NCS000330_MONITORING INFO_20101216

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
c-:, c>c>
DOC TYPE
❑ FINAL PERMIT
-I -MONITORING -REPORTS— -_- ----.------___-_- __
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ Zvt
YYYYMMDD

RECEIVED
DIVISION OF WATER QUALITY
j ATI Allvac
2020 Ashcraft Avenue, P.O. Box 5030, Monroe, NC 28110
phone:[phone] fax: 704,282.0667
email: [e-mail]
� Idr�-
December 14, 2010
NCDENR - Division of Water Quality
1610 East Center Avenue, Suite 301
Mooresville, NC 28115
DEC 16 2010
SWP SECTION
MOORESVILLE REGIONAL OFFICji
STORM WATER PERMIT NO. NCS000330 — ZINC TIER RESPONSE:
Dear Ron Krebs:
This letter is to notify the DWQ Regional Office that ATI Allvac — Monroe Site has collected
valid sampling results required for the permit monitoring periods, and the results for zinc have
exceeded the benchmark value established in Stormwater Permit No. NCS000330. The sampling
results collected under the newly modified permit are as follows:
Discharge
Characteristic
Benchmark
Value
Year 1 —
Period 1
Year 1.—
Period 2.
MonthlyMonitorin
August
Sept
October
November
2010
2010
2010
2010
Zinc
0.067
0.228
0.365
0.145
0.134
0.447
0.223
m /L
The facility has fulfilled obligations to meet the requirements set forth in the Tier One and Tier
Two system called out in the permit. Our responses and efforts have been documented and are
maintained in our Stormwater Pollution Prevention Plan, The Tier One and Tier Two
documentation is attached to this letter.
During Year 1 — Period 1 sampling period, the facility implemented a sweeping program, which
involves the sweeping of the impervious surfaces by a mobile industrial sweeper on a 2-week
basis to control tire wear materials (source of zinc), and other potential pollutants dust.
During Year i — Period 2 sampling period, the facility sampled Outfall #02 shortly after the
impervious area was swept. The sampling results for zinc indicated no improvement in
comparison to previous zinc sampling.
Since the facility did not meet the benchmark values required in the stormwater permit for period
1 and period 2 sampling timeframe, monthly monitoring was instituted at Outall #02 for zinc
only. By the end of August 2010, a physical improvement was made to Outfall #02
(representative outfall) where our samples are collected. The outfall area was regraded so that
the run-off exiting the outfall pipe is channeled through an 8 — 10 ft. wide ditch that is
approximately 75 — 100 ft. long. The ditch begins at the exit of the outfali pipe and runs towards
6I

Richardson Creek. The ditch has been lined with rip -rap to control the suspended solids that
leave our property.
It should also be noted that during the October, 2010 sampling event, total zinc and dissolved
zinc was sampled. The sampling values for total zinc equaled 0.447 mg/L and dissolved zinc
equaled 0.339 mg/L.
Our concern with meeting the benchmark values were expressed to NCDENR while the permit
was in "draft" state. The Monroe facility processes titanium -based alloys and nickel -based
alloys. We feel that zinc is in the permit only because it is a regulated constituent in EPA's
Effluent Limit Guidelines (ELG) for titanium processors. However, there is no zinc in our
products, nor is zinc used in any of our processes. Technical data sheets for our most common
titanium alloys processed at the facility have been sent to NCDENR for review. This
documentation provides proof that zinc is not an element found in our titanium products.
We've researched this issue and found that the most common sources of zinc in industrial
stormwater are from galvanized steel (roofing, siding, equipment, fencing, etc.), tire dust and oil.
We have implemented BMP's to reduce the stormwater contribution of zinc from tire dust and
oil, however we have not identified any reasonable control measures for galvanized steel. Since
the facility has acres of galvanized metal that make up our buildings, we are not confident that
these BMPs will reduce our zinc below the proposed permit limit.
Again, Allvac requests a re-evaluation of the zinc limit. If this can not be granted, then we will
accept a condition of "monitoring only" for zinc, so that we can evaluate the effectiveness of the
BMPs mentioned above.
The Monroe facility is open to suggestions and requests the NC Division of Water Quality to
provide any reasonable recommendations. Please feel free to contact me in the future. Thank
you.
Sincerely, [�
Preston M. Baucorn,
EHS Manager
ATI Allvac - Monroe Site
cc: Ed Stegall, Allvac
Greg Laney, Allvac
Kyle Dunn, Allvac
"Pommy Long, Allvac

Permit No. NCS000330
"Tier One Response
November 20, 2009
Tier One Response
A storm water sample was collected on October 12, 2009 at the ATI Allvac Monroe plant's
representative outfall # 02 (M). This sampling event is the first for the monitoring schedule for
Year I — Period 1 for Permit No. NCS000330 effective August 7"', 2009. Below are the results
of this sampling event compared to the benchmark values that were applied in the permit:
~:Cltaracteristtc
:UnitsBesichniark'
Vale .:::.:.
Sampling .,
;.' : :Value
BOD
ni L
30
19.1
COD
m
120
72
TSS
m L
100
45.4
Cadmium
m L
0.001
ND
Chromium
na L
1
0.0445
Lead
mg/L
0.03
ND
Nickel
m /L
0.26
0.200
Zinc
m /L
0.067
0.228
Oil & Grease
mg/L
30
ND
PH
I standard
6-7
6.4
The facility enviromnental department began a sweeping program in September, 2009 consisting
of sweeping the impervious areas for outfall #02 (M) on a 2-week basis. This change improved
the sampling results compared to historic.
However, the facility slid not meet the benchmark values established for Zinc. A facility
inspection was conducted on October 271", 2009 by Tommy Long and Preston Baucom. There
were some minor secondary containment issues that were identified to be addressed, however we
do not feel that this will bring our Zinc levels down to the benclunark values established by the
Permit.
The products that the Monroe facility manufactures do not include Zinc, and Zinc is not used in
our processes. It is believed that the Zinc levels are related to the acres of galvanized steel that
makes up our facility. This was a concern and documented in correspondences with NC DENR
on June 3=d, 2009 and August 4"', 2009 during our new permit draft. As of now, we have not
determined a control method to address this facility structure issue. We will continue to monitor
this at the facility.
Preston M. Baucom
12HS Manager C v
L� �

acMnalytical
www.pace)abs.com
October 20, 2009
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
RE: Project: STORMWATER
Pace Project No.: 9255128
Pace Analytical Services, Inc.
2225 R iversid e Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
0800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
qt�nt,waz�
Erin Waters
[e-mail]
Project Manager
Endosures
cc: Ms. Alison Gallagher, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 9

v
laneAnalytical
wwwpaodabs.wm
Project: STORMWATER
Pace Project No.: 9255128
Charlotte Certification lDs
West Virginia Certification #: 357
Virginia Certification #: 00213
Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627
Kentucky UST Certiflcation #: 84
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012
Pace Analytical Services, Inc,
2225 Riverside Dr.
Asheville, NC 2BB04
[phone]
CERTIFICATIONS
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification* 68-00784
South Carolina Certification #: 990060001
South Carolina Drinking Water Cert, #: 990060003
Tennessee Certification #: 04010
Asheville Certification Ids
West Virginia Certification #: 356
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
Pennsylvania Certification #: 68-03578
LouisianalLELAP Certification #: 03095
South Carolina Bioassay Certification #: 99030002
Massachusetts Certification #: M-NCO30
South Carolina Certification #: 99030001
New Jersey Certification #: NCO 11
Tennessee Certification #: 2980
North Carolina Bioassay Certification #: 9
Virginia Certification #: 00072
Connecticut Certification #: PH-0106
North Carolina Drinking Water Certification #: 37712
Ff N1 5nAl G (14!�
Z /At �, , Z R f nilvle-
v:%� GF-111
9-
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Ile
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
Page 2 of 9

aceAnalytical
www.pacelabsxom
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: STORMWATER
Pace Project No.: 9255128
Sample. SW02 Lab ID: 9266128001 Collected: 10/12/09 14:35 Received: 10/13/09 14:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. {dual
HEM, Oil and Grease
Oil and Grease
200.7 MET ICP
Cadmium
Chromium
Lead
Nickel
Zinc
2540D Total Suspended Solids
Total Suspended Solids
5210B BOD, 5 day
BOD, 5 day
5220D COD
Chemical Oxygen Demand
Date: 10/20/2009 11:02 AM
Analytical Method: EPA 1664A
ND mglL
5.0
1
10/15/09 10:08
Analytical Method: EPA 200.7 Preparation
Method:
EPA
200.7
ND ug1L
1.0
1
10/14/09 15:20
10/15/09 19:54
7440-43-9
44.5 ug/L
5.0
1
10/14/09 15:20
10/15/09 19:54
7440-47-3
ND uglL
5.0
1
10/14/09 15:20
10/15/09 19:54
7439-92-1
200 uglL
5.0
1
10/14/09 15:20
10/15/09 19:54
7440-02-0
228 ug1L
10.0
1
10/14/09 15:20
10/15/09 19:54
7440-66-6
Analytical Method: SM 2540D
45.4 mg1L
7.1
1
10/15/09 22:14
Analytical Method: SM 5210B
19.1 mg1L
2.0
1
10/14/09 08:35
10/19/09 11:00
Analytical Method: SM 5220D
72.0 mglL
25.0
1
10/17/09 09:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
cco.o�
Page 3 of 9

® Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pamlabs.c+om Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 9255128
QC Batch: MPRP15214
Analysis Method:
EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 9255128001
METHOD BLANK: 350496
Matrix: Water
Associated Lab Samples: 9255128001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Cadmium
ug/L
ND
1.0
10/15/0919:09
Chromium
ug/L
ND
5.0
10115/0919:09
Lead
ug/L
ND
5.0
10/15/0919:09
Nickel
ug/L
ND
5.0
10115/0919:09
Zinc
ug/L
ND
10.0
1011510919:09
LABORATORY CONTROL SAMPLE: 350497
Spike LCS
LCS %
Roc
Parameter
Units
Cone. Result
% Rec Limits
Qualifiers
Cadmium
ug/L
500 514
103
85-115
Chromium
uglL
500 519
104
85-115
Lead
uglL
500 512
102
85-115
Nickel
uglL
500 511
102
85-115
Zinc
ug/L
500 515
103
85-115
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 350498
350499
MS MSD
9255002004
Spike Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Cadmium
ug/L ND
500 500
490
503
98 101
70-130 3
Chromium
ug/L ND
500 500
497
508
99 102
70-130 2
Lead
ug/L ND
500 500
485
498
97 100
70-130 3
Nickel
ug/L ND
500 500
486
498
97 100
70-130 2
Zinc
ug/L 6.4J
500 500
507
519 100 103
70-130 2
SAMPLE DUPLICATE: 350500
9255002005 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Cadmium
ug/L
ND
ND
Chromium
ug1L
0.951
.86J
Lead
ug/L
ND
ND
Nickel
ug/L
2.0J
N❑
Zinc
ug/L
6.1J
5.7J
I Date: 10/20/2009 11:02 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fu),
without the written consent of Pace Analytical Services, Inc..
Page 4 of 9

_ aceAna p cal
xww.pacefaCs.00m
Project: STORMWATER
Pace Project No.: 9255128
Pace Analytical Services, Inc.
2225 Riverside ❑r.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WET/111114 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids
Associated Lab Samples: 9255128001
METHOD BLANK: 351826
Associated Lab Samples: 9265128001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 351827
Parameter Units
Total Suspended Solids mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 2.5 10/15109 22:09
Spike LCS. LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 236 94 80-120
SAMPLE DUPLICATE: 351828
9255049001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 41.5 39.0 6
Date: 10120/2009 11:02 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 9

acMnalytical
WZacefabs.com
{
Project: STORMWATER
Pace Project No.: 9255128
QC Batch: GCSV16467
QC Batch Method: EPA 1664A
Associated Lab Samples: 9255128001
METHOD BLANK: 351289
Associated Lab Samples: 9255128001
Parameter
Units
Oil and Grease
mg/L
LABORATORY CONTROL SAMPLE:
351290
Parameter
Units
Oil and Grease
mg/L
MATRIX SPIKE SAMPLE:
351291
Parameter
Units
Oil and Grease
mg/L
Pace Analytical Services, Inc,
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664A
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
N❑ 5.0 10115/0910:07
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
HunlersviQe, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 38.0 95 78-114
9255153001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 40 34.8 84 78-114
Date: 10/20/2009 11:02 AM REPORT OF LABORATORY ANALYSIS Page 6 of
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
o,r ,cede.
o`� *o

aceAnalylical
www.pacefabs.com
Project: STORMWATER
Pace Project No.: 9255128
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 KinceyAve. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: WET/10080 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 9255128001
METHOD BLANK: 350355
Associated Lab Samples: 9255128001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 350356
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 2.0 10/1910911:00
Spike LCS LCS %Rec
Conc. Result % Rec Limits Qualifiers
198 220 111 84-115
SAMPLE DUPLICATE: 350357
9255072001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L ND ND
Date: 1012012009 11 .02 AM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 9

aceAnalytrcal
www.pacelabs.com
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 KinceyAve. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 9255128
QC Batch: WETA/6059 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description. 5220D COD
Associated Lab Samples: 9255128001
METHOD BLANK: 352562
Associated Lab Samples: 9255128001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 352563
Parameter Units
Chemical Oxygen Demand mg1L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 10/17/09 09:15
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 738 98 90.110
MATRIX SPIKE SAMPLE:
352564
9254455001
Spike
MS
MS
% Rec
Parameter
Units
Result
Cone.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
325
750
1060
97
-131 .646-283.
MATRIX SPIKE SAMPLE:
352566
9254622001
Spike
MS
MS
% Rec
Parameter
Units
Result
Cone.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg/L
366
750
1090
97
-131.646-283.
SAMPLE DUPLICATE: 352565
9264455002
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Chemical Oxygen Demand
mg/L
98.0
91.0
7
SAMPLE DUPLICATE: 352567
Parameter Units
Chemical Oxygen Demand mg/L
i Date: 10/20/2009 11:02 AM
9254624001 Dup
Result Result RPD Qualifiers
ND 26.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, i nc..
Page 8 of 9

lacmnalyfical
www.pacelabs.com
QUALIFIERS
Project: STORMWATER
Pace Project No.: 9255128
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NG - Not Calculable,
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
Date: 10/20/200911:02 AM REPORT OF LABORATORY ANALYSIS Page 9 of 9
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
cco.e�

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'Face A INYtielf Cfient Nam4( Project # �` 1
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Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ Commercial Pace Other. O toriappi'i "-"'
,,.!!! �... -4.�.- r-'-'.ter?.,a;,•.:,,
Custody Seal on CoolorlSox Present: ❑ yes Ql,[ _no Seals intact: ❑ yes no
,�.� ..� ..�,�=z, ,Pie . •fit
Packing i41aterlal: ❑ Bubble Wrap Oubble Aags ❑ Nonee��❑Other
'rkarmmm�fpr lkprf T0130 Tvn2 of ice: f SNPfJ E31ue Honp Samnles on ice- cantina process has begun
Biological Tissue is Frozen: Yes o NI date and In' at e��
Cooler Temperature
aramining
contents:
Temp should be above freezing to WC
Comments:
Chain of Cuslody Present:
Yes ❑No
❑NIA
1.
Chain of Custody Filled Out:
Yes ONo
0NIA
2,
Chain of Custody Relinquished: Y
Yes ONO
ONIA
3.
Sampler Name & Signature on COC:
Yas ONO
❑NIA
q,
Samples Arrived within Hold Time:
Yes ONO
❑NIA
5.
Short Hold Time -Analysis (<72hr):� =
Yes
DNA
£• - _ ., �_
Rush Turn-Airriulsd-TTM' keyuested:
0WA
7.
Sufficient Volume:
Yas ONO
©NIA
$,
Correct Containers Used:
�iYes -©No
❑NIA
g•
-Pace Containers Used:
Yes ONO,
ONIA
Containers Intact: -
Yes ❑No
❑NIA
10. .
Filtered volume received for Dissolved tens
©Yes Ono
NIA
11.
Sample Labels match COC:
KJYes ❑No
DWA
12•
-Includes dateltime/lD/Analysis Matrix,
All containers needing presarvalion have been checked.
.
�7Yes ONo
lrfjYes
ONIA
13.
AN containers needing preservation are found to be.in
ONO
❑NIA
compliance with EPA recommendation.
�r
exceptions: VOA, conform, ?-oC, O&G, Wl-DRO {water)
❑Yas ONO
Initfal when completed
Samples checked for dechlorinatiom
Yes ❑No
❑NIA
14. lq' lGiwj t� echkri.�� l '� S` p�
Headspace in VOA Vials >6mm}:
❑Yes QNo
NIA
15.
Trip Blank Present:
Oyes ©No . NIA
16.
Trip Blank Custody Seals Present
E1Yes ❑No
NrA
!f
Pace Trip Blank Lot # (if purchased): NIA
Client Notification! Resolution: Field data Required? Y / N / NIA
Person Contacted: Daterrime:
Comments/ Resolution:
Project Manager Review: - - - Date; 0 , !
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
cerliHcaiion Office ( i.e cut of hold, incorrect preservative, out of temp, incorrect con(ainers)

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.
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CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chaln-or•Cu."Is a LEGAL DOCUMENT. A3 ro(evant teids must be completed accurately.
Soctlon A Section B sawon C
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Requlrud Client WntamiaWn: Roqulred Projort IMormalian: Imm1w Inkumct(cm
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nmpwWt Noks: By s vft ae swm ye'a dM d=P* O Paws NET 30 day p■rmo::etmrna aw w" to sale dMV"a1.5% pr. moan for Any Wd&7d V.34 30d4. V F-ALL-W20rev.07, tSMay-20m

