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HomeMy WebLinkAboutWQ0012662_Residual Annual Report 2014_20141219ANNUAL LAND APPLICATION CERTIFICATION FORM sa Permit#: t '�tQO012662 County: Facility Name (as shown on permit): Land Application Operator: Harnett Year: 2014 Dunbar Foods Corp. Carl Hite Phone: 910-892-3175 Land application of residual solids as allowed by the permit occurred during the past calendar year? R1 Yes 0 No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Part B: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. R1 Yes E3 No If no please, provide a written description why the facility was not complia plain corrective action taken. DEC 19 1. Only residuals approved for this permit were applied to the permitted sites. 2014 2. Soil pH was adjusted as specified in the permit and lime was applied (if n GV0M soil pH of at least 6.0 or the limit specified in the permit.. ®PROCESSING UNIT 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) -copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part'503 regulated facilities). 8. All operations and maintenance requirements in the` permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. —9.No--contravention-of-Ground-Water -Qualify-Standards--occurred-at a monitoring well -or -explanations --of - - -- - violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this• site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.- 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Carl Hite, Plant Operations Manager �_ J Z (I l o'l I Permittee Name and Title (type or print) Signature of Permittee Date 2,11 gn re o reparer* Date Signature of and Applier Date (if di€fe nt from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) DENR FORM ACF (5/2003) ANNUAL DISTRIBUTION AND PERMIT #: WQ0012662 FACILITY N PHONE: 910-892-3175 COUNTY: _ FACILITY TYPE (please check one): SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Dunbar Foods Corp. Harenett OPERATOR: Carl Hite Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) - 13 Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendlar year? 13 Yes OXo No If No skip parts A, B, C and certify form below t Part A*: Part B*• Month Sources s include NPDES # if () (. applicable) ' Volume (dry tons) Recipient Information . Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February March j April May June July August September sweet potatoes 0 114.564 October sweet potatoes j 0 156.516 November December i Totals: Annual(dry tons):. j 0 271.08 0 0 Amendments used: 0 i Bulking Agent(s) used: 1 0 * If more space than given is required, please attach additional information sheet(s). El Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality. RI Yes [3 No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, "ding the possibility of fines and imprisonment for knowing violations." Signature of Permittee 1 Date S' a re of Preparer** Date (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(0 DENR FORM DMSDF (11/2005) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Dunbar Foods Corp/ Total Dry Tons Applied (Annual): 177.5737 WQ0012662 Cation Exchange Capacity *(non 503 only): 7.9 Carl Hite Owner: R. Dewayne Weeks 45 Acres Permitted 73 Site #: 2 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Total Phos- pwrUSMENEENEENEENE. Annual Heavy Metal Field Loadings (Calculated in lbs/acre): o �0�00000000000 t � 0000000000� i � . "___ �000000000000 � � 0000�000000 t � . �0�00�0000000� . 