NCS000329_MONITORING INFO_20160926

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
AJ CS O Oc>'�'Z%
DOC TYPE
❑FINAL PERMIT
-�: MONITORING REPORTS- - - ------ -- --
❑ APPLICATION
❑ COMPLIANCE
0 OTHER
DOC DATE
p 2016. OR �(p
YYYYMMDD

September 21, 2016
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
REV 0VED
SEP 2 6 2016
CENTRAL FILES
DWR SECTION
i*ATI
P.O. Box 5030
2020 Asheraft Avenue
Monroe, NC 28111-5030
Phone: (704) 289A51 1
Fax: [phone]
Ftnail: joe.hinkle(a)atimetals.com
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
Start
I End
Year 7 — Period 1
13
March 1, 2016
1 August 31, �2016
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (13), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-451 1.
Thank you.
Sine ely,
f!4-
Jo inkle
E ironmental Manager

.� 1 y
Jill %1
joAA
t*
A`I'I - Bakers Plant
Stormwater Monitoring Report Form
Sample Date:
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analvsis:
Sample Time: % 1Y a^- _
Stormwater Discharge Outfal #1 01 Commingled)
Drainage Area = 2,915,470sq. ft. = 69 acres
% Impervious = 34%
.2464 PO�AAA�fZ
laze Analdlka L
40 CFR Part 136
Parameter
Results (mgll)
Benchmark Values (mgll)
BOD
a
30
COD
120
TSS
100
Cadmium
AIP
0.001
Chromium, total recoverable
p
1
Copper, total recoverable
0.007
Nickel, total recoverable
D
0.26
Zinc, total recoverable
//A?
0.067
Oil and Grease
20
Temp (effluent)
��, I (deg C)
n/a
Temp (downstream)
(deg C)
n/a
Temp (upstream)
91.3 (deg C)
n/a
Total Residual Chlorine
3
0.017
pH
7.8 (std units)
6-9 (std units)
Storm Date: Storm Duration: .3 O (Hrs.) Inches of Rainfall: Q• 'V0
Duration of time preceding rain event exceeding 0.1": /�A _ (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34)
Q(Total, cfs) = 1.5180 x Q. qO (Inches of rain) + 1.7595 x 10,1/0 (Inches of rain)
= __ / 3/I - cfs
F.NS--.LW—mmit-4i .Ra.vxfW___Ran 1

�r
55'neAnalytical*
www.AacWahs.com
September 07, 2016
Mr. Joe Hinkle
Allvac
RE: Project: BAKERS STORMWATER
Pace Project No.: 92309568
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew. [e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 19

` aceAnalytical'
www.pacelaea.com
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite too
Huntersvifle, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Flodda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaA/ELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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i
` acmnalytical o
www.pwMbacom
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
BAKERS STORMWATER
92309568
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92309568001
BSW01
SM 2540D
ALC
1
PASI-A
92309568002
BSW01
SM 5210B
CJH1
1
PASI-A
92309568003
BSW01
SM 5220D
CJH1
1
PASI-A
92309668004
BSW01
EPA 1664B
JMS
1
PASI-C
92309568005
BSW01
EPA200.7
SH1
5
PASI-A
92309668006
BSW01
SM 4500-CI G
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, Inc.
` lac,Analytli(ialo
9800 KinceyAve. Suite 100
Huntersville, NC 28078
wWW Pecelebd.cam
[phone]
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Sample: BSW01
Lab ID: 92309568001 Collected: 08/19/16
07:14
Received: 08/19/16 07:20 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
06/18/16 07:20
Collected Date
08/18/16
1
08/18/16 07:20
Collected Time
07:12
1
08/18/16 07:20
Field pH
7.8 Std, Units 0.10
1
08/18/16 07:20
Field Temperature
31.1 deg C 0.50
1
08/18/16 07:20
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
18.3 mg1L 8.3
1
08/22/16 15:26
REPORT OF LABORATORY ANALYSIS
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Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 19

` Iace Analytical
(�wxwpecefehs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Sample: BSW01 Lab ID: 92309568002 Collected: 08/19/16 07:15 Received: 08/19/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
5210B BOD, 5 day Analytical Method: SM 52106
BOD, 5 day 26.4 mg1L 2.0 1 08120/16 03:44 08/24/16 22:07
Date: 09/07/2016 09:46 AM
REPORT OF LABORATORY ANALYSIS
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r
V laneAnapical"
www.pecelabaoam
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Samplo: BSW01 Lab ID: 92309568003 Collected: 08/19/16 07:16 Received: 08/19/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD
Chemical Oxygen Demand
Date: 09/07/2016 09:46 AM
Analytical Method: SM 52201)
72.0 mg1L 25.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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08/30/16 06:30
Page 6 of 19

aceftlyfical
www.paceiab3.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW01 Lab ID: 92309568004 Collected: 08/19/16 07:18 Received: 08/19/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease N❑ mg1L 5.0 1 08/23/16 08:14
Date: 09/0712016 09:46 AM
REPORT OF LABORATORY ANALYSIS
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(�IacldatdeAnalytical
www.pacNabi.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Sample: 9SW01 LabID: 92309568005 Collected: 08/19/16 07:19 Received: 08119/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 2003
Cadmium
ND ug/L 1.0 1 08/22/16 21:55
08/23/16 11:43
7440-43-9
Chromium
ND ug/L 5.0 1 08/22/16 21:55
08/23/16 11:43
7440-47-3
Copper
19.3 ug/L 5.0 1 08122/16 21:55
08/23/16 11:43
7440-50-8
Nickel
ND ug/L 5.0 1 08122/16 21:55
08/23/16 11:43
7440-02-0
Zinc
ND ug/L 10.0 1 08/22/16 21:55
08/23/16 11:43
7440.66-6
REPORT OF LABORATORY ANALYSIS
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Date: 09/07/2016 09:46 AM
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Page 8 of 19

laneAnal)&cal"
w ww.pecelebs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW01 Lab ID: 92309568006 Collected: 08/19116 07:20 Received: 08/19/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.043 mglL 0.024 1 09/02/16 16:35 7782-50-5 H1
Date: 09/07/2016 09:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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IceAnalytical
tvww.pacelah&com
Project: BAKERS STORMWATER
Pace Project No.: 92309568
QC Batch: 325932
QC Batch Method: EPA 1664B
Associated Lab Samples: 92309568004
METHOD BLANK: 1805587
Associated Lab Samples: 92309568004
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 08/23/16 08:09
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1805588
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg1L
40 35.1
88
78-114
MATRIX SPIKE SAMPLE:
1805589
92309031001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg1L
ND 40
34.3
86
78-114
Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc„ Page 10 of 19

e
5aceAnalXical
(�wwwpnobs cam
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309568
QC Batch: 325888
QC Batch Method: EPA200.7
Associated Lab Samples: 92309568005
Analysis Method:
Analysis Description:
EPA 2007
200.7 MET
METHOD BLANK: 1805455
Matrix: Water
Associated Lab Samples: 92309568005
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Cadmium
ug1L
ND
1.0
08/23/1610:13
Chromium
ug/L
NO
5.0
0812311610:13
Copper
ug/L
ND
5.0
08/23/1614:25
Nickel
uglL
ND
5.0
08/23/1610:13
Zinc
uglL
ND
10.0
0812311614:25
LABORATORY CONTROL SAMPLE: 1805456
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug1L
500
506
101
85-115
Chromium
ug1L
500
494
99
85-115
Capper
ug1L
500
520
104
85-115
Nickel
ug1L
500
493
99
85-115
Zinc
ug1L
500
512
102
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1805457
1805458
MS
MSD
92309373001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
ND
500
500
505
502
101
100
70-130
1
Chromium
ug1L
ND
500
500
471
458
94
91
70-130
3
Copper
ug1L
ND
500
500
519
507
103
101
70-130
2
Nickel
ug1L
ND
500
500
430
429
85
85
70-130
0
Zinc
ug1L
ND
500
500
473
472
93
93
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1805503
1805504
MS
MSD
92309549002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
ND
500
500
467
455
93
91
70-130
3
Chromium
uglL
ND
500
500
451
439
90
88
70-130
3
Copper
ug1L
ND
500
500
486
472
96
94
70-130
3
Nickel
ug1L
8.9
500
500
462
451
91
88
70-130
2
Zinc
ug1L
41.9
500
500
502
490
92
90
70-130
2
Results presented on this page are in the units Indicated by the -Units" column except where an ahemate unit Is presented to the right at the result,
REPORT OF LABORATORY ANALYSIS
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Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc..
Page 11 of 19

