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HomeMy WebLinkAboutWQ0005763_Residual Annual Report 2014_20150223TUCKASEIGEE WATER & SEWER AUTHORITY SERVING JACKSON COUNTY 1246 West Main Street Sylva, NC 28779 Phone: (828) 586-5189 • Fax: (828) 631-9089 February 0, 2015 NCDENR Division of Water Resources Water Quality Permit Section Non -Discharge Permitting Unit 1636 Mail Service Center Raleigh NC 27699-1636 Attn: Non -Discharge Compliance Unit, Enclosed are three copies of the Annual Residuals Report for the Tuckaseigee Water and Sewer Authority Residuals Stabilization facility (permit #WQ0005763) for the period of January 1, 2014 - December 31, 2014. There were two samples collected during 2014 that resulted in non-compliance with the Non - Discharge permit. Samples collected for compliance on June 9t' and 12"', 2014 exceeded 1000 mpn fecal coliform/gram/dried solid. All of the residuals associated with these sampling events were landfilled and were not distributed to the public. Subsequent sampling and analysis of the stored residuals resulted in no additional non-compliance. events. Should you have questions or comments or if I can provide you any additional information, please don't hesitate to contact me. Sincerely, Stan Bryson Wastewater Plant Operations Superintendent Tuckaseigee Water & Sewer Authority xc: Mr Dan Harbaugh Executive Director Tuckaseigee Water and Sewer Authority RECEIVEDIDEMIDWR FP. 2,i 2015 water�ua�lil permitu"I Se This institution is an equal opportunity provider and employer. 2014 Annual Residuals Stabilization Report for The Tuckaseigee Water and Sewer Authority Distribution of Class A Residuals Permit # WQ0005763 for the period of January 1, 2014-December 31, 2014 as required by 40 CFR, Part 503 Standards for the use or disposal of Sewage sludge TABLE OF CONTENTS (1) REPORTING REQUIREMENTS/PERTINENT INFORMATION (2) CERTIFICATION APPENDIX (a) 2014 distrubution and marketing summary Parts A and B (b) 2014 annual sludge production data (c) Annual Residuals sampling summary form (d) Residuals Sampling Data (e) TCLP analysis (f) Annual Pathogen and Vector Attraction Reduction Forms (g) Daily Dryer record ANNUAL SEWAGE SLUDGE REPORT OF r TUCKASEIGEE WATER AND SEWER AUTHORITY PLANT # 1-NPDES # NCO039578 (WQ0005763) for the period of January 1, 2014-December 31, 2014 as required by 40 CFR, PART 503 STANDARDS FOR THE USE OR DISPOSAL OF SEWAGE SLUDGE REPORTING REQUIREMENTS Facilities responsible for reporting annually are described in the regulations as: 1. Publicly Owned Treatment Works (POTW) with an average design influent flow rate equal to or greater than 1.0 MGD. 2. POTW s serving a population of 10,000 or more. 3. Class I (facilities with an approved pretreatment program) sludge management facilities. The Tuckaseigee Water and Sewer Authority Wastewater Treatment Plant #1 is rated as a 3.5 mgd facility. The facility also treats the sludge from two additional plants owned by the authority. Pertinent information includes: facili , name: Tuckaseigee Water & Sewer Authority Plant # 1 NPDES # NCO039578 correspondence address: 1246 West Main St Sylva NC 28779 physical address: 1871 North River Rd Sylva NC 28779 facility operator: Stan Bryson Wastewater Plant Operations Superintendent ph. 828-586-9318 CERTIFICATION REQUIREMENTS PART I -POLLUTANT CONCENTRATIONS Permitted Concentrations _ PARAMETER Avg_ MAXIMUM monthly avg ceiling Arsenic....................<1.4 mg/kg .................. 2.4 mg/kg 41 mg/kg 75 mg/kg Cadmium..................1.1 mg/kg .................... 1.5 mg/kg 39 mg/kg 85 mg/kg Copper.....................368 mg/kg ................. 405 mg/kg 1500 mg/kg 4300 mg/kg Lead ........................18.4 mg/kg ................. 21.1 mg/kg 300 mg/kg 840 mg/kg Mercury...................0.46 mg/kg ................ 0.68 mg/kg 17 mg/kg 57 mg/kg 1 Molybdenum...............4.7 mg/kg .................. 5.3 mg/kg n/a 75 mg/kg Nickel..................13.0 mg/kg ..................... 13.9 mg/kg 420 mg/kg 420 mg/kg Selenium....................4.3 mg/kg ................... 5.4 mg/kg 100 mg/kg 100 mg/kg Zinc .........................823 mg/kg .................. 938 mg/kg 2800 mg/kg 7500 mg/kg PART H - PATHOGEN REDUCTION (40 CFR 503.32) X Class A Class B PART III - VECTOR ATTRACTION (40 CFR 503.33) _ Option 1 _ Option 2 _ Option 3 _ Option 4 Option 5 _ Option 6 _ Option 7 X Option 8 PART IV - CERTIFICATION " I certify under penalty of law, that the Class A pathogen requirements in 40 CFR, Part 503. 32 have been met and the vector attraction reduction requirement in 40 CFR, Part [503. 33(b)(6)] . has been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Signed this 4th day of February_ , 2015. Stan Bryson, Wastew er Superintendent Appendix (a) 2014 Distribution and Marketing Summary Parts A and B E ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM PERMIT #: WQ0005763 FACILITY NAME: Tuckaseigee Water and Sewer Auth/TWSA Plant #1 PHONE: 828-586-9318 COUNTY: Jackson OPERATOR: Stan Bryson FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) 21 Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? 21 Yes ❑vo No If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) s) (include NPDES # if applicable) Volume (d tons) Reci ient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume tons) (dry Mended use(s) January 16.05 16.05 See Appendix A February 32.91 32.91 Part B March 20.78 20.78 Soil Plus Inc. 20 Soil amendment April 30.16 30.16 May See Appendix A 25.91 25.91 Soil Plus Inc. 47 Soil amendment June Part A. 28.08 28.08 July 8.89 8.89 August 17.65 17.65 September 13.5 13.5 October 32.92 32.92 November 23.59 23.59 December 26.82 26.82 Totals. Annual d tons 0 277.26 277.26 ..... -:::, ::.:::.:::::::::. 67 Amendments used: 1 0 Bulking Agent(s) used: 1 0 * If more space than given is required, please attach additional information sheet(s). ❑ Check box if additional sheet(s) are attached Part C: Facility was compliant during calendar year 2014 with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality. p Yes ❑ No If No, please provide a written description why the facility was not compliant. 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware t7thet there ar ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." re ar Signature of Pre Signature of Pe ee a e gn arer* * Date p (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) DENR FORM DMSDF (11/2005) Part A Residual Sources and Volume Sludge Volume Produced Month Source (dry tons January TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 16.05 0 0 16.05 February TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 32.91 0 0 32.91 March TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 20.52 0.26 0 20.78 April TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 29.85 0 0.31 30.16 May TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 22.39 1.87 1.65 25.91 June TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 21.96 5.41 0.71 28.08 Appendix A Part A Residual Sources and Volume Sludge Volume Produced Month Source (dry tons July TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) MonthlyTotal 8.23 0.66 0 8.89 August TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 15.06 0 2.59 17.65 September TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 9.92 3.58 0 13.5 October TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 30.37 2.55 0 32.92 November TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 21.60 1.99 0 23.59 December TWSA Plant # 1 (NC0039578) TWSA Plant # 2 (NC0020214) TWSA Plant # 3 (NC0063321) Monthly Total 26.56 0.26 0 26.82 Total "sludge" produced by all sources for 2014= 277.26 dry tons Total "sludge" dewatered by belt press in 2014= 277.26 dry tons Total number of dryer loads in 2014 = 210 Total "residual' produced for distribution in 2014= 291.9 DRY TONS* * assumes an avg total solids content of 95% Appendix A TWSA PLANT # 1 ANNUAL DISTRIBUTION AND MARKETING SUMMARY 2014 Part B Recipient Information Est. Volume Month Name Address (wet tons) Intended Use Januaryl Monthly Total 0 Februaryl I Monthly Total 1 0 March Soil Plus Inc. 208 Williams St 20 Commercial User Greenville NC 27858 distributes as a 252-917-4288 soil amendent Monthly Total 20 tons April 0 May Soil Plus Inc. 208 Williams St (5115) 23.5 tons Commercial User Greenville NC 27858 (5113) 23.5 tons distributes as a 252-917-4288 soil amendent Monthly Total 47 tons Junel I Monthly Total 1 0 Julyl Monthly Total 1 0 Augustj Monthly Total 0 Septemberl I Monthly Total 1 0 Z)'ctoberl Monthly Total 1 0 Novemberl I Monthly Total 1 0 Decemberl Monthly Total 1 0 Annual Total 67 tons (est.) TWSA 0006 NON -HAZARDOUS MANIFEST Generator Generator's Mailing Address: Generator's Site Address (If different than mailing): Emergency Contact in case of Accidental Spill Tuckaseigee Water and Sewer Auth. TWSA Plant # 1 Stan Bryson, WWTP Supt. 1246 West Main St. 1871 North River Rd. M-F 7:00am-5:00 pm ph: 828-508-1072 SYLVA, NC 28779 SYLVA, NC 28779 After Hours-TWSA bnCall ph: 828-586-5189 ph: 828-586-9318 828-506-0681 Residuals Info These residuals are not Hazardous Waste as defined by 40CFR Part 261 or any applicable state law. information and instructions in case of accidental spill are on the back of this document. Date: Estimated Load Size, tons: Transporter Transporter's Mailing Address Transporter's Driver Info Emergency Contact Name: �� "`^" L�"'�F"'/�� Address:" �j L---w `ice Driver Name: I I �� V}y in case of Accident or Spill: name ph# � (fie —c ' �✓ L 21 City: l Llupq' , ` S Driver Phone #: �%b ` Truck ID u ' cog or name: State,, Zipri _Nc, i2-1 ( !- PH: ph#: Destination Info r Residuals to be Delivered To: Emergency Contact q� p Physical Address: — ` �' '� `� V </ in case of Accent or Spill name: 6c, NMA.-, LQ2_ ph#: n2`,7r�? -9)7 �o't8t�i or City: Contact: name: ph#: State Zip PH: Generators Certificate I hereby certify that the above -described materials are not hazardous wastes as definedby 40 CFR Part 261 or any applicable state law, have been fully and accurately described, classified and packaged and are in proper condition for transportation according to applicable regulations. Tuckaseigee Water and Sewer signs " On behalf of�Z Month / Day / Yr Authorityct_��% Transpor r Acknowledge ot Receipt of Materials Printed Name Signature Month / Day / Yr Certificate of Receipt and Final Disposal/Application By signature and agreeing to accept the bulk class A residuals it is recognized that the application of Class A residuals is allowed under the conditions of the utilization agreement. The application of these Class A residuals is considered the beneficial reuse of a waste under 15A NCAC.1103(4) provided the conditions of this agreement are met. Any action resulting in the damages to surface waters or groundwater caused by failure to follow the conditions of the utilization agreement is subject to enforcement action by the NC Division of Water Quality Printed Name Signature Month / Day / Yr Spill Response Plan In the event of a spill, the following actions shall be taken immediately. (1) Management of spill clean-up activities The transporter should take immediate charge and initiate clean-up activities. If there is danger to motorists, the general public or employees the first call should be to 911 so emergency services and traffic control can be routed to the site as soon as possible. If additional labor and equipment is required, assistance may be requested from the NC DOT or other private contractors as necessary. (2) Halt the source of the spill Such as a rupture or container or damaged transport unit. (3) Contain the spill Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The transporter or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime and other items necessary to complete the clean-up operation, i.e. local farmers, farm supply centers, nurseries, etc. (4) Clean-up Employ front-end loaders, vacuum equipment, sludge application vehicles and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw -and -sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. (5) Final Clean-up Employ rotary brush sweeper if needed, and apply lime to the spill area. Clean up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the area to its original condition if possible. (6) Notification As soon as possible after the spill occurs, the transporter will notify the TWSA Wastewater ; Operations Staff at (828-586-9318) or if after hours the TWSA ON -Call employee at (828-506-0681). The operator or on- call employee will notify the WWTP Superintendent. (7) Reporting The TWSA Superintendent or their designee will notify the Asheville Regional Office of the NCDENR by telephone (828-296-4500) as soon as possible, but not more than 24 hours after the occurrence. If after hours, weekends or holiday the State Emergency Operations phone number (828-858-0368) shall be used for notification. The transporter shall provide a written report within 48 hours of the spill to the TWSA WWTP Superintendent detailing the information and actions taken related to the spill. TWSA personnel will file a written report to the Asheville Regional office of the NCDENR within five days of the spill occurrence. TWSA 0007 NON -HAZARDOUS MANIFEST Generator Generator's Mailing Address: Generator's Site Address (If different than mailing): Emergency Contact in case of Accidental Spill Tuckaseigee Water and Sewer Auth. TWSA Plant # 1 Stan Bryson, WWTP Supt. 1246 West Main St. 1871 North River Rd. M-F 7:00am-5:00 pm ph: 828-508-1072 SYLVA, NC 28779 SYLVA, NC 28779 After Hours-TWSA OnCall ph: 828-586-5189 ph: 828-586-9318 828-506-0681 Residuals Info These residuals are not Hazardous Waste as defined by 40CFR Part 261 or any applicable state law. Information and instructions in case of accidental spill are on the back of this document. (� Date: 6y 1 ch 'Estimated Load Size, tons: (�Ci��' I DOV`.�j Transporter Transporter's Mailing Address Transporter's Driver Info Emergency Contact II y_ Name: v 1q / �h Address: City: C_ Dr�� ive N e: m^ �. �h� ,� 9 1�i � Driver Phone #: �' "ib�� ^ ®l —1 Truck ID in case of Accident or Spill �"_� A �P•` �1 /� _ name: ph#: or name: RA," 1 1t 5 )A1 _ ph#: A 4e State, Zip INC_ ap 7 1r� PH: s Destination In o Residuals to be Delivered To: Emergency Contact /�yy �y �(� Pro in case of Acc nt or Spill Physical Address: I 1 —1 s pe-ei— 4 j City: �� 0.�P���(1� I P _ Contact:, t e, L �S L'j eV- IIAJ /n►��JJ�/^1 State- r Zip ��!9(��i _ PH: � 0 name: 6611.1 �_% 5 ph#: .s��caZ - `t I "1 ^ 14B►8' 9- or . name: 5cn- k ccrF�n 1�- ph#: Generators Certificate I hereby certify that the above -described materials are not hazardous wastes as definedby 40 CFR Part 261 or any applicable state law, have been fully and accurately described, classified and packaged and are in proper condition for transportation according to applicable regulations. Tuckaseigee Water and Sewer Signature "On bE I 0f.. Month / Day / Yr Authority Transporter Acknowledge ot Receipt ot Materia Pri ted Namei Signature Month / Day / Yr CertWit—eof Reqeipt and Fin a Dis,posa. App ication By signature and agreeing to accept the bulk class A residuals it is recognized that the application of Class A residuals is allowed under the conditions of the utilization agreement. The application of these Class A residuals is considered the beneficial reuse of a waste under 15A NCAC.1103(4) provided the conditions of this agreement are met. Any action resulting in the damages to surface waters or groundwater caused by failure to follow the conditions of the utilization agreement is subject to enforcement action by the NC Division of Water Quality Printed Name Signature Month / Day / Yr Spill Response Plan In the event of a spill, the following actions shall be taken immediately. (1) Management of spill clean-up activities The transporter should take immediate charge and initiate clean-up activities. If there is danger to motorists, the general public or employees the first call should be to 911 so emergency services and traffic control can be routed to the site as soon as possible. If additional labor and equipment is required, assistance may be requested from the NC DOT or other private contractors as necessary. (2) Halt the source of the spill Such as a rupture or container or damaged transport unit. (3) Contain the spill Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The transporter or the person in charge on the spill site will advise the clean-up personnel where to get the straw, lime and other items necessary to complete the clean-up operation, i.e. local farmers, farm supply centers , nurseries, etc. (4) Clean-up Employ front-end loaders, vacuum equipment, sludge application vehicles and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw -and -sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. (5) Final Clean-up Employ rotary brush sweeper if needed, and apply lime to the spill area. Clean up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the area to its original condition if possible. (6) Notification As soon as possible after the spill occurs, the transporter will notify the TWSA Wastewater Operations Staff at (828-586-9318) or if after hours the TWSA ON -Call employee at (828-506-0681). The operator or on- call employee will notify the WWTP Superintendent. (7) Reporting The TWSA Superintendent or their designee will notify the Asheville Regional Office of the NCDENR by telephone (828-296-4500) as soon as possible, but not more than 24 hours after the occurrence. If after hours, weekends or holiday the State Emergency Operations phone number (828-858-0368) shall be used for notification. The transporter shall provide a written report within 48 hours of the spill to the TWSA WWTP Superintendent detailing the information and actions taken related to the spill. TWSA personnel will file a written report to the Asheville Regional office of the NCDENR within five days of the spill occurrence. TWSA 0005 NON -HAZARDOUS MANIFEST Generator Generator's Mailing Address: Generator's Site Address (If different than mailing): Emergency Contact in case of Accidental Spill Tuckaseigee Water and Sewer Auth. TWSA Plant # 1 Stan Bryson, WWTP Supt. 1246 West Main St. 1871 North River Rd. M-F 7:00am-5:00 pm ph: 828-508-1072 SYLVA, NC 28779 SYLVA, NC 28779 After Hours-TWSA OnCall ph: 828-586-5189 ph: 828-586-9318 828-506-0681 Residuals Info These residuals are not Hazardous Waste as defined by 40CFR Part 261 or any applicable state law. Information and instructions in case of accidental spill are on the back of this document. Date: 113 / 7 Estimated Load Size, tons: o lop. Transporter Transporter's Mailing Address Transporter's Driver Info Emergency Contact -1 _ Name: 4<111564 L �9 Y', Driver Name:name: '11; in cas of Ac iden or Spil 't (/1� Address:44 LlrVl ph#: or City: (r Driver Phone #: ����1� D1�i C� G. State, Zip W _ name: PH: as - q I !q " 15-1 Truck ID ph#: Destination Info Residuals to be Delivered To: Emergency Contact T fi�®- in case of Acc' nt or S III Physical Address: f name: �$ ph#: or gdl� 1%i cj lP� I c City:__ / Contact: `� 141 �j ®r� p name: ph#: State Zip PH:_ '/to�— 91 "8 3,30 Generators Certificate I hereby certify that the above -described materials are not hazardous wastes as definedby 40 CFR•Part 261 or any applicable state law, have been fully and accurately described, classified and packaged and are in proper condition for transportation according to applicable regulations. Tuckaseigee Water and Sewer Signatur "J& behalf of Month / Day / Yr Authority Transpor er Ac now e e of Receipt of Materials Printed Name Signature Month / Day / Yr �n'4C CerVricate of R ceipt and Final Disposal/Application By signature and agreeing to ccept the bulk class A residuals it is recognized that the application of Class A residuals is allowed under the conditions of the utilization agreement. The application of these Class A residuals is considered the beneficial