Permit No. NCS000330
Tier Two Response
AUgLISt 9, 2010
Tiel• Two Response
A storm water sample was collected on June 30, 2010 at the ATI Allvac Monroe plant's
representative outfall # 02 (M). This sampling event is the first for the monitoring schedule for
Year 1 — Period 2 for Permit No. NCS000330. Below are the results of this sampling event
compared to the benclllrtark values that were applied in the permit:
Characteristic
Units
Renelmial•k
Value
Sampling
Value
BCD
m L
30
28.3
COD
In /L
120
152
TSS
mg/L
100
57.5
Cadmium
nlg/L
0.001
ND
Chromium
nlg/L
1
0.0541
Lead
mg/L
0.03
0.0065
Nickel
in /L
0.26
0.372
Zille
Ill
0,067
0.365
Oil & Grease
n] /L
30
ND
pH
standard
6-7
6.8
The facility environmental department began a sweeping program in September, 2009 consisting
of sweeping the impervious areas for outfall H02 (M) on a 2-week basis. Since implementation,
this change has yielded improvement compared to historic sampling data, however the
impervious areas for outfall 402 (M) were swept on June 29, 2010 (the day before this sampling
event) and benchmark values were not niet for COD, Nickel, and Zinc.
A facility inspection was conducted on July 21, 2010 by Preston Baucom. There 'were some
minor secondary containment issues that were identified, however we do not feel that this will
bring our COD, Nickel, or Zinc levels down to the benchmark VaIIICS established by the permit.
In addition, monthly monitoring will be instituted for outfall 902 (M) for Zinc only, as long as
there is flow.
The products that the Monroe facility manufactures do not include Zinc, and Zinc is not used in
our processes. It is believed that the Zinc levels are related to the acres of galvanized steet that
makes tip our facility. This was a concern and documented in correspondences with NC DENR
on June 3`d, 2009 and August 41", 2009 during our new permit dram. As of now, we have not
determined a control method to address this facility structure issue. We will continue to monitor
this at the facilittyy...
/''yam , " ` • �d�tu-sN-�t
Preston M. Baucom
ERS Manager

aceAnalytical
mvwpxefaucom
July 12, 2010
Mr. Preston Baucom
Allvac
2020 Asheraft Ave
Monroe, NO 28110
RE: Project: MONROE- STORMWATPR
Pace Project No.: 9272638
Pace Analyltcal Sorvlces, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Sorvlces, Inc.
9000 KlnceyAve. Sulle 100
HuntersviIle, NC 26078
[phone]
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on July 01, 2010. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace HuntersviIle laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Erin Waters
[e-mail]
Project Manager
Endosures
cc: Ms. Alison Gallagher, Allvac
Mr, Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, excopt in full,
wilhoul the vaillen consCrll or Pace Analytical SeNIces, Inc.,
o�
Page 1 of B

1aceArr Xical�
wNn PoWahscom
Project: MONROE- STORMWATER
Pace Project No.: 9272836
Charlotte Certification lDs
9800 Klnoey Ave. Ste 100, Huntersville, NC 28078
LoulslanalL£LAP Certification M 04034
New Jersey Certification M NC012
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification M 68.00784
Ashovillo Certification lDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification #: PH-0106
FloridalNELAP Certiricallon #: E87648
Massachusetts Certification #: M-NC030
Now Jersey Certificallon M NC011
North Carolina Bioassay Certification #: 9
Paco Analytical Services, Inc,
2225 Riverside Ur.
Asheville, NG 28804
[phone]
CERTIFICATIONS
South Carolina Certificatlon #: 09006001
South Carolina Drinking Water Cert. #: 09006003
Virginia Certification #: 00213
Connecticut Certification #: PH-0104
FloddalNELAP Certification #: E87627
Kentucky UST Certification M 84
Louisiana DHH Drinking Water # LA 10D031
North Carolina Drinking Water Certification #: 37712
North Carolina Wastevrater Certification #: 40
Pennsylvania Certification #: 68-03578
South Carolina Bioassay Certification It: 9903002
South Carolina Certification #: 9903001
Virginia Certification #: 00072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull,
tivdlrout the vaillen consent of Pare Analytical Services, Inc..
a
Paco Analytical Servlcos, Inc,
9800 KlnceyAve. Suite 100
Hunlersville, NC 28078
[phone]
Page 2 of 8

+ aceAnalytical
w%wpa00Mbawrn
Pace Analytical Services, Inc.
2225 Riverskfe Dr.
Asheville, NC 29804
(026)2S4-7178
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincoy Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: MONROE- STORMWATER
Pace Project No.: 0272638
Sample: MONROE SW 02 Lab ID: 9272636001 Collected: 06130/1016AI Received: 0710111013:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664A
Oil and Grease
ND mg1L 5.0 1 0710211009A0
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND ug1L 1.0 1 0710211012:00 07/06/10 20:12 7440-43-9
Chromium
64.1 ug1L 5.0 1 0710211012:00 07100110 20,12 7440.47-3
Lead
6-5 ugA- 5,0 1 07/02/1012:00 07/06/1020:12 7439-92-1
Nickel
372 ugfL 5.0 1 07/02110 12:00 07100/10 20:12 7440.02-0
Zinc
366 ugA- 10.0 1 0710211012:00 07106/10 20:12 7440-66,6
62110B BOD, 6 day
Analytical Method: SM 5210E
BOD, 6 day
28.3 mg1L 2.0 1 07102/10 11:20 07/07/10 09:20
62200 COD
Analytical Method: SM 522()D
Chemical Oxygen Demand
162 mg1L 25.0 1 0710611021:65
Date: 07/12/2010 11:13AM
REPORT OF LABORATORY ANALYSIS
This repDA shall not 6e reproduced, except In full.
withoul the written consent of Pace Analytical Servkos, Inc..
Page 3 of 8

aceAnalytical"
nwnpaou1aU=n
Project: MONROE-STORMWATER
Pace Project No.: 927263E
Pace Analyllcal Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services. Inc.
9800 ftcey Ave. Guile 100
Huntersville, NC 2807E
[phone]
QC Catch: GCSV17948 Analysis Method: EPA 1664A
QC Batch Method: EPA1664A Analysis Description: 1664 HGM, Oil and Grease
Associated Lab Samples: 927263B001
METHOD BLANK: 484434 Matrix: Water
Associated Lab Samples: 0272638001
Blank Reporling
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grouse mg1L ND 6.0 07102/10 09:39
LABORATORY CONTROL SAMPLE: 464435
Spike LCS LCS %Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Oil and Grease mg1L 40 37.8 94 78-114
MATRIX SPIKE SAMPLE: 464436
9272607001 Spike MS MS % Re(;
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L ND 41.7 38.3 01 78-114
Date: 0711212010 11:13AM REPORT OF LABORATORY ANALYSIS Page 4 of 8
This report shall not be reproduced, except In full,
withoul the vaillen consent of Pace Analytical Services, Inc..

IacAnapical"e
Pace Analytical Services, Inc. Pace Analytical Services, Inc,
I
2225 Rivers?de Dr. 9800 KlnceyAve. Suite 100
wwwpacafabcom
Asheville. NC 28804 Huntersvil%, NC 28078
(s28)254-7176 [phone]
QUALITY CONTROL DATA
Project: MONROE- STORMWATER
Pace Project No.: 9272638
QC Batch: MPRP16614
Analysis Method:
EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Assoclated Lab Samples: 9272638001
METHOD BLANK: 464451
Matrix: Water
Associated Lab Samples: 927263B001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cadmium
ug1L
ND
1.0 0710511019:56
Chromium
ug1L
ND
5.0 0710611019:56
Lead
ug1L
ND
5.0 0710611019:56
Nickel
uglL
NO
6.0 0710611019:56
zinc
ug/L
ND
10.0 0710611019:56
LABORATORY CONTROL SAMPLE:
464452
Spike LCS
LC6 % Rao
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Cadmium
ug/L
500 496
99 85-i15
Chromium
ug1L
500 490
100 85-115
Lead
ugR.
500 496
99 85-115
Nickel
ug1L
500 497
99 85-115
Zinc
ug(L
600 602
100 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
464453
464454
MS
MSD
9272636001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
%, Rec
Limits
RPD Qual
Cadmium
ug1L
NO
600
500
498
492
99
98
70-130
1
Chromium
ugR,
54.1
500
500
555
550
100
99
70-130
1
Lead
ug1L
6.5
500
500
500
492
99
97
70-130
2
Nickel
ug1L
372
500
500
871
861
100
98
70-130
1
Zinc
ugR.
365
500
500
878
854
103
98
70.130
3
SAMPLE DUPLICATE: 464455
Parameter
Cadmium
Chromium
Lead
Nickel
Zinc
Units
9272488001
Result
Dup
Result
ug1L
0.0039 m91L
5.6
ugR.
0.032 m91L
31.5
ugR.
0.38 mg1L
391
uglL
0.030 m91L
31.3
ug1L
0.59 mgfL
621
RPD OualiRers
34 R1
0
3
4
5
Date:07/1212010 11:13AM REPORT OF LABORATORY ANALYSIS Page 5 of a
This report shall net be reproduced, except in full,
whhout the written consent of Pace Analytical Services, Inc..
o to
cee,a