aceAnalytical
www.pecefabs.conr
QUALITY CONTROL DATA
Paco Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92309568
QC Batch: 325866
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92309568001
METHOD BLANK: 1805270
Matrix: Water
Associated Lab Samples: 92309568001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mglL
NO 2.5 08/22116 15:20
LABORATORY CONTROL SAMPLE: 1805271
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mglL
250 240 96 90-110
SAMPLE DUPLICATE: 1806272
92309381001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mglL
14.9 14.5 3
SAMPLE DUPLICATE: 1805273
92309570001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mglL
12.2 12.4 2
Results presented on this page are In the units Indicated by the 'Units" column except where an ahernate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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laneAnaVical"
www.pateiabs.00m
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309568
QC Batch: 326649 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 9230956B006
METHOD BLANK: 1809616 Matrix: Water
Associated Lab Samples: 92309568006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg1L NO 0,024 09/02/16 16:35
SAMPLE DUPLICATE: 1809617
92309578001 Dup
Parameter Units Result Result RPD qualifiers
Chlorine, Total Residual mg/L NO NO H1
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an ahernate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.
Page 13 of 19

aceAnalytical
www.pacefabLown
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309568
QC Batch: 325737 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92309568002
METHOD BLANK: 1804788 Matrix: Water
Associated Lab Samples: 92309568002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOO, 5 day mg/L ND 2,0 08124/16 22:07
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1804789
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 193 97 84.6-115.4
SAMPLE DUPLICATE: 1804790
92309572002 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg1L 2.0 NO
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc..
Page 14 of 19

4
aceAnalytical
www.pe Mh3.com
Project: BAKERS STORMWATER
Pace Project No.: 92309568
QC Batch: 326642
QC Batch Method: SM 5220D
Associated Lab Samples: 92309568003
METHOD BLANK: 1809582
Associated Lab Samples: 92309568003
Parameter
Chemical Oxygen Demand
QUALITY CONTROL DATA
Analysis Method: SM 5220D
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg1L ND 25.0 08/30/16 06:30
Pace Analytical Services, Inc.
980o Kincey Ave. Suite 100
Huniersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1809583
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 741 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809584 1809585
MS MSD
92308849002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc, Result Result % Rec % Rec Limits RPD Qua)
Chemical Oxygen Demand mg1L 77.0 750 750 781 779 94 94 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809586 1809587
MS MSD
92309513002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 92.0 750 750 801 801 95 95 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc..
Page 15 of 19

aceAnalytical
.pecefebxwm
QUALIFIERS
Project: BAKERS STORMWATER
Pace Project No.: 92309568
DEFINITIONS
Paco Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit,
RL - Reporting Limit.
5 - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in S1N846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute,
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H 1 Analysis conducted outside the EPA method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 16 of 19

lanemapiole
wwwpecelabscom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: BAKERS STORMWATER
Pace Project No.: 92309568
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample 10
QC Batch Method
QC Batch Analytical Method
Analytical
Batch
92309568001
BSW01
92309568004
BSW01
EPA 1664B
325932
92309568005
BSW01
EPA 200.7
325888 EPA 200.7
325920
92309568001
BSW01
SM 2540D
325866
92309568006
BSW01
SM 4500-CI G
326649
92309568002
BSW01
SM 52108
325737 SM 5210B
325753
92309668003
BSWo1
SM 5220D
326642
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 19

Document Name:
Document Revised:Aprif 25, 2016
R
ace,4nalytical
Sample Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CHR-CS-003-rev.19
Face Huntersvllle Quality Office
Client Name:
7 Project N:
Courier: ❑Fed Ex ❑UPS ❑USPS Client
❑ Commercial (apace [-]other:
Custody Seal Present? ❑Yes I`❑i No Seals Intact? ❑Yes []No
Wio# : 92309563
} 8Y�095i�ts
r -+�
Date/Initials Person Examining Contents: ' Mt
Packing Material: ❑Bubble wrap OBubbfe Sags ❑None ❑Other:
Thermometer: T1505 Type of Ice: ❑Wet ❑Slue ❑None ©Samples on Ice, cooling process has begun
Correction Fattor: 0.0'C Cooler Temp Corrected ('C): /'..3 Biological Tissue Frozen? []Yes ONo ❑N/A
Temp should be above freezing to 6'C
USDA Regulated Soil ( ©N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
❑Yes ONo including Hawaii and Puerto RICO)? ❑Yes [DNii
Comments/Discrepant :
Chain of Custody Present?
Yes
ONO
[I N/A
1.
Samples Arrived within Hold Time?
©Yes
❑No
N/A
2.
Short Hold Time Analysis (02 hr.)?
QYS
❑No
[]NIA
3.
Rush Turn Around Time Requested?
QYes
No
N A
4.
Sufficient Volume?
Yes
No
❑N/A
5.
Correct Containers Used?
QYes'
[:]No
❑N/A
6.
-Pace Containers Used?
QYes
❑No
N/A
Containers Intact?
CoYelf
❑No
❑N/A
7.
Samples Field Filtered?
Yes
❑No
[DN/A 1
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
QY s
❑No
[I N/A
9.
-Incfudes Date/T1me/ID/Anal sis Matrix: U"
All containers needing acid/base preservation have been
10. HNc,°H„
checked?-------- ---- -
-[Dyes.
- ❑Nor❑N/A-
All containers needing preservation are found to be in
KC,
compliance with EPA recommendation?
Hssw°HQ
(HNO3, H2SO4, HCIQ; NaOH >9 Sulfide, NaOH>12 Cyanide)
gYes
[]No
[]N/A
N-di°H-12
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLHg
No
[]NIA
rookVZ 0ACPH's
Samples checked for dechlorination?
❑Yes
[]No
N]A
11.
Heads ace In VOA Vials >5-6mm)7
Yes
EINo
ON/a
12.
Trip Blank Present?
❑Yes
❑No
Orem
13.
Trip Blank Custody Seals Present?
[]Yes
❑No
Qr4(A
Pace Trip Blank Lot q ifpurchased):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: _ Datejfime: _
Comments/Sample
Discrepancy:
Field Data Required? []Yes ❑No
Project Manager SCURF Review: `LI _ Date: U let f
Project Manager SRF Review: - Date: 1 [ .4 , /r
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEH�N(R Certification Office (Le.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 18 of 19

v
FaceAnalytical'
, .patelafa.tvm
Section A
Required Client Information:
/?%
Section B
Required Project Information:
�fRena,Tw, io/Y,.,•,y tor,
Copy To:ry
E L
Duo baterTAT; Project Number.
i
CHAIN -OF -CUSTODY / Analytical Request Document
The Chainof-Custody is a LEGAL DOCUMENT. All relevant fields mess be completed accumtcly.
Section C
Invoico Inicmi Lion_
Section D Matrix Codos
RequlrcdCb-4 lnttxmnton MAIRI% r COOE
—
4
COLLECTED
Drinking Water ON
U
. z0
Water WT
Waste Wa[or WW
$
3
a1
Compmrm
CONaOSnE
U
Product f?
_
Simi
r Aa
j
soil,solid SL
0
w
SAMPLE ID 0 OL
v
(A-Z. 0-9 f; ) Air AR
w
O
LU
a
W
Z
Sample 10s MUST BE UNIQUE Tissue TS
a
w
Oder OT
V
x
w
L
m
0
ac
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a
a
�
H
Q
C
¢
O
—
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rn
DATE
TIME
DATE
TIME
m
C, -cp- 1 - 1� ayt rLso„
V me:
i
. z
Presaw.tives `}
Page: of
1995723
REGULATORY AGENCY
t' •1(_ FV NPDES F GROUNDWATER f- DRINKING WATER
f UST i RCRA OTHER
Site Location , //''
STATE:
Requested Analysis Filtered (YIN)
MI
~ J tV f
t V
41
O c 2,o
izZ o
Z
CID
�v
.s
_o r� L)
UCl
X Pace Protect Nod Lab I.D.
12 I
ADDITIONAL COMMENTS f RELINQ
U
ISHED BY I AFFILIATION DATE TIME ACCEPTED BY f AFFILIATION DATE TIME SAMPLE CONDITIONS
�, � �•'/Iz � % � r- —•-', :� Y/�4' "�x' � �-, P!'-t E �i�1� x-19-1r, f3cc 1. � V f� i
r, r
I ORIGINAL SAMPLER NAME AND SIGNATURE
PRINT Name at SAMPLER: ap,:4 P t
o SIGNATURE of SAMPLER: DATE Signed
H
v
U m r
E
N
h
'tmpDnant Note: BY sKF.Ml Ih. tone you arc aa: -pImq P,is NET 30 tlay pgmmrt terms and aq,eeirn to lam eh-rrr or 1.5 : wr rnonlh for wW inveip6 not Pod -Shin 30 days
F-ALL-0-020rev.07, 15-May-2007

