NCS000330_MONITORING INFO_20110207

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
DOC TYPE
❑ FINAL PERMIT
5zMONITORING-REPORTS----- --- --- —
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ o ?
YYYYM M DD

RECEIVED
DIVISION OF WATER QUALITY
OATI Allvac
2020 Ashcraft Avenue, P.O. Box 5030, Monroe, NC 28110
phone:[phone] fax: 704.282,0667
email- [e-mail]
February 3, 2011
NCDENR - Division of Water Quality
610 East Center Avenue, Suite 301
Mooresville, NC 28115
STORMWATER PERMIT NO. NCS000330 — ZINC MONITORING:
Dear Samar Bou-Ghazale:
FEB - 7 2011
SWP SECTION
MOORESVILLE REGIONAL OFFICE
This letter is to notify the DWQ Regional Office that ATI Allvac — Monroe Site has collected the requested
analytical monitoring for zinc off of the galvanized steel structures positioned in the drainage area for our
representative outfall. The analytical report is attached and the summary of values are as follows. -
Finishing Bldg. — 0.,294 mg/L
GFM Bldg. — 0.187 mg/L
Press Bldg. — 0.116 mg/L
Conditioning Bldg — 0.098 mg/L
Stormwater #02(M) Outfall — 0.392 mg/LOB
Again, I would like to ceiterate that we communicated to NCDENR our concerns with meeting the
benchmark values for (zin when our permit was in draft stage. There is no zinc in our products and zinc is
not used in any of our processes. Again, we feel that our zinc benchmark value is in our permit only
because it is a regulated constituent in EPA's ELG for titanium producers. As stated before, technical data
sheets for our most common titanium alloys processed at the Monroe facility were sent to NCDENR and
show that zinc is not in our products.
Allvac requests a re-evaluation of the zinc limit and propose that we be given a condition to "monitor only"
for zinc, so that we can evaluate the effectiveness of the BMPs for sweeping our impervious areas for this
outfall. In the meantime, we plan to duplicate the zinc monitoring stated above as requested by DWQ.
Sincerely,
14.
Preston M. BaLICom,
EHS Manager
AT] Allvac - Monroe Site
cc: Ed Stegall, Allvac
Greg Laney, Allvac
Kyle Dunn, Allvac
Tommy Long, Allvac

aceAnalytical
wwwpacelaftcom
February 02, 2011
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: ZINC SAMPLES
Pace Project Ni 9286543
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on January 26, 2011.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
qt�nMWa;lz°'
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qc c�o
Page 1 of 11

e
acmnalytical
www.pecelabs com
Project: ZINC SAMPLES
Pace Project No.: 9286543
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
LouisianalLELAP Certification #: 04034
New Jersey Certification #: NCO12
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
South Carolina Drinking Water Cert. #: 99006003
Virginia Certification #: 00213
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification #: 357
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
[phone]
Page 2 of 11

lac
eAnalytical�
www.pacebbs.cam
Project: ZINC SAMPLES
Pace Project No.: 9286543
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2226 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
9286543001
FINISHING
EPA 200.7
JMW
1
PASI-C
9286643002
GFM
EPA 2003
JMW
1
PASI-C
9286543003
PRESS
EPA 200.7
JMW
1
PASI-G
9286643004
CONDITIONING
EPA 200.7
JMW
1
PASI-C
9286543006
SW02M
EPA 200.7
JMW
1
PASI-C
REPORT OF LABORATORY ANALYSIS Page 3 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceArralytr'cal
www.pacefaDs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
Project: ZINC SAMPLES
Pace Project No.: 9286543
Sample: FINISHING Lab ID: 9286543001 Collected: 01/26/11 09:20 Received: 01/26111 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
20D.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2007
Zinc 294 ug1L 10.0 1 01/27/11 16:10 02/04/11 17:39 7440-66-6
Date: 02/02/2011 04:05 PM -
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�cT1�C5.
Page 4 of 11

aceAnalytical
wmpecefaAt.rxur+
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC SAMPLES
Pace Project No.: 9286543
Sample: GFM Lab ID: 9286543002 Collected: 01/26/11 09:20 Received: 01/26/11 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 187 ug1L 10.0 1 01/27/11 16:10 02/01/11 17:42 7440-66-ti
Date: 02/02/2011 04:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 11