00�0000000� . �000�0000000�0 Total Phos- phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the,possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL PLEASE MAKE A COPY OF THIS BLANK PLACE A " Facility Name: Dunbar Foods Corp. Owner: Site #: 2 R. Dewayne Weeks Field #: AND APPLICATION FIELD SUMMARY FORM ORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. /A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Permit #: WQ0012662 Annual Dry Tons Applied: 175.67793 - Ior: Carl Hite Cation Exchange Capacity (non 503): 7.9 3 Acres Utilized: 45 Acres Permitted: 73 o A S eci Totals Per Acre % Solid s Dry Tons Per Acre { Residual Sources ! (Summarize) ite Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate* * Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 * Gal. Cu.Yd. Report inoGal. Crop 1 Crop 2 10/2/14 279000 6200 15.1 3.903954 sweet potatoes wet No INC 1 0.4 11000 150 93 35.7836 ####### Wheat 1 0 0 0 0 2 0 0 j 0 0 3 0 0 i 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 1 8 0 0 -0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 6200 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 11 PAN 2 Lime Applied Annuallbs/acre 0 0.02604 .0 0.1026 .0.02604 0 0 0.1026 0 0.26044 7.33971 35.7836 0 Date lbs/ac Current Cumulative lbs/ac 0 0.15174 0 0.72658 0.14574 0 . 0 0.43438 0 1.4134 0 0.1257 ,.0 0.62398 0.1197 0 0 0.33178 0 1.15296 NA 9 NA 250 1000 NA NA 250 NA 500 160 200 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document wais prepared under my direction or supervision in accoraance witn a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, nncluding the possibility of fines and imprisonment for knowing violations." C-,,4 tA�%� / *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and WLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach.this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Dunbar Foods Corp/ Total Dry Tons Applied (Annual): Permit #: Operator: Acres Used: 93.506 WQ0012662 Cation Exchange Capacity (non 503 only): 7.6 Carl Hite Owner: R. Dewayne Weeks 25 Acres Permitted: 121 Site #: 3 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Total Phos- phorusMEEEEEEEEEEE Annual Heavy Field Loadings (C Metal alculated in Ibs/acre): �1 �000000000000� 1 1 � 0�0�00000�0 1 1 ' WIN �00000000�0000 IMM 1 1 1 1 1 1 1 1 1 1 1 1 Joe 1 1 000©�000000 1 1 ' �00000000�0000 MeMM �000000000�0001 Total h. • •: 1 1 1 1 1 1 1 1 1 1 1 •• •: . • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM f PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "PT/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Dunbar Foods Corp. Permit #: WQ0012662 Annual Dry Tons Applied: 93.505995 - Owner: Carl Hite Operator: R. Dewayne Weeks Cation Exchange Capacity (non 503): 7.6 Site #: 3 Field #: 1 Acres Utilized: 25 Acres Permitted: 121 �. ° ° A Specify Totals Per Acre % Solid s Dry Tons Per Acre j Residual I Sources (Summarize) Site Cond. Dry, Wet, Inches Precip. Past 24 His. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- . zation Rate TKN Ammo nia- Ni- trogen Ni- . trate and Nitrite PAN 1 PAN 2 Must Select Crop C p 1 or Crop 2 * Gal. Cu Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 10/2/14 148500 5940 15.1 3.7402398 sweet potagoes wet No INC 1 0.4 11000 150 93 34.283 '####### wheat 1 0 0 0 0 2 0 0 j 0 0 3 0 0 0 0 4 0 0 ! 