i IaceftlAcal
(�Hwff.P.cc'aDsoonr
Project: MONROE-STORMWATER
Pace Project No.: 927263a
QC Batch: WET112969
QC Batch Method: SM 5210B
Associated Lab Samples: 9272638001
METHOD BLANK: 464431
Associated Lab Samples: 9272638001
Parameter Units
BOD, 5 day n1gIL
LABORATORY CONTROL SAMPLE: 464432
Parameter Units
BOD, 5 day rnglL
Paca Analytical Services, Inc.
2225 Rlverslde Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Descdptlen: 5210E ROD, 5 day
Matrix: Water
Blank Repotting
Result Limit Analyzed Qualiflers
ND 2.0 07/07110 09:20
Paco Analytical Services, Inc,
9800 KlnceyAve, Suile 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
198 204 103 84.115
SAMPLE DUPLICATE; 464433
9272681001 Cup
Parameter Units Result Result RPD Qualifiers
E
BOD, 5 day mg1L 408 393 4
Cate: 071121201011:13AM REPORT OF LABORATORY ANALYSIS Page 6of8
This report shall not be reproduced, except In tub,
without the written consent of Pace Analytical Services, Inc..

Paco Analyllcai Servlees, Inc, Pace Analytical Services, Inc.
f aceAnalyticalB 2225 Riverside Dr. 9800 Wncey Ave. Suite 160
NrmmWaDsoom Asheville, NC 28804 Huntersvllle, NC 28078
[phone] [phone]
QUALITY CONTROL. DATA
Project: MONROE-STORMWATER
Pace Project No.: 0272638
QC Batch: WETA11677
Analysis Method: SM 5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D
COD
Associated Lab Samples: 9272638001
METHOD BLANK: 465518
Matrix: Water
Associated Lab Samples: 9272638001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Chemical Oxygen Demand
mg1L
ND 25.0
07106/10 21:58
LABORATORY CONTROL SAMPLE:
465519
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result %Rec
Limits Qualifiers
Chemical Oxygen Demand
mg1l.
750 767
101
90.110
MATRIX SPIKE SAMPLE:
465524
9272638001 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
I
Chemical Oxygen Demand
mg1L
152 760
966
109
76-125
MATRIX SPIKE SAMPLE:
465526
9272608001 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Chemical Oxygen Demand
mg1L
155 750
931
103
75.125
SAMPLE DUPLICATE: 465525
9272638001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Chemical Oxygen Demand
mg1L
152 152
0
SAMPLE DUPLICATE: 465527
9272608001 Dup
Parameter
Units
Result Result
RPD
Qualifiers
Chemical Oxygen Demand
mg1L
155 147
5
Date: 071121201011:13AM REPORT OF LABORATORY ANALYSIS Page 7 of 8
This report shell not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..

aceAnalyticalo
wwwpaon'ab&mm
QUALIFIERS
Project: MONROE- STORMWATER
Pace Projecl No.: 927263B
DEFINITIONS
PacoAnalylical Sorvlces, Inc.
2225 Riverside Dr,
Asheville, NO 28804
[phone]
Paco Analytical Sorvices, Inc.
9800KInc4yAve. Suite100
Nuntersvilie, NC 28078
DF - Dllutton Factor, if reported, represents the factor applled to the reported data due 10 changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting Iimit.
MOL -Adjusted Method Detection Limit.
S - surrogate
1,2-Dtpheny1hydrazine (8270 Bled analyte) decomposes toAzobenzene.
Consistent with EPAguide1nes, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplica(e)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RFD - Relative Percent Difference
NC - Not Calculable.
U - indicates the compound was analyzed for, but not detected.
N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical Is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
ANALYTE QUALIFIERS
R1 RPD value was outside control limits.
[phone]
Dale: 07/12/2010 11:13AM REPORT OF LABORATORY ANALYSIS Page 8 of 8
This report shall not be reproduced, except In full,
whhoul the written consent of Pace Analytical Services, Inc..
���ae},-
GICfS.S:

Pace Analytical
9800 Kincey Suite 100
Huntersville
Entered 7/6/2010
Reported: 7112/2010
Sample Remark
Analytical Results
NC 28078
Sample W Parameter Cost ID
10076-8 TSS
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755.
EPA NCO0909
For 9272638
Result Units Method Date Analyzed Analyst
Monroe SW 02 57.5 mg1L SM2540D 716110 WL
P.U. Box 228 • Statesville, North Carolina 28681. 70418721,1697

;:� ..PaceArialytical'
CHAIN -OF -CUSTODY I Analytical Request Document
7ho Char-of-0ustody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section $ Section C
Roqulrvd Cllont IMormaUon: Required Project 1reormaUon: Involm Irecr=tten;
comaanr• Rapen To: AL drlCon:
1380867
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ADDITIONALCONMENTS
RELINQUISHED BYIAFF"ATION
DATE
TIME
ACCEPTED BYIAFFILIATION
DATE
TIME
SAMPLECONDIT)ONS
h cAcj t .m o po PA'I,
Ph 45cd J,
ORIGINAL SAMPLER NAMEAND SIGNATURE
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SIGNATURE of SAAIPLF3t:�I ^i? DATE Signed
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..mt NW. By slgalag a,iG tarn you ote occoping Paws NET 33 day DAytaerlt mnm and a9rcatng 10 Is:e Curgaa of 1 S,4 pot mono far any " -" 4 oot pOld wtdl 331104 F-ALL-"20mv.07, t S•May-2007

��-3c"`AnajWla'
Where Received:
Client Name:._ �`�1 Project #
0//Huntersville ❑ Asheville ❑ Eden
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑
Client ❑
Commercial ❑ Pace Other
Custody Seal on CooierlBox Present: ❑
yes ❑
np/"'seals intact: ❑ yes
Ai no
[?rdj Due;pate
Pro : Ndme:
Packing Material: ❑ BubbleWrap Q/Erubbls Bags
❑ None ❑ Other
Thermometer Used: IR Gun T904
Type of Ice: Wet Blue None
0-2- mples on Ice, cooling process has begun
Tpmn Cnrrpnfinn Factor: Add I Subtract
I 0 n
Me and itfa s of pe e a lning
Corrected Cooler Tamp.: 1 G
Biological
Tissue is Frozen: Y©s Na
contents .
Temp should be above freezing to 6T
Comments,
Chain of Custody Present:
es [IN.
❑NrA
1.
Chain of Custody Filled Out:
ea ON-
❑WA
2.
Chain of Custody Relinquished:
It's DNo
❑NIA
3.
Sampler Name & Signature on COC:
P4. DN.
DIVA
4.
Sam les Arrived within Hold Time: 1
❑No
❑NIA
5.
Short Hold Time Analysis <72hr :
ffY. ❑Noo
QNIA
B.
Rush Turn Around Time R uested:
❑Yes 134 OwA
7.
Sufficient Volume:
yams F No
OWA
B.
Correct Containers Used:
as ©No
[atuA
9.
-Pace Containers Used:
os ©No
❑NrA
Containers Intact:
RKas ©No
❑NIA
AO,
Filtered volume received for Dissolved tests
❑Yes ©No
❑NIA
11,
Sample Labels match COC:
dYes ©No
OwA
12.
-Includes dateltimeliD/Anal sis Matrix:,'
All contelners needing proservatlon have bean checked.
YYees ONo
❑NIA
13.
All containers needing preservatlon are found to be In
'pyB9 ❑Ne
i�NIA
compliance with EPA recommendation.
exec Iona: VOA, coliform, TOO, OSO, MORO (waler)
❑Yes ❑No
initial when wmpleted
Samples checked for dechlorination:
ErY. (IN.
DwA
14,
Heads ace in VOA Vials ( >8mm):
❑Ycs ❑No 6WA
15.
Trip Blank Present:
❑Yoe ❑NoKw"(
16.
Trip Blank Custody Seals Present
❑Yes ❑No
❑wA
Pace Trip Blank Lot # if urchasedj: '
Client Notification/ Resolution: Pleld Data Required? Y 1 N
Person Contacted:
Comments/ Resolution:
Datefrime:
Project Manager Review: . 1(2� pate 1110
Note: Whenever there Is a cl&fepancy affecting North Carona compliance samples, a copy of this form 4 l be sent to the North Carolina DEHNR Certiftcallon
Office (I.e out of hold, incorrect preservative, out of temp, incorrect conlalnera)
Pate SCUR revision 072308

