NCS000330_MONITORING INFO_20150202

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
%`}GS o co �2
DOC TYPE
El FINAL PERMIT
—- --- ---- -- -
MONITORING- REPORTS- -
APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ `1015. 01.02
YYYYMMDD

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
k
Permit Number NCS D a D 33 6,
FACILITY NAME 14 7 4 V"I L'
PERSON COLLECTING SAMPLEAS) 5j
CERTIFIED LABORATORY(S) Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 1Q
(This monitoring report shall be received by the Division no later than 30 dam
the date the facility receives the sampling results from the laboratory.)
COUNTY _ �(
r PHONE NO. C7L)j_
SIGNATURE OF PERMITTEE OR DESIGNEE CQ
REQUIRED ON PAGE 2.
1
1
DateII
Sample
Collected
I
ITotal
Flowapp.)
Rainfall
--�
. , _
i
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes Zno
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH'
New Motor
Oil Usage
mo/dd/ r
MG
inches
m
m
unit
al/mo
Form SVIU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
Division of Water Quality
Date ,� Attn: Central Files
Total Event Precipitation (inches): Q,. Q 1617 Mail Service Center
Event Duration (hours): (only if applicable —see permit.) Raleigh, North Carolina 27699-1617
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
includine possibility of fines and imprisonment for knowing violations."
of Permittee)
/-C�- ?-/s
(Date)
Form SWU-247, last revised 21212012
Page 2 of 2

January 27, 2015
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
REFCL I V
2015ED
QWRtz4
S L F►LES
rION
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Email: Joe.Hinkleodatimetals.com
Attached, please find stormwater monitoring data for Permit No NCS000330. The originals and
one copy are included. The monitoring data is for the following monitoring schedule -
Monitoring Period
Sample Number
I Start
IEnd
Year 6 — Period 1
11
I September 1, 2014
1 February 28, 2015
Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
J e Hinkle
EHS Manager

leAnalytical"
wwwpacalab&com
January 22, 2015
Mr. Joe Hinkle
Allvac
RE: Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
Pace Analytical Services, Inc.
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on December 22, 2014,
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample anaiyte
page for analysis unless otherwise footnoted.
Revised report issued on 1/22115 with COC attached.
Revised report issued on 1/22/15 with correct COC attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Laura J Cooper
[e-mail]
Project Manager
Enclosures
pcco,i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
98 without the written consent of Pace Analytical Services, Inc..
Page 1 of 14

aceAnalytical
wnwcPeceA8bs.00m
January 22, 2015
Page 2
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Anatytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 2807E
[phone]
Page 2 of 14

Pace Analytical Services, Inc.
aceAnalytical •
Kincey Ave. te
9B00Huntersvlle,
NC1280078
www.pocefeftcom
[phone]
CERTIFICATIONS
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
Charlotte Certification Ins
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
FloridalNELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #; 40
FloridalNELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 14

1
Pace Analytical Services, Inc.
Nt�t
aC,e
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wwwpeoobs cam
[phone]
SAMPLE ANALYTE COUNT
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
Analytss
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92230664001 MONROE STORMWATER
EPA 1664B
CLW
1 PASI-C
EPA200.7
SH1
5 PASI-A
SM 2540D
MDW
1 PASI-A
SM 5210B
MLS
1 PASI-A
SM 5220D
EWS
1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 14

accAnalytical
www.pacelabsoxn
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Hunlersville, NC 28078
[phone]
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
Sample: MONROE STORMWATER
Lab ID: 92230664001 Collected: 12/22/14 03:06
Received: 12122/14 12:30 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared
Analyzed
CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg1L
5.0
1
12/22/14 16:42
200.7 MET ICP
Analytical Method: EPA 2003 Preparation Method: EPA 200.7
Cadmium
NO ug1L
1.0
1
12/23/14 15:10
12/23/14 22:36
7440-43-9
Chromium
17.4 ugfL
5.0
1
12/23/14 15:10
12/23/14 22:36
7440-47-3
Lead
NO uglL
5.0
1
12/23/14 15:10
12/23/14 22i36
7439-92-1
Nickel
66.2 ug/L
5.0
1
12/23/14 15:10
12/23/14 22:36
7440-02-0
Zinc
176 ug1L
10.0
1
12/23/14 1510
12/23/14 22736
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
25.0 mg1L
6.2
1
12/26/14 17:11
5210E BOO, 5 day
Analytical Method: SM 5210B
BOD, 5 day
5.5 mg1L
2.0
1
12/23/14 15:45
12/28/14 16:10
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
162 mglL
25.0
1
12I30114 08:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/22/2015 04:51 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14

