwater program was well developed and implemented and this
Office commends the permittee's efforts to ensure compliance with your NPDES permit.
The enclosed report should be self-explanatory; however should you have any questions
concerning this report or have any questions regarding your permit, please do not hesitate to
contact Ms. Marcia Allocco of this Office at [phone].
Sincerely,
for Robert B. Krebs
Regional Supervisor
Surface Water Protection Section
Mooresville Regional Office
Enclosure
cc: NPS-ACO Unit
Rusty Rozzelle, Mecklenburg County
Craig Miller, City of Charlotte
Mooresville Regional Office
Location: 610 East Center Ave., Suite 301 Mooresville, NC 28115 One
Phone: [phone] Fax: VO4) 663-60401 Customer Service: 1-877-623-6748 NortrhCarQlina
Intemet: wncwaterquality.org
ww.
An Equal opporonily %Afirmative Action Employer— 50% Recyc!eeft0% Past Consumer paper Naturally

Compliance Inspection Report
Permit: NCGO30556 Effective: 11/01/07 Expiration: 10/31/12 Owner: American Truetzschler Inc
SOC: Effective: Expiration: Facility: American Truetzschler
County: Mecklenburg 12300 Moores Chapel Rd
Region: Mooresville
Charlotte NC 28214
Contact Person: Dirk Jaekel Title: Phone: [phone]
Directions to Facility:
1-85 South to Sam Wilson Road, Exit 29. Right onto Sam Wilson Rd. Go 50 yds. First left onto Performance Rd. Go 1 mile at stop sign
take a left ontoMoores Chapel Road. Be on right.
System Classifications:
Primary ORC: Certification: Phone:
Secondary ORC(s):
On -Site Representative(s):
Related Permits:
Inspection Date: 02/24/2009 Entry Time: 10:00 AM Exit Time: 1 1:30 AM
Primary Inspector: Water Quality Program Meckenburg County Phone: [phone]
Secondary Inspector(s):
Reason for Inspection: Routine Inspection Type: Compliance Evaluation
Permit Inspection Type: Metal Fabrication Stormwater Discharge COC
Facility Status: ■ Compliant rl Not Compliant
Question Areas:
Storm Water
(See attachment summary)
Page:1

,.i
Permit: NCG030556 Owner - Facility: American Truetzschler Inc
Inspection Date: 02/24/2009 inspection Type: Compliance Evaluation Reason for Visit: Routine
Inspection Summary:
Facility Description:
American Truetzschler is an international machinery manufacturer, specializing in preparation machines for spinning mills
and the non -woven industry. American Truetzschler has its own service department, sales department, spare parts
department, and an electrical repair center that supplies controls for textile lines and non-wovens.
Compliance History:
The permittee/facility does not have any prior compliance issues with the NC Division of Water Quality or
Charlotte -Mecklenburg Storm Water Services (CMSWS).
Industrial Operations/City of Charlotte Stormwater Ordinance Review:
There was some excess sediment and debris observed under the trash compactor. Excess sediment was also observed
in the storm drain down gradient of the compactor. Charlotte -Mecklenburg Storm Water Services recommends that the
sediment and debris be cleaned up around the compactor and storm drain and properly disposed.
Page:2

Permit: NCG030556 Owner - Facility: American Truetzschler Inc
Inspection Date: 02/24/2009 Inspection Type: Compliance Evaluation Reason for Visit: Routine
Stormwater Pollution Prevention Plan Yes No NA NE
Does the site have a Stormwater Pollution Prevention Plan?
■
n
n
n
# Does the Plan include a General Location (USGS) map?
■
n
n
n
# Does the Plan include a "Narrative Description of Practices"?
■
n
n
n
# Does the Plan include a detailed site map including outfall locations and drainage areas?
■
n
n
n
# Does the Plan include a list of significant spills occurring during the past 3 years?
■
n
n
n
# Has the facility evaluated feasible alternatives to current practices?
■
n
n
n
# Does the facility provide all necessary secondary containment?
■
n
n
n
# Does the Plan include a BMP summary'
■
n
n
n
# Does the Plan include a Spill Prevention and Response Plan (SPRP)?
■
n
n
n
# Does the Plan include a Preventative Maintenance and Good Housekeeping Plan?
■
n
n
n
# Does the facility provide and document Employee Training?
■
n
n
n
# Does the Plan include a list of Responsible Party(s))
■
n
n
n
# Is the Plan reviewed and updated annually?
■
n
n
n
# Does the Plan include a Stormwater Facility Inspection Program?
■
n
n
n
Has the Stormwater Pollution Prevention Plan been implemented?
■
n
n
n
Comment:
Qualitative Monitorin
Yes
No
NA
NE
Has the facility conducted its Qualitative Monitoring semi-annually?
■
n
n
n
Comment:
Analytical Monitoring
Yes
No
NA
NE
Has the facility conducted its Analytical monitoring?
■
n
n
n
# Has the facility conducted its Analytical monitoring from Vehicle Maintenance areas?
n
❑
■
n
Comment:
Permit and Outfalls
Yes
No
NA
NE
# Is a copy of the Permit and the Certificate of Coverage available at the site?
■
n
n
n
# Were all outfalls observed during the inspection?
■
n
n
# If the facility has representative outfall status, is it properly documented by the Division?
n
n
■
n
# Has the facility evaluated all illicit (non stormwater) discharges?
■
n
n
n
Comment:
Page: 3

