NCS000330_MONITORING INFO_20110318

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
IVC—c7
DOC TYPE
❑ FINAL PERMIT
-- MONITORING- REPORTS--- �- -- -- - -
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ 2okk • o�,•
YYYY M M D D

r
10�AITI Allvac
2020 Ashcraft Avenue, P.O. Box 5030, Monroe, NC 28110
phone:[phone] fax: [phone]
email: [e-mail]
March 11, 2011
NCDENR - Division of Water Quality
610 East Center Avenue, Suite 301
Mooresville, NC 28115
RECEIVED
DIVISION OF WATER QUALITY
MAR 18 2011
GWP 'S1.iCi 1QN
MOORESVILLE REGIONAL OFFICE
STORMWATER PERMIT NO. NCS000330 — ZINC MONITORING:
Dear Samar Bou-Ghazale:
This letter is to notify the DWQ Regional Office that ATI Allvac — Monroe Site has collected the requested
analytical monitoring for zinc off of the galvanized steel structures positioned in the drainage area for our
representative outfall. This is the 2"d sampling event conducted as requested by DWQ. The analytical
report for the second sampling event is attached and the summary of values are as follows:
Samnle Location Analytical Value (1`t samole) Analvtical Value (2"d samnle)
Finishing Bldg downspout
0,294 m L
0.0583 m g/L
GFM Bldg downspout
0.187 m /L
0,450 m g/L
Press Bldg downspout
0.116 m f/L
0.383 m 7/L
Conditioning Bld downspout
0.098 m f/L
0.0769 m L
Stormwater #02(M) Outfall
0.392 mg/L
0.177 mg/L
Again, I would like to reiterate that we communicated to NCDENR our concerns with meeting the
benchmark values for zinc when our permit was in draft stage. There is no zinc in our products and zinc is
not used in any of our processes. We feel that our zinc benchmark value is in our permit only because it is
a regulated constituent in EPA's ELG for titanium producers. As stated before, technical data sheets for
our titanium alloys were sent to NCDENR and show that zinc is not in our products.
Also, we have implemented BMPs to control potential sources of zinc, such as oil and rubber from tire
wear. These include routine cleaning of our roads by an industrial service provider, and routine
maintenance of our mobile equipment to reduce hydraulic oil leaks.
Allvac requests to "monitor only" for zinc, so that we can evaluate the effectiveness of these BMPs . In
the meantime, we plan to duplicate the zinc monitoring stated above for a.) time as requested by DWQ.
�' cerely,
Preston M. Baucom,
EH S Manager
ATI Allvac - Monroe Site
cc: Ed Stegall, Allvac
Greg Laney, Allvac
Kyle Dunn, Allvac
Tommy Long, Allvac

acmnalytical'
wrmpeoffWA n
March 09, 2011
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: ZINC SAMPLES
Pace Project No.: 9288805
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on March 01, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
IqA�nY-tx)
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
without the written consent of Pace Analytical Services, Inc..
Pneh
(704 )875-9092
Page 1 of 12

(�5a'cmnalyfical `
wWntpeD9bbacvm
Project: ZINC SAMPLES
Pace Project No.: 9288805
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
[phone]
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106
Pennsylvania Certification #: 68-03578
Florida/NELAP Certification #: E87648
South Carolina Bioassay Certification #: 99030002
Massachusetts Certification #: M-NC030
South Carolina Certification M 99030001
New Jersey Certification #: NC011
Virginia Certification #: 00072
North Carolina Bioassay Certification #: 9
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�cnelac�=
Page 2 of 12

aceAnalytical
wwlrpWslW&C(m
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pate Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Sorvices, Inc.
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
ZINC SAMPLES
Pace Project No.:
9288805
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
9288805001
FINISHING GUTTER
EPA 200.7
JMW
1
PASI-A
9288805002
CONDITIONING GUTTER
EPA 200.7
JMW
1
PASi-A
9288805003
PRESS GUTTER
EPA 200.7
JMW
1
PASI-A
9288805004
GFM GUTTER
EPA 200.7
SHB
1
PASI-A
9288805005
SW02
EPA 200.7
SHB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 12

leAnalytical'
xv►w.pecelabacom
Project: ZINC SAMPLES
Pace Project No.: 9288805
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: FINISHING GUTTER Lab ID: 9288805001 Collected: 02/28/11 06:45 Received: 03/01/11 13:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 METICP Analytical Method: EPA200.7 Preparation Method: EPA200.7
Zinc 58.3 ug1L 10.0 1 03/04/11 17:00 03/07/11 22:50 7440-66-6
Date: 03/09/2011 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
o,o
Page 4 of 12

