WQ0010583_Residual Annual Report 2014_20150216

�61 &-b 10- 51U
Davie County Water System
2014 Annual Report
Residuals Land Application
Permit No. WQ0010583
Prepared,By:
EMA Resources, Inc.
Phone 336*751 * 1441 —Fax [phone] * 1442
755 Yadkinville Rd — Mocksville, NC 27028

esources, Inc.
February 12, 2015
DENR/Water Quality Section
Non -Discharge Compliance Unit R3 E.GEIER
1617 Mail Service Center
Raleigh, NC 27699-1617 FEB 1 201
OR vE�(I;i01N
Re: 2014 Annual Report — Davie County
Treatment and Land Application of Residuals
Permit No. W0010583
Dear Sir or Madam:
Enclosed are three copies of the 2014 Annual Report for the above referenced land
application permit.
During 2014 EMA Resources, Inc. land applied 102.52 dry tons of wastewater residuals
to 29 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
SincereI
a
Brent Collins
Director of Technical Services
brent.collinskemaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27029

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0010583 County: Davie Year: 2014
Facility Name (as shown on permit):
Land Application Operator:
Davie County Water System
EMA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
4 Yes D No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
7
Total number of fields utilized for land application during the year:
1
Total amount of dry tons applied during the year for all application sites:
102.52
Total number of acres utilizes for land application during the year:
29
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
- 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
i 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in.15A NCAC 02T .1105(a) or the Pollutant
r Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
' 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality,
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
'Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
F, possibility of fines and imprisonment for knowing violations."
l
Mike Ruffin - County Manager
Perinitte-e Name and � Title (type �orr//print) Signature of Permittee Date '44-y,',�'v , �� �!� S l/8/2014
Signature of Preparer* , Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) . DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010583 Laboratory: 1) A&L Eastern Laboratories, Inc.
Facility Name: Davie County Water Systems 2)
Residual Source WQ # or NCO024872 3)
NPDES #: 4)
WWTP Name: Cooleemee WWTP 5)
DmiAI A—owaia 11n*o
Parameter
(mg/kg)
Conc.
Limit
m k a
Sample or Composite Date
4/24/14
Percent Solids (%)
NA
3.47
Arsenic
75
6
Cadmium
85
2
Copper
4,300
452
Chromium
NA
58
Lead
840
52
Mercury
57
3.2
Molybdenum
75
5
Nickel
420
32
Selenium
100
6
Zinc
7,500
1580
Total Phosphorus
NA
16800
TKN
NA
38600
Ammonia -Nitrogen
NA
5480
Nitrate and Nitrite
1
66.3
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals lumts.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
------ _
L�— 16A�
Signature o Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010583
Facility Name: Davie County Water Systems
Residual Source NC0024872
NPDES # or WQ#:
WWTP Name: Cooleemee WWTP
Residual Analvsis Data
Laboratory: 1) A&L Eastern Laboratories, Inc.
2)
3)
4)
5)
Parameter
Sample or Composite Date
MMMMMMMMMM�
:11
-----------
Potassium
1
-----------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davie County Water System WQ Permit #: WQ0010583 Field #: 4 Acres Utilized: -
Land Owner: Hoyt Pope Annual Dry Tons Applied: 102.52 Site #: RA08 Acres Permitted: -
Operator: Hoyt Pope Predominant Soil Series: EnB Cation Exchange Capacity (non 503): -
Crop 1 Name: Soybeans Crop 1 Max. PAN: 148 Crop 2 Name: Crop 2 Max. PAN:
29
29
&-
+�
Q .
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, 'WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
Wei
Moist)
Precip.
Past 24
ems•
inches
Y
4 'Cl
cc '5
0
a o
o
w
--
CD
*
P
w P
C w
*
0
TKN
mg/kg
Z >
o El
as o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop 1
Crop 2
5/2/14
52000
3.47
0.259
NCO024872
Dry
<.5"
S
0.5
0.3
38600
5480
66.3
6.612
NA
Beans
5/3/14
j
149500
3.47
0.746
NCO024872
Dry
<.5"
S
0.5
0.3
38600
5480
66.3
:-19.010
===NA ---
Beans
5/4/14
149500
3.47
0.746
NCO024872
Dry
<.5"
S
0.5
0.3
38600
5480
66.3
19.010
NA
Beans
515/14
201500
3.47
1.005
NCO024872
Dry
<.5"
S
0.5
0.3
38600
5480
66.3
.25.622
NA
Beans
5/6/14
156000
3.47
0.778
NCO024872
Dry
<.5"
S
0.5
0.3
38600
5480
66.3
19..837
NA
Beans
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000-
0.000
0.006
0.000
0.000
Residuals Applications totals
on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
0
708500
::::::::::::::
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
-90.092
0.000
Lime Applied
Annuallbs/acre
0.042
0.014
3.196
0.410
0.368
0.023
0.035
0.226
0.042
11,171
118.776::::::::::::::::::::::::::::
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.042
0.014
3.196
0.410
0.368
0,023
0.035
0.226
0.042
11.171
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1 374
1 89
1 2498
2 Crop
'nd i PAN Limit 1st/ Permit P
14 8
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/6/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davie County Water System Total Dry Tons Applied (Annual): 102.52
Permit #: WQ0010583 Cation Exchange Capacity (non 503 only):
Operator: Hoyt Pope Owner: Hoyt Pope Predominant Soil Series: EnB
Acres Used: 29 Acres Permitted: 29 Site #: RA08 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Com-
posite
Date
4/24/14
% Solids
3.47
Arsenic
6
Cadmium
2
Copper
452
c hromium
58
Lead
52
Mercury
3.2
Molyb-
denum
5
Nickel
32
Selenium
6
Zinc
1580
Total
16800
IPhos-
nhnnic
knnual
Heavy Metal Field Loadings
(Calculated in lbs/acre):
ITotal
DT/Ac./
App.
Event
1
3.54
2
3
4
5
6
7
8
9
10
11
12
0
a
Arsenic
0.042.
0.000 ;
- ,0,000
. 0,000 :
F O.00Q
O,Oy00
, Q,, 00:0 ,
:. 0,,000; ,
..O,.O.OA ,
:,.-0,000,
0.000..
0.000:;
,,. 0.042
�admmm
: 0 0:14`
0 000
L
0:000
`; 0 000%,
, 0:00'0`„
,0�.000
,
., 0 OQO ���
0' 00,0
�0;000
`0 000
Copper
3''19`6'
:,-.0:OA0
0;000.
0 000''
' O OQ0
0000
0 OUO ;<
0 000
O DOU
;,:0 000.
r-
Molyb-
�"bJ000
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