Michael F. Easley, Governor
William G. Ross Jr., Secretary
Noah Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
December 8, 2006
Mr. Dick Jaekel, Site Manager
American Truetzschler Inc.
12300 Moores Chapel Road
Charlotte, North Carolina 28214
Subject: General Permit No. NCG030000
American Truetzschler Inc.
COC No. NCG030556
Mecklenburg County
Dear Mr. Jaekei:
In accordance with your application for a discharge permit received on November 17, 2006, we
are forwarding herewith the subject certificate of coverage (COC) to discharge under the subject state—
NPDES general permit. -This permit is issued pursuant to the requirements of North Carolina General
Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the US
Environmental Protection Agency dated May 9, 1994 (or as subsequently amended).
If any parts, measurement frequencies, or sampling requirements contained in this permit are
unacceptable to you, you have the right to request an individual permit by submitting an individual
permit application. Unless such demand is made, this certificate of coverage shall be final and binding.
Please take notice that this certificate of coverage is not transferable except after notice to the
Division of Water Quality. The Division of Water Quality may require modification or revocation and
reissuance of the certificate of coverage. This permit does not affect the legal requirements to obtain
other permits which may be required by the Division of Water Quality or permits required by the
Division of Land Resources, Coastal Area Management Act or any other federal or Iocal governmental
permit that may be required:
If you have any questions concerning this permit please contact Bill Diuguid at telephone
number [phone] ext. 382.
Sincerely,
%"IGINAL SIGNED BY
RADLEY BENNETT
Alan W. Klimek, P.E.
cc: Mooresville Regional Office
Central Files
Stormwater Permitting Unit Files
Attachments
Nqr Carolina
Aaturn!!il
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone [phone] Customer Service
Internet: w y ncwaterr uality.org Location: 512 N. Salisbury St. Raleigh, NC 27604 Fax [phone]
An Equal opportunity/Affirmative Action Employer— 50% RecyclecV10% Post Consumer Paper

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
GENERAL PERMIT NO. NCG030000
CERTIFICATE OF COVERAGE No. NCG030556
STORMWATER DISCHARGES
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
American Truetzschler Inc.
is hereby authorized to discharge stormwater from a facility located at
American Truetzschler Inc.
12300 Moores Chapel Road
Charlotte
Mecklenburg
to receiving waters designated as Ut to Catawba River, a Class WS-V, B; in accordance with the effluent
limitations, monitoring requirements, and other conditions set forth in Parts I, I1, III, IV, V and VI of General Permit
No. NCG03000, as attached. -
This Certificate of Coverage shall become effective December 8, 2006.'
This Certificate of Coverage shall remain in effect for the duration of the General Permit.
Signed this day December 8, 2006.
BRADLEY P-F-t"1E- "1
Alan W. Klimek, P.E. Director
Division of Water Quality
By Authority of the Environmental Management Commission

Markers
Name: NCG080774 -- CSX Intermod I
Short Name: 80774
Coordinates: 0 ° 16' 29. N, 0800 53' 40.94" W
Comment: CSX Int al, Stewart Creek to Irwin Creek, a Class C creek to Catawba
River & s Mt Island Lake Quad 35080-C8-TF-024, Subbasin 03-08-34, stream
inde 11-137-1-
Name: NCG100188 — Dave's Auto Salvag
Short Name: 1001
Coordinates: 035° 20' 7" N 800 54' 43.62" W
Comment: Dave's Auto Salv Gar Creek to Mountain Island Lake, Catawba River Basin,
Mecklenburg ounty, Su asin 03-08-33, stream index 11-116 (2), WS-IV,CA;
15 Mt Island Lake
Name: NCG030556 American�Truetz�schler, Inc.
Short Name: 030556
Coordinates: 035' 15' 18.09" N, 081' 00' 4.44" W
Comment: American Truetzschler, Inc.; Ut to Catawba River, Class WS-V, B; Subbasin
03-08-34; stream index 11-(123.5); Quad Belmont Mount Holly