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 5940 As Cd ;Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0 0.02604 10 0.1026 0.026041 0 0 0.1026 0 0.26044 7.33971 34.283 0 Date I lbs/ac Current Cumulative lbs/ac 0 0.03014 0 0.2084 0.02651 0 0 0.13333 0 0.46422 0 0.0041 ; 0 0.1058 0.00047 0 0 0.030731 0 0.20378 N/A 4.5 1J/A 125 500 N/A N/A 125 N/A 250 160 200 Prior Years Cumulative lbs/ac Permitted C. P. L. R. * * * Permit PAN Limit 1st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant pena ies for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation ignature of Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) OESC 1 Mr. Thomas Ammons EHC, Inc. PO Box 902,_ Red Springs, NC 28377 Report Summary Thursday Odtober 02, 2014 Report Number: L719491 Samples Received: 09/03/14 Client Project: 14-MI0109-3 Description: Dunbar Foods 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 75B-5858 1-800-761-5859 Cax (615) 158-5859 Tax I.D. 62-OB14289 Est. 1970 The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: JimW Hunt ESC Representative LaboratoryCertification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BI0041, ND - R-140, NJ - TN0021, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV- 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI.- 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed par guidance provided in laboratory standard operating procedures: 060302, 060303,.and 060304. Page 1 of 7 12065 Lebanon Rd, Mt. Juliet, TN 37122 OESC (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 L,A B S•C•I•E• 4-C,E,S Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Thomas Ammons October 02,2014 EHC, Inc. Po Box 902 Red Springs, NC 28377 ESC Sample # L719491-01 Date Received September 03, 2019 Description Dunbar Foods Site ID MAXTON, NC Sample ID RESIDUALS Project 14-MI0109-3 # : Collected By Grady Dobson Collection Date 09/02/14 11:30 Parameter Dry Result Det. Limit Units Method Date Dil Nitrate -Nitrite 93. 13. mg/kg 9056 09/09/14 1 Phosphate as P 930 13. mg/kg 9056 09/10/14 2 Ammonia Nitrogen 150 33. mg/kg 35D.1 09/09/14 1 pH 4.8 su 9045D 09/08/14 1 Kjeldahl Nitrogen, TKN 11000 660 mg/kg 4500N0rg C- 09/11/14 5 Total Solids 15.1 % 2540 G-2011 09/06/14 1 Mercury BDL 0.13 mg/kg 7471 10/02/14 1 Aluminum 170 66. mg/kg 6010C 09/10/14 1 Arsenic BDL 13. mg/kg 6010C 09/10/14 1 Cadmium BDL 3.3 mg/kg 6010C 09/10/14 1 Copper B6L 13. mg/kg 6010C 09/10/14 1 Lead BDL 3.3 mg/kg 6010C 09/10/14 1 Molybdenum BDL 3.3 mg/kg 6010C 09/10/14 1 Nickel BDL 13. mg/kg 6010C 09/10/14 1 Potassium 19000 660 mg/kg 6010C 09/10/14 1 Selenium BDL 13. mg/kg 6010C 09/10/14 1 Zinc BDL 33. mg/kg 6010C 09/10/14 1 Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted Reported: 10/02/14 11:19 Printed: 10/02/14 13:05 L719491-01 (,PH) - 4.8@19.6c Page 2 of 7 12065 Lebanon Rd. Mt. Juliet, TN 37122. OESC (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 L'A•B S-C•I•M-N-C,M.S Tax I.D. 62-0914289 EHC• Inc. Est. 1970 Mr. Thomas Ammons PO Box 902 Quality Assurance Report Level II Red Springs, NC 28377 October 02, 2014 L719491 Laboratory Blank Analyte Result Units % Rec Limit Batch Date Analyzed Total Solids < .1 q WG741073 09/06/14 07:59 Ammonia Nitrogen < 5 mg/kg WG741115 09/09/14 12:10 Nitrate -Nitrite < 2 mg/kg WG741665 09/09/14 12:51 Phosphate as P < 1 mg/kg WG741665 09/09/14 12:51 Aluminum < 10 mg/kg WG741596 09/10/14 15:52 Arsenic Cadmium < 2 mg/kg WG741596 09/10/14 15:52 Copper < .5 mg/kg WG741596 09/10/14 15:52 Lead < 2 mg/kg WG741596 09/10/19 15:52 < .5 mg/kg WG741596 09/10/14 15:52 Molybdenum < .5 mg/kg WG741596 09/10/14 15:52 Nickel < 2 mg/kg WG741596 09/10/14 15:52 Potassium < 100 mg/kg WG741596 09/10/14 15:52 Selenium < 2 mg/kg WG741596 09/10/19 15:52 Zinc < 5 mg/kg WG741596 09/10/14 15:52 Kjeldahl Nitrogen, TKN < 20 mg/kg WG742192 09/11/14 12:25 Mercury < .02 mg/kg WG745944 10/02/14 09:07 Duplicate Analyte Units Result Duplicate RPD Limit Ref Samp Batch Total Solids % 83.4 83.3 0.0644 5 L719466-01 WG741073 PH su 5.10 5.10 0.196 1 L719308-01 WG741380 PH su 6.30 6.30 0.637 1 L719643-01 WG741300 Ammonia Nitrogen mg/kg 0.0 0.0 0.0 20 L718997-32 WG741115 Ammonia Nitrogen mg/kg 0.0 0.0 0.0 20 L718997-21 WG741115 Nitrate -Nitrite mg/kg 16.0 15.6 5.00 20 L720412-01 WG741665 Phosphate as P mg/kg 420. 