reuse of a waste under 15A NCAC.1103(4) provided the conditions of this agreement are met. Any action resulting in the damages to surface waters or groundwater caused by failure to follow the conditions of the utilization agreement is subject to enforcement action by the NC Division of Water Quality Printed Name Signature Month / Day / Yr Spill Response Plan In the event of a spill, the following actions shall be taken immediately. (1) Management of spill clean-up activities The transporter should take immediate charge and initiate clean-up activities. If there is danger to motorists, the general public or employees the first call should be to 911 so emergency services and traffic control can be routed to the site as soon as possible. If additional labor and equipment is required, assistance may be requested from the NC DOT or other private contractors as necessary. (2) Halt the source of the spill Such as a rupture or container or damaged transport unit. (3) Contain the spill Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The transporter or the person J in charge on the spill site will advise the clean-up personnel where to get the straw, lime and other items necessary to complete the clean-up operation, i.e. local farmers, farm supply centers , nurseries, etc. (4) Clean-up Employ front-end loaders, vacuum equipment, sludge application vehicles and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw -and -sand -soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. (5) Final Clean-up Employ rotary, brush sweeper if needed, and apply lime to the spill area. Clean up will be completed to the satisfaction of the property owner and state regulatory representatives. The ultimate goal will be to restore the area to its original condition if possible. (6) Notification As soon as possible after the spill occurs, the transporter will notify the TWSA Wastewater Operations Staff at (828-586-9318) or if after hours the TWSA ON -Call employee at (828-506-0681). The operator or on- call employee will notify the WWTP Superintendent. (7) Reporting The TWSA Superintendent or their designee will notify the Asheville Regional Office of the NCDENR by telephone (828-296-4500) as soon as possible, but not more than 24 hours after the occurrence. If after hours, weekends or holiday the State Emergency Operations phone number (828-858-0368) shall be used for notification. The transporter shall provide a written report within 48 hours of the spill to the TWSA WWTP Superintendent detailing the information and actions taken related to,the spill. TWSA personnel will file a written report to the Asheville Regional office of the NCDENR within five days of the spill occurrence. Appendix (b) 2014 Annual S ludg e Production Data • 0 APPENDIX B 2014 SLUDGE PRODUCTION DATA TWSA PLANT # 1 (3.5 mgd plant capacity) NPDES # NCO039578 Sludge dewatered on belt press.................................................................2,735,346 gallons total tons...............................................277.26 tons total metric tons............................................251.5 dry metric tons The following residuals were included in the above totals. TWSA PLANT # 2 (0.5 mgd plant capacity) NPDES # NCO020214 Sludge Hauled to Plant # 1 digestor............................................................. 121,200 gallons total tons...................................................................... 16.58 tons total metric tons...............................................................15.04 dry metric tons TWSA PLANT # 3 (0.2 mgd plant capacity) NPDES # NCO063321 Sludge Hauled to Plant # 1 digestor............................................................. 52,404 gallons total tons............................................................................... 5.26 dry tons totalmetric tons.................................................................4.77 dry metric tons A portion of the sludge that was generated at the Tuckaseigee Water and Sewer Authority during 2014 was hauled by a private contractor to a designated landfill in Georgia. Landfill: Rand B Landfill 610 Frank Bennett Rd. Homer, GA 30080 A total of 231.19 tons were hauled to the landfill during 2014. Copies of haul tickets can be provided if needed. Appendix (c) 2014 Annual Residuals Sampling Summary t 2014 Annual Residual Sampling Summary Form Permit Number: WQ 0005763 Facility Name: Tuckasei4ee Water and Sewer Auth. NPDES f# NC 0039578 WQ # : WQ 0005763 WWTP Name: TWSA Plant # 1 Sample Date 2/18 5/6 6/9 6/12 6/30 6/30 7/10 8/5 11/4 Avg. Percent Solids 96 96.4 97 96 96.5 97 95.3 96.7 97.8 96.5 Aluminum 20, 00 ,400 2 500 26100 22,625 P Arsenic <11.0 < 1.0 < 0.89 2.4 < 1.4 A Cadmium 5 0. 1.11 R Calcium UN- 8, 80 963 3 8,485 A Chromium 25. 21.0 2 .4 9. 21.7 M Copper 350 32 392 405 368 E Lead 17.9 15.7 18.9 21.1 18.4 T magnesium 3,05 3,450 300 2 0 3,145 E Mercury 0. 4 5 .68 0.62 0.461 R Molybdenum 5.3 3.4 4.8 5.2 4.7 S Nickel 11.6 3. 3.0 .9 13.0 h, s.u. .4 5.8 5.5 5. Potassium 4,5 0 5,670 39 3200 4,333 Selenium 3.7 .6 5.4 3.3 4.3 Sodium 594 7 59 487 586 Zinc 938 652 83 7 823 TKN 9, 00 15,900 28100 43300 36,775 mg/ Ammonia -Nitrogen 82 9 0 650 220 1,422 kg Nitrate -Nitrite < 2 < 2 4.9 < 2 4.9 Plant Available N 17,40 5, 70 8760 3 00 11,133 Total Phosphorous 21,600 20,0 00 6 20 15,457 Corrosivity 5.8 5.4 6.0 6.1 5.1 5.4 Ignitability > 140 F > 140 F > 140 F > 140 F > 140 of SAR sodium adsorption ratio 1.4 1.1 1.3 1.2 1.3 ppm Reactivity, cyanide < 0.50 < 0.50 < 0.125 < 0.005 < 0.50 < 0.50 < 0.50 m Reactivity, sulfide < 25 < 25 < .251 < 0.0251 < 25 < 25 < 25 mpn/g I Fecal Coliform 1 1.9 2.3 1 22310* 1 4320* 1.9 1 < 175 1 1.9 1.9 1.8 21 I certify, under -penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submittipq false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer 2/4/2015 " All of the residuals that produced fecal coliform values above 1000 mph/gm/solids were landfilled and were not distributed to the public. Appendix (d) 2014 Residuals Sampling Data • aceAnalytical i wYnvpacelabs.com March 07; 2014 Mr. Stan Bryson Tuckaseigee Water & Sewer Co. 1246 West Main Street Sylva, NC 28779 RE: Project: TWSA Dried Residual 2/18 Pace Project No.: 92189911- Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 26804 (828)254-7176 Dear Mr. Bryson: Enclosed are the analytical results for sample(s) received by the laboratory on February 18, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses Were performed at the Pace Analytical Services location indicated on the sam ple analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, d-U, o,clt,_P Tabitha M Dacal tabitha.dacal@ pacelabs.com Project Manager Enclosures /'=p �C$F _�� :: f REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 19 -aceAnalytical twrw.pacelabs.com i ANALYTICAL RESULTS Project: TWSA Dried Residual 2/18 Pace Project No.: 92189911 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: TWSA Dried Residual Lab ID: 92189911001 Collected: 02/18/14 09:00 Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Received: 02/18/14 12:31 Matrix: Solid Prepared Analyzed CAS No. Qua] 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 20100 mg/kg 102 10 02/20/14 14:20 02/2111413:04 7429-90-5 Arsenic ND mg/kg 1.0 1 02/20/14 14:20 02/21/14 03:34 7440-38-2 Cadmium 1.5 mg/kg 0.10 1 02/20/14 14:20 02/21/14 03:34 7440-43-9 Calcium 8000 mg/kg 102 10 02/20/14 14:20 02/21/1413:04 7440-70-2 Chromium 25.2 mg/kg 0.51 1 02/20/14 14:20 02/21/14 03:34 7440-47-3 Copper 350 mg/kg 0.51 1 02/20/14 14:20 02/21/14 03:34 7440-50-8 Lead 17.9 mg/kg 0.51 1 02/20/14 14:20 02/21/14 03:34 7439-92-1 Magnesium 3050 mg/kg 10.2 1 02/20/14 14:20 02/21/14 03:34 7439-95-4 Molybdenum 5.3 mg/kg 0.51 1 02/20/14 14:20 02/21/14 03:34 7439-98-7 Nickel 11.6 mg/kg 0.51 1 02/20/14 14:20 02/21/14 03:34 7440-02-0 Potassium 4560 mg/kg 511 1 02/20/14 14:20 02/21/14 03:34 7440-09-7 Selenium 3.7 mg/kg 1.0 1 02/20/14 14:20 02/21/14 03:34 7782-49-2 Sodium 594 mg/kg 511 1 02/20/14 14:20 02/21/14 03:34 7440-23-5 Zinc 938 mg/kg 1.0 1 02/20/14 14:20 02/21114 03:34 7440-66-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.54 mg/kg 0.087 20 02/18/14 17:40 02/18/14 20:52 7439-97-8 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.0 % 0.10 1 02/26/14 16:41 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 1 02/19/14 12:51 1g 254OG Total Percent Solids Analytical Method: SM 2540G - Total Solids 96.0 % 0.000010 1 02/26/14 11:25 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 5.4 Std. Units 0.10 1 02/20/14 13:35 Plant Available Nitrogen Analytical Method: 40CFR PART 432.2 Plant Available Nitrogen 17400 mg/kg 1.0 1 02/25/14 11:23 N2 Total Nitrogen Calculation Analytical Method: 40CFR PART 432.2 Nitrogen 57400 mg/kg 40.0 1 02/25/1411:26 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Nitrogen, Ammonia 826 mg/kg 10.4 1 02/21/14 15:50 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 59800 mg/kg 3720 100 02/21/14 12:37 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 2.0 1 02/18/14 23:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/07/2014 09:52 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 19 ��.ceAnalytical www.pacelabs.com i _i ANALYTICAL RESULTS Project: TWSA Dried Residual 2/18 Pace Project No.: 92189911 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: TWSA Dried Residual Lab ID: 92189911001 Collected: 02/18/14 09:00 Received: 02/18/14 12:31 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA353.2 Nitrogen, Nitrite ND mg/kg 1.0 1 02/18/14 23:30 Nitrogen, NO2 plus NO3 ND mg/kg 2.0 1 02/18/14 23:30 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phos h p orus 21600 mg/kg 965 250 03/04/1411:55 7723-14-0 M6 Date: 03/07/2014 09:52 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 19 2"I ^, ram - ?, �'?� �} u, 04,E - u.0.�s � xfi e: } �-;•2�tlti�3l�fat«t`-.h:Ta?�. "i:€:;'�#tit.'�LG�>=`a.'. ui:i, February 26, 2014 Tabitha Dacal Pace Analytical Services Inc 9800 Kincey Avenue Suite 100 Huntersville, NC 28078 TEL: (704) 875-9092 FAX: (704) 875-9091 RE: TWSA Dried Residual 2/18 Dear Tabitha Dacal: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 61%bsite: http://www.setfelc.com Order No.: 14021363 Summit Environmental Technologies, Inc. received 1 sainple(s) on 2/19/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS- L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Pagel of7 Page 1 of 9 Summit Environmental 01 Technologies, Inc, WO#: 14021363 3310 Win St. Cuyahoga Falls, Ohio 44223 Date Reported: 2/26/2014 TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Pace Analytical Services Inc Website: http://www.settek.com Address: 9 800 Kincey Avenue Suite 100 HuntersvilleNC 28078 Received: 2/19/2014 Project#: TWSA Dried Re Client ID# Lab 1D# Collected Analyte Result Units Matrix Method DF RL Run Analyst 92189911002 001 2/18/2014 Flashpoint (140T) >140 T Solid EPA 1010 1 212412014 TJR 92189911002 001 2/18/2014 Cyanide, Reactive ND ppm Solid EPA 9014 1 0.50 2/20/2014 TIR 92189911002 001 2/18/2014 pH 5.8 s.u. Solid EPA 9045 D 1 2/19/2014 AYS 92189911002 001 2/18/2014 Sulfide, Reactive ND ppm Solid EPA 9034 1 25 2120/2014 TIR SAR Calculations- 2/18/2014 SAR = Sodium (Na) Milli Equivalent 0.5 X (Calcium (Ca) Milli Equivalent+ Magnesium(Mg) Milli Equivalent)o.5 Na= 594 mg/kg- Na Milli Equivalent(ME)= 594/23 equivalent wgt=25.8ME Ca= 8000 mg/kg- Ca Milli Equivalent(ME)= 8000/20 equivalent wgt= 400 ME Mg= 3050 mg/kg- Mg Milli Equivalent(ME)= 3050/12 equivalent wgt= 254 ME SAR= 25.8 Na Milli Equivalent 0.5 X , (400 Ca Milli Equivalent + 254 Mg Milli Equivalent)0.5 25.8 Na Milli Equivalent (0.5X654)0.5 = 25.8 Na Milli Equivalent (327)0.5 = 25.8 Na Milli Equivalent 18.1 SAR= 1.4. aceAnalXical www.pacelabs.com June 03, 2014 Mr. Stan Bryson Tuckaseigee Water & Sewer Co. 1246 West Main Street Sylva, NC 28779 RE: Project: Dried Residual 5/6 'Pace Project No.: 92200099 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Dear Mr. Bryson: Enclosed are the analytical results for sample(s) received by the laboratory between May 06, 2014 and May 20, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen Christopher.derouen@pacelabs.com Project Manager Enclosures 4eO REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pagel of 30 17aceAnalytical www.pacelabs.com r ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual 5/6 Pace Project No.: 92200099 Sample: TWSA BIO RESIDUAL Lab ID: 92200099001 Collected: 05/06/14 00:00 Received: 05/06/14 14:35 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS Nc 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum Arsenic 21400 mg/kg 203 20 05/07/14 16:15 05/09/1413:03 7429-90-5 Cadmium ND mg/kg 1.0 1 05/07/14 16:15 05/08/14 17:07 7440-38-2 Calcium 0.74 mg/kg 0.10 1 05/07/14 16:15 05/08/14 17:07 7440-43-9 Chromium 8380 mg/kg 10.2 1 05/07/14 16:15 05/08/14 17:07 7440-70-2 Copper 21.0 mg/kg 0.51 1 05/07/14 16:15 05/08/14 17:07 7440-47-3 Lead 325 mg/kg 0.51 1 05/07/14 16:15 05/08/14 17:07 7440-50-8 Magnesium 15.7 mg/kg 0.51 1 05/07/14 16:15 05/08/14 17:07 7439-92-1 Molybdenum 3450 mg/kg 10.2 1 05/07/14 16:15 05/08/14 17:07 7439-95-4 Nickel 3.4 mg/kg 0.51 1 05/07/14 16:15 05/08/14 17:07 7439-98-7 Potassium 13.3 mg/kg 0.51 1 05/07/14 16:15 05/08/14 17:07 7440-02-0 Selenium 5670 mg/kg 508 1 05/07/14 16:15 05/08/14 17:07 7440-09-7 Sodium 4.6 mg/kg 1.0 1 05/07/14 16:15 05/08/14 17:07 7782-49-2 Zinc 671 mg/kg 508 1 05/07/14 16:15 05/0811417:07 7440-a3-5 652 mg/kg 1.0 1 05/07/14 16:15 05/08/14 17:07 7440-66-6 7471 Mercury Analytical Method: EPA7471 Preparation Method: EPA7471 Mercury 0.0057 mg/kg 0.0022 1 05/07/14 17:30 05/07/14 19:41 7439-97-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.6 % 0.10 1 05/14/14 15:20 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.3 MPN/g 0.019 1 05/08/14 10:22 254OG Total Percent Solids Analytical Method: SM 2540G Total Solids 96.4 % 0.000010 1 05/14/14 10:30 9045 pH Soil Analytical Method: EPA9045 pH at 25 Degrees C 5.8 Std. Units 0.10 1 05/08/14 17:24 Plant Available Nitrogen Analytical Method: 40CFR PART432.2 Plant Available Nitrogen 5170 mg/kg 1.0 1 05/27/14 16:47 Total Nitrogen Calculation Analytical Method: 40CFR PART 432.2 Nitrogen 15900 mg/kg 40.0 1 05/27/14 16:43 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Nitrogen, Ammonia 1990 mg/kg 50.9 5 05/07/14 14:00 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 15900 mg/kg 926 50 05/27/14 10:58 7727-37-9 353.2 Nitrogen, N021NO3 Analytical Method: EPA353.2 Nitrogen, Nitrate i ND mg/kg 2.1 1 05/21/14 18:16 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06l03/2014 09:47 AM without the written consent of Pace Analytical Services, Inc.. Qua[ 1g,H3 N2 Page 4 of 30 -_ aceAnalytical f www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual 516 Pace Project No.: 92200099 Sample: TWSA BID RESIDUAL Lab ID: 92200099001 Collected: 05/06/14 00:00 Received: 05/06/14 14:35 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA353.2 Nitrogen, Nitrite ND mg/kg 1.0 1 05/21/14 18:16 Nitrogen, NO2 plus NO3 ND mg/kg 2.1 1 05/21/14 18:16 365.1 Phosphorus, Total Analytical Method: EPA365.1 Phosphorus 20000 mg/kg 471 100 05/2311416:34 7723-14-0 M6,R1 Sample: TWSA DRIED SLUDGE Lab ID: 92200099003 Collected: 05/20/14 10:00 Received: 05/20/14 12:51 Matrix: Solid FECAL Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.4 % 0.10 1 05/22/14 16:19 92210E Fecal Coliform, MPN RAIL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 2.3 MPN/g 0.019 1 05/21/14 11:16 254OG Total Percent Solids Analytical Method: SM 254OG Total Solids 95.6 % 0.000010 1 05/22/14 09:11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2014 09:47 AM without the written consent of Pace Analytical Services, Inc.. Qual 1g,H1 Page 5 of 30 Summit Environmental Technologies, Inc. su, f"Puma , ,' "_ a 1 3310 Win St. Cuyahoga Falls, Ohio 44223 i.4t`' "1'F::�a'<n `; TEL: (330) 253-8211 FAX (330) 253-4489 Website: hgp.,11www.set1ekcom May 20, 2014 Chris Derouen . Pace Analytical Services Inc 9800 Kincey Avenue Suite 100 Huntersville, NC 28078 TEL: (704) 875-9092 FAX: (704) 875-9091 RE: Dried Residual 516 Dear Chris Derouen: Order No.: 14050810 Summit Environmental Technologies, Inc. received 1 sample(s) on 5/8/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-D735, California 07256CA, Colorado, Connecticut PH 0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-011-13, Kansas E-1D347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS- L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C andE87688, Wisconsin399013010 Page 1 of 7 Page 20 of 30 °. � Summit Environmental Technologies, Inc. tf 3310WinSt. Case Narrative r.. , c'It'idtal§1�il. gt. rity[,, ;d« Cuyahoga Falls, Ohio 44223 C TEL: (330) 253-8211 FAX.- (330) 253=4489 WO#: 14050810 Website: htW.-11www.settek com Date: 5/20/2014 CLIENT: Pace Analytical Services Inc Project: Dried Residual 516 This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical.Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied .with this sample set. . Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as estimated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request Any comments or problems with the analytical events associated with this report are noted below. Original Page 3 of 7 Page3of9 ge 22 of 30 . ' a eg r Summit Environmental Technologies, Inc. r' * 3310 Win St. Cuyahoga Falls, Ohio 44223 ; _ • 'tt` " 'l`t�R k'=^' TEL: (330) 253-8211 FAX.•'(330) 253-4489 Website: http.-Ilwww.setiek.com WO#: 14050810 Date Reported: 5/20/2014 Company: Pace Analytical Services Inc Address: 9800 Kincey Avenue Suite 100 Huntersville NC 28078 Received: 5/8/2014 Project#: Dried Residual 5 Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst 92200099002 001 .5/6/2014 Flashpoint (140°F) >140 °F Solid EPA 1010 1 5/9/2014 TAH 92200099D02 001 5/6/2014 Cyanide, Reactive ND mg/Kg Solid EPA 9014 1 0.50 5/9/2014 TIR 92200099002 001 5/6/2014 pH 5.4 s.u. Solid EPA 9045 D 1 5/9/2014 AYS 92200099002 001, 5/6/2014 Sulfide, Reactive ND mg/Kg Solid EPA 9034 1 25 5/9/2014 . TIR P g 23 of 3 '-AR Calculations- 5/6/2014 SAR = Sodium (Na) Milli Equivalent 0.5 X (Calcium (Ca) Milli Equivalent+ Magnesium(Mg) Milli Equivalent)o.5 Na= 671 mg/kg- Na Milli Equivalent(ME)= 671/23 equivalent wgt=29.2ME Ca= 8380 mg/kg- Ca Milli Equivalent(ME)= 8380/20 equivalent wgt= 419 ME Mg= 3450 mg/kg- Mg Milli Equivalent(ME)= 3450/12 equivalent wgt= 287.5 ME SAR= 29.2 Na Milli Equivalent 0.5 X (419 Ca Milli Equivalent + 287.5 Mg Milli Equivalent)0.5 29.2 Na Milli Equivalent (0.5X706.5)0.5 29.2 Na Milli Equivalent (706.5)0.5 = 29.2 Na Milli Equivalent 26.6 SAR= 1.1 y�:��< x' 4� Environmental Testir g solutions, Inc. Certificate of Analysis Project name: Tuckaseime Water & Sewer Collection date: 12-Jun-14 Date received: 12-Jun-14 Sample identification: Dried Residual - Grnh Parameter Method Percent Solids SM 2540 G Mulitple Tube Fermentation Procedure SM 9221-E Reactive Cyanide 335.4 Reactive Sulfide SM 4500 S D Ignitability SW 846 1030 pH in Soil' 9045 C PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 140612.506 Sample number: 117072 Result - RL Units Date Analyzed Analyst Footnotes 96 % 12-Jun-14 KW 4320 173 MPN 12-Jun-14 KEK <0.005 0.005 mg/kg 264un-14 ECHEM 1 <0.251 0.251 mg/kg 26-Jun-14 ECHEM 1 <0.8 0.8 nM /sec 17-Jun-14 ECHEM 1 6.1 S.U. 12-Jun-14 KW 2 Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. 1. Sample analyzed by Rogers & Callcott Environmental. 2. Sample analzyed outside holding time. Date reviewed: N • NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 — Signature: K NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. • nvirochem / SM l ANALYTICAL.