laneAnalytical
www.pwefabs.com
f
August 27, 2010
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
RE: Project: Stormwater-Monroe
Pace Project No.: 9276032
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kircey Ave, Suite 100
Hunlersville, NC 2807E
[phone]
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on August 20, 2010. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
IqA�n M oa'&�
Erin Waters
[e-mail]-n
Project Manager
Enclosures
cc: Ms. Alison Gallagher, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSES
This report Shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
a,
Page 1 of 5

aceAnalytical
www.patela0s.nom
Project: Stormwater-Monroe
Pace Project No.: 9276032
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LGLA3Ila[H-A1111 U-1
Pace Analytical Services, Inc,
9800 Ktncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification i0s
2225 Riverside Dr., Asheville, NC 28804
North Carolina Drinking Water Certification #: 37712
Connecticut Certification #: PH-0106
North Carolina Wastewater Certification #: 40
F)orida/NELAP Certification #: E87648
Pennsylvania Certification #: 68-03578
Massachusetts Certification #: M-NCO30
South Carolina Bioassay Certification #: 99030002
New Jersey Certification #: NC011
South Carolina Certification* 99030001
North Carolina Bioassay Certification #: 9
Virginia Certification #: 00072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 5

aceAnalytical
www.pace)abs.com
Project: Stormwater-Monroe
Pace Project No.: 9276032
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Stormwater-Monroe Lab ID: 9276032001 Collected: 08/19110 08:30 Received: 08/20/10 16:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 145 ug/L 10.0 1 08/23/10 13:00 08/25/10 02:55 7440-66-6
Date: 08/27/2010 08:48 AM
REPORT OF LABORATORY ANALYSIS
This report shal} not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 5

aceAnalytical
www.pacetabs.corn
I
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Sidle 100
Asheville, NC 28804 Huntersville, NC 2BO78
[phone] " [phone]
QUALITY CONTROL DATA
Project: Stormwater-Monroe
Pace Project No.: 9276032
QC Batch: MPRP16916 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9276032001
METHOD BLANK: 487012
Associated Lab Samples: 9276032001
Parameter Units
Zinc ugl1.
LABORATORY CONTROL SAMPLE: 487013
Parameter Units
Zinc ug/L
Matrix: Water
Blank Repor-ting
Result Limit Analyzed Qualifiers
ND 10.0 08/25/10 01:19
Spike LCS LCS % Rec
Conic. Result % Rec Limits Quaiifters
500 479 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 487014 487015
MS MSD
9275683001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Zinc ug/L 87.8 500 500 578 572 98 97 70-130 1
SAMPLE DUPLICATE: 487016
Parameter
Zinc
Date: 08/27/2010 08:48 AM
t
9275682002 Dup
Units Result Result
ug1L ND .57J
RPD Qualifiers
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�o
co.o
Page 4 of 5

aceAnalytical
www.pacolabs.com
{
QUALIFIERS
Project: Stormwater-Monroe
Pace Project No.: 9276032
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable,
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
Date: 08/27/2011) 08:48AM REPORT OF LABORATORY ANALYSIS Page 5 of 5
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

:f aceAnalytical'
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. Alt relevant fields must be completed accurately.
-------------
Section A Section B Section C
Page: of
Required Client Inrormatiom Required Project Information: Invoice Inrormatow
Company: Report To: Attention: f_�
1380868
���
/ L m D�.a GfJ
Address: Copy
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To:
CS /L G ctsw
Company Name: r
1 ��✓AC
REGIt TORY AGENCY
v� L gq//U
Address: I O do jeS��D i�%GArEe-
NPDES F GROUNDWATER ►- DRINKING WATER
T- UST �` RCRA � OTHER
Email To: Purchase
Order No.:
Pace Quota
emaj
Rereretxa:
P on �S/�
Fax: Project
Name:
lot
Pace
SIte Location
Yn L-)e c% — Df %D �-
Manaper
STATE: N
Requested Due DaleffAT: Project
Number:
Pace Profde #:
Requested
Analysis
Filtered
{Y1N}
Secllon D Matrix Codes
z
Required Client Information MATRIX I CODE
o
COLLECTED
Preservatives
>
Dunking Water DW
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Q
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Water WT
Waste Water WW
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SAMPLE ID
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Sample IDS MUST BE UNIQUE Tissue TS
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U
Other OT
U
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ADDITIONAL COMMENTS
RELINQUISHED Y I AFFILIATION
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
4 G su
�
�-z� ro
SAMPLER NAME AND SIGNATURE
o
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ORIGINAL
0 v z
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PRINT Name of SAMPLER:
n
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SIGNATURE of SAMPLER: -- ''� II ((_/�/ DATE Signed Q-
/.�.s (MMIDDIYY): 0 -Za
0
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'Impo le: By stpninp dds form you are accepting Pace's NET 30 day payment temp and agreeig to late charges of 1.5% per month re,_ 4s not paid within 30 days. F-ALL-"20rev.07, 15- 107

FkeAnalytica! Client Name: ` Project # cL77 4o3 2-
i are Received: Guntersville ❑ Asheville ❑ Eden
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ?no
mmercial Pace Other - `tier
Custody Seal on Cooler/Box Present. ❑ yes Seals intact: ❑ yes Elno PToj:'Dui?`nate;
Proj. Narrie:
Packing Material: ❑ Bubble Wrap ubble Bags ❑ None ❑Other
Thermometer Used: IR Gun: T809 Type of Ice: Wei Blue None mples on ice, cooling process has begun
Temn Correction Factor: Add I Subtract 0 C
Corrected Cooler Temp.:_C
Temp should be above freezing to 6°C
Biological Tissue is Frozen: Yes No
Comments:
Date and I iti p e mi ing
�'
contents.
chain of Custody Present:
Q*65"C]No
❑NIA
1.
chain of Custody Filled Out:
e<s ❑No
❑NIA
2.
chain of Custody Relinquished:.
P
► les ❑No
❑wA
3.
Sampler Name & Signature on COC:
12e No
El NIA
4,
Samples Arrived within Hold Time:
❑Yes ONO
❑NIA
5.
ihort Hold Time Analysis (a72hr):
❑Yes E;Ko'
ON/A 16.
Rush Turn Around Time Requested:
❑Yes -i'INo
❑NIA
7.
Sufficient Volume: ,
es ❑No-
❑NIA
8.
',orrect Containers Used!
-Pace Containers Used:
0.-�-❑No
es ❑No
©N/A
❑NIA
g.
ainers Intact:
fY7ONo
❑NIA
10.
-iltered volume received for Dissolved tests-
Oyes ONO
IA
11.
;ample labels match COC:
-includes date/time/ID/Analysis Matrix:
s s ❑No
❑NIA
12.
,II containers needing preservation have been checked.
,II containers needing preservation are found to be in
ompliance with EPA'recommendation.
Kceptions: VOA, coliform, TOC, 08G, WI-DRO (water)
Yes ❑No
❑Ye o
❑Yes ❑No
❑NIA
❑NIA
13.
Initial when completed
;amples checked for dechlorination-
❑ves ONO
IA
14.
leadspace in VOA Vials( >6mm):
❑Yes ONO
IaNK
15.
rip Blank Present:
rip Blank Custody Seals Present
'ace Trip Blank Lot # (if purchased):
❑Yes ❑No „1 9
Oyes ONO ENIA
16,
Ilent Notification/ Resolution, Field Data required? Y i N
Person Contacted: DaleCTime:
Comments/ Resolution:
I )ject Manager Review: C/ �..� Date: �3 �d
ote: Whenever there is a discrepan a ling North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
ertification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-CHR-CS-003-rev.00

aceAnalX cal
n wpacel &C"
October 06, 2010
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
RE: Project: STORMWATER 9/29
Pace Project No.: 9278818
Paco Analytical Sorvlcos, Inc.
2225 Riverside or,
Asheville, NC 28804
[phone]
PaceAnalyllcal Services, Inc.
9800KinceyAve. Suite 100
Huntersvilre, NC 28078
[phone]
Bear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on September 30, 2010.
The results relate only to the samples included in this report. Results reported heroin conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace HUntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concealing this report, please feel free to contact me.
Sincerely,
q4-�nMwa;&td
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Tommy Lang, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not Be reproduced, except In full,
withoul lho wrillen consent of Pace Analyllcal Services, Inc..
Ye
Page f of 5

aceAnalytical�
nwn!paoelalia,com
Project: STORMWATER 9129
Pace Project No.: 9278818
Paco Analytical Sorvicos, Inc.
2225 Riverside Or,
Asheville, NO 2S804
CERTIFICATIONS
[phone]
Paco Analytical Sorvfcos, Inc.
9800KincoyAve. Suite 100
Hunlcrsvllro. NC 28078
[phone]
Ashovllle Certification lDs
2225 Riverside Dr., Asheville, NC 28804
North Carolina thinking Water Certification #: 37712
Connecticut Certification M PH-0106
North Carolina Wastewater Certifcalion #: 40
Florida/NELAP Coriiffcation M E87648
Pennsylvania Certification #: 68-03578
Massachusetts Certification M M-NCO30
South Carolina Bioassay Certification #: 99030002
Naw Jersey Certification #: NC011
South Carolina Cedifiealion M 92030001
North Carolina Bloassay Certification M 9
Virginia Certification #: 00072
REPORT OF LABORATORY ANALYSIS
This report shall not be raproevCod, except In fult,
without the vaitlen consent of Pace Analytical Services, tnc..
Page 2 of 5

acsAnalytical o
nwripacelabs_mm
Project: STORMWATER 9129
Pace Project No.: 9278818
PaceAnalytical Services, Inc.
2225 Riverside Dr.
Ashaville, NC 20804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800KinceyAva. Suite 100
HuntersvIllo, NC 28078
[phone]
Sample: SW02M Lab ID-. 9278818001 Collected: 0912911006:15 ReceNed: 0913011016:15 Matrix: Water
Parameters Results Units Report Limil DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7
Zinc 134 ugl1. 10.0 1 10101/10 11:50 10/04/10 21:38 7440-60-6
Date: 10106/2010 02.39 PM REPORT OF LABORATORY ANALYSIS Page 3 of 5
This report shall not be reproduced, except in full,
whhoul the written consent of face Anatyyftal Services, Inc..