413. 3.00 20 L720412-01 WG741665 Kjeldahl Nitrogen, TKN mg/kg 990. 1200 19.2 20 L720150-01 WG742192 --- ---- a oratory Control Sample--------"-"--""-"- Analyte Units Known Val Result $ Rec Limit Batch Total Solids % 50 50.0 100. 85-115 WG741073 PH su 6.33 6.30 99.5 98.3-101.7 WG741380 Ammonia Nitrogen mg/kg 768 655. 85.3 70-130 WG741115 ° Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 3 of 7 OESC EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L7194 91 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5B58 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 October 02, 2014 Laboratory Control Sample Analyte Units Known Val Result % Rec Limit Batch Nitrate -Nitrite mg/kg 40 40.7 102, 80-120 WG741665 Phosphate as P mg/kg 20 20.7 104. 80-120 WG741665 Aluminum mg/kg 10100 11700 115. 50.6-150 WG741596 Arsenic mg/kg 237 234. 99.0 83.1-117 WG741596 Cadmium mg/kg 191 181. 95.0 83.2-117 WG741596 Copper mg/kg 123 116. 95.0 83.7-116 WG741596 Lead mg/kg 103 102. 99.0 83.1-117 WG741596 Molybdenum mg/kg 91.1 90.7 100. 81.4-119 WG741596 Nickel mg/kg 118 110. 93.0 82-118 WG741596 Potassium mg/kg 2870 3100 108. 67.9-132 WG741596 Selenium mg/kg 110 ill. 101. 78.7-122 WG741596 Zinc mg/kg 183 178. 97.0 82-118 WG741596 Kjeldahl Nitrogen, TKN mg/kg 983 1170 119. 50-150 WG742192 Mercury mg/kg 12.4 13.0 109 71 6-128 WG745944 Laboratory Control Sample Duplicate Analyte Units Result Ref $Rec Limit RPD Limit Batch PH su 6.31 6.30 100. 98.3-101.7 0.159 20 WG74138O Ammonia Nitrogen- mg/kg 665. 655. 86.0 70-130 1.52 20 WG741115 Nitrate -Nitrite mg/kg 41.3 40.7 103. 80-120 2.00 20 WG741665 Phosphate as P mg/kg 20.0 20.7 104. 80-120 0.0 20 WG741665 Aluminum mg/kg 11700 11700 116. 50.6-150 0.0 20 WG741596 Arsenic mg/kg 237. 234. 100. 83.1-117 1.00 20 WG741596 Cadmium mg/kg 108. 181, 98.0 83.2-117 4.00 20 WG741596 Copper mg/kg 120. 116. 98.0 83.7-116 3.00 20 WG741596 Lead mg/kg 102. 102. 99.0 83.1-117 1.00 20 WG741596 Molybdenum mg/kg 95.1 90.7 104. 81.4-119 5.00 20 WG741596 Nickel mg/kg 113. 110. 95.0 82-118 3.00 20 WG741596 Potassium mg/kg 3100 3100 108. 67.9-132 0.0 20 WG741596 Selenium mg/kg 111. ill. 101. 78.7-122 0.0 20 WG741596 --Zinc-------- ------------mg/kg-182--------ha.-------99.0-----------82-119 -----2,-00 -- - --2C-----14G7415S6--- -- Kjeldahl Nitrogen, TKN mg/kg 1110, 1170 113. 50-150 5.26 20 WG742192 Mercury mg/kg 14.6 13.0 117 71 6-120 12.0 20 WG745944 Matrix Spike Analyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch Ammonia Nitrogen mg/kg 438. 0.0 500 88.0 80-120 L718997-26 WG741115 Phosphate as P mg/kg 121. 66.2 50 110. 80-120 L720086-01 WG741665 i Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 4 of 7 OESC I EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L719491 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Eat. 1970 October 02, 2014 Matrix Spike Analyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch Arsenic mg/kg 92.3 0,866 100 91.0 75-125 1,720345=02 WG741596 Cadmium mg/kg 95.9 0.0688 100 96.0 75-125 L720345-02 WG741596 Copper mg/kg 110. 