$ CONSULTING CHEMISTS Environmental Testing Solutions, Inc. Post Office Box 7565 Asheville NC 28802 Attention: Kelley Keenan (ETS) Lab ID 14-17151 Test RCI lgnitability Cyanide pH Sulfide Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) 0 (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Date of Report: Jun 26, 2014 Customer PO #: Customer ID: 08100055 Report #: 2014-06973 Project ID: TWSA Sample ID: Dried Residual Collect Daterrime Matrix Sampled by Site: 6/12/2014 9:00 AM Solid/Sludge Client Method Results Date Analvzed Comment: r _ Reviewed by. EPA 1030 EPA 335.4 SM 4500 H B SM 4500 S D <0.8 mm/sec 06/17/2014 < 0.005 mg/kg 06/26/2014 5.86 units 06/18/2014 <0.251 mg/kg 06/26/2014 Report #.: 2014-06973 Page 1 of 1 311 x Environmental Testing Solutions, Inc. Certificate of Analysis, Project name: Tuckaseigee Water & Sewer Collection date: 9-Jun-14 Date received: 9-Jun-14 PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 140609.506 Sample identification: Dried Residual - Grab Sample number: 116850 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Percent Solids SM 2540 G 97 % 9-Jun-14 KW Mulitple Tube Fermentation Procedure SM 9221-E 22310 175 MPN 10-Jun-14 KEK Reactive Cyanide 335.4 <0.125 0.125 mg/kg 26-Jun-14 ECHEM I Reactive Sulfide SM 4500 S D <0.251 0.251 mg/kg 26-Jun-14 ECHEM I Ignitability SW 846 1030 <0.8 0.8 mm/sec 13-Jun-14 ECHEM 1 pH in Soil 9045 C 6.0 S.U. 10-Jun-14 KEK 2 Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. 1. Sample analyzed by Rogers & Callcott Environmental. 2. Sample analzyed outside holding time. Date reviewed: (x •Z?.II NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 (, NC Drinking Water Certification Number: 37786 Signature: LA - This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis, Environmental Chemists, Inc. envirochem 6602 Windmill Way - Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 l3owsertown Road - Manteo, NC 27954 l — ANALYTICAL &CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37729 Environmental Testing Solutions, Inc. Date of Report: Jun 26, 2014 Post Office Box 7565 Customer PO #: Asheville NC 28802 Customer ID: 08100055 Attention: Kelley Keenan (ETS) Report #: 2014-06897 Project ID: TWSA Lab 1D Sample ID: Collect Date/Time - Matrix Sampled by 14-16920 Site: Dried Residual 6/9/2014 5:00 PM Solid/Sludge Client Test Method Results Date Analyzed RCI Ignitability EPA 1030 <0.8 mm/sec 06/13/2014 Cyanide EPA 335.4 <0.125 mg/kg 06/26/2014 Sulfide SM 4500 s D <0.251 mg/kg 06/26/2014 Comment Reviewed by: / Report#_: 2014-06897 Page 1 of 1 COD -- Environmental Testing Solutions, Inc. Certificate of Analysis Project name: Tuckaseigee Water & Sewer Collection date: 30-Jun-14 Date received: 30-Jun-14 Sample identification: Dried Residual - Grab PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 140630.504 Sample number: 117540 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Percent Solids SM 2540 G 97 % 30-Jun-14 KW Mulitple Tube Fermentation Procedure SM 9221-E <175 175 MPN 30-Jun-14 KEK Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: Q r'7 i(y NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 _ Signature: NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted for analysis. 'aceAnalXical wmpacelabs.com July 28, 2014 Mr. Stan Bryson Tuckaseigee Water & Sewer Co. 1246 West Main Street Sylva, NC 28779 RE: Project: Dried Residual Fecal 6/30 Pace Project No.: 92207373 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Dear Mr. Bryson: Enclosed are the analytical results for sample(s) received by the laboratory on June 30, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. \ j Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feeIr free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures NC eORA� I� REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 10 1 �r aceAnalXical www.pacelabs.com ANALYTICAL RESULTS Project: Dried Residual Fecal 6130 Pace Project No.: 92207373 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Sample: TWSA DRIED SLUDGE Lab ID: 92207373001 Collected: 06/30/1411:00 Received: 06/30/14 12:30 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.6 % 0.10 1 07/03/14 18:30 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 07/01/1410:40 1g 2540G Total Percent Solids Analytical Method: SM 2540G Total Solids 96.6 % 0.000010 1 07/03/1412:01 Date: 07/28/2014 10:53 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pade 4 of 10 f' www.pacalabs.com t July 21, 2014 Mr. Stan Bryson Tuckaseigee Water & Sewer Co. 1246 West Main Street Sylva, NC 28779 RE: Project: Dried Residual 7/10 Pace Project No.: 92208741 ECIEW FA2 s 2014 PacecAnalytical Services, Inc 2225 Riverside D Asheville, NC 2880• (828)254-71 7 Dear Mr. Bryson: Enclosed, are the analytical results for sample(s) received by the laboratory on July 10, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, /4-- Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 1 aceAna6d cal www.pacelabsxom ANALYTICAL RESULTS Project: Dried Residual 7/10 Pace Project No.: 92208741 Pace Analytical Services, Inc 2225 Riverside D Asheville, NC 2880• . (828)254-717 -'ample: I VIISA DRIED RESIDUAL Lab ID: 92208741001 Collected: 07/10/14 12:50 Received: 07/10/14 14:07 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed. CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 4.7 % 0.10 1 07/14/14 15:48 92210E Fecal Colifonn, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.019 1 07/11/14 10:13 1g Date: 07/21/2014 05:14 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 1 aceAnalXical www.pacelabs.com. 1 August 25, 2014 Mr., Stan Bryson Tuckaseigee Water & Sewer Co. 1246 West Main Street Sylva, NC 28779 RE: Project: Dried Residual 8/5 Pace Project No.: 92212017 0 AUG 2 9 2014 D Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Dear Mr. Bryson: Enclosed are the analytical results for sample(s) received by the laboratory on August 05, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. r Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen @ pacelabs.com -- Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, q without the written consent of Pace Analytical Services, Inc.. Page 1 of 17 ac6Analy4ical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 (_ ANALYTICAL RESULTS Project: Dried Residual 8/5 Pace Project No.: 92212017 Sample: TWSA DRIED RESIDUAL Lab ID: 92212017001 Collected: 08/05/14 12:30 Received: 08/05/14 14:09 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum Arsenic 22500 mg/kg 178 20 08/06/14 16:20 08/08/14 14:53 7429-90-5 Cadmium ND mg/kg 0.89 1 08/06/14 16:20 08/07/14 20:17 7440-38-2 Calcium 1.1 mg/kg 0.089 1 08/06/14 16:20 08/07/14 20:17 7440-43-9 Chromium 9630 mg/kg 178 20 08/06/14 16:20 08/08/14 14:53 7440-70-2 Copper 21.4 mg/kg 0.45 1 08/06/14 16:20 08/07/14 20:17 7440-47-3 Lead 392 mg/kg 0.45 1 08/06/14 16:20 08/07/14 20:17 7440-50-8 Magnesium 18.9 mg/kg 0.45 1 08/06/14 16:20 08/07/14 20:17 7439-92-1 Molybdenum 3300 mg/kg 8.9 1 08/06/14 16:20 08/07/14 20:17 7439-95-4 Nickel 4.8 mg/kg 0.45 1 08/06/14 16:20 08/07/14 20:17 7439-98-7 ' Potassium 13.0 mg/kg 0.45 1 08/06/14 16:20 08/07/14 20:17 7440-02-0 Selenium 3900 mg/kg 446 1 08/06/14 16:20 08/07/14 20:17 7440-09-7 Sodium 5.4 mg/kg 0.89 1 08/06/14 16:20 08/07/14 20:17 7782-49-2 Zinc 591 mg/kg 446 1 08/06/14 16:20 08/07/14 20:17 7440-23=5 834 mg/kg 0.89 1 08/06/14 16:20 08/07/14 20:17 7440-66-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 (: ° "srcury 0.68 mg/kg 0.10 25 06/06/14 16:20 08/07/14 12:24 7439-97-6 arcent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 3.3 % 0.10 1 08/07/14 15:11 9221 CE Fecal Coliform, MPN RAL Analytical Method: SM9221 C E (MPN) 503 Fecal Coliforms, MPN 1.9 MPN/g 0.018 1 08/06/14 10:00 1 g 2540G Total Percent Solids Analytical Method: SM 2540G Total Solids 96.7 % 0.000010 1 08/07/14 09:36 9045 pH Soil Analytical Method: EPA 9045 - pH at 25 Degrees C 5.5 Std. Units 0.10 1 . 08/06/14 11:32 Plant Available Nitrogen Analytical Method: 40CFR PART 432.2 Plant Available Nitrogen 8760 mg/kg 1.0 1 08/18/14 11:30 N2 Total Nitrogen Calculation Analytical Method: 40CFR PART 432.2 Nitrogen 28100 mg/kg 40.0 1 08/18/14 11:45 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Nitrogen, Ammonia 1650 mg/kg 51.7 5 08/07/14 17:30 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 • Nitrogen, Kjeldahl, Total 28100 mg/kg 940 50 08/13/14 15:44 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 rogen, Nitrate 4.9 mg/kg 2.1 1 08/15/14 22:34 REPORT OF LABORATORY ANALYSIS ' Date: 08/25/2014 04:17 PM This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 17 aceAnalytical ( www.pacerabs.com f� ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual 8/5 Pace Project No.: 92212017 Sample: TWSA DRIED RESIDUAL Lab ID: 92212017001 Collected: 08/05/14 12:30 Received: 08/05/14 14:09 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrite ND mg/kg 1.0 1 08/15/14 22:34 Nitrogen, NO2 plus NO3 4.9 mg/kg 2.1 1 08/15/14 22:34 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 126 mg/kg 4.2 2 08/14/14 16:38 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, ')ate: 08/25/2014 04:17 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 17 • ` �. Summit Environmelttal Technologies, Inc. y v r �A .., .._ 3310 Win St. CAI 90 Cuyahoga Falls, Ohio 44223 trtTh rya ;49i`A.S'f� TEL: (330) 253-8211 FAX.• (330) 253-4489 Website: httn•//www settek com August 11, 2014 Chris Derouen Pace Analytical Services Inc 9800 Kincey Avenue Suite 100 Huntersville, NC 28078 TEL: (704) 875-9092 FAX: (704) 875-9091 RE: 92212017 Dried Residual 8/5 Dear Chris Derouen: Order.No.: 14080458 Summit Environmental Technologies, Inc. received 1 sample(s) on 8/6/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this. report unless noted in the Case Narrative. Quality control data is within laboratory defined or method'specified acceptance limits except where noted.. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, A-Z , �' Dr. Mo Osman Project Manager 3310. Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA,, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996. New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon 0142O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDAIAPHIS P330-11-00244, Utah OH009232011-1 Virginia 248 and 9957C and E87688, Wisconsin 399013010 , Vermont VT•67688, Virginia 00440 and 1581, Washington C891, West Page 1 of 5 Page 1 of 7 ' Summit Environmental Technologies, Inc. .: 3310Win St. Workorder Cuyahoga Falls, Ohio 44223 Sample Summary TEL: (330) 2S3-8217 FAX.- (330) 2S3-4489 Website: httn_//www.settek com WO#: 140804.58 17 Aug-l4 CLIENT: Pace Analytical Services Inc Project: 92212017 Dried Residual 8/5 -Lab'SampleID Client Sample ID Tag No Date Collected 14080458-001 92212017002 Date Received Matrix 8/5/2014 12:30:00 PM 8/6/2014 9:55:00 AM' Solid Page 2 of 5 Page 2 of 7 ,• u ' , _ __, Summit Environmental Technologies, Inc. '� h �it WO#: 14080458 a%.- ", 3310 Win St. fl Cuyahoga Falls, Ohio 44223 Date Reported: 8/11/2014 TEL: (330)253-8211 FAX. 330 ( ) 253 4489 Company: Pace Analytical Services Inc Website: htto://www.settelccom Address: 9800 Kincey Avenue Suite 100 Huntersville NC 28078 Received: 8/6/2014 Project#: 92212017 Dried Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst 92212017002 001 8/5/2014 Flashpoint (140°F) >140 °F Solid EPA 1010 1 8/7/2014 TAH 92212017002 001 8/5/2014 Cyanide, Reactive ND ppm Solid EPA 9014 1 0.50 8/7/2014 TIR 92212017002 001 8/5/2014 pH 5.1 s.u. Solid EPA 9045 D 1 8/7/2014 AYS 92212017002 001 8/5/2014 Sulfide, Reactive ND pprn Solid EPA 9034 1 25 8/7/2014 TIR Pggee4 of57 i c SAR Calculations- 8 5/2014 SAR = Sodium (Na) Milli Equivalent 0.5 X (Calcium (Ca) Milli Equivalent+ Magnesium(Mg) Milli Equivalent)o.s Na= 591 mg/kg- Na Milli Equivalent(ME)= 591/23 equivalent wgt=25.7ME Ca= 9630 mg/kg- Ca Milli Equivalent(ME)= 9630/20 equivalent wgt= 481.5. ME Mg= 3300 mg/kg- Mg Milli Equivalent(ME)= 3300/12 equivalent wgt= 275 ME SAR= _ 25.71 Na Milli Equivalent 0.5 X (481.5 Ca Milli Equivalent + 275 Mg Milli Equivalent)o.s 25.71 Na Milli Equivalent (0.5X756.5)0' 25.71 Na Milli Equivalent (378.3)o.s = 25.71 Na Milli Equivalent 19.4 SAR= 1.3 N Pace Analytical services, 111a. 2225 Riverside Dr. u�/+Q /{ n / �+ r ® Asheville, NC 28804 [dlieA alXi a (828)254-7176 www.pacela6scom November 21, 2014 Mr. Stan Bryson Tuckaseigee Water & Sewer Co. 1246 West Main Street Sylva, NC 28779 RE: Project: Dried Residual 11/4 Pace Project No.: 92223951 Dear Mr. Bryson: Enclosed are the analytical results for sample(s) received by the laboratory between November 04, 2014 and November 06, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte , page for analysis unless otherwise footnoted. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYST This report shall not reproduced, except in full, eORp(fl without the written consent of Pace Analytical Services, Inc.. Page 1 of 27 ® Pace Analytical Services, Inc. aceAnalytical 2225 Riverside Dr. www.pacelabs.com . Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Project: Dried Residual 11/4 Pace Project No.: 92223951 Raleigh Certification IDS 6701 Conference Drive, Raleigh, NC 27607 North Carolina Wastewater Certification #: 67 North Carolina Bioassay Certification M 16 North Carolina Drinking Water Certification M 37731 Charlotte Certification IDS 9800 Kinsey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification M 37706 Florida/NELAP Certification'* E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Virginia/VELAP Certification M 460221 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification M E87648 North Carolina Wastewater Certification M 40 Massachusetts Certification #: M-NC030 South Carolina Certification M 99030001 West Virginia Certification M 356 North Carolina' Drinking Water Certification M 37712 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of27 I �alceAnalytical" www.pacelabs.com .ANALYTICAL RESULTS Project: Dried Residual 1114 Pace Project No.: 92223951 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 sample: TWSA DRIED RESIDUAL Lab ID: 92223961001 Collected: 11/04/14 09:30 Received: 11/04/1411:16 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3050 Aluminum 26100 mg/kg 193 20 11/05/1416:05 1110611413:02 7429-90-5 Arsenic 2.4 mg/kg 0.96 1 11/05/1416:05 11/06/14 04:27 7440-38-2 Cadmium 1.1 mg/kg 0.096 1 11/05/1416:05 11/06/14 04:27 7440-43-9 Calcium 7930 mg/kg 9.6 1 11/0511416:05 11/06/14 04:27 7440-70-2 Chromium 19.1 mg/kg 0.48 1 11/05/1416:05 11/06/14 04:27 7440-47-3 Copper 405 mg/kg 0.48 1 11/05/14 16:05 11/06/14 04:27 7440-50-8 Lead 21.1 mg/kg 0.48 1 11/05/1416:05 11/06/14 04:27 7439-92-1 Magnesium 2780 mg/kg 9.6 1 11/05/1416:05 11/06/14 04:27 7439-95-4 Molybdenum 5.2 mg/kg 0.48 1 11105/1416:05 11/06/14 04:27 7439-98-7 Nickel 13.9 mg/kg 0.48 1 11/05/1416:05 11/06/14 04:27 7440-02-0 Potassium 3200 mg/kg 482 1 11/05/1416:05 11/06/14 04:27 7440-09-7 Selenium 3.3 mg/kg 0.96 1 11105/1416:05 11/06/14 04:27 7782-49-2 Sodium 487 mg/kg 482 1 11/05/1416:05 11/06/14 04:27 7440-23-5 Zinc 867 mg/kg 0.96 1 11/05/1416:05 11/06/14 04:27 7440-66-6 7477 Mercury Analytical Method: EPA7471 Preparation Method: EPA7471 Mercury 0.62 mg/kg 0.063 20 11105/1416:00 11/06/1412:57 7439-97-6 254OG Total Percent Solids Analytical Method: SM 254OG Total Solids 97.8 % 0.000010 1 11/06/14 09:02 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.2 % 0.10 1 11/06/1413:09 9045 pH Soil Analytical Method: EPA9045 pH at25 Degrees C 5.7 Std. Units 0.10 1 11/07/14 12:35 H1 Plant Available Nitrogen Analytical Method: SM 2710B Plant Available Nitrogen 13200 mg/kg 0.12 1 11/19/1415:16 N2 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Nitrogen 43300 mg/kg 40.0 1 11/1911415:30 7727-37-9 350.1 Ammonia Analytical Method: EPA 350.1 Nitrogen, Ammonia 1220 mg/kg 50.1 5 11/12/14 03:15 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 43300 mg/kg' 4870 100 11/1811415:24 7727-37-9 M6 353.2 Nitrogen, NO2/11403 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 2.0 1 11/11/14 21:45 Nitrogen, Nitrite ND mg/kg 0.98 1 11/11/14 21:45 Nitrogen, NO2 plus NO3 ND mg/kg 2.0 1 11/11/1421:45 Date: 11/21/2014 04:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 aceAnalXical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual 11/4 Pace Project No.: 92223951 Sample: TWSA DRIED RESIDUAL Lab ID: 92223951001 Collected: 11/04/14 09:30 Received: 11/04/14 11:16 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 20100 mg/kg 818 200 11/10/14 16:07 7723-14-0 Sample: TWSA DRIED RESIDUAL Lab ID: 92223951003 Collected: 11/06/14 11:40 Received: 11/06/1414:03 Matrix: Solid FECAL Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 2.1 % 0.10 1 1112111412:57 92210E Fecal Coliform, MPN RAL Analytical Method: SM9221C E (MPN) 503 Fecal Coliforms, MPN 1.8 MPN/g 0.018 1 11/07/14 10:05 1g Date: 11/21/2014 04:07 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 27 1<; SUMM01- ;�._Suluutil Errriranrrerrral Teclrrrolagies, Grc. J 3310 nrNr sr. EHVIROW6IENTAL TECHWOLOGIESr we CrryahogaFalls, Ohio 44223 z_ti,: Arraf� final LaE�oratales TEL: (330) 253-8211 FAA, (330) 253-4489 ►Yebsile: h1(a.•11irlru,,senek.conr November 10, 2014 Chris Derouen Pace Analytical Services Inc 9800 Kincey Avenue Suite 100 Huntersville, NC 28078 TEL: (704) 875-9092 FAX: (704) 875-9091 RE: 92223951 Dried Residual 11/4 Dear Chris Derouen: Order No.: 14110445 Summit Environmental Technologies, Inc. received 1 sample(s) on 11/6/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the Iabor•atory. Sincerely, Allq-� �" Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88.0735, Californiaa 07256CA, Colorado, Connecticut P1r-0105, Delaware, Florida NELAC E87688, Georgia E97689 and 943. Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-01-1-13, Kansas E-10347, Kentucky (Underground Storage Tad:) 3, Kenlucky 90146, Louisiana 04061 and LA 12004, hlaine 2Ol2Ol5, N-lary4ard 339, \dassac[nuselts M-OPH923, \finnnesoia 409711, \9ontara CE•RT0099, New Hampshire 2996, Ncw Jersey 01-1006, New York 11777. North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP C1.0052, Oklahor n 9940, Oregon 0H2O0001, Pennsyhmnia 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466.11-5. Region 8 8T\rS-1, USDA/APHIS P330.11-00244, Utah OH009232011-1, Vermont VT-87688, V6ginia 00440 and 1581, Washington C891, \Vest Virginia 248 and 9957Cand E87688, Wisconsin 399013010 Page I of 4 Page 1 of 6 Page 19 of 27 E Si -mil En "Ironmental Technologies, Ine. Workorder 3310 Wn St. E S, i Nir, C19'alloga Falls, Oldo 44223 Sample Summary Analytiral 1,91, le TEL: (330) 253-8211 FAir.. (330) 2s3-4489 woll: 14110445 Website-, IM-1-11inviv.sellek.tour 10-Nop-14 CLIENT: Pace Analytical Services Inc Project:- 92223951 Dried Residual 11/4 Lab8amplell) Client Sample lD Tag No Date Collected Date Received Matrix 14110445-001 92223951002 11/4/2014 9:30:00 AM 11/6/2014 10:15:00 AM Solid Page 2 of 4 Page 2 of 6 Page 20 of 27 l y �.1 r ' 1 /g; a�, t; Summit Environmental Technologies, life. s N Case l�faY�)f�iitlVe liY[ 3310WinSt. y f hVIRONfdEfJ1'AL I'�CHPd�LOG:CS, Inc. Cu3nhogaFalls Olrio 44223 ,T �= nnelytira! G,hohafuh'les , TEL: (330) 253-8211 r r.• (330) 253-4489 WO#' 14110445 ❑�ebsite: Trap://um v.settek coo, Date: 11/10/2014 CLIENT: Pace Analytical Services Inc Project: 92223951 Dried Residual 1114 This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Covet' Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. Original Page 3 of 4 Page 3 of 6 Page 21 of 27 3y1. Sromrri(EmtrarureulnlTecJnrologies, hra ' `f�� �1r0#' 14110445 J� r eti%'IRONliE1dYA�rECHNo�Uci.cs,INC Cuyahoga rails, DtRo Date Reported: 11/10/2014 P _- Analytlral t.;3l:ai:�torles TEL: (330) 253.8211 FAX' (330) 253-4489 Company: Pace Analytical Services Inc Website.lr(tp.