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HomeMy WebLinkAboutNCG030502_MONITORING INFO_20180510STORMWATER DIVISION CODING SHEET NCG PERMITS PERMIT NO. � CC'� D 3 O DOC TYPE ❑HIS ICAL FILE ONITORING REPORTS DOC DATE ❑ 0 YYYYMMDD Semi-annual Stormwater Discharee Monitoring.Report, for°North Carolina Division,of'Water QVzb�;7 ty General Permit 'No. NCG03000Q Date submitted` CERTIFICATE OF COVERAGE NO. N G03 4 S 6 FACIUWNAME .59aQ , COUNTY PERSON COLLE G_SAMPLES �UrMil �(,fsr LABORATORY Lab Cert. #9�a93�18 Comments on sample collection.or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 00 /� SAMPLE PERIOD Ek,,fan-June ❑July -Dec or ❑'Monthly'_ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA []Zero -flow [�ater.Supply [:]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -) M No.discharge•this period?' Outfall No: Date Sample Collected i (moJddJyr). 24=hour:rainfall amount, Inches'. Total Suspended Solids pH; Standard units Copper Lead Zinc Non -Polar 0&G/ Total Petroleum Hydrocarbons Total TOXIC Organics s Benchmarks =_ _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.'007 mg/L 0:033'mg/L 0.067 mg/L 15'mg/L 1 mg/L 14 Montfily.sampling (instead of semi-annual) must begin with.the.second consecutive benchmark exceedance for the -same parameter at the same outfall. a Forsampling,periods'with no discharge at any single outfall, you must-sti -submit this discharge monitoring report;with a•checkmark hete. 3The.total precipitation must be recorded using data. from an on -site rain gauge. Unattended sites may be eligible for a waiver of. the rain gauge requirement. "See°General lPermit, Table',3 identifyingithe: especially,sensitive:receiving`►i ater'classifications where!thi more protective benchmark applies. s Total Toxic Organics sampling is applicable only for,those facilities which perform metal finishing operations, manufacture -semiconductors, manufacture electronic crystals; or manufacture cathode ray tubes. For purposes;of this permit•the definition of Total Toxic Organics is that -definition contained in the EPA Effluent Guidelines for the.facility subject to the.requiremerit:to sample.(for'metal.finishing use the definition as.found in 40 CFR 433.11;.for semiconductor manufacture use the definition ras found in 40 CFR 469.12; for`electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40.CFR:469.31): Permit Dates 41/1/2012-10/31/2017 SWU-245, last revised 10125/2012 Page 1 of 3 /L Nate: if you report a sample value in excess of the benchmark, you must implement Tier I, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONfTORING'RESULTS: - A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. - 2 EXCEEDANCES IN A ROW FOR THE.SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. - TIER 3:, HAS YOUR FACILITY-HADA OR MORE BENCHMARK EXCEEDENCES FOR:THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES; HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ 'REGIONAL OFFICE CONTACT NAME: in the case of "No Discharge" re ortsl pivision of WaterOuality Inn Attn: DWQ Central Files 1617 Mail Service Center Raleigh; North Carolina 27699-1617 YQU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law„that this document and;all'attachrrients were prepared under -my direction or supervision in:accordance with a,system designed:to assure that. qualified personnel properlygather and evaluate the information submitted. Based on. my inquiry of'the person or. persons who, manage the system, or those persons directly responsible for gathering -the information, the -information submitted is, to'the,best of my knowledge and. belief,.true, accurate, and complete. am,aware that there!are significant penalties for submitting false information„including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee Permit Dat---" 1/1/2012-10/31/2017 (Date1 SWU-245, last revised 101715/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Qua7/0 'ty General Permit No. NCG030000 Date submitted .7 CERTIFICATE OF COVERAGE NO. N G03 6 5 4 c2 FACILITY NAME 604a& — — — — COUNTY PERSON COLLECTING SAMPLES (J�Mi/G�hP(�.SrI�J LABORATORY Lab Cert. #i Comments on sample collection or analysis: �� e_ Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR °'?Q �� SAMPLE PERIOD [)'Tan -June ❑ July -Dec or El Monthly' month DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA ]Zero -flow EgWater Supply ❑SA [—]Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?z Outfall No. Date Sample ' (mo/dd/yr) 24-hour rainfall amount, Inches Total suspended Solids PH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum . Hydrocarbons Total Toxic s Qrganics Benchmarks =__0> - - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L / y,?y n /.a" L G yo �O,oas 1u,Qos a.o yI 5.0 /G z ,sa / G 3 '1 ay IF /. D " /V L , 025/ 41G, oaS -dQ.DaS p.030 eS o r-giL 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still'submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data'from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water'classifications wheIre,the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requiremert to sample (formetal finishing use the definition as found in 40 CFR 433,11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as fou � CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469,31). FQ� I � � 1R MAY 15 2018 CENTRAL FILES DWR SECTION Permit Date 1.1/1/2012-10/31/2017 u ir�MAY 15 2018 SWU-245, last revised 10/25/2012 ' Page 1 of 3' Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. Y TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: in the case of "No Discharge" reports) to:�� Yn� Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �llol/,Y (Signature of Permittee) (Date) Permit Dat.^r-' 1/1/2012-10/31/2017 SWU-245, last revised 1rl'15/2012 � — Page 3 of 3 t �r.. 711* nn� NCDENR Stormwater Discharge- Outfall.(SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit: bUg;././porM].i-ic.derir.org/web/wQ/ws/su/npdessw#tab-4 Permit No.: Facility Name: SAab Bctr'Ac. County: %-\PcNe-jr Inspector: Date of Inspection: Time of Inspection: or Certificate of Coverage No.: LLC _ Total Event Precipitation (inches): / 0 Phovke N4, 910- 0&14- Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring o7ust be per formed during a "representative storm event" or "leasureable storm event" (requiren2ents vary, depending on the permit). 1 Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than! 0.1 inches has occurred. A single storm event may contain up to 10 consecutive Fours of no t f precipitation. l A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does riot apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I cer�fij that this report iAaccurate and complete to the best of my knowledge: (Signature of Permittee or Designee) sWU-242, Last modified 10/25/2012 Page 1 of 2 CDENR Stormwater Discharge, Outfall. (SDO) Qualitative Monitoring Report Forguidance on filling out thisform, please visit. hn:.//12ortal.ncdenr.org/webjwq/ws/-$u.Inp—deaaw--#tab-I Permit No.: Facility Name: SAb BarAt,aA County: NIP+cNt44 Inspector: Date of inspection: a��! Time of Inspection: or Certificate of Coverage No.: Ur— Phflne No. 910- $14,04"U Total Event Precipitation [inches]: O Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ��YesCFJ No Please verify whether Qualitative Monitoring must he performed during a "representative storm event" or "measureahle storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement, Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours {3 days] in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. 1 i l A "measurable storm event" is a storm event that results in an actual discharge from the ' permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this sign �re, I certify .� , - r -- (Signature of Permittee or Designee) rt is accurate and complete to the best of my knowledge: SWU-242, Last modified 10/25/2012 Page 1 of 2 aceAnalytical WW.pacefab1cW May 02, 2018 Patricia Anderson Saab Barracuda LLC 608 E. MCNEIL STREET Lillington, NC 27546 RE: Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Dear Patricia Anderson: Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2018. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, o" �-hl Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 28 aceAnaljftal www.p"abs.com SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Pace Project No.: Stormwater Permit #MCG030000 92382268 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92382268001 Saab Outfall 002 EPA 1664B JMS 1 PASI-C EPA 608.3 PKS 29 PASI-C EPA 200.7 SH1 3 PASI-A EPA625 RES 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D WC 1 PASI-A 92382268002 Saab Outfall 003 EPA 1664B JMS 1 PASI-C EPA 608.3 PKS 29 PASI-C EPA200.7 SH1 3 PASI-A EPA625 RES 58 PASI-C EPA624 GAW 34 PASI-C SM 2540D WC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report Shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 28 aceAnalytrcal WW ►petelab&CoM ANALYTICAL RESULTS Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: Saab Outfall 002 Parameters Lab ID: 92382268001 Results Units Collected: 04/24/18 14:15 Report Limit DF Received: 04/25/18 12:50 Matrix: Water Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Benzo(g,h,i)perylene NO ug?L 5.2 1 04/26/18 20:35 04/30/18 12:32 191-24-2 Benzo(k)fluoranthene NO ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 207-08-9 4-Bromophonylphenyl ether NO ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 101-55-3 Butylbenzyiphthalate ND ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 85-68.7 4-Chloro-3-methylphenol NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 59-50-7 bis(2-Chloroethoxy)methane NO ug/L 10.4 1 04126/1820:35 04130/1812:32 111-91-1 bis(2-Chloroethyl) ether NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 111-44-4 2-Chloronaphthalene NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 91-58-7 2-Chlorophenol ND ug/L 52 1 04/26/18 20:35 04/30/18 12:32 95-57-8 4-Chlorophenylphenyl ether NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 7005-72-3 Chrysene ND ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 218-01-9 Dibenz(a,h)anthracene NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 53-70-3 3,3'-Dichlorobenzidine NO ug/L 26.0 1 04/26/18 20:35 04/30/18 12:32 91-94-1 2,4-Dichlorophenol NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 120-83.2 Diethylphtha late NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 84-66-2 2,4-Dimethylphenol NO ug/L 10.4 1 04/26/18 20:35 04/30/18 12:32 105-67-9 Dimethylphthalate NO ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 131-11-3 Di-n-butylphthalate NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 84-74-2 4,6-Dinitro-2-methylphenol NO ug/L 20.8 1 04/26/18 20:35 04/30/18 12:32 534-52-1 2,4-Dinitrophenol NO ug/L 52.1 1 04/26/18 20:35 04/30/18 12:32 51-28-5 2,4-Dinitrotoluene NO ug/L 5.2 1 04/26118 20:35 04/30/18 12:32 121-14-2 2,6-Dinitrotoluene NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 606-20-2 Di-n-octylphthalate NO uglL 5.2 1 04/26/18 20:35 04/30/18 12:32 117-84-0 bis(2-Ethylhexyl)phthalate NO ug/L 52 1 04/26/18 20:35 04/30/18 12:32 117-81.7 Fluoranthene NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 206-44-0 Fluorene ND ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 86-73-7 Hexachloro-1,3-butadiene NO ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 87-68-3 Hexachlorobenzene NO ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 118-74-1 Hexachlorocyclopentadiene NO ug/L 10.4 1 04/26/18 20:35 04/30/18 12:32 77-47-4 Hexachloroethane ' NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 67-72-1 L2 Indeno(1,2,3-cd)pyrene NO ug/L 5.2 1 0412611820:35 04130/1812:32 193-39-5 Isophorone ND ug/L 10.4 1 04/26/18 20:35 04/30/18 12:32 78-59-1 Naphthalene NO ug/L 5.2 1 04/2611820:35 04130/1812:32 91-20-3 Nitrobenzene NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 98-95-3 2-Nitrophenol ND ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 88-75-5 4-Nitrophenol NO ug/L 52.1 1 04/26/18 20:35 04/30118 12:32 100-02-7 N-Nitrosodimethylamine NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 5.2 1 04/26/18 20:35 04/30118 12:32 621-64-7 N-Nitrosodiphenylamine NO ug/L 10.4 1 04/26/18 20:35 04/30/18 12:32 86-30-6 2,2'-Oxybis(1-chloropropane) NO ug/L 5.2 1 04/2611820:35 04/30118 12:32 108-60-1 Pentachlorophenol NO ug/L 10.4 1 04/26/18 20:35 04/30/18 12:32 87-86-5 Phenanthrene NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 85-01-8 Phenol ND ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 108-95-2 Pyrene NO ug1L 5.2 1 04/26/18 20:35 04/30/18 12:32 129-00-0 1,2,4-Trichlorobenzene NO ug/L 5.2 1 04/26/18 20:35 04/30/18 12:32 120-82-1 2,4,6-Trichlorophenol NO ug1L 10.4 1 04/26/18 20:35 04/30/18 12:32 88-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 28 Pace Analytical Services, LLC aceAnalytieal e 6701 Conference Drive Raleigh, NC 27607 www.pacefab&cam (919)834-4984 ANALYTICAL RESULTS Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 Sample: Saab Outfall 003 tab ID: 92382268002 Collected: 04/24/18 14:05 Received: 04/25/18 12:5D Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons ND mg/L 5.0 1 04/27/18 05:50 608 PCB Pest RVE Analytical Method: EPA 608.3 Preparation Method: EPA 608.3 Alddn ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 309-00-2 alpha-BHC ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 319-84-6 beta-BHC ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 319-85-7 delta-BHC ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 319-86-8 gamma-BHC (Lindane) ND uglL 0.050 1 04/27/18 20:59 05/01118 13:03 58-89-9 Chlordane (Technical) ND ug/L 0,50 1 04/27/18 20:59 05/01/18 13:03 57-74-9 alpha -Chlordane ND ug/L 0.050 1 04127/1820:59 05/01/18 13:03 5103-71-9 gamma -Chlordane ND ug/L 0.050 1 04127/1820:59 05101/1813:03 5103-74-2 4,4'-DDD ND ug/L 0.050 1 04127/1820:59 05/01/18 13:03 72-54-8 4,4'-DDE ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 72-55-9 4,4'-DDT ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 50-29-3 Dieldrin ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 60-57-1 Endosulfan I ND ug/L 0.050 1 04/27/18 20:59 05101/18 13:03 959-98-8 Endosulfan II ND uglL 0.050 1 04/27/18 20:59 05/01/18 13:03 33213-65-9 Endosulfan sulfate ND ug/L 0,050 1 04127/1820:59 05/01/18 13:03 1031-07-8 Endrin ND ug/L 0.050 1 04127/1820:59 05/01/18 13:03 72-20-8 Endrin aldehyde ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 7421-93-4 Heptachlor ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 04/27/18 20:59 05/01/18 13:03 1024-57-3 PCB-1016 (Aroclor 1016) ND ug/L 0.50 1 04/27/18 20:59 05/01/18 13:03 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 0.50 1 04/27/18 20:59 05/01/18 13:03 11104-28-2 PCB-1232 (Aroclor 1232) ND ug1L 0.50 1 04/27/18 20:59 05/01/18 13:03 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 0.50 1 04/27/18 20:59 05/01/18 13:03 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 04127/18 20:59 05/01/18 13:03 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 0.50 1 04/27/18 20:59 05/01/18 13:03 11097-69-1 PC6-1260 (Aroclor 1260) ND ug1L 0.50 1 04/27/18 20:59 05/01/18 13:03 11096-82-5 Toxaphene ND ug/L 0.50 1 04/27/18 20:59 05/01/18 13:03 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 39 % 60-140 1 04/27/18 20:59 05/01/18 13:03 877-09-8 S5 Decachlorobiphenyl (S) 55 % 60-140 1 04/27/18 20:59 05/01/18 13:03 2051-24-3 S5 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND mg/L 0.0050 1 04/27/18 05:15 05/01/18 02704 7440-50-8 Lead ND mg/L 0.0050 1 04/27/18 05:15 05/01/18 02:04 7439-92-1 Zinc 0.030 mg/L 0.010 1 04/27/18 05:15 05/01/18 02:04 7440-66-6 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Acenaphthene ND ug/L 5.7 1 04/26/18 20:35 04/30/18 13:01 83-32-9 Acenaphthylene ND ug/L 5.7 1 04/26/18 20:35 04/30/16 13:01 208-96-8 Anthracene ND ug/L 5.7 1 04/26/18 20:35 04/30/18 13:01 120-12-7 Benzo(a)anthracene ND ug/L 5.7 1 04/26/18 20:35 04/30/18 13:01 56-55-3 Benzo(a)pyrene ND ug/L 5.7 1 04/26/18 20:35 04/30/18 13:01 50-32-8 Benzo(b)Fluoranthene ND ug1L 5.7 1 04/26/18 20:35 04/30/18 13:01 205-99-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02I2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 28 Pace Analytical Services, LLC aceAnalytical ® 67p1 Conference Drive Raleigh, NC 27607 w%wpace/ab&com (919)834-4984 ANALYTICAL RESULTS Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 Sample: Saab Outfall 003 Lab ID: 92382268002 Collected: 04/24/18 14:05 Received: 04/25/18 12:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Surrogates Nitrobenzene-d5 (S) 75 % 10-120 1 04/26/18 20:35 04/30/18 13:01 4165-60-0 2-Fluorobiphenyl (S) 70 % 15-120 1 04/26/18 20:35 04/30/18 13:01 321-60-8 Terphenyl-d14 (S) 266 % 11-131 1 04/26/18 20:35 04/30/18 13:01 1718-51-0 S3 Phenol-d6 (S) 27 % 10-120 1 04/26/18 20:35 04/30/18 13:01 13127-88-3 2-Fluorophenol (S) 38 % 10-120 1 04/26/18 20:35 04/30/18 13:01 367-12-4 2,4,6-Tribromophenol (S) 84 % 10-137 1 04/26/18 20:35 04/30/18 13:01 118-79-6 624 Volatile Organics Analytical Method: EPA 624 Benzene ND ug1L 2.0 1 04/26/18 19:12 71-43-2 Bromodichloromethane ND ug/L 2.0 1 04/26/18 19:12 75-27-4 Bromoform ND ug/L 2.0 1 04126/1819:12 75-25-2 Bromomethane ND ug/L 2.0 1 04/26/18 19:12 74-83-9 Carbon tetrachloride ND ug1L 2.0 1 04/26/18 19:12 56-23-5 Chlorobenzene ND ug/L 2.0 1 04/26/18 19:12 108-90-7 Chloroethane ND ug1L 2.0 1 04/2611819:12 75-00-3 Chloroform ND ug/L 2.0 1 04/2611819:12 67-66-3 Chloromethane ND ug/L 2.0 1 04126/1819:12 74-87-3 Dibromoch lorom ethane ND ug/L 2.0 1 04126/1819:12 124-48-1 1,2-Dichlorobenzene ND ug/L 2.0 1 04126/1819:12 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 