M
Page: 1 of 2
Report Number: 14-115-0207
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 55033
Sample Id: COOLEEMEE WWTP LAGOON
L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastem.com
Project: DAVIE COUNTY
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 4/24/2014 14:00:00
Date Received: 04/25/2014 00:00
Date Reported: 04/30/2014
Total Solids
3.47
34700
100.0
JM
04/25/2014 14:30
SM-2540G
Moisture'
96.53
100.0
JM
04/25/201414:30
SM-2540G
Total Kjeldahl Nitrogen
3.86
38600
10.0
JM
04/28/2014 09:40
SM-4500-NH3C-TKN
Total Phosphorus
1.68
16800
100
KM
04/28/2014 13:09
SW 6010C
Total Potassium
0.22
2190
100
KM
04/28/2014 13:09
SW 6010C
Total Sulfur
0.70
6960
100
KM
04/28/2014 13:09
SW 6010C
Total Calcium
1.18
11800
100
KM
04/28/2014 13:09
SW 6010C
Total Magnesium
0.27
2670
100
KM
04/28/2014 13:09
SW 6010C
Total Sodium
0.23
2310
100
KM
04/28/2014 13:09
SW 6010C
Total Iron
49500
100
KM
04/28/2014 13:09
SW 6010C
Total Aluminum
37800
100
KM
04/28/2014 13:09
SW 6010C
Total Manganese
1730
5
KM
04/28/2014 13:09
SW 6010C
Total Copper
452
5
KM
04/28/2014 13:09
SW 6010C
Total Zinc
1580
5
KM
04/28/2014 13:09
SW 6010C
Ammonia Nitrogen
0.55
5480
10.0
JM
04/28/2014 09:40
SM-4500-NI3C
Organic N
3.31
33120
10.0
04/28/2014 09:40
CALCULATION
Nitrate+ N itrite-N
66.3
2.00
JM
04/28/2014 09:40
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
04/28/2014 13:09
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and Got ifidential use of ouit clients, nand may not be reproduced in whole or pat t. not may any reference be made
to the work, the results. or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization
Debbie Holt