`A�ATI
Allvac - Bakers Plant
Stormwater Monitoring Report Form
Sample Date:
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analvsis:
Sample Time:S.,o�•-
Stormwater Dischar eg Outfall #02 (Non-Commin led)
Drainage Area = 212,952sq. ft. = 4.9 acres
% Impervious = 12%
_payiai AF1�.3R. , X/4., C/cn fit
Pace Anal iea.l
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
a ,
30
COD
got
120
TSS
/ DO
100
Cadmium
Alp
0.001
Chromium, total recoverable
. 0 j
1
Copper, total recoverable
0.007
Nickel, total recoverable
D Dl
0.26
Zinc, total recoverable
0.067
pH
(std units)
6-9 (std units)
Storm Date: /g' Storm Duration: 3. 40 (Hrs.) Inches of Rainfall: Q. 4)0
Duration of time preceding rain event exceeding 0.1": /68 _ (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 4.9 acres x .88) -+- .9 x inches rain/12inches/ft. x 4.9 x .12)
Q(Total, cfs) = 0.1437 x 49• YO (Inches of rain) + 0.0441 x O (Inches of rain)
6. 075, cfs
Allvac - Bakers Plant
FHC — RW — Mnnitorinn Rpi m Fnrm — Rev 1

1aceAnalyltircal•
wvw pecalatu.mm
August 30, 2016
Mr. Joe Hinkle
Allvac
RE: Project: BAKERS STORMWATER
Pace Project No.: 92309572
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
(704 )875-9092
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
PA - - ���'�D
W. �o
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wdtten consent of Pace Analytical Services, Inc..
Page 1 or 15

leac,malxicalo
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
wmpsceleftcom
[phone]
CERTIFICATIONS
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Charlotte Certification Ids
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87W
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
VifginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 15

aceAnalytical.
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SAMPLE ANALYTE COUNT
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92309572001
BSW02
SM 25400
ALC
1
PASI-A
92309572002
BSW02
SM 52106
CJH1
1
PASI-A
92309572003
BSW02
SM 5220D
CJH1
1
PASI-A
92309572004
BSW02
EPA200.7
SH1
5
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 15

leAnalytrcal"
www.ppceletu.wm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersvilte, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Sample: BSW02 Lab ID: 92309572001 Collected: 09/18/16 07:25 Received: 08119/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data Analytical Method:
Collected By
DPJ
1
08/18/16 07:35
Collected Date
08/18/16
1
08/18/16 07;35
Collected Time
07:26
1
08/18/16 07:35
Field pH
7.6 Sid. Units
0.10 1
08/18/16 07:35
Field Temperature
28.4 deg C
0.50 1
08/18/16 07:35
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
100 mg1L
6.2 1
08/22/16 15:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:49 PM without ft written consent of Pace Analytical Services, Inc..
Page 4 of 15

aceAnalytical
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ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: -BSW02 Lab ID: 92309572002 Collected: 08/18/16 07:27 Received: 08/19/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day Analytical Method: SM 5210B
BOD, 5 day 2.0 mg/L 2.0 1 08/20/16 03:44 08/24/16 22:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/3012016 08:49 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 15

aceAnalytical
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ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW02 Lab ID: 92309572003 Collected: 08/18/16 07:28 Received: 08/19116 07:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 82.0 mg1L 25.0 1 08/30/16 06:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 15

aceAnalytical
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ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW02
Lab ID: 92309572004
Collected: 08/18/16 07:29
Received: 08/19/16 07:20 Matrix: Water
Parameters
Results
Units
Report Limit DF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug1L
1.0 1
08/22/16 21:55
08/23/16 18:14
7440-43-9
Chromium
19.1
ug1L
5.0 1
08/22/16 21:55
08/23/16 18:14
7440-47-3
Copper
118
ug1L
5.0 1
08/22/16 21:55
08/23/16 18:14
7440-50-8
Nickel
14.6
ug1L
5.0 1
08/22116 21:55
08/23/16 18:14
7440-02-0
Zinc
116
ug1L
10.0 1
08/22/16 21:55
08/23/16 18:14
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08130/2016 08:49 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 15

aceAnalytical
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QUALITY CONTROL DATA
Pate Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92309572
QC Batch: 325889
Analysis Method: EPA 200.7
QC Batch Method: EPA200.7
Analysis Description: 2003 MET
Associated Lab Samples: 92309572004
METHOD BLANK: 1805461
Matrix: Water
Associated Lab Samples: 92309572004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
ND 1.0
08/2311618:08
Chromium
ug/L
ND 5.0
08123/1618:08
Copper
ug1L
ND 5.0
08123/1618:08
Nickel
ug1L
ND 5.0
08/2311618:08
Zinc
ug1L
ND 10.0
08/24/1615A3
LABORATORY CONTROL SAMPLE:
1805462
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Cadmium
ug1L
500
465
93 85-115
Chromium
ug1L
500
462
92 65-115
Copper
ug/L
500
479
96 85-115
Nickel
ug1L
500
455
91 85-115
Zinc
ug1L
500
467
93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1805463
1805464
MS
MSD
92309572004
Spike
Spike MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc, Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
ug1L
ND
500
500 479
479 96 96
70-130
0
Chromium
ug/L
19.1
500
500 498
500 96 96
70-130
0
Copper
ug1L
118
500
500 616
613 100 99
70-130
0
Nickel
ug1L
14.6
500
500 479
479 93 93
70-130
0
Zinc
ug1L
116
500
500 586
585 94 94
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1805501
MS
92309538002
Spike
Parameter
Units
Result
Conc.
Cadmium
ug1L
ND
500
Chromium
ug1L
ND
500
Copper
ug1L
0.0078
500
mg/L
Nickel
ug1L
ND
500
Zinc
ug1L
0.039
500
mg1L
1805502
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc,
Result
Result
% ReC
% ReC
Limits
RPD
500
483
477
97
95
70-130
1
500
481
479
96
96
70-130
0
500
508
505
100
99
70-130
1
500
466
462
92
91
70-130
1
500
504
500
93
92
70-130
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc..
Qual
Page 8 of 15

aceAnalytical®
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QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309572
QC Batch; 325866 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92309572001
METHOD BLANK; 1805270
Associated Lab Samples: 92309572001
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE: 1805271
Parameter Units
Total Suspended Solids mg1L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 08/22/1615:20
Spike LIDS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 240 96 90-110
SAMPLE DUPLICATE: 1805272
92309381001 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 14.9 14.5
SAMPLE DUPLICATE: 1805273
92309570001 Dup
Parameter Units Result Result
Total Suspended Solids mg1L 12.2 12.4
RPD Qualifiers
3
RPD Qualifiers
2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 15

aceAnalytical
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QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 325737
Analysis Method:
SM 5210B
QC Batch Method: SM 5210B
Analysis Description:
5210B BOD, 5 day
Associated Lab Samples: 92309572002
METHOD BLANK: 1804788
Matrix: Water
Associated Lab Samples: 92309572002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
SOD, 5 day
mg1L
ND
2.0 08124/16 22:07
LABORATORY CONTROL SAMPLE: 1804789
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 193
97 84.6-115.4
SAMPLE DUPLICATE: 1804790
92309572002 Dup
Parameter
Units
Result Result
RPD Qualifiers
BOD, 5 day
mg/L
2.0
NO
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15