-lA nivettekconr Address: 9800 Kincey Avenue Suite 100 Huntersville NC 28078 Received: 11/6/2014 Project#: 92223951 Dried Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst 92223951002 001 11/4/2014 Flashpoinl (1407) >140 T Solid EPA 1010 i 11/10/2014 TAH 92223951002 001 11/4/2014 Cyanide, Reactive ND ppm Solid EPA 9014 1 0.50 11/7/2014 TIR 92223951002 001 11/4/2014 pH 5.4 sm. Solid EPA 9045 D 1 11/7/2014 AT 92223951002 001 11/4/2014 Sulfide, Reactive ND ppm Solid EPA 9034 1 25 1.11712014 TIR Pdtwc4e,6 Page 22 of 27 r-, Appendix (e) 2014 TCLP Analysis 0 7 aceMalXical www.pacelabs.com t August 25, 2014 Mr. Stan Bryson Tuckaseigee Water & Sewer Co. 1246 West Main Street Sylva, NC 28779 RE: Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 Dear Mr. Bryson: SEP 1 5 2014 D Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Enclosed are the analytical results for sample(s) received by the laboratory on August 05, 2014. The results relate only to the samples included in this report: Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Chris Derouen christopher.derouen@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 18 aceAnalytical www.pacelabs.com i Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Alabama Certification #: 41320 Arizona Certification #: AZ0735 Colorado Certification: FL NELAC Reciprocity Connecticut Certification M PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Kentucky Certification #: 90050 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate M 05007 Maryland Certification: #346 Massachusetts Certification M M-FL1264 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersvilie, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS-28-14 Nevada Certification: FL NELAC Reciprocity New Hampshire Certification #: 2958 New Jersey Certification M FL765 New York Certification M 11608 North Carolina Environmental Certificate M 667 North Carolina Certification #: 12710 Pennsylvania Certification #: 68-00547 Puerto Rico Certification #: FLO1264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 Washington Certification #: C955 West Virginia Certification #: 9962C Wisconsin Certification M 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity Florida/NELAP Certification M E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 2 of 18 El aceAnalXical 1 www.pacelabs.com Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 Lab ID Sample ID 92212018001 TWSA DRIED RESIDUAL TCLP SAMPLE ANALYTE COUNT Method EPA 8081 EPA 8151 EPA 6010 EPA 7470 EPA 8270 EPA 8260 EPA 9095 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 2225 Riverside Dr. - Asheville, NC 28804 (828)254-7176 Analytes Analysts Reported Laboratory RES 8 PASI-C LJM 3 PASI-O JMW 7 PASI-A HVK 1 PASI-A RES 18 PASI-C DLK 14 PASI-C MDW 1 PASI-A Page 3 of 18 aceAnalXical / www.pacelabs.com fr= ANALYTICAL RESULTS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 Sample: TWSA DRIED RESIDUAL Lab ID: 92212018001 Collected: 08/05/14 12:30 Received: 08/05/14 14:09 Matrix: Water TCLP Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP` gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8151 Chlorinate Herbicide TCLP 2,4-D 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP, TCLP l Arsenic Barium Cadmium Chromium Lead Selenium Silver Analytical Method: EPA8081 Preparation Method: EPA3510 Leachate Method/Date: EPA 1311; 08/06/14 13:45 ND ug/L 2.5 5 08/12/14 09:28 08/12/14 22:35 58-89-9 ND ug/L 15.0 5 08/12/14 09:28 08/12/14 22:35 57-74-9 ND ug/L 2.5 5 08/12/14 09:28 08/12/14 22:35 72-20-8 ND ug/L 2.5 5 08/12/14 09:28 08/12/14 22:35 1024-57-3 ND ug/L 5000 5 08/12/14 09:28 08/12/14 22:35 72-43-5 ND ug/L 15.0 5 08/12/14 09:28 08/12/14 22:35 8001-35-2 0 % 10-138 5 08/12/14' 09:28 08/12/14 22:35 2051-24-3 D3,S4 0 % 10-110 5 08/12/14 09:28 08/12/14 22:35 877-09-8 Analytical Method: EPA 8151 Preparation Method: EPA 3510 ND mg/L 0.010 1 ND mg/L 0.010 1 94 % 42-142 1 08/13/14 08:05 08/14/14 03:06 94-75-7 08/13/14 08:05 08/14/14 03:06 93-72-1 08/13/14 08:05 08/14/14 03:06 19719-28-9 Analytical Method: EPA6010 Preparation Method: EPA3010 Leachate Method/Date: EPA 1311; 08115/14 16:30 ND mg/L 0.050 1 08/18/14 19:05 08/19/14 04:23 7440-38-2 0.38 mg/L 0.25 1 08/18/14 19:05 08/1.9/14 04:23 7440-39-3 ND mg/L 0.0050 1 08/18/14 19:05 08/19/14 64:23 7440-43-9 ND mg/L 0.025 1 08/18/14 19:05 08/19/14 04:23 7440-47-3 ND mg/L 0.025 1 08/18/14 19:05 08/19/14 04:23 7439-92-1 ND mg/L 0.10 1 08/18/14 19:05 08/19/14 04:23 7782-49-2 ND mg/L 0.025 1 08/18/14 19:05 08/19/14 04:23 7440-22-4 ® 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 08/15/14 16:30 Mercury 0.48 ug/L 0.20 1 08/18/14 20:00 08/19/14 15:42 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 08/06/14 13:45 1,4-Dichlorobenzene ND ug/L 50.0 1 08/07/14 08:23 08/08/14 20:57 106-46-7 2,4-Dinitrotoluene Hexachloro-1,3-butadiene ND ug/L 50.0 1 08/07/14 08:23 08/08/14 20:57 121-14-2 Hexachlorobenzene ND ug/L 50.0 1 08/07/14 08:23 ND ug/L 08/08/14 20:57 87-68-3 Hexachloroethane 50.0 1 08/07/14 08:23 ND ug/L 08/08/14 20:57 118-74-1 2-Methylphenol(o-Cresol) 50.0 1 08/07/14 08:23 ND ug/L 08/08/14 20:57 67-72-1 3&4-Methylphenol(m&p Cresol) 50.0 1 08/07/14 08:23 104 ug/L 50.0 1 08/08/14 20:57 95-48-7 Nitrobenzene 08/07/14 08:23 ND ug/L 08/08/14 20:57 Pentachlorophenol 50.0 1 08/07/14 08:23 ND ug/L 100 08/08/14 20:57 98-95-3 • Pyridine 1 08/07/14 08:23 ND ug/L 08/08/14 20:57 87-86-5 2,4,5-Trichlorophenol 50.0 1 08/07/14 08:23 ND ug/L 08/08/14 20:57 110-86-1 2,4,6-Trichlorophenol 50.0 1 08/07/14 08:23 ND ug/L 08/08/14 20:57 95-95-4 50.0 1 08/07/14 08:23 08/08/14 20:57 88-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 18 aceAnalytical t www.pacelabs.com Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 Sample: TWSA DRIED RESIDUAL TCLP - Parameters 8270 MSSV TCLP Sep Funnel Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane s - 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) 9095 Paint Filter Liquid Test ® Free Liquids Date: 08/25/2014 06:44 PM Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Lab ID: 92212018001 Collected: 08/05/14 12:30 Received: 08/05/14 14:09 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 08/06/14 13:45 28 % 12-102 1 08/07/14 08:23 08/08/14 20:57 4165-60-0 28 % 13-107 1 08/07/14 08:23 08/08/14 20:57 321-60-8 36 % 21-132 1 08/07/14 08:23 08/08/14 20:57 1718-51-0 9 % 10-110 1 08/07/14 08:23 08/08/14 20:57 13127-88-3 S5 8 % 10-110 1 08/07/14 08:23 08/08/14 20:57 367-12-4 S5 21 % 27-108 1 08/07/14 08:23 08/08/14 20:57 118-79-6 S5 Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 08/14/14 11:03 ND ug/L 192 38.5 08/14/14 18:00 71-43-2 1540 ug/L 385 38.5 08/14/14 18:00 78-93-3 ND ug/L 192 38.5 08/14/14 18:00 56-23-5 ND ug/L 192 38.5 08/14/14 18:00 108-90-7 ND ug/L 192 38.5 08/14/14 18:00 67-66-3 ND ug/L 192 38.5 08/14/14 18:00 106-46-7 ND ug/L 192 38.5 08/14/14 18:00 107-06-2 ND ug/L 192 38.5 08/14/14 18:00 75-35-4 ND ug/L 192 38.5 08/14/14 18:00 127-18-4 ND ug/L 192 38.5 08/14/14 18:00 79-01-6 ND ug/L 192 38.5 08/14/14 18:00 75-01-4 139 % 70-130 38.5 117 % 67-135 38.5 101 % 70-130 38.5 Analytical Method: EPA 9095 PASS 1.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 08/14/14 18:00 17060-07-0 1 g,S5 08/14/14 18:00 2037-26-5 08/14/14 18:00 460-00-4 08/15/14 10:10 Page 5 of 18 aceAnalytical I www.pacelabs.com I _ i 0 Project: Dried Residual TCLP 8/5 P P tN^' no�,on-io ace rotec QC Batch: MERP/6979 QC Batch Method: EPA 7470 Associated Lab Samples: 92212018001 METHOD BLANK: 1266511 Associated Lab Samples: 92212018001 Parameter Units Mercury ug/L LABORATORY CONTROL SAMPLE: 1266512 Parameter Units Mercury ug/L Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: EPA 7470 Analysis Description: 7470 Mercury TCLP Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.20 08/19/1415:37 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.7 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1266513 1266514 MS MSD 92212018001 Spike Spike MS MSD MS , MSD % Rec /—_ Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L 0.48 2.5 2.5 3.4 3.1 118 105 75-125 9 _ Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. t c- REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 18 Pace Analytical Services, Inc. aceAna1Xical ® 2225 Riverside Dr. % Asheville, NC 28804 wrw+pacelabs.com (828)254-7176 t QUALITY CONTROL DATA Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 QC Batch: MPRP/16697 Analysis Method: EPA6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP Associated Lab Samples: 92212018001 METHOD BLANK: 1266495 Matrix: Water Associated Lab Samples: 92212018001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic mg/L ND 0.050 08/19/14 04:16 Barium mg/L ND 0.25 08/19/14 04:16 Cadmium mg/L ND 0.0050 08/19/14 04:16 Chromium mg/L ND 0.025 08/19/14 04:16 Lead mg/L ND 0.025 08/19/14 04:16 Selenium mg/L ND 0.10 08/19/14 04:16 Silver mg/L ND 0.025 08/19/14 04:16 LABORATORY CONTROL SAMPLE: 1266496 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Arsenic mg/L 2.5 2.7 106 80-120 Barium mg/L 2.5 2.6 106 80-120 Cadmium mg/L 2.5 2.6 102 80-120 Chromium mg/L 2.5 2.4 97 80-120 Lead mg/L 2.5 2.4 96 80-120 Selenium mg/L 2.5 2.6 106 80-120 Silver mg/L 1.2 1.3 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1266497 MS 92212018001 Spike Parameter Units Result Conc. Arsenic mg/L ND 2.5 Barium mg/L 0.38 2.5 Cadmium mg/L ND 2.5 Chromium mg/L ND 2.5 Lead mg/L ND 2.5 Selenium mg/L ND 2.5 Silver mg/L ND 1.2 1266498 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 2.5 3.0 2.9 120 115 75-125 4 2.5 3.3 3.1 116 110 75-125 4 2.5 2.9 2.8 116 112 75-125 4 2.5 2.8 2.7 112 109 75-125 3 2.5 2.7 2.6 107 105 75-125 2 2.5 3.0 2.9 120 114 75-125 5 1.2 1.4 1.4 114 110 75-125 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Qual Page 7 of 18 aceAnalytical www.pace/abs.wm f QUALITY CONTROL DATA Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual TCLP 815 Pace Project No.: 92212018 QC Batch: MSV/27953 Analysis Method: EPA 8260 QC Batch Method: EPA 8260 Analysis Description: 8260 MSV TCLP Associated Lab Samples: 92212018001 METHOD BLANK: 1264272 Matrix: Water Associated Lab Samples: 92212018001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1-Dichloroethene ug/L ND 5.0 08/14/14 15:00 1,2-Dichloroethane ug/L ND 5.0 08/14/14 15:00 1,4-Dichlorobenzene ug/L ND 5.0 08114/1415:00 2-Butanone (MEK). ug/L ND 10.0 08/14/14 15:00 Benzene ug/L ND 5.0 08114/1415:00 Carbon tetrachloride ug/L ND 5.0 08/14/14 15:00 Chlorobenzene ug/L ND 5.0 08/14/14 15:00 Chloroform ug/L ND 5.0 08/14/14 15:00 Tetrachloroethene ug/L ND 5.0 08/14/14 15:00 Trichloroethene ug/L ND 5.0 08/14/14 15:00 Vinyl chloride ug/L ND 5.0 08/14/14 15:00 1,2-Dichloroethane-d4 (S) % 98 70-130 08/14/14 15:00 4-Bromofluorobenzene (S) % 101 70-130 08/14/14 15:00 ��- Toluene-d8 (S) % 109 67-135 08/14/14 15:00 LABORATORY CONTROL SAMPLE: 1264273 Spike LCS LCS % Rec _ Parameter Units Conc. Result % Rec Limits Qualifiers 1,1-Dichloroethene ug/L 50 50.0 100 66-135 1,2-Dichloroethane ug/L 50 50.1 100 67-128 1,4-Dichlorobenzene ug/L 50 51.6 103 78-130 2-Butanone (MEK) ug/L 100 94.6 95 61-144 Benzene ug/L 50 50.0 100 80-125 Carbon tetrachloride ug/L 50 44.6 89 69-131 Chlorobenzene ug/L 50 51.6 103 81-122 Chloroform ug/L 50 53.3 107 73-127 Tetrachloroethene ug/L 50 54.1 108 78-122 Trichloroethene ug/L 50 48.6 97 78-122 Vinyl chloride ug/L 50 47.3 95 . 58-137 1,2-Dichloroethane-d4 (S) % 97 70-130 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 97 67-135 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1264274 1264275 MS MSD 92213282002 Spike Spike MS MSD MS MSD % Rec " Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,1-Dichloroethene ug/L ND 1920 1920 2440 1940 127 101 70-150 23 _ Results presented on this r page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. - REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 18 aceAnalytical www.pacelabs.com t QUALITY CONTROL DATA Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1264274 1264275 MS MSD 92213282002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,2-Dichloroethane ug/L ND 1920 1920 2670 2150 139 112 70-150 22 1,4-Dichlorobenzene ug/L ND 1920 1920 2290 1980 119 103 70-150 14 2-Butanone (MEK) ug/L ND 3850 3850 5360 3870 139 101 70-150 32 R1 Benzene ug/L ND 1920 1920 2630 2270 136 118 70-150 14 Carbon tetrachloride ug/L ND 1920 1920 2190 1810 114 94 70-150 19 Chlorobenzene ug/L ND 1920 1920 2280 2040 119 106 70-150 11 Chloroform ug/L ND 1920 1920 2780 2400 144 125 70-150 15 Tetrachloroethene ug/L ND 1920 1920 2260 1960 117 102 70-150 14 Trichloroethene ug/L ND 1920 1920 2430 2040 126 106 70-150 17 Vinyl chloride ug/L ND 1920 1920 2610 2120 136 110 70-150 21 1,2-Dichloroethane-d4 (S) % 109 95 70-130 4-Bromofluorobenzene (S) % 98 95 70-130 Toluene-d8 (S) % 103 98 67-135 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 18 E7 aceAnalytical www.pacelabs.com Project: Dried Residual TCLP 8/5 Pace Project No.: 9221.2018 QC Batch: OEXT/29356 QC Batch Method: EPA 3510 - Associated Lab Samples: 92212018001 METHOD BLANK: 1261629 Associated Lab Samples: 92212018001 Parameter Units Chlordane (Technical) ug/L Endrin ug/L gamma-BHC (Lindane) ug/L Heptachlor epoxide ug/L Methoxychlor ug/L Toxaphene ug/L Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % QUALITY CONTROL DATA Analysis Method: EPA 8081 Analysis Description: 8081 GCS TCLP Pesticides Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 3.0 08/12/14 21:25 ND 0.50 08/12/14 21:25 ND 0.50 08/12/14 21:25 ND 0.50 08/12/14 21:25 ND 1000 08/12/14 21:25 ND 3.0 08/12/14 21:25 89 10-138 08/12/14 21:25 78 10-110 08/12/14 21:25 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 LABORATORY CONTROL SAMPLE & LCSD: 1261630 1261631 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Endrin ug/L 1.2 1.1 1.0 87 85 20-134 3 30 gamma-BHC (Lindane) ug/L 1.2 1.0 1.1 83 86 20-118 4 30 Heptachlor epoxide ug/L 1.2 0.99 0.94 80 76 22-133 - 6 30 Methoxychlor ug/L 3.7 ND ND 83 87 44-150 30 Decachlorobiphenyl (S) % 92 95 10-138 Tetrachloro-m-xylene (S) % 80 78 10-110 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 18 Is acemalytical t www.pacelabs.com f Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 QC Batch:. OEXT/18481 QC Batch Method: EPA 3510 Associated Lab Samples: 92212018001 METHOD BLANK: 977943 Associated Lab Samples: 92212018001 Parameter Units 2,4,5-TP (Silvex) mg/L 2,4-D mg/L 2,4-DCAA (S) % QUALITY CONTROL DATA Analysis Method: EPA 8151 Analysis Description: 8151 GCS Herbicides TCLP Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.010 08/14/14 00:35 ND 0.010 08/14/14 00:35 83 42-142 08/14/14 00:35 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville,, NC 28804 (828)254-7176 METHOD BLANK: 978055 Matrix: Water Associated Lab Samples: 92212018001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 2,4,5-TP (Silvex) mg/L ND 0.010 08/14/14 04:07 2,4-D mg/L ND 0.010 08/14/14 04:07 2,4-DCAA (S) l -- % 84 42-142 08/14/14 04:07 LABORATORY CONTROL SAMPLE: 977944 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 2,4,5-TP (Silvex) mg/L .012 0.012 99 27-170 2,4-D mg/L .06 0.054 90 23-163 2,4-DCAA (S) % 87 42-142 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 978053 978054 MS MSD 10276067001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 2,4,5-TP (Silvex) mg/L <0.0000 .0134 .0134 0.014 0.014 105 105 27-170 .5 55 2,4-D mg/L <0.0002 .0672 .0672 0.062 0.061 92 90 23-163 2 5 2,4-DCAA (S) % 90 85 42-142 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 18 aceAnalytical % www.pacelabs.com QUALITY CONTROL DATA Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 QC Batch: OEXT/29254 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 TCLP MSSV Associated Lab Samples: 92212018001 METHOD BLANK: 1258496 Associated Lab Samples: 92212018001 Matrix: Water Parameter Units Blank Result 1,4-Dichlorobenzene ug/L ND 2,4,5-Trichlorophenol ug/L ND 2,4,6-Trichlorophenol ug/L ND 2,4-Dinitrotoluene ug/L ND 2-Methylphenol(o-Cresol) ug/L ND 3&4-Methylphenol(m&p Cresol) ug/L ND Hexachloro-1,3-butadiene ug/L NO Hexachlorobenzene ug/L ND Hexachloroethane ug/L ND Nitrobenzene ug/L ND Pentachlorophenol ug/L ND Pyridine ug/L ND 2,4,6-Tribromophenol (S) % 106 2-Fluorobiphenyl (S) % 94 2-Fluorophenol (S) % 48 Nitrobenzene-d5 (S) % 89 Phenol-d6 (S) % 33 Terphenyl-d14 (S) % 109 Reporting Limit Analyzed 50.0 08/0711414:02 50.0 08/0711414:02 50.0 08/07/1414:02 50.0 08/0711414:02 50.0 08/07/1414:02 50.0 08/07/1414:02 50.0 08/07/1414:02 50.0 08/07/1414:02 50.0 08/07/1414:02 50.0 08/07/1414:02 100 08/07/1414:02 50.0 08/07/1414:02 27-108 08/07/1414:02 13-107 08/07/1414:02 10-110 08/07/1414:02 12-102 08/07/1414:02 10-110 08/07/1414:02 21-132 08/07/1414:02 LABORATORY CONTROL SAMPLE: Parameter 1258497 Units Spike Conc. LCS Result LCS % Rec ® 1,4-Dichlorobenzene ug/L 500 365 73 2,4,5-Trichlorophenol ug/L 500 482 96 2,4,6-Trichlorophenol ug/L 500 474 95 2,4-Dinitrotoluene ug/L 500 504 101 2-Methylphenol(o-Cresol) ug/L 500 336 67 3&4-Methylphenol(m&p Cresol) ug/L 500 319 64 Hexachloro-1,3-butadiene ug/L 500 360 72 Hexachlorobenzene ug/L 500 456 91 Hexachloroethane ug/L 500 400 80 Nitrobenzene ug/L 500 455 91 Pentachlorophenol ug/L 1000 933 93 Pyridine ug/L 500 203 41 2,4,6-Tribromophenol (S) % 111 2-Fluorobiphenyl (S) % 90 2-Fluorophenol (S) % 46 Nitrobenzene-d5 (S) % 87 Phenol-d6 (S) % 33 Terphenyl-dl4 (S) % 102 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Qualifiers % Rec Limits Qualifiers 10-110 39-108 40-104 42-109 31-110 30-110 10-110 39-121 10-110 32-101 18-108 10-110 27-108 SO 13-107 10-110 12-102 10-110 21-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 08/25/2014 06:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 18 r 11�aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1258498 1258499 MS MSD 92211759001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dichlorobenzene ug/L ND 500 500 195 236 39 47 30-150 19 2,4,5-Trichlorophenol ug/L ND 500 500 242 270 48 54 30-150 11 2,4,6-Trichlorophen ol ug/L ND 500 500 225 260 45 52 30-150 14 2,4-Dinitrotoluene ug/L ND 500 500 286 310 57 62 30-150 8 2-Methylphenol(o-Cresol) ug/L ND 500 500 171 253 34 51 30-150 39 R1 3&4-Methylphenol(m&p ug/L ND 500 500 156 238 31 48 30-150 41 R1 Cresol) ' Hexachloro-1,3-butadiene ug/L ND 500 500 185 237 37 47 30-150 25 Hexachlorobenzene ug/L ND 500 500 266 256 53 51 30-150 4 Hexachloroethane ug/L ND 500 500 178 238 36 48 30-150 29 Nitrobenzene ug/L ND 500 500 228 274 46 55 30-150 18 Pentachlorophenol ug/L ND 1000 1000 547 537 55 54 30-150 2 Pyridine ug/L ND 500 500 101 130 20 26 30-150 25 MO 2,4,6-Tribromophenol (S) % 58 58 27-108 2-Fluorobiphenyl (S) % 42 52 13-107 2-Fluorophenol (S) % 23 29 10-110 Nitrobenzene-d5 (S) % 44 54 12-102 Phenol-d6 (S) % 16 23 10-110 j-- Terphenyl-d14 (S) % 62 57 21-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. t REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 18 r� u 0 aceAnalytical I www.pacelabs.com t Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 QC Batch: WET/32683 QC Batch Method: EPA 9095 Associated Lab Samples: 92212018001 SAMPLE DUPLICATE: 1264977 Parameter Free Liquids Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: EPA 9095 Analysis Description: 9095 PAINT FILTER LIQUID TEST 92212018001 Dup Units Result Result RPD Qualifiers PASS PASS Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 18 1�;a'cemalyticalo r www.pacelabs.com i QUALIFIERS Project: Dried Residual TCLP 8/5 Pace Project No.: 92212018 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contabt your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte PASI-O Pace Analytical Services - Ormond Beach ANALYTE QUALIFIERS 1g 8260 results are from a total analysis which show that analytes are not present or that they are present but at such low levels that the appropriate regulatory levels could not possibly be exceeded, per Section 1.2 of Method 1311. D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. M0 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. R1 RPD value was outside control limits. SO Surrogate recovery outside laboratory control limits. S4 Surrogate recovery not evaluated against control limits due to sample dilution. S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis). Date: 08/25/2014 06:44 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 15 of 18 aceAnalyfical r' www.pacelabs.com t Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Project: Pace Project No.: QUALITY CONTROL DATA CROSS REFERENCE TABLE Dried Residual TCLP 8/5 92212018 Analytical Lab ID' Sample ID QC Batch Method QC Batch Analytical Method Batch 92212018001 TWSA DRIED RESIDUAL TCLP EPA 3510 OEXT/29356 EPA 8081 GCSV/18531 92212018001 TWSA DRIED RESIDUAL TCLP EPA 3510 0EXT/18481 EPA 8151 GCSW12124 92212018001 TWSA DRIED RESIDUAL TCLP EPA 3010 MPRP/16697 EPA 6010 ICP/15076 92212018001 TWSA DRIED RESIDUAL TCLP EPA 7470 MERP/6979 EPA 7470 MERC/6718 92212018001 TWSA DRIED RESIDUAL TCLP EPA 3510 OEXT/29254 EPA 8270 MSSW9499 92212018001 TWSA DRIED RESIDUAL TCLP EPA 8260 MSV/27953 92212018001 TWSA DRIED RESIDUAL TCLP EPA 9095 WET/32683 f ` ( REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/25/2014 06:44 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 18 CHAIN -OF -CUSTODY / Analytical Request Document aeeAnal� ��(�cal The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. i www.pacelahs:Eom `- - �-, o Section A Section B Section C Page: of ., Required Client Information: `41 q �,.