s
Page: 2 of 2
Report Number: 14-115-0207
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 55033
Sample Id: COOLEEMEE WWTP LAGOON
�L A &L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]"6
www.aleastem.com
Project: DAVIE COUNTY
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/24/2014 14:00:00
Date Received: 04/25/2014 00:00
Date Reported: 04/30/2014
Total Chromium
58
5
KM
04/28/2014 13:09
SW 6010C
Total Nickel
32
5
KM
04/28/2014 13:09
SW 6010C
Total Lead
52
5
KM
04/28/2014 13:09
SW 6010C
Total Arsenic
6.0
3.0
KM
04/28/2014 13:09
SW 6010C
Total Mercury
3.2
0.4
KM
04/28/2014 09:00
SW-7471 B
Total Selenium
6.0
5.0
KM
04/28/2014 13:09
SW 6010C
pH (Standard Units) *
7.08
2.00
JM
04/28/2014 09:40
SW-9045D
Total Volatile Solids
53.06 530600
100.0
JM
04/25/2014 14:30
SM-2540G
Total Molybdenum
5
5
KM
04/28/2014 13:09
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results. or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization.
Debbie Holt

AILB10SOLIDS SALE TRANSIVLiTTAL I III�II011l llllllllllilltll1fllllllllllllllllllll lull llll lnl o624 o; '
A&L Eastezn Ag>l,
EMA RESOURCES INC 1'1:96•97
EIDLAa'. 7621 Whitepine Road Richmond VA 23237 Tel, 804-743-94 DA1/IE COUNTYtNC.CERTtt257
Account.*
Customer Information
Submitted lay
Charge To Copy To
EMA Resources Inc EMA .Resources Inc
755 Yadkinville Rd
755 Yadkinville Rd
Mocksville, NC 27028
Mocksville, NC 27028
rbject
V r ufv i '-�
Sample Information
Lab Number
Collection Information
Conialnerinformation
Please Check Desired Tests
3amplee ID
(Lab Use
Number
503
Nitrogen
Volatile
Only)
Type
Date
TM
of Bottles.
Type
Volume
SLI
SL2
Melais
Series
pH
CCE
Ag
Cl
Solids
Others
C
Glass
int
nl
[��
J
osieomp
—
at
Grab
Glass
— oZ
`Composite
`Plastic
—pint
—
t
--- oz
_Grab
— Composite.
_Glass
Plastic
_pint
—
t
_ Grab.
_ Glass
— Qz
pint
Composite
Plastic
t
R ' uished By: ignature)
Date
Time
Received By: 51nature)
Date
Tune:
Test -Package Details
Lf: Total Solids (Moisture) Total KjehlaW Nitrogen, Phosphorus and Potassium
L2: Bask Test SLI plus Sulfur, Calcium, Niz.onesium.Sodium, Iron, Alumimma, Manganese_ Copper And Zinc
33 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper R Zinc included in SL2)
itrogen Series: Total Kjeldahl. AmmUninm, Nitrale &: Organic Nitrogen.
CE: Calcium Carbonate Equivalent or Total neutralization. Value (For Lime Treated Sludge)
or. Remarks
a

YOUR LAB OF C1-fQICE
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
Report Summary
Friday May 02, 2014
Report Number: L695505
Samples Received: 04/25/14
Client Project:
Description: Davie Count
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Terrie Fudg ESC Vresentative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 5