12.0 100 98.0 75-125 L720345-02 WG741596 Lead mg/kg 110. 7.61 100 100. 75-125 L720345-02 WG741596 Nickel mg/kg 95.0 1.44 100 94.0 75-125 L720345-02 WG741596 Kjeldahl Nitrogen, TKN mg/kg 800. 480. 400 80.0* 90-110 L720086-01 WG142192 Mercury mg/kg 0.448 -0.00851 5 90.0 80-120 L724402-01 WG745944 Matrix Spike Duplicate Anal to Units MSD Ref %Rec' Limit RPD Limit Ref Samp Batch Ammonia Nitrogen mg/kg 426. 438. 85.2 80-120 2.76 20 L718997-26 WG741115 Phosphate as P mg/kg 120. 121. 107. 80-120 1.00 20 L720086-01 WG741665 Arsenic mg/kg 100. 92.3 99.2 75-125 8.00 20 L720345-02 WG741596 Cadmium mg/kq 103. 95.9 103. 75-125 7.00 20 L720345-02 WG741596 Copper mg/kg 116. 110. 104. 75-125 5.00 20 L720345-02 WG741596 Lead mg/kg 119. 110. ill. 75-125 8.00 20 L720345-02 WG741596 Nickel mg/kg 101. 95.0 99.8 75-125 6.00 20 020345-02 WG741596 Kjeldahl Nitrogen, TKN mg/kq 764. 800. 71.0* 90-110 4.60 20 L720086-01 WG742192 Mercury mg/kg 0.462 0.448 94.2 80-120 3.00 20 L724402-01 WG745944 _�- Post Spike Serial Di Batch number /Run number / Sample number Cross reference WG741073: R29859BB: 019491-01 --------*---Performance-o' this-Ara-l-yte-is-outside-of-estabYished-criteria.--'-- '--' - - -�- --- ' -- -- -' For additional information,' please see Attachment A 'List of Analytes with QC Qualifiers.' Page 5 of 7 OESC I EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 26377 WG741380: R2986694: L719491-01 WG741115: R2987131: L719491-01 WG741665: R2987290: L719491-01 WG741596: R2987848: L719491-01 WG742192: R2988199: L719491-01 WG745944: R2994558: L719491-01 Quality Assurance Report Level II L719491 * ` Calculations are performed prior to rounding of reported values. " Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 6 of 7 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 October 02, 2014 OESC I EMNMNe�� EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax {615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Quality Assurance Report Level II October 02, 2014 L719491 The data package includes a summary of the analytic results of the quality control samples required by the SW-646 or CWA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is effected is flagged with the appropriate qualifier in Appendix S of the analytic report. Method Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytes above the reporting limit in the method blank are qualified with the "B" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control". If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "J4" qualifier for all effected samples, Matrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spiked with known concentrations of target analytes. The percent recovery of the target analytes also has statistical control limits. If any recoveries that are outside the method control limits, the sample that was selected for matrix spike/matrix spike duplicate analysis is flagged with either a "J5" or a "J61'. The relative percent difference (%RPB) between the matrix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the affected samples are flagged with a "J3" qualifier. Page 7 of 7 Hlins Inksrmation: Analysis; Ce'ntaimet/ Preservative Zft; a'ut custO P.rr _:.:.'__: ii �EHC' Inc. r . A, � S . ,_ .:. ;__ . Reed Springs, NC Z9377 .., g :3riss eGmr " ,' :°< tAounC1JIPr,` ii j i " Report to: Email a l hdpm r rlt I R arse TO: Mr. Thomas Ammons — pj re: As Pri'rr:&GC7d. Fax;KE i,' .P"t•;Yb `? i PraJ_ct �Iti/StatB Des_riptiterr. Dunbar FOOdS Coltected: r O f fE r. h L#!' t ;. _ r Glent ProjeLt tt tab Prejert fF Fhanr3:910-$43-4456 �tj-@yll{i�tl9b ER9VWD-32-Mt0702_3 H: o Cs` 1= Fax: 910-843-5376In Z L _ Collected by ,printj: SltejFacility CD 4 NC P.O. P /f iViAiLT4Gil, [ a ,' TemFalatecY""'`S erQlLc$ins. P�v <ii�iSa. • CaN Cte[iy (s; tug C Rush? 42ib MUST Bt! 