aceAnalytical
rnrypace/ahoaa
Project: STORMWATER 9/29
Pace Project No.: 9278818
QC Batch: MPRP/7158
QC Batch Method: EPA200.7
Associated Lab Samples: 9278816001
METHOD BLANK: 505824
Associated Lab Samples: 9278816001
Parameter Units
Zinc ug/L
LABORATORY CONTROL SAMPLE: 505825
Parameter Units
Zinc ug/L
Pace Analytical Services, Inc.
2225 Rlversldo or.
Asheville, NO 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA200.7
Analysis Description: 200.7 MET
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 10105/1017:16
Paco Analytical Services, Inc.
9800KInceyAve. Stifle 100
Huntersville, NC 28078
[phone]
Spike LCS LCS °% Rec
Cone. Result % Rec Limits Qualifiers
500 163 93 85-115
MATRIX SPIKE SAMPLE: 505826
9278741001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Zinc ug/L ND 500 454 91 70-130
MATRIX SPIKE SAMPLE: 505828
9278476001 Spike MS MS % Rec
Parameter Units Result Cone. Result %Rec Limits Qualifiers
Zinc ugfL 143 500 606 93 70-130
SAMPLE DUPLICATE: 505827
Parameter
Zinc
SAMPLE DUPLICATE: 505829
Parameter
Zinc
Date: 1010612010 02:39 PM
92786280D1 Dup
Units Result Result RPD Qualifiers
ug/L ND 7J
9278417001 Dup
Uniis Result Result RPD Qualifiers
ug/L 23.9 23.3 3
REPORT OF LABORATORY ANALYSIS
This repod shall not be reproduced, except In full,
wilhout the written consent of Pace Analytical Services, Inc.,
.co."
YII-t�1��1�
Page 4 of 5

(�IacleAnalj*al"
rme pacerahcmr
QUALIFIERS
Project: STORMWATER 9129
Pace Project No.: 9278818
DEFINITIONS
Paco Analytical Sorvlees, Inc.
2225 RNerslde Dr.
Asheville, NC 26804
(828)2544178
Pace Analytical Services, Inc.
9800 KincoyAve. Suite 100
HuniersvIle, NC 28078
DF - Dllulion Factor, If reported, represents the factor applied to the reported data due to changes in sample preparation, d'dulion of
the sample aliquot, or wofslure, content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting Limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Dlphenylhydraz1ne (8270listed analyte) decomposes toAzobenzene.
Consistent with EPA guldellnes, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NO - Not Calculable.
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and eannol be separated from Diphonylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical Is NELAP accredited. Contact your Pace PM for the current list of accredited analyles.
[phone]
Dale: W10612010 02:39 PM REPORT OF LABORATORY ANALYSIS Page 5 of 5
This repot] shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, inc..
/nil c

/!2ceAnS
CHAIN -OF -CUSTODY / Analytical Request Document
The Cheh-or-Custody is a LEGAL DOCUMENT. All rolevant fields must be comploted accurat*.
SoctlanA Section a Section C
1165534
Required Chant fnforMabom R*cZWr4)d PrQJ= Womt1*rL hvolm lnfo=ation:
Roper% To: Aftntfon:
FiE0
AeZ.,ge 6 6
AddrAu= IVSd,< WK,,Ide,
77r,;pDEs r GROUND WATER r- DRINKING WATER
F UST r- RCRA OTHER
Ema3 Tw. PUrCh=0
Order No.:
J•e Qow
Raromnew
• F= Project
N=o: 15f4lA
Paco Pqw
RaquosUd Duo DaEofrATI. JPrqJ=
Numbor.
Pa00 prormo r,
(WIT
Section D MAbU Codes
15z",
PArquirodOn"t Inf0tMadon
COLLr-=D
Pmservavves
,
onnVN Water MV
0
water
wastewater Aw
p
compoum
composrm
Product p
rrART
%VS011C SL
SAMPLE ID Ou OL.
a:
wpo WP
(A-?- Ar AR
Sarnp4 Jos
w
0
zuq
2
<
MUST er UMOUE Tit-_Lw TS
w Ol�OT
0
0
X
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2:
0
0
-
0
V U
0
a
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0
0
=
DATE
TIME
DATE
TIME
:r
x
z
z
M
Pace Pro
. ject Not Lab4.D._
104111
lyl
1
2
4
10
12
ADVIrIONAL COMNENTS
FM:lKQ=HEREr�fAFFl�",.:
EPTF D BY, I AFFIL LATION
:DATE
Tlla
SAMPLE CONDITIONS
-W
?Ifello
leis
ORIGINAL
PRINT Nara of SAMPUEIR_,
E-
SICHATURE
DATE�Slqnod
1
,40,f
'LwpafL= N=: By so*,g Vft forth you are scoop" Pace. Nw,730 day pdr=t ton = b0mabg to 40A owmes of 1_1% porv,; 7s W.4 "*As -M P24 %ft-44 & c*vwl r_Aj I ­/ .. . ...

Pike Aw4ltical JJ/
C ' nt Name: 1fYaG Project #
Where Received: Huntersville ❑ Asheville ❑ Eden
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ C mercial Pace OtherDue, I
O flonal .,
Custody Seal on Cooler/Box Present: ❑ es no S S Intact: rj, T
F'rvj:.iaiie: ,
Packing Material: ❑ Bubble Wrap ❑Bubble Bags Noe DOther
Thermometer Used: IR Gun: T809 Type of Ice: /9 Blue None Samples on ice, cooling process has begun
Temp Correction Factor: Add i Subtract 0 C
Corrected Cooler Temp.: C
Biological Tissue Is Frozen: Yes No
Date and lnitia s f�orsr e ing
contents:
Temp should be above freezing to M
Comments:
Chain of Custody Present:
E Yes ONO
ONIA
t,
Chain of Custody Filled Out:
Yos ❑No
ONIA
2•
Chain of Custody Relinquished:
Yes ❑No
ONIA
3,
Sampler Name & Signature on COC:
Ye ❑uo
OWA
4.
Sam les Arrived within Hold Time;
Yes t=7No
©NrA
5.
Short Hold Time Analysis <72hr):
Oyes No
ONIA
6.
Rush Turn Around Time Requested:
Oyes o
©NIA
7.
3uffclent Volume:
Yu3 1JNo
ONIA
8.
;orrecl Containers Used:
aNo
UNIA
9.
-Pace Containers Used:
;Y�'SoNo
ONiA
lontainers Intact:
ras ONO
❑Ntn
10.
:11tered volume received for Dissolved tests
Cite nNo
NiA
11,
>ample Labels match COC:
grYes ONO
ONIA
12,
.includes date) irneliDlAnalysis Matrix:
r
dt con lalners: needing preservation have been checked.
la�os ONO
LINIA
13.
311 containers needing preservation are found to be in
es ONO
❑NIA
omptiance with EPA recommendation.
xcepllons: VOA, collrorm, TOC, Oe G, MORO (waler)
❑Yes ONO
lnival when compleled
',am les checked for dechforination:
©Yes ONO
ONG
14•
teadspace in VOA Vials }Bmm):
OYes ©No
wA
15,
'rip Blank Present:
Oyes ONO
Efw
16.
rip Blank Custody Seals Present
Oyes ONO
NIA
,ace Trip Blank Lot # (if purchased):
:Rent Notification/ Resolution: Field Data Required? Y 1 N
Person Contacted: Date/Time:
Comments) Resolution:
SCURF Review: Data: I S 1O ftF Review:
ote: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form vill be sent to the North Carolina OEHNR
,rtiflcaflon Office ( Le out of hold, incorrect preservative, out of 101np, Incorrect containers)
F-CHR-CS-003-rev.01