1 04126/1819:12 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 1 04126/1819:12 106-46-7 1,1-Dichloroethane ND ug1L 2.0 1 04/26/1819:12 75-34-3 1,2-Dichloroethane ND ug/L 2.0 1 04/26/18 19:12 107-06-2 1,1-Dichloroethene ND ug/L 2.0 1 04126/1819:12 75-35-4 cis- 1,2-Dichloroethene ND ug/L 2.0 1 0412611819:12 156-59-2 trans-1,2-Dichloroethene ND ug/L 2.0 1 04/2611819:12 156-60-5 1,2-Dichloropropane ND ug/L 2.0 1 04126/1819:12 78-87-5 cis-1,3-Dichloropropene ND ug1L 2.0 1 04/26/18 19:12 10061-01-5 trans- 1,3-Dichloropropene ND ug1L 2.0 1 04/26/1819712 10061-02-6 Ethylbenzene ND ug1L 2.0 1 04/2611819:12 100-41-4 Methylene Chloride ND ug/L 2.0 1 04/26/18 19:12 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 04/2611819:12 79-34-5 Tetrachloroethene ND ug/L 2.0 1 04/26/18 19:12 127-18-4 Toluene ND ug1L 2.0 1 04126/1819:12 108-88-3 1,1,1-Trichloroethane ND ug1L 2.0 1 0412611819:12 71-55-6 1,1,2-Trichloroethane ND ug1L 2.0 1 04/26/18 19:12 79-00-5 Trichloroethene ND ug/L 2.0 1 04/26/1819A2 79-01-6 Trichlorofluoromethane ND ug1L 2.0 1 04/26/18 19:12 75-69-4 Vinyl chloride ND ug1L 2.0 1 04/26/18 19:12 75-01-4 Surrogates 4-Bromofluorobenzene (S) 106 % 70-130 1 04/26/18 19:12 460-00-4 Toluene-d8 (S) 118 % 70-130 t 04/26/18 19:12 2037-26-5 1,2-Dichloroethane-d4 (S) 85 % 70-130 1 04/26/18 19:12 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 7.1 mg/L 2.9 1 04/30/18 19:11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 28 laneAnalyficaf* www.pacelabs.corn Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 QC Batch: 408162 QC Batch Method: EPA 200.7 Associated Lab Samples: 92382268001, 92382268002 METHOD BLANK: 2264813 Associated Lab Samples: 92382268001, 92382268002 Parameter Units Copper mglL Lead mglL Zinc mg1L QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 05/01/18 01:00 ND 0.0050 05/01/18 01:00 ND 0,010 05/01/18 01:00 Qualifiers Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 2264814 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper mg1L .5 0.47 93 85-115 Lead mg1L .5 0.45 90 85-115 Zinc mg1L .5 0.45 91 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2264815 MS 92382002001 Spike Parameter Units Result Cone. Copper mglL ND .5 Lead mglL ND .5 Zinc mglL 10.4 .5 uglL MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2264817 MS 92382256001 Spike Parameter Units Result Cone. Copper mg1L ND .5 Lead mglL 5.3 ug1L .5 Zinc mglL 15.0 .5 ug1L 2264816 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 5 0.46 0.46 92 92 70-130 0 .5 0,44 0.44 88 87 70-130 0 .5 0.46 0.46 90 90 70-130 0 2264818 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD .5 0.46 0.47 92 93 70-130 1 .5 0.45 0.46 88 90 70-130 2 .5 0.47 0,47 90 92 70-130 2 Results presented on this page are in the units indicated by the "Unite" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Qual Qua[ Page 11 of 28 aceAnalytical wwwpacelabs.00m QUALITY CONTROL DATA Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 LABORATORY CONTROL SAMPLE: 2264588 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,2-Trichloroethane uglL 20 21.1 106 52-150 1,1-Dichloroethane uglL 20 19.7 98 59-155 1,1-Dichioroethene uglL 20 22.5 113 1-234 1,2-Dichlorobenzene uglL 20 20.3 102 18-190 1,2-Dichloroethane uglL 20 21.3 106 49-155 1,2-Dichloropropane ug1L 20 21.2 106 1-210 1,3-Dichlorobenzene ug1L 20 20.4 102 59-156 1,4-Dichlorobenzene uglL 20 20.2 101 18-190 Benzene uglL 20 21.4 107 37-151 Bromodichloromethane uglL 20 22.1 111 35-155 Bromoform uglL 20 19.0 95 45-169 Bromomethane ug1L 20 17.6 88 1-242 Carbon tetrachloride ug1L 20 22.6 113 70-140 Chlorobenzene ug1L 20 20.1 100 37-160 Chloroethane ug1L 20 18.6 93 14-230 Chloroform ug1L 20 19.3 96 51-138 Chloromethane uglL 20 18.7 93 1-273 cis-1,2-Dichloroethene ug1L 20 20.4 102 68-146 cis-1,3-Dichloropropene ug1L 20 20.9 104 1-227 Dibromochloromethane ug1L 20 20.5 102 53-149 Ethylbenzene ug1L 20 20.2 101 37-162 Methylene Chloride uglL 20 21.2 106 1-221 Tetrachloroethene ug/L 20 17.2 86 64-148 Toluene ug1L 20 19.7 98 47-150 trans-1,2-Dichloroethene ug1L 20 21.1 106 54-156 trans-1,3-Dichloropropene ug/L 20 21.0 105 17-183 Trichloroethene ug1L 20 21.7 108 70-157 Trichlorofluoromethane ug/L 20 18.8 94 17-181 Vinyl chloride ug1L 20 21.1 105 1-251 1,2-Dichloroethane-d4 (S) % 102 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 98 70-130 MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2264589 2264590 MS MSD 92382308002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD 1,1,1-Trichloroethane ug1L NO 20 20 29.3 30.1 147 150 46-171 2 1,1,2,2-Tetrachloroethane ug1L NO 20 20 27.3 27,2 136 136 73-159 0 1,1,2-Trichloroethane uglL NO 20 20 28.3 29.5 141 147 64-152 4 1, 1 -Dichloroethane uglL ND 20 20 25.3 28.7 126 143 43-172 13 1, 1 -Dichloroethene uglL ND 20 20 31.1 32.1 156 160 48-189 3 1,2-Dichlorobenzene uglL NO 20 20 27.2 28.8 136 144 54-154 6 1,2-Dichloroethane uglL NO 20 20 25.9 27.9 129 139 42-171 7 1,2-Dichloropropane ug/L NO 20 20 29.1 31.2 145 156 55-157 7 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right or the result. REPORT OF LABORATORY ANALYSIS Qual This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 28 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 QC Batch: 408348 Analysis Method: EPA 608.3 QC Batch Method: EPA 608.3 Analysis Description: 608 PCB Pest Red Vol Associated Lab Samples: 92382268001, 92382268002 METHOD BLANK: 2265929 Matrix: Water Associated Lab Samples: 92382268001, 92382268002 Pace Analytical Services, i 6704 Conference Drive Raleigh, NC 27607 (919)834-4984 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 4,4'-DDD ug1L ND 0.050 0510111812:00 4,4'-DDE ug/L ND 0.050 0510111812!00 4,4'-DDT ug1L ND 0.050 05/01/18 12:00 Aldrin ug/L ND 0.050 05/0111812:00 alpha-BHC ug/L ND 0.050 05/0111812:00 alpha -Chlordane uglL ND 0.050 05101/1812:00 beta-BHC uglL ND 0.050 05/01/1812:00 Chlordane (Technical) ug1L ND 0.50 05/01/18 12:00 delta-BHC ug/L ND 0.050 0510111812:00 Dieldrin ug1L ND 0.050 05/0111812:00 Endosulfan I ug/L ND 0.050 05/01/18 12!00 Endosulfan II ug1L ND 0.050 05/01/18 12:00 Endosulfan sulfate ug1L ND 0.050 05/01/18 12:00 Endrin ug1L ND 0,050 05/01/18 12:00 Endrin aldehyde ug/L ND 0.050 05/01118 12:00 gamma-BHC (Lindane) ug1L ND 0.050 05101/18 12:00 gamma -Chlordane ug1L ND 0.050 0510111812:00 Heptachlor ug1L ND 0.050 05/0111812:00 Heptachlor epoxide ug/L ND 0.050 05101/1812:00 PCB-1016 (Aroclor 1016) ug1L ND 0.50 05/01/18 12:00 PCB-1221 (Aroclor 1221) ug1L ND 0.50 05/01/18 12:00 PCB-1232 (Aroclor 1232) 1 ND 0.50 05/01/18 12:00 PCB-1242 (Aroclor 1242) ug1L ND 0.50 05/01/18 12:00 PCB-1248 (Aroclor 1248) uglL ND 0.50 05/01/18 12:00 PCB-1254 (Aroclor 1254) ug/L ND 1 05/01/18 12:00 PCB-1260 (Aroclor 1260) ug/L ND 0.50 05/01/18 12:00 Toxaphene i ND 0.50 05/0111812:00 Decachlorobiphenyl (S) % 83 60-140 05/01/18 12:00 Tetrachloro-m-xylene (S) % 52 60-140 05/01/18 12:00 SO LABORATORY CONTROL SAMPLER LCSD: 2265930 2265931 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 4,4'-DDD uglL .25 0.14 0.18 58 73 31-141 24 39 4,4'-DDE ug/L .25 0.17 0.18 68 74 30-145 8 35 4,4'-DDT ug1L .25 0.16 0.18 63 73 25-160 16 42 Aldrin ug1L .25 0.12 0.12 46 48 42.140 3 35 alpha-BHC ug/L .25 0.18 0.17 71 67 37-140 6 36 alpha -Chlordane ug/L .25 0.16 0.20 67 82 45-140 20 35 beta-BHC ug/L .25 0.16 0.15 64 61 f 7-147 5 44 Results presented on this page are In the units Indicated by the -Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, li Page 15 of 28 aceAnalytical wwwpacelabsmm QUALITY CONTROL DATA Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 QC Batch: 407970 Analysis Method: EPA 625 QC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 92382268001, 92382268002 METHOD BLANK: 2263603 Associated Lab Samples: 92382268001, 92382268002 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug1L ND 5.0 04/26/1816:42 2,2'-Oxybis(1-chloropropane) ug1L ND 5.0 04126/1816:42 2,4,6-Tdchlorophenol ug1L ND 10.0 04/26/1816:42 2,4-Dichlorophenol ug/L ND 5.0 0412611816:42 2,4-Dimethylphenol ug/L ND 10.0 04/2611816:42 2,4-Dinitrophenol ug/L ND 50.0 04126/1816:42 2,4-Dinitrotoluene ug/L ND 5.0 04/2611816:42 2,6-Dinitrotoluene ug/L ND 5.0 04/26/1816:42 2-Chloronaphthalene ug1L ND 5.0 04/26/1816:42 2-Chlorophenol uglL ND 5.0 04/2611816:42 2-Nitrophenol ug1L ND 5.0 04/2611816:42 3,3'-Dichlorobenzidine ug1L ND 25.0 04/2611816:42 4,6-Dinitro-2-methylphenol ug/L ND 20.0 04126/1816:42 4-Bromophenylphenyl ether ug/L ND 5.0 04/26/18 16:42 4-Chloro-3-methylphenol ug/L ND 5.0 0412611816:42 4-Chlorophenylphenyl ether ug/L ND 5.0 04/26/18 16:42 4-Nitrophenol ug/L ND 50.0 04126/1816:42 Acenaphthene ug/L ND 5.0 0412611816:42 Acenaphthylene ug/L ND 5.0 0412611816:42 Anthracene ug/L ND 5.0 0412611816:42 Benzo(a)anthracene ug/L ND 5.0 0412611816:42 Benzo(a)pyrene ug/L ND 5.0 04126/1816:42 Benzo(b)fluoranthene ug1L ND 5.0 04/26/1816:42 Benzo(g,h,i)perylene ug/L ND 5.0 04/26/1816:42 Benzo(k)fluoranthene ug1L NO 5.0 0412611816:42 bis(2-Chloroethoxy)methane ug/L ND 10.0 04/26/1816:42 bis(2-Chloroethyl) ether ug/L ND 5.0 04/26/18 16:42 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/2611816:42 Butylbenzylphthalate ug/L ND 5 O 04/26/18 16:42 Chrysene ug/L ND 5.0 0412611816:42 Di-n-butylphthalate uglL ND 5.0 04126/1816:42 Di-n-octylp htha late ug/L ND 5.0 04/2611816:42 Dibenz(a,h)anthracene ug/L ND 5.0 04/26/1816:42 Diethylphtha late ug/L ND 5.0 04/2611816:42 Dimethylphthalate ug1L ND 5.0 04/26/1816:42 Fluoranthene ug/L ND 5.0 04/2611816:42. Fluorene ug1L ND 5.0 04/26/1816:42 Hexachloro-1,3-butadiene ug1L ND 5.0 04126/1816A2 Hexachlorobenzene ug1L ND 5.0 04126/1816:42 Hexachlorocyclopentadiene ug/L ND 10.0 04/2611816:42 Hexachloroethane ug/L ND 5.0 04/26/1816:42 Qualifiers Pace Analytical Services, LLG 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 28 Pace Analytical Services, LLC ® aceAnall ca! 6701 Conference Drive Raleigh. NC 27607 www,pacelabs-corn (919)834-4984 QUALITY CONTROL DATA Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 LABORATORY CONTROL SAMPLE: Parameter 2263604 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Benzo(g,h,i)perylene ug1L 50 34.9 70 1-219 Benzo(k)fluoranthene ug/L 50 37.3 75 11-162 bis(2-Chloroethoxy)methane ug/L 50 33.1 66 33-184 bis(2-Chloroethyl) ether ug1L 50 33.1 66 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 36.0 72 8-158 Butylbenzylphthalate ug1L 50 36.2 72 1-152 Chrysene ug1L 50 39.2 78 17-168 Di-n-butylphthalate ug1L 50 36.5 73 1-118 Di-n-octylphthalate ug/L 50 41.6 83 4-146 Oibenz(a,h)anthracene ug/L 50 36.8 74 1-227 Diethylphthalate uglL 50 37.3 75 1-114 Dimethylphtha late uglL 50 36.1 72 1-112 Fluoranthene ug[L 50 38.7 77 26-137 Fluorene ug/L 50 37.2 74 59-121 Hexachloro-1,3-butadiene uglL 50 18.7 37 24-116 Hexachlorobenzene ug/L 50 39.1 78 1-152 Hexachlorocyclopentadiene ug1L 50 28.4 57 25-150 Hexachloroethane ug1L 50 15.2 30 40-113 L2 Indeno(1,2,3-cd)pyrene ug/L 50 35.6 71 1-171 Isophorone ug/L 50 33.5 67 21-196 N-Nitroso-di-n-propylamine ug/L 50 34.3 69 1-230 N-Nitrosod imethyla mine ug/L 50 20.5 41 25-150 N-Nitrosodiphenylamine ug1L 50 36.9 74 25-150 Naphthalene ug/L 50 26.8 54 21-133 Nitrobenzene ug/L 50 31.2 62 35-180 Pentachlorophenol ug/L 100 87.6 88 14-176 Phenanthrene ug/L 50 37.9 76 54-120 Phenol ug/L 50 14.8 30 5-112 Pyrene ug1L 50 40.1 80 52-115 2,4,6-Tribromophenol (S) % 83 10-137 2-Fluorobiphenyl (S) % 69 15-120 2-Fluorophenol (S) % 35 10-120 Nitrobenzene-d5 (S) % 65 10-120 Phenol-d6 (S) % 25 10-120 Terphenyl-d14 (S) % 52 11-131 MATRIX SPIKE SAMPLE: 2263605 92382071001 Spike MS MS % Rec Parameter Units Resuit Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug1L ND 49 30.9 63 44-142 2,2'-Oxybis(1-chloropropane) ug[L ND 49 27.6 56 36-166 2,4,6-Trichlorophonol ug1L ND 49 40A 82 37-144 2,4-Dichlorophenol ug1L ND 49 42.6 87 1-191 2,4-Dimethylphenol ug/L ND 49 51.8 93 32-119 2,4-Dinitrophenol ug/L ND 245 196 80 1-181 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, LLC, Page 19 of 28 laceAnalytical wwwpacefabs.cam QUALITY CONTROL DATA Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 MATRIX SPIKE SAMPLE: 2263605 92382071001 Spike MS MS Parameter Units Result Conc. Result % Rec 2-Fluorobiphenyl (S) % 70 2-Fluorophenol (S) % 33 Nitrobenzene-d5 (S) % 73 Phenol-d6 (S) % 22 Terphenyl-d14 (S) % 44 SAMPLE DUPLICATE: 2263606 92382072001 Dup Parameter Units Result Result RPD Qualifiers 1,2,4-Trichlorobenzene ug/L ND ND 2,2'-Oxybis(1-chloropropane) ug/L ND ND 2,4,6-Trichlorophenol ug/L ND ND 2,4-Dichlorophenol uglL ND ND 2,4-Dimethylphenol ug/L ND ND 2,4-Dinitrophenol ug/L ND ND 2,4-Dinitrotoluene ug/L ND ND 2,6-Dinitrotoluene ug/L ND NO 2-Chloronaphthalene ug/L ND NO 2-Chlorophenol ug/L NO ND 2-Nitrophenol ug/L NO NO 3,3'-Dichlorobenzidine ug/L ND ND 4,6-Dinitro-2-methylphenol ug/L ND ND 4-Bromophenylphenyl ether ug/L ND ND 4-Chloro-3-melhylphenol ug/L ND ND 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitrophenol ug/L ND ND Acenaphthene ug/L ND NO Acenaphthylene uglt_ ND ND Anthracene ug/L ND NO Benzo(a)anthrace ne ug/L NO ND Benzo(a)pyrene ug/L NO NO Senzo(b)fluoranthene ug/L NO ND Benzo(g,h,i)perylene ug/L NO ND Benzo(k)fluoranthene ug/L NO ND bis(2-Chloroethoxy)methane ug/L NO ND bis(2-Chloroethyl) ether ug/L ND NO bis(2- Ethyl hexyl)phthalate ug/L ND ND Butylbenzylphthalate ug/L ND NO Chrysene ug/L ND NO Di-n-butylphthalate ug/L ND ND Di-n-octylphthalate ug/L ND NO Dibenz(a,h)anthracene ug/L ND ND D(ethylphthalate ug/L NO ND Dimethylphthalate uglL ND ND Fluoranthene ug/L ND ND Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 % Rec Limits 15-120 10-120 10-120 10-120 11-131 Results presented on this page are In the units Indicated by the -Units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS Qualifiers This report shall not be reproduced, except in full, Date: 05/02/2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 28 aceAnalytical www.pacela6&wm QUALITY CONTROL DATA Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 QC Batch: 408602 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92382268001. 92382268002 METHOD BLANK: 2267154 Matrix: Water Associated Lab Samples: 92382268001, 92382268002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/30/18 19:05 LABORATORY CONTROL SAMPLE: 2267155 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 244 98 90-110 SAMPLE DUPLICATE: 2267156 92382211002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L 12.1 12.7 5 SAMPLE DUPLICATE: 2267157 92382261002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg1L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05102/2018 04:13 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 28 1�55'ceAnalytica( f www.pacMa65.torn I QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Stormwater Permit #MCG030000 Pace Project No.: 92382268 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92382268001 Saab Outfall 002 EPA 1664B 408181 92382268002 Saab Outfall 003 EPA 1664E 408181 92382268001 Saab Outfall 002 EPA608.3 408348 EPA608.3 92382268002 Saab Outfall 003 EPA608.3 408348 EPA608.3 92382268001 Saab Outfall 002 EPA 200.7 408162 EPA 200.7 92382268002 Saab Outfall 003 EPA 200.7 408162 EPA 200.7 92382268001 Saab Outfall 002 EPA 625 407970 EPA 625 92382268002 Saab Outfall 003 EPA 625 407970 EPA 625 92382268001 Saab Outfall 002 EPA 624 408127 92382268002 Saab Outfall 003 EPA 624 408127 92382268001 Saab Outfall 002 SM 2540D 408602 92382268002 Saab Outfall 003 SM 2540D 408602 Date: 05/02/2018 04:13 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 408637 408637 408325 408325 408107 408107 Page 25 of 28 Document Name: Document Revised: February 7, 2018 Sample Condition Upon Recelpt(SCUR) Page 2 of 2 Cewyf/cal ' Document No.: Issuing Authority: [ 1 F-CAR-CS•033-Rev.06 Pace Caralinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Collform, TOC, Oil and Grease, DRO/8015 (crater) DOC, LLHg "Bottom half of box is to list number of bottle Projecttl WO#:92382268 PM: AMB Due Date: 05/02/18 CLIENT: 91—Saab Barr t�tJy 7 i E to of n 7 u E e7 ' E m U m m a 6 E in = V a E in E m m .V to E m a y} L o G u a 4 _ V_ 7 .i E 4 E 4 4 N_ a Q 4 i E E 4 > s o r -C . 4 E O y 2 Q E > 7 4 } E > S a E fo O 5 1p > - G > e''i y E v, 6 E ? '� E 40 z t 4 p b E 7 Z Ci a E O 1 I Z r 3 3 4 5 fi 7 4 10 11 11 NNNN pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot R Note: Whenever there is a drscrepancY aHectfng North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (I.e. Out of hold, incorrect preservative, otn of temp, incorrect contarners. Page 27 of 28 Lawyer, Mike From: Sent: To: Cc: Subject: Attachments: Good Morning Mr. Lawyer, Anderson, Patricia <Patricia.Anderson@saabusa.com> Thursday, May 11, 2017 10:30 AM Lawyer, Mike Keller, Brian FW: Saab Barracuda Semi Annual Storm water Discharge Monitoring Report for Jan - June 2017 92338283_frc.pdf; Sssa-rdu-mel70SO9l3570.pdf Please find attached our Semi -Annual Storm water Discharge Monitoring Report for Jan -June 2017, along with PACE Analytical test results. As you will see we were below all permit benchmarks. We will send the original and a copy of the attached to the Division of Water Quality (Storm water Permitting Program) via postal service per our permit requirement. If you should have any questions/concerns, please give me a call at 910-814-3014. Regards, Patricia Anderson VP Quality/Safety/Environmental Saab Barracuda 608 East McNeill St. Lillington, NC 27546 This message is intended only for the addressee and may contain information that is company confidential or privileged. Any technical data in this message may be exported only in accordance with the U.S. International Traffic in Arms Regulations (22 CFR Parts 120-130) or the Export Administration Regulations (15 CFR Parts 730-774). Unauthorized use is strictly prohibited and may be unlawful. If you are not the intended recipient, or the person responsible for delivering to the intended recipient, you should not read, copy, disclose or otherwise use this message. If you have received this email in error, please delete it, and advise the sender immediately. Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quali y eneral Permit No. NCG030000 Date submitted .5,1l / CERTIFICATE OF COVERAGE NO.(NCG03D-2— FACILITY NAME J�GICA. j =�l7.iCQ..- 06A COUNTY 44met I PERSON COLLECTING AMPLES _ po�/ 0-/O_ ryl-11 LABORATORY A CE Lab Cert. P gg;�g3$!g Comments on sample collection or analysis: -/� rune. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR IrUI _J_ SAMPLE PERIOD Q'6`n-June ❑ July -Dec or ❑ Monthly' month DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA []Zero -flow [11�Iater Supply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, lnches' Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks =__> _ 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L 3,3 ,7� ,�vs �v.vrs a,o3�. �sv,��,IG ��7.50�►� ,q L (9_�y -za00s <v.00S ec►�`z x Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies, -'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Oat,-..1.1/1/2012-10/31/2017 SWU-245, last revised 0/25/2012 Page 1 of 3 Note: 1f you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART 8 MONITORING RESULTS: o A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART Il SECTION B. O 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. e TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one cony of this DMR, including all "No Discharge" reports. within 30 days of receipt of the lab results for at end of monitoring period Dithe case of " Discharge" reports) to.- Division of Wafterr Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: " I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those pers ns directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am award at there are significant penalties for submitting false information, 'including the possibility of fines and imprisonment for knowing violations." r (Signature of Permittee) (Date) Permit pat- 1/1/2012-10/31/2017 SWU-245, last revised 1005/2012 Page 3 of 3 s� MCDENR Stormwater Discharge Dutfall-(SDO) Qualitative Monitoring Report For,yuidanceonfillh-,goutthisfora?,please visit: htwj/portal.ncdenroref%veh/«,q/ws/su/npdessw#tab-4 Permit No.: /0 /'—' l Facility Name: -SAo,6 8(xrac,- a.A-- Co LIntV: V\ArNe." + Il1spector: Date of Inspection: rime of Inspection: --- or Certificate Of Covel'age No.-, N{C jG/ U/31015101 ;y- LLC_ 1.30 Phone No. 1t Total Evellt Precipit.atJon (inches): 3 _5 _ -3o] V 'as this a "RepreselltaO e Sif31'lll t'?nt 71" ItiIL' ?alli E?�i le Stos'lll i'.V it`L" .a5 det111CC1 ii jr 'llE' pal illlt! (See i►lformatioti below.) i Yes ❑ NO Please verilry ivhethei- Quolita ive ivlooitol h1 y must be I)CI.,Qw 7 ed duriog Q Storm el'eltt"or "rmeasureableStonn eventt'(requil-twerps vml ,, depending oil the per-niit). Qualitative monitorilig rep. uirelllents val-y. !110S: Il I-Mits 1'etluir4 r_lualitative rlionitoring to be - pel formed C 0fing 3 "reprosimtative StOI.111 eVellt" Ol' fllll-In- a "measureatble storm event." }{€ vvever some permits do not nave this reyuiremer t, Please i"efer ro these definitions, if applicable. A 'reur•esentat-ive stoat :aver." is a storm evpm- that m(e,;S.Ires greater than 0.1 il,ches Of rainfall alld that is pr-'sceded by at least 72 hom-s (3 (lays) in which 1io storm event measuring greater than 0.1 inches has occur -reel. A single storm event may contain up to 1.0 consecutive hours of no PI ecipitation. i A "measurable storm evert" is a storm event that results in an actual discharge from the I permitted site outfall. The previous measurable storm event mLlst have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to document that a shorter interval is representative for local Storm events durirl; the sampling period, and the permittee obtains approval from the local D'vVQ Regional Office. by this simW.ure, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 2 SwU•242, L-ast mourned 10/25/2012 NCDEN S Storinwater Discharge Outfall,(SDO) Qualitative Monitoring Report Forguidance 017 filling out this form, please visit: h tu: 1. cdenr. rg/web /vvtq/tivs�slt/ntldessw;�tab 4 Permit No.: NIC/G/O / or Certificate of Coverage No.: Facility Name: 5aa13 BctrAC-.aa I-t-C- _ County: 1n+c�-� Phone No. Inspector: Bate of Inspection: 1—! Time of Inspection: 1:q6- i= To'L.al Event Precipitation (inches): 3-5 'Al"s this a fl:t7rt'St.iltcitllr2 Storm Eveitt ol'StOrlll 1% nt �.]S deiincLi by dl( p.Lrillit) (See information below.) eY-G, ❑ No pkase vei- V wheti,er 011nWati, e Monitoring 17w,5t be pee onned t(ttl'liitr a .,r'epre eil o i e Storm event" r Pled ilre(TWe siur ml event" (} equir'-mea s "'my, depending oil tdie Pen -nit). Qualitative mcmitol ing reclulretnents !nary. iIHOSt perliliiS require qualitative monitorina to be performed iiui-iiig a "representative storm event" or during a "measureable storm event.," Hotlrt -er, some permits do not have this requirement. Please i efer to these definitions, if applicable. A "represetitaNve stiji-oo vent` is a storm event that measures greater than 0.I inches of rainfall and that is prec:.eded by at least 72 hours (3 days) in v%,hich m Storm event measuring greater than 0. i iffheS IMS oCCtirred. A single Acirm event may contain lip to I G consecutive IIpUrS of 110 precipitation. A "measurable storm event" is a storm ovent that:-esults in an actual discharge from the permitted site outfall. The previous measurable storm evet)t must have been at least 72 hours prior. The 72-hour storm interval does not apply if the pennittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permitteu obtains approval from the local D1NQ Regional Offce. By this signatuy.,e, i certify that this report is accurate and complete to the bestof my knoodedge: (Signature of Permittee or Designee) Page ! of 2 SWU-242, Last modified 110/25/2012 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quali y qeneral Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. NCG03L L o o-L.,, FACILITY NAME J�gGt� ?mro cQZ7 05A COUNTY r/1e PERSON COLLECTING -SAMPLES �Qkhl12i hiu4ildwyi j LABORATORY CE Lab Cert. # gc?ot+g381g Comments on sample collection or analysis: awe — Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YfAR A01 rI SAMPLE PERIOD an -June ❑ July -Dec or ❑ Monthly'_ (monttU kij (5- TO CLASS ❑ORW ❑HQW T Trout ❑PNA []Zero -flow CDVUater Supply ❑SA MAY 16 2017 []Other DVVR CENTRAI_EC FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 rION ❑ No discharge this period?z Outfall No. • •pate Sainple - Collected' (ma/i!d/yr}... 24-hour rainfall amount, 3 Inches � • Total Suspended Solids .. pH, Standard units • . Copper Lead Zinc .. Non -Polar O&G/ Total Petroleum Hyd rocar.bons ,:.,:..... Total Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 - 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L / . 41 ZV I7 3.5 3,3 mq L 6,79 L ,QUA 40.006' 0,032-. SD M5L .SD 03 y /7 3 �S . � 6 . (q <p. avS <o. ouS o, 0a2.- S v G 4-v ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date 1.1/1/2012-10/31/2017 SWU-245, last revised 10t25/2012 Page 1 of 3 r Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDANCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on inal and one covy of this OMR., including all "No Dischar e" reports within 30 days o recei t o the lab results or at end o monitorin eriod in the case o "No Discharge" reports) to: Division of Water Quality bkr1r1&a40- Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those peXrat s directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete war am athere are significant penalties for submitting false information, including the possibility of fines and imprisonment for Knowing violations." (Signature of Permittee) (Date) Permit Dat:r;—,1/1/2012-10/31/2017 SWU-245, last revised 1005/2012 Page 3 of 3 . yrC NCDGNR Stormwater Discharge Outfall-(SDO) Qualitative Monitoring Report Forguidance on filling out this farm, please visit: h ortal,ncdenr. r we w w u de w#ta -4 Permit No.: N/G/G/o / /a/o /a /t' / or Certificate of Coverage No.: N/C/G/ O/ 3/o/S/ a/ �-f-~ Facility Name: SAnb BarAc.aA LLr— County:yaPrNtA+ Phone No. -949-9:-uO Inspector: --V� Date of Inspection: Time of Inspection: 11 Total Event Precipitation (inches):_ 3.5 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "Ineasureable storm event" (requirements vary, depending oil the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." however, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this sigrAure, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Pagel of 2 SWU-242, Lastmodified 10/25/2012 yr ;I�� CDENR Stormwater Discharge Outfall'(SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: hm:././­portal.ilcdenr,orgjwe jwq/wsjsu/npdessw#tab-4 Permit No.:/a/d /p p / or Certificate of Coverage No.: N/C/G/ D// O Facility Name: Ste, County: HPcNf-A-+ Inspector: `r% Date of Inspection: Time of Inspection: f �► Total Event Precipitation (inches): 3•a Phone No. is Sp'>d /D - Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See info-n7ation below.) ' Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or `rneasureable storm event" (requirements vuiy, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A"representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatuie, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 /55'ceAnalytical' wwwpecefaba com May 02, 2017 Patricia Anderson Saab Barracuda LLC 608 E. MCNEIL STREET Lillington, NC 27546 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-0984 RE: Project: SAMPLING EVENT STQRMWATER Pace Project No.: 92338283 Dear Patricia Anderson: Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2017. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sarah Graham for Angela Baioni angela.baioni@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 26 aceAnalytical www.pacelabs.com Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 Lab ID Sample ID 92338283001 SAAB OUTFALL 002 92338283002 SAAB OUTFALL 003 SAMPLE ANALYTE COUNT Method EPA 16646 EPA 608 EPA 200.7 EPA 625 EPA 624 SM 2540D EPA 1664E EPA 608 EPA 200.7 EPA 625 EPA 624 SM 2540D REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919 )834-4984 Analyses Analysts Reported Laboratory JMS 1 PASI-C RES 27 PASI-C SH1 3 PASI-A RES 58 PASI-C GAW 34 PASI-C GJH1 1 PASI-A JMS 1 PASI-C RES 27 PASI-C SH1 3 PASI-A RES 58 PASI-C GAW 34 PASI-C CJH1 1 PASI-A Page 3 of 26 lacieAnalyfical" www.pscelabs.mn ANALYTICAL RESULTS Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 Pace Analytical Services, LLG 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: SAAB OUTFALL 002 Lab ID: 92338283001 Collected: 04/24/17 13:40 Received: 04/25/17 10:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 4-Bromophenylphenyl ether NO ug1L 5.0 1 04/28/17 10:16 05/01/17 14:49 101-55-3 Butylbenzylphthalate NO ug/L 5.0 1 04/2811710:16 05101/1714:49 85-68-7 4-Chloro-3-methylphenol ND ug1L 5.0 1 04/28/17 10:16 05/0111714:49 59-50-7 his(2-Chloroethoxy)methane ND ug/L 10.0 1 04128/1710:16 05101/17.14:49 111-91-1 bis(2-Chloroethyl) ether NO ug/L 5.0 1 04/28/17 10:16 05/01/17 14:49 111-44-4 2-Chloronaphthalene NO ug1L 5.0 1 04/2811710:16 0510111714:49 91-58-7 2-Chlorophenol NO ug/L 5.0 1 04/28/17 10:16 05/01/1714:49 95-57-8 4-Chlorophenylphenyl ether NO ug/L 5.0 1 04/28/17 10:16 05/01/17 14:49 7005-72-3 Chrysene NO u9/1- 5.0 1 0412811710A6 05/0111714:49 218-01-9 Dibenz(a,h)anthracene NO ug/L 5.0 1 04/28/17 10:16 0510111714:49 53-70-3 3,3'-Dichlorobenzidine NO ug/L 25.0 1 0412811710:16 05/0111714:49 91-94-1 2,4-Dichlorophenol NO ug/L 5.0 1 04/28/17 10:16 0510111714:49 120-83-2 Diethylphthalate NO ug/L 5.0 1 04/2811710:16 0510111714:49 84-66-2 2,4-Dimethylphenol NO ug/L 10.0 1 04/2811710A6 05/01/1714:49 105-67-9 Dimethylphthalate NO u911- 5.0 1 04/2811710:16 05/01/1714A9 131-11-3 Di-n-butyiphthalate ND ug/L 5.0 1 0412811710:16 05/01/1714:49 84-74-2 4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 0412811710:16 05/01/1714A9 534-52-1 2,4-Dinitrophenol ND ug/L 50.0 1 04/2811710:16 0510111714:49 51-28-5 2,4-Dinitrotoluene ND ug/L 5.0 1 04/28/17 10:16 05/01/1714:49 121-14-2 2,6-Dinitrotoluene ND ug/L 5.0 1 0412811710:16 05/0111714:49 606-20-2 Di-n-octylphthalate ND ug/L 5.0 1 0412811710:16 05/01/1714:49 117-84-0 bis(2-Ethyl hexyl)phthalate ND ug/L 5.0 1 04/28/17 10:16 05/01/1714:49 117-81-7 Fluoranthene ND ug/L 5.0 1 0412811710:16 05/01/1714A9 206-44-0 Fluorene ND ug/L 5.0 1 04/2811710:16 05/01/1714:49 86-73-7 Hexachloro-1,3-butadiene ND ug/L 5.0 1 04/2811710:16 05101/1714:49 87-68-3 Hexachlorobenzene ND ug/L 5.0 1 04/2811710:16 05/01/1714A9 118-74-1 Hexach lorocyclopen tad iene ND uglL 10.0 1 04/28/17 10:16 05/01/1714:49 77-47-4 Hexachloroethane ND ug1L 5.0 1 04/28/17 10:16 05/01/1714:49 67-72-1 tndeno(1,2,3-cd)pyrene ND ug1L 5.0 1 04/28/17 10:16 05/01/1714:49 193-39-5 Isophorone ND ug1L 10.0 1 04/2811710:16 05/01/1714A9 78-59-1 Naphthalene ND ug1L 5.0 1 04/28/17 10:16 05/01/1714:49 91-20-3 Nitrobenzene NO ug1L 5.0 1 0412811710:16 05/01/1714:49 98-95-3 2-Nitrophenol NO ug1L 5.0 1 04/28/17 10:16 05/01/1714:49 88-75-5 4-Nitrophenol NO ug1L 50.0 1 04/2811710:16 0510111714:49 100-02-7 N-Nitrosodimethylamine NO ug1L 5.0 1 04/28/17 10:16 05/0111714:49 62-75-9 N-Nitroso-di-n-propylamine NO ug/L 5.0 1 04/28/17 10:16 05/01/1714:49 621.64-7 N-Nitrosodiphenylamine NO ug1L 10.0 1 04128/1710:16 0510111714:49 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug1L 5.0 1 04/28/17 10:16 0510111714:49 108-60-1 Pentachlorophenol N❑ ug/L 10.0 1 04/2811710:16 05101/1714:49 87-86-5 Phenanthrene NO ug1L 5.0 1 04/28/17 10:16 05101/1714:49 85-01-8 Phenol NO ug1L 5.0 1 04/28/17 10:16 05/01/1714:49 108-95-2 Pyrene NO ug/L 5.0 1 04/28/17 10:16 0510111714:49 129-00-0 1,2,4-Trichlorobenzene ND ug1L 5.0 1 04/28/17 10:16 05/01/1714:49 120-82-1 2,4,6-Trichlorophenol NO ug1L 10.0 1 04/28/17 10:16 05101/1714:49 88-06-2 Surrogates Nitrobenzene-d5 (S) 54 % 10-120 1 04/28/17 10:16 05/01/17 14:49 4165-60-0 2-Fluorobiphenyl (S) 52 % 15-120 1 04/28/17 10:16 05/01/17 14:49 321-60-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 0510212017 05:48 PM without the written consent of Pace Analytical Services, LLC, Page 5 of 26 aceAnalytical www.peoefabxcom ANALYTICAL RESULTS Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 Pace Anatytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Sample: SAAB OUTFALL 003 Lab ID: 92338283002 Collected: 04/24/17 13:50 Received: 04/25/17 10:10 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Total Petroleum Hydrocarbons ND mg/L 5.0 1 04/27/17 06:51 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 Aldrin NO ug/L 0.050 1 04/2611713:50 04127/1716:36 309-00-2 alpha-BHC NO ug1L 0.050 1 04126/1713:50 04/27/17 16:36 319-84-6 beta-BHC NO uglL 0.050 1 04126/1713:50 04127/1716:36 319-85-7 delta-BHC ND ug1L 0.050 1 04/26/17 13:50 04/27/17 16:36 319-86-8 gamma-BHC (Lindane) NO ug/L 0.050 1 04126/17 13:50 04/27/17 16:36 58-89-9 Chiordane (Technical) NO ug/L 0.50 1 04/26/17 13:50 04/27/17 16:36 57-74-9 4,4'-DDD NO ug/L 0.050 1 0412611713:50 04/27/17 16:36 72-54-8 4,4'-DDE NO ug/L 0.050 1 04126/1713:50 04/27/17 16:36 72-55-9 4,4'-DDT NO ug/L 0.050 1 04126/1713:50 04/27/17 16:36 50-29-3 Dieldrin NO ug/L 0.050 1 04126/1713:50 04/2711716:36 60-57-1 Endosulfan I ND ug1L 0.050 1 04/26/17 13:50 04/27/17 16:36 959-98-8 Endosulfan II NO ug/L 0.050 1 04/26/17 13:50 04/27/17 16:36 33213-65-9 Endosulfan sulfate ND ug/L 0.050 1 04/26/17 13:50 04/27/17 16:36 1031-07-8 Endrin NO ug/L 0.050 1 04/26/17 13:50 0412711716:36 72-20-8 Endrin aldehyde NO ug/L 0.050 1 04/26/17 13:50 04/27/17 16:36 7421-93-4 Heptachlor NO ug/L 0.050 1 04/2611713:50 0412711716:36 76-44-8 Heptachlor epoxide NO ug/L 0.050 1 04/26/17 13:50 04/27/17 16:36 1024-57-3 PCB-1016 (Aroclor 1016) NO ug/L 0.50 1 04/26/17 13:50 04/27/17 16:36 12674-11-2 PCB-1221 (Aroclor 1221) NO ug/L 0.50 1 04/26/17 13:50 04/27/17 16:36 11104-28-2 PCB-1232 (Aroclor 1232) NO ug/L 0,50 1 04/26/17 13:50 04/27/17 16:36 11141-16-5 PCB-1242 (Aroclor 1242) NO ug/L 0.50 1 04/26/17 13:50 04/27/17 16:36 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 0.50 1 04/26/17 13:50 04/27/17 16:36 12672-29-6 PCB-1254 (Aroclor 1254) ND ug1L 0.50 1 04/26/17 13:50 04/27/17 16:36 11097-69-1 PCB-1260 (Aroclor 1260) ND ug1L 0,50 1 04/26/17 13:50 04127/17 16:36 11096-82-5 Toxaphene NO ug1L 0.50 1 04/26/17 13:50 0412711716:36 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 67 % 20-110 1 04/26/17 13:50 04127/17 1&36 877-09-8 Decachlorobiphenyl (S) 40 % 20-138 1 04/26/17 13:50 04/27/17 16:36 2051.24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2007 Copper ND mgA. 0.0050 1 05/01/1712:05 0510211714:37 7440-50-8 Lead ND mg/L 0.0050 1 05101/1712:05 05/02/1714:37 7439-92-1 Zinc 0.022 mg/L 0.010 1 05101/1712:05 05102/1714:37 7440-66-6 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Acenaphthene NO ug/L 5.0 1 04/28/1710:16 05/0111715:19 83-32-9 Acenaphthylene ND ug/L 5.0 1 04128/1710:16 05/01/1715:19 208-96-8 Anthracene NO ug/L 5.0 1 04128/1710:16 05/01/1715:19 120-12-7 Benzo(a)anthracene ND ug/L 5.0 1 04/2811710:16 05/01/1715:19 56-55-3 Benzo(a)pyrene NO ug/L 5.0 1 0412811710:16 05/0111715:19 50-32-8 Benzo(b)fluoranthene NO ug/L 5.0 1 04/28/1710:16 0510111715:19 205-99-2 Benzo(g,h,i)perylene ND ug/L 5.0 1 04/2811710:16 05/0111715:19 191-24-2 Benzo(k)fluoranthene NO ug/L 5.0 1 04/28/1710:16 0510111715:19 207-08-9 Date: 05/02/2017 05:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 7 of 26 Pace Analytical Services, LLC ® 6701 Conference Drive laceAnalyfical Raleigh, NC 27607 wwwpacelabs.cvm (919)834-4984 ANALYTICAL RESULTS Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 Sample: SAAB OUTFALL 003 Lab ID: 92338283002 Collected: 04/24/17 13:50 Received: 04/25/17 10:10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Surrogates Terphenyl-dl4 (S) 78 % 11-131 1 04/28/17 10:16 05/01/17 15:19 1718-51-0 Phenol-d6 (S) 32 % 10-120 1 04/28/17 10:16 05/01/17 15:19 13127-88-3 2-Fluorophenol (S) 43 % 10-120 1 04/28/17 10:16 05/01/17 15:19 367-12-4 2.4,6-Tribromophenol (S) 86 % 10-137 1 04/28/17 10:16 05/01/17 15:19 118-79-6 624 Volatile Organics Analytical Method: EPA 624 Benzene ND uglL 2.0 1 0412611719:07 71-43-2 Bromodichloromethane ND uglL 2.0 1 04126/1719:07 75-27-4 Bromoform ND uglL 2.0 1 04/26/17 19:07 75-25-2 Bromomethane ND uglL 2.0 1 04126/1719:07 74-83-9 Carbon tetrachloride N❑ uglL 2.0 1 04/26/17 19:07 56-23-5 Chlorobenzene ND ug1L 2A 1 0412611719:07 108-90-7 Chloroethane ND ug1L 2.0 1 04126/1719:07 75-00-3 Chloroform ND uglL 2.0 1 04/2611719:07 67-66-3 Chloromethane ND uglL 2.0 1 04/26/17 19:07 74-87-3 Dibromochloromethane ND ug1L 2.0 1 0412611719:07 124-48-1 1,2-Dichlorobenzene ND ug1L 2.0 1 04f26/1719:07 95-50-1 1,3-Dichlorobenzene N❑ ug1L 2.0 1 0412611719:07 541-73-1 1,4-Dichlorobenzene ND uglL 2.0 1 04126/1719:07 106-46-7 1. 