aceAnalytical
www.pmdabs.cnm
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC SAMPLES
Pace Project No.: 9286543
Sample: PRESS Lab ID: 9286543003 Collected: 01/26/11 09:40 Received: 01/26/11 15:45 Matrix: Water
Parameters Results units Report Limit DF Prepared Analyzed CAS No. 4ual
200.7 MET ICP
Zinc
Date: 02/0212011 04:05 PM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
116 ug/L 10.0 1 01/27/11 16:10 02/01/11 17:45 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�inP�.Cr
Page 6 of 11

aceAnalytical'
w...p8cekb&=n
Pace Analytical Services, Inc.
205 East Meadow Road - Su'he A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Hurtersville, NC 28078
[phone]
Project: ZINC SAMPLES
Pace Project No.: 9286543
Sample: CONDITIONING Lab ID: 9286543004 Collected: 01/26/11 09:50 Received: 01/26/11 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2007
Zinc 98.2 ug/L 10.0 1 01/27/11 16:10 02/01/11 17:58 7440-66-6
Date: 02/02/2011 04:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc._
ll
Page 7 of 11

e
aceAnalytical
.Pacelahacom
Project: ZINC SAMPLES
Pace Project No.: 9286543
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW02M Lab ID: 9286543005 Collected: 01/26/11 10:00 Received: 01/26/11 15A5 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2007
Zinc 392 ug/L 10.0 1 01/27/11 16:10 02/01/11 18:01 7440-66-6
Date: 02/02/2011 04:05 PM REPORT OF LABORATORY ANALYSIS Page 8 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
n

Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
aceAnalytrca!
205 East Meadow Road - Suite
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
wwwpecawmcorn
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: ZINC SAMPLES
Pace Project No.: 9286643
QC Batch: MPRPl7798
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 9286543001, 9286543002,
9286543003, 9286543004, 9286543005
METHOD BLANK: 556393
Matrix: Water
Associated Lab Samples: 9286543001, 9286543002,
9286543003, 9286543004, 9286543005
Blank Reporting
Parameter
Units
Result Limit Analyzed
Qualifiers
Zinc
ug/L
NO 10.0 0210111113:40
LABORATORY CONTROL SAMPLE:
556394
Spike LCS LCS
% Rec
Parameter
Units
Conic. Result % Rec
Limits Qualifiers
Zinc
ug1L
500 480 96
85-115
MATRIX SPIKE SAMPLE:
556395
9286345004 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Zinc
ug1L
220 500 704
97
70-130
MATRIX SPIKE SAMPLE:
556397
9286299001 Spike MS
MS
% Rec
Parameter
Units
Result Conc. Result
% Rec
Limits Qualifiers
Zinc
ug/L
106 500 592
97
70-130
SAMPLE DUPLICATE; 556398
9286300001 Dup
Parameter
Units
Result Result RPD
Qualifiers
Zinc
ug1L
70.1 65.3
7
SAMPLE DUPLICATE: 556528
9286544001 Dup
Parameter
Units
Result Result RPD
Qualifiers
Zinc
ug1L
53.8 53.7
0
Date: 02/0212011 04:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
/%5 ��:
ec
Page 9 of 11

aceAnalj4 cal
www.pewlab&cam
Project: ZINC SAMPLES
Pace Project No.: 9286543
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc,
9800 KinceyAve. Suite 100
Huniersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL- Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
PASI-C Pace Analytical Services - Charlotte
Date: 02/02/2011 04:05 PM REPORT OF LABORATORY ANALYSIS Page 10 of 11
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
:il_IGIaS..S;

0
aceAnalytical
rnvwpacabbLcam
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
(704)B75-9092
Project:
ZINC SAMPLES
Pace Project No.:
9286543
Analytical
Lab ID
Sample ID
CIC Batch Method
OC Batch
Analytical Method
Batch
9286643001
FINISHING
EPA 2003
MPRPI7798
EPA 2003
ICP77195
9286WO02
GFM
EPA 200.7
MPRPI7798
EPA 200.7
ICP77195
9286543003
PRESS
EPA 200.7
MPRPI7798
EPA 200.7
ICP17195
9286543004
CONDITIONING
EPA200.7
MPRPI7798
EPA200.7
ICP17195
9286543005
SW02M
EPA 200.7
MPRP17798
EPA 2003
ICP(7195
Date: 02/02/2011 04:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
lceo.a
�`cnehac�
Page 11 of 11