ace"Iytical.
www.pacelebs.com
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
QC Batch: GCSV119881 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92230664001
METHOD BLANK: 1356035
Associated Lab Samples: 92230664001
Parameter Units
Oil and Grease mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 12/2211416:40
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1358036
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 38.0
95
78-114
MATRIX SPIKE SAMPLE:
1358037
92230565001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg1L
ND 40
39.0
94 78-114
Results presented on this page are In the units Indicated by the "units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/22/2015 04:51 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 14

aceAnalytical
www.pacabbs.com
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
QC Batch: MPRP117612 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92230664001
METHOD BLANK: 1358768
Associated Lab Samples: 92230664001
Parameter Units
Cadmium
Chromium
Lead
Nickel
Zinc
ug1L
ug/L
ug/L
ug/L
ug/L
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
1.0
12/23/14 21:56
ND
5.0
12/23/14 21:56
ND
5.0
12/23/14 21:56
ND
5.0
12/23/14 21:56
ND
10.0
12/23/14 21756
Pace Anatytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1358769
Spike
LCS.
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
ug1L
500
462
92
85-115
Chromium
uglL
500
438
88
85-115
Lead
ug/L
500
447
89
85-115
Nickel
uglL
500
462
92
85-115
Zinc
ug1L
500
439
88
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1358770
1358771
MS
MSD
92230489001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ugA-
ND
500
500
475
460
95
92
70-130
3
Chromium
ug1L
575
500
500
1010
974
87
80
70-130
4
Lead
ug1L
ND
500
500
422
406
83
80
70-130
4
Nickel
uglL
193
500
500
636
615
89
84
70-130
3
Zinc
ug/L
392
500
500
816
804
85
82
70.130
2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1358772
1358773
MS
MSD
92230486001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
uglL
NO
500
500
465
458
93
92
70-130
2
Chromium
uglL
ND
500
500
437
434
87
87
70-130
1
Lead
uglL
ND
500
500
441
439
88
88
70-130
0
Nickel
ug)L
ND
500
500
462
457
92
91
70-130
1
Zinc
ug)L
4.8J
500
500
442
435
87
86
70-130
2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/22/2015 04:51 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 14

sp
acmnalytical
www.pacelabscorn
QUALITY CONTROL DATA
Pate Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
QC Batch: WETI34994
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92230664001
METHOD BLANK: 1360241
Matrix: Water
Associated Lab Samples: 92230664001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids mg/L
ND
2.5 12/26/14 17:08
LABORATORY CONTROL SAMPLE. 1360242
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids mg/L
250 230
92 90-110
SAMPLE DUPLICATE: 1360243
92230657001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids mg1L
11.1
13A 19 D6
SAMPLE DUPLICATE: 1360244
92230718001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids mg/L
ND
ND
Results presented on this page are In the units Indicated uy the "Unite" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/22/2015 04:51 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14

aceAnalytical`
www.pecelaimmm
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
QC Batch: WETI34942 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210B GOD, 5 day
Associated Lab Samples: 92230664001
METHOD BLANK: 1358934
Associated Lab Samples: 92230664001
Parameter Units
GOD, 5 day mglL
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 12/28/14 16:10
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1358935
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
GOD, 5 day
mglL
198 184 93
84.5-115.4
SAMPLE DUPLICATE: 1358936
92230700001 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg1L
3340 2970
12 D6,H3
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the resu@.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/22/2015 04:51 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 14