- Required Project Information: Invoice Information: - o! -d Company_ ! /LI't1 f ; ;., .yam. y ReportTo: I a..)n j ICV'1625436 Attention: •�. Address: / tw• 1 �i r (7 .-.. Copy -My, ' '1 !.1 .' tf 4 `� t •. •� . ' Company Name: REGULpcTORY=' 1 1. R �' l i - !1 , _ Address: r t %; ; F / I :I : r'� j (- NPDES )- GROUND WATERY j- DRINKING WATERI'' Email To: J Purchase Order No.: Para Ouote Phone: - Fax: Project Name: Reference: (- UST [- RCRA (- OTHER Pace Project - - ;........ Manager. Requested Due Date/TAT: - Project Number. 1 Pace Pmmle =:LEI -'R®puesfedAnal sisF-ilfered Bectlon D'- Matrix Codes RequiredClientlnfonnation MATRIX /CODE - a. i COLLECTED TED Prose rvatives :z- - -- - -- - - - Drinking Water DIN 9 O - Water WT O = _ " Waste Water WW Product P' = m COMPOSITE START COMPOSITE 'ENDIGRAB 1 W — SAMPLE ID SoiVSolid SL oil. OL 11 v 1 Wipe WP A-Z; 0.9 / : Air AR . Sample IDS MUST BE UNIQUE Tissue w O SEL a ¢ w z_ Q y: d c ^ TS Other OT U �\ ~a z H a ��� ' ;� a U 2 l H i! Q O C 1<5 N Z U O n1 a) •C + C' rn DATE TIME DATE TIME; 3t 2' 2 2 2 Z Z O y= y ` / Pace Project No./ Lab I.D. =2s a, 10. ADDITIONA' >r:REC = _ - LCO :_.:. '.,:: :_e.r;. ;.r<.,c.;: ::<<: z•,,:_:INQUISHED,:BYaAF.II ATION.: ,t>>a:; >:;b:.DATE:.-^., ::.: 1 7 ME `.. A EPTED.BYI.A 4. .cF SAMPLER,NAME'Ayq;SIG14ATURE- PRINT Name of SAMPLER: f•' SIGNATURE of SA PLER: Ii f �d•r •Im; .ote: By signing this form you are accepting Pace's NET 30 day payment terns and agreeing to late charges of 1.5 % permon lvolces not paid within 30 days. SAMPLE CONDITIONS E •a �Z � oCZ c m m �i c.i✓ E L f Co ' F-ALL-Q-020rev.07, 1F I -2007 0 Document Name: Sample Condifion Upon. Document Revised: June 10, 2014 aceAnalytical9 www.pacolab ,.00n Receipt (SCUR) Page 1 of 2. ; Document No,:' Issuing Authorities: F-ASV-CS-003-rev.14 Pace Asheville Quality Office Client Name:_ ` ,(,i,, J Courier (Circle): Fed Ex UPS USPS Commercial Pace Other Custody. Seal on Cooler/Box Present: El yes no Seals intact: yes no Packing Material: Bubble Wrap �. Bubble Bags V] NonEet Other T ermy. omer Used: IR Gun#3-130265963 Type of Ice: Blue None Samples on ice, cooling process has begun R Gun #4 SN:1402 036 Other: Temp Correc io ctor: Add /. ubtrac i C Corrected Cooler Temp.: C Tem should be above freezing to 6°C P 9 Biological Tissue -is Frozen:: Yes No /A Comments:. Date and Initia s of person examining- contents: Chain of'Custody Present: Yes ONo ❑N/A 1. Chain of Custody Filled Out:' ' es ❑No ❑N/A 2. Chain of Custody Relinquished: - Xs ❑No. ❑N/A 3. Sampler Name •& Signature on COC: �es ❑No ❑N/A 4. Samples Arrived within Hold Timer �es []No. ❑N/A 5. Short Hold Time Analysis (<72hr): Dyes • No' ❑N/A 6. Rush-Turn.Around Time Requested: ❑Yes , trgN ❑N/A Sufficient Volume: Yes ❑No ❑N/A 8. Correct Containers Used: -Pace Containers Used: I 'es ❑No j es El No ❑N/A ❑N/A 9. - Containers Intact: Yes ❑No ❑N/A 10. Filtered volume received for Dissolved tests Dyes No ❑NIA 11. Sample' Labels match COC: Axis/ { ❑N/A -Includes date/timeAD/Anal sis Matrix '9,�q't 12. All containers needing preservation have been checked. All containers needing preservation are found to be in compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, WI-DRO'(water) es ❑No Dyes ❑No ❑Yes dN. ❑NIA ❑N/A 13. Samples checked for dechlbrination: -Dyes ❑No N/A 14. Headspace in VOA Vials (>6mm): ❑Yes .❑No N/A 15. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): Dyes ❑No Dyes ❑No 1�61A N/A 16. Client Notification/ Resolution: Person Contacted:. Date[Time: Comments/ Resolution: SCURF Review: Date:ff77 SRF Review: Date: Note: Whenever there is a discrepancy affecting -North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) Field Data Required? Y / N Page 18 of 18 Appendix (f) 2014 Pathogen and Vector Attraction Reduction ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Tuckaseigee Water and Sewer Auth. Permit Number: WQ 00005763 WWTP Name: TWSA Plant #1 NPDES Number: NC 0039578 Monitoring Period: From l/l/2014 To 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 Alternative 4 pplicable to alternative performe apost Heat Drying i Ray Gamma Ray Class B: Alternative 1 pplicable to alternative performe e Stabilization Air Lerobic Digestion pplicable to alternative verforme Parameter in Sludge Mini 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per gram of 1000 mpn per gram of total solid Salmonella bacteria I 3 MPN per 4 (in lieu of fecal grams total solid 0► Alternative 2 Alternative 3 Alternative 5 Alternative 6 Class A only) indicate "Process to Further Reduce Pathogen Heat Treatment Thermophilic P t zatio-= as eun n _-_ - _ __- -- Alternative 2 Alternative 3 Class B only) indicate "Process to Significantly Reduce Path .ying Composting jAerobic Digestion Class A or Class B) complete the following monitoring data: Pathogen Density Number of Frequency Sample rr Geo. Mean Maxim Units Excee- de c s of Analysis Type 22 22310 mpn/g 2* quarterly grab Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: 11 Tech- 15m ::A2alc.E tion 1 ❑Option 2 ❑ Option 3 ❑ tion 4 ❑ Option 5 ❑ tion 6 Option 7 ion - O t 8 Option 9 Option 1 ❑ ❑ 0 p P P P p No vector attraction reduction options were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector - attraction reduction requirement in 40 CFR 503.33 have been met." 1 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector" attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met.. I am aware that there are significant penalties for false certification including fine and imprisonment." Stan Bryson, WWTP Operations Supt Preparer ame and itle (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer l to Signature of Land Applier (6-EOplla@Ml) RF (5/2003) Date its Ok 11"! 1 41,11' Y TYU A (VA ZAMA 1JAWAj, --I,, On Van AM oil A YO OL; fvAmL 'A Y. vuq:%' -acy0011o)=11 MyM"r0AW3y Pyl ifulwo • I PIQ i I TS 4 :1 1700Mm "AAmS'-:; A: Vy �rjB.. 0 lip sell 0 1 AO P)a 4VE 0; O.yn NO 11 syQuinva n"hwunn, 1"ITMAKupyl 1"Obly tow! %n im Kv OUNPAqwn Ou nbruroh nr" I Anal Caton mukk wa: n. ."W11-110 .00 P401" clanumqu buWalf. man "mm :I kx,woh v; 11mys "'Oi Op"441"! vivo: noQuAvy 'm mA 10005 Do, 70 'SAMMKI ymmsk-hy win -ado 001 )OW", GO Attachment to Annual Pathogen and Vector Attraction • Reduction Form Samples collected and analyzed for fecal coliforms on June 9tn1 2014 and June 12t", 2014 exceeded 1000 mpn/gm/solids. All of the residuals associated with this sampling event were landfilled and were not distributed to the public. A sample collected June 30t" and analyzed by two separate certified labs revealed the maximum coliforms to. be < 175 mpn/g/solids and the stored residuals were considered to be compliant with 503 regulations. Signed -111� ��4 Stan Bryson ® WWTP Operations Supt. • Appendix (g) 2014 Daily Dryer Record ' TWSA DRYER OPERATIONS : DAILY RECORD DATE r� START STOP TOTAL RUN TIME, HRS ��� '1 51 i? 4 1st Dryer Batch Fill Cycle Started @ - :Dry Cycle Started @ "Discharge Cy�IStarted @" "%.._!�; Temperatures - Time Discharge Exhaust Discharge Product Dry + ' Timer. chamber In Chamber Out Rotor ° In Rotor :" Out Operator 1 10,1.. 2 !6) E. o.. 3 a' Time Discharge Exhaust Discharge Product Dry ,.. -Timer Chamber. In Chamber Out Rotor . In. Rotor. Out.. Operator o '4q3 4 DRYER OUTPUT % SOLID Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams 17, 1 39,) x 100 = l� % Total Solids 0602 Discharge Discharge Dry Chamber ' Chamber Rotor Rotor Time Exhaust Product Timer . In Out In ::Out ' Operator 56 DRYER OUTPUT % SOLID Dish Wgt Wet Sample + Dish Dried. Sam le.+ Dish. rams rams '.- rams �S,� Total,Solids. . Alarms or Comments - _ ' 0 TWSA DRYER OPERATIONS- : DAILY RECORD DATE START' STOP T( RUN TIME, HRS 1 st Dryer Batch : -Sta Fill Cycle Started Cycle Started @ 71 Q`­'�igchargid' rted Temperatures Time Discharge Exhaust Discharge Product Dry Timer. Chamber In Chamber' Out Rotor R'dfbr Operator 3 -4-77-1 I _�qt V245 to �4 1, L-2,(j ,,Time Discharge Exhaust Discharge Product Dry., -Timer, Chamber. In Chamber Out Rotor In*. Rotor, Out Operator' 3`2 W. -7 19, b 4�9 - 1361 ")44 100 '445 43 i 4�145 378" -74 has J50 sc�n DRYER OUTPUT % SOLID,' Dish -'V �Jgt ,,-s) (gI rams Wet Sample + Dish Dried Sample + Dish (grams) (grams) 7,01 1:6) R z� X % Total Solids me Ti'l Discharge Exhaust Discharge Product Dry Timer.. Chamber In Chamber out Rotor In Rotor Out O erator �y TWSA DRYER OPERATIONS DAILY RECORD DATE STARTSTOP TOTAL RUN,T[.M.E,-HRS 1st Dryer Batch Fill Cycle Started Dry Cycle Started @ ycliFstarted @ Temperatures .. ......... Time Discharge Exhaust Discharge Product Dry Timer. Chamber In Chamber Out Rotor In —A-6"t"or Out Operator- P-05, 1-11/1J. 0 39,6) 25 L '10 0 445 Y3z �L 3�� 4�w ,7irne -Discharge Exhaust Discharge Product-' Dry -Timer Chamber In Chamber. Out Rotor In . Rot . or. Out. Operator V Z374; �00 V,36�7 DRYER OUTPUT % SOLID E Dish Wgt Wet Sample + Dish Dried Sample + (grams) (grams) (grams) _32-31 q C( x 100 �sy Total Solids .71602 IR TWSA 'DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch G� ;j�%f ' � 7`o ���� s 7 y_ @ Dry Cycle Started @ Discharge Cycle Started.@ Fill C cle Started Tem eratures Discharge Discharge Dry Chamber' Chamber Rotor Rotor Time Exhaust Product Timer . In Out In Out Operator DRYER OUTPUT% SOLID Dish Wgt rams ..Wet Sample +:Dish: rams ` ­ Dried.Sample.} Dish . - rams 04 0 RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started @ Dry Cycle Started @ 1 Dischar e C CIeVStarted g y @-. Temperatures _....._._ .. Time Discharge Exhaust Discharge Product Dry -Timer. Chamber In Chamber Out Rotor .: In" ` - :. Rotor Out Operator CL /fL? E` jet! Discharge Exhaust Discharge . Product-' - Dry _ .-Timer chamber In Chamber Out Rotor . In'. Rotor.. . Operator /Time l `33 ��1 ✓ ..g ` +Out z3 2�Z G? 33 yz3 y3�� % `7 `f l fifes v� l �P- DRYER OUTPUT % SC 12.,2, Wet Sample + Dish I Dried Sample + Dish 7-3 S7 f % Total Solids psCiz Time Discharge Exhaust Discharge Product Dry • Timer.. Chamber In Chamber Out Rotor In Rotor --.,.---Out Operator. 42 d-7� DRYER OUTPUT% SOLIDS Dish Wgt Wet Sample+:Dish Dried. Sam le.+Dish. p rams rams rarris (;C sir 9i % Total, Solids,, . Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD START STOP TOTAL RUN TIME, HRS `7 `� "E�.LA • 1st Dryer Batch _ .__:.......-.. Dischar :- Fill Cycle Started @ lP'^ Dry Cycle Started @ - ge Cycle -Started @ -./ "` - -- - Temperatures Time Discharge Exhaust Discharge Product Dry --Timer. Chamber In Chamber Out Rotor In' -': Out Operator P-3V -6 67 3�> J7-7 'Pll Y Y 3',�z T DRYER OUTPUT-% SOLIDS' Dish Wgt Wet Sample +Dish Dried Sample + Dish -. rams • rams rams �7 . x 100:. .... a I. plids Lt c� SAh _5• a �d Dryer Batc... a v . Fill Cycle Started < : =:= .Dry-Cycle.Started @: Discharge Cycle Started .@ � Temperatures . Time Discharge Exhaust Discharge Product Dry _.. `Timer Chamber. 'In chamber Out Rotor.* In '. . Rotor. 'Out. Operator 5 z AM ti/39' k 3� a 3 �-�-7 � 3 fo DRYER OUTPUT % S Dish Wgt . Wet Sample +Dish Dried SamU+Dishrams rams ra i 3 Z6 70 -7, '3 1, 7,33513 X1oo= b %Total Solids W602 Time Discharge Exhaust Discharge Product Dry Timer..' Chamber In Chamber Out ' Rotor In, Rotor -Out - Operator TWSA DRYER OPERATIONS DAILY RECORD ram., DATE ; START STOP TOTAL. 5 RUN TIME, HRS 1 st Dryer Batch- 3 :. , Fill Cycle Started @ I Dry Cycle Started @ !` I bischerg"e-Cycli Started lS�=:.. .. .... - Tem eratures Discharge Discharge _ Dry + Chamber Chamber Rotor ..'.. Rotor Time 7; 3() Exhaust Product -.Timer. In Out In "`. " "Out O erator-------------- F lob 3 as l�f a44 : )d%D as a3 / 3 .:.3 5� � -.... 3.Q.1� . �3 � DRYER OUTPUT % SOLID Dish-Wgt ..:Wet Sample +Dish— Dried Sample:+.Dish ' rams rams gams - ,,Time Discharge Exhaust Discharge Product' :. Dry --Timer. Chamber. 'In Chamber Out Rotor .. In'. Rotor. Out . Operator cfo IDV � `7 gLa � . :-!�;D J1 �11? c DRYER OUTPUT % SOLIDS 102 Dish Wgt . rams Wet Sample + Dish I Dried Sample + Dish rams rams . 0g5 0, 1a2 1 l 3 7 �L YS� _ I�c x100= M �j o al Solids - -216112 TWSA DRYER OPERATIONS DAILY RECORD DATE C� f 1 START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch - Dischar e C cl Started " Fill Cycle Started @- Dry Cycle Started @ Time Discharge Exhaust Discharge Product Dry Timer. Chamber In Chamber Out Rotor .... - In" = Rotor Out Operator 3 OIL- 3 D a e)5 /R G' DRYER OUTPUT % SOLID Dish Wgt .. Wet Sample .+ Dish' Dried Sample.+ Dish rams 6rams ' rams. 11,2f 9.o •Time Discharge - Exhaust Discharge Product Dry.. - :'Timer Chamber In Chamber Out Rotor In'. Rotor.. Out. :. - - Operator DRYER OUTPUT % SOLID; Dish Wgt rams Wet Sample + Dish rams Dried Sample + Dish rams x100= n 1JF�` a Vi c?1 % Total Solids .WPt 2 TWSA DRYER, OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS _ - 1 st Dryer Batch .'-Dry tamed @ -1. S D Cycle Started @ Discharge Cycle Fill Cycle Started Tem eratures Discharge Discharge Dry Chamber Chamber Rotor _:. Rot Tirrie Exhaust Product - -Timer. In Out In Out Operator 6. �A :.. r DRYER OUTPUT % SOLID D sh-Wgt .:.Wet Sample +Dish • Dried Sample.+ Dish rams rams rams �; 011Q3 = x 100 % Total Solids 2nd D er Batch _ . ry Discharge Cycle:Started. @ ; -Fill Cycle Started. @ Q Dry Started @. r r :Tem eratures Chamber. Chamber . Rotor Rotor. Discharge Discharge Dry Out . O erator. _ Time Exhaust Product' : `Timer In Out In AJ ' • _ -- -.. carer )44 L2 � �j � 27( / DRYER OUTPUT % SOLIDS ish Wgt Wet Sa p+ Dish Dried (g amse + Dish rams(grams)/ . x 100 = QI�; ` � %Total Solids 1 W6/12 r ' START STOP TOTAL RUN TIME, HRS.. 1 st Dryer Batch Fill Cycle Started Y @ Dry Cycle Started @ DisehargeCgr;le Started Temperatures Time Discharge Exhaust Discharge Product ~ Dry -'---Timer . Chamber In Chamber Out Rotor In -' °: " Out Operator. d Dd ! C a-� a43 ,,-Time Discharge Exhaust' Discharge . Product"'' Dry , - : `Timer ' Chamber. In Chamber Out Rotor In'. Rotor. Out . :. Operator • JL D a�f .� ki- DRYER OUTPUT % SOLIDE Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams �, L7s�81 Y, b� D2� x100= � J l O s` D % Total Solids W602 . Time Discharge Exhaust Discharge Product Dry Timer..' Chamber In Chamber Out Rotor In' Rotor . _.:-Out Operator 1311 .TWSA DRYER. OPERATIONS DAILY RECORD ; DATE — '2 e-{ START' STOP TOTAL :.... _ . . RUN TIME, HRS 1 st Dryer Batch : - - "Disehar e C CI'E tamed Fill Cycle Started @ Dry Cycle Started @ 5- -:..y. t @-- Discharge Discharge Dry r Chamber Chamber Rotor Time 7; 3 Exhaust (J Product f -'---Timer. C� In �� Out I 7r In '- .v Out � a Operator r ,�(,�,�'�' 97,5-- Ey. 13 23& X41 1O o3��� h 14 C�24'1 kb.- ,I 144 .. -3 r`?vr g 4q*b q-C : DRYER OUTPUT % SOLID Dish Wgt .. Wet Sample + Dish ' - Dried Sample.+ Dish rams rams ' rams. -Time Discharge Exhaust Discharge Product Dry ': - :`Timer . Chamber 'In 9 Chamber Out Rotor In'. Rotor. Out . 06,E Operator �10 - 3�� 3 :445 • DRYER OUTPUT % SOLID: k Dish Wgt rams Wet Sample + Dish rams I Dried Sample + Dish rams x 100 = �� % Total Solids .WPi12 TWSA DRYER OPERATIONS,-"--' DAILY RECORD. 3rd Dryer Batch Fill Cycle Started @ Dry Cycle Started @ Discharge Cycle Started, @ Tem eratures : : . Discharge Time Exhaust Discharge Product Dry Chamber Chamber Timer... In Rotor Rotor . Ou# � O erator r; d � 3 C�l DRYER OUTPUT% SOLID Dish Wgt WetSample +:Dish Dried.Sample.t Dish. :... 3. rams rams ..: - rarris ::. ::: .•. % TotaF,Solids. Alarms or Comments I I iat TWSA D.RYER.OPERATIONS DAILY RECORD DATE. _. . START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started Dry Cycle Started @ Discharge Cyclic Started @ -'-' ✓� """ - " `� Time Discharge Exhaust Discharge Product Dry =.Timer. Chamber In Chamber Out Rotor _:. In :Rotor ":'` :.Out Operator ETA DRYER OUTPUT % SOLID Dish Wgt ..Wet Sample + Dish Dried Sample.+ Dish rams rams gams Time Discharge Exhaust Discharge Product :Dry ., - :`Time r . Chambery In v Chamber Out . Rotor In'. Rotor. Out . Operator 42. ; l -f I lV/ DRYER OUTPUT % SOLID; Dish Wgt . rams Wet Sample + Dish Dried Sample + Dish rams rams r u /o x100= a Total Solids .?JP02 TWSA •DRYER OPERATIONS -':• DAILY. RECORD . 3rd Dryer Batch Fill Cycle Started @ F ` •• c-' Dry Cycle Started @ - • • �� Discharge Cycle Started.@ 2 5 e Discharge Time Exhaust Discharge Product Ter eratures Dry Chamber Chamber Timer..• In Rotor Rotor _ Out In - Out O erator 4 f y. DRYER OUTPUT%SOLID DishWgt :.WetSample--.:Dish Dried: Sample.+Dish. . - .. rams rams -. rarris X _. %o Total -Solids. Alarms'or Comments :. f i r TVVSA DRYEROPERATIONS- DAILY RECORD DATE START* STOP TOTAL RUN TIME, HRS. 1 st Dryer Batch Fill Cycle Started Cycle Started @ 813 TPmnerntures Time Discharge Exhaust Discharge Product Dry y .-'-.:Timer. Chamber In Chamber Out Rotor "Out Operator .13IR9 -`36r b9 4-5 al) A Z).. _3z)S - I Discharge Discharge Dry.*.. •- Chamber.. Chamber Rotor Rotor .• Time Exhaust Product- - Timer. 'in Out In'. Out . Operator' 0 3-5 'Aa/0 '14 DRYER OUTPUT % Dish Wgt. Wet Sample + (grams) (grams) +Dish I % Total Solids .;yP02 Fill Cycle Started @ Dry Cycle Started @ y/ Discharge Cycle Started.@ Time Discharge Exhaust Discharge Product Dry Timer _ Chamber ' . In v Chamber o/u7t Rotor In Rotor - ;Out . Operator v ✓ •- f � � TWSA DRYER OPERATIONS - DAILY RECORD DATE START' STOP TOTAL RUN TIME, HRS .. .... ' . `f'� _A5Q0 LQ:. 4A%� L 1st Dryer Batch Fill Cycle Started -.Dry Cycle Started @,'� Dischar e C r;IStarted Temperatures _ - -- Time Discharge Exhaust Discharge Product ~ Dry .-'---Timer . Chamber In Chamber Out Rotor -:.. : , Rotor ,Out Operator �7f2s- 7 O 3qo 3 i0 21) 110,371 +0 : (-/V/ Time Discharge Exhaust Discharge Product Dry , . "Timer Chamber.. 'In Chamber Out Rotor In'. Rotor Out-. Operator 715 Y` �, ys y3�s DRYER OUTPUT % SOLID Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams) (grams 7700. x100= LpJ.�G Total Solids .wPV2 Time Discharge Exhaust Discharge Product Dry Timer..• Chamber In J. Chamber ' Out Rotor In" --Rotor . � :.-Out 'Operator .TWSA DRYER OPERATIONS DAILY RECORD DATE. START' AL RUNTIME, HRS 1 st Dryer Batch Fill Cycle Started @ - "" Dry Cycle Started @ - V Discharge=Cgcle-Sta t6d @`� Tem neratu res Time Discharge Exhaust Discharge Product DryJ .-'-:Timer. Chamber In Chamber Out Rotor " In � �--� ` ':"" 'Out Operator % a Q D, OC' ~� Time Discharge Exhaust' Discharge Product- - Dry , . :. Tmer Chamber 'In Chamber Out Rotor In'. Rotor. "Out . . Operator ILI �93 b 5 Ab'6 Q 3 a #) 3? �7 C' K ► (� o a JV3 may . 2-134 1 • DRYER OUTPUT % SOLIDz Dish Wgt . Wet Sample + Dish I Dried Sample + Dish rams rams rams - x100= %Total Solids .2/6M / !tom . Time Discharge Exhaust Discharge Product Dry Timer.. Chamber Chamber Rotor in Out In ' . Rotor . - ;Out 'Operator' 7..i.. TWSA .D.RYER.OPERATIONS- DAILY RECORD ; DATE RUN TIME, HRS... 1 st Dryer Batch Fill Cycle. Started ~- ``" =` -Dry Cycle Started @ ""Diseharge CyCl Started @- ... ry Y Time Discharge Exhaust Discharge Product Dry =Timer. Chamber In Chamber Out Rotor .:.. In-:,.-' :' Rotor ':` `"Out Operator 367 3 y� 3.53 OA Time Discharge Exhaust Discharge Product Dry ".. - ' : `Timer . Chamber. 'In Chamber Out ..Rotor.. In'. -..-Rotor.-:,: Out-- Operator cv a 3 . 