LI_1
' . �aceAnalytical'
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CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page: of
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Company. �' Report To: Attention:
1433898
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Address:
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CopyTo:�'
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Company Name: .�
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REGULATORY AGENCY
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Address: ©
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r NPDES F GROUND WATER INKING WATER
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UST 'i RCRA OTHER
Email To:
Purchase Order No.:
Pace Quote
Releranoe:
Fax:
Project Name'.
Puce Project
Site Location
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Manager.
STATE:
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Requested Duo DatelrAT:
Project Number.
Pace Profile
Requested
Analysis
Filtered
(YIN)
Section O Matrix Codes
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Required0lert information MAV1V I COnF
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COLLECTED
Preservatives
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DrinkNg Water OW
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Water W7
Waste Water WW
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ADDITIONAL COMMENTS
RfflJNQUISHED BY f AFFI IATION
DATE
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'ACCEPTED BY f AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
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ORIGINAL SAMPLER NAME AND SIGNATURE
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PRINT Name of SAMPLER:
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DATE Signed yy
SIGNATURE of SAMPLER: 'G
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Ir t Note. B si nin this torm re acceptingPace's NET 30 day payment teens and a reei to data es of 1.5% or month for an invokes not paio\ithin 30 deyi. F-AI I-r)-n,)nrav n'r -s��•• �^^'
' porlan - Y B 9 )roe a Y paY 9 n9 ata'9 P Y

SiaM616'Cosiditiod Upon Receipt
FceAnaiyiicai Client Name: (( mac. Project # �
Where Received: F,. Huntersviile ❑ Asheville ❑ Eden
Courier: Fed Ex UPS USPS
❑ ❑ ❑ ❑Client ❑Commercial Pace Other
W'6j4DiT uDate ice` !il
Custody Seal on Cooler/Box Present: ❑ yes a no Seals intact: ❑ yes [I no
Packing Material: ❑ Bubble Wrap [Bubble Bags P9 None ❑Other
Thermometer Used; IR Gun: T904 Type of Ice: Gwe
Blue None Samples on ice, cooling process has begun
Tema Correction Factor: Add 1 Subtract 0 C
�t
Corrected Cooler Temp.:—\ C
_
Temp should be above freezing to 6'0
Biological Tissue is Frozen: Yes nro
Comments:
Date and IniC xamining
s p r on
contents: G
chain of Custody Present:
Yes
0No
❑NIA
1.
chain of Custody Filled Out:
Yes
❑No
❑NIA
2.
:hain of Custody Relinquished:
Yes
❑No
I]N1A
3,
;ampler Name & Signature on COC:
Yes
ONO
❑NIA
4.
Samples Arrived within Hold Time:
Yes
ONO
©N/A
5.
ihort Hold Time Analysis (<72hr):
Dyes
bo
❑NIA
6.
tush Turn Around Time Requested:
❑Yes
No
❑wA
7.
ufficient Volume:
Yes
❑No
CINIA
8,
:orrect Containers Used:
-face Containers Used:
l%lYes
rI Yes
ONO
ON.
❑NIA
❑NIA
g.
ontainers Intact:
Yes
ONO
❑N1A
110.
Itered volume received for Dissolved tests
Dyes
ONO
C N!A
11.
ample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
hs o
L'' l
El NIA
12.
containers needing preservation have been checked.
containers needing preservalion are found to be in
mpliance with EPA recommendation.
eplions: VOA, coiiform, TOC, O&G, WI-DRO (water)
Yes ©No
]Yes ❑No
❑Yes ❑No
❑N1A
❑N!A
13.
Initial when completed
Imples checked for dechlorinatiom
1:1Yes
❑No
N/A
14,
!adspace in VOA Vials ( >6mm):
Dyes
ONO
N/A
15.
p Blank Present:
p Blank Custody Seals Present
ce Trip Blank Lot #t (if purchased):
❑Yes
❑Yes
❑No
ONO
]NIA
]NIA
ff
16,
ent Notification/ Resolution: Field Data Required? Y 1 N
Person Contacted: DateMme:
ommentsl Resolution:
URF Review: Date: 3� If SRF Review: Date: � f
Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form Wil be sent to the North Carolina DEHNR
tification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.02 28Dec2010