aceAnalytical"
www.pecelahimm
Project: ZINC SAMPLES
Pace Project No.: 9288805
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2728B
[phone]
Pace Analytical Services, Inc.
2225 Riverside Or,
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvitie, NC 2807E
[phone]
Sample: CONDITIONING GUTTER Lab ID: 9288805002 Collected: 02/28/11 18:50 Received: 03/01/11 13:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 76.9 ug1L 10.0 1 03/04/11 17:00 03/07/11 22:53 7440-66-6
Date: 03109/2011 04:51 PM REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
v�ne�ac�=
Page 5 of 12

acmnalytical
WWW..PWgW .ccnr
Project; ZINC SAMPLES
Pace Project No.: 92BB805
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: PRESS GUTTER Lab ID: 9288805003 Collected: 02/28/11 19:04 Received: 03/01/11 13:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 383 ug/L 10.0 1 03/04/11 17:00 03/07/11 22:57 7440-66-6
Date: 03/09/2011 04:51 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�cnelac;
Page 6 of 12

lacieAnalytical'
www.pecefehacam
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC SAMPLES
Pace Project No.: 9288805
Sample: GFM GUTTER Lab ID: 9288805004 Collected: 02128/11 19:12 Received: 03/01/11 13:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 450 ug/L 10.0 1 03107/11 10:50 03/09/11 00:28 7440-66-6
Date: 03/09/2011 04:51 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
cnela&
Page 7 of 12

aceAnalytical
w►vw.pacelehacom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC SAMPLES
Pace Project No.: 92BB805
Sample: SW02 Lab ID: 9288805005 Collected: 02/28111 19:18 Received: 03/01/11 13:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7
Zinc 177 ug/L 10.0 1 03/07/11 10:50 03/09/11 00:35 7440-66-6
Date: 03109/2011 04:51 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
cnela'&
Page 8 of 12

e Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceMalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
wwwpecaleDscom Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: ZINC SAMPLES
Pace Project No.: 9288805
QC Batch: MPRP17960
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 9288805001. 9288805002, 9288805003
METHOD BLANK: 573301
Matrix: Water
Associated Lab Samples: 9288805001, 9288805002, 9288805003
Blank Reporting
Parameter
Units
Result Limit Analyzed
Qualifiers
Zinc
ug/L
ND 10.0 03/07/1122:03
LABORATORY CONTROL SAMPLE:
573302
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Zinc
ug/L
500 461 92
85-115
MATRIX SPIKE SAMPLE:
573303
9288310001 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Zinc
ug/L
ND 600 472
94
70-130
MATRIX SPIKE SAMPLE:
573305
9288858001 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Zinc
ug/L
22.5 500 489
93
70-130
SAMPLE DUPLICATE: 573304
9288310002 Dup
Parameter
Units
Result Result RPD
Qualifiers
Zinc
ug1L
ND 3.4J
SAMPLE DUPLICATE: 573306
9288858002 Dup
Parameter
Units
Result Result RPD
Qualifiers
Zinc
ug/L
ND 9.2J
Date: 03/09/2011 04:51 PM
REPORT OF LABORATORY ANALYSIS
Page 9 of 12
This report shall not be reproduced, except in full,
without the written consent of Pare Analytical Services, Inc.
.inela6

leAnalytical `
wwn pecahbacarn
Project: ZINC SAMPLES
Pace Project No.: 9288805
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr,
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: MPRP/7973 Analysis Method: EPA 200,7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9288805004, 9288805005
METHOD BLANK: 574063
Associated Lab Samples:
Parameter
9288805004, 9288805005
Units
Zinc
ug/L
LABORATORY CONTROL SAMPLE: 574064
Parameter Units
Zino
ug/L
MATRIX SPIKE SAMPLE:
Parameter
574065
Units
Zinc
ug/L
MATRIX SPIKE SAMPLE:
Parameter
574067
Units
Zinc
ug/L
SAMPLE DUPLICATE: 574066
Parameter
Zinc
SAMPLE DUPLICATE: 574068
Parameter
Zinc
Date: 03/09/2011 04:51 PM
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 03/09/1100:22
Pace Analytical Services, Inc.
9800 KinceyAve. Suite too
Huntersville, NC 28078
(704 )875-9092
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 477 95 85-115
9288805004 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
450 500 932 96 70-130
9288990001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
13.8 500 493 96 70-130
9288805005 Dup
Units Result Result
ug/L 177 180
9288990002 Dup
Units Result Result
ug/L 10.1 8.91
RPD Qualifiers
2
RP[) Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�t1 e�dC'
Page 10 of 12