6,57. DRYER OUTPUT % SOLID; 2!6/'12 Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams ILI I o y , 1 � _� ,� f i %Total Solids s TWSA -'DRYER OPERATIONS DAILY RECORD :... 3rd Dryer Batch Fill Cycle Started @ Dry Cycle Started @ .. Discharge Cycle Started-@ C/15 Tem eratures Discharge Time Exhaust Discharge -Product Dry Chamber Timer.; In Chamber Out Rotor Rotor In- ---Out - - O erator _ �, 40 fir'! �� c)�, � ' a ' DRYER OUTPUT% SOLID Dish Wgt : Wet Sample +:Dish' Dried. Sample.+ Dish . rams rams)*':. rarris . • x :100 : .• / % Tota!,Solids. _ . Alarms or Comments -.:;. :...: . I I f TWSA DRYER. OPERATIONS DAILY RECORD_ DATE START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started -Dry Cycle Started @ `.I : Discharge-Cycl:L,�Started @ Temr)eratures -- ..Time Discharge Exhaust Discharge Product Dry .-'---Timer . Chamber In Chamber Out Rotor .:.. In `-- ' : R�►or '. -Out Operator '. Time Discharge Exhaust Discharge Product' ' Dry.', - ::Timer - Chamber. 'In Chamber Out Rotor In ". Rotor.. Out . Operator 1; a �A b ~ Lf� G v ;? �l �. �1 ` `j --� �i� y'� ✓�. iG1-- DRYER OUTPUT % - Sample.+ Dish `"-oases C , x100= .7J902 - I �6 ) % Total Solids Time Discharge Exhaust Discharge Product Dry Timer . Chamber In Chamber Out Rotor In" Rotor . ::Out Operator vc/zv-� 3977']��I-Oj DRYER OUTPUT% SOLIDZ Dish Wgt ::Wet Sample +:Dish Dried. Sample.+ Dish. :_.....:.:..: _.. - - rams rams '., rams -- /�335 1 :.. X100,7 .-Q `% Total -,:Solids. Alarms or Comments TWSA DRYER. OPERATIONS DAILY RECORD DATE J START STOP TOTAL RUN TIME, HRS .. ..._ O y ° 1 st Dryer Batch Fill Cycle Started @ '- - "Dry Cycle Started @ ` Dischkge,CycI�Started Temperatures — Discharge Discharge Dry Chamber Chamber Rotor..... • Rotor Time Exhaust Product .-*=Timer. In Out " In- - ": " Out Operator 4l -,-Time Discharge Exhaust ' Discharge Product- Dry.', - : `Timer Chamber- 'In Chamber Out Rotor In'. Rotor. Out . Operator Al O 3 . A-3' �� - 1437 4 973 ' 3 i'7 5 -� 0 DRYER OUTPUT % SOLID Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams 16.3 c ��� 17. 7 9 v x 100 = (� a/a TO Solids TWSA `DRYER OPERATIONS DAILY. RECORD :. 3rd Dryer Batch � Fill Cycle Started @ �J ,.. .. Dry Cycle Started @ .. Discharge Cycle Started.@ Temp eratures Discharge Discharge Dry Chamber Chamber Rotor Rotor Time Exhaust Product Timer..' In Out . In- - Out - O erator TWSA DRYER OPERATIONS - DAILY RECORD DATE START' STOP TOTAL RUN TIME, HRS. I st Dryer Batch Fill Cycle Started -.Dry Cycle Started @ TprnnizrAti irp-q Time Discharge Exhaust Discharge Product Dry .-'---Timer. Chamber In Chamber Out Rotor Rotor a Operator qJ 0. .9, d,3 .2413 4 4-.7 435 Time Discharge Exhaust Discharge Product- Dry 1:`Timer - Chamber- In Chamber Out Rotor. In'. Rotor Out Operator _1P IR V1 If 6 4.13. V-17 DRYER OUTPUT % SOLID sF Dish /021 .7W12 ■ )ried Sample + Dish (6rams /7, D'oD vX 1010-- %Total Sol C) 0 a z Time Discharge Exhaust Discharge Product Dry Timer.." Chamber' In Chamber Out Rotor in, '.Rotor :Out O erator 25 705. � DRYER OUTPUT% SOLID Dish Wdt Wet Sample +:Dish Dried: Sample.+ Dish . rams(grams)'.,:rams 7q j x100 :%o Total,Solids.. . . Alarms or Comments �- ��,� � , . �,� o, G, � . •��'•' � � • . • r - .. rya .Q7.t J' RUN TIME, HRS 1 st Dryer Batch C:: ___-.Dry Fill Cycle Started @� • Cycle Started @ �a'1 � �" ••Discharge=Cgcl�Started @'`�� - Temperatures Time Discharge Exhaust Discharge Product Dry , =.-Timer. Chamber In chamber Out Rotor .:.. In`- : Rotor Out Operator 433 mjqol a 6s .. 0. ] . -Time Discharge Exhaust Discharge Product- Dry ; . `Timer Chamber. Iri Chamber Out Rotor In . Rotor.. Out . Operator J f3-0 a It r j -o -144 371 _9q- al �r 3.:�r clele DRYER OUTPUT % SOME Dish Wgt . Wet Sample +Dish Dried Sample + Dish rams rams rams sue- J 100= .S d a x% Total Solids . ,wP 12 Time Discharge Exhaust Discharge Product Dry Timer..' Chamber In Chamber Out Rotor in Rotor - ::Out 'Operator 7 0 TWSA DRYER. OPERATIONS - DAILY RECORD DATE START" STOP TOTAL RUN TIME, HRS ­7o _154 1st Dryer Batch P:d. n ft t-0 7, 1i (c)- yci e-Sta Fill Cycle Started -.Dry Cycle Started Temnerqtures Time Discharge Exhaust Discharge Product Dry .-*---Timer. Chamber In Chamber Out Rotor I In"' - -.:,Rotor Out Operator ­7 t. .7, Z) cl.-63 a P 43 Time Discharge Exhaust Discharge Product" Dry.', Timer chamber. 'in Chamber Out Rotor In'. Rotor. Out . Operator D4'a. 1. . V 06 7 A5, 0- 414 q,3139 DRYER OUTPUT % . WRI 2 ish Wgt Wet Sample + Dish Dried Samp le Dish] grams ) (grams) rams 033 9-,3 t�s 5 x 1+00 111, 0.1 Total Soli Time Discharge Exhaust Discharge Product Dry Timer.. Chamber ^ In Chamber out Rotor in. Rotor . 'Operator' - -76 Dv� at, I t/I > op 76 c�7S Q 6, -77Si b LIN RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started @ f� `==- -Dry Cycle Started @ ✓ 3 'Discharge--Cycl Started -.. ... . Temneratures Time Discharge Exhaust- Discharge Product 4Dry, -'==Timer. Chamber In Chamber Out Rotor _:.. In- "' R&or ". ` '-.Out Operator !3. _ v 1 U 310 3 -7D . 3� 27 vy "Time Discharge Exhaust Discharge Product :`.-Timer Dry.', - Chamber. In Chamber Out . Rotor. In'.. Rotor.. Out,.. Operator ` v i J P, - v � V `C DRYER OUTPUT % SOLID; .WP 12 nple + Dish sms s r.0017 f x100= 7,) % Total Solids '75 TWSA DRYER. OPERATIONS' DAILY RECORD DATE STARTSTOP TOTAL - �— �� F RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started �- D C cle Started Dischar e C cle-Started ... ...... . Temoeratures -- Time Discharge Exhaust Discharge Product Dry, ---Timer. Chamber In Chamber Out Rotor " In':----' '. ` 'Out Operator - 3; 0 36 )., r .b Syr yes Y-V 4 � ' y3 7 0,`j.6 �s`�' sus1137 �(1r Time Discharge Exhaust Discharge Product - Dry , . - *.--Timer . Chamber. In Chamber Out Rotor In'. Rotor. Out- . Operator I2-J7 �2a?* 5-6 Y� e f Lly y.3� Yy 36� 2:►7 66 : �C,5r �qyy `/ V� DRYER OUTPUT % SOLIDz Dish Wgt . Wet Sample + Dish Dried Sample + Dish rams rams rams r. x100= / � � - b ) % Total Solids Time Discharge Exhaust Discharge Product Dry Timer.. Chamber In Chamber Out Rotor In**' Rotor - ::-Out - Operator' .�_e��y�v. �r9 -TvVSA DRYER. OPERATIONS - DAILY RECORD, DATE — START STOP TOTAL RUN TIME, HRS low 1 st Dryer Batch ycIL-Started, Fill Cycle Started -.Dry Cycle Started @ --Dischkdet C Temperatures Time Discharge Exhaust Discharge Product Y Dry .-'---Timer Chamber In Chamber Out Rotor In Rotor 'Out Operator J- 6-5 Y5 Llo C/ V. b 3 too.- 1,L-U ya E-9 3 6. y Time Discharge Exhaust Discharge Product- Dry Timer - Chamber. In Chamber Out Rotor In' -Rotor. Out-- Operator y�Y)�Y 23 511 //1 371- 171 WV C/o DRYER OUTPUT % ' S .W6M Dish Wgt Wet Sample + (grams) (grams) 19. d-1�41-c� Dried Sample + Dish (grams) 1q. x 100 % Total Solids Time Discharge Exhaust Discharge Product Dry Timer_ • Chamber In Chamber Out Rotor In Rotor . - :_-Out O erator START' STOP TOTAL ..RUN TIME, HRS % ".� '•� 1i:c 1 st Dryer Batch Fill Cycle Started Iry "= ` =D . Cycle Started 713 " Dischar e C cIe Started Y @ ".-.Dry* Y @ Y @._..._ . W Time Discharge Exhaust Discharge Product _ Dry' =-:..Timer. Chamber In Chamber Out Rotor .:.. -In Rotor ':' :Out Operator _?123 v7 �o i y 3? T;" D15�t D 5 YJ - Time Discharge Exhaust Discharge Product Dry :. : `:Tmer Chamber. inG Chamber- Out Rotor . In*. .. Rotor. Out.. Operator DRYER OUTPUT % SCILIDs Dish Wgt Wet Sample + Dish I Dried Sample * Dish rams rams rams 7a _56 x1oo= % 6, % %Total Solids 2/6M2 Time Discharge Exhaust Discharge Product Dry Timer . Chamber' In Chamber Out Rotor In Rotor . -Out 'O erator �l 3-7.J. u TWSA DRYER OPERATIONS DAILY RECORD :. . DATE . L I START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started @ --Dry Cycle Started Temperatures -- Discharge Discharge Dry Chamber Chamber Rotor .:.. =' R6ior Time Exhaust ProductTimer. In Out In' "' Out Operator j4 01 - Time Discharge_ Exhaust Discharge . Product' � Dry , . "Timer Chamber. 'In Chamber Out Rotor . - In'. Rotor. 'Out.: Operator loo DRYER OUTPUT % SOLID Dish Wgt + Dish I Dried Sample + Dish l I CG7/ I _30„37 Ste.. I `7GI 3� g x1oo= �5M 2/602 % Total Solids Time Discharge Exhaust Discharge Product Dry Timer . Chamber' In Chamber Out Rotor In, Rotor . - ---Out Operator yam-�S.C. n u TWSA DRYER. OPERATIONS-,- : DAILY RECORD DATE`' RUN TIME, HRS fo= J m 1 st Dryer Batch Fill Cycle Started D C cle Started ; Dischar a-C-c�e Started =. - - - Temperatures Time Discharge Exhaust Discharge Product Dry .. Timer. Chamber In Chamber Out Rotor "In".— ': ' "Out Operator TO 10? -0 Y gig, ,._• � D), .931 (P 100. S; Time Discharge Exhaust Discharge . Product' Dry ; ... . `Timer , Chamber. 1n Chamber Out Rotor . In:. Rotor. -Out.: Operator' .� i� �p 2 ,31 OM DRYER OUTPUT % S( (0�2 ,2/6/12 rams x1oo= q U %TO' tal Solids Time Discharge Exhaust Discharge Product Dry Timer..' Chamber In Chamber Out Rotor In' : Rotor . Out Operator V. DRYER OUTPUT % SOLID 103 Dish Wgt rams :Wet Sample +:Dish ..:, rams ` Dried. Sample.+ Dish. . . rams EESTART STOP TOTAL - RUN TIME, HRS t�J ; 3 •. `�' ° 1 st Dryer Batch Fill Cycle Started 7-D y Cycle Started Dischar -e'-C-cle Started Y @ ry Y @ g Y Tempe tures Time Discharge Exhaust Discharge Product Dry .•Timer. Chamber In Chamber Out Rotor .:.',----Rotor " In' :' ` 'Out Operator 7 �. .. -3Z 5 *15 44 :1 YS-•.. ' 3 ef-. P7. DRYER OUTPUT % SOLID- Dish Wgt .. Wet Sample + Dish Dried Sample.+ Dish L� g1a rams rams : rams 1 x 100: - - _... ` 'a/o Total Solids 2nd Dryer Batch Fill Cycle Started @ -: =' Dry::y C cle.. Started .@ Discharge Cycle Started@ yi Tem eratures . --Time Discharge Exhaust Discharge . Product : Dry , - :`Timer Chamber 'In Chamber Out Rotor . In . Rotor.. Out Operator 3 14 l �� �. J00 1,5 v2 �0 cqLJ, -• ,qA4J L v = 46s`3 1, DRYER OUTPUT % SI 2/6„2 Uish wgt wet Sample + Di rams rams 17 q t -7 pie + Dish 171 0 OfQ[Lt�. x100= Total Solids Time/ Discharge Exhaust Discharge Product Dry -.••Tii�mer.. Chamber Chamber Out Rotor In- Rotor :--Out Operator jIn DRYER OUTPUT% SOLID; Dish Wgt rams) - Wet Sample +:Dish. (grams)" Dried.Sample.+ Dish. rams T\A/SA DRYER. OPERATIONS DAILY RECORD. DATE— m L Pf. START STOP TOTAL RUN TIME, HRS I st Dryer Batch Fill Cycle Started ".Dry Cycle Started @ 700 y*icle�Stgrt6d,@ Temperatures Time Discharge Exhaust Discharge Product _--bry ..-Timer. chamber In Chamber Out Rotor In" ­F&br *.-Out Operator 3 42 373 3-75- 3 73 ;Z, 2 y v 4_.�v1�1 13 X5, v v )11 y y 16 0 Y v 7 Time Discharge Exhaust aust Discharge Product- Dry Chamber 'in Chamber 4 Out Rotor In Rotor. Out..-.— 'Operator J �,9 '7 J. 2 '7q 30 75 DRYER OUTPUT % SOLID s Dish Wgt Wet Sample + Dish I Dried Sample + DiiTh (grams)— grams) (grams) Z) x 1,00 % Tota I Solids ?16112 DRYER OUTPUT% SOLID Dish Wgt rams Wet'Sample +Dish , rams)"--: Dried. Sample.+ Dish . rams TWSA DRYER OPERATIONS DAILY RECORD DATE - START STOP TOTAL RUNTIME, HRS F 'I V-C� 1 st Dryer Batch Fill Ccle Started y ate. '`; 5 = ..Dry Cycle Started @ Disch6rge-- C-Started @- Temperatures Time Discharge Exhaust Discharge Product Dry .. Timer. Chamber In Chamber Out Rotor .:.. In .= Rotor " -Out Operator 60 ` .: ','rime Discharge Exhaust Discharge Product' Dry ; - '-.`Timer - Chamber In Chamber Out - . Rotor .'- In:. ....Rotor.:: 'Out.: . Operator' 0 V - i •P r ' a a. ,P- 0 d 0 DRYER OUTPUT % W6„2 Dish Wgt Wet Sample + Dish rams rams /w/ von Dried Sample + Dish rams �r x100='. . v � %Total Solids Time Discharge Exhaust Discharge Product Dry '-....Timer Chamber —In Chamber Out, Rotor In' Rotor . :Out ' Operator. 4RT STOP TOTAL RUN TIME, HRS 1 st Dryer Batch, Fill Cycle Started r Y @ `` Dry Cycle Started @ .-Discharge:CyolE�:Started -@:- Tem .eratures ._ Time Discharge Exhaust Discharge Product ... ....... .....__ Dry ..-Timer. Chamber In Chamber Out. Rotor '.:..: " In -` Rotor :' ' "Out Operator 3 1s 71 A :-zI3 Time Discharge Exhaust Discharge . Product- :. Dry '. - ' : `Timer . Chamber 'In Chamber Out Rotor . In'. Rotor. -Out.: ' O erator. • : 0 /b AV' 6 %�e, 06 DRYER OUTPUT % SOLJYJ Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams 7( V793 Y 05;:i X1oo= r W602 % Total Solids Time Discharge Exhaust Discharge Product Dry .Timer . Chamber In Chamber Out Rotor In' '- - Rotor Out Operator J -�779.'.. 0 RUN TIME, HRS ';Au 1 st Dryer Batch Fill Cycle Started @ "Dry Cycle Started @ Discharge:--Cyc'l'esStarted @ II7 Temperatures Time Discharge Exhaust Discharge Product Dry Timer. Chamber In Chamber Out Rotor In FULor "Out Operator 3--ts zz y �fa.� z o 6 - zoo .: �;�.-.-:.. � y � �y� 3 ���� 3� � �-� ipv i -Y31*- V-V. 6 .3 22 T 6 3 3-9S Time Discharge Exhaust' Discharge Product- :':'Tirrier Dry.'.. - Chamber 'in Chamber Out Rotor In7. Rotor. 'Out. Operator 5 -,Z 73 N�L-A ?.. / Y( . ... .. 10 Sys TIS 37 '0 -4 71 �3 ArO DRYER OUTPUT % SOLID s I Dried Sample + Dish Dish Wgt Wet Sample + Dish (grams) (grams) (grams) ..2160 2 X.1 00 % Total Solids Fill Cycle Started @ = Dry Cycle Started Y @ Discharge Cycle Started,@ Time, Discharge Exhaust Discharge Product Dry Timer . Chamber Chamber Rotor In Out In, Rotor . - .,-Out O erator TWSA DRYER. OPERATIONS -- DAILY RECORD DATE L7 �. V. START STOP TOTAL RUN TIME, HRS 700 1st Dryer Batch • Fill Cycle Started @ - -D Cycle Started 6 Dikhar e.C-cle�Started ".Dry Y @ g Y @ _ Temperatures - Time Discharge Exhaust Discharge Product Dry J Timer. Chamber In Chamber Out Rotor .:.. In- -' = R6►or " Out Operator 0 317 3A. 3 97 7 J �5-w �_3? �� � ..._ y.7 �3G y`�7 3/ 13 �Z Z '2-13 /00 q: 3 YYs 3�G Time Discharge Exhaust Discharge Product Dry :. '-Timer Chamber. 'In Chamber Out Rotor. In'. Rotor...:: Out : 'Operator y 3 3 y_ DRYER OUTPUT % SOUps Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams l%-1q3 v otal Solids •2J602 3rd Dryer Batch Fill Cycle Started @ DyCycltared @ Discharge Cycle Started.@ i em eratures Discharge Discharge Dry Chamber Chamber Rotor Rotor . Time Exhaust Product =-Timer.. In Out In, -Out -- Operator. TWSA D.RYER.OPERATIONS* DAILY RECORD DATE 1- START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch _. Fill Cycle Started @ Jr'=_- .Dry Cycle Started (a�- t Discharge Cycl 'Started @" o - , rn :-;_::_•----__: Temperatures - -- - Time Discharge Exhaust Discharge Product Dry y� Timer. Chamber In Chamber Out Rotor -:.. In-.- .-Rotor : Out Operator G� lai QD3 . J q. Q -4 0 9 jla d-a - d':0 2-35 c2Qe - q a 4 • . � ;..9 .9 12,5 Time Discharge Exhaust Discharge . Product-: Dry ': - ':'Timer, Chamber. In Chamber Out Rotor . In'. Rotor Out. 'Operator - /.�-/�,i/�" a, Z3-. 3 70 . 3; �3 .2 -9- . ,5-0 - V 7 3S DRYER OUTPUT % SOLIps Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams) (grams x 100 = v % Total Solids oduct Dry Timer . Chamber' in Chamber out Rotor In RotorTime :Out O erator WDischargeharge 46 �. . 0 TVVSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS I st Dryer Batch Fill Cycle Started Cycle Started@ '-.'.'Di�ch�rdeF--C�6lcStarted @ Temperatures 'Time Discharge Exhaust Discharge Product Dry Timer. Chamber In Chamber Out Rotor fn '­,�'Out Operator � 53 � 1-Y45 43 la - 1 1141 U iD' 41�5 4 4`-tics". 6_0 Time Discharge Exhaust Discharge Product-: Dry -Timer Chamber .1n Chamber Out Rotor . In'. Rotor Out.: 40 —Operator P-3 i Q_ LO'7. -IZ)Z) 421to �// Lp a,33 -Pa -/01/70- )44,5_ 42? 1�14151 C_ Z4 1 4cf ( 1: -�4YT DRYER OUTPUT % . .7/602 k K 9 + Dish Dried Sample + Dish )S) (grams) X.1,00 96� d % Total Solids Time Discharge Exhaust Discharge Product Dry .',.Timer.. Chamber In Chamber Out Rotor In' - Rotor -----.--Out = Operator 1. ©:( :' . y'.V'6 r 3 6 0 TWSA DRYER. OPERATIONS -" : :.. DAILY RECORD DATE 6 y START STOP TOTAL RUN TIME, HRS� 1 st Dryer Batch Fill Cycle Started @ - -"- :Dry Cycle Started @ - J .• Discharge -Cycle Started Temperatures - Time Discharge Exhaust Discharge Product _ Dry ' Timer. Chamber In chamber Out Rotor -:.. ° fn" ..:,'Rotor " "'"" Out Operator '71-t"5 C_ g.b.5 .i;3 4 '5 37D . "Time Discharge Exhaust Discharge . Product Dry'... "Timer chamber" In Chamber Out Rotor . In'. Rotor.. -Out.: Operator 76. CO °1 4 3 75� L{t3 ,5 37 C', DRYER OUTPUT % SOLIDE Dish Wgt Wet Sample + Dish Dried Sample + rams (grams)' rams rr Doi ? ` 3 x100= •2/602 Time Discharge Exhaust Discharge Product Dry Timer.. Chamber In Chamber Out Rotor In- :Rotor . ----.:-Out 'Operator Gr DRYER- OUTPUT% SOLID Dish W rams We t et Sample +:Dish . Dried. Sample.+ Dish. rams " rards • TWSA DRYER OPERATIONS DAILY RECORD DATE 1 START STOP TOTAL RUN _ RUN TIME, HRS C3 1 st Dryer Batch SS Fill Cycle Started �. - r .: - Y @- '. -R� •. 0- :. _.Dry Cycle Started' Discharge=Cgcl�Started @_._ .� �_ _� N- •._ :: .::.: Temperatures - Time Discharge Exhaust Discharge ProductTimer. Dry Chamber In Chamber Out Rotor .:. In Rotor Out Operator `3 c�2,S� C� b , G _, z �= 0C `- `�7 ' �S �{ -T'f Time Discharge Exhaust Discharge . Producfi Dry ; - : 'Timer Chamber. In Chamber Out Rotor . In'. Rotor. . Out. Operator x ,t��f.5 f r'3s" Lf 7 `321 Ds 5: l5 DRYER OUTPUT % SOLID Dish Wgt Wet Sample + Dish 7 Dried Sample + Dish rams rams rams .��_'1$L( 1 -70 c x1oo= 9 7 %Total Solids Time Discharge Exhaust Discharge Product Dry Timer.. Chamber In Chamber Out Rotor In :Rotor - : -Out Operator 44S DRYER OUTPUTSOLID Dish Wgt rams .Wet Sample +:Dish rams ' Dried. Sample.+ Dish. rams t -- TWSA DRYER. OPERATIONS - DAILY RECORD DATE*_ - 'LP — — START STOP .TOTAL RUN TIME, HRS 1 st Dryer Batch Fill C cle Started - - -" Y @ Dry Cycle Started @ o� " 'Discharge=CY6 tarted Temperatures ._ Time Discharge Exhaust Discharge Product Dry -..-Timer. Chamber In chamber Out Rotor In " "Out Operator V �+ ( � . • fY 44 i C ; . 67 7 2 C' '• Time Discharge Exhaust Discharge . Product : Dry ; - . `Timer , Chamber. 'In Chamber Out Rotor . In'. Rotor Out.: Operator :.0 r 5 1) 3 -1 SD ' -1-11-IS I 431P- 1445 47 l lo7 1H,5 DRYER OUTPUT % SOLIDE Dish Wgt Wet Sample + Dish I Dried Sample + rams rams rams 03 .W602 aV--0�Ka< % Total Solids Time Discharge Exhaust Discharge Product Dry - ... Timer. •' Chamber' In Chamber Out Rotor In :Rotor -.,-.--Out O erator ;t6 zsv. S ply 3? l� �.�3 DRYER OUTPUT% SOLID Dish Wgt rams Wet Sample +:Dish .. rams Dried. Sample.+ Dish . rams • TWSA DRYER OPERATIONS DAILY RECORD - DATE START STOP / TOTAL RUN TIME, HRS 3. U 1 st Dryer Batch Fill Cycle Started --- Y @ -. � - ��-�' I• ° - .D Cycle Started � � � Dischar e=C-cle Started �� ---••� --- - --•--- - Temperatures = -- Time Discharge Exhaust Discharge Product Dry Timer. Chamber In Chamber Out Rotor In Rotor Out Operator 139� 1B P) �7 �a ei. .:� . Era )44 Time Discharge_ Exhaust Discharge Product : Dry , - Timer Chamber y' 'In y Chamber Out Rotor . In . Rotor.. -Out - Operator 419 2>05 � S57 4:;;, f�146;, -fq� Z ;7 �Q DRYER OUTPUT % SOLID Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams 77 x1oo= (::�15O/ . %Total Solids 2/602 Time Discharge Exhaust Discharge Product Dry ,-Timer.. Chamber In Chamber Out Rotor In : Rotor - :Out O erator 9-3 Y9L Yc `f L DRYER OUTPUTSOLID Dish Vygt rams Wet Sample +:Dish rams Dried. Sample.+ Dish. rams a;:- y3s : 7c, v RUN TIME, HRS ,V 1 st Dryer Batch Fill Cycle Started y @� -. :"-�., .-- - .Dry Cycle Started @ / � %�� -Discharge-CjiclE'Started.@_�.__- ,•_ ........_.._.._ -..._.._._. Temperatures Time Discharge Exhaust Discharge Product Dry .'..Timer. Chamber In Chamber Out Rotor .:.. _ In -` : Rotor ' ` Out Operator 6 39 Ing - 4- 43.E ,Y46 30 ' 5 1 - 3- %b.b4q .1,5) 422 4.1b Time Discharge Exhaust Discharge . Product :. _ Dry : - , '"Timer . chamber In Chamber Out Rotor . In'. Rotor. - Out.: Operator ° �93 6Z6-5. /00 440 43 . ( 38 - 63 DRYER OUTPUT %.SOLIDz Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams i. D I YO � 3 % Al- x100= % Total Solids. Time Discharge Exhaust Discharge Product Dry Timer.. Chamber' in Chamber Out Rotor in" .Rotor . Out O erator .Ys _3j� E RUN TIME, HRS I : of `7 I b 116 1 1 st Dryer Batch Fill Cycle Started T Y @ Dry Cycle Started @ 7•- Discharge=Cycla�Started Temperatures --- Time. Discharge Exhaust Discharge Product Dry -..