(�5a'cmnalyttal*
www.pacelebs.omn
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309572
QC Batch: 326642 Analysis Method: SM 5220D
OC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92309572003
METHOD BLANK: 1809582 Matrix: Water
Associated Lab Samples: 92309572003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mglL NO 25.0 08/30/16 06:30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE; 1809583
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 741 99 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1809584 1809585
MS MSD
92308849002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 77.0 750 750 781 779 94 94 90-110 0
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 1809586 1809587
MS MSD
92309513002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 92.0 750 750 801 801 95 95 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an aitemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc,. Page 11 of 15

Pace Analytical Services, Inc.
aceMalytical 9aDD ney Ave. Suite 100
Huntersville, NC 28078078
www.pac&bs.com
[phone]
QUALIFIERS
Project: BAKERS STORMWATER
Pace Project No.: 92309572
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anaiyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyt ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc„
Page 12 of 15

lacmnalyficalo
www.pecerabs.cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704 )87S909 2
Project: BAKERS STORMWATER
Pace Project No.: 92309572
Analytical
Lab ID' Sample ID QC Batch Method QC Batch Analytical Method Batch
92309572001
BSW02
92309572004
BSW02
EPA 200.7
325889 EPA 200.7 325919
92309572001
BSW02
SM 2540D
325866
92309572002
BSW02
SM 5210B
325737 SM 52106 325753
92309572003
BSW02
SM 52200
326642
Date: 08/30/2016 08:49 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 15

1.,,Aa'c6Ana&Vca1
Document No.:
F-CH R-CS-003=rev.19
Page 1 of 2
Issuing Authority:
Pace Huntersvilie Qua lltv.Office
Pann 7 of? for Intorn-I 11— nnl
Client Name: Projec bWO# • 92309572
A -T ..j1
Courier: ❑Fed Ex ❑UA5 ❑USPS ❑Client
❑ Commercial QPac'e ❑Other: 1111 Illlll i
921.109572
Custody Sea! Present? []Yes QNo-�- Seals Intact? ❑Yes QNo'
Date/Inkials Person Examining Contents:iA<<Y'19`rG
Packing Material: ❑Bubble Wrap []Bubble Bags QNane ❑Other:
Thermometer: T1505
Type of Ice: ❑Wet ❑Blue ❑None [pSamples on Ice, cooling process has begur
Correction Factor: 0.0'C Cooler Temp Corrected (°C): _ f 3 Biological Tissue Frozen? ❑Yes QNtf ❑N/A
Temp should be above freezing to 6'C
USDA Regulated Soil ( CAI,Wr, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Old samples originate from a fareign source (internationally,
❑Yes [. o Including Hawaii and Puerto Rico)? ❑Yes [Duo
Camments Discrepant :
Chain of Custody Present?
: YC
dNo
N/A
1,
Samples Arrived within Hold Time?
Y!! CS
QN0
N/A
2.
Short Hold Time Analysis (<72 hr.)?
OYeT
No
N/A
3.
Rush Turn Around Time Requested?
OYes
I No
(]N/A
4.
Sufficient Volume?
Q Y s
ONo
N/A
5.
=orrect Containers Used?
©Ye
ONo
❑N/A
6.
-Pace Containers Used?
[]Y¢s
[]No
ONJA
-ontainers Intact?
QYes
❑No
[:]NIA
7.
iamples Field Filtered?
❑Yes
No
QN/A
8. Note if sediment is visible In the dissolved Container
sample Labels Match COC?
QYe
❑No
❑N/A-
• 9:
-Includes Date/Time/ID/Analysis Matrix: V11
tll containers needing acid/base preservation have been
10, HHu �Ha
hecked.Z_. - --_ -_—
©es _❑No.
_[]N/A
__... — ..... --- —�__� �_�_ _ — ---
ill containers needing preservation are found to be in
HaoH<:
ompliance with EPA recommendation?
HuwoH<1
HNO3, H2SO4, HCI<2; NaOH n9 Sulfide, NaOH>12 Cyanide)
©Yes
❑No
❑N/A
1rloHpH>u
xceptions: VOA, Coilform, TOC, Oil and Grease,
IR6/S015 water DOCALHg
OYes
[]No
JDA
am les checked for dechlorinatlon?
❑Yes
[:]No
N%A
11.
leads ace in VOA Vials >5-6mm)?
QYes
ONO
E/A
12.
rip Blank Present?
❑Yes
[]No
014/A
13.
rip Blank Custody Seals Present?
[--]Yes
[]No
©N'I'A
ace Trip Blank Lot q if purchased):
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? Des ONO
Person Contacted: _ _ Date/Time: _
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review: L."`
Note: Whenever there Is a discrepancy affecting North Carolina compii
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Date:
Date:
a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Page 14 of 15

1
o CHAIN -OF -CUSTODY 1 Analytical Request Document -'
-FacEAnalytical The Chaim -of -Custody is a LEGAL DOCUMENT. AV relevant fields must be completed accurately.
' nmr.p�celatrs.rom
Section A SeCtion B Section C Paya. Ot
Required 6llii-einti Information: Required Prvterd Intormaton; Invoice Inronnalion:
7 V1 1 1
Compawl 2L'Ic.1 �'fGr-JC°i Ik;y RcpitTo: ram. AltcnEion: ,Ll"' OG(itfa� 9 03271
Adtlress:
�r� 410' 1l%
Copy To:
1 �ut' /nx%E'
Cn,rgvnrry Nn
j1 f C��/Nt cicfS
REGULATORY AGENCY
A471-o-e �/L
Address& r
X ��sO !°Jo�rr-ot tjCG
NPDES r GROUND WATER r DRINKING WATER
r UST RCRA OTHER
Emai TO: Purchase
Order NO.:
Pace o„r+le
I
Ref�:
e' '
Fax; P
geil Name;
S�'a._r, y„dr�f'Br
Px Proelp
Site Location
d �2�y' j//
i a1C�rj
Mnnarier.
STATE: A/C
Requested Due DaterrAT: PfOjoGt
Number:
Paw Prerde #:
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes I
g
z
Required 0i ilnfo woo MATRix i CODEt
s
o
COLLECTED
Preservatives
'-
Drinking Wafer aW
U
zz
Wafer WT
Waste Water WW
PfOtlVCt P
$
v
-q
U
m
Q
COUPOSPE
START
COPA-M,TE
ENpTR.\B
U
W
_
Z
'
SO111solid SL
SAMPLE ID wipe
=
"
'L-
v
(A-Z. 0-91 ,-) Air AR
p
w
C.
UJ
z
m
Sampic IOs MUST BE UNIOUE Tissue TS
Other OJT
O
U
d
ti
z
2
y
J i.J
x�
�0N
0(
o�
aa�
�G
a
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p
=O
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2
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DATE
TIME
DATE
nME
y
OLL
-t
a
=
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z
Z
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2
V
Pace Project Nol Lab I.D.
1
L'Si�O I
) I
9
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wr
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a
gsnly ''
wr
G
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9
10
I
11
I
12
i
I ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
i-
I �ti
`,�-
1- Lb
r1�2z� P.'4-i-� A V a_
� -I Y �
i :3 C� Q
i . �
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hZ !a
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SAMPLER NAME AND SIGNATURE
U
+..
m
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PRINT Name of SAMPLER:v j� Po�c: J�c y Cle/�
a
N n }
m
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o
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u
"_
Of
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E
-,
DATE Signed Q /
SIGNATURE of SAMPLER :��j� /'
�Cr%
,- Ij
tMMIDDfYY); U
ilmpnnant Nine_ 8Y :iitlmnn this Imm you are acmpG,gl P.ur i NET 30 m tied ch-gr s of 1.5 : t+cr n+eran lur.m+y'onoir.,ls m, Prue r„thin 30 unyx. FALL-0.020rov.07. 15-May-2007

