NCS000389_MONITORING INFO_20050729

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
f V CJS GOD "��
DOC TYPE
❑ FINAL PERMIT
'� MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ 'Z acf::> 07
YYYYM M D D

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DAK Americas
FIBERS. MONOMERS & RESINS
To: NCDENER, DWQ
From: DAK Americas, LLC (Anthony Hudson)
# Subject: NPDES NC5000389, Analytical Monitoring
Date: 10-31-05
Follow up to our July 29, 2005 report submitted a sample from our Stormwater
Outfall # 003 was taken on October 6, 2005 during a rain event. The sample
analysis was 13.3 MGIL of COD and <.005 MGIL of 1,4, Dioxane which support
our historical numbers. The analysis report is included with this letter and if
additional information or actions are required please contact me at 910-433-
8338.
Sincerely,
Anthony Hu son
Safety, Health and Environmental Manager
DAK Americas LLC
3216 Cedar Creek Road • PO Box 1690 (28302) • Fayetteville. NC 28312
910-433-8300 • fax:[phone]

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Date l 10l612005 Attn: Central Files
Total Event Precipitation (inches; 2_7 1617 Mail Service Center
Event duration (hours): 36 Raleigh, North Carolina 27699-1617
" I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
Including the possibility of fines and imprisonment for knowing violations.
(Signature of Permittee)
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(Date)

2401 W. 5" St. PO Box 589
Lumberton, NC 28358 Lumberton, NC 28359
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Phone: [phone] FAX: [phone]
Environmental Laboratory Email: tbllab65Mcrrbiz.com
FINAL REPORT OF ANALYSES
DAY, AMERICAS PROJECT NAME: TBL-16132
CEDAR CREEK PLANT REPORT DATE: 10/26/05
3216 CEDAR CREEK RD.
FAYETTEVILLE, NC 28301-
Attn: MR. DONALD ALLBRIGHT
SAMPLE NUMBER- 31898 SAMPLE ID- OUTFALL 003 SAMPLE MATRIX- OT
DATE SAMPLED- 10/06/05 TIME SAMPLED- 1515
DATE RECEIVED- 10/07/05 SAMPLER- D. ALLBRIGHT RECEIVED BY- KNH
TIME RECEIVED- 1025 DELIVERED BY- JOHNNY HESTER
Page 1 of 1
ANALYSIS QUAL DET.
ANALYSIS METHOD DATE BY RESULT UNITS CODE LIMIT
CHEMICAL OXYGEN DEMAND 8000 10/07/05 PSH 13.3 MG/L 10.0
LABORATORY DIRECTOR L
NCDENR DWQ # 37, NCDENR DW #37781
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PARADIGM ANALYTICAL LABORATORIES, INC.
5500 Business Drive
Wilmington, North Carolina 28405
[phone]
Fax [phone]
Ms. Pam Hester
TBL Laboratory
2401 West 5th Street
Lumberton NC 28359
Report Number: G477-41
Client Project: DAK Americas
Dear Ms. Hester:
Enclosed are the results of the analytical services performed under the referenced
project. The samples are certified to meet the requirements of the National
Environmental Laboratory Accreditation Conference Standards. Copies of this report
and supporting data will be retained in our files for a period of five years in the event
they are required for future reference. Any samples submitted to our laboratory will
will be retained for a maximum of thirty (30) days from the date of this report unless
other arrangements are requested.
If there are any questions about the report or the services performed during this project,
please call Paradigm at [phone]. We will be happy to answer any questions or
concerns which you may have.
Thank you for using Paradigm Analytical Labs for your analytical services. We look
forward to working with you again on any additional analytical needs which you may have.
Sincerely
7. Patrick Weaver
Laboratories, Inc.
ate
1 of 4
N.C. Certification #481 S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Client Sample ID: Outfall 003
Client Project ID: DAK Americas
Lab Sample ID: G47741-1 C
Lab Project ID: G47741
Compound
1,4-Dioxane
2-Fluorobiphenyl
Nitrobenzene-d5
4-Terphenyl-d 14
Comments:
Flags:
BOIL = Below Quantitation Limits.
Results for Semlvolatiles
by GCMS 8270
Result Quantitation
ug/L Limit ug/L
BQL 5.00
Spike
Added
10
10
10
— _ L Page 1 of 1
Analyzed By: MRC
Date Collected: 10/6/2005 15:15
Date Received: 10/11/2005
Date Extracted: 10/11/2005
Matrix: Water
Dilution Date
Factor Analyzed
1 —10/1 8/2005
Spike
Percent
Result
Recovered
8.9
89
8.9
89
9.7
97
Reviewed By:
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2 of 4
N.C. Certification #481 S.C. Certification #99029

• 4 PARADIGM ANALYTICAL LABORATORIES, INC.
List of Reporting Abbreviations
and Data Qualifiers
B = Compound also detected in batch blank
BQL = Below Quantitation Limit
DF = Dilution Factor
Dup = Duplicate
D = Detected, but RPD is > 40% between results in dual column method.
E = Estimated concentration, exceeds calibration range.
J = Estimated concentration, below calibration range and above MDL
LCS(D) = Laboratory Control Spike (Duplicate)
MDL = Method Detection Limit
MS(D) = Matrix Spike (Duplicate)
PQL = Practical Quantitation Limit
RL = Reporting Limit
RPD = Relative Percent Difference
mg/kg = milligram per kilogram, ppm, parts per million
ug/kg = micrograms per kilogram, ppb, parts per billion
mg/L = milligram per liter, ppm, parts per million
ug/L = micrograms per liter, ppb, parts per billion
% Rec = Percent Recovery
% soilds = Percent Solids
Special Notes:
1) Metals and mercury samples are digested with a hot block, see the standard
operating procedure document for details.
2) Uncertainty for all reported data is less than or equal to 30 percent.
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M134.092205.2
3 of 4
N.C. Certification #481 S.C. Certification #99029

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STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS000389--or SAMPLES COLLECTED DURING CALENDAR YEAR: 2005
Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from
the date the facitity receives the sampling results from the laboratory.)
FACILITY NAME DAK RESINS LLC COUNTY CUMBERLAND
PERSON COLLECTING SAMPLE(S) DONALD ALLBRIGHT PHONE NO. 910 4 3-822
CERTIFIED LABORATORY(S) TBL Lab# 37
Environmental Science_Corp Lab# ENV 375 (SIGNATU F PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Specific Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00340
82388
Total
Flow
COD
1,4,DIOXANE
molddlyr
MG
MGIL
MGIL
003
7/29/2005
2.97
2040
BDL*
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes X no
* SEE ATTACHMENT*

STORM EVENT CHARACTERISTICS:
Date I 7/29/2005
Total Event Precipitation (inches): 4.2
Event duration (hours): 4
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
" I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my Inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
Including the possibility of fines and imprisonment for knowing violations.
Si nature I Permittee Date