-Timer. Chamber In chamber Out Rotor In Out Operator _g•::Q apt a��S 30 05 ) 0D : Discharge Discharge . Product' Dry '; - :`Tmer Chamber 'In Chamber Out Rotor . In,*. Rotor. : 'Out.:,. Operator }}Time,J'L �}Exha�uust 0 0 )4(e 3()5 7/� '-qqL41© � DRYER OUTPUT % SOLIDE Dish Wgt Wet Sample + Dish Dried Sample + Dish rams rams rams 1.o130 23, S3 13 ,;2,,',& 9s- x1oo= % Total Solids Time Discharge Exhaust Discharge Product Dry Timer.. Chamber In Chamber Out Rotor In- Rotor -,-Out Operator 22, J. DRYER OUTPUT% SOLID Dish Wgt rams Wet Sample �Uis�Dried.Sample.+ (grams)'".. Dish . rams 40 RUN TIME, HRS I Le • -5ti3 j . ©O 1st Dryer Batch Fill Cycle Started @ =: `Dry Cycle Started @ ' . =" Discharge :Cgole-Starte'd Temperatures - .. Time Discharge Exhaust Discharge Product Dry ..Timer. Chamber In Chamber Out Rotor IIn '` Out Operator as �sD L.�019 Time Discharge Exhaust' Discharge . Product Dry , . :'-Timer Chamber 'In Chamber Out Rotor . In'. Rotor . 'Out.: 'Operator U .5� JLD- ,� �3 3 a )DO� ` V v/ / VJ [ L a L DRYER OUTPUT % SOL]Dz Dish Wgt Wet Sample + Di (grams rams 1,03)3 M Disr (9. 96 7 S . .WSM Dried Sample + (grams) �o.��r� x100= % /-D Total Solids Time Discharge Exhaust Discharge Product Dry ,.,.Timer..' Chamber in Chamber Out Rotor in : Rotor . --:--Out Operator �44- 17 DRYER OUTPUT% SOLIDs DishWgt rams Wet Sample+.:Dish: Dried.Sample,+Dish. rams rams 10 I TWSA DRYER OPERATIONS DAILY RECORD DATE Le — . ` `` i START STOP TOTAL RUN TIME, HRS 1st Dryer Batch Fill Cycle Started @ ;.,.f{;✓�--= Dry Cycle Started @ l "Discharge Cy�lStarted @-` Temperatures Time Discharge Exhaust Discharge Product Dry .. Timer. Chamber In Chamber Out Rotor .:.. In' " = Rb"t- "' -Out Operator 6/. a aQ,�- d6 46a as C -19: �A qu .. g . X7 9.. ��. Ig qqS 4ffXX.I. (5- 39 . _ Time Discharge Exhaust Discharge . Product :*:'-Timer : Dry :. '-Timer Chamber. In Chamber Out Rotor.. In ". Rotor....- Out ' O erator. 4) 46 2-53 9 6 7 s DRYER OUTPUT % SOLIDE Dish Wgt Wet SamPle + Dish Dried SamPle + Dish rams rams rams 12 26, �3. 9/3D x100= % Total Solids Time Discharge Exhaust Discharge Product Dry '-.-,-Timer . Chamber In Chamber Out Rotor In Rotor . - :Out Operator 3 ys �.... TWSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS S 1 st Dryer Batch �y Fill Cycle Started @ . to;,-- .Dry Cycle Started @ I Discharge7Cyle Started Temperatures Time Discharge Exhaust Discharge Dry -.• °Timer. Chamber In Chamber Out Rotor -'In* . -_. ;" Out Operator �J / � ,PP,(�roduct "�� �� q 03 ( CJo4 , �L to. #6L 4,38, 41--11,6 3 t3 ,/ 44 Time Discharge Exhaust Discharge . Product- Dry , - ..,. Tmer - Chamber.Chamber In Out Rotor.` In'. ' . Rotor.. Out 'Op erator. 66 ems! a �3 q' b 2 57' 1 O0 q4� I i43 & - 65 c- DRYER OUTPUT % SOLI?s Dish Wgt Wet Sample + Dish Dried Sample +Dish rams rams rams(q�, C� �- D,y 73 y, 7Y a s?�3 I'D. rD (o 3 7�5 S x1oo= q ,/ / 7 % Total Solids 2/602 - Time Discharge Exhaust Discharge Product Dry Timer.. Chamber' In Chamber Out Rotor In' Rotor - :-Out ' Operator ��. 3 z. a • TWSA DRYER OPERATIONS DAILY RECORD DATE �e START STOP TOTAL RUN TIME, HRS LO =.3 `f 1 st Dryer Batch Fill Cycle Started @ ,' �3 Dry Cycle Started @ a �- Discharge Cycle Started @ l Temperatures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 0? 9 0 aa� 3 ( S-0 4y5Y 433 3AO cli 3 :)-3A �� 1,6 D )fIYS 4,3� DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Drie_d4Sampie + Dish (grams) .(grams) (grams) 1, 01 6 3 S 6 a 3 3- , s -33 �s 937,1) �2 &, 0 7 2- x 100 = (� % Total Solids 2nd Dryer Batch -' C Fill Cycle Started @ - Dry Cycle Started @ %) ; )4R Discharge Cycle Started @ Temperatures °F Time Discharge Exhaust Discharge Product Dry" Timer Chamber In Chamber Out Rotor - In Rotor Out Operator aa`? b e) 1p l� �23z ( —1 -155 S O T 60 43 94 - 3 35 : Cil 144,5 L� �3& 2445 2R? C�7�J agg g a -1163R 3 �73 E-'.o �3 A93 3 o,G- lb ? -q1 q L(. )-,/- �6 fc, � sjo DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) x100= 0 • y % Total Solids 2/6/12, 6/23/14 TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch f Fill Cycle Started @ -Dry Cycle Started @ :2 / Discharge Cycle Started @ Temperatures °F Disch D' Time arge Exhaust scharge Product Dry Timer Chamber In Chamber Out Rotor In ' T 7-7-7-- s S 2-9 1 / LI3 lyq/ 4(�(3 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) i ?70 ��, gy33T a4. Sa s'y= q. x100= Alarms or Comments ( d Rotor Out Operator �3q. _2% Total Solids /-� 14 P E TWSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS rn t :�,S 1 -5 a y 1 )0.9 1 st Dryer Batch Fill Cycle Started (nt9Dry Cycle Started @ -7"�5 Temneratures OF i•. Discharge Cycle Started @y D� . Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber. Out Rotor In Rotor Out Operator 7ra5' ;L65 a ()li, "C) 2S>3 eD �8 •` ,5 i Q 244 b 413 q '4'V- 16 32 55 0-I P- I Fs--'Sb -�-kq 22�'- 3 ly, 5 Z35 G60 I el®S. `� 41�5 q4 f -iI45 301 4L-1 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) a3V o e a S,..7 �-q(� x 100 = 96, y 9 Ifi °TTotal Solids 2nd Dryer Batch Fill Cycle Started @ /a-3 Dry Cycle Started @ L Discharge Cycle Started @ Temoeratures °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 1:a1 Q4 aa1 0 03 a6 Ji;5f )-59 ao 6-V W-4;. 434 4/166 3MO <EV 1�D 44) Z3/r 438 A4 La DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) 216/12, 6123/14 x 100 = qq-. % / ( (� 6 0-f, olids TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ ¢_ pry Cycle Started @ �� �c'% Discharge Cycle Started @�� Discharge Time Exhaust Discharge Product Dry Timer Temperatures °F Chamber Chamber In i Rotor Rotor � � � � �� � ��� Out In Out O erator Y y; 2 3 T S': z Li Z/1 z 33C/ J DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams). (grams) %,0 Sd a.2, IUD 0-l.sos7 4-,70 ( efa 9 5 �..... !/ �" 7" x100= a c %Total Solids Alarms or Comments E TWSA DRYER OPERATIONS DAILY RECORD DATE `7 — SL START STOP TOTAL U RUN TIME, HRS ' 3 q t5: oLk \E) q 6 1 st Dryer Batch Fill Cycle Started @ fi Dry Cycle Started @ Discharge Cycle Started @, b= )3 Temneratures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor_ . Out Operator bb •:5e Io /C)Q q#5 4f3j --S DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) 2nd Dryer Batch Fill Cycle Started @ d-3 x100= Dry Cycle Started @ Discharge Cycle Started @ J?7 Temoemftlres OF: Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator .4 9-.. ace �"� 43 A _ a23 AL 200 l tea( 7' ' aD �3 D 1445 q 38 ly4 3 7 0/- �d DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) 216/12, 6123/14 �t % Total Solids I W5A UNYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ _ Dry Cycle Started @ � Discharge Cycle Started @ Time Discharge Exhaust Discharge Product Dry Timer Temperatures OF Chamber Chamber In Out Rotor Rotor j b-5 In Out s O erat 3;Oy )-06 )w 3��. Y `-� 3 y y� �b,� z1/ y fc4i 3 y V VI 3sa -Z� ys 00 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams). (grams) 01 � x 100 % �� Total Solids Alarms or Comments z TWSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS U 1 st Dryer Batch Fill Cycle Started @ Lo ' iL( Dry Cycle Started @ �7 / (�- Discharge Cycle Started @� 5 : "51 Tamnarnfiiroc or: Time Discharge Exhaust Discharge Product Dry -Timer Chamber In Chamber Out Rotor In Rotor Out Operator P6� a r I qjk - `f33 41/,p 37 � 3 R -�-J45 37 3 asp 4,K5 4 Lobs 4 P DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) ( 6 ram/ % Total Solids 2nd Dryer Batch Fill Cycle Started @ , b LP Dry Cycle Started @ �.3 a' Discharge Cycle Started @ Temoemtures °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 0'3,5 615 a Q`7 9 - L(�33 sS /LOB 3 D5 J-o5 -4w 393 FJ DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) --)% 'Total Solids x 100 = 2/6/12, 6/23/14 TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ . ' Dry Cycle Started Discharge Cycle Started @ T=mnorn+tir=c 01= Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 90q a ®� �� �l L? 4.A3a a4 a 00 2 Lk 4 ao yC �a8l Lt4 4a 3. 3z 3,? u l00 %-5- yYs -37K j ` ayLAC) LcL� Li 30L L-i. 2-914 C5 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) I (grams). (grams) 6.57�� X goo = Q c�A- �).e l�}E " 2 `1, I / r �% c a r� Alarms or Comments t % Total Solids V TWSA DRYER OPERATIONS DAILY RECORD DATE ` H START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started @ . �5 Dry Cycle Started @ a Discharge Cycle Started @' o TemDeratares OF Time Discharge Exhaust Discharge Product Dry Timer .Chamber In Chamber Out Rotor In Rotor Out Operator T- -ate C�o 45 q 3a 1,9, 33 C 5 g - i lf�" 3 -L0,5- �3� 0. iFO Le D %S�f'`� �{ N DRYER OUTPUT % SOLIDS Dish .Wgt. Wet Sample + Dish Dried Sample + Dish (grams) .(grams) - (grams) y �a� 3 0,06 I a�q,1 �7 i x 100 = 9 oho Total Solids 2nd Dryer Batch Fill Cycle Started @ Dry Cycle Started-@ (0. Discharge Cycle Started @ Temperatures °F Time Discharge Exhaust Discharge' Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator rO c�> 4 405I Alm)a0 L c 1+4.5 9 Lf 0 �qL 3q 5 L\L�. I �t�l _ 394. aw (�-ko 61 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) rams,) ys 3a79� X100=91. Total Solids 2/6/12, 6/23/14 TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @. D -Dry Cycle Started @ cP �Od Temperatures °F Discharge Discharge Dry Chamber Chamber Time I Exhaust Product Timer In Out Discharge Cycle Started @ a 03 3� I` 43� Rotor Out Operator DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) ( r g ams). (grams) ---� x 100 = 9-3 773 Total Solids�'___, Alarms or Comments - TWSA. DRYER OPERATIONS DAILY RECORD DATE START RUN TIME, HRS STOP TOTAL 1 st Dryer Batch Fill Cycle Started @ �o " L40 Dry Cycle Started @ 7 ol4o Discharge Cycle Started @' TPmnArnftlrPs °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In ' Chamber Out Rotor In Rotor Out Operator r5 L C� S I D8 lbo �i y 3 L� 3 i L(49 3`3c D 5" 33 21 v 1 00 4 35,E _ �"P�s- DRYER OUTPUT % sOLIDs Dish Wgt . Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) oo >-o 91 x1O0= a % Total Solids 2nd Dryer Batch / Fill Cycle Started @ / Q �l a Dry Cycle Started @ Discharge Cycle Started @ TPrnnP_ratl irac 0;: Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator AD'AD7 5 ya as 4,35 ��- tr3� s0 4 - a 35 911 I D D J445 1-133 -Zl4s � 3 ev DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) yarns) acl, E/S( / s 7S x 100 �� %Total Solids 216/12, 6/23/14 TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ Dry Cycle Started @ Discharge Cycle Started @ Tamnaratrirac °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 5 ;�0 ';L D r7 0 4 33 Lit9 'q 3.3 :258 -S a o '_7 50 ((I a 1 H )- l 9 19. 350 3 L 3 3 3 �Z yys L3 62 22 2I7 3&l SCE �i`�s �f y/ `� 3 r�/ z 3 b� 3L 3- 15-1 V YY yV3 V `f 3 _. - DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams). (grams) y 670 %O72 17.0? d S-7 x100= / %Total Solids TWSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL } RUN TIME, HRS . 1st Dryer Batch F r i c Fill Cycle Started @ ` Dry Cycle Started @ , i Discharge Cycle Started @ 5 S • Tamnarnhirae PP • Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator ac)P * 5 v 5b :' ,, 1 01 C)r� C� t) Q 6� Lo L4 \ LA L I C4 l c1 i 1 - f J DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) - .(grams) (grams) v3`7 30, x�oo= sotals `�olids 2nd Dryer Batch Fill.Cycle Started @ O O rp Dry Cycle Started @ \L ?j Discharge Cycle Started @ T=mnarntf irce 017 Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator �-33 l o o. o . cl I 1305 t 5'5 4c, 3 qc-( DRYER OUTPUT % SOLIDS I Dish Wgt I Wet Sample + Dish 2/6/12, 6/23/14 0 - )_ 6, � V3- u � 19(P_ �qS� �� ✓ a l ; �._ x , of Sample + Dish rams) ©/ % Total Solids TWSA UKYER UPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ Dry Cycle Started @ Discharge Cycle Started @ I Temperatures °F -- Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 1 ', q q D Li 3 2_1 aAJ ca `(`fS 36.Ll y; 2- 3 C)s L�ys DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) b % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE / ij Z START STOP TOTAL RUN TIME, HRS ; s 1st Dryer Batch r• fi Fill Cycle Started @ `:53 Dry Cycle Started @ `� 3 Discharge Cycle Started @ J J Temnc­4­r - 0C Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In _Rotor Out Operator 2 3 �vV a 03 `-(v 3 �� 110 C� v 3 2 07 Z )_ 16 ® 3 PI 2- 13 0 14,15 439 LN1571- 3os s� � " f4 F-2.35d DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) 3 qr& 90 <c % Total Solids 2nd Dryer Batch Fill Cycle Started @ M Dry Cycle Started @ Discharge Cycle Started @_ Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 11 :3 aqa �u v� � 3 � CD J a� O`ere- DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish, (grams) (grams) rams) �.i07s x1oo= Qr� / T5 % Total Solids . 2/6/12, 6/23/14 I VVSA UKYtK UNLKA 1 IUIVS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ 4� a Dry Cycle Started @ Discharge Cycle Started @ Temperatures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out O erator s� 1 q 6��a aye D C� LAL 5 36 Lly L44C) Lilly 3(8a DC) 0 -1'-i 5 Y i H IM DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish I Dried Sample + Dish (grams) (grams) (grams) -- �� x 100 = �3 % Total Solids. Alarms or Comments TNSA DRYER OPERATIONS DAILY RECORD DATE START RUN TIME, HRS STOP TOTAL 1st Dryer Batch Fill Cycle Started Dry Cycle Started @ Discharge Cycle.Started @- �P Ta...�.,.-....L.. .. Oc' Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 7. ;aZ 3 ads ill I ��{ e4 7 co DRYER.OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) o 9 9'7 y aL � (9 t I\ a. 5: ,5 d o x1oo= c9 `7 11 % Total Solids 2nd Dryer Batch /� p Fill Cycle Started @ U - -� DryCycle Started @ Discharge Cycle Started @ Tcmnoro+sir- ' OC Time Discharge Exhaust Discharge Dry Timer •r- Chamber In Chamber Out Rotor In Rotor Out Operator **Product 0 A? 4f C • / [' �� / • ( V�V C efi • DRYER,OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) rams) ioD3-Ta(ey adr9 s_ _- x100= q %7oora olds . 2/6/'12, 6/23H4 TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ 4 "t Dry Cycle Started @-=�-I-- Discharge Cycle Started @ Temperatures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator L( L( 39 3', LA4,5 q 3 3 q L� 5 65.9 -3 _w �'•), 13v 3D - P5. 1�q �A\ 'A Lk 3-1 'A DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) 1-7 x100= q % Total Solids Alarms or Comments E TWSA DRYER OPERATIONS DAILY RECORD DATE — `_"% i L4 START RUN TIME, HRS STOP TOTAL 1 st Dryer Batch R, Fill Cycle Started @ Dry Cycle Started @ �. " f -Discharge Cycle Started @ 9="5-3 Tomner,4---, OC Time Discharge Discharge Exhaust Product Dry Timer r- Chamber In. Chamber Out Rotor In Rotor Out Operator Z - j �7 c)- D ? aQ�?- Q �/)19 7)13 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) q 7 4;, x 100 = % Total Solids 2nd Dryer Batch Fill Cycle Started @ 3 Dry Cycle Started @ V: Discharge Cycle Started @ Tnm--+-r oC Time Discharge Exhaust Discharge Product Dry Timer Chamber in Chamber Out Rotor In Rotor Out Operator auR D ._ f t QS- L�� 1rw =� A Aq, ao S' qqq 431 141q� :C DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish — (grams) (grams) rams) liOtIl 2--(o,2033 f x100= 14-6li, % `rnfal �nliric 2/6/12, 6/23114 TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ ` -Dry Cycle Started @ Discharge Cycle Started @ 44 3�9,► `u lamed ca.r TPmnernfFirPc °P - Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator04 o 41A 14 2kb q 2, -7 1-f 3a qq,-ki 33 c 'All 3 0 c)q 15 Lk �4 q Ls 3 �OA L\ . 380 L� u ,�_D H LA 1 L� C-r LA1t 3 j019' /") DRYER OUTPUT % SOLIDS 'Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams)) 1. 0 2-9 L 5 2 to, 3 Co G- 5 1�t ql 3? l l `� 3�`73 x1oo= o /o Total Solids Alarms or Comments E 17, TWSA DRYER OPERATIONS DAILY RECORD DATE t� (� % L4 START RUN TIME, HRS STOP 1 st Dryer Batch Fill Cycle Started @ J % DryCycle Started @ 3 i Tamrnarnhir=e Of: TOTAL Discharge Cycle Started @ Time Discharge Exhaust' Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator r �4 3 3 :2- b s 1-1,Y-5 43D z4 3�3 ED 1"S 23 MI6 J 0 o yys V33 yY_5- 3�6 0. /A 3C)6 y,5 At s 3 E DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) ( rams) 5 3 a x 100 = 9 5/ 7% Total Solids 2nd Dryer Batch )) ,,11 31 Vv- Fill Cycle Started @ ! U ' Dry Cycle Started @ D` Discharge Cycle Started @ Tamnarati ircc OC' Time Discharge Exhaust Discharge Product Dry Timer Chamber . In Chamber Out Rotor In Rotor Out Operator E D 414s Z�3 / `7� :3 : -3 I b a 1414 3y 3 l®174q3 mot' 'f. 3 3 97 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams)(grams) 7. 3R -7 9 ag. 7q-.77 x100= / % Total Solids 216/12, 6/23/14 VVJH UKYtK UPERATIONS DAILY RECORD 3rd Dryer Batch j Fill Cycle Started @ `? Dry Cycle Started @ } Discharge Cycle Started @ J ( 0 — r= TcmnernF...rn.. Oc — Time Discharge Exhaust Discharge Product Dry Timer •r- Chamber In Chamber Out Rotor In Rotor Out Operator =l a(5�11 10 j q �� �?,_q3 E-*r0 a a a 0-� (A cC L( 31 ti Lj t0 .�) 2 2 . . Z-; S Z o 00 H 3 Z Cjq ._�_? •1-�,� LI: `�9 14LA J / v �c 3 (o `MCP 5 b5 1-7) ti 3 3� 0 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) I,c� I i2 3i .0 i oU J V3/i vv l q1.��� g x oa = 73 ` t" % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD C DATE -I ` I q START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started @ L-P 1 Dry Cycle Started @ 7- 2, h Discharge Cycle Started @' 0,3 Temoeratures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor . In Rotor Out Operator v C? lop c�, 5D ')f 933 4 3g -/44-,j" 310� 0-9 63 ;�G p &,3 '/q5 -4qI I 39A �f/ DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish I Dried Sample + Dish (grams) .(grams) (grams) i3OOoG �41V `l l b 1 x 100 % Total Solids 2nd Dryer Batch Fill Cycle Started @ l Dry Cycle Started @ �•� Discharge Cycle Started @ -� 33 Temoeratures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator P-3 ,� 9.a9 _ -q4,5 .413A ---�,5— 3i 6-,D 2- D 13 W6,- 3 S 8 ;)L 91� 36. & 4 44< zy�Zrl,6 3�,3 C- DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (9 rams) (grams) (grams) �L 5� x100= cI %Total Solids 216112, 6/23/14 i vvoH UKyt:N UIJI=HATIOIVS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ D Cycle Started ' f . Dry Y @ _Q_ 1� Discharge Cycle Started @ �j -33VI TPmnomftirnc °C Time l,5 3105 C 5� Li b% ITO Discharge I Exhaust 1 P Q 3 I Discharge ' Product aD-� IC> 1 Dry Timer . —� 15 1Do 1(0 3 Chamber In q l L j 'A 44 '�LAb Chamber Out �i 3c� 'A�a C- 30i L L[ I Rotor In �4 -( � LjL_�S Lc (4 tp LAIA 2 Rotor Out Operator 3Cf 3R _ DRYER OUTPUT % SOLIDS Dish Wgt (grams) �g.353 Wet Sample + Dish (grams). Dried Sample + Dish (grams) ��.3 j r` ash 30, �35 C� -, 51 x 100 = gs j d % Total Solids Alarms or Comments • TWSA DRYER OPERATIONS DAILY RECORD DATE & _ r START r STOP TOTAL RUN TIME, HRS J •'D & 1st Dryer Batch Fill Cycle Started @ .5`7 Dry Cycle Started @ % i ), y Discharge Cycle Started @ 00-D Temperatures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator -)ag Z06 vo3 3-) 3 S, )Z d 6 off' 6-D 443 Cf-D -114 ( a a ) 0-0 '/ 433 3/o �f 160 "-4q6 J4L5'- 3 g 1 3 - 5 4,�5 I `f 4 ( . `f4 39-�' 1 C J) DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) -(grams) (grams) O,-79q ZL(, 3-7 3 5 3 (-�?3 136 x1oo= a 3_'� 5 � � I % Total Solids 2nd Dryer Batch � Fill Cycle Started @ Dry Cycle Started @ / = vc�(� Discharge Cycle Started @ 7 , Temperatures °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator l ��v vL:r a os 41J a38 -'3 23 D 1� aqq& 432 -246 3y6-19 66), q� T 705 A(i� DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) rams) -72,0$ 3, 216112, 6/23114 r1r196 x100= %Total Solids VVOH UKTtK UNtKA I IUN8 DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ � -Dry Cycle Started @ ' A a Discharge Cycle Started @ O� 3 12�w Temperatures °F t Discharge Time Exhaust a)) a0� i Discharge Product c a6 1 Dry =Imn TimerOut 13 (f Cf Chamber 31� Rotor In 13 Rotor Out � Operator `1 z3 3 Li 5�. �� a 30 445 �o �`kS q39 ��1 31� v DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams)(grams) / 3 9 -393 � 9 S �G 5� x�oo= a o /o `� Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD. DATE / 0 —,--A L START STOP TOTAL { RUN TIME, HRS 1 st Dryer Batch rr j. Fill Cycle Started @ Dry Cycle Started @ Discharge Cycle Started @' Temperatures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator Inn l� U1 ' II / 5 0 (c./ t 3 CW, 43 C0 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) x x100= G 1�p - 9q % Total Solids 2nd Dryer Batch Fill Cycle Started @ Dry Cycle Started @ IP Discharge Cycle Started @ Temperatures °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 1 I D (� �r� D 385 (,,5fe 9,9, c .D 5D 44`7 /-(3! Ll 934 9 DD DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) rams) 3-3,9 oZ (e �4- i, % Total Solids 216112, 6/23/14 i V V�� vIN I LIB vrCfCP1I IUIVJ DAILY RECORD. 