OATI Allvac
Allvac - Bakers Plant
Stormwater Monitoring Report Form
Sample Date: _ 9-/$ /6
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analvsis:
Sample Time: _ 7.: ?'vim•. -
Stormwater Discharge Outfall #03 (Non -Commingled)
Drainage Area = 336,580sq. ft. = 7.8 acres
% Impervious = 15%
11zw11w J-e - . �}l G/a f�
Ake a Ala IyAie a
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
0 8
30
COD
a 4
120
TS S
a , 02
100
Cadmium
V
0.001
Chromium, total recoverable
D 3 7
1
Copper, total recoverable
0.007
Nickel, total recoverable
0D68
0.26
Zinc, total recoverable
0.067
pH
(std units)
6-9 (std units)
Storm Date: 4 '-M / e Storm Duration: J 4 (Hrs.) Inches of Rainfall: Q}�
Duration of time preceding rain event exceeding 0.1": la 8 (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (.4 x inches rain/12 inches/ft. x 7.8 acres x .85) + .9 x inches rain/I2inches/ft. x 7.8 x. 15)
Q(Total, cfs) = 0.2210 x (Inches of rain) + 0.0878 x a. �/'0 (Inches of rain)
�9• /023 efs

aCMnalyfcal
wnrw.pecWb&com
August 30, 2016
Mr. Joe Hinkle
Allvac
RE: Project: BAKERS STORMWATER
Pace Project No.: 92309570
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)87Er9092
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preslon Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
'q8
This report shall not W reproduced, except in full,
without the wdtlen consent of Pace Analytical Services, Inc..
Page 1 of 15

lac
eAnalyticale
wwwpm*ebs.com
CERTIFICATIONS
Project: BAKERS STORMWATER
Pace Project No.: 92309570
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
North Carolina Drinking Water Certification #: 37706
Florida/NEl-AP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification A M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 15

lac,
Pace Analytical Services, Inc.
A IGl�fla fo
9800 Kinley Ave. Suite 100
078fl�[�r Huntersville, NC 28078
www.pecofobs.com
[phone]
SAMPLE ANALYTE COUNT
Project: BAKERS STORMWATER
Pace Project No.: 92309570
A nalytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92309570001 BSWD3
SM 2540D
ALC
1 PASI-A
92309570002 8SW03
SM 52106
CJH1
1 PASI-A
92309570003 BSW03
SM 5220D
CJH1
1 PASI-A
92309570004 BSW03
EPA200.7
SH1
5 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 15

Pace Analytical Services, Inc.
�ceAml 1r^al•
LrJI/`T Vi[
3800 KineyAve. Suite 100
Huntersville, NC 28078
www.pecWbs.cam
[phone]
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309570
Sample: BSW03
Lab ID: 92309570001 Collected: 08/18/16 07:34
Received: 08119/16 07:20 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
08/18/16 07:40
Collected Date
08118/16
1
08/18/16 07:40
Collected Time
07;33
1
08/18/16 07:40
Field pH
7.2 Std. Units 0.10
1
08/18/16 07:40
Field Temperature
28.8 deg C 0.50
1
08/18/16 07A0
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
12.2 mg/L 5.0
1
08/22/16 15:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc. Page 4 of 15

(?9ac,eAnalytical*
www.pnoWebi.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309570
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvitle, NC 28078
[phone]
Sample: BSW03 Lab ID: 92309570002 Collected: 08/18/16 07:35 Received: 08/19116 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
52108 BQD, 5 day
BOD, 5 day
Date: 08/30/2016 08:48 PM
Analytical Method: SM 5210B
10.8 mg1L 2.0 1 08/20/16 03:44 08/24/16 22:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 15

aceAnalytrcal®
www.peoNa6aoom
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92309570
Pace Analytical Services, Inc.
9800 Kinsey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW03 Lab ID: 92309670003 Collected: 08/18/16 07:37 Received: 08/19/16 07:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 32.0 mg1L 25.0 1 08/30/16 06:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 15

e
acmnalytical
wwwp&oW&63.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92309570
Sample: BSW03 Lab ID: 92309570004 Collected: 08118/16 07:39 Received: 08/19/16 07:20 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
NO
ug1L
1.0
1
08/22/16 21:55 08123/16 11:46
7440-43-9
Chromium
23.7
ug1L
5.0
1
08/22/16 21:55 08123/16 11:46
7440-47.3
Copper
58.8
ug1L
5.0
1
08/22/16 21:55 08/23/16 11:46
7440-50-8
Nickel
6.8
ug1L
5.0
1
08/22/16 21:55 08/23/16 11:46
7440-02.0
Zinc
65.9
ug1L
10,0
1
08/22/16 21:55 08/23/16 11:46
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 15

aceAnalytical
www.pesefabs.oam
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309570
QC Batch: 325888 Analysis Method: EPA200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92309570004
METHOD BLANK: 1805455
Matrix: Water
Associated Lab Samples: 92309570004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug1L
NO
1.0
08123/1610:13
Chromium
uglL
NO
5.0
0812311610:13
Copper
ug1L
NO
5.0
081231% 14:25
Nickel
ug1L
NO
5.0
08/23/16 10:13
Zinc
ug1L
NO
10.0
08123/1614:25
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1805456
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
uglL
500
506
101
85-115
Chromium
uglL
500
494
99
85-115
Copper
uglL
500
520
104
85-115
Nickel
uglL
500
493
99
85-115
Zinc
ug1L
500
512
102
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1805457
1805458
MS
MSD
92309373001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug1L
NO
500
500
505
502
101
100
70-130
1
Chromium
ug1L
NO
500
500
471
458
94
91
70-130
3
Copper
ug1L
ND
500
500
519
507
103
101
70-130
2
Nickel
ug1L
NO
500
500
430
429
85
85
70-130
0
Zinc
ug1L
NO
500
500
473
472
93
93
70-130
0
MATRIX SPIKE R MATRIX SPIKE DUPLICATE:
1805503
1805504
MS
MSD
92309549002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
uglL
NO
500
500
467
455
93
91
70-130
3
Chromium
ug1L
NO
500
500
451
439
90
88
70-130
3
Copper
ug1L
NO
500
500
486
472
96
94
70-130
3
Nickel
ug1L
8.9
500
500
462
451
91
88
70-130
2
Zinc
ug1L
41.9
500
500
502
490
92
90
70-130
2
Results presented an this page are In the units Indicated by the "Units" cotumn except where an alternate untt Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/3012016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 15

15n6Ana1jfta1"
wwwpecelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309570
OC Batch: 325866 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis description: 2540D Total Suspended Solids
Associated Lab Samples: 92309570001
Pace Analytical Services, Inc.
9800 Kincay Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1805270
Matrix:
Water
Associated Lab Samples: 92309570001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5
08/22/16 15:20
LABORATORY CONTROL SAMPLE: 1805271
Spike
LCS
LIDS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
240
96 90-110
SAMPLE DUPLICATE: 1805272
92309381001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 14.9 14.5 3
SAMPLE DUPLICATE: 1805273
92309570001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 12.2 12.4 2
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08130/2016 08:48 PM without the written consent of Pace Analytical Services, Inc..
Page 9of15

aceAnalytical
www.Peoawwoom
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309570
QC Batch: 325737 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92309570002
METHOD BLANK: 1804788
Associated Lab Samples: 92309570002
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 08/24/16 22:07
LABORATORY CONTROL SAMPLE:
1804789
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
BOD, 5 day
mg/L
198 193 97
84.6-115.4
SAMPLE DUPLICATE: 1804790
92309572002 Dup
Parameter
Units
Result Result RPD
Qualifiers
BOD, 5 day
mg1L
2.0 ND
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 15

laneAnalyficals'
www.pacelab&oem
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92309570
QC Batch: 326642 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92309570003
METHOD BLANK: 1809582
Associated Lab Samples: 92309570003
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 1809583
Parameter Units
Chemical Oxygen Demand mg1L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 25.0 08/30116 06:30
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
750 741 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809584 1809585
MS MSD
92308849002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cane. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg1L 77.0 750 750 781 779 94 94 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809586 1809587
MS MSD
92309513002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 92.0 750 750 801 801 95 95 90-110 0
Results presented on this page are In the units Indicated by the "Unks" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15