REPORT OF ANALYSIS
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
Date Received April 25, 2014
Description Davie County
Sample ID COOLEEMEE WWTP LAGOON
Collected By Roy Whitaker
Collection Date 04/24/14 14:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
May 02,2014
ESC Sample # L695505-01
Site ID
Project
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time
By
Dil
Corrosivity
Non-Corrosiv
9045D
04/28/14
1516
MGM
1
Ignitability
See Footnote
Deg. F
D93/101
04/30/14
1615
DR
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
04/29/14
2005
MCG
1
Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
04/29/14
1614
DR
1
TCLP Extraction
-
1311
04/28/14
0930
LJN
1
Mercury
BDL
0.0010
mg/l
0.20
7470A
04/29/14
1230
BRJ
1
Arsenic
BDL
0.45
mg/l
5.0
6010C
04/29/14
1945
ALT
1
Barium
BDL
1.4
mg/l
100
6010C
04/29/14
1945
ALT
1
Cadmium
BDL
0.45
mg/l
1.0
6010C
04/29/14
1945
ALT
1
Chromium
BDL
0.45
mg/l
5.0
6010C
04/29/14
1945
ALT
1
Lead
BDL
0.45
mg/l
5.0
6010C
04/29/14
1945
ALT
1
Selenium
BDL
0.45
mg/l
1.0
6010C
04/29/14
1945
ALT
1
Silver
BDL
0.45
mg/l
5.0
6010C
04/29/14
1945
ALT
1
TCLP ZHE Extraction
-
1311
04/28/14
0930
LJN
1
TCLP Volatiles
Benzene
BDL
0.050
Carbon tetrachloride
BDL
0.050
Chlorobenzene
BDL
0.050
Chloroform
BDL
0.25
1,2-Dichloroethane
BDL
0.050
1,1-Dichloroethene
BDL
0.050
2-Butanone (MEK)
BDL
0.50
Tetrachloroethene
BDL
0.050
Trichloroethene
BDL
0.050
Vinyl chloride
BDL
0.050
Surrogate Recovery
Toluene-d8
98.2
Dibromofluoromethane
93.9
a,a,a-Trifluorotoluene
104.
4-Bromofluorobenzene
99.7
TCLP Pesticides
Chlordane
BDL
0.0050
Endrin
BDL
0.0050
Heptachlor
BDL
0.0050
L695505-01 (IGNITABILITY)
- Did Not Ignite Q 170
F
mg/1 0.50 8260B 04/29/14 1645 JC 1
mg/l 0.50 8260B 04/29/14 1645 JC 1
mg/l 100 8260B 04/29/14 1645 JC 1
mg/l 6.0 8260B 04/29/14 1645 JC 1
mg/1 0.50 8260B 04/29/14 1645 JC 1
mg/l 0.70 8260D 04/29/14 1645 JC 1
mg/l 200 8260B 04/29/14 1645 JC 1
mg/l 0.70 6260B 04/29/14 1645 JC 1
mg/l 0.50 8260B 04/29/14 1645 JC 1
mg/l 0.20 8260E 04/29/14 1645 JC 1
16 Rec. 114. 8260B 04/29/14 1645 JC 1
%- Rec. 125. 8260B 04/29/14 1645 JC 1
96 Rec. 114. 8260B 04/29/14 1645 JC 1
Rec. 128. 8260D 04/29/14 1645 JC 1
mg/l 0.030 8081A 05/02/14 1219 CBB 1
mg/1 0.020 8081A 05/02/14 1219 CBB 1
mg/l 0.0080 8081A 05/02/14 1219 CBB 1
Page 2 of 5