leAnalyiical'
www.yetcefehaeom
Project: ZINC SAMPLES
Pace Project No.: 9288805
I6I4.11,11killO K
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphonylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
Date: 03/09/2011 04;51 PM REPORT OF LABORATORY ANALYSIS Page 11 of 12
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
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`
Pace Analytical Services, Inc.
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acemalytiol
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
wwupmaalsbsoom
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: ZINC SAMPLES
Pace Project No.: 9288805
Analytical
Lab ID Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
9288805001 FINISHING GUTTER
EPA 200.7
MPRP17960 EPA 200.7
ICPI7352
9288805002 CONDITIONING GUTTER EPA 200.7
MPRP17960 EPA 200.7
ICPI7352
9288805003 PRESS GUTTER
EPA 200.7
MPRP17960 EPA 200.7
ICPI7352
9288805004 GFM GUTTER
EPA 200.7
MPRP17973 EPA 200.7
ICP17361
9288805005 SW02
EPA 200.7
MPRP17973 EPA 200.7
ICPl7361
Date: 03/09/2011 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc..
Mtn lac,,
Page 12 of 12

aceAnalytica!'
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be Completed accurately.
Page: of
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Report To: Attention: ,.�
1434199Company:
Address: 7 /
Copy To:
Company Name: /
REGIf ORY AGENCY
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NPDES I— GROUNDWATER I— DRINKING WATER
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mail To:
Purchase Order No.:
Pace quote
Reference:
Ph a
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Project Name:
Pg� PreiBc=
Site Location
ManaP
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Requested Due baterTAT;
Protect Number:
Pace Profile
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
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RequlrWCllenl Information MATRi� XU I ODE
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COLLECTED
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LINQUISSHED BY f AFFILIATION
DATE
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DATE
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SAMPLE CONDITIONS
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SAMPLER NAMEANUSIGNATURE
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SIGNATURE of SAMPLER: 'tt_ MMTtBDgned 5 I_//
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Important Natg: Ely signing this form you are a pfi g Pace's NET 30 day payment lemur and agreeing to late charges of 1.5% per month for any invoices nA pargprmin 30 days. F-ALI -0J 11201 v n7 1.S.Mav_7nn7

sample■ndition Receipt
'..PaceAnalytical Client Name, Ailu Project #_-�iA�BgC��j
Where Received: i Huntersville ❑ Asheville ❑ Eden
Courier: ❑ Fed Ex ❑ UPS ❑ USPS [IClient ❑ Commercial Pace Other 0" #ia altt�s
ProjDue D ''e:'
Custody Seal on Cooler/Box Present: [I yes no Seals intact: El Yes ❑ no a}`
Pr°J.ameI 1"Mou"l,
Packing Material: ❑ Bubble Wrap []Bubble Bags ,None ❑Other
Thermometer Used: IR Gun : T904 Type of Ice: & Blue None Wamples on ice, cooling process has begun
Temn Correction Factor: Add / Subtract 0 C
Corrected Cooler Temp.:2
._-. � C
temp should be above freezing to VC
Biological Tissue is Frozen: Yes No
Comments:
Hate and Ini ' s of pers n e amining
contents G 3 o Y
chain of Custody Present:
Yes
❑No
©NIA
1.
3hain of Custody Filled Out:
Yes ❑No
41N/A
2.
chain of Custody Relinquished:IlYes
❑No
❑NIA
3,
;ampler Name & Signature on COC:
Yes
❑No
ONIA
4.
)amples Arrived within Hold Time:
Yes
ONo
©NIA
5.
short Hold Time Analysis (<72hr):
❑Yes
4No
❑NIA
6.
tush Turn Around Time Requested:
❑Yes
ONo
❑NIA
7.
;ufficfent Volume:
Yes
ONo
❑NIA
8.
'orrect Containers Used:
-Pace Containers Used:
Yes
tlYes
ONo
ONo
❑NIA
❑N/A
9,
Ontainers Intact:
Yes
ONo
❑N/A
10.
ltered volume received for Dissolved tests
❑Yes
ONo
NIA
11.
Rmple Labels match COC:
-Includesdateltime/ID/Analysis Matrix:
/�iYes ❑No
/"'(�--
❑NIA
12.
containers needing preservation have been checked.
containers needing preservation are found to be in
mpliance with EPA recommendation.
.eptions: VOA, coliform, TOC, O&G, W I-DRO (water)
Yes ONo
❑No
I❑Yes ❑No
❑N1A
❑N!A
13.
Initial when completed
Imples checked for dechforination:
❑Yes
ONo
N/A
14.
:adspace in VOA Vials ( >6mm):
❑Yes
ONo
NIA
15,
p Blank Present:
p Blank Custody Seals Present
ce Trip Blank Lot #f (if purchased):
❑Yes
❑Yes
ONo
❑No
11N/A
ffJWA
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16,
ent Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Tfine:
:omments/ Resolution:
URF Review:l U, 2 mate: I f SRF Review:� -`�LIU IDate:
a: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
tification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.02 28Dec201 0