1 -Dichloroethane ND uglL 2.0 1 04126/1719:07 75-34-3 1,2-Dichloroethane ND uglL 2.0 1 0412611719:07 107-06-2 1,1-Dichloroethene ND uglL 2.0 1 04/26/17 19:07 75-35-4 cis-1,2-Dichloroethene ND uglL 2.0 1 04126/1719:07 156-59-2 trans-1,2-Dichloroethene ND uglL 2.0 1 04/26/17 19:07 156-60-5 1,2-Dichloropropane ND uglL 2.0 1 0412611719:07 78-87-5 cis- 1,3-Dichloropropene ND ug1L 2.0 1 04/2611719:07 10061-01-5 trans-1,3-Dichloropropene ND ug1L 2.0 1 04/2611719:07 10061-02-6 Ethylbenzene ND ug1L 2.0 1 0412611719:07 100-41-4 Methylene Chloride ND ug1L 2.0 1 04/26/17 19:07 75-09-2 1,1,2,2-Tetrachloroethane ND ug1L 2.0 1 04/2611719:07 79-34-5 Tetrachloroethene ND ug1L 2.0 1 0412611719:07 127-18-4 Toluene ND ug1L 2.0 1 04/2611719:07 108-88-3 1, 1, 1-Trichloroethane ND ug1L 2.0 1 0412611719:07 71-55-6 1,1,2-Trichloroethane ND uglL 2.0 1 04/26/17 19:07 79-00-5 Trichloroethene ND ug1L 2.0 1 04/26/17 49:07 79-01-6 Trichlorofluoromethane ND uglL 2.0 1 04/2611719:07 75-694 Vinyi chloride ND uglL 2.0 1 04/26/17 19:07 75-01-4 Surrogates 4-Bromofluorobenzene (S) 93 % 70-130 1 04/26/17 19:07 460-00-4 Toluene-d8 (S) 107 % 70-130 1 04/26/17 19:07 2037-26-5 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 04/26/17 19:07 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 3.4 mg1L 2.8 1 04/27/17 00:49 Date: 05102/2017 05:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 9 of 26 (�IaceAnalytical www.pacelab&com Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 QC Batch: 358592 QC Batch Method: EPA 200.7 Associated Lab Samples: 92338283001, 92338283002 METHOD BLANK: 1988822 Associated Lab Samples: 92338283001, 92338283002 Parameter Units Copper mg/L Lead mg/L Zinc mgJL QUALITY CONTROL DATA Analysis Method: EPA 200.7 Analysis Description: 200.7 MET Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 05/02/1714:22 ND 0.0050 05l0211714:22 ND 0.010 05102/1714:22 Qualifiers Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 {919}834-4984 LABORATORY CONTROL SAMPLE: 1988823 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Copper mg/L .5 0.49 98 85-115 Lead mg/L .5 0,47 95 85-115 Zinc mg/L .5 0.49 99 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1988824 1988825 MS MSD 92338283001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND .5 .5 0.51 0.51 102 102 70-130 0 Lead mg1L ND .5 .5 0.48 0.49 96 98 70-130 2 Zinc mg1L 0 032 .5 .5 0.52 0.53 98 99 70-130 1 Results presented on this page are In the units Indicated by the -Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2017 05:48 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 26 (�5a'cieAnalytical" www.pacelaUcern QUALITY CONTROL DATA Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 LABORATORY CONTROL SAMPLE: 1986717 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers 1,1,2-Trichloroethane ug1L 20 19.5 98 52-150 1,1-Dichloroethane ug1L 20 20.3 102 59-155 1,1-Dichloroethene ug1L 20 22.6 113 1-234 1,2-Dichlorobenzene ug1L 20 20.0 100 18.190 1,2-Dichloroethane ug1L 20 20.2 101 49-155 1,2-Dichloropropane uglL 20 19A 97 1-210 1,3-Dichlorobenzene ug1L 20 19.9 100 59-156 1,4-Dichlorobenzene uglL 20 19.3 96 18-190 Benzene uglL 20 20.4 102 37-151 Bromodichloromethane ug/L 20 19.7 98 35-155 Bromoform uglL 20 15.4 77 45-169 Bromomethane ug1L 20 21.2 106 1-242 Carbon tetrachloride uglL 20 20.7 103 70-140 Chlorobenzene uglL 20 19.8 99 37-160 Chloroethane ug1L 20 23.7 118 14-230 Chloroform ug1L 20 20.9 105 51-138 Chloromethane ug1L 20 19.2 96 1-273 cis-1,2-Dichloroethene uglL 20 20.5 102 68-146 cis- 1,3-D ichloropropene ug1L 20 17.2 86 1-227 Dibromochloromethane uglL 20 18.1 90 53-149 Ethylbenzene uglL 20 19.4 97 37-162 Methylene Chloride ug/L 20 23.6 118 1-221 Tetrachloroethene uglL 20 19.4 97 64-148 Toluene uglL 20 19.3 96 47-150 trans- 1,2-Dichloroethene uglL 20 21.4 107 54-156 trans- 1,3-Dichloropropene uglL 20 17.0 85 17-183 Trichloroethene ug1L 20 19.8 99 71-157 Trichlorofluoromethane uglL 20 22.9 115 17-181 Vinyl chloride ug1L 20 18.5 92 1-251 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 93 70-130 Toluene-d8 (S) % 101 70-130 MATRIX SPIKE SAMPLE: 1986719 92338111003 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane uglL ND 20 24.9 125 46-171 1,1,2,2-Tetrachloroethane ug/L ND 20 17.3 87 73-159 1,1,2-Trichloroethane ug/L ND 20 26.0 130 64-152 1,1-Dichloroethane ug/L ND 20 25.5 127 43-172 1,1-Dichloroethene ug/L NO 20 26.2 131 48-189 1,2-Dichlorobenzene uglL NO 20 20.7 103 54-154 1,2-Dichloroethane uglL ND 20 22.3 111 42-171 1,2-Dichloropropane uglL ND 20 21.9 110 55-157 1,3-Dichlorobenzene uglL NO 20 20.2 101 57-148 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2017 05:48 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 26 aceAnalyltrcal www.pecelaba.cam Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 SAMPLE DUPLICATE: 1986718 Parameter Chloroethane Chloroform Chloromethane cis- 1, 2-Dichloroethene cis- 1,3-Dichloropropene Dibromochloromethane Ethylbenzene Methylene Chloride Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units 92338111001 Result Dup Result ug/L NO NO ug/L 3.3 3.2 uglL NO NO ugfL ND NO ug[L NO NO ug1L ND NO ug1L ND ND ug/L ND ND ug/L NO NO ug/L NO NO ug/L NO NO uglL NO NO ug/L NO NO ug1L NO NO ug/L NO NO % 86 89 % 92 93 % 109 107 RPD Qualifiers 41 3 1 2 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2017 05:48 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 26 aceAnalytrcal www.pacelabs.com QUALITY CONTROL DATA Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE 8 LCSD: 1985396 1985397 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Endosulfan II ug/L 25 0.22 0.22 90 88 1-202 3 30 Endosulfan sulfate ug1L .25 0.23 0.22 91 88 26-144 4 30 Endrin ug/L .25 0.22 0.22 88 87 30-147 1 30 Endrin aldehyde ug1L .25 0.21 0.20 85 81 50-150 6 30 gamma-SHC (Lindane) ug1L .25 0.21 0.22 83 87 32-127 5 30 Heptachlor ug1L .25 0,19 0.20 76 81 34-111 6 30 Heptachlor epoxide ug1 .25 0.19 0.19 78 77 41-126 0 30 Decachlorobiphenyl (S) % 82 77 20-138 Tetrachloro-m-xylene (S) % 77 86 20-110 Results presented on this page are In the units Indlwted by the "Units" column except whore an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2017 05:48 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 26 laneAnalXical` wwwpecetabs.com QUALITY CONTROL DATA Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 METHOD BLANK: 1988070 Matrix: Water Associated Lab Samples: 92338283001, 92338283002 Blank Reporting Parameter Units Result Limit Analyzed Indeno(1,2,3-cd)pyrene uglL ND 5.0 05/01/17 09:59 Isophorone ug1L ND 10.0 05/01/17 09:59 N-Nitroso-di-n-propylamine ug1L ND 5.0 05/01/17 09:59 N-Nitrosodimethylamine ug1L ND 5.0 05/01/17 09:59 N-Nitrosodiphenylamine uglL ND 10.0 05/01/17 09:59 Naphthalene uglL ND 5.0 05/01/17 09:59 Nitrobenzene uglL ND 5.0 05/01/17 09:59 Pentachlorophenol ug1L ND 10.0 05/01/17 09:59 Phenanthrene ug1L ND 5.0 05/01/17 09:59 Phenol ug1L ND 5.0 05101117 09:59 Pyrene ug1L ND 5.0 05101117 09:59 2,4,6-Tribromophenol (S) % 75 10-137 05/01/17 09:59 2-Fluorobiphenyl (S) % 64 15-120 05/01117 09:59 2-Fluorophenol (8) % 36 10-120 05/01/17 09:59 Nitrobenzene-d5 (S) % 64 10-120 05/01/17 09:59 Phenol-d6 (S) % 25 10-120 05/01/17 09:59 Terphenyi-d14 (S) % 80 11-131 05/01/17 09:59 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1988071 Units Spike Conc. LCS Result LCS % Rec. % Rec Limits 1,2,4-Trichlorobenzene ug1L 50 35.0 70 44-142 2,2'-Oxybis(1-chloropropane) ug/L 50 37.7 75 36-166 2,4,6-Trichlorophenol ug1L 50 44.1 88 37-144 2,4-Dichlorophenol ug/L 50 41.4 83 1-191 2,4-Di methyl phenol uglL 50 42.4 85 32-119 2,4-Dinitrophenol ug/L 250 232 93 1-181 2,4-Dinitrotoluene ug1L 50 50.5 101 39-139 2,6-Dinitratoluene ug1L 50 51.6 103 50-158 2-Chloronaphthalene ug1L 50 38.8 78 60-118 2-Chlorophenol ug1L 50 37.1 74 23-134 2-Nitrophenol uglL 50 41.5 83 29-182 3,3'-Dichlorobenzidine ug/L 100 81.0 81 1-262 4,6-Dinitro-2-methyl phenol uglL 100 94.3 94 1-181 4-Bromophenylphenyl ether uglL 50 41.7 83 53-127 4-Chloro-3-methylphenol uglL 100 86.9 87 22-147 4-Chlorophenylphenyl ether uglL 50 40.5 81 25-158 4-Nitrophenol uglL 250 88.9 36 1-132 Acenaphthene uglL 50 40.6 81 47-145 Acenaphthylene uglL 50 39.3 79 33-145 Anthracene uglL 50 42.2 84 1-166 Benzo(a)anthracene ug1L 50 43.4 87 33-143 Benzo(a)pyrene ug/L 50 43.0 86 17-163 Benzo(b)tluoranthene ug1L 50 43.2 86 24-159 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Qualifiers Results presented on this page are in the units Indicated by the -Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05102/2017 05:48 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 26 aceMalytical www.pecelabscom QUALITY CONTROL DATA Project; SAMPLING EVENT STORMWATER Pace Project No.: 92338283 OC Batch: 358192 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92338283001, 92338283002 METHOD BLANK: 1986846 Matrix: Water Associated Lab Samples: 92338283001, 92338283002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg1L ND 2.5 04/27/17 00:44 Pace Analytical Services, LI_C 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 1986847 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg1L 250 270 108 90-110 SAMPLE DUPLICATE: 1986848 92338368005 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1986849 92338356001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are In the units indicated by the "Unite" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/02/2017 05:48 PM without the written consent of Pace Analytical Services, LLC, Page 21 of 26 aceAnalytical www.pace/sU o n QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SAMPLING EVENT STORMWATER Pace Project No.: 92338283 Pace Analytical Services, LLC 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92338283001 SAAB OUTFALL 002 EPA 1664B 358230 92338283002 SAAB OUTFALL 003 EPA 1664B 358230 92338283001 SAAB OUTFALL 002 EPA 3510 357911 EPA 608 92338283002 SAAB OUTFALL 003 EPA 3510 357911 EPA 608 92338283001 SAAB OUTFALL 002 EPA 200.7 358592 EPA 2007 92338283002 SAAB OUTFALL 003 EPA 200.7 358592 EPA 200.7 92338283001 SAAB OUTFALL 002 EPA 625 358432 EPA 625 92338283002 SAAB OUTFALL 003 EPA 625 358432 EPA 625 92338283001 SAAB OUTFALL 002 EPA 624 358162 92338283002 SAAB OUTFALL 003 EPA 624 358162 92338283001 SAAB OUTFALL 002 SM 2540D 358192 92339283002 SAAB OUTFALL 003 SM 2540D 358192 Date: 05/02/2017 05:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 358284 358284 358693 358693 358591 358591 Page 23 of 26 m cm m N CA 0 N Q1 Y v n v tL x b �a N 9 � m O Y a O n C � HI iD 3 rD d H 0 � yg� m Z 4 170E m s ae Xv ZZZIXIA _...._.........................-- BP4U-115 mL Plastic Unpreserved (N/A) (CI-) MU-250 mt. Plastic Unpreserved (N/A) SP2U-500 mL Plastic Unpreserved (N/A) BPLU-1 rater Plastic Unpreserved (N/A) —"" AA8P3S-250 mL Plastic H2504 (pH <21(M) BP314.250 mL plastic HNO3 (pH < 2) BP3Z-250 mL Ptasdc ZN ACetate & NaOH (>9) BP3C-250 mL Plastic NaOH (pH 3-12) (CI-) WGFU-Wide-mouthed Glass jar Unpreserved AMU-1 liter Amber Unpreserved (N/A) (0-) AGIH-1 liter Amber HCl (pH a 2) ACOU-250 mL Amber Unpmerved (N/A) (CI-) AMS-I liter Amber H2SO4 (pH < 21 AG35-250 mLArnber H2SO4 (pH < 11 AG BA(0(334250mt Amber N1440 (NIAHCI-) W OGSH-40mL VOA IICI (N/A) VG9T40 ml. VOA Na2S203 (N/A) VG91i40 mL VOA Unp (N/A) DG9P•401nL VOA H3PO4 (NIA) VOAK (6 vials per kit)-5035 kit (NIA) V/GK (3 vlals per kit}VPHIGas kit (N/A) SPST-125 mL Sterile Plastic (NIA— lab) SPZT-250 mLSterile Plastic (NIA —lab) zz z 7 17 BP3A-250 mL Plastic (NH2)ZSO4 (9,3.9.7) GMUlner VSGU-20MI.Scintillatianvials (NIA) GN A t9 r. n 00 3 ._. a 3 n7 7 a C '* ` W t c 0 m u X N 7 y, 0 iq Cu o � n x C 0) rr A at � � O rr CL O ;T p d S 3 N O v T C rt A 7 e. O Cna g n C R 2 i V < ep N� n M A � at O l Lawyer, Mike From: Anderson, Patricia <Patricia.Anderson@saabusa.com> Sent: Tuesday, January 16, 2018 3:27 PM To: Lawyer, Mike Cc: Natt och Dag, Magnus Subject: [External] Semi -Annual Stormwater Discharge Monitoring Report for July -December: Saab Barracuda USA Attachments: Sssa-rdu-me18011613520.pdf External email Do -not click 11 inks, pr open attachments unlesss erified Send all;suspiccous email as'an.attachment.to� ', Lm@nc.gov.: fi Hello Mike, hope all is well. Please find attached Saab Barracuda USA's Semi -Annual Stormwater Discharge Monitoring Report and Test Data for July -Dec 2017 Period. 2 Hardcopies were placed in the mail, as well. The report indicates we had no discharge for this reporting period. If you should have any questions, please let me know. Thanks Patricia Anderson VP, Quality/Safety/Environmental Saab Barracuda USA 910-814-3014 This message is intended only for the addressee and may contain information that is company confidential or privileged. Any technical data in this message may be exported only in accordance with the U.S. International Traffic in Arms Regulations (22 CFR Parts 120-130) or the Export Administration Regulations (15 CFR Parts 730-774). Unauthorized use is strictly prohibited and may be unlawful. If you are not the intended recipient, or the person responsible for delivering to the intended recipient, you should not read, copy, disclose or otherwise use this message. If you have received this email in error, please delete it, and advise the sender immediately. i Semi-annual Stor:mwater Discharge Monitorin8 Report:. for North Carolina Divisionlof, water Quality eneral Pe"rm_ it:No.'NCG030000 Date submitted / �5 CERTIFICATE OF COVERAGE NO.-NCGO3 L a. FACILITY NAME _iZA'b 164 COUNTY rne_ PERSON COLLECTING SAMPLES LABORATORY Lab Cert. # " Comments oil sample collection or analysis: Part.A: StormwateT Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 15 (/ SAMPLE -,PERIOD' ❑ Jan -June [Bluly-Dec or ❑„Monthly' (month) . DISCHARGING TO CLASS, ❑ORW ❑HQW ❑Trout ❑PNA ❑Zero=fldW QWater Supply [:]SA ❑Other PLEASE REMEMBER"TO_SIG MON.PAGE5',2 AND/0113' 4 o.discharge this period?' s� i • . outfall No. F , Date Sample; Coliected ,(mo/dd/yr1` 24-hotir r'alnfall amount, s ,Inches- , Total Suspended Solids pH; Standard units Copper �, Lead Zinc Non-PolarO&G/ Total Petroleum . Frydrocarbons Total „Toxic Organics s Ber�chmarks:=> - - 100 mg/L or50 mg/L 6:o - 9.0 0.007 mg/L 0.033 mg/L 0.067.; mg/L 15 mg/L 1 mg/L z Monthly'sampling (instead of semiannual) musi'begin°with the.second conse_cutive,benchmar.k exceedance for the same parameter at the same outfall. 2:Foe sa"mpling:periods with'no,dis barge at any single outfall, you must still submit this discharge monitoring report:with a'checkmark here. 3-T he total':p�recipitation must be4ecorded..using data from an on -site rain gauge:. Unattehded,sites may be eligible for a.waiver of the rain.gauge requirement. °"See General Permit, Table 3 identifying -the especially sensitive recejVlrlgwater..classificat, ons:wheret hemoreaprotective bench mark;applies. 