OESCL-A•8 5•C•I•E•N•C•E•S
REPORT OF ANALYSIS
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
Date Received April 25, 2014
Description Davie County
Sample ID COOLEEMEE WWTP LAGOON
Collected By Roy Whitaker
Collection Date 04/24/14 14:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
May 02,2014
ESC Sample # L695505-01
Site ID
Project
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time By
Dil
Lindane
BDL
0.0050
mg/1
0.40
8081A
O5/02/14
1219 CBB
1
Methoxychlor
BDL
0.0050
mg/1
10.
8081A
05/02/14
1219 CBE
1
Toxaphene
BDL
0.010
mg/l
0.50
8081A
O5/02/14
1219 CBB
1
Surrogate Recovery
Decachlorobiphenyl
116.
% Rec.
123.
8081A
O5/02/14
1219 CBB
1
Tetrachloro-m-xylene
58.5
% Rec.
114.
8081A
O5/02/14
1219 CBB
1
TCLP Herbicides
2,4,5-TP (Silvex)
BDL
0.0020
mg/1
1.0
8151A
05/01/14
1744 KLM
1
2,4-D
BDL
0.0020
mg/l
10.
8151A
05/01/14
1744 KLM
1
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
77.8
% Rec.
8151A
05/01/14
1744 KLM
1
TCLP Semi-Volatiles
1,4-Dichlorobenzene
BDL
0.10
mg/1
7.5
8270D
04/30/14
0246 KMF
1
2,4-Dinitrotoluene
BDL
0.10
mg/1
0.13
8270D
04/30/14
0246 KMF
1
Hexachlorobenzene
BDL
0.10
mg/1
0.13
8270D
04/30/14
0246 KMF
1
Hexachloro-1,3-butadiene
BDL
0.10
mg/l
0.50
8270D
04/30/14
0246 KMF
1
Hexachloroethane
BDL
0.10
mg/1
3.0
B270D
04/30/14
0246 KMF
1
Nitrobenzene
BDL
0.10
mg/1
2.0
8270D
04/30/14
0246 KMF
1
Pyridine
BDL
0.10
mg/l
5.0
6270D
04/30/14
0246 KMF
1
3&4-Methyl Phenol
BDL
0.10
mg/l
400
8270D
04/30/14
0246 KMF
1
2-Methylphenol
BDL
0.10
mg/l
200
8270D
04/30/14
0246 KMF
1
Pentachlorophenol
BDL
0.10
mg/l
100
8270D
04/30/14
0246 KMF
1
2,4,5-Trichlorophenol
BDL
0.10
mg/1
400
8270D
04/30/14
0246 KMF
1
2,4,6-Trichlorophenol
BDL
0.10
mg/l
2.0
8270D
04/30/14
0246 KMF
1
Surrogate Recovery
2-Fluorophenol
51.0
% Rec.
87.0
8270D
04/30/14
0246 KMF
1
Phenol-d5
30.9
% Rec.
67.0
8270D
04/30/14
0246 KMF
1
Nitrobenzene-d5
60.8
% Rec.
120.
8270D
04/30/14
0246 KMF
1
2-Fluorobiphenyl
71.2
% Rec.
122.
8270D
04/30/14
0246 KMF
1
2,4,6-Tribromophenol
87.4
% Rec.
148.
8270D
04/30/14
0246 KMF
1
p-Terphenyl-d14
74.3
% Rec.
149.
8270D
04/30/14
0246 KMF
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation
Limit(EQL)
Limit - Maximum Contaminant Level as
established by the US
EPA
Note:
The reported analytical results relate only to
the sample
submitted.
This report shall not be reproduced,
except in
full, without the
written
approval
from ESC.
Reported: 05/02/14 15:46 Printed: 05/02/14
15:46
L695505-01 (IGNITABILITY) - Did Not
Ignite @ 170 F
Page 3 of
5

Sample
Number
L695505-01
I
Attachment A
List of Analytes with QC Qualifiers
Work
Sample
Group
Type
Analyte
WG718414
SAMP
Endrin
WG718414
SAMP
Lindane
WG718414
SAMP
Methoxychlor
Run
ID Qualifier
R2914112 J5
R2914112 J5
R2914112 JS
Page 4 of 5

Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J5 The sample matrix interfered with the ability to make any accurate
determination; spike value is high
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as IRI (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 5 of 5

Summary of Remarks For Samples Printed
05/02/14 at 15:46:49
TSR Signing Reports: 064
R5 - Desired TAT
Sample: L695505-01 Account: EMARES Received: 04/25/14 10:00 Due Date: 05/02/14 00:00 RPT Date: 05/02/14 15:46