3rd Dryer Batch Fill Cycle Started @"3 -Dry Cycle Started @ �'�'-� ii Discharge Cycle Started @ 5 ;4U Temperatures °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator Li Z_ 14(4 3� 5 4, zov`�3 (_v -( 3 -3 S 5, L\ 0 z 18i0 'ju -72 L[ 3G �f `f (A 0'i 5 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish I Dried Sample + Dish (grams) (grams) (grams) iIc,03s 31 W t 9,87,)6 mod: i�f x1oo= Spy% Alarms or Comments 1j . �f �b0��7� % Total Solids TWSA DRYER OPERATIONS DAILY RECORD DATE /v!' . t START STOP TOTAL RUN TIME, HRS %37 1 st Dryer Batch Fill Started Cycle -� y @ Dry Cycle Started @ `/ Discharge Cycle Started @ D `% Temneraftlres OF Time Discharge Exhaust Discharge. Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator c � '12 273 9�43 %60 4V,51 _z19 D'D7 q �3 1 3b - '7 i 4�5 I 14 r 3 9 4 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) r,bz-y 3i,cAS7 .d � a g-d3_Q S-6Vo7 '?7 C� � x 100 = M o Total Solids 2nd Dryer Batch g Fill Cycle Started @ 7 Dry Cycle Started @ l Discharge Cycle Started @ 1. 3 Temperatures °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator "'39 J33 as 4� q 44 3a )',oM a3 a 3 2 CO DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish I Dried Sample + Dish (grams) (grams) (grams) '7, v976 v J &D `ti r x 100 = n % Total Solids 2/6/12, 6/23/14 I vvaH UMT 1=K UNtKA I IUNS DAILY RECORD 3rd Dryer Batch /� Fill Cycle Started @ _1 / Dry Cycle Started @101, . I V) Discharge Cycle Started @ C31 0 Temperatures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator ©� a���`1 33 �I'D LA45, 41-f 13 W-f z DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) 1,D17o 33; -L 7 �a a �3 x100= Alarms or Comments il) 606. lids TWSA DRYER OPERATIONS DAILY RECORD r DATE / Q -,,Z7� — START STOP TOTAL RUN TIME, HRS d- 1 st Dryer Batch Fill Cycle Started @ UP Ir F C Dry Cycle Started @ �•coi Discharge Cycle Started @ %J Tamnarnfllrac Or: Time Discharge Exhaust Discharge Product Dry Timer Chamber In ' Chamber Out Rotor In Rotor Out Operator `Z.-' J 3 62-) 3 YJ 462) 3Y' . 1 3 6 961 S--O 6" A13a JA4, 9,04 3 '" c o d L)45 33 <<� i X71 c9,9�' 15o 414s -440 445 Z7 4, 2)b's-1 - M 14 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) 26 , 3 C,%-Total x100Solids 2nd Dryer Batch C Fill Cycle Started @ U Dry Cycle Started @ Discharge Cycle Started @ 5? �T mnarntiirac �� Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator Dal au-7 d 4z6r 07 "N5 37�, �fB ` laq 163 qqz� -44 44,5 C DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish I Dried Sample + Dish (gramms) rams) rams) � x 100 216/12, 6/23/14 % Total Solids I VVSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @— Dry Cycle Started @ ` �� Discharge Cycle Started @ r� Temoeratures °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator Z v Z, Lo C7 o(� 3 L((D(0 Al� 5� 13l S' 3 � 3a 1O 1Eb L195 L�35 H95 '� �`� 31 3 1(� �3S wr) 3 o DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) I,o13(0 C-tBZ� .-Ell +1�io d6 c x100= % Total Solids Alarms or Comments nn �" n.l •SCyI qi..e. rs d u nG?,r'• Y TWSA DRYER OPERATIONS DAILY RECORD • DATE START STOP RUN TIME, HRS Lo- �-i , ,N TOTAL 1st Dryer Batch Fill Cycle Started @ V & Dry Cycle Started @ Discharge Cycle Started Time Discharge Exhaust Discharge Product Dry Timer Chamber _ In ' Chamber Out Rotor In Rotor Out Operator Aab q D-i)O �2g�- 3? 0�� '23a 19 a , 0 445 qd, tic1611) 14'3 DRYER OUTPUT % SOLIDS Dish'Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) i,v Zt�i .3 3 o9.3�3 - A9, D ZD.vd('3 x100= 9q-37--1 :D- % Total Solids 2nd Dryer Batch j Fill Cycle Started @ Dry Cycle Started @ % Discharge Cycle Started @ 0C Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 46 i , q6� C LI 4D - a� 14 �5- 64) =.3 � iQp �5 a g45- 37 Y 'c n 3U5 .'-J45 )41q ---7'- //- � 39 r DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish ® (grams) (grams) (grams) b, 92 33 - 3a.i`713 3(.gg(D-- 2/6/12, 6/23/14 x1oo= 94.63('7 & 04° % Total Solids TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @--�- '— -Dry Cycle Started @ L3 Discharge Cycle Started @ 1 33 TPmnaratiirac OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out O erator 34/ tit DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) �.Z/ %S g / �. /� I �— % Total Solids Alarms or Comments LIre n �� �' ��M�2 'j `M P_ki, t TWSA DRYER OPERATIONS DAILY RECORD DATE J 1 -" 1 q START RUN TIME, HRS STOP TOTAL 1 st Dryer Batch Fill Cycle Started ' Y @ Dry Cycle Started @ , 1 Discharge Cycle Started Temnarnftirac °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor Rotor In Out Operator a a r0i 65' -5�0 (off ,'q:3 /6Z_0 �4;) 4,37 J4 4� 3� f �. DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) -(grams) (grams) I� �DSl 3 O-HLt7-1 9, x100= 2nd Dryer Batch Fill Cycle Started @ �j Dry Cycle Started @ �= TemnPratiirac 0P 9�, a q-/-I 99, D -D D- % Total Solids Discharge Cycle Started @ - 9 _ Time Discharge Exhaust Discharge Product Dry Timer Chamber I In vChamber Out Rotor In Rotor Out Operator "10 alb U 301 3-/9 39' as f` '. al:2-9 b° 5D zllf #33 Yq o 4 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish I Dried Sample + Dish (grams) (grams) rams) 1,02ul 3Z, (,_NL _S7 - �v. a3(d x100= 216112, 6/23/14 6 5 v3 % Total Solids I VV5A UKYtK UI'tKA 1 IUNS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ Dry Cycle Started @ Discharge Cycle Started @ y Ti=mnarPfiirac'P Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator L[ 0 z -Y z 39 ),a LAH L 3 3 L\1A 5 �� DH '239 ac)u )bo 44:5- Li3I q45 3-7.3 5 1� a, aIq lSv - 5 4 3 5 , LA 'Z I DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams). (grams) i,o2-7S 31,7197 3a. �6�3 �j 3335 3o. 6'r9 (�6) x100= 99,57q Alarms or Comments cl.4 r.3 L,J Q_ �1 - fl �� % Total Solids .TWSA DRYER OPERATIONS DAILY RECORD DATE [•-0019 RUN TIME, HRS TOTAL 1st Dryer Batch Fill Cycle Started @ (g, q Dry Cycle Started @ J 43' Discharge Cycle Started @' TamnarnfFm=Q OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator :lg a�(D �5 f 3, 1 a v q45 :3A �f/ DRYER OUTPUT % SOLIDS Dish. Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) . x100= 9,73/3(l 2nd Dryer Batch j �y Fill Cycle Started @ I 9" 3 p� ST Total Dry Cycle Started @_ Discharge -Cycle Started @ Tamnaratiirac 0F: Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator D: �t_ o A�o l 4v a 3 A cqlD 433 S�OICI) 3 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) :3a,v RLP7 30. 9��� 216112, 6/23114 x100= "I.D83/ V % Total Solids I W5A DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ Dry Cycle Started @�� �' Discharge Cycle Started @ Z Or Time Discharge Exhaust Discharge Product Dry Timer r- Chamber In Chamber Out Rotor In Rotor Out Operator i� 2 Zo 3 7 �r �1 �� 4 q-7 315 � C4 �c S 3 � 3C to DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) �v -�ss�j x1oo= i�.a�� Total Solids Alarms or Comments !� D r;q APay % {�- J E = ST. RUN TIME, HRS r' TWSA DRYER OPERATIONS 1DAILY RECORD DATE STOP 1"4 If -all 1st Dryer Batch Fill Cycle Started @ Dry Cycle Started @ %r�J Discharge Cycle Started @i 01 /A Timm nPratrirPc °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 0 31K -e r �e(C ��� 1c7� 4. c�/ `4 T 5 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample '+ Dish Dried Sample + Dish (grams) .(grams) (grams) 1 3 L�,)( I b --T-3o x 100 = (^ /a % Total Solids 2nd Dryer Batch Fill Cycle Started @ �; +�''Z Dry. Cycle Started @ / t�= J Discharge Cycle Started @1 TPmneraturaG °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator �If C � 2 0 q"-I 1f33 4 7q t7�� o e✓ -3 1 a O 3A- IYgb 373 c- 5� 7o� DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish (grams) (grams) t 06-� o 3 u ,I gc� z7a'—�� 2/6/12, 6/23/14 Dried Sample + Dish _ (grams) xloo—,:�`y I v 9_�i,r% Total Solids ,N TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ D b Dry Cycle Started @ - 33� Discharge Cycle Started @ 4 ` 1_ 5 T__ ..t. Or Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 3� �[ rZS SO C� �(Y �ZU 4) DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) i,vz3 32,3.5y'I = Jrl- ce x1oo= otal Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE ( (- 1 '7 -1 4 START STOP.... TOTAL RUN TIME, HRS `3� �• �� l 1 st Dryer Batch ` Fill Cycle Started � ` � � ' Y @ Dry Cycle Started @ % "Z 7 Discharge Cycle Started Time Discharge Exhaust Discharge Product Dry Timer Temperatures OF Chamber Chamber In Out Rotor In Rotor _ .-2. vL/ Out Operator o A/ 1� 601 VV'S 3 w -7/-- DRYER OUTPUT % SOLIDS I Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams). .(grams) (grams) 56, -37iaq x100= ?0,((4-7 %Total Solids 2nd Dryer Batch Fill Cycle Started @ W ; .3 Dry Cycle Started @ I Discharge Cycle Started @ 7n— res °F DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample +Dish Dried Sample + Dish (gram - s) (grams) ( rams) x100= qs, 9 '7�s 216/12, 6/23/14 /o Total SOIIdS UHILY NLUUKU 3rd Dryer Batch Fill Cycle Started @ �, -Dry Cycle Started @ Discharge Cycle Started @ (�� �.0 8 Temperatures °F Discharge Time Exhaust Discharge Product Dry Timer Chamber In ChamberPRotor Out Rotor Out O erator �0 Zz3'. 53 _ ° , C45 Lf 5( 3oo 5 s a b 1 `f 11 l J� A (4 S Y-f - r 0• DRYER OUTPUT % soLIDs Dish Wgt Wet Sample + Dish Dried Sample + Dish —� (grams) (grams) (gramt:�: 1.C>LI�r� % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS To o ' 1 st Dryer Batch T� Fill Cycle Started @ �J ] Dry Cycle Started @ Discharge Cycle Started @ Temperatures OF DRYER OUTPUT % SOLIDS I Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) Total Solids 2nd Dryer Batch Fill Cycle Started @ Dry Cycle Started @ { L 5 6' Discharge Cycle Started @ ® Temperatures OF Time Discharge Exhaust Discharge Product Dry Chamber Timer In Chamber Out Rotor In Rotor Out Operator a :4 �-3 C EO 3 P3(o )I)o 4qb 1-133 :C :J1Lo n V J50 Z�,�A j 3 ; S ��( L I-(�( I 4. �o Ca DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (g rams`)) (grams) (grams) !�\\ (� ai/ -5/ J` DVf, 2/6n2, 6123/14 �� % % Total Solids DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ I -Dry Cycle Started @ 3 3 —f Discharge Cycle Started @ Temperatures OF (— Discharge Discharge Dry Chamber Chamber Rotor Rotor Na�� Exhaust Product Timer In Out In Out O erator a o H ai(j 0 3c��� Sul 3 i�� aa.-1 CA aQ6 5(). q_-) Nz a � ov a �t 5 `50 L `4`45 ��Cp � V DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) C) D L D Sl a-0 aL r x 100 = �, �� 3 % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD 0 RUN TIME, HRS DATE START STOP TOTAL E: rc)� 1st Dryer Batch I Fill Cycle Started @ - I Dry Cycle Started @ 1 Discharge Cycle Started g Temperatures OF DRYER OUTPUT % SOLIDS I Dish Wgt I Wet Sample + Dish I Dried Sample + Dish I l,u(3�I 33,ciSim3 3 � s (s � X,00- 5 /o Total Solids 2nd Dryer Batch � II Fill Cycle Started @ U' = Dry Cycle Started- @ l..d Discharge Cycle Started @ ' 63 Temperatures OF DRYER OUTPUT %SOLIDS I Dish Wgtj Wet Sample +Dish Dried Sample +Dish (grams) (arams) (nr�rncl I � , 0 Sg� 13 H , � —105 I � � () -7 a x100= 9� 2J6/12, 6/23114 L S ° % Total Solids -11 . � I INL_%, V I\V 3rd Dryer Batch Fill Cycle Started @ ` l -Dry Cycle Started @_ Discharge Cycle Started @ �- Timm nerafirirac "P Time Discharge Exhaust Discharge Product Dry Timer ...r -. _._. Chamber In -- Chamber Out Rotor In Rotor Out Operator 3 ; � Li45 1 L+3S 1445 j a a 9 a s /00 114q C) 0 305 1 7C� �i9 4Q ( 4 Ct -� 17 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) 5 x1oo= r % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE L� _ 1 - RUN TIME, HRS - "'START : 5 -7 STOP ..- TOTAL 1 st Dryer Batch Fill Cycle Started @ T Dry Cycle Started @ 1,35 Discharge Cycle Started Temperatures OF Discharge Time Exhaust Discharge Product Dry Timer Chamber Chamater In Ouperator 44� 6 143 )JI 3dS DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) . C' off, x 100 = 9 S�. S` S cF � °r'T-otai-Solids 2nd.Dryer Batch Fill Cycle Started @ 3 Dry Cycle Started @ v2� Discharge Cycle Started @ , Temperatures OF Discharge Time Exhaust Discharge Product Dry Timer Chamber Chamber In Out Rotor Rotor In Out Operator J�' fib . a� ,3 32. 4// . OS' c;LM 9-bb ova 433 44, 3�.5 Lfoi DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) i,obZta rams) (grams) 3 9, 0 s, 9 d.G/3 j x100= ( 7o TOtai SOIIdS 2/6/12, 6/23/14 -rvL I f`CIIUMU 3rd Dryer Batch Fill Cycle Started @c2 -Dry Cycle Started @ «' Discharge Cycle Started @ ` Temperatures °F Discharge Discharge Dry Chamber Chamber Rotor Rotor Time Exhaust Product Timer In Out In Out O erator q b -7 a a -1 5 H i Q 3Q 5 /.s C) Iq S DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) x 100 .7 `� ' 7 q�• %G % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS 1st Dryer Batch Fill Cycle Started @ Dry Cycle Started @ 7.` % Discharge Cycle Started (g" Temperatures °F Discharge Discharge Time Exhaust Product Dry Chamber Timer In Chamber Out Out Operator ell 1 g jVBoa jRctorRitor �� Y, 3L 7y A34 T_cM 16-o )4 Lf 6 z4 q4 b tal - 3 o 5• S If 4q 5 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) .(grams) (grams) x 100 % Total Solids 2nd Dryer Batch p� Fill Cycle Started @ U :3 A Dry Cycle Started @ Discharge Cycle Started @ 40 Temperatures °F a ischarge Product Dry Chamber Timer In Chamber Rotor Out In Rotor Out Operator 00a o JAB �14� '133. -44�� �3�� DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) �L3.10q-3 3 x 100 = --G� --_------- % Total Solids 2/e/12, 5/23/14 DAILY RECORD ` 3rd Dryer Batch Fill Cycle Started @ :1 7 Dry Cycle Started @ 1� Discharge Cycle Started @ Temperatures OF Rotor Time Discharge Exhaust Discharge I Product Dry Timer Chamber Chamber In Out Rotor r7''O aV %�v, r G'V E �`�' 3(V In / I �V Out O erator 435 3� DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) I. 005 ?9, x100= 9�'73� o ,, /o Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE -- (7 -- _ p START STOP TOTAL RUN TIME, HRS c €� 1 st Dryer Batch Fill Cycle Started @ p Jam' Dry Cycle Started @ Discharge Cycle Started Temoeratures OF Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator 7'A ); a t.15 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish I Dried Sample + Dish (grams) _(grams) (grams) 274 a s- ?O 5� x 100 = `a % Total Solids 2nd Dryer Batch Fill Cycle Started @ � Dry Cycle Started @ I l = I Discharge Cycle Started @ (O Temperatures °F Time Discharge _Exhaust Discharge. Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator -7 4io aqa t .S a 3- Ob 111,60 1-f4S # 3 S 4it�) D� 3S�a 3 305 I-S"? 14*6 �*/ �,� DRYER OUTPUT % SOLIDS Dish Wgt Wet ample '+ Dish Dried Sample +A (grams) (grams) (grams) 1,t>)"V �i ?�32 x100 2/6/12, 6/23/14 3��7k ��L = l �' L, � a % Total Solids DAILY RECORD 3rd Dryer Batch Fill Cycle Started ` @_ Dry Cycle Started @ J � , (.� Discharge Cycle Started @ Temperatures OF DRYER OUTPUT % SOLIDS % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE ;L — S �- START STOP t, RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started @ co- S Time Exhaust Product %3 0 TOTAL Dry Cycle Started @ _ ` Discharge Cycle Started @ 0�: Temperatures OF Dry Chamber Chambe*Rotor Timer In Out Rotor Out Operator 5'76 !0; 4 v 4-6 DRYER OUTPUT %a SOLIDS Dish Wgt Wet Sample + Dish (grams). .(grams) 3D. 73 & Dried Sample + Dish (grams) x 100 = 9 % Total Solids 2nd Dryer Batch r� Fill Cycle Started @ 0 ' 5D Dry Cycle Started @ Discharge Cycle Started @ 'Temperatures' OF Time Discharge Exhaust Discharge Product Dry Chamber Time In ChamberW.Ro Outator � d a-5 a I d-, .. a �� O,6 If 14,35 �� 2 J' )sv ` `f ;�` DRYER OUTPUT % SOLIDS Wgt i Wet Sample '+ Dish Dried Sample + Dish ms) (grams) (grams) sD•4k7CP0 x100= �--- �• 2 d % 6 % Total Solids 2/6/12, 6/23/14 9 �"L_ I Mic:UUMU 3rd Dryer Batch Fill Cycle Started @ �!.:. J` C' -Dry Cycle Started @ 2) + Discharge Cycle Started @ (4 -c-f3 Temperatures°F Rotor Time Discharge Exhaust Discharge Product Dry Timer Chamber Chamber In Out Rotor �, � ace add ii �a5 In 3° -7 Out O erator 3-)9 ,.. `�Cr, Sc�5 LA �S`{ 3�13 5� 39 �E `D 14 �b4��1 r, - DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) ::::� 97, 3a•r37 x100= % Total Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD DATE START STOP TOTAL RUN TIME, HRS LZ 3 1st Dryer Batch Fill Cycle Started (0: b ' .` Y @ Dry Cycle Started @ � Discharge Cycle Started @ Temperatures °F Discharge Discharge Dry Chamber Chamber Rotor Rotor Time Exhaust Product Timer In Out In Out �peratorOperator D4-0, 1'� 0- a 0- J43 1 49 4,-�q je;��& 1 ."' E � 13 6 D .� ,Q,5 �t351" �l S 3 Ei DRYER OUTPUT % soLIDS Dish Wgt Wet Sample + Dish Dried Sample +Dish (grams) .(grams) (grams) ��-- 9j • % Total Solids 2nd Dryer Batch Fill Cycle Started @ %q,p Dry Cycle Started @ :;. Discharge Cycle Started @ -Q. ?39 Time Discharge Exhaust Discharge Product Dry Timer Chamber Chamber In Out Rotor In Rotor Out Operatort; -3 D 6 L) 43 4,54(,, -,3-71 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (grams) 23%8��c� 5 J (P.� a7.566V- 216/12, 6/23/14 x100=--....... % Total Solids t ✓rUL 1 UNZL Uf %U 3rd Dryer Batch Fill Cycle Started @ � Lj 9 -Dry Cycle Started @ ' "24 Discharge Cycle Started @ (o �� 3C) Temperatures- °F Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor D -3 �� ��' 3R Out Operator i ` ' D Lt l­�q If 5.5'� � ► �{ i rb D Li '� � y S 1-3 t� 36 l c LA 4 q 3 2 (4 4 C) -2 DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish Dried Sample + Dish (grams) (grams) (gramt 5�o � x goo = 9� •l % N � %Total Solids Alarms or Comments TWSA DRYER. OPERATIONS- , DAILY RECORD DATE l,2 - / !. START STOP TOTAL RUN TIME, HRS 1 st Dryer Batch Fill Cycle Started @ f l Dry Cycle Started @%' % Discharge Cycle Started @ TAmn,Arat„ra-R Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Op erator ` DRYER OUTPUT % SOLID Dish Wgt Wet Sample + Dish Dried Sample + Dish rams (grams) rams 0;9375. 32, ?Sob x 100 = i5c .. % Total Solids 2nd Dryer Batch Fill. Cycle Started @ 3 : Dry Cycle Started @ r" + ! Discharge Cycle Started @ , Tem eratures . Discharge_ Discharge .Dry . Chamber, Time Exhaust Product Timer In Chamber. Out - Rotor . In - Rotor Out O erator 38 ?� C DRYER OUTPUT % SC > Dish Wgt Wet Sample + Dish. Dried Sample + Dish rams rams rams 1,o7-4-� 3q,Li3Ig 3� U� f x100= Total Solids .2J5V2 TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started @ i ; w Dry Cycle. Started @ 3_� 5_ Discharge Cycle Started. @ Temperatures Discharge Discharge Dry Chamber Chamber Rotor Rotor Time Exhaust Product Timer . In Out In Out O erator ` o - Do 77 2_v 5 U DRYER oUT-Pu T % SOLID . Dish 1Ngt . -Wet Sample.+ Dish ' Dried Sample + Dish rams rams rams 0.9 -X 100:= Solids Alarms or Comments TWSA DRYER OPERATIONS DAILY RECORD 1, DATE START STOP TOTAL RUN TIME, HRS . 7 15. 0 ° I.A. 1 st Dryer Batch Fill Cycle Started @ ,�-� Dry Cycle Started @ CID Discharge Cycle Started @ Tem eratures Time Discharge Exhaust Discharge Product Dry Timer Chamber In Chamber Out Rotor In Rotor Out Operator Lp 7 y� Ylv,� DRYER OUTPUT % SOLiD8 Dried Sample + Dish ., Dish Wgt Wet Sample + Dish rams rams rams - ... p,ct 9 Z� - �Ja �/ D. �,2 1. x100= n I _ % Total Solids 2nd Dryer Batch : : 2 Fill. Cycle Started @ (� : 3 u: Dry. Cycle Started @ _(� `��% Discharge Cycle Started @- ` TS Temperatures . Discharge Discharge Dry Chamber. Time Exhaust Product Timer In Chamber Out - Rotor In Rotor Out .:. Operator D`� �. O 6 YV 6 -�36 Y `/ YY Lfu _4aa H145 Lt.35 c4c'5 5- DRYER OUTPUT % SOLIDS Dish Wgt Wet Sample + Dish. Dried. Sample + Dish _ rams rams rams c� x 100 = % Total Solids 21E/12 C� TWSA DRYER OPERATIONS DAILY RECORD 3rd Dryer Batch Fill Cycle Started ` L , @ Dry Cycle. Started @ �- Discharge Cycle Started. @ Temperatures Alarms or Comments