5 Total Toxic Organics sampling'is applicable:oniy for those facilities which perform metal finishing operations, manufacture"semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this.permit-th"e;definition of Total"Toxic"Organics is.that.definition contained in the EPA Effluent. Guidelines for the facilityaubject to the requirement to sample (for metal finishing use.the.definition as found in 40 CFR 433.11;:for semiconductor manufacture use the definition as..found inA0.CFR 469.12 for electronic crystal manufacture use"the definition as foundfin 40 CFR 469 22; and for'cathode ray tube -manufacture use.the definition found in 40 CFR 469,31). Permit Datp-1.1/1/2012-10/31/2017 SWU-245, last revised:10/25/2012 Page.1 of. 3 �' Note: if you reporta sample value In excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3`responses. See General Permit. text. FOR PART A AND,PART B MONITORING RESULTS: A BENCHMARK'EXCEEDANCE TRIGGERSTIER 1.REQUIREMENTS. SEE PERMIT PART II SECTION e. • I EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER1 REQUIREMENTS: SEE.PERMIT PART..II SECTION B. TIER+3: HAS YOUR FACILITY. HAD 4 OR MORE BENCHMA.RKEXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES, ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mallon ri in l and; ne-co of this DMA. -including all "No.DiS har e" re arts withi in the case of"No.Discharge" reports) to: Division of Water Quality LSht/i�u Attn: DWQCentral Files 1617 Mail Service Center Raleigh, North Carolina 2769911617 YOU -MUST SIGN THIS CERTIFICATION FOR ANY•INFORMATION'REPORTED: "kertify, under pen aftyiof,law,that this docunierit and all attachments were prepared under my direction or. supervision In accordance with -a system designed to assure that qualified,p'ersonnel properly gather and evaluate:the information.submitted. Based'on my inquiry of the person &r Oprsonswho rrianage.the;system,.or those persons directly responsible for;gathering the information; -the information'submitted is, to'the:best of my.knowledge and belief,,true, accurate,,and complete. I am aware that there are significant penalties1cir submitting false information, including the possibility of fines and`imprisonment for knowing violations." re of.Permlttee) Permit Dat-601/1/2012-10/31/2017 /1/S- (Date) SWU-245, last revised 10"3S/2012 Page;3 of-3 Lawyer, Mike From: Anderson, Patricia <Patricia.Anderson@saabusa.com> Sent: Thursday, January 05, 2017 9:18 AM To: Lawyer, Mike Subject: FW: Message from KM_C364e Attachments: Sssa-rdu-mel70105O7110.pdf Good Morning Mike, Happy New Year Please see the attached Semi- Annual Storm water Discharge Monitoring Report IWA NCG030503. There were no discharge during the 2016 July -Dec period (during regular scheduled operations) which met the required parameters for a rain event. The original and copy of this report will be mailed to the following address: Division of Water Quality (Storm water Permitting Program) ATTN: DWQ Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 If you should have any questions, please do not hesitate to contact me. Patricia Anderson 910-814-3014 Saab Barracuda USA 608 East McNeill St. Lillington, NC 27546 This message is intended only for the addressee and may contain information that is company confidential or privileged. Any technical data in this message may be exported only in accordance with the U.S. International Traffic in Arms Regulations (22 CFR Parts 120-130) or the Export Administration Regulations (15 CFR Parts 730-774). Unauthorized use is strictly prohibited and may be unlawful. If you are not the intended recipient, or the person responsible for delivering to the intended recipient, you should not read, copy, disclose or otherwise use this message. If you have received this email in error, please delete it, and advise the sender immediately. Semi-annual Stormwater Discharpte Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted / 5 /�7 CERTIFICATE OF COVERAGE NO. NCG030 5 FACILITY NAME wYY(%7m7GctC(�_ C�Sfi COUNTY 7?rt1L f PERSON COLLECTING SAMPLE Ati �G LABORATORY �1% __ Lab Cert. #1 f� Comments on sample collection,or analysis: Part A: 5tormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR /6 �) SAMPLE PERIOD ❑ Jan -June 2 July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS Q ._. ❑ORW ❑H W ❑Trout ❑RNA ❑Zero -flow C ater Supply []SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 [a►vo discharge this period?' Outfail No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks ===> _ 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L l�v f"/+rGU /ciu !,' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfail. 0For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only foi those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Datr;.-1 I/1/2012-10/31/2017 SWU-245, last revised 1nt25/2012 Page 1 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULT5: 0 A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 0 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. 0 TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO REGIONAL OFFICE CONTACT NAME: Mail an original and one copv of this DMR, including all "No Discharae" reports, within 30 dovs of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." t /J (Signature of Permittee) Permit DaV- 1/1/2012-10/31/2017 (Date) SWU-245, last revised P"15/2012 Page 3 of 3 1r... Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Qualit General Permit No. NCG030000 Date submitted 5 / CERTIFICATE OF COVERAGE NO. NCG030 5 _L d. FACILITY NAME ::�u6 l q/?Fa- 1� 03A COUNTY rne_ PERSON COLLECTING SAMPLESG(iiyif0,fa19'y---__ LABORATORY lJ./A Lab Cert. #i — NIA Comments on sample collection or analysis: J. Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR __11 1(JIQ} SAMPLE PERIOD [] Jan -June July -Dec or ❑ Monthly' _ (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA R EC L I VE D ❑Zero -flow []Water Supply ❑SA JAN 10 2017 ❑other CENTRAL FILE'S PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 D'M SECTION P- discharge this period?z Outfall No. ' ` `Date Sample ' Collected' (ind/dd/yrj 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L mo I Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. QFor sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Da 11/l/2012-10/31/2017 . SWU-245, last revised 5/2012 Page 1 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS; • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an on final and one copy of this DMR including all "No Discharge' reports, within 30 days of receipt of the lab results or at end of monitoring period in the case o "No Discharge" reports) to. Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) /15/1-�7- Permit Da61/1/2012-10/31/2017 • SWU-245, last revised 1�/2012 Page 3 of 3 Ir Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality G neral Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. N0003 O !S D FACILITY NAME �fqrrC'cG4 C (% COUNTY 7711717,14 f PERSON COLLECTING rkMPLES_ _ _y�/�/21jC� 6 4 '2i �--- LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR %(.C, SAMPLE PERIOD [ 1an-June ❑ July -Dec or ❑ Monthly' (month) DISCHARGING TO CLASS ❑ORW ❑HQW ❑Trout�❑PNA []Zero -flow [`Water Supply [:]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?2 Outfall No. Date Sample Collected' (mo/dd/yr) 24hour rainfall amount, Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 4 100 mg/L or 50 mg/L4 6.0 — 9.0 0.007 mg/t. 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L 'Benchmarks v ( CIU��. `� lc �C�+ �, JiU� `7. /1"�•ll.^. ��J.Gis '��,Uc�� D,�`� aCii fZ {) ; // DO �' 4f /.� f G ��' � %�. '7 � L �. U„`',---- '� C� • �%Cts� ,� G . UaS� i) U� �� -'..� • � m °%, E D. S� n� / ` Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. A See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes, For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Datp } 1/l/2012-10/31/2017 SWU-245, last revised 10125/2012 Page 1 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B, • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS, SEE PERMIT PART II SECTION B. a TIER 1 HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMii, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case o "No Discharge" reports) to: f� �7 Division of Water Quality (�7�Ur�'?L�C1/� t�i/ �r / /�J' 1 o✓€%�tii�� —� Attn,, DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r (Signature of Permittee) Permit Dat- ' 1/1/2012-10/31/2017 (Date) 1 `I 1 w SWU-245, last revised 101).S/2012 Page 3 of 3 €� MCDENR Storniwater Discharge Outfall,(SDO) Qualitative Monitoring Report For -guidance onfilling out this form, please visit: h 1.1 e enr. re web/wa /ivs/sulnudessw#tab-4 Permit No.: or Certificate of Covet -ace No.: N/C/G/0/ Facility Name: SAOLb BaCnc.,�A. t-L- (,011nty: L�Ar jf- 4 12 his pector: Date of Inspection; V/Z /1A Time of lnl pection: l oo Total Eveilt Precipiradon (inches): Phone No. 910- $14 Was this a "Representative Storm > vent." Ear '! leasnreable Storm Event" as defined by the permit? (See irlfol-Marion belo%m.) res ❑ No �lr(75 l'Li j J whe.i:her fvualitot vo +1400torllig must be pe f4rn"M a "representative ri"'or71 eve)lt 01 iT?[QSClrC?GI7jF StCll'177 2l'Gilt �7'EL�IIII �lTlplltS VC11�J, L1e21JG'17C1ii14] O11 1 j7G p8r 1TlIr�. (�€ralitative nlpnitoring r-Er�uirenlents vary. �lost perrllits redluiie dlualitati�te r��orlitoriny to be performed dluritic, a" representative storm event" or during a "nleasul-eable stclrni event." Flowe,-er, some hermits do not have this requirement. Please refer to these definitions, if applicable. A „€-epresentadve storm event" is a storin event that measures greater than 0,1. inches of nfall 311d that is preceded, by at least 72 hours (3 days} in vrhich no storm event ineasurinb greater- than 0.1 Inches has occurred. A single storm event may contain up to 10 cmisecutive Fours of no precipitation. 3f A "measurable cable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hourstorm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from Lhe local Dk,%'Q Regional Office. By hi_iArIature, 1 certify that this report is accurate and complete to the best of lny knovdedge: (Signature of Perrnittee or Designee) Page 1 of 2 $thlt,'-242, Last ;nodifted 20/25/2012 NCDENR Stormwater Discharge Outfall,(SDO) Qualitative Monitoring Report Forgufdance on filling out this form, please visit, 11ttp:C/p9.rta1.ncdenr.org/web/wq/,u .-y In=od w Permit No.. /o or Certificate of Coverage No.: N/C/C/�/�/O/.2/D / .2,�- FacilityNamte�: ,SA&)= BWAC.aA CO1111tti%: WPfCNt7T Inspector: - -� Bate of Inspection: Time of Inspection: LL,L Total Event Precipitation (inches): S Phone No. 9 10 - a I q t'iias this a "Representative Storm Event"or "Heasureable Storm Event" as defined by the perinit? {See information below.) e5 I� No Please ver;f3� v.diet}ter Qucalitative ,Alonitoring must he Fei forined daring a "representative smi-m event" or "measureable storm event" (requirements vary, dependit-g on the permit). Qualitative 1-non"staring requirernents vary. Most uermits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." HovVe✓er, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative stoma, event"is a storm event that measures gi-eater than 0.1 in ches of rainfall and that is preceded by at least 72 hours (3 days) in which no storin event measurijig greater thau 0.1 inches has occurred. A single stcrm event rrsav contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The pi-evious measurable storm event inust have been at least 72 hours prior. The 72-1,eur storm interval does not.apply if the permittee is able to document that a shorter i interval is representative for local storm events during the sampling period, and the permittee obtains approval frcm the local DWQ Regional Office, By thioi&ature, I certify that this report is acclarate and complete to the best of ;ry knowledge: (Signature of Permittee or Designee) Page 1 of 2 SwU-242, i..ast modified 10/ 25/L41Z Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted JT l If CERTIFICATE OF COVERAGE NO. NCG03 D S 0� T FACILITY NAME �h �[:4-�CUS/ COUNTY rne PERSON COLLECTING 3�e�MS LABORATORY Lab Cert. ff LDS 1g Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 010 SAMPLE PERIOD Jan -June ❑ July -Dec or []monthly' fmonth) DISCHARGING TO CLASS ❑ORW ❑HQW []Trout ❑PNA []Zero -flow [� ater Supply []SA []Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period:2 Outfall No. ' Date Sample' Collected' = (mo/dd/yr) 24-hour rainfall amount, lnches� Total Suspended Solids = pH; Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks yb� 1& - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L O 'l 00111 `O445 D•605 0.45rF DSO �L D So o / vo3 S//a �� ,Sa'' ��, L �,a �a-DUS Za.aas` dv9 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). RCCE AEA NAY 0 9 261 Permit Datp,1.1/1/2012-10/31/2017 r0MA R RLIy �1I'rT'NG SWU-245, last revised 10/25/2012 Page 1 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. 0 2 EXCEEDANCFS IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. e TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one covy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" re orts to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) 5ly/14 (Date) Permit Datl�y- 1/1/2012-10/31/2017 SWU-245, last revised 10/75/2012 Page 3 of 3 NCDENR Stormwater Discharge OutfaIl. (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: http:.//por.W.iicdgnr.org.Zweb/wQ/wu n de w#tab-4 3 Permit No.: or Certificate of Coverage No.: N/C/G/O/ Facility Name: 5AO�- &srAC .t*4—A• �-�- County: "ArNt.TT 19 Phone No. Inspector: Date of Inspection: y/Z Time of Inspection: / av Total Event Precipitation (inches): 14b Was this a "Representative Storm Event" or °Measureable Storm Event" as defined by the permit? (See information below.) es ❑ No Please verify whether- Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. . A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By thioAnature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 2 SWU-242, Last modified 10/25/2012 PA MCDENR Stor mwater Discharge Outfall- (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: httl2:/ZpoMl,iicdenr,ore/webl.wg/ws/su/­ni2dessw#tab-4 Permit No.: N/C/G/o / /Q/a /o p / or Certificate of Coverage No.: N/C/{i / Facility Name: SAab gCIrrAC,,aA County: NIPxNt4 Inspector: _ _ Date of Inspection: Time of Inspection: Total Event Precipitation (inches): ' Ux - Phone No. 910- 914- 4"ft Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) es ❑ No Please verify whetlier Qualitative Monitoring must be petformed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). i Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be Performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the f permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By thi4Aonature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 1 of 2 5WU-242, Last modified 10/25/2012 aceAnalytical e www.pacelaftwn April 29, 2016 Patricia Anderson Saab Barracuda LLC 608 E. MCNEIL STREET Lillington, NC 27546 RE: Project: METALS TESTING Pace Project No.: 92293818 Dear Patricia Anderson: Pace Analytical services, Inc. 6701 Conference Orive Raleigh, NC 27607 (919)834-4984 Enclosed are the analytical results for sample(s) received by the laboratory on April 14, 2016. The results relate only to the samples included in this report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Liamm Harrison liamm.harrison@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pagel of 29 aceAnalytical ! www.peceFaDs cam SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: METALS TESTING Pace Project No.: 92293818 Analyses Lab ID Sample ID Method Analysts Reported Laboratory 92293a18001 SAAB OUTFALL 002 92293818002 SAAB OUTFALL 003 EPA 1664B JMS 1 PASI-C EPA 608 SWB 27 PASI-C EPA 200.7 CDF 3 PASI-A EPA 625 BPJ 58 PASI-C EPA 624 GAW 34 PASI-C SM 2540D MJP 1 PASI-A EPA 1664B JMS 1 PASI-C EPA608 SWB 27 PASI-C EPA 200.7 CDF 3 PASI-A EPA625 BPJ 58 PASI-C EPA624 GAW 34 PASI-C SM 2540D MJP 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fuH, without the written consent of Pace Analytical Services, Inc.. Page 3 of 29 aceAnalytical www.pacarabs.00m ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: METALS TESTING Pace Project No.: 92293818 Sample: SAAB OUTFALL 002 Lab ID: 92293818001 Collected: 04/12/16 13:30 Received: 04/14/16 09:25 Matrix: Water Parameters Results Units Report Limit DF Prepared 625 MSSV 4-Bromophenylphenyl ether Butylbenzylphthalate 4-Chloro-3-methylphenol bis(2-C h loroethoxy)methane bis(2-Chloroethyl) ether bis(2-Chloroisopropyl) ether 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenyl ether Chrysene Dibenz(a,h)a nth racene 3,3'-Dichlorobenzidine 2,4-Dichlorophenol Diethyiphthalate 2,4-Dimethylphenol Dim ethyl phthalate Di-n-butylphthalate 4,6-pin itro-2-methyl phenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene Di-n-octylphthalate bis(2-Ethylhexyl)phthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentad iene Hexachloroethane I ndeno(1,2, 3-cd )pyrene Isophorone Naphthalene Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-N itrosodimethylamine N-Nitroso-di-n-propyiamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene 12,4-Trichlorobenzene 2,4,6-Tdchlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyi (S) Analytical Method: EPA 625 Preparation Method: EPA 625 Analyzed CAS No NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 101-55-3 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 85-68-7 ND ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 59-50-7 NO ug1L 10.0 1 04/15/16 09:01 04/19116 16:14 111-91-1 NO ug/L 5.0 1 04/15/16 09:01 04/19/16 16:14 111-44-4 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 108-60-1 ND ug1L 5.0 1 04/15/16 09:01 04/19116 16:14 91-58-7 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 95-57-8 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 7005-72-3 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 218-01-9 ND ug1L 5.0 1 04/15/16 09:01 04/19/16 1614 53-70-3 NO ug1L 25.0 1 04/1511609:01 04/19116 16:14 91-94-1 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 120-83-2 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 84-66-2 NO ug/t_ 10.0 1 04/15/16 09:01 04/19116 16:14 105-67-9 NO ug/L 5.0 1 04/15/16 09:01 04M 9116 16:14 131-11-3 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 84-74-2 NO ug1L 20.0 1 04/15/16 09:01 04/19116 16:14 534-52-1 NO ug/L 50.0 1 04/15/16 09:01 04/19116 16:14 51.28-5 NO ug1L 5.0 1 04/15/16 09:01 04/19116 16:14 121-14-2 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 606-20-2 NO ug/L 5.0 1 04/15/16 09:01 04/19/16 16:14 117-84-0 ND ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 117-81-7 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 206-44-0 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 86-73-7 NO ug/L 5.0 1 04/15/16 09:01 04/19/16 16:14 87-68-3 NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 118-74-1 NO ug/L 10.0 1 04/15/16 09:01 04/19/16 16:14 77-47-4 ND ug/L 5.0 1 04/15/16 09:01 04/19/16 16:14 67-72-1 NO ug/L 5.0 1 04/15/16 09:01 04/19/16 16:14 193-39-5 NO ug/L 10.0 1 04/15/16 09:01 04/19/16 16A4 78-59-1 ND ug1L 5.0 1 04/15/16 09:01 04/19/16 1614 