Pace Analytical Services, Mc.
IeLIC,Analjdical"9600 Kinsey Ave. Suite t00
Huntersville, NC 28478
+ D WM [phone]
QUALIFIERS
Project: BAKERS STORMWATER
Pace Project No.: 92309570
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N -Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not qe reproduced, except in full,
Date: 08/30/2016 08A8 PM without the written consent of Pace Analytical Services, Inc..
Page 12 of 15

Document Name:
le Condition Upon Recel
Document No.:
F-CHR-CS-003-rev.19
• • Client Name:
- 1+ 71. � Project
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial wFace— ❑Other:
Document Revised:April 25, 2016
Page 1 of 2
Issuing Authority:
Pace Huntersvllle Quality Office
WIO# : 92309570
III III III 11111111111111111
92.109570
Custody Seal Present? ❑Yes []Na Seals intact? ❑Yes ❑No
Date/Initials Person Examining Contents: ��I ' 16
Packing Material: []Bubble Wrap ❑Bubble Bags []None ❑Other.1/rrst'cipk,r-t_
Thermometer: T1505 Type of Ice: [:]wet [-]Blue ❑None ❑Samples on Ice, cooling process has begun
Correction Factor: 0.O'C Cooler Temp Corrected ('C): A 5 Biological Tissue Frozen? []Yes QNo ❑N/A
Temp should be above freezing to VC
USDA Regulated SoII ( Q.N/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Internationally,
❑Yes RNo- Including Hawaii and Puerto Rico)? []Yes ©No-
Comments/Discrepant :
Chain of Custody Present?
Yes
ON.
NIA
1,
Samples Arrived within Hold Time?
es
QNo
❑N A
2.
Short hold Time Analysis (<72 hr.)?
QXC
❑No
❑N/A
3.
Rush Turn Around Time Requested?
(--]Yes
Nii
[]N/A
4.
Sufficient Volume?
[DYs
QN.
N/A
5.
Correct Containers Used?
[Dyes
(:]No
❑N/A
6.
-Pace Containers Used?
Yes
❑No
❑N/A
Containers Intact?
Rfe,
ON.
El N/A
7.
Samples Field Filtered?
❑Yes
❑No
ON%A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC? ,Ar ,
es
❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix: vV
All containers needing acid/base preservation have been
/
10, H„CIpH,r
checked?—_---_-_-__ . M- _ _ ..__DYes-_
❑No__
❑N/A-
-. ---- . - -- .. - - -- - - - - -- - - - - - -- . ._,--
All containers needing preservation are found to be in
HOpH`1
compliance with EPA recommendation?
HuwpH.:
WNN H2504, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide)
(y)Yes
[]NO
❑N/A
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLHg
Dyes
No
N/A
Ni01nn0A`p"
Samples checked for dechlorination?
❑Yes
[]No
N/A
11.
Headspace in VOA Vials >5-6mm ?
Yes
No
N,A
12.
Trip Blank Present?
❑Yes
[]No
mrf/A
13.
Trip Blank Custody Seals Present?
❑Yes
❑No
QN/A
Pace Trip Blank Lot q (if purchased):
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: Date/Tlme:
Comments/Sample
Discrepancy:
Field Data Required? ❑Yes []NO
i
Project Manager SCURF Review: _ I�% r Date:
Project Manager SRF Review: Date: Z
Note: Whenever there is a discrepancy affecting North Caro u6-compliance samples, a copy of this form will be sent to the North Carolina DEHN Certification Office (Le,
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 14 of 15

-PaceAnalytical'
wrr.02celabs.com
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section'A Section B Section C
Page: of
Required Gicnt Information: Required Project Information; lnvoice tnformatiom
Report To. Atsenton:
2063513
��%
Address: 1 Copy
To:
Company N me - r
REGULATORY AGENCY
IAJC /
I
Atldres���Q �1 p� w`� �G
NPDES j GROUNDWATER ♦— PRINKING WATER
UST r RGRA j OTHER
Email To: Purahase
Order No.:
Pave Owrn
I
Reference:
117 e:
Far: Project
Name: L
'Er
Paco Prpjocl
Site Location
] !!fa°r
qer.
Requested Duo DatorTAT: Project
Number:
PdC° PrON" N. "1
� � > T � �'
STATE:
Requested
Analysis
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Section D Matrix CodezI
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SAMPLER NAME AND SIGNATURE
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ATlan
Sample Location:
Person Collecting Samples:
' Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Allvac - Bakers Plant
Stormwater Monitoring Report Form
Non -Contact Cooling Wastewater
cw,aL Pope -1'R._, 3&Axes /ngse,
pace na1 e-c,;J
40 CFR Part 136
Non -Coot
Sampling
Sampling
Estimated
Total Res
Temperature
pH
Effluent
Downstream
Upstream
p
Cool Water
Date
Time
Flow (MGD)
Ch1�)e
(std. units)
3oS,—
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acMnalytical
wnvwpacobs com
September 07, 2016
Mr. Joe Hinkle
Allvac
RE: Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„
Page 1 of 18

leAnaly ical *
www:p&CWab&torrr
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification* E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNE LAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 18

Pace Analytical Services, Inc.
aceMalyilcal o
9(300 Kinsey Ave. Suite 100
Huntersville,
NC 28U7878
wwwpacefabs.com
{704}875-9092
SAMPLE ANALYTE COUNT
Project:
NONCONTACT COOLING WATER
Pace Project No.:
92309578
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92309578001
BAKERS NON CONTACT #1
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92309578002
BAKERS NON CONTACT 02
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92309578003
BAKERS NON CONTACT #3
EPA 16646
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92309578004
BAKERS NON CONTACT #4
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASi-A
92309578005
BAKERS NON CONTACT #5
EPA 1664E
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92309578006
BAKERS NON CONTACT #6
EPA 1664B
JMS
1
PASI-C
SM 4500-Cl G
MDW
1
PASI-A
92309578007
BAKERS NON CONTACT #7
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
92309578008
BAKERS NON CONTACT #8
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, tnc.. Page 3 of 18

IeAnalytical
wwwPxwbs.mm
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28070
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Sample: BAKERS NON CONTACT Lab ID: 92309578001 Collected: 08/18/16 07:30 Received: 08/19116 07:20 Matrix: Water
#1
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease NO mg1L 5.0 1 08/23/16 08:15
4500CL G Chlorine, Residual Analytical Method: SM 4500-Cl G
Chlorine, Total Residual ND mg1L 0.024 1 09/02/16 16:35 7782-50-5 1-11
Date: 09/07/2016 09A6 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 18

ac6Analyiical.
www.pwalabs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Pace Analytical Servicea, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BAKERS NON CONTACT Lab Il): 92309578002 Collected: 08/18/16 07:49 Received: 08119/16 07:20 Matrix: Water
#2
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 08/23/16 08:16
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual ND mg1L 0.024 1 09/02/16 16:35 7782-50-5 H1
Date: 09/07/2016 09:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, tnc..
Page 5 of 18