1aceAnalytrcal"
wwwpeoehftcom
QUALITY CONTROL DATA
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
QC Batch: WETA/21408 Analysis Method: SM 5220D
OC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92230664001
METHOD BLANK: 1359896
Associated Lab Samples: 92230664001
Parameter Units
Chemical Oxygen Demand mg1L
LABORATORY CONTROL SAMPLE: 1359897
Parameter Units
Chemical Oxygen Demand mg1L
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 12/30/14 08:30
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 776 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359898 1359899
MS MSD
92230124003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 223 750 750 932 929 95 94 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1359900 1359901
MS MSD
92229858002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mglL ND 750 750 768 756 102 101 90-110 2
Results presented on this page are In the units Indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/22/2015 04:51 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 14

leAnalytical"
www.pecedahaoom
QUALIFIERS
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
DEFINITIONS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Get - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RFD) between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shack not be reproduced, except in full,
Date: 01/22/2015 04:51 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14

aceAnalytical
®
wwwpacalab.cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MONROE STORMWATER SW02
Pace Project No.: 92230664
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Analytical
Batch
92230664001
MONROE STORMWATER
EPA 1664E
GCSV119881
922306 4001
MONROE STORMWATER
EPA 200.7
MPRPl17612 EPA 200.7
ICPI15865
92230664001
MONROE STORMWATER
SM 2540D
WET134994
92230664001
MONROE STORMWATER
SM 5210B
WETl34942 SM 5210B
WET134946
92230664001
MONROE STORMWATER
SM 5220D
WETAl21408
Date: 01/22/2015 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 14

��'"Anaolcal'
Client Name:
sample Condition Upon Recei t SCU
Document Number:
Fyy-CHR-CS
AA-003-rev.15
Mi1'tte(A Alit/ kc
Page 1 of 2
Issuing Authority:
Pace Huntersville Quality Office
Courier: ❑ Fed Ex ❑ UPS[] USPS❑ _ lien Commercial❑ Pace Other
Custody Seal on Cooler/Box Present: ❑ yes [9/no Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble V❑p ❑ Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1401 Type of Ice: Blue Norte
Temp Correction Factor T1401 No Correction L/
Im
L; s e
M
Samples on fce, cooling process has begun
Corrected Cooler Temp.: •C
Biological Tissue is Frozen: Yes no
�
Date and In iti I f paMon examining
contents: �
Temp should be above freezing to VC
Comments:
Chain of Custody Present:
Vr ONO
❑NIA
1.
Chain of Custody Filled Out:
Y s ❑No
❑NIA
2.
Chain of Custody Relinquished:
9yo ONO
❑NIA
3.
Sampler Name & S1 nature on COC:
t(yfl ONO
❑NIA
4.
Samples Arrived within Hold Time:
Y a ❑No
❑NIA
5.
Short Hold Time Anal sis <72hr :
c4ps ©No
❑NIA
6.
Rush Turn Around Time Re uested:
12(YSP ❑No
❑NIA
7.
Sufficient Volume:
ONO
❑NIA
8.
Correct Containers Used:
es ONO
❑NIA
9.
-Pace Containers Used:
34s ❑No
❑NIA
Containers Intact:
Yes ONO
❑NIA
10.
Filtered volume received for Dissolved tests
❑Yes ❑No
S6A
1 11.
Sample Labels match COC:
es ONO
❑NIA
12.
-Includes dateltime/ID/Anal sis Matrix:
All containers needing preservation have been checked.
MYas ❑No
❑NIA
13,
All containers needing preservation are found to be in
!(Yes ❑No
❑NIA
compliance with EPA recommendation,
s4s ❑No
exceptions: VOA, coliform, TOC, O&G, W -ORO (water)
Samples checked for dechlorination:
Yes ONO
❑NIA
14.
Headspace in VOA Vials >6mm :
❑Yes ONO
91A
15.
Trip Blank Present:
Dyes ONO
(NIA
16.
Trip Blank Custody Seals Present
Dyes ONO
15NIA
Pace Trip Blank Lot # if purchased):
Client Notification/ Resolution: Field Data Required? Y I N
Person Contacted: Daterrime:
Comments/ Resolution:
SCURF Review: Date: 1 /
SRF Review: bw Date: 12 d3
Note: Whenever th s a discrepancy affecting North Carolina complian
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( I.e out of hold, incorrect preservative, out of temp,
Incorrect containers)
WO#:92230664
1111111111111111111111
92230654
Page 13 of 14

���//�,1 CHAIN -OF -CUSTODY 1 Analytical Request Document
.� - aceAnalytieal • /`� The Chain
is a LEGAL DOCUMENT- All relevant fields must be completed acatrately.
ame.pacetaba.cam , } (/�
a
- -
Section A Section B Section C
Page: or
Required Client Information: Required Project Information: Invoice Information
Ryi Repon To- Attention
1886855
Z c'
A say,
Copy To: r
dG l
paay e:
�
REGULATORY AGENCY
rD
lEmair-ro:
F NPDES r GROUNDWATER F DRINKING WATER
r usT r RCRA r OTHER
Purchase
Order No.:
ace Quota
n
Fax: Project
Name:
Pace Pro)aa
Site Location
" .S/%
O �4/r!L(lQ Cr
Manage:
STATE:
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I-- BY synvlg Ws lam you are ecce0bng Paces NET 30 day payment terms end agreeing to la[e charges or 1.5% per month for any invogs not OW,&th- 30 days. ' / F-ALL-0-020rev.07,.15-May-2007

II .
Allvac - Monroe Plant i;tATI Allvac
Stormwater Monitoring` Report Form
Sample Date: ��"�� "�7 Sample Time:52)6,41n
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Stormwater_Discharge Outfall #2
Drainage Area = 272 590sq. ft. = 6.25 acres
% Impervious = 36%
/v X o o el I r
&Z Ie'1
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
NO
0.001
Chromium, total recoverable
D1 7 1/1
Lead, total recoverable
0.03
Nickel, total recoverable
0.26
Zinc, total recoverable
0.067
Oil and Grease
30
pH
(std units)
6-9 (std units)
Storm Dater Storm Duration: 5 (Hrs.) inches of Rainfall:
Duration of time preceding rain event exceeding 0.1": / / 7 - - (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(lmpervious Area)
Q(tot., cfs) = (A x inches rain// 2 inches/ft. x 6.25 acres x .64) + 9 x inches rain/] 2inches/ft. x 6.25 x .36)
Q(Total, cfs) = .1333 x (Inches of rain) +- .1688 x , 3 (Inches of rain)

rt
46
NCDENR
Stormwater Discharge Outfall (SD4)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http://portal.ncdenr.oriz/web/wQ/ws/su/npdessw#tab:4
Permit No.: N/C/,S/6/C 1L)1j1j/L)/ or Certificate of Coverage No.: N/C/C/—/_/_/—/—/`/
Facility Name:
County: a4 /D i-I Phone No. s ll
Inspector: I/ ZO/ly
Date of Inspection: -Al /-Z/
Time of Inspection: [),' S1q/YZ
Total Event Precipitation (inches):
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
0 Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signoure, I certify th4j this report is accurate and complete to the best of my knowledge:
(Signature of Perrqqee or D
SWU-242, Last modified 10/25/2012
Page 1 of 2

A.
1. Outfall Description:
Outfall No. GjCi
Receiving Stream:
(pipe, ditch, etc.)
Describe the)ndu5trial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 4 L /] '—'
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 0 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
7.
8.
9
1 2 0
Is there any foam in the stormwater discharge?
4 5
Yes No
Is there an oil sheen in the stormwater discharge? Yes No
Is there evidence of erosion or deposition at the outfall? Yes DNo
10. Other Obvious indicators of Stormwater Pollution:
List and describe 1,2617
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
SWU-242, Last modified 10/25/2012
Page 2 of 2

f..
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: http;llportal.ncdenr.org/web/wq/ws/su/npdessw#tab:4
Permit No.: N/C/S/&P/*241 or Certificate of Coverage No.:Facility Name:�-
County: Phone No.
Inspector:
Date of Inspection: /oZ- -ZY
Time of Inspection: %L; Q 41--n
Total Event Precipitation (inches): 0. as
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
OYes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of PermiWe or Design
SWU-242, Last modified 10/25/2012
Page 1 of 2