aceAnalyfical
www.pacelabs.="
r
October 27, 2010
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
RE: Project: STORMWATER
Pace Project No.: 9280372
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on October 21, 2010.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
qtn 9 uOaJz�
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
/ � l
Page 1 of 6

aceAnalytical
wim-pacelabs,com
Project: STORMWATER
Pace Project No.: 9280372
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
CERTIFICATIONS
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
North Carolina Drinking Water Certification M 37712
Connecticut Certification #: PH-0106
North Carofna Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
Pennsylvania Certification #: 68-03578
Massachusetts Certification #: M-NCO30
South Carolina Bioassay Certification #: 99030002
New Jersey Certification #: NCO11
South Carolina Certification #: 99030001
North Carolina Bioassay Certification #: 9
Virginia Certification M 00072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
y�GlCit.7=
Page 2 of 6

acmnalytical
www.pacelabscom
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)B75-9092
Project: STORMWATER
Pace Project No.: 9280372
Sample: SW02 Lab ID: 9280372001 Collected: 10/20/10 09:15 Received: 10/21110 15:25 Matrix: Water
Parameters Results Units Report Limit ❑F Prepared Analyzed CAS No, Qua!
200.7 MET ICP
Zinc
200.7 MET ICP, Dissolved
Zinc, Dissolved
Date: 10127/2010 02:28 PM
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
447 ug/L 10.0 1 10/22/10 11:15 10/26/10 18:46 7440-66-6
Analytical Method: EPA 200.7 Preparation Method: EPA 2003
339 ug/L 10.0 1 10/22/10 12:30 10/26/10 22:25 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
k
� cs:
Page 3 of 6

aceAnalytical
www.paceiabs.corn
I
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 2BB04
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 9280372
QC Batch: MPRP17279 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9280372001
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 515866
Matrix: Water
Associated Lab Samples: 9280372001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Zinc
ugfL
ND
10.0
10/2611018A0
LABORATORY CONTROL SAMPLE:
515867
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Zinc
ug1L
S00
495
99
85-115
MATRIX SPIKE SAMPLE:
515868
9280372001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Zinc
ug1L
447
500
904
91
70-130
MATRIX SPIKE SAMPLE:
515870
9280171002
Spike
MS
MS
% Roc
Parameter
Units
Result
Cone.
Result
% Rec
Limits Qualifiers
Zinc
ug/L
143
500
636
99
70-130
SAMPLE DUPLICATE: 515869
9280155001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Zinc
ug/L
80.9
77.9
4
SAMPLE DUPLICATE: 515871
9280171003
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Zinc
ug/L
2270
2290
1
Date: 10/27/2010 02:28 PM
t
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
c„
Page 4 of 6

aceAnalytical
www,pacelabs.com
f
Project: STORMWATER
Pace Project No.: 9280372
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP17284 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Dissolved
Associated Lab Samples: 9280372001
METHOD BLANK: 516080
Associated Lab Samples: 9280372001
Parameter Units
Zinc, Dissolved
ug/L
LABORATORY CONTROL SAMPLE:
Parameter
516081
Units
Zinc, Dissolved
ug/L
MATRIX SPIKE SAMPLE:
Parameter
516082
Units
Zinc, Dissolved
ug/L
SAMPLE DUPLICATE: 616083
Parameter
Units
Zinc, Dissolved
ug/L
Date: 10/27/2010 02:28 PM
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 10/2611022:18
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 495 99 85-115
9280372001
Spike MS MS
Result
Conc. Result % Rec
339
500 781 88
9280243001
Dup
Result
Result RPD Qualifiers
147
140 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
4 `cco,
Rec
Limits Qualifiers
70-130
Page 5 of 6

acmnalytical
r�ww.pacefabs.carn
i
QUALIFIERS
Project: STORMWATER
Pace Project No.: 9280372
DEFINITIONS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
(82B)254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
Date: 10127/2010 02:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
�A )
Page 6 of 6

Pacemalytrcal `
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. An relevant fields must be completed accurately.
Page: of
Section A
Section B Section C
Required Client Information:
Required Project Information: Invoice Information.
Report To: Attention:
1436176
Company:
Address'. -
Copy To:.OoV
Company m—
REGULATORY AGENCY
/
/i�
Adtlressr' O `� r.
NPDES i-" GROUNDWATER j DRINKING WATER
r UST ; E— RCRA (-` OTHER
Ernait To:
Purchase Order No.:
Pace O to
Rererertca:
P
Fax:
Project Name:
Pace Projacl
Site Location
l� S�
Manager:
STATE: ��
Requested Due DaterrAT:
Project Number-
Paco Profile III:
Requested
Analysis
Filtered
(YIN)
Section D Ma riA Codes
g
z
Required Client Information:
COLLECTED
Preservatives
i
Drinking ater OW
u
O
V
zz
Water WT
$
Waste Oter WW
Product! p
y
d]
COMPOSITE
START
COMPOSITE
ENn/GRAB
W
J
Z
SaIlfSplib SL
SAMPLE ID °r P e O
(A-Z. 0-9 !
d
u
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O0
"
¢
or]
It
W
?
a)
c
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r/Jy`
:) Air AR
Sample IDs MUST BE UNIQUE Tssue TS
O
W
a.
a
F
Other I OT
V
el
Lu
zpI
Q
R
�
~DATE
a
J
a
Inj(X�
O
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TIME
DATE
TIM>=
y
P
z
S
Z
Z
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Pace Project No./ Lib I-D.
1
's
i
i
LJ
c
3
4
S
6
7
B
9
10
i1
12
ADDITIONAL COMMENTS
RELINQUISHED BY t AFFILIATION
DATE
TIME
ACCEPTED BY t AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
d •• /O
�,'/S
�! 4'<r
aria
/,ZaS
Srt
es
4
t
-
:
RIG�NAL
SAMPLER NAME AND SIGNATURE
U
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PRINT Name of SAMPLER:
AWm
-
m
~
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—
U �+ E
SIGNATURE of SAMPLER:
DATE Sined
MW (MD1gYY).
'Import T By signing this loan you are a cspting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for. cee nAad wQhln 30 dayrCN F-ALL-Q-020rev.07. 15-M. _ .07
w

.W=..
hiceAnalytical' Client Name:_ _ " [ Ve. Project #
f" ire Received: —E Huntersville ❑ Asheville ❑ Eden
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ Commercial ace Other O fional
Custody Seal on Cooler/Box Present: El Yes o Seals intact: yes ❑ no P. Dub Date:.
Proj. IValne: ,
Packing Material: ❑ Bubble Wrap []Bubble Bags,,Ei"I�one [I Other
Thermometer Used: IR Gun: T809 Type of lce�et_ Blue None _ amples on ice, cooling process has begun
Tema Correction Factor: Add I Subtract _0 C
;orrected Cooler Te m p- j' C
emp should be above freezing to 6°C
Biolo icai Tissue is Frozen: Yes No
9
Comments:
Date and Init Is of perm examining
contents: ( r
1
;hain of Custody Present:
No
El NIA
1.
;hain of Custody Filled Out:
'❑No
❑NIA
2.
;hain of Custody Relinquished:
❑No
❑NIA
3.
')ampler Name Signature on COC:
_�..❑No
❑NIA
4,
;amples Arrived within Hold Time:
1—EJ'?e3
FJNo
❑NIt,
6, -
;hort Hold Time Analysis (<72hr):
Oyes
NIA
6.
tush Turn Around Time Requested:
❑Yes
NIA
7,
;ufflclent Volume:
Yeses ❑No
❑NIA
8,
:orrect Containers Used:
-Pace Containers Used:
1Yes
115Y�C_
ClNo
❑No
❑NIA
❑NIA
9.
uners Intact:
es
[]No
❑NIA
10.
iltered volume received for Dissolved tests
❑Yes PfI_o__❑NIA
11.
ample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
��(es
❑No
❑NIA
12.
i containers needing preservation have been checked.
II containers needing preservation are found to be in
mptiance with EPA recommendation.
ceptions: VOA, coliform, TOC, 0&G, WI-0RO {water}
�.s-
es
❑Yes
pNo
❑No
[]No
[iN/a
❑NIA
13.
Initial when completed
amples checked for dechlorination:
❑Yes
❑No NIA
14.
eadspace in VOA Vials (>6mm):
❑Yes
❑No _;3</A
15.
-ip Blank Present:
-ip Blank Custody Seals Present
ace Trip Blank Lot # (if purchased):
❑Yes
❑Yes
❑No
❑No
®<A
1,3WA
16.
lient Notification/ Resolution:
Person Contacted: Date/Time:
Z�ommentsl Resolution:
Field Data Required? Y I N
-IF Review: Y16f) Date-. SRF Review:1 TW IDate: Lo ) t jO
r«. Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
:rtification Office { i.e out of hold, incorrect preservative, out of temp, incorrect containers}
F-CHR-CS-003-rev.01
go)

r
aceAnalytical
vAmpacelabs.com
December 03, 2010
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
RE: P-ve,.-eT. Stsr,rnwater
Face Project No.: 9282963
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Asheville, NC 28804 Huntersville, NC 28078
[phone] _ _ [phone]
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on November 30, 2010.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
I
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYsis
This reportshall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
.«o+e
�`nelac,
Page 1 of 7