91-20-3 ND uglL 5.0 1 04/15/16 09:01 04/19/16 16:14 98-95-3 NO uglL 5.0 1 04/15/16 09:01 04/19/16 16:14 88-75-5 ND uglL 50.0 1 04/15/16 09:01 04/19/16 1614 100-02-7 ND ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 62-75-9 ND uglL 5.0 1 04/15/16 09:01 04/19/15 16:14 621-64-7 NO uglL 10.0 1 04/15/16 09:01 04/19/16 16: t4 86-30-6 NO ug/L 10.0 1 04/15/16 09:01 04/19/16 16:14 87-86-5 ND ug1L 5.0 1 04/15/16 09:01 04/19/16 16:14 85-01-8 NO uglL 5.0 1 04/15/16 09:01 04/19/16 16:14 NO uglL 5.0 1 04/15/16 09:01 04/19/16 16:14 129-00-0 NO ug/L 5.0 1 04/15/16 09:01 04/19/16 16:14 120-82-1 NO ug/L 10.0 1 04/15/16 09:01 04/19/16 16:14 88-06-2 52 % 10-120 1 04/15/16 09:01 04/19/16 16:14 4165-60-0 47 % 15-120 1 04/15/16 09:01 04/19/16 16:14 321-60-8 REPORT OF LABORATORY ANALYSIS Qual This report shalt not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 29 aceAnalytical *".pacafab&=n 1 ANALYTICAL RESULTS Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: METALS TESTING Pace Project No.: 92293818 Sample: SAAB OUTFALL 003 Lab ID: 92293818002 Collected: 04/12/16 13:30 Received: 04/14/16 09:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual 1664 SGT-HEM, TPH Analytical Method: EPA 1664E Total Petroleum Hydrocarbons NO mg/L 5.0 1 04/28/16 08:44 608 GCS Pesticides and PCBs Analytical Method: EPA 608 Preparation Method: EPA 3510 Aldrin NO ug/L 0.050 1 04/1511615:54 04/1811618:20 309-00-2 alpha-BHC NO ug/L 0.050 1 0411511615:54 04/1811618:20 319-84-6 beta-BHC ND ug/L 0.050 1 0411511615:54 0411811618:20 319-85-7 delta-BHC NO ug/L 0.050 1 04/15/16 15:54 04/18/16 18:20 319-86-8 gamma-BHC (Lindane) NO ug/L 0.050 1 04/15/16 15:54 04/18/16 18:20 58-89-9 Chlordane (Technical) NO ug/L 0.50 1 04/15/16 15:54 04118/16 18:20 57-74-9 4,4'-DDD NO ug/L 0.050 1 04/15/16 15:54 04/1811618:20 72-54-8 4,4'-DDE NO ug/L 0,050 1 04115/1615:54 0411811618:20 72-55-9 4,4'-DDT NO ug/L 0.050 1 0411511615:54 0411811618:20 50-29-3 Dieldrin NO ug1L 0.050 1 0411511615:54 0411811618:20 60-57-1 Endosulfan I NO ug/L 0.050 1 04/15/16 15:54 04/18/16 18:20 959-98-8 Endosulfan II NO ug/L 0.050 1 04/15/16 15:54 04/18/16 18:20 33213-65-9 Endosulfan sulfate NO uglL 0.050 1 04/15/16 15:54 04/18/16 18:20 1031-07-8 Endrin ND uglL 0.050 1 04115/1615:54 04/1811618:20 72-20-8 Endrin aldehyde NO ug1L 0.050 1 04/15/16 15:54 04/18/16 18:20 7421.93-4 Heptachlor NO ug1L 0.050 1 04/15/16 15:54 04/1811618:20 76-44-8 Heptachlor epoxide ND ug1L 0.050 1 04/15/16 15:54 04/18/16 18:20 1024-57-3 PCB-1016 (Aroclor 1016) NO ug1L 0.50 1 04/15/16 15:54 04/18/16 18:20 12674-11.2 PCB-1221 (Aroclor 1221) NO ug1L 0.50 1 04/15/16 15:54 04/18/16 18:20 11104-28-2 PC13-1232 (Aroclor 1232) ND ug/L 0.50 1 04/15/16 15:54 04/18/16 18:20 11141-16-5 PCB-1242 (Aroclor 1242) NO ug1L 0.50 1 04/15/16 15:54 04/18/16 18:20 53469.21-9 PCB-1248 (Aroclor 1248) ND ug1L 0.50 1 04/15/16 15:54 04/18/16 18:20 12672-29-6 PCB-1254 (Aroclor 1254) ND ug1L 0.50 1 04/15/16 15:54 04/18/16 18:20 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 0.50 1 04/15/16 15:54 04/18/16 18:20 11096-82-5 Toxaphene NO ug/L 0.50 1 04/15/16 15:54 04/1811618:20 8001-35-2 Surrogates Tetrachloro-m-xylene (S) 46 % 20-110 1 04/15/16 15:54 04/18/16 18:20 877-09-8 Decachlorobiphenyl (S) 42 % 20-138 1 04/15/15 15:54 04/18/16 18:20 2051-24-3 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Copper ND mg/L 0,0050 1 04/15/16 19:00 04/22/16 20:21 7440-50-8 Lead NO mg1L 0.0050 1 04/15/16 19:00 04/22/16 20:21 7439-92-1 Zinc 0.029 mg1L 0,010 1 04/15/16 19:00 04/22/16 20:21 7440-66-6 625 MSSV Analytical Method: EPA625 Preparation Method: EPA625 Acenaphthene NO ug/L 5.0 1 04/15/16 09:01 04/19/16 16:45 83-32-9 Acenaphthylene NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:45 208-96-8 Anthracene NO ug1L 5.0 1 04115/16 09:01 04/19/16 16:45 120-12-7 Benzo(a)anthracene NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:45 56-55-3 Benzo(a)pyrene NO ug/t_ 5.0 1 04/15/16 09:01 04/19/16 16:45 50-32-8 Benzo(b)fluoranthene NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:45 205-99-2 Benzo(g,hJ)perylene NO ug/L 5.0 1 04/15/16 09:01 04/19/16 16:45 191-24-2 Benzo(k)ftuoranthene NO ug1L 5.0 1 04/15/16 09:01 04/19/16 16:45 207-08-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analyticat Services, Inc.. Page 7 of 29 Pace Analytical Services, Inc. aceAnalytical ® 6701 Conference Drive Raleigh, NC 27607 www.pacelab.oam (919)834-4984 ANALYTICAL RESULTS Project: METALS TESTING Pace Project No.: 92293818 Sample: SAAB OUTFALL 003 Lab ID: 92293818002 Collected: 04/12/16 13:30 Received: 04/14/16 09:25 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625 Surrogates Terphenyi-d14 (S) 75 % 11-131 1 04/15/16 09:01 04/19/16 16:45 1718-51-0 Phenol-d6 (S) 24 % 10-120 1 04/15/16 09:01 0411906 16:45 13127-88-3 2-Fluorophenol (S) 36 % 10-120 1 04/15/16 09:01 04/19/16 16:45 367-12-4 2,4,6-Tribromophenol (S) 75 % 10-137 1 04/15/16 09:01 04/19/16 16:45 118-79-6 624 Volatile Organics Analytical Method: EPA 624 Benzene ND ug/L 2.0 1 04/15/16 03:32 71-43-2 Bromodichloromethane ND ug/L 2.0 1 04/15/16 03:32 75-27-4 Bromoform ND ug1L 2.0 1 04Y15116 03:32 75-25-2 Bromomethane ND ug1L 2.0 1 04/15/16 03:32 74-83-9 Carbon tetrachloride ND ug1L 2.0 1 04/15/16 03:32 56-23-5 Chlorobenzene ND ug1L 2.0 1 04/15/16 03:32 108-90-7 Chloroethane ND ug1L 2.0 1 04/15/16 03:32 75-00-3 Chloroform ND ug/L 2.0 1 04/15/16 03:32 67-66-3 Chloromethane ND ug/L 2.0 1 04/15/16 03:32 74-87-3 Dibromoch lorom ethane NO ug/L 2.0 1 04/15/16 03:32 124-48-1 1,2-Dichlorobenzene NO ug/L 2.0 1 04115/1603:32 95-50-1 1,3-Dichlorobenzene NO ug/L 2.0 1 04/1511603:32 541-73-1 1,4-Dichlorobenzene NO ug1L 2.0 1 0411511603:32 106-46-7 1,1-Dichloroethane NO ug/L 2.0 1 04115/1603:32 75-34-3 1,2-Dichloroethane NO ug/L 2.0 1 04115/1603:32 107-06-2 1,1-Dichloroethene NO ug/L 2.0 1 04/15/16 03:32 75-35-4 cis-1,2-Dichloroethene NO uglL 2.0 1 04/15/16 03:32 156-59-2 trans-1,2-Dichloroethene NO ug/L 2.0 1 04/15/16 03:32 156-60-5 1,2-Dichloropropane NO ug/L 2.0 1 04115/1603:32 78-87-5 cis-1,3-Dichloropropene NO ug/L 2.0 1 04/15/16 03:32 10061-01-5 trans-1,3-Dichloropropene NO ug/L 2.0 1 04/15/16 03:32 10061-02-6 Ethylbenzene NO ug/L 2.0 1 04/15/16 03:32 100-41-4 Methylene Chloride NO ug/L 2.0 1 04/15/16 03:32 75-09-2 1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 04115/1603:32 79-34-5 Tetrachloroethene ND ug/L 2.0 1 04/15/16 03:32 127-18-4 Toluene ND ug/L 2.0 1 04/15/16 03:32 108-88-3 1, 1, 1 -Trich loroethane ND ug/L 2.0 1 0411511603:32 71-55-6 11,1.2-Trichloroethane ND ug1L 2.0 1 04/15/16 03:32 79-00-5 Trichloroethene ND ug1L 2.0 1 04/15/16 03:32 79-01-6 Trichlorofluoro methane ND ug1L 2.0 1 04/15/16 03:32 75-69-4 Vinyl chloride ND ug1L 2.0 1 04/15/16 03:32 75-01-4 Surrogates 4-Bromofluorobenzene (S) 103 % 70-130 1 04/15/16 03:32 460-00-4 Toluene-d8 (S) 105 % 70-130 1 04/15/16 03:32 2037-26-5 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 04/15/16 03:32 17060-07-0 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids NO mg/L 2.7 1 04/15/16 12:01 Date: 04/29/2016 09:26 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 29 aceAnalyficalo sww.pao&%bacam 1 QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 QC Batch: MPRP121392 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92293818001, 92293818002 METHOD BLANK: 1711756 Associated Lab Samples: 92293818001, 92293818002 Parameter Units Copper mg/L Lead mg/L Zinc mg/L Matrix: Water Blank Reporting Result Limit Analyzed ND 0.0050 0412211619:28 ND 0.0050 04/22/1619:28 ND 0,010 0412511617:30 Qualifiers Pace Analytical Services, Inc. 6701 Conference Orive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 1711757 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Copper mg/L 5 0.49 98 85-115 Lead mg/L .5 0.47 95 85-115 Zinc mg/L .5 0.46 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1711758 1711759 MS MSD 92293741004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual Copper mg/L 32.4 .5 .5 0.49 0.50 91 94 70-130 3 ug/L Lead mg/L ND .5 .5 0.45 0.46 91 93 70-130 2 Zinc mg/L 2510 .5 .5 30 3.0 89 95 70-130 1 ug1L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1711760 1711761 MS MSD 92293818002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/L ND .5 .5 0.47 0.46 94 92 70-130 2 Lead mg/L ND .5 .5 0.46 0.47 92 93 70-130 1 Zinc mg/L 0.029 .5 .5 0.47 0.47 89 89 70-130 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 29 aceAnaljftal www.pacelabscom QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 1710617 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,2-Trichloroethane ug/L 50 47.6 95 52-150 1,1-Dichloroethane ug/L 50 473 95 59-155 1,1-Dichloroethene ug/L 50 52.5 105 1-234 1,2-Dichlorobenzene ug1L 50 45.9 92 18-190 1,2-Dichloroethane ug/L 50 45.8 92 49-155 1,2-Dichloropropane ug/L 50 47.6 95 1-210 1,3-Dichlorobenzene ug1L 50 49.1 98 59-156 1,4-Dichlorobenzene ug1L 50 48.4 97 18-190 Benzene ug/L 50 48.7 97 37-151 Bromodichloromethane ug1L 50 48.5 97 35-155 Bromoform ug1L 50 45.3 91 45-169 Bromomethane ug1L 50 20.1 40 1-242 Carbon tetrachloride ug1L 50 53.9 108 70-140 Chlorobenzene ug1L 50 48.4 97 37-160 Chloroethane u911- 50 67.9 136 14-230 Chloroform ug1L 50 47.2 94 51-138 Chloromethane ug1L 50 40.5 81 1-273 cis- 1,2-Dichloroethene ug/L 50 46.6 93 68-146 cis- 1,3-Dichloropropene ug/L 50 48.0 96 1-227 Dibromochloromethane ug/L 50 48.9 98 53-149 Elhylbenzene ug/L 50 48.1 96 37-162 Methylene Chloride ug/L 50 55.1 110 1-221 Tetrachloroethene ug/L 50 42.7 85 64-148 Toluene ug/L 50 46.8 94 47-150 trans-1,2-Dichloroethene ug/L 50 46.5 93 54-156 trans-1,3-Dichloropropene ug/L 50 47.0 94 17-183 Trichooroethene ug/L 50 45.2 90 71-157 Trich lorofluoro methane ug/L 50 48.7 97 17.181 Vinyl chloride ug/L 50 48.2 96 1-251 1,2-Dichloroethane-d4 (S) % 99 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8 (S) % 101 70-130 MATRIX SPIKE SAMPLE: 1710619 92293708002 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits 1,1,1-Trichooroethane ug/L ND 20 20.9 105 46-171 1, 1,2,2-Tetra chloroethane ug/L ND 20 16.9 85 73-159 1,1,2-Trichloroethane ug/L ND 20 18.5 92 64-152 1,1-Dichloroethane ug/L ND 20 21.0 105 43-172 1,1-Dichloroethene ug/L ND 20 22.7 113 48-189 1,2-Dichlorobenzene ug/L ND 20 17.2 86 54-154 1,2-Dichloroethane ug/L ND 20 19.1 96 42-171 1,2-Dichloropropane ug/L ND 20 19.0 95 55-157 1,3-Dichlorobenzene ug/L ND 20 18.2 91 57-148 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Qualifiers Page 13 of 29 acmnalytical f www.pacela6smm I QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 SAMPLE DUPLICATE: 1710618 Parameter Units 92293708001 Result Dup Result Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Ethylbenzene ug/L ND ND Methylene Chloride ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl chloride ug/L NO ND 1,2-Dichloroethane-d4 (S) % 102 99 4-BromoRuorobenzene (S) % 102 98 Toluene-d8(S) % 103 104 RPD Qualifiers 3 4 1 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are In the units Indicated by the "Units" column except where an altemate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 0926 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 29 aceAnalytical •ww.pacele imm 1 QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 LABORATORY CONTROL SAMPLE: Parameter 1711997 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Endosulfan 11 ug/L .25 0.21 85 1-202 Endosulfan sulfate ug/L .25 0.22 87 26-144 Endrin ug/L .25 0.19 78 30-147 Endrin aldehyde ug/L .25 0.20 80 50-150 gamma-BHC (Lindane) ug/L .25 0.19 78 32-127 Heptachlor ug/L .25 0.18 72 34-111 Heptachlor epoxide ug/L .25 0.19 79 41-126 Decachlorobiphenyl (S) % 58 20-138 Tetrachloro-m-xylene (S) % 78 20-110 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Qualifiers MATRIX SPIKE SAMPLE: Parameter 1711998 Units 92293727003 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 4,4'-DDD ug/L ND .25 0.15 62 31-141 4,4'-DDE uglL ND .25 0,14 55 30-145 4,4'-DDT ug/L ND .25 0.11 44 25-160 Aldrin ug/L ND .25 0.13 52 42-122 alpha-BHC ug/L ND .25 0.14 56 37-134 beta-BHC ug/L ND .25 0.16 63 17-147 delta-BHC ug/L ND .25 0.16 67 19-140 Dieldrin ug1L ND .25 0.13 54 36-146 Endosulfan I ug/L ND .25 0.15 59 45-153 Endosulfan 11 ug/L ND .25 0.15 61 1-202 Endosulfan sulfate ug/L ND .25 0,15 62 26-144 Endrin ug/L ND .25 0.16 64 30-147 Endrin aldehyde ug/L ND .25 0.13 54 50-150 gamma-BHC (Lindane) ug/L ND .25 0,14 57 32-127 Heptachlor ug/L ND .25 0.14 55 34-111 Heptachlor epoxide ug/L ND 25 0.15 59 41-126 Decachlorobiphenyl (S) % 21 20-138 Tetrachloro-m-xylene (S) % 51 20-110 SAMPLE DUPLICATE: 1711999 92293597001 Dup Parameter Units Result Result RPD Qualifiers 4,4'-DDD ug/L ND ND 4,4'-DDE ug/L ND ND 4,4'-DDT ug/L ND ND Aldrin ug/L ND ND alpha-BHC uglL ND ND beta-BHC ug/L ND ND Chlordane (Technical) ug/L ND ND delta-BHC ug/L ND ND Dieldrin ug/L ND ND Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 29 lb aceAnalytical %".pacefabs.corrl QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 QC Batch: OEXT141974 Analysis Method: EPA 625 QC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 92293818001, 92293818002 METHOD BLANK: 1711188 Associated Lab Samples: 92293818001, 92293818002 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed 1,2,4-Tdchlorobenzene ug1L ND 5.0 04/18/46 20:26 2,4,6-Trichlorophenol ug1L ND 10.0 04/18/16 20:26 2,4-Dichlorophenol ug/L ND 5.0 04/18/16 20:26 2,4-Dimethylphenol uglL ND 10.0 04/18/16 20:26 2,4-Dinitrophenol uglL ND 50.0 04118/16 20:26 2,4-Dinitrotoluene ug/L ND 5.0 04/18/16 20:26 2,6-Dinitrotoluene ug1L ND 5.0 04/18/16 20:26 2-Chloronaphthalene ug/L ND 5.0 04118/16 20:26 2-Chlorophenol uglL ND 5.0 04118/16 20:26 2-Nitrophenol ug/L ND 5.0 04/18/16 20:26 3,3'-Dichlorobenzidine ug/L ND 25.0 04118/16 20:26 4,6-Dinitro-2- methyl phenol ug1L ND 20.0 04/18/16 20:26 4-Bromophenylphenyl ether ug1L ND 5.0 04/18/16 20:26 4-Chloro-3-methylphenol ug/L ND 5.0 04/18/16 20:26 4-Chlorophenylphenyl ether ug1L ND 5.0 04/18/16 20:26 4-Nitrophenol ug1L ND 50.0 04/18/16 20:26 Acenaphthene ug1L ND 5.0 04/18/16 20:26 Acenaphthylene ug1L ND 5.0 04/18/16 20:26 Anthracene ug1L ND 5.0 04/18/16 20:26 Benzo(a)anthracene ug/L ND 5.0 04/18/16 20:26 Benzo(a)pyrene ug1L ND 5.0 04/18/16 20:26 Benzo(b)fluoranthene ug1L ND 5.0 04/18116 20:26 Benzo(g,h,i)perylene ug/L ND 5.0 04/18/16 20:26 Benzo(k)fluoranthene ug/L ND 5.0 04/18116 20:26 bis(2-Chloroethoxy)methane ug/L ND 10.0 04/18/16 20:26 bis(2-Chloroethyl) ether ug1L ND 5.0 04/18116 20:26 bis(2-Chloroisopropyl) ether ug/L ND 5.0 04/18/16 20:26 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/18/16 20:26 Butylbenzylphthalate ug1L ND 5.0 04/18/16 20:26 Chrysene ug/L ND 5.0 04/18/16 20:26 Di-n-butylphthalate ug/L ND 5.0 04/18/16 20:26 Di-n-octylphthalate ug/L ND 5.0 04/18/16 20:26 Dibenz(a,h)anthracene ug/L ND 5.0 04/18/16 20:26 D iethylphtha late ug/L ND 5.0 04/18/16 20:26 Dimethylphthalale ug/L ND 5,0 04/18/16 20:26 Fluoranthene ug/L ND 5.0 04/18/16 20:26 Fluorene ug/L ND 5.0 04/18/16 20:26 Hexachloro-1,3-butadiene ug/L ND 5.0 04/18/16 20:26 Hexachlorobenzene ug/L ND 5.0 04/18/16 20:26 Hexachlorocyclopentadiene ug1L ND 10.0 04/18/16 20:26 Hexachloroethane ug1L ND 5.0 04/18/16 20:26 Qualifiers Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Results presented on this page are In the units indicated by the "Units- column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Page 19 of 29 aceAnalytical m wwwpat'e+abs.aom QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 LABORATORY CONTROL SAMPLE: 1711189 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits 6enzo(k)ftuoranthene ug/L 50 46.0 92 11-162 bis(2-Chloroethoxy)methane ug1L 50 38.5 77 33-184 bis(2-Chloroethyl) ether ug/L 50 42.1 84 12-158 bis(2-Chloroisopropyl) ether ug1L 50 36.8 74 36-166 bis(2-Ethylhexyl)phthalate ug/L 50 61.0 122 8-158 8 utylbenzylphtha late ug/L 50 58.0 116 1-152 Chrysene ug/L 50 44.6 89 17-168 Di-n-butylphthalate ug/L 50 53.7 107 1-118 Di-n-octylphthslate ug/L 50 65.7 131 4-146 Dibenz(a,h)anthracene ug/L 50 49.0 98 1-227 Diethylphtha late ug/L 50 47.8 96 1-114 Dimethylphthalate ug/L 50 45.1 90 1-112 Fluoranthene ug/L 50 44.0 88 26-137 Fluorene ug/L 50 43.8 88 59-121 Hexachloro-1,3-butadiene ug/L 50 28.9 58 24-116 Hexachlorobenzene ug/L 50 42.0 84 1-152 Hexachlorocyclopentadiene ug1L 50 28.9 58 25-150 Hexachloroethane ug/L 50 32.6 65 40-113 Indeno(1,2,3-cd)pyrene ug/L 50 52.2 104 1-171 Isophorone ug/L 50 42.2 84 21-196 N-Nitroso-di-n-propylamine ug/L 50 46.1 92 1-230 N-Nitrosodimethylamine ug/L 50 27.7 55 25-150 N-Nitrosodiphenylamine ug/L 50 41.8 84 25-150 Naphthalene ug/L 50 33.7 67 21.133 Nitrobenzene ug/L 50 38.6 77 35-180 Pentachlorophenol ug/L 100 77.3 77 14-176 Phenanthrene ug/L 50 42.3 85 54-120 Phenol ug/L 50 19.6 39 5-112 Pyrene ug/L 50 46.2 92 52-115 2,4,6-Tribromophenol (S) % 91 10-137 2-Fluorobiphenyl (S) % 77 15-120 2-Fluorophenol (S) % 46 10-120 Nitrobenzene-d5 (S) % 83 10-120 Phenol-d6 (S) % 33 10-120 Terphenyl-d14 (S) % 96 11-131 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Qualifiers MATRIX SPIKE SAMPLE: 1711190 92293727005 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L ND 50 14.5 29 44-142 M1 2,4,6-Tdchlorophenol ug1L ND 50 21.8 44 37-144 2,4-Dichlorophenol ug/L ND 50 12.7 25 1-191 2,4-Dimethylphenol ug/L ND 50 12.8 26 32-119 M1 2,4-Dinitrophenol ug/L ND 250 218 87 1-181 2,4-Dinitrotoluene ug1L ND 50 44.4 89 39-139 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Page 21 of 29 aceAnalytical wwwpaaeiabs.c:om QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 MATRIX SPIKE SAMPLE: 1711190 92293727005 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Fluorobiphenyl (S) % 33 15-120 2-Fluorophenol (S) % 17 10-120 Nitrobenzene-d5 (S) % 31 10-120 Phenol-d6 (S) % 11 10-120 