IeAnalytical�
www.pacobs.com
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Pace Analytical Services, Inc.
9800 Kincey Ave, SuRe 100
Huntersville, NC 28078
[phone]
Sample: BAKERS NON CONTACT Lab ID: 92309578003 Cotlected: 08/18/16 08:05 Received: 08/19/16 07:20 Matrix: Water
#3
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 08/23/16 08:16
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual ND mg1L 0.024 1 09/02/16 16:35 7782-50-5 H)
Date: 09/07/2016 09:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fell,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 18

aceAnalytical
wwwpacefaUcom
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BAKERS NON CONTACT Lab ID: 92309578004 Collected: 08/18/16 08:22 Received: 08/19/16 07:20 Matrix: Water
#4
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg1L 5.0 1 08/23/16 08:16
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.047 mg1L 0.024 1 09/02/16 16:35 7782-50-5 H1
Date: 09/07/2016 09:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 18

aceAnalytical
wrwpeoOASUMM
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Pace Analytical Services, Inc.
9B00 Kincey Ave, Suite 100
Hunlersville, NC 28078
[phone]
Sample: BAKERS NON CONTACT Lab ID: 92309578005 Collected: 08/18/16 08:36 Received: 08/19/16 07:20 Matrix: Water
#5
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/23/16 08:17
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.050 mglL 0.024 1 09/02/16 16:35 7782-5C-5 H1
Date: 09/07/2016 09A6 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 18

aceAnalytrcal
wwwpecabbs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Sample: BAKERS NON CONTACT Lab ID: 92309578006 Collected: 08/18/16 08:50 Received: 08/19/16 07:20 Matrix: Water
#6
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1 08/23/16 08:18
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.089 mg1L 0.024 1 09/02/16 16:35 7782-50-5 1-11
Date: 09/07/2016 09:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 18

aceAnalytical
www.pamrabs cam
ANALYTICAL RESULTS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: BAILERS NON CONTACT Lab ID: 92309578007 Collected: 08/18/16 09:10 Received: 08/19116 07:20 Matrix: Water
#7
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mglL 5.0 1 08/23/16 08:18
4600CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.45 mglL 0.024 1 09/02/16 16:35 7782-50-5 H1
Date: 09/07/2016 09:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 18

IeAnalytical"
wnnrpecafabimm
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Sample: BAKERS NON CONTACT
#8
Parameters
HEM, Oil and Grease
Oil and Grease
4500CL G Chlorine, Residual
Chlorine, Total Residual
Date: 09/07/2016 09:46 AM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab lD: 9230957800B Collected: 08/18/16 09:27 Received: 08/19/16 07:20 Matrix: Water
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 1664B
NO mg/L 5.0 1 08/23/16 08:19
Analytical Method: SM 4500-Cl G
NO mg1L 0.024 1 09/02/1616:35 7782-50-5 1-11
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 18

aceAnalXical!p
www.pacalabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
QC Batch: 325932
Analysis Method:
EPA 1664E
QC Batch Method: EPA 1664E
Analysis Description:
1664 HEM, Oil and Grease
Associated Lab Samples: 92309578001, 92309578002,
92309578003, 92309578004,
92309578005, 92309578006, 92309578007,
92309578008
METHOD BLANK: 1805587
Matrix: Water
Associated Lab Samples: 9230957B001, 92309578002,
92309578003, 92309578004,
92309578005, 92309578006, 92309578007,
92309578008
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Oil and Grease mg/L
ND 5.0 08/23/16 08:09
LABORATORY CONTROL SAMPLE: 1805588
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Oil and Grease mg1L
40 35.1
88 78-114
MATRIX SPIKE SAMPLE: 1805589
92309031001 Spike
MS MS % Rec
Parameter Units
Result Cone.
Result % Rec Limits Qualifiers
Oil and Grease mg[L
ND 40
34.3 86 78-114
Results presented on this page are In the units Indicated by the "Units" column except vAere an alternate unN Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc..
Page 12 of 18

leAnalrytical"
wSYw,pacelafis.cam
QUALITY CONTROL DATA
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 326649 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92309578001, 92309578002, 92309578003, 92309578004, 92309578005, 92309578006, 92309578007,
92309578008
METHOD BLANK: 1809616 Matrix: Water
Associated Lab Samples: 92309578001, 92309578002, 92309578003, 92309578004, 92309578005, 92309578006, 92309578007,
92309578008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg/L ND 0.024 09/02116 16:35
SAMPLE DUPLICATE: 1809617
92309578001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg1L ND ND H1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in N4,
Date: 09107/2016 09:46 AM without the written consent of Pace Analytical Services, Inc..
Page 13 of 18

IeAnalytical"
www.pecelobs.com
QUALIFIERS
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonilrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 18

aceAna1jfta1"
www.pacelahs.00m
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc,
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NONCONTACT COOLING WATER
Pace Project No.: 92309578
Analytical
Lab lD Sample ID QC Batch Method QC Batch Analytical Method Batch
92309578001
BAKERS
NON
CONTACT #1
EPA 16648
325932
92309578002
BAKERS
NON
CONTACT #2
EPA 16646
325932
92309578003
BAKERS
NON
CONTACT #3
EPA 16648
325932
92309578004
BAKERS
NON
CONTACT #4
EPA 16649
325932
92309578005
BAKERS
NON
CONTACT #5
EPA 16648
325932
92309578006
BAKERS
NON
CONTACT #6
EPA 1664E
325932
92309578007
BAKERS
NON
CONTACT #7
EPA 16648
325932
92309578008
BAKERS
NON
CONTACT #8
EPA 16648
325932
92309578001
BAKERS NON CONTACT #1
SM 4500-CI G
326649
92309578002
BAKERS NON CONTACT #2
SM 4500-CI G
326649
92309578003
BAKERS NON CONTACT #3
SM 4500-CI G
326649
92309578004
BAKERS NON CONTACT #4
SM 4500-CI G
326649
92309578005
BAKERS NON CONTACT #5
SM 4500-CI G
326649
92309578006
BAKERS NON CONTACT #6
SM 4500-CI G
326649
92309578007
BAKERS NON CONTACT #7
SM 4500-CI G
326649
92309578008
BAKERS NON CONTACT #8
SM 4500-CI G
326649
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc., Page 15 4f 18

Document Name:
Document Revised:Aprll 25, 2016
aceAnal1�1lCc?��
�
Sample Condition Upon Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CHR-CS-003-rev.19
Pace Huntersville Quality Office
•• F Client Name:
W(D# : 92309578
DomCourier;
Project a
Fed Ex ❑UPS ❑USPS
[]Client
❑ Commercial ❑Q Pace ❑Other:
I 92ZO9576
Custody Seal Present? [-]Yes ©No Seals Intact?
[]Yes ❑No SI`i
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap COBubble Bags
❑None/ ❑Other: /
Thermometer; T1505 Type of Ice: ©Wet ❑Blue []None ❑/ Samples on Ice, coolingpocess has begun
Correction Factor: 0.0'C Cooler Temp Corrected ('C): �j, 12
Biological Tissue Frozen? ❑Yes QNo []N/A
_
Temp should be above freezing to 6'C
USDA Regulate Soil ( VN/A, water sample)
Did samples griginate in a quarantine zone within the United States: CA, NY,
or 5C (check maps)? Did samples originate from a foreign source (internationally,
Dyes ®No
including Hawaii and Puerto Rico)? ❑Yes 060
Comments/Discrepancy;
Chain of Custody Present?
i
FlYes,
ONo
N/A
1.
Samples Arrived within Hold Time?
esONO..,
N/A
2.
Short Hold Time Analysis (02 hr.)?
Dyes
❑No i
Q N/A
3.
Rush Turn Around Time Re uested?
Yes"
ti No
N/A
4.
Sufficient Volume?
©Yes.
ON.
N/A,
S.
Correct Containers Used?
[E]Yes
❑No
❑N/A
6.
-Pace Containers Used?
Yes❑Nv
NIA
Containers Intact?
Yes
❑No/
ONIA
7.
Samples Field Filtered?
❑Yes,'
©No
N/A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
©Yes
❑No
❑N/A
9.
-Includes Date/Time/JD/Analysis Matrix: T
All containers needing acid/base preservation have been
10, wc34n�1
checked? -- _ __k . _
- DYes --
❑No- -0
/A-
. - - - — - - —
AII containers needing preservation are found to be In
wnoe.l
compliance with EPA recommendation?
„uaPH«
(HNO3, H7SO4, HCIc2; NaOH >9 Sulfide, NaOH>12 Cyanide)
❑Y '
ONO
❑ /A
Ha ONplbll
Exceptions: VOA, Coliform, TOC, Oil and Grease,
DRO/8015 (water) DOC,LLH
Yes
ONO
❑N A
"jO"n"QAC
samples checked for dechlorinatlon?
QYes
❑No
O NIA
11,
Heads ace in VOA Vials >5.6mm ?
[]Yes
QNo
0 /A
12,
Trip Blank Present?
Oyes
04
❑N A
13.
Trip Blank Custody Seals Present?
❑Yes
ONO
QN/A
Pace Trip Blank Lot # (if purchased):
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? [-]Yes ONO
Person Contacted: Date/Time.
Comments/Sample
Discrepancy:
Project Manager SCURF Review: �i f . Date:
Project Manager SRF Review: /G71 Date:
Note: Whenever there Is a discrepancy affecting North Carolina comp ante samples, a copy of this form will be sent to the North Carolina OE NH R Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 16 of 18