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Gxkm1krid y Sample ID 'v'.a-nplGIab MaVix Depot Pate Time rtrs _ _fz. :Q, RESIDUALS U., S5 5 � X X X X , e - gking�ter OT-+Dtk;er tv1atrat: 35-SviJ GW-'GrO.tn'(tWi-ter WW-JUasteWater DW-Dri _ i I _ Remarks: PH 1X6Mp Flaat'___,•_____ i7ther k906�;tt ' 1 `aeIIM(IpISt� c¢jby; Slgna.t oate: Time: Received by: (Signature) Samples returned vla: 0 UPS condlilo): ".' -jk6 use- ' `' FedE t Courier FLI i _ Relin§uis ed by: bi -' = :: ' _ Data; Time: Rereiaeti by; iSlgna"C►r�i :Tens °C Boni t?wed: Relnyvish'edby=(Slpxirsr�)'` Date- Tines: tv;{ (l56 gnaturej tlat�- I `Tr. ` COO se�llnm=' pF�'C4ttked: N.r'. __. _ NCDA&CS Agronomic Division Phone: (919) 7334655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SLO16165 Client: Moody Dunbar, Inc. Advisor: ..''` Predictive Dunbar Foods Corp. P.O. Box 519 °a Soil Report Mehlich-3 Extraction Dunn, NC 28335 Sampled County: Harnett Sampled: 11/11/2014 Received: 11/13%2014 I Completed: 12/09/2014 Farm: Links to Helpful Information Sample ID: 23 Recommendations: Lirne Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, grain . 0.0 120 - 160 0 0 .0 0 0 0 0 0 Note: 3 2-Small Grain (SG) p.0 80-100 0 0 0 0 0 0 0 0 Note: 3 Test Results [units =WIV in gicd; CEC and Na in meq/100 i 0; NO3-N in mg/drrf]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P.-1 j K-I ' Ca% - Mg% S-1 Mn-I Mn-AI1 Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.02 1.21 7.9 86 1.1 6�1 128 1 159 68 9 46 143 102 95 335 335 170 0.1 1 Sample ID: 31 Recommendations: Lirne Nutrients (lb/acre) More Crop (tons�/acre) N P205 K20 Mg S- Mn Zn . Cu B Information Lime History: 1- Corn, -grain 0.0 120 -160 0 0 0 0 0 0 0 0 Note: 3 2- Small Grain (SG) 0.0 80-100 0 0 0 0 0 0 0 0 Note: 3 Test Results [units - W/V in g/crtf; CEC and Na in meq/100 inn; NO3-N in mg/drrr'i]: Soil Class: Mineral HM% WIV CEC. BS% Ac pH P-1 K-1 Ca% Mg% S4 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.14 1.21 7.6 83 1.3 6.0 101 136. 64 10 57. 84 67 60 142 142 102 0.1 1 North Carolina �R Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture .NC D A&C - S Agronomic. Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomic Report No. FY15-SLO16165 Moody Dunbar, Inc. Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity T If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas; are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples 1 Mn-AI1 Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 j Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z Mn-I manganese index notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not M-0 N mineral -organic soil class nitrogen need to be concerned about micronutrients. Various crops notes also address lime fertilizer needs; visit Na sodium nc8gr.gov/agronomiipubs.htm. i NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncacgr.govlaaronorniloboart4.htrn#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowners Guide to Fertilizer P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS°�o, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cud, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I zinc index routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.govlar�onoinilirvrst.htm for more information.