Terphenyl-d14 (S) % 74 11-131 SAMPLE DUPLICATE: 1711191 Parameter Units 92293818002 Result Dup Result 1,2,4-Trichlorobenzene ug/L NO ND 2,4,6-Trichlorophenol ug1L NO N❑ 2,4-Dichlorophenol ug1L NO NO 2,4-Dimethylphenol ug1L NO ND 2,4-Dinitrophenol ug1L NO ND 2,4-Dinitrotoluene ug1L NO ND 2,6-Dinitrotoluene ug1L NO NO 2-Chloronaphthalene ug/L NO NO 2-Chlorophenol ug/L ND NO 2-Nitrophenol ug/L NO NO 3,3'-Dichiorobenzidine ug/L ND ND 4,6-Dinitro-2-methylphenol ug/L ND NO 4-Bromophenylphenyl ether ug/L ND ND 4-C h loro-3-methyl phenol ug/L NO NO 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitrophenol ug/L ND NO Acenaphthene ug/L NO NO Acenaphthylene ug/L ND NO Anthracene ug/L ND NO Benzo(a)anthrace ne ug/L ND NO Benzo(a)pyrene ug/L ND NO Benzo(b)fluoranthene ug/L NO NO Benzo(g,h,i)perylene ug/L ND ND Benzo(k)fluoranthene ug/L NO ND bis(2-Chloroethoxy)methane ug/L ND NO bis(2-Chloroethyl) ether ug/L NO NO bis(2-Chloroisopropyl) ether ug/L NO NO bis(2-Ethyl hexyl)phtha late ug/L NO NO Butylbenzytphthalate ug/L NO NO Chrysene ug/L NO NO Di-n-butylphthalate ug/L NO ND Di-n-ocWphthalate ug/L NO NO Dibenz(a,h)anthracene ug/L ND NO Diethylphthalate ug/L ND NO Dimethylphthalate ug/L NO NO Fluoranthene ug/L NO NO RPD Qualifiers Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Page 23 of 29 m 5aceAnaljftal 1�lwww.pacdgb&com I QUALITY CONTROL DATA Project: METALS TESTING Pace Project No.: 92293818 QC Batch: WETl44273 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92293818001, 92293818002 METHOD BLANK: 1711144 Matrix: Water Associated Lab Samples: 92293818001, 92293818002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L NO 2.5 04/15/16 11:57 Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 LABORATORY CONTROL SAMPLE: 1711145 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 262 105 90-110 SAMPLE DUPLICATE: 1711146 92293727001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 7.6 10.2 29 D6 SAMPLE DUPLICATE: 1711147 92293750002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 11.2 10.6 6 D6 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/29/2016 09:26 AM without the written consent of Pace Analytical Services, Inc.. Page 25 of 29 aceAnalytical® www.pacelabsaam QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 6701 Conference Drive Raleigh, NC 27607 (919)834-4984 Project: Pace Project No.: METALS TESTING 92293818 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92293818001 SAAB OUTFALL 002 EPA 1664B GCSVI24816 92293816002 SAAB OUTFALL 003 EPA 1664B GCSV124816 92293818001 SAAB OUTFALL 002 EPA 3510 OEXTY41995 EPA 608 GCSV124700 92293818002 SAAB OUTFALL 003 EPA 3510 OEXT141995 EPA608 GCSV/24700 92293818001 SAAB OUTFALL 002 EPA 200.7 MPRP121392 EPA 200.7 ICPI19215 92293818002 SAAB OUTFALL 003 EPA 200.7 MPRPl21392 EPA 200.7 ICPI19215 92293818001 SAAB OUTFALL 002 EPA 625 OEXTI41974 EPA625 MSSV/12131 92293818002 SAAB OUTFALL 003 EPA 625 OEXT141974 EPA625 MSSV112131 92293818001 SAAB OUTFALL 002 EPA 624 MSVl36377 92293818002 SAAB OUTFALL 003 EPA 624 MSVl36377 92293818001 SAAB OUTFALL 002 SM 2540D WET144273 92293818002 SAAB OUTFALL 003 SM 2540D WET144273 Date: 04/29/2016 09:26 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 27 of 29 CHAIN -OF -CUSTODY I Analytical Request Document The Chain -of -Custody is - 'a LEGAL DOCUMENT. All relevant fields must be completed accuratety. 0 CD Section A Section B secthm r ReWred Client intoffnation: Ramfired Protect Inf—Bon- Invoice Irdorrnatlow Pane I Of COMParY Saab Barr=da LLC Report TO: !to Menton: tricia Arxknon Addrew 05 E. MCNEIL STREET Copy Tcr. Company Narner. Lillingwn. NC 27546 cee;= Address: g ftg Email: pavjaa.ardecom Purchase Order V: Pace Quote: Phone: 1a 2084 Fax Project Nam: Metals Testing Pow PmjeO Manager: . ILwnrrLharn&on@paceh3bz cam. L50caticn 7r M, —17e�75,- Requested Due Date: Project It Pow Profile 0: 5158-9 f— E, z MIFRIK COX 0 COLLECTED z Preservatives z- 4? OdAft wA. Dw WT Q rtieany P 9 SAMPLE ID aws .1 0 N ad OL z START ENO w One Cheater per boa.W.P. ova JA-7, 0.9 1, .1 All AR 0� 07 Sample Us must be unique T— TS w r F 2 z F, Z DATE TIME DATE TIME :5 -C/ 6oak-,)-6 16 4041 -11all" 0:)l -4a z PRINT Name of SAMPLER: K SIGNATURE Signed: of w • • .!► C2f 15- CDENR Stormwater Discharge, OutfaIl.(SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. h=://i)ortal.iicdenr.org./wgb/wQ/ws/su/nl2dessw#tab-4 Permit No.: N/C/G/o //�/d /a /' / or Certificate of Coverage No.: N/C/G/�// Facility Name: S,Aab BmraCucl—a LLC county-. v�Pr N#04 Phone NO. 910- $14-�4%Sb ., , . - Inspector: M - to-1+-1 Date of Inspection: 0 Time of Inspection: 16 Total Event Precipitation (inches): 01 16 /l Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verb/ whether Qualitative Monitoring must be pelfO]-172ed during a "representative storm event" or `measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a °measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this si n ture, I certify t t] ' report is accurate and complete to the hest of my knowledge: (Signature of Permittee or Designee) SWU-242, Last modified 10/25/2012 Page 1 of 2 f t !Cyr - , i a7 /GZa &Z � NCDENR • Stormwater Discharge, Outfall. (SDO) 41, w,,j Qualitative Monitoring Report For guidance on filling out this form, please visit: hn://,Dortal.iicdenr.ora/web/wa./ws/su/nDdessw#tab-4 essw#tab-4 Permit No.: N/C/G/0 /a/O/cl /Q la / or Certificate of Coverage No.: Facility Name: -SAn�- BcxrAC..LA► L-V— County: V\PWNf E+ Phone No. 910"-RI4-q%Sg=-go/f/ _ Inspector: Date of Inspectian: Time of Inspection: Total Event Precipitation (inches): i 1 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify Whether Qualitative Monitoring must; be pellormod during a "representative store? • evert" or "177easureable storm event" (requirements vary, depending ojr the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 fours (3 days) in which no storm event measuing greater than r 0.1 inches has occurred. A single storm event tnay contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, 1 c tify that this report is accurate and complete to the best of my knowledge:1113J(Jfl�— (Signature of Permittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 Pat McCrory Govemor WENR m North Carolina Departent ofEnVironment and Natural Resources June 23, 2014 Saab Barracuda LLC Attn: Marls Cauthen, Quality/Safety/Environmental Manager 608 East McNeill Street Lillington, NC 27546 Subject: Request for Regulatory Relief from Monthly Monitoring - Saab Barracuda LLC General Permit NCG030000, Certificate of Coverage NCG030502 Harnett County Dear Mr. Cauthen: John E. Skvarfa, III Secretary The Fayetteville Regional Office of the Division of Energy, Mineral and Land Resources, Land Quality Section is in receipt of your letter requesting regulatory relief from monthly monitoring due to occasional exceedances of the benchmark value.for copper and consecutive exceedances of the benchmark value for zinc at outfall 2, which has triggered the monthly monitoring requirements as outlined in the Tier Two response actions of the NCG030000 General Permit. Please keep in mind that benchmark exceedances are NOT limit violations or violations of permit conditions; however, you are obligated to follow the tiered response actions outlined'in your permit. Prior to receipt of your letter, a Compliance Evaluation Inspection was conducted by Mike Lawyer of this office on October 31, 2013. At the time of theinspection, the facility was found to be in compliance with the tiered response actions and. other conditions of the NCG030000 General Permit. During the inspection, it was relayed that some potential sources for the exceedances had been identified such as a large metal warehouse building adjacent to outfail 2, metal pallets stored outside and some scrap metal in open top dumpsters. A follow-up site visit was conducted by Mike Lawyer on June 3, 2014 to discuss,monthly monitoring results and any actions taken to address or account for the exceedances. As observed during the June. 3, 2014 site visit and/or outlined in your letter; the metal pallets were relocated, indoors, the scrap metal dumpsters were moved to the other side of the facility and sampling was conducted at two roof drains coming directly off the warehouse building, which resulted in benchmark exceedances for zinc. In addition to these actions, facility personnel confirmed that zinc is not used in any part.of the manufacturing process. Based on the aforementioned items, we are granting regulatory relief in the form of a collapsed Tier 2 - Tier 3 response. Upon receipt of this letter, Saab Barracuda LLC may resume the permit specified semi-annual analytical monitoring for the remainder of the current permit term. Your current permit is set to expire on October 31, 2017.7his decision applies only to the copper and zinc benchmarks. A benchmark exceedance of any other parameter listed In your permit will trigger the tiered response actions as described in the general permit. You must notify this office, in writing, within five business days if you become aware of any significant source of copper or zinc at your facility that has the'potential to be exposed to stormwater. The -relief granted in this letter is contingent upon the current industrial practices at Saab Barracuda LLC. If industrial practices change and copperor zinc does become a significant stormwater exposure risk then this office reserves the right to .withdraw this decision and reinstate the permit specified tiered response or other actions that may be .warranted by the new set of circumstances. Division of Energy, Mineral and Land Resources Land Quality Section Fayetteville Regional Office, 225 Green Street - Suite 714, Fayetteville, North Carolina 28301 Phone: 910-433-3300 /.FAX: 910-486-0707/ Internet: hgp://Dodal.nedenr,org./web![r/ Plea§e retain and ' append this letter. to, your Stormwater Pollution Prevention Plan (SPPP) or permit. If you have any questions or concerns, please contact Mike Lawyer or myself at (910) 433-3300. Sincerely, Brad Cole, PE Regional Engineer Land Quality Section BC/ml 0c: Bethany Georgoulias — Stormwater Permitting Program .(via e-mail) FRO — Land Quality Section, Stormwater Files-NCG036602 SAMPLE COLLECTION YEAR _ 0?0 SAMPLE PERIOD ❑ Jan -June my -Dec or ❑ Monthly' (month} DISCHARGING TO CLASS ❑ORW ❑HQW [Trout ❑P ❑Zero -flow EeVVater Supply SA ❑Other ��' � Q��r'i�rr�1, ,�L1ir•-�� G / , Alll�, Semi-annual Stormwater Discharge Monitoring Re ort for North Carolina Division of Water Quality general Permit No. NCG030000 Date submitted / 5 CERTIFICATE OF COVERAGE NO. N0003 1) S d 2 FACILITY NAME 3Gct6 Mrra COUNTY C,rr) PERSON COLLECTING SAMPLES T7?a k ltlerJlx) LABORATORY CI _ Lab Cert. # Va �yi�s d 9z�7'�993 Comments on sampip collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results 6� EefflVEPLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 JAN 0 7 2016 CENTRAL~ FILES DWR gF:r.TIrw ❑ No discharge this period?" - Outfall No. ` Date Sample' Collected' (mo/dd/yr) 24-hour rainfall- amount, Inches Total Suspended Solids pH Standard units Copper Lead Zinc Non-Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organicss Benchmarks 100 mg/L or 50 mg/L 6.0 -- 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L (2u1611 60,2, l0aj( Ir 0,/0" (�.q 0,06ggI+d%L --U,00° M fc- U Ab L�lrUs,v. )ul./ ll 003 ►o a$ rS L 10" 5•(0 nr D, Iq fall 00� Jlf3Uf lS V'lSy� r �` CSrO�S � 0&/,4 l 003 11I3o1rf p,151, 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Dab' 1/1/2012 -10/31/2017 SWU-245, last revised 1 25/2012 0 Page 1 of 3 Note: eyou report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Moil an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Quality ,1-116rml(,a,� Attn: DWQ Central Files JJ 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) (Date) Permit Dat 1/1/2012-10/31/2017 SWU-245, last revised 1o/2012 0 0 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring „Report for North Carolina Division of Water Qualit General Permit No. NCG0300'01© Date submitted l V3 a�U � CERTIFICATE OF COVERAGE NO(N 03 U S Q ==II11 SAMPLE COLLECTION Y , FACILITY NAME �GiQh �ljfy SAMPLE PERIOD an -June ❑ July -Dec COUNTY /' or ❑Monthly' Di PERSON COLLECTIN MPL S , �Ll/.11-�� DISCHARGING TO CLASS ❑ORW ❑HQW [:]TroutMAA LABORATORY Lab Cert. # ���'�ll i ❑zero- low [:]Water Supply' []SA OtheComments on sample collgction or analysis _ 1 V �D Part A: Stormwater Benchmarks and Monitoring Results DEC Q I 201JLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 CENTRAL F1L ES DWR SECTION [/No discharge this period?2 Outfail No. Date Sample Collected' (md/dd/yr) 24-hour rainfall amount, Inches 3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L I ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals,.or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit 1611/1/2012-10/31/2017 SWU-245, last revised 1 Z5/2012 0 - Page 1 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART it SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of_"No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete, am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) -76 ii1a3/,ls (Date) Permit Da 1/1/2012-10/31/2017 • SWU-245, last revised 1 5/2012 0 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 4 CERTIFICATE OF COVERAGE NO. NCG03 0 5 U FACILITY NAME COUNTY n�e�'� _^ PERSON COLLECTING SAMPLES AA -CA LABORATORY Lab Cert. # _ Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR ' .J14 SAMPLE PERIOD ❑ Jan -June my -Dec or ❑ Monthly' (month) 4kpRGING TO CLASS ❑ORW ❑HQW ❑Trout ❑PNA �s ►�j,J ❑Zero -flaw ❑Water Supply [:]SA�� zo�� ❑Other G C O$ PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 3 D No discharge this period: Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar 0&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks 100 mg/GL 5CA 0 mg/L4 0 -9.0 0!V�.007L7 0.0.a3"v3�ml' g/.StL.�, 0.067 mgn/L 15L m/.g�/'L 0C09Mr G.00ii 0.7aV {l`1 JVliTQ` >� . LoMr �6.- �mgM/5L J1 j` oV 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date,11/1/2012-10/31/2017 _ SWU-245, last revised 1-0/25/2012 Page 1 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lob results (or at end of m_ o_ nitorina_ period in the case of "No Discharge" reports to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there,are signifycant penalties for submitt'ng false information, including the possibility of fines and imprisonment for knowing violations." {Signatur6of Perm lakk �i (Date) Permit Date- 11/1/2012-10/31/2017 SWU-245, last revised In /25/2012 Page 3 of 3 ,P!wrwwrA- ram' w. CDER Stormwater Discharge Outfall, (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit: httD_//uoi-tal.iicdenr.ore/web jwn/ws,/su/nudessw#tab-4 Permit No.: N/C/G /0 /3/0/c5/0 /i? / or Certificate of Coverage No.: Facility Narne: Swab BcsrAC .41A LLC- County: �Nt-A4 Phone No. 910-$1Li--4%Sd Inspector: M , C/ 1 --+ Date of Inspection: lilt -III Time of Inspection: 1; 3-,, t� .�— `« Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) VYes ❑ No Please verify whether- Qualitative Monitoring must be per fiat razed during a "representative stormy event" of ineasureable storm event" (requirements vary, depending on the per mit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "reuresentaLive storiai event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0,1 inches has occurred. A single story» event may contain up to 10 consecutive hours of no precipitation. A "measurable storm eveni" is a storm event that results in an actual discharge from the permitted site outfalI. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter 3 interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this s0ature, lAertify Oat this report is accurate and complete to the best of my knowledge: IDeli E [Signature of Permittee or Designee) Pagel of 2 SWU-242, Last modified 10/25/2012 DENR Stormwater Discharge Outfalf (SDD) Qualitative Monitoring Report Forguidartce on filling out this form, Please visit: htti):/ t-tal.ncdenr,ore/web./wq.ws/su/nDdessw4tab-4 Permit No.: N/C/G /0 /a/0/12/0 /t / or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/ Facility Name: SAM", BcxrAc.aA I -LC -- County: x-\Fc Nt-'4 Phone No. 910, 81I1--14%Sb Inspector: Fri • CA4 w Date of Inspection: 14i Time of Inspection: T r� Total Event Precipitation (inches): L 3`:� Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) es ❑ No Please verij�, whether- QUO tative Monitoring musi be performed during a "representative star in event" or'Meosur'eable storm event" (requirements vary, depending on the permit), Qualitative monitoring requirements vary. most permits require qualitative monitoring to he performed during a "representative storm event" or during a "measureab_le storm event." However, some permits do not have this requirement, Please refer to these definitions, if applicable. A "representative stormi event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours [3 clays) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 coizsecutive hours of no precipitation. A Iiieasurable storm event" is a storm event That results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter i interval is representative for local storm events during the sampling period, and the permittee i obtains approval from the local DWQ Regional Office. By this sWnature;ll certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Designee) Page 2 of 2 SWU-242, Last modified J d/25/2012 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE NO. N0003 U S` z- FACILiTY NAME S�4,, COUNTY i_cZe V- PERSON COLLECTING SAMPLES ik -G{ , LABORATORY Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2iD1—( SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or �Ionthlyl A:: month DISCHARGING TO CLASS ❑ORW ❑ QW ❑Trout ❑PNA ❑Zero -flow ❑Water Supply [:]SA ❑Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period: Outfall No. Date Sample p Collected' (mo/dd/yr) 2�4-hour rainfall amount, Inches s Total Suspended Solids PM, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic s Organics Benchmarks ===> - - 100 mg/L or 50 mg/L4 6.0 - 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L QL kt tq- a, 0,02`4 " 0.0-23 Prn �-`` 1 14 sl I s1 I� O o 3,6 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 4 tube manufacture use the definition found in 40 CFR 469.31), to Team, IIW, raI Permit Date:21/1/2012-10/31/2017 1►y17M Page 1 of 3 Facilities than incorporate a solvent management plan into the Stormwater POI luLion Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shali sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." Name (Print name) Title (Print titl0 e tN U {Signature} (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format, "<XX me/I_", where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B. Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period ?2 Outfall No. Date Sample Collected,. (mo/dd/yr) 24-hour rainfall amount, Inches' Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_=> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3; HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES n NO ❑ REGIONAL OFFICE CONTACT NAME: 11\1k,ti LVAw it Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware thaX there are t ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permittee) f u �- (Date) Permit Date, 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 — < -t Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted q( z-',,''f CERTIFICATE OF COVERAGE NO. NCG03 0 5- s7 a FACILITY NAME SIAQ,�- L.Ae... QLC COUNTY 1� r1,1L 'r PERSON COLLECTING SAMPLES 6A, G4JtL--- LABORATORY lle*te. Lab Cert. # Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR 2,011.1-A SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or EIGlonthly1 Ale,k (month) RDIISCHARG�IrNG TO CLASS ❑ORW ❑HQW [:]Trout ❑PNE(A Ei V E1) ❑Zero -flow ❑Water Supply [:]SA APR 2 5 2014 ❑Other CENTRAL F)PIL ASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 Lt:DWO/BOG ❑ No discharge this period: Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics5 Benchmarks =__> _ - 100 mg/L or 50 mg/L° 6.0 — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 001z -141 4 LS1% NC NC ^1C NC 0(.54 NG 41 lal+ LT ItNC &�< N C 44C . l Q N C. tV A,- k . 2s e, Or— NC NC /y C' /%K At w Z g,� ?r5 " N 'L N G �t G N C e� NG ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. " See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. S Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 5WU-245, last revised 10/25/2012 Page 1 of 3 1 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the Tf0 monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (T O), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the stormwater Pollution Prevention Plan." M CO, Name (Print name) QV 4tAl t I Title (Print title) ILK (Signs ure) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be reported in the format. "<XX mg/L!' , where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Qutfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar O&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks =_=> - - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See Genera! Permit text. FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: (� ty VKW—%w4 �$rvti ,�+5 'Crav0,., Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature &f Permittee) q 1,114 (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted 2 11.4 CERTIFICATE OF COVERAGE NO. NCG03 O -EQ '2 FACILITY NAME o &xra CvJ& Ur — COUNTY OM;ift PERSON COLLECTING SAMPLES �+► LABORATORY ?"e Lab Cert. fi Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR TO V*A SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or [��onthly1 ?;02 month RECEIVED ` w ��VDI�H�GING TO CLASS ❑ORW ❑HQW [:]Trout ❑PNA ❑Zero -flow [:]WaterSupply [:]SA MAR 0 4 2014 ❑Other CENTRAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 DWQ/BOG No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches; Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics5 Benchmarks ===> - - 100 mg/L or 50 mg/L4 6A — 9.0 0.007 mg/L 0.03 mg/L 0.067 mg/L 15 mg/L 1 mg/L 0 tl oo Z Z 1°I S "00 0.01,11 ta.,. l ► �. U.4 ' Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. Z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. -'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 Facilities that incorporate a solvent management plan into the Stormwater Pollution Prevention Plan may so certify, and the requirement for TTO monitoring may be waived. The solvent management plan shall include a list of the total toxic organic compounds used and the other elements listed in the General Permit. For those facilities electing to employ the TTO monitoring waiver, the discharger shall sign the following certification statement: "Based upon my inquiry of the person or persons directly responsible for managing compliance with the permit monitoring requirement for total toxic organics (TTO), I certify that to the best of my knowledge and belief, no dumping of concentrated toxic organics into the stormwater or areas which are exposed to rainfall or stormwater runoff has occurred since filing the last discharge monitoring report. I further certify that this facility is implementing the all the provisions of the solvent management plan included in the Stormwater Pollution Prevention Plan." M AA, Name (Print name) i Title (Pri t title) (Sign at e) (Date) Note: Results must be reported in numerical format. Do not report Below Detection Limit, BDL, <PQL, Non -detect, ND, or other similar non -numerical format. When results are below the applicable limits, they must be re orted in the format "<XX m L" where XX is the numerical value of the detection limit, reporting limit, etc. in mg/L. Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. Part B: Vehicle Maintenance Area Monitoring Results: only for facilities averaging > 55 gal of new oil per month. ❑ No discharge this period?' Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches3 Non -polar 0&G/TPH by EPA 1664 (SGT-HEM) Total Suspended Solids pH Benchmarks -__> _ - 15 mg/L 100 mg/L or 50 mg/L* 6.0 — 9.0 SU Footnotes from Part A also apply to this Part B * See General Permit text, Table 5, identifying the especially sensitive receiving water classifications where the more protective benchmark applies. Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 2 of 3 Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. FOR PART A AND PART B MONITORING RESULTS: A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an original and one copy o f this DMR including all "No Discharge" reports within 30 days of receipt of the lab results for at end of monitoring period in the case of "No Discharge" reports) to: Division of Water Quality Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am awarg that theta are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signat4re of Permittee) ZZ,i! (Date) Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 Page 3 of 3 Semi-annual Stormwater Dischar a Monitorin Report for North Carolina Division of Water uality General permit No. NCG030000 Date submitted 7,236114 CERTIFICATE OF COVERAGE NO. NCG03 0 S o �2 SAMPLE COLLECTION YEAR w... SAMPLE PERIOD Ja June Jul D FACILITY NAME �'�► b a�- L tG_ �- ❑-Y ec COUNTY i--}-� _ _ or Monthl:, a month PERSON COLLECTING SAMPLES M-G V (b. DISCHARGING TO CLASS ❑ORW ❑HQ []Trout ❑PNA LABORATORY. K e— _ Lab Cert. # ❑Zero -flow ❑Water Supply []SA Comments on sample collection or analysis- ❑Other '-: Part A: Stormwater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 ❑ No discharge this period?z Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, Inches Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic Organics Benchmarks =__> _ - 100 mg/L or 50 mg/L 6.0 -- 9.0 0.007 mg/L 0.033 mg/L 0.067 nig/L 15 mg/L 1 mg/L COP -fi,, ao 1 0.005 a S.O <o. 001�) WAN A0 � d oas C� e w� o t S.a U <0.05-1a 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter atthe same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a che,ckmark here. 'The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. ° See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. 'Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes.. For purposes.of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CPR 469.12; for electronic crystal manufacture use the definition as found in 40 ,CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CPR 469.31). c Permit Date: 11/1/201Z-10/31/2017 SWU-245, last revised 10/25/2012 Page 1 of 3 r1k Semi-annual Stormwater Discharge Monitoring Report for North Carolina Division of Water Cluality General Permit No. NCG030000 Date submitted I ZS4 .f4 CERTIFICATE OF COVERAGES No. NCG03 0 5 O a FACILITY NAME Sib >y p c_v�-A L tiG COUNTY PERSON COLLECTING SAMPLES Iy\-LA,10—e4 LABORATORY.Pt,C.0 Lab Cert Comments on sample collection or analysis: Part A: Stormwater Benchmarks and Monitoring Results SAMPLE COLLECTION YEAR SAMPLE PERIOD ❑ Jan -June ❑ July -Dec or EMo1nthly" A-;,: month DISCHARGING TO CLASS ❑ORW [:]HQ[:]Trout❑PNA ❑Zero -flow ❑Water Supply ❑SA JAN 2-7.2014 ❑Other ;Eiji i RAL FILES PLEASE REMEMBER TO SIGN ON PAGES 2 AND OR 3 4 DWQIBOG ❑ No discharge this period:2 Outfall No. Date Sample Collected' (mo/dd/yr) 24-hour rainfall amount, inches3 Total Suspended Solids pH, Standard units Copper Lead Zinc Non -Polar O&G/Total Total Petroleum Hydrocarbons Toxic Organics Benchmarks 100 mg/L or 50 mg/L4 6.0 -- 9.0 0.007 mg/L 0.033 mg/L 0.067 mg/L 15 mg/L 1 mg/L 03,-� ; i`f ;20 l �. O.00S Q l S O <O•rDS to5 Q Q b o S.osor <O.arM 1 Monthly sampling (instead of semi-annual) must begin 'With the second consecutive benchmark exceedance for the same parameter at the same outfall. 2 For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. 4 See General Permit, Table 3 identifying the especially se6sitive receiving water classifications where the more protective benchmark applies. 5 Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes., For purposes.of this,permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469,12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). IR Permit Date: 11/1/2012-10/31/2017 SWU-245, last revised 10/25/2012 . • Page 1 of 3 0 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. PART AAND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS, SEE PERMIT PART II SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER ATTHE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ❑ NO ❑ IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: Mail an oriainal and one copy of this DMR, including all "No Discharge" reports, within 30 days of receipt of the lab results (or at end of monitoring period in the case o "No Discharge" reports) to: Division of Water Quality rnwa�b- Ant�"!ti�►1Trasr+�r.� Attn: DWQ Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that There are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee) i[Z31 It+ (Date) Permit Da t /1/2012-10/31/2017 SWU-245, last revised 1 /2S/2012 1 I� 0 Page 3 of 3 ........ ---....._..-.,-_...------- L, Semi-annual Stormwater Discharge Monitoring Re vrt for North Carolina Division of Water Qu lity General Permit No. NCG030000 Date submitted CERTIFICATE OF COVERAGE N . NCG03 O S 0 SAMPLE COLLECTION YEAR '20k SAMPLE PERIOD Jan -June u ` D FACILITY NAME �•� �ri�-t..�r, �(� ❑ ❑ h+- ec COUNTY Aor [0,Monthly1_-_ G `� (month) PERSON COLLE NG SAMPLESI I'�`iM� DISCHARGING TO CLASS F ]ORW ,E]HQW []Trout ❑PNA LABORATORY 4ce _ Lab Cert. # ❑Zero -flow: ❑Water Supply ❑SA Comments on sample collection or analysis: ]Other Part A: 5tormuuater Benchmarks and Monitoring Results PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 -✓ No discharge this period Outfall No. Date Sample, Collected 1 (rno/dd/yr) 24-hour rainfall amount, Inch es3 Total Suspended Solids pH, Standard units Copper Lead - ;'," Zinc ': ; on -Polar O&G/ Total Petroleum Hydrocarbons Total Toxic s Organics Benchmarks ===> _ - 100 mg/L or 50 mg/L 6.0 — 9.0 0.007 mg/L 0.033 mg/L 0.067 ini(L 15 mg/L 1 mg/L �t�.E�� 1. t3,pS U -7. l0 5.1 0 0 1. 0.005 L,->-) `' 'I 4� 4 <c�.�o i 1 Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same para peter at the same outfall. zFor sampling periods with no discharge at any single outfalI, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation must be recorded using data from an on -site rain gauge. Unattended sites maybe eligible for a waiver 64 the rain gauge requirement. a See General Permit, Table 3 identifying the especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable only for those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22, and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). I Permit Datew11/1/za12-10/31/2a1'7 SWU-245, last revised 1 0/25/2012 Page 1 of 3 g ISA Note: If you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier responses. See G FOR PART A AND PART B MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER 1 REQUIREMENTS. SEE PERMIT PART 11 SECTION B. • 2 EXCEEDANCES IN A ROW FOR THE SAME PARAMETER AT THE SAME OUTFALL TRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PAR • TIER 3: HAS YOUR FACILITY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER AT ANYONE OUTFALL? YE IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME: in the case o "No Discharge" reports) to. Attm DWQ Central Files l 1617 Mail Service Center Raleigh, North Caroiina 27699-1617 YOU MUST SIGN THIS CERTIFICATION FOR ANY INFORMATION REPORTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance wits• assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowir (Signature of Pbrmittee) Permit Datp, 11/1/2012-10/31/2017 (Date) Permit text. SECTION B. ]NO❑ 3 system designed to nanage the system, or accurate, and complete. I violations." CERTIFICATE OF CO,VERAGE FACILITY NAM 1 COUNTY CO- i Semi-annual Stormwater Discharge Monitoring Report For North Carolina Division of Water Quality General Permit No. NCG030000 Date submitted iZZ t3 NCG03 4 O SL d PERSON COLLECTING SAPAPLESI M 14- LABORATORY IAArIii _ Lab Cert. # Comments on sample collection or analysis: No -i- Part A; Stormwater Benchmarks and Monitoring Results 11 1 ,. SAMPLE COLLECTION YEAR 2-4t5 / SAMPLE PERIOD ❑ J n-June ❑ ly-Dec or K Monthly'_o� fnC, (month) DISCHARGING TO MSS ❑ORW ❑Hqw� ❑Trout ❑PNA ❑Zero -flow ater Supply❑SA [-]Other PLEASE REMEMBER TO SIGN ON PAGES 2 AND/OR 3 4 VNo discharge this period?2 outfall No. Date Sample Collected =u (mo/dd/yr 244hour rainfall amount, Inches Total Suspended Solids pH, :Standard units Copper :Lead : Zinc :.Non -Polar O&G/ Total Petroleum -Total Hydrocarbons Toxic Organicss Benchmarks 100 mg/L or 50 mg/L 6.0 -- 9.0 0.007 mg/L.' ::0.03 mg/L. 0.067 mg/L 15 mg/L . 1 rng/L .: it it Ij i Monthly sampling (instead of semi-annual) must begin with the second consecutive benchmark exceedance for the same parameter at the same outfall. z For sampling periods with no discharge at any single outfall, you must still submit this discharge monitoring report with a checkmark here. 3The total precipitation mustbe recorded using data from an on -site rain gauge. Unattended sites may be eligible for a waiver of the rain gauge requirement. d See General Permit, Table 3`dentifyingthe especially sensitive receiving water classifications where the more protective benchmark applies. s Total Toxic Organics sampling is applicable onlyfor those facilities which perform metal finishing operations, manufacture semiconductors, manufacture electronic crystals, or manufacture cathode ray tubes. For purposes of this permit the definition of Total Toxic Organics is that definition contained in the EPA Effluent Guidelines for the facility subject to the requirement to sample (for metal finishing use the definition as found in 40 CFR 433.11; for semiconductor manufacture use the definition as found in 40 CFR 469.12; for electronic crystal manufacture use the definition as found in 40 CFR 469.22; and for cathode ray tube manufacture use the definition found in 40 CFR 469.31). Permit Date: 11/1/2012-10/3 SWU-245, last revised 10/25/2012 Page 1 of 3 Note: if you report a sample value in excess of the benchmark, you must implement Tier 1, Tier 2, or Tier 3 responses. See General Permit text. ii I FOR PART AAND PART MONITORING RESULTS: • A BENCHMARK EXCEEDANCE TRIGGERS TIER I REQUIREMENTS. SEE PERMIT PART If SECTION B. • 2 EXCEEDANCES IN A ROW kFOR THE SAME PARAMETER ATTHE SAME OUTFALLTRIGGER TIER 2 REQUIREMENTS. SEE PERMIT PART II SECTION B. TIER 3: HAS YOUR FACT ITIY HAD 4 OR MORE BENCHMARK EXCEEDENCES FOR THE SAME PARAMETER ATANY ONE OUTFALL? YES ❑ NO [] IF YES, HAVE YOU CONTACTED THE DWQ REGIONAL OFFICE? YES ❑ NO ❑ REGIONAL OFFICE CONTACT NAME:I Mail an original and one coptdthis DMR includin all "No Disc in the case o "No Dischar e" iel arts to. Attn: DWQ Central Files i 1617 Mail Service Center Raleigh, North Carolina 27699-1627 "I certify, under penalty of law, tl assure that qualified personnel p those persons directly responsibl am aware thapt there are significa (Signature of Permittee) this document and all attachments were prepared under my direction or supervision in accordance with a system designed to J,erly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or or gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1 2[C (Date) Permit Date: 11/1/2012-10/31/20171 SWU-245, last revised 10/25/2012 Page 3 of 3