1. Outfall Description: ,
Outfall No. / tru26n
e (pipe, ditch, etc.)
Receiving Stream: ,�t',Xa C rGe-l�
Describ the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: ,-L
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): z!(2z2C
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 6) 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 0 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe d a 4 e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: htt/portal.ncdenr.org/wP /wq/ws/su/ni2dessw#tab-4
Permit No.: N/L/S5/ )1-01)1j1j/v/ or Certificate of Coverage No.:
l
Facility Name: _
County: Phone No.
Inspector:
Date of Inspection: zy
Time of Inspection: /4 .."SO AM_
Total Event Precipitation (inches):
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signatye, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee)pr Designee)
Pagel of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No.1N5.WQ3 Structure (pipe,
Receiving Stream: 6
Descri a the ind}�strial activities that occur
wlt �n the outfall drainage area:
v/z e'- . s-/v /A e f_ e,' 5 'a /e c .;l
2. Color: Describe the color of the disch i
(light, medium, dark) as descriptors: G
basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 40/Ie
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 V 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, last modified 10/25/2012

ALF
;A
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisform, please visit: hUp: /portaLncdennorg/web/wq /ws%su/nj2dessw#
Permit No.: �/ or Certificate of Coverage No.:
Facility Name: / c.
County: __ 6/1 , D2_ Phone No O
Inspector: _';/ rr .o t/ l an G
Date of inspection: / ? -/62 Z� _
Time of Inspection: 1Y,`QS I?IX _
Total Event Precipitation (inches):&-45
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
xYes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permitto or Design
Pagel of 2
5WU-242, Last modified 10/25/2012

1. Outfall Descriptio
Outfall No. i�Ls 'j Structure pipe, ditch, etc.) . G k
Receiving Stream:
Describe the industrial activities that occur w thin the outfall drainage area: at
2. Color: Describe the color of the
(light, medium, dark) as descriptors:
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /?0Z2�0—
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy-
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 (9 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 6) 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
B. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe /16L-9 e-
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

A�
;h,J��
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. http://portal.ricdenr.org/web/wq/ws/su/npdessw#tab--A
Permit No.: h /-C113160Q/,3/1—I/Q/ or Certificate of Coverage No.:
Facility Name: /
County: __ _661,
Inspector:�71
Date of Inspection:
Time of Inspection: 14"WO 4-M
Phone No.
Total Event Precipitation (inches):
S
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
AYes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureablestorm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event' is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature certify that this r
(Signature of Permittee or esignee)
is accurate and complete to the best of my knowledge:
SWU-242, last modified 10/25/2012
Page 1 of 2

1. Outfall Description:
Outfall No. Stru
Receiving Stream: A�-X
Describe the industrial activities
(pipe, ditch, etc.) - /, T,,- z
within the
2. Color: Describe the color of the discharge
(light, medium, dark) as descriptors:
. Lgkl-
drainage area:
basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): —17,04el-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 6) 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
O1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe �^zQ ,--
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
le-
Page 2 of 2
SWU-242, Last modified 14/25/2012

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. hUp: j/aortal.ncdenrargI web Jwq /ws%su/npdessw##tab-4
Permit No.: N/L/S/6/0/DIjAIL? or Certificate of Coverage No.:
Facility Name: 19 % 1
County: ZZA i 0d Phone No.
Inspector: %nZ24
Date of Inspection:
Time of Inspection: ZZ10,
Total Event Precipitation (inches):
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that�this report is accurate and complete to the best of my knowledge:
(Signature of PermitttAe or D
or ~ Pagel of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No.
Receiving Stream:/
Describe the industrial activi
re (pipe, ditchetc.)
that occur within the outfall drainage area:
ez G L 1i� Z-AIIr711 I /7.TI
2. Color: Describe the color of the disc
(light, medium, dark) as descriptors: h
'Sk
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /IQ/1G
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 a 3 4 5
7. Is there any foam in the stormwater discharge? Yes e°
8. Is there an oil sheen in the stormwater discharge? Yes 49
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe z�oAc�
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
"• Page 2 of 2
SWU-242, Last modified 10/25/2012