lal
EM4 Resources
esLpies — -— � y_ _,.-f Cust—T PaMe�vr
Mr. Brent Collins � ag"
755 Yadkinville Road ig ��a f � =� ILI
255 Yadklnville Road
Mockwille, IBC 2702$ Y � ES
htlostcsville SIC 27028
irv�crr
Report t4«t6A
Entail' Ta: brent.coi6ins@entares�lureesttte.caiis " - ' ' ` `
r '��`° ^ .'sue' a` q ,.; `' k 12os5 Lebaman Rd
Mr. Brent Cnllins �� -� �
"' r+k a`d Alvuntr�ileKr73a37122
P'.ro eEt z s v� p 6onv: e15 i5i3 5NS8
i CitV State a , v Pnoriv stun'r6? 5es8 1
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- 'e.. s 4da_„� g '€^ ?' t t �„ ° ,ai MA,d zR' 'f s:r*w rr
Client p/bj[Ct # Lab Project #i �`A' x ss w r c
Phone: [phone] i x Ml:
Fax: 396.7'51-1442 kt
C+JiI ed {Prl'ntj: She/Facility fD # P.O. $s-15
'
Cdiie by{sitmatur , Date Results Needed CJ�' Rush? {cob MUST Se Notified) 5�
mw Same Da}' .............,._..,._ ..... T 7�i &— F� -t *
Next Day ............................. t ': 4
r -- En3dii? �No X Yes * .' Y r Tt §".: T``"z'�T l;• 5 s�' '?illy # f ` „' .,vi ` s^
immediate) r
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Packeci^rlin Ice tJ 1r 4 •' fihreeba ._........................ FAX? __No —yes
- Y 2596 __ ' of c
Sample ID Comp/Grab Matrix, Depth Efate Teme nzrs
RemJURUMinnni 5 Uf tJ b M
W`` L"- 4 q}h E afi1 8 {la on
,,��.�,yy qq ` 5 {� � .-"3 ka 'ry,' ' b .. y , _ . y , . r."..
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f latrix: SS - SGi! OW - Groundwater WN - wastewater DW - Drinking Water OT - Other
-
Remarks.
pH lamp
Flow tither
ttelinqui .en Date: Time: Receive,! by (Signature) Samples turned v'r.« ®41�'S�ttr1{
�r8 a I �a ° ilirxse �SIpX `' r*t
Reis Gl1IS edby {.Silk al 41 i? ° T • G' 5t 74 �% Courier
6iry ata. Time: Receive b
�r
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�
'..9 c, s^• xr ^�. t a s sr4<, t,r f,.Ft# z `%
Rei➢nyuisited r>y: {$i ilii6r(3dr '^ CQ
.. _ Date:

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Davie County Water System
WWTP Name: Cooleemee WWTP
Monitoring Period:
W.Q Permit Number: WQ0010583
PWS Number: NCO024872
From 1/1/2014 To 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative aerformed:
Class A:
Alt. A (time/temp) ® Alt B (Alk Treatment®
Alt. C (Prior TestinL®
•.
::
A1t.D (No Prior Test) ®
Process to Further Reduce Pathogenp-P
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ®
Heat Drying ®
Heat Treatment®
Thelmophilic®
Beta Ra ®
Y
Gamma Ra ®
Y
Pas teurization
Class B:
JAIt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogen:'
..............
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ® Air Drying ® Composting ® Aerobic Digestion®
Anaerobic
ar obic Digestion n 0
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
Pathogen Density
g Ty
Number o
Excee-
Frequency
Sample
Analytical
Minimum
Geo. Mean
Maximurr
Units
in Sludge
dences
of Analysis
'Type.
Tech -pique
2 x 10 to the
6th power
MPN
525
588
1050
MPN/g
0
Annualy
Grab
SM92210E
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
coliform
weight)
. ccwi [iLLI-MAIUl1 ickwu UG1 .11®l) - riease maicate aiterna-r--re performer:
Alt.l (VS reduction) ® Alt. 2 (40-day bench) El Alt. 3 (30-day bench) ® I Alt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic) ® Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) JAIL 8 (Drying - Unstable)
Alt. 9 (Injection) Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed
UkEl1'1VIUA'1'lUN STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
_® vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Tim Smith - WWTP ORC Brent Collins - Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1/6/2015
Signature of Prep er* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville NC 27028
Entered 4/28/2014
Reported: 6/4/2014
For: Davie Co Cooleemee WWTP
Sample ID Parameter Cust ID Result Units Date
Method Analyzed Analyst
140428-3.1
% Solids
Cl
3.81
%
SM254OB-1997
4/28/14
CL
140428-3.1
Fecal Collform MTF
C I
1050
MPN/g
SM9221 CE-2006
4/28/14
CL
140428-3.1
Geometric Mean
C1
588
MPN/g
dry wt. basis
4/29/14
CL
140428-3.2
% Solids
C2.
3.73
%
SM25408-1997
4/28/14
CL
140428-3.2
Fecal Coliform MTF
C2
536
MPN/g
SM92210E-2006
4/28/14
CL
140428-3.3
% Solids
C3
3.81
%
SM254OB-1997
4/28/14
CL
140428-3.3
Fecal Coliform MTF
C3
<525
MPN/g
SM92210E-2006
4/28/14
CL
140428-3.4
% Solids
C4
3.81
%
SM254OB-1997
4/28/14
CL
140428-3.4
Fecal Conform MTF
C4
<525
MPN/g
SM92210E-2006
4/28/14
CL
140428-3.5
% Solids
C5
3.63
%
SM254OB-1997
4/28/14
CL
140428-3.5
Fecal Coliform MTF
C5
<551
MPN/g
SM92210E-2006
4/28/14
CL
140428-3.6
% Solids
C6
3.79
%
SM254OB-1997
4/28/14
CL
140428-3.6
Fecal Coliform MTF
C6
<528
MPN/g
SM92210E-2006
4/28/14
CL
140428-3.7
% Solids
C7
3.72
%
SM254OB-1997
4/28/14
CL
140428-3.7
Fecal Coliform MTF
C7
<538
MPN/g
SM92210E-2006
4/28/14
CL
140428-3.8
Bench 30 Day
Cooleemee
<1
%
EPA625R-92/0
4/28/14
CL
P.O. Box 228 - Statesville, North Carolina 28687 - 704/87214697