Storm Water Monitoring
(NON CONTACT)
Baker North
Chain of Custody Record
OATI
SPxia4&t&trriWs
Dane a1
Project Number/Name: NonContact Cooling Water
Project Location: Allvac Baker
Sampler's Signature:
�c 7
u.G.�C.`ir i — , /�I�S >�
Date:
CL
E
v1
w
i=
a
E
CL
N
tS
m
io
o
{
CL
>_
L
a
u
y
CL
y
N
a
V
"
41
C
O
C
O
a
E
°J
c
D
Requested Test
Parameters U
J
'" 7
GI f)
None
Y
7. 9
3r✓•�
Residual Chlorine W
j fL`rrf.nl. f%
y%w.
G
G/A)
None
Y
7
j'
Residual Chlorine(,)
rr.�lrCui;iy
,9
G
G/D
None
Y
j
o?%./°�
Residual ChlorineLU
f' rfrl`•�- G°•, ,f z
:02,
G
G/_Pr
None
Y
17 6
2 7.g"'
Residual Chlorine v
�rfr�rir<'rfo;i trf'
, •'�b.�
G
G/,P
None
Y
7. `%
� (C
Residual Chlorine
/ta rrlrn '; 1fk
SU.�
G
G/P
None
Y
• 7
�76. /°�
Residual ChlorineLU
G
G)J�
None
Y
�7.y°�
Residual Chlorine(.
C,nrl'.v,6w b- r
9 • 7r�_
G
G/_A
None
Y
b',�
�$ 7r�
Residual Chlorine L
Meter Calibrated:
/ N
IThermorneter Calibrated
/ N
Sampling and Field analysis completed by:
n
!j
Relinquished By:
I Received By: r`z
~�
Date:
Time:
jDate:
Y,11,i
Time:
Relinquis d y:
Recelved By : -t_L(
•,ra
Date_;_
Time:--- = C'Ls
Date:- 2
=
EMS8akerSouthSWREV#2 5/10/2016
Page 17 of 18

Storm Water Monitoring
(NON CONTACT)
Baker north
Chain of Custody Record
ion ATI
Specialty Materials
page 42
Project Number/Name: NonContact Cooling Water
Project location: Allvac Baker
Sampler's Signature:
,� >''U 4-1 , ���_�rC` „,u r] •�.
Date: 611 lu' /(,
0
CL
0
o
a
ti
a
0
ai
CL
�
0
�
�,
o
G7
a
?
CDa
a
U
U
a
o
«'
M
a
H
c
O
Requested Test
Parameters
;
f 1 "o
G
G
HCL
Y
30'
Oil & Grease
i /.!vr['edrrr�i
'`i9a�
G
G
HCL
Y
$, 9``
Oil &Grease
�zyCrs/.iv,c'e��;�,f3
Goa
G
G
HCL
Yf
Oil &Grease
I,{rY�G1h'ic'ht,,,
,�
G
G
HCL
Y
7 V L:
Oil & Grease
trr!lmcrr�ti't/f
�;��,L
G
G
HCL
Y
�� U`t
Oil &Grease
G
G
HCL
Y
30, / °�
Oil & Grease
,��fr/ronl'�iitalt
:/lJ
G
G
HCL
Y
2 ���'
Oil & Grease
'IWelif//m(IIA-409
G
G
HCL
Y
�.?`�
Oil & Grease
Meter Calibrated: CO / N
IThermometer Calibrated: N
Sampling and Field analysis completed by:
Relinquished By:
f' �!' Relinquished By:
Date : fi/9-
Time: jam,,_
Date : C,1/G Tlme; '"y.• iL%
Relinquished By:
1,
lRelinquished By:
.� 1�c-
Date : /,
Time:
Date :
Time:
EHS Baker South SW REV 4 Z 5/10/2016
1,aisC r-I'�'L `'_(q-(( I SC L Cy.6
}i
Page 18 of 18

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NC.-S�� or
Certificate of Coverage Number: NCG
FACILITY NAME r= A/Iyac �s
PERSON COLLECTING SAMPLES) Jiuvii� oft T12., /can eig.ez-
CERTIFIED LABORATORY(S) _ awe A04 JVA6L j Lab #-a
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 1;?4914
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY a idA _
PHONY, NO. (?pV) A89----
(SIGNATUREf'O PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
SampleDate
Collected
�•
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? — yes ✓o
(if yes, complete Part B)
Part B: Vehicle Maintenance Ac vity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
Oil and
Grease
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/dd/ r
MG
m
m
unit
Rallmo
Form SWU-246-051100
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date
Total Event Precipitation (inches): 49• 'tO
Event Duration (hours): 3, O
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours):
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
44 9 i3
(Signature of Per itte (Date)
Form SWU-246-051100
Page 2 of 2

,i-; AA
RMENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: httn:/ jportal.p�denr.orU jwebjw jws/su/npdessw#tab-4
Permit No.: or Certificate of Coverage No.: N/C&/_/—/—/_/_/—/
Facility Name:
County: e
Phone No.
Inspector: -Axyrd root SK„ Z&dn C/onTz
Date of Inspection:
Time of Inspection: 7-'e20P= _
Total Event Precipitation (inches): N. 35Q -
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
El"Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event" However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:

1. Outfall Description:
Outfall No. S914/ _ Structure (pi
Receiving Stream: 7v Br_
ditch, etc.) '�'-a/h4at( _
C
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the
(light, medium, dark) as descriptors: —
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): ?z�, ? G „!
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 © 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 ® 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
© 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes ®o
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

AL
4 '
MC®ENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out thisform, please visit: bttp:/Iportal.ticdcnr.org/web/wq/ws/su/npde5sw#tab-4
Permit No.: or Certificate of Coverage No.:
Facility Name: ATl
County: L 17,"On , Phone No. 7441 a?89-0-11
Inspector: %J�►.��� /o�c �. /91a07 G%anTz
Date of Inspection: 8-/8 /b
Time of Inspection: % 30
Total Event Precipitation (inches): tQ
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
El"Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
.. Jr —

r
t
a
1. Outfall Description:
Outfall No.SAL— Stru
Receiving Stream:
Describe the industrial activities
C S
re (pi e, ditch, etc.)
CAeeZ
occur within the outfall drainage area:
2. Color: Describe the color of the
(light, medium, dark) as descriptors:
using basic colors (red, brown, blue, etc.) and tint
) , 1 1- J—.+_ .-
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 04W 0 _
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 © 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 ® 3 4 5
4. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 © 3 4 5
7. Is there any foam in the stormwater discharge? Yeso
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yeso
10. Other Obvious Indicators of Stormwater Pollution:
List and describe ._. �l I& e_
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
SWU-242, Last modified 10/25/2012
Page 2 of 2

k.
RC-®EN�
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out thisform, please visit: htto:lloortaLudenr.org jebJwq jws/suApdessw#tab-4
Permit No.: N/C/S/Q/ o / D/ 3 /a/S/ or Certificate of Coverage No.: N/lc/G/_,._/_..,/_/—/ /_/
Facility Name: T Va.c - cif
County: Zn/,0,7 Phone No. _70y889- ysl/ TT
Inspector: So , I Av c zrg. c/e'de
Date of Inspection: 8-f8 j6
Time of Inspection: S�4
Total Event Precipitation (inches): D. YD -
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
�es ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for Iocal storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signature, I certify that this report is accurate and complete to the best of rimy knowledge:

1. Outfall Description:
Outfall No5kdl St
Receiving Stream:
Describe the industrial activiti
re (pipe, ditch, etc.) n/i
r within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: G Gam
I Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 9Zorr e
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy-
2 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 ® 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
© 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
10. Other Obvious Indicators of "St�ormwater Pollution:
List and describe _ /V qwG.. _
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
sWU-242, last modified 10/25/2012