/ lzAnalXical
�/ mvivpacelabs.crm
i
i
Project: Stormwater
Pace Project No.: 9282963
Asheville Certification lDs
2225 Riverside Dr„ Asheville, NC 28804
Connecticut Certification #: PH-0106
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
New Jersey Certification #: NC011
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
4
North Carolina Wastewater Certification #: 40
Pennsylvania Certification #: 68-03578
South Carolina Bioassay Certification #: 99030002
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification M 356
r
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
a
Page 2 of 7

. 'aceAnalXical�
r w w.pacelabiccm
i
I
Project: Stormwater
Pace Project No.: 9282963
Lab ID Sample ID
9282963001 SW-02
f
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
EPA 200.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytica} Services, Inc..
,`nelac;
PaceAnalytical Services, Inc.
9800 Kincey Ave. Suite 100
Hunlersviae, NC 28078
[phone]
An alytes
Analysts Reported Laboratory
SHB 1 PASI-A
Page 3 of 7
0

f accAnafyft{cal v
www.pacelabs.ccm
f
Project: Stormwater
Pace Project No.: 9282963
Sample: SW-02
Parameters
200.7 MET ICP
Zinc
Date: 12/03/2010 04:43 PM
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 Kincey Ave. Suite 100
Asheville, NC 28804
Nuntersville, NC 28078
[phone]
[phone]
ANALYTICAL RESULTS
LabID: 9282963001 Collected: 11/20/10 08:30 Received: 11/30/10 14:00 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
223 ug/L 10.0 1 12/01/10 10:15 12/02/10 19:27 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc..
Page 4 of 7

6
,FaceAnalytical
/ www.pacefa6s.opm
Project: Starmwater
Pace Project No.: 9282963
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/7512 Analysis Method: EPA 200.7
QC Balch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 9282963001
METHOD BLANK: 534508
Associated Lab Samples: 9282963001
Parameter
Units
Zinc
ug/L
LABORATORY CONTROL SAMPLE:
534500
Parameter
Units
Zinc
ug/L
MATRIX SPIKE SAMPLE:
534510
Parameter
Units
Zinc
uglL
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 12/02/10 18:28
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 500 100 85-115
9282730001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
1.2 mg1L 500 1650 98 70-130
MATRIX SPIKE SAMPLE:
534512
9282785001
Spike
MS
MS % Rec
Parameter
Units
Result
Conc.
Result
% Rec Limits Qualifiers
Zinc
ug/L
47.4
500
528
96 70-130
SAMPLE DUPLICATE: 534511
9282895001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Zinc '
ug/L
43.5
44.9 `
3
SAMPLE DUPLICATE: 534513
9282811001
Dup
Parameter
Un'rts
Result
Result
RPD
Qualifiers
Zinc
uglL
18.5
19A
5
I Date: 12/03/2010 04:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
•ceo.
nelac � '
Page 5 of 7

d
Pace Analytical Services, Inc.
a r7 i
"'Ar lal(Xlcal
2225 Riverside Dr.
mvwpacelaDs.ccm
Asheville, NC 28804
r!
[phone]
QUALIFIERS
Project: * Stormwater
Pace Project No.: 9282963
DEFINITIONS
Pace Analytical Services, Inc.
9800 KinceyAve. Su10 100
Huntersville. NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limil and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 fisted analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MSfD)- M.trix Spike (Duplicate) -
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration,
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
r
Date: 12 O312010 04:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�`nelac:
Page 6 of 7

Y
- aceAnalytical
r' KVw-pacelabacom
r
f
Project: 0 Stormwater
Pace Project No.: 9282963
Lab ID Sample ID
9282963001 SW-02
0
Date: 12/03/2010 04:43 PM
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
2225 Riverside Dr.
9800 KinceyAve. Suite 100
Asheville, NC 28804
kuntersville, NC 28078
[phone]
(71)4)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
•
QC Batch Method QC Batch Analytical Method
EPA 200.7 MPRPl7512 EPA 200.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent or Pace Analytical Services, Inc..
°ne�,cx
Analytical
Batch
ICP16932
Page 7 of 7

PaceAnalytiO
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -cif -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page: of
Section A Section B Section C
Required Client Infomiatiorr Required Project Information: M%rafce Information:
Company: Report To: // Attention:1365822
/hirr LO /71
Address:
D J
Copy To:
Company Name:
Allt/l
REGIiL TORYAGENCY
address:Aiq
NPDES f GROUND WATER i" DRINKING WATER
40 L
030
UST i— RCRA OTHER (-`
mail To•.
Purchase Order No.:
Pace awte
Rererence:
Phone: — ' .S/ _
Fax:
Project Name:
Pace Project
Site Location
$r,4Tlc:
Requested Doe Date/TAT;
Project Numher:
Pace Pro Profile p: r
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
m
Z
Requlrod Clenl Informalfon MATRIX r CODE
a
g
COLLECTED
Preservatives
>
Drinking Water DW
^'
OU
O
Water WT
Waste Water W W
$
�j
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COMAOSiTE
STAnT
COMPDSiTE
ENGlGRAn
W
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Product P
Soillsolid St.
a
p
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SAMPLE ID D1pe wP
to
j-
w
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(A-Z. l Air AR
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�%�q�1 ' ] �
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Sample Ids MUST BE UNIQUE Tissue TS
E
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H
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N
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U
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Other OT
U
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J
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O
N
—p
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1/
f ,
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DATE
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DATe
TIME
#
_
_
=
Z
Z
O
y
0'_
Pace Project No./ Lab W.
1
-
2
3
4
5
6
7
8
9
10
ti
12
ADDITIONAL COMMENTS
RELINQUISHED BY AFFILIATION
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
Yoe-
q o0
3'
nJ
ORIGINAL SAMPLER NAME AND SIGNATURE
�
o —
PRINT Nome of SAMPLER:
DATE Signed
' SIGNATURE of SAMPLER: (MMlDDIYY):-30-10
m
•I" re: By signing this form you are accepting Pace's NET 30 day payment lerms and a]reaing to late charges of 1.5% per month. iTXms 4 paid within 30 days. F-ALL-0-020rev.07. It 2007

PaceAnalytica! Cli t Name:,4 LIlVa G Project #
are Received: Huntersville ❑ Asheville ❑ �P�aceOther-
Courier: ❑Fed Ex ❑UPS ❑ USPS ❑Client ❑ C mercial Optional
Custody Seal on Cooler/Box Present: ❑ yes no S als intact: ❑ yes ❑ no Proi.-Due.,Date:
Prot. Name:
Packing Material: ❑ Bubble Wrap ❑Bubble Bags None [--]Other
Thermometer Used: IR Gun: T809 Type of Ice: (9 Blue None Samples on ice, cooling process has begun
Temo Correction Factor: Add/ Subtract 0 C
Corrected Cooler Temp.: C
Biological Tissue is Frozen: Yes No
Date and Initial f P. rs g
contents: f f 4
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
Yes o
❑NIA
1.
chain of Custody Filled Out:
es o
❑NIA
2.
chain of Custody Relinquished:
Yeslaho
❑N1A
3.
Sampler Name & Signature on COC:
Yes o
❑NIA
4.
Samples Arrived within Hold `lime.-
Yes ❑No
❑NIA
5.
Short Hold Time Analysis (<72hr):
❑Yes No
IONIA
6.
Rush Turn Around Time Requested:
C]Yes No
❑NIA
7.
Sufficient Volume:
E Ye No
❑NIA
8,
correct Containers Used:
Yes No
❑N!A
9.
-Pace Containers Used:
es Nc
❑NIA
ainers Intact:
Yes ONO
❑NI
10.
-filtered volume received for Dissolved tests
❑Yes No
NIA
11,
Sample Labels match COC:
Oyes ❑No
❑NIA
12,
-Includes date/ ime/ID/Analysis Matrix:
u) r
kit containers needing preservation have been checked.
Yes ONO
❑N1A
13*
kIl containers needing preservation are found to be in
i�Yes ONO
❑NIA
:empliance with EPA recommendation.
!xceptions: VOA, coliform, TOC, O$G. WI -SRO (water)
❑Yes ENO
Initial when completed
iamples checked for dechlorinadon:
©Yes ❑No
Nu
14.
-leadspace in VOA Vials ( >6mm):
❑Yes El No
O/Nhy
15..
Trip Blank Present:
©Yes ❑No
N!
15.
Trip Blank Custody Seals Present
[]Yes ENO
NIA
'ace Trip Blank Lot # (if purchased):
,lient Notification! Resolution: Field Data Required? Y ! N
Person Contacted: Dateffime:
Comments! Resolution:
RF Review: Date: SRF Review: Date: Q
tote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
:ertification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers)
F-C H R-C S-003-rev.01