EIVIA Resources, Inc.
755 Yadkinville Rd.
Mocksville NC 27028
Entered 4/28/2014
Reported: 6/4/2014
For: WWTP
Date
Sample ID Parameter Cust ID Result Units Method Analyzes! Analyst
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 • Statesville, North Carolina 28687 e 704/872/4697

EMA Resources, Inc
958 Hoots Rd
Roaring River, NC 28669
Entered:4/28/2014
Reported: 6/4/2014
Sample ID: 140428-3.8
Analytical Results
For: Davie Co -Coolee
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids Volatile Solids % Volatile Solids
Week 1 2.32 1.20 0.5186
Week
2
2.31
1.20
0.5187
Week
3
2.26
1.18
0.5205
Week
4
2.27
1.20
0.5292
Week
5
2.27
1.20
0.5307
Volatile Solids Reduction: 0.5186 - 0.5307 X 100 = <1
0.5186 - (0.5186 X 0.5307)
Respectfully submitted,
Dena Myers r�J
Statesville Analytical, Inc.
NC WW Cert.# 44ONC
DW Cert. #37755
P.O. Box 228 • Statesville, North Carolina 28687 ® 704/872/4697

ure c
I
STATESVILLE ANALYTICAL
122Court Street - P.O.Box 228
Address:
Statesville, NC 28687
[phone]
I
lo
4_��
Contact Person: 7? Phone #
FAX# .17
1,_.' / t
Chain of
Custody Record
PO ;�;�)Requisifioned by: (Time Date)
Z
Customer
Samplo ID4
Lab ID
Time Sampled
(Grab Only)
Date Sampled
Only)
Matrix
Parameters requested for analysis
ISIU11901
W
I VAV
(Grab
'5
C'
:7 o
17.
(7- 7
-6 '4'A
V
110 Pwr�
cwc A(
1-1-ce-I.. 1-z' J, i 7f
A
Relinquished by: ; �`( ';�_ �_ ,t _ __ Time
am; m)Date /w?
Sampled by:
Received by:vim
Time
am; T ate
D
Transported by: Me
Relinquished by: Time
am, pm Date
Holding times met:
Received by: Time
am, pm Date
Composite Sampling #1:
Compliance work:
Time begin- am, pm Date
Non-compliance -work:
Time end am, pm Date
Lab Comments:
Composite Sampling #2:
Time begin- am, pm Date
Time end am, pm Date

Qy� 1 of
Report Number: 15-026-0905
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE NC 27028
Date Received: 01/26/2015
A A &L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastem.com
Grower:
HOYT POPE Farm ID: 008
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date OfAnalvsis: 01/27/2015 Date Of Renort- 01/27/2015
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
% Rate
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
pH
Index
meq/100g
meq/100g
04
11508
6.0 H 150
17 L
164 VH
322 VH
1200
M
15 VL
6.5
0.7
9.9
NC=14
NC=84
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Chloride
Aluminum
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
AI
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
04
16 M
5.9 H
135 VH
75 VH
3.7 VH
0.4 L
0.09 VL
4.2
27.1
60.6
0.7
7.4
NC = 33
NC =147.5
NC = 844
NC = 185.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre),,ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by ?&V,.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary