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HomeMy WebLinkAboutWQ0004893_Residual Annual Report 2014_20150219�� o 60 Z, 7 CAMPBELL SOUP SUPPLY COMPANY, LLC LAN® APPLICATION ANNUAL REPORT 2014 PERMIT #WQ0004693 2120 NC 71 Highway North 3iE' Maxton, NC 28364 February 16, 2015 North Carolina Department of Environment and Natural Resources Aquifer Protection Section 1617 Mail Service Center Raleigh, NC 27699-1617 Reference: 2014 Land Application Annual Report Campbell Soup Supply Company Maxton, North Carolina Permit No. WQ0004893 Information Processing Unit: Enclosed Campbell Soup Supply Company is submitting all monitoring and reporting mo information as required in the referenced permit'for the facility in Maxton, North Carolina. This report includes: 1) Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual Land Application Field Summary Form, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen and Vector Attraction Form, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data, 10) 2014 Application Summary Table, and 11) Application Condition Summaries. This is a non-503 permit that is not required to have pathogen reduction or vector attraction reduction requirements to be met. A total of 686,740 gallons (89.9357 dry tons) of industrial residuals were land applied to 56.8 acres. If any further information is required regarding this land application program, please do not hesitate to contact me at (910) 844-1654. Sincerely, amie C. Collins Environmental & Facilities Manager TABLE OF CONTENTS I Certification Form II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Form VIII Pathogen and Vector Attraction Reduction Documentation IX Soil Analysis Report X 2014 Application Summary Table XI 2014 Application Condition Summaries Certification Form ANNUAL LAND.APPLICATION CERTIFICATION FORM Permrt#: WQ0004893 County: Robeson Year: 2014 . Facility Name (as shown on permit): Campbell Soup Supply Company -Land Application'Operator: -Campbell Soup.Supply Company Phone:. (910) 844-5.631 •-. PP. Y P g.• P and a hcation.of residual.sohds as allowed b the ermit occurred- the ast:ca . - " lendaryear? ..'. RI, .Yes ❑ No If No,'skip Part A; and Part B and proceed to`the certification. Also., if.residuals were. . generated but not land applied; please -attach an explanation on how the residuals were handled. Part'Ac: Total number. of application fields in permit: 7 . Total number of acres land.application occurred during the year':. 56.8: Part B: Facility. was compliant during:calendaryear .2014 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water-Resources.0 Yes ❑ No'. If no please, provide a written description why the facility was. not compliant, the dates, and explain . corrective action taken. . 1. Only'residuals approvedfor this permit were applied to .the permitted sites.. 2. Soil pH was adjusted as specified in the permit. and, lime was applied (if. needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils -analysis were performed on each site receiving residuals during.the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed -and three (3) copies of certified.laboratory results are attached.. ` All other monitoring was performed in. accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not, exceed any of the Pollutant Concentration Limits in Table 1- of.40 CFR Part 503.13 or the Pollutant Loading.Rates in Table 2 of 40 CFR part 503.13. (applicable to 40 CFR Part 503 regulated facilities).. 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part. 503.14 were complied 'with.(applicable. to 40 CFR Part 503 regulated:'facilities). 8. All operations and maintenance requirements .in. the permit were complied with or, in the' case of a deviation, prior authorization was received from the Divisio"n of Water Resources. 9. No contravention. of Ground Water.'Quality Standards occurred at a'monitoririg well or explanations .of . violations are attached to include appropriate actions and remediations. 10..Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan-: :11.. No runoff of residuals from the application.sites onto adjacent property ornearby,surface-waters has occurred:: 12. All.buffer'regpirements as specified on,.the.permit were maintained during each application. of residuals: "I certify 'under penalty of law, that the above information is, to the best of my knowledge and belief, true,., accurate; and complete. I am .aware, that there, are significant penalties for submitting false information; - including the possibility of fines and imprisonment for knowing vio ati s "Michael G:Miller - Sr..Dir. Of Operation_ s 2 1�� Permittee Name and Title (type or print) . � . - Signature of Pen'nittee Date -4. - Si nature of Preparer* Date Signature of. -Land Applier - Date .(if different from Permittee) ; (if different from Permittee and Preparer) * Preparer is defined in 40 CFI .Part'503 9'(r) DENR FORM ACF (5i2003) Annual Residual Sampling Summary Form ANNUAL RESIDUAL SAM LTG SUMMARY FORM Attach this form to the corresponding Annual.Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004893- Laboratory: 1) A & L Eastern Laboratories, Inc. - Facility Name: Campbell Soup Supply Company 2) NPDES # or WQ0003.626 3) WQ#: 4) WWTP Name: Campbell Soup Supply Company - DAF 5) R.,Qidnal Ana1v6.c data Sample or Composite Date 2/27/14 4/1/2014 7/7/2014 10%6/2014 Percent Solids 4.34 0.93 1.39 4.76 Arsenic NR NR NR NR Cadmium 2 2 2 2 Chromium NR NR NR NR Copper 7 25. 50 23. Lead 5 5 5 5..' Mercury NR NR NR NR Molybdenum' NR NR NR NR y Nickel' 7 21 45 . 28 Selenium NR NR NR, NR Zinc 141 364 236 284. Total Phosphorus 744 1090 1970 1400 TKN 6680 24700 12200 27100 Ammonia -Nitrogen 461 9680 2160 2310 Nitrate and Nitrite 134 53.8 14.4 2 "I certify, .under penalty of law, that this document was prepared under my direction or -supervision in' accordance. with a system. designed to. assure that qualified personnel properly gathered and evaluated, the, information submitted. I.am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Si1rhature. of Preparer Date DENR.FORM RSSF.(5/2003), ANNUAL RESIDUAL -SAN.. SING SUMMARY FORM Attach this form to the corresponding Annual Report, Please note that your permit may contain additional parameters to be analyzed than those required to, be summarized on this form. Permit Number: WQ0004893 Laboratory: 1) A & L Eastern Laboratories, Inc. Facility Name: Campbell Soup Supply Company 2) NPDES # or 3) WQ#.. WQ0003626 4) WWTP Name:, Campbell Soup Supply Company- DAF 5) RPcirinal Analveic data Co I• •site • , I ® , , ®®® , ' I ®.®®®' I ® •' ® ,• •1 • � • � 11 ® III S�-® "I certify, .under penalty of law, that this document was prepared under my direction or supervision in accordance with 'a system . designed to assure that, qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Si nature of Preparer 12 - /d - iS Date DENR FORM RSSF-B-(5/2003) Annual Metals Field Loading Summary Forms ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 11.84628 Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0 1' ator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company acres Used: 5.1 Acres Permitted: 5.1 Site #: S Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date Ill 2/27/14 _2j 4/1/14 3 7/7/14 4 10/6/14 5 6 7 8 9 10 11 12 % Solids 4.34 0.93 1.39 1 4.76 Arsenic 0 0 0 0 Cadmium 2 2 2 2 Chromium 0 0 0 0 Copper 7 25 50 23 Lead 5 5 5 5 Mercury 0 0 0 0 Molyb- denum 0 0 0 0 Nickel 7 21 45 28 Selenium 0 0 0 0 Zinc 141 364 236 284 Total Phos- nhn,.ug 744 1090 1970 1400 - ial Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 L 2 3L_j L4J 5j 6j L7J_8 9j 10 11 12 •`, d-- o 0.369 0.2642 0.137 1.5526 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.0015 0.0011 0.0005 0.0062 0 0 0 0 0 0 0 0 0.0093 hromi 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.0052 0.0132 0.0137 0.0714 0 0 0 0 0 0 0 0 0.1035 0.0037 0.0026 0.0014 0.0155 0 0 0 0 0 0 0 0 0.0232 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0.0052 0.0111 0.0123 0.0869 0 0 0 0 0 0 0 0 0.1155 I 0 0 0 0 0 0 0 0 0 0 0 0 0 0.1041 0.1923 0.0647 0.8819 0 0 0 0 0 0 0 0 1.2429 0.5491 0.576 0.5398 4.3473 0 0 0 0 0 0 0 0 6.0121 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the i d " mation submitted. I am aware that there are significant penalties for submitting false information, i ding the possibility of fines and imprisonment for knowing violations" s .2-/G-/� Sigdture of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* �. Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 19.67364 Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 8.4 Acres Permitted: 8.4 Site #: S Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 2/27/14 2/27/14 4/1/14 4/1/14 10/6/14 % Solids 4.34 4.34 0.93 0.93 4.76 Arsenic 0 0 0 0 0 Cadmium 2 2 2 2 2 Chromium 0 0 0 0 0 Copper 7 7 25 25 23 Lead 5 5 5 5 5 Mercury 1 0 0 0 0 0 Molyb- denum 0 0 0 0 0 Nickel 7 7 21 21 28 Selenium 0 0 0 0 0 Zinc. _ _ 141 __. 141. 3M4 364 284, L 744 744 1090 1090 1400 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): � o o " 0.293 0.3269 0.18 0.0418 1.5004 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.0012 0.0013 0.0007 0.0002 0.006 0 0 0 0 0 0 0 0.0094 Chromiurr 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.0041 0.0046 0.009 0.0021 0.069 0 0 0 0 0 0 0 0.0888 Lead 0.0029 0.0033 0.0018 0.0004 1 0.015 0 0 1 0 0 1 0 0 0 10.0234 Mercury. 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0041 0.0046 0.0076 0.0018 0.084 0 0 0 0 0 0 0 0.102 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0.0826 0.0922 0.131 0.0304 0.8522 0 0 0 0 0 0 0 1.1885 Total Phos- 0.436 0.4864 0.3924 0.0911 4.2011 0 0 0 0 0 0 0 5.6071 horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" S gnature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 19.6352 Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 26 Acres Permitted: 26 Site #: S Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 2/27/14 2/27/14 2/27/14 4/1/14 7/7/14 7/7/14 10/6/14 % Solids 4.34 4.34 4.34 0.93 1.39 1.39 4.76 Arsenic 0 0 0 0 0 0 0 Cadmium 2 2 2 2 2 2 2 Chromium 0 0 0 0 0 0 0 Copper 7 7 7 25 50 50 23 Lead 5 5 5 5 5 5 5 Mercury 1 0 0 1 0 0 1 0 0 1 0 Molyb- denum 0 0 0 0 0 0 0 Nickel 7 7 7 21 45 45 28 Selenium 0 0 0 0 0 0 0 Zinc 141 141 141 364 236 236 284 Total Phos- horus 744 744 744 1090 1970 1970 1400 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): C o �a� y CD d o 0.0949 0.0739 0.2948 0.0486 0.0371 0.0684 0.1375 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.0004 0.0003 0.0012 0.0002 0.0001 0.0003 0.0006 0 0 0 0 0 0.003 Chromiurr 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.0013 0.001 0.0041 0.0024 0.0037 0.0068 0.0063 0 0 0 0 0 0.0258 Lead 0.0009 0.0007 0.0029 0.0005 0.0004 0.0007 0.0014 0 0 0 0 0 0.0076 Mercury 1 0 0 0 0 0 1 0 0 1 0 0 0 0 0 1 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0013 0.001 0.0041 0.002 0.0033 0.0062 0.0077 0 0 0 0 0 0.0257 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0.0268 0.0208 0.0831 0.0354 0.0175 0.0323 0.0781 0 0 0 0 0 0.294 Total Phos- 0.1412 0.11 0.4387 0.1059 0.1462 0.2695 0.385 0 0 0 0 0 1.5965 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, ' including the possibility of fines and imprisonment for knowing violations" -2-Id - /.S Si ature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 16.21347 Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 9.1 Acres Permitted: 9.1 Site #: S Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 2/27/14 2/27/14 7/7/14 7/7/14 10/6/14 % Solids 4.34 4.34 1.39 1.39 4.76 Arsenic 0 0 0 0 0 Cadmium 2 2 2 2 2 Chromium 0 0 0 0 0 Copper 7 7 50 50 23 Lead 5 5 5 5 5 Mercury 1 0 0 0 0 0 Molyb- denum 0 0 0 0 0 Nickel 7 7 45 45 28 Selenium 0 0 0 0 0 Zinc 141 141 236 236 284 Total Phos- horus 744 744 1970 1970 1400 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): o � t7 o " 0.3215 0.485 0.1149 0.1994 0.6609 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.0013 0.0019 0.0005 0.0008 0.0026 0 0 0 0 0 0 0 0.0071 hromiu 0 0 0 � 0 0 0 0 0 0 0 0 0 0 Copper 0.0045 0.0068 0.0115 0.0199 0.0304 0 0 0 0 0 0 0 0.0731 Lead 0.0032 0.0049 0.0011 0.002 0.0066 0 0 0 0 0 0 0 0.0178 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0045 0.0068 0.0103 0.0179 0.037 0 0 0 0 0 0 0 0.0766 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0.0907 0.1368 0.0542 0.0941 0.3754 0 0 0 0 0 0 0 0.7512 Total Phos- 0.4784 0.7217 0.4527 0.7856 1.8505 0 0 0 0 0 0 0 4.2889 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" SiiKature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 10.00416 Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 3.4 Acres Permitted: 3.4 Site #: S Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 2/27/14 4/1/14 7/7/14 10/6/14 % Solids 4.34 0.93 1.39 4.76 Arsenic 0 0 0 0 Cadmium 2 2 2 2 Chromium 0 0 0 0 Copper 7 25 50 23 Lead 5 5 5 5 Mercury 0 0 1 0 0 Molyb- denum 0 0 0 0 Nickel 7 21 45 28 Selenium 0 0 0 0 Zinc 141 364 236 284 -Total Phos- horus 744 1090 1970 1400 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ti o a� o CD ��a o � 0.8455 0.08 0.2869 1.73 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.0034 0.0003 0.0011 0.0069 0 0 0 0 0 0 0 0 0.0118 Chromiun 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.0118 0.004 0.0287 0.0796 0 0 0 0 0 0 0 0 0.1241 Lead 0.0085 0.0008 0.0029 0.0173 0 0 0 0 0 0 0 0 0.0294 Mercury 1 0 0 1 0 0 0 0 0 1 0 0 0 0 0 1 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0118 0.0034 0.0258 0.0969 0 0 0 0 0 0 0 0 0.1379 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0.2384 0.0582 0.1354 0.9826 0 0 0 0 0 0 0 0 1.4147 Total Phos- 1.2581 0.1744 1.1304 4.844 0 0 0 0 0 0 0 0 7.4069 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 0.73554 Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 2.3 Acres Permitted: 2.3 Site #: S Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in lbs/acre): o �a� y 0 o 0.3198 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.0013 0 0 0 0 0 0 0 0 0 0 0 0.0013 Chromiun 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.016 0 0 0 0 0 0 0 0 0 0 0 0.016 Lead 0.0032 0 0 0 0 0 0 0 0 1 0 0 0 0.0032 Mercury 0 0 1 0 0 0 1 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0134 0 0 0 0 0 0 0 0 0 0 0 0.0134 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0.2328 0 0 0 0 0 0 0 0 0 0 0 0.2328 Total Phos- 0.6972 0 0 0 0 0 0 0 0 0 0 0 0.6972 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" 2:2 � V -/14-/S Si ature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 3.322 Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 2.5 Acres Permitted: 2.5 Site #: S Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Rase Percent #): Sample or Com- posite Date 4/1/14 10/6/14 10/6/14 % Solids 0.93 4.76 4.76 Arsenic 0 0 0 Cadmium 2 2 2 Chromium 0 0 0 Copper 25 23 23 Lead 5 5 5 Mercury 1 0 0 1 0 Molyb- denum 0 0 0 Nickel 21 28 28 Selenium 0 0 0 Zinc 364 284 284 Total Phos- horus 1090 1400 1400 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): �o �J y w H 0 o 0.3229 0.7921 0.2138 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.0013 0.0032 0.0009 0 0 0 0 0 0 0 0 0 0.0053 Chromiutr 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.0161 0.0364 0.0098 0 0 0 0 0 0 0 0 0 0.0624 Lead 0.0032 0.0079 0.0021 0 0 0 0 0 0 0 0 0 0.0133 Mercury 1 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0136 0.0444 0.012 0 0 0 0 0 0 0 0 0 0.0699 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 0.2351 0.4499 0.1214 0 0 0 0 0 0 0 0 0 0.8064 LPhorus 0.7039 2.2179 0.5986 0 0 0 0 0 0 0 0 0 3.5204 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form Annual Land Application Field Summary ANNUAL LAND APPLICATIOT ELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX_ WHEN NOT APPLICABLE. Facility Name:'. ..Campbell Soup Supply Company Permit #: WQ0004893 Annual Dry Tons Applied: 11:84540458 Owner: Campbell. Soup Supply Company ..'Operator: Campbell Soup Supply Company Cation Exchange Capacity (non 503): >5.0. Site #:. S. Field #: 1 AcresUtilized: 5.1. Acres Permitted: 5.1 o" 0 o A >: Specify, Totals Per Acre % Solid s Dry Tons Per Acre Sources (Summarize) site Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- - tili- zation Rate* * Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 -Must Select Cro 1 or Crop p p 2 *= Gal.: Cu.Yd. . . Report Totals in Gal. crop 1 "Crop 2 Jan 14. 10398 - 2038.8- 4.34 0.368982205 DAF. - Dry .0 S 0.5 0.4 6680 461 134 ####### 2.10475 Rye 1 May 14 . 34736. 6811 0.93 0.264136631 DAF Dry 0 S .0.5 0.4- 24700 9680 53.8 5.75913 ####### Bermuda 2 .Sep 14. 12050 ..2362.7 L39 0.136951794 DAF Dry 0 S 0.5 0.4 12200 2160 14.4 1.39976 ####### Bermuda 3 Oct 14 " 39,891 1821.8 4.76 1.55255772 DAF Dry 0 S 0.5 0.4- 27100 2310 2 34.3829 ####### Bermuda 4 0 0 0 0 5 0 .0 0 0 - 6- 0 0 0 0. 7 0 0 0 0 8 0 0 0 0. 9 0 0. -0 0 = 10 0 : 0 0 0 11 0 0 0 0 12 TOTALS: 19034 :::::::::::::::: As Cd ' Cr Cu Pb Hg Mo Ni Se' Zn P -PAN 1 PAN 2 Lime A lied Annuallbs/acre 0 0.00929 0 0.1035 9.02323 0 0 0.11554 0 1.24294 6.01209. 41.5418 2.10475 Date lbs/ac Current Cumulative lbs/ac 0 0.00929 0 0.1035 0.02323 0 0 0.11554 0 1:24294:'.'•.'•>.'•.'•::::::::`::':::.'::'::::::::::`::::::::: ............ 100 50 Prior. Years Cumulative lbs/ac . Permitted C. P. L. R. Permit PAN Limit l st/2nd Crop "I certify, under. penalty of law, that this document was prepared.under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I.am aware that there are significant penalties for submitting false information; including the possibility of fines'and imprisonment_ for: knowing violations." -2 -1d - i-s *Application Method: S - Surface, IN --Injection, INC - Incorporation Signature of Land Applier Date *.*Volatilization Rate: Surface - 0.5. Iniection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate. * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be -entered into the same numbered column. on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column #.1. DENR FORM FSF (5/2003): ANNUALLAND APPLICATIOP ' 'ELD SUMMARY FORM . PLEA, . • iVIAKE A COPY OF THIS BLANK FORM TO BE COMP: 'ED AND SUBMITTED FOR EACH APPLICATION FIE] - PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: - Campbell Soup Supply Company . Permit #: WQ000493 Annual Dry Tons Applied: 19.67388361 Owner: -Campbell. Soup Supply Company Operator: Campbell Soup Supply Company 'Cation Exchange Capacity (non 503): >5.0 Site #:.: S Field #: 2 Acres Utilized: 8.4 Acres Permitted: 8.4. o Specify Totals Per Acre % : Solid s Dry- Tons Per .Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- nation Rate* * Miner- ali- nation Rate TKN Ammo nia- Ni- trogeri = Ni- trate and Nitrite PAN 1 PAN -2 Must Select Crop 1.or Crop 2 *: *. Gat. Cu.Yd. Report Totals in Gal. Crop i rCrop 2 Jau.14 13600 1619 4.34 0.293012 - DAF. Dry 0 S 6.5 0.4 6680 461 134 ####### 1.6714 Rye 1 Feb 14 15173 1806.3 4.34 0.326902285 DAF Dry 0 S 0.5 0.4 6680 461 134 ####### 1.86472 Rye . 2 May 14 38995 4642.3 0.93 0.180031559 DAF Dry 0 S 0.5 0.4. 24700 9680 53.8 3.92534 ####### Bermuda 3 Jun 14 9048 1077.1 0.93 0.041772677: DAF. Dry 0 S 0.5 0.4 24700 9680 53.8 0.91079 ####### Bermuda 4 Nov 14 . 63496 7559 4.76 1.50041048 DAF Dry 0 - S 0.5 0.4 27100 2310 2. 1####### 33.2291 Rye. 5 0 0 .. 0 0 6 0 0 0 0 7 0 0 0 0 8. a.. 0 -0 0 0 9 0 0 0 1 0 10 '0 0 „ 0 0 11 0.. 0 0 0 12 TOTALS: 16704 :::::::::::`:: As Cd Cr Cu Pb Hg Mo Ni Se Zn R PAN 1 PAN 2 Lime A lied Annuallbs/acre 0 0.00937 0 0.08879 0.02342 0 0 0.10202 0 1.18851 5.60706 14.83613 36.7642 Date lbs/ac Current Cumulative lbs/ac . 0 0.00937 0 0.08879 0.02342 0 0 0.10202 0 1.18851 ::::'? : »»:::::: »>: 299 50 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** it PAN Limit 1 st/2nd Crop Perm L p "I certify, under penalty of law, that this document was prepared under my direction or supervision'm accordance with a system . designed to -assure that qualified personnel properly gathered. and evaluated the information submitted. I am aware that there are -significant penalties for submitting false information, including the possibility of fines 'and imprisonment for knowing violations." *Application Method: S - Surface, IN Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation -,1.0. * * * C.P.L.R.: Cumulative Pollutant Loading Rate - . The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this informationneeds to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF.row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. ANNUAL LAND APPLICATIOT . ELD SUMMARY FORM PLEASE.MAKE,A COPY. OF -THIS BLANK FORM TO BE COMPLETED AND SUBMITTED•FOR EACH APPLICATION'FIELD. PLACE A "N/A". IN A BLANK OR BOX WHEN NOT APPLICABLE. . Facility Name: Campbell Soup Supply Company. ' _ Permit #: WQ0004893 Annual Dry Tons Applied: 28.1415 Owner: Campbell Soup Supply Company Operator: Campbell. Soup Supply Company Cation Exchange Capacity (non.503): Site #: -S Field #: 3 Acres Utilized: 26. Acres Permitted: 26 � 4. A Specify Totals- -. Per .Acre. % Solid s - - Dry Tons Per : Acre Residual Sources (Summarize} Site Cond. Dry, Wet Moist Inches- Precip. Past 24 Hrs: Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate T&N Ammo ma- Ni- trogen Ni-- trate and Nitrite PAN 1 PAN 2 Must Select .. Crop 1 Qr..Crop 2 *: . Gal. CuNd. . • Report Totals in Gal. Crop T .Crop 2 Jan 14 13631 52421 4.34 - 0.094881197 DAF :Dry 0 S 0.5 0.4 6680 461 ' 134 0.54122 ####### Pines 1 Fe1i'14 10616 40831 4:34 0.07389471 DAF Dry 0 S 0.5 0.4 6- 461 134 0.42151 ####### . Pines 2. ivlai 14 42356 1629.,1 : 4.34 . 0.294827083 DAF, Dry 0. S 0.5 0.4. 6680 461. 134. 1.68175 ####### . Pines: 3' Apr 14 32549 1251.9- 0.93 0.048549337, DAF . Dry 0 S- 0.5 0.4 24700 9680 53.8 1.05.855 ####### . Pines 4 Aug 14_ '1663.1 '639.65 1.39 : _ 0.037076256 DAF. Dry 0 S . 0.5. 0.4 , 12200 2160 14A_ 0.37895 ####### Pines- 5 Sep 14. 30695 .1.180.6 1.39. °0.06842978. DAF Dry, 0 S -0.5, : 0.4 1.2200.. 2160 . _ 14.4 0.69941 .####### ' Pines 6 Oct 14 18017 692.96 - 4.76 0.137547322 DAF 'Dry 0 S 1 0.5 0.4 27100 2310 2 3,04612 ####### Pines 7 Nov 14 2105.0 809.62 4.76 . 0A6070207.DAF Dry . 0 S 0.5 0.4 27100 2310 2 3.55891 #######. ' Pines ' 8 Dec 14 21804 83 $.62 4.76, 6.1664H445 : • • DAF Dry 0 S 0.5 .0.4 ' 27100 2310 2 :3.68639 1 ####### : Pines' 9 1Q .. 11 12 TOTALS: 7975 `:: °'::`: As Cd Cr Cu Pb H Mo Ni. Se. ' Zn P PAN.1 PAN 2 Lime A lied . Annual.lbs/acre,. 0. - 0.00302 0. 0.0258 0.00755 0_ • b . 0.02573 0 ,:. 0.29401 1.59645 15.07281 0 Date. lbs/ac. Current Cumulative lbs/ac 0 0.06302 0 . - 0.0258 0.00755 0' 0 0.02573' 0 0.29401 ' 60. Prior Years Cumulative lbs/ac Pemitted C. P. L. R. 2 r Permit PAN Limit 1st/ nd C o Perm L x P "I certify, under penalty:of law, that -this document was prepared under my direction or supervision in accordance with a system. designed to assure that.qualifed personnelproperly gathered and'evaluated the information submitted. I am aware that there are: significant penalties for. submitting false information, including: the possibility of fines and imprisonment for knowing violations." *Application.Method: S - Surface: -Injection, INC -Incorporation Signature of Land Applies Date . **Volatilization Rate: Surface 7-0.5, Iniection/Incorporation - 1:0 ***C.P.L.R.: Cumulative Pollutant Loading Rate . * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered.into - the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column #.1. PLEA:..,-. `,MAKE A COPY OF THIS BLANK FORM TO BE COMP__ _'ED AND. SUBMITTED FOR EACH APPLICATION FIEL_: PLACE A -"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company . Permit #:. WQ0004893 Owner: Site #: Campbell Soup Supply Company Operator: Campbell Soup Supply Company S Field #:. 4 Acres Utilized: 9.1. Annual Dry Tons Applied: 16.2.1309719 Cation Exchange Capacity (non 503): >5.0 Acres Permitted: 9.1 o ° �, 0 o Specify Totals Per 'Acre..: % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e . Cond. Dry, Wet, -Inches Precip. Past 24 Hr8. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- . zation Rate TKN Ammo ma- Ni- trogen Ni- trate and . Nitrite PAN 1 PAN2 1Vlust Select Crop 1 or Crop' p 2 Gal.. .. Cu.Yd. 1:1Jan Report Totals . in Gal. Crop 1 Crop 2 14 16165 1776.4 4.34 0.321484546 DAF Dry 0 S 0.5 0.4 6680 461 134 ####### 1.8338.1 Rye .1 Feb 14 24388 - 2680 4.34 0.48502104 DAF Dry 0 S 0.5 0.4 6680 461 134 ####### 2.76666 Rye . 2 Jul 14 18038 -1982.2 1.39 0.114894131 DAF Dry 0 S 0.5 0.4 12200 2160 14.4 1.17431 ####### Bermuda 3 Aug 14 31307 3440.3 1.39; 0.199411829_ DAF Dry. 01. S 0.5 .0.4 12200 2160 14.4 2.03815 ####### Bermuda . 4' Dec 14 30297 3329J 4.76 0.660847486 DAF Dry 0 S 0.5 0.4 27100 2310 2 ####### ' 14.6351 1 Rye 5 0 0 0 0 6 0 0 0 0 7. 0 0 0. 0 $ 0 0 0 0 9 0 0 0 0 10 0.. 0 0 0 11 0 p 0*. 0 .. 12 TOTALS: 13208 :::" As Cd Cr Cu Pb. Hg Mo Ni Se Zn P PAN 1 PAN Lime'A lied Annual lbs/acre 0 0.00713 0 0.07312 0.01782 0 0 0.07659 0 0.75117 4.28893 3.21246 19.2356 . Date lbs/ac Current Cumulative lbs/ac.- 0 0.007.13 0 . 0.07312 0.01782 0 0 0.07659 0 0.75.117..............:::.......:....:.:.:.:::.:.... 1 10 50 Prior Years Cumulative lbs/ac Permitted C. P. L: R. 2 r Perm Permit PAN Limit 1st/ nd Crop p "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system . designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that thereare significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application. Method: S -Surface, IN Injection,. INC -Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorooration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered: on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the'MFLSF as is. entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF 'row # 1 to MFLSF column # 1. ANNUAL LAND APPLICATIOr rAELD SUMMARY FORM -PLEASE MAKE.A COPY_ - OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: WQ0004893 Annual Dry Tons Applied: - 10.-00412107 Owner: Campbell .Soup Supply Company Operator:. Campbell Soup Supply Company Cation Exchange Capacity (non 503): ->5.0. Site #: .S.:Field #: 5 Acres Utilized: 3.4. Acres Permitted: 3.4 o- „ � o .. Specify-- Totals Per Acre . % Solid s Dry Tons Per Acre Residual . Sources . (Summarize) i e Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni-' trogen Ni- trate - and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop. p p. 2 _ Gal. CuNd. Report Totals in Gal. Crop 1 Crop 2 Jan 14 .15885 4672.1 4.34 0.845539862 DAF - - Dry 0 .. S 0.5 0.4 6680 461 134 ####### .4.82313 - Rye 1 Jun 14. 7010 2061.8 0.93 0.079957297 DAF Dry 0 S 0.5 0A 24700 _ 9680 53.8 1.74336 ####### Bermuda 2 Jul 14 -168-30. 4950 .1.39- 0.28691685. DAF Dry. 0 S 0.5 0.4 12200. 2160 14.4 . 2.93252 ####### Bermuda 3• Dec 14 : 29633 8715.6 4.76 1.72997454 DAF Dry 0 • S 0.5 0.4 27100 2310 .2: ####### 38.312 Rye: - 4 p.. 0 0 -0 5 0-- 0 •0' 0 6: 0 0 0 0 7. 0 p 0 0 8 0­ 0.. 0 0 9 O.. 0 0 10 0 0 0.. .0. 11 0 0 0. 0 12 TOTALS: 20399 :::::::::::::::: As Cd Cr ..Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre .0 0.01177 0 0.12411 0.02942 0 0 0.1379 0 1.41473 7.40689 4.67588. 43.1351 Date lbs/ac Current Cumulative lbs/ac 0 = 0.01177 0 0.12411 0.02942 0 0 0.1379 0.. 1.41473:::::::::::::::::::: 50 Prior. Years Cumulative lbs%ac Permitted C. P. L. R. i Limit lst/2nd Cropllb Perm t PAN " I certify, under. penalty of law, that this document was prepared under my direction ,or supervision in accordance with a system designed to assure that qualif ed personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including'the possibility of fines'and imprisonment for knowing violations." . -16 -%S' *Application Method: S - Surface, IN --Injection, INC = Incorporation Signature of Land Applies Date **.Volatilization Rate: Surface - 0,5; Iniection/Incorporation - 1.0 - * * * C.P.L.R.: Cumulative Pollutant Loadinz Rate. : . ***.* The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and. MFLSF are mathematically linked so'this information needs to be entered into the same numbered column, on=the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF. row # 1. to MFLSF column # 1. ANNUAL. LAND APPLICATIOT ., ,, _ELD SUMMARY FORM PLEASE MAKE A COPS. OF.THIS BLANK FORM TO. BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A". IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name:- Campbell Soup Supply Company. 'Permit #: WQ0004893 Annual Dry Tons Applied: 0.735559227 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Cation Exchange Capacity (non.505): >5.0 -Site #: S Field #: 6 Acres Utilized: 13. Acres Permitted:. 23 o o A s eci Totals. - Per Acre %_ Solid -s: Dry Tons Per - Acre' Residual Sources (Summarize) . i e Cond. Dry, = � Wet, : Inches Precip. Past 24 Hrs. Appli- cation Meth- od * Vola- tili- zation Rate *� Miner- ali- , zation Rate TKN Ammo nia- Ni- trogen" Ni- trate - and Nitrite :. PAN .1 PAN 2 Must Select . . Crop 1 or Crop p p 2 * , * . 1. Gal. Cu.Yd. .. ::: Report Totals in Gal.: Crop 1 Crop 2 Jun 14 18967 � �. 8246.5' 0.93. -0.31980836 DAF . Dry 0 S 0.5 0.4 24700 •9680 53.8 16,97297 ####### Bermuda . 1 0 0 '0 2 0: 0 0 0. 3' 0. 0 0 0 .. 4. 0- 0. .. 0 0 5 0 0 0 6 0 0 - 0:. .0- 7 0 0 0 .. 0 8. 0., 0 0 0.. 9 0 . 0. 0 0 10 0. .0. 0' . 0 , 11 0. -0 0 0 12 TOTALS:. 8247 :::....... As Cd Cr :Cu. Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annual lbs/acre 0 0.00128 0 .0.01599 . 0.0032 0 0 0:01343 0 0.23281- 0.69716. 6.97297.1 0 Date - lbs/ac Current Cumulative lbs/ac 0 0.00128 0 0.01599 0.'0032 0. 0. 0.01343 0,. 0.23281:::::::::::::..........::::`::::::::::::::::: 224 50 Prior. Years Cumulative lbs/ac Permitted C. P: L. R. i • it 'Ts 2nd Cro L Permit PAN m t1 p . "I certify, under. penalty of -lawthat this document was prepared.under,my direction.br_supervision.in accordance with a system designed to assure that qualified personnel properly gathered and. evaluated the information submitted. I.am aware :that there are significant penalties -for submitting. false Information, including the possibility of fines'and imprisonment, for knowing violations."- /� -/� *Application Method:. S -Surface, IN - Injection, INC - Incorporation Signature of Land Applies Date **.Volatilization Rate: Surface - 0.5, Iniection/Incorporation * * * C.P.L:R.: Cumulative Pollutant Loading Rate The RSSF Data and the Dry- Tons.Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are, mathematically linked so this information needs to be -entered into the same numbered. column. on the MFLSF as is entered on the identically numbered FSF row to. properly complete the metals equations: ie. FSF row #.1 to MFLSF-column.# 1. ANNUAL LAND APPLICATIO1', _ _ZELD SUMMARY FORM PLEASE, MAKE A COPY OF THIS BLANK FORM, TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A". IN A•BLANK OR BOX WHEN NOT APPLICABLE. Facility Name:. Campbell Soup Supply Company Permit #: WQ0004893 . Annual Dry Tons Applied: 3.321921663 ' Owner: Campbell Soup Supply Company Operator: Campbell. Soup Supply Company Cation Exchange Capacity (non 503): >5.0 Site #: S Field #: 7 Acres Utilized:, 2.5 Acres Permitted: 2.5., o . Q -Specify Totals Per Acre • % . Solid a Dry Tons Per Acre Residual - Sources (Suminarize) .61 e Cond. Dry, - Wet, Inches Precip: Past 24 I Appli- -cation Meth- * odist. Vola- tili- . zation Rate ** Miner- ali- zation Rate TKN Amino nia- Ni--- trogen Ni- trate and- Nitrite_ PAN .l T PAN 2 Must Select ' Crop 1 or Crop 2 Gal. Gal. Cu.Yd. Report - .Totals in Gal. - Crop l _Crop 2 Jun-14 - - 20815. 8326 0.93 0.322890606 DAF Dry 0 S 0.5 0.4' - 24700 9680 - 53.8 7;04018 ####### Bermuda- 1 Oct 14: 9976 : 3990.4 4.76 0.792062477 DAF Dry 0 S - 0.5 0.4 - 27100 2310 2. 17.541 ####### Bermuda 2 Nov 14, 2693 . 1077.2 .4.76 0.213815582 DAF Dry. 0 S - . 0.5 .. 0.4 .. '27100, 2-310 :2 ####### 4.73516 Rye 3 0 0 .0 4 0 0. 0 0 5 0.:0 ' .0 0 6 0 0. 0: 0.- 7 0 p 0 0 8 0 p 0. 0 9 p 0 0 10 __..: 0. :' 0. 0. 0 11 0.. 0 0 .0 12 TOTALS-... 13394 :::::::::::::::: .,As.: Cd Cr Cu Pb" Hg Mo Ni Se • . Zn P PAN'1 I PAN 2 Lime Applied Annual lbs/acre .0 0.00532 0 -0.06242 .0.01329 0 0 0:06989 0 : 0.80642 3.52044. 24:58I2 4.73516 ' Date lbs/ac Current'Cumulative lbs/ac 0' 0:00532 0 0.06242 0.01329 0 0 0.06989 0:0:80642 ::::::::::::::::: ` ............................................................•.•........•. . 2 4 50 2 Prior. Years Cumulative lbs%ac Permitted C.T. L. R. * * 1 t/2nd Crop rmit PAN Limrt s Pe P "I certify, under penalty, of law; that this document -was prepared under my direction or supervision in accordance witn a system designed to assure that qualified -personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false.information; including the possibility of fines: and imprisonment for: knowing violations." �-14 _/jC- *Application Method: S - Surface, IN --Injection, INC : Incorporation Signature of Land Applier Date "volatilization Rate: Surface - 0.5,- Iniection/Incorvoration =1.0. ***C.P.L:R.: Cumulative -Pollutant Loading Rate: * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically -linked so this information needs to be entered into the same numbered.column on:the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1-to MFLSF colurun.# 1. Residual Analysis Lab Sheets t Page: 1-of 2 Report Number: 14-059-0205L A&L Eastern Laboratories, Inc.., Account Number: 00327 7621 Whitepine Road Richmond, Virginia 23237, (804) 743-9401 Fax (804) 271-WS Submitted By: GRADY DOBSON www.aleastern.com Send Tor EHC Inca Project: CAMPBELL SOUP DAF PO, Box 902 NC CERT#257 RED SPRINGS , 'NC 28.377 REPORT OF ANALYSIS Date Sampled: 2/27/2014 11:30:00 Lab Number: 98171 ,Date Received: 02/28/2014 00:00 Sample Id : DAF 1ST QTR A Date Reported: 03/07/2014 .. PARAMETER . QUANTITATION LIMITANALYSIS D. •. Total Solids 4.34 43400 100.0 JM 03/04/2014 09:20 SM-2540G Moisture " 95.66. 100.0 JM 03/04/2014 09:20 SM-2540G Total Kjeldahl Nitrogen 0.67 6680 10.0 JM 03/03/2014 07:54 SM-4500-NH3C-TKN Total Phosphorus 007 744 100 KM 03/03/2014 12:51 SW 6010C Total Potassium 0.11 1080 100 KM 03/03/2014 12:51 SW 6010C Total Calcium 0.15 1510 100 KM 03/03/2014-12:51 . SW 6010C Total Magnesium 0.02 194 100 KM 03/03/2014 12:51 SW 6010C Total. Sodium 0.08 814 . 100 KM 03/03/2014 12:51 SW 6010C Total Aluminum 600 100 KM 03/03/2014 12:51 SW 6010C Total Copper 7 5 KM 03/03/2014 12:51 SW 601 OC Total Zinc 141 5 KM 03/03/2014 12:51 SW 6010C Ammonia Nitrogen 0.05 461 10.0 JM 03/03/2014 07:54 SM-4500-NH3C Organic N 0.62 6219 10.0 03/03/2014 07:54 CALCULATION Nitrate+Nitrite-N 134. 2.00 JM 03/03/2014 07:55 SM-4500NO3F .Total Cadmium <2.0 .2.0 KM 03/03/2014 12:51 SW 6010C Total Nickel 7 5 KM 03/03/2014 12:51 SW 6010C Total Lead <5 5 KM 03/03/2014 12:51 SW 6610C PH (Standard Units) * 3.70 2.00 JM 03/03/2014 09:09 SW-9045D All values are on_ a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt i Page: 2 of 2 Report Number: 14-059-0205 w A&L. EaStel71 Laboratofies, Inc. Account Number: 00327 � � 7621 Whitepine Road Richmond, Virginia23237 (804)743.9401 Fax (B04)271.6446 Submitted By:: GRADY DOBSON wll uleastemcom Send To: EHC Inc. Project: CAMPBELL SOUP DAF . PO Box 902 NC CERT#257 RED SPRINGS NC 28377 REPORT OF ANALYSIS Date Sampled: 2/27/201411:30:00 Lab Number.: 98171 'Date Received: 02/28/2014 00:00 Sample Id : DAF 1 ST QTR A Date Reported: 03/07/2014 Comments: ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al"., "CA", AND "NO3/NO2=N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.-� Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE TRANSNIITTA A&L E step 7621_ WWWDim Read Rich 1oil il i lii1 l 1,11, 1 o 14 ENC lqc. 1 GAF 1ST QTR A f3fHoe SUbr�iiRte�t3 ..To CopY To Ptaed RADY DOBSON ApotRem! 9 !onj- POS 902 Esiail RED SPRING$ NC 29S.77ab 1�9tttttDer (t,ab USo._... a ID_ ._ _ .1909 -._.... 53rrt _%d Dab,AA7/ i3a>g: find: `i� 1 : r�o� s, .�d �rfts« T, Is._c�. :►: I Rai' i• d .:' tt'atut+e Dale Tinia Rc�eiu04 BY: Slgnatur� . Date Time ..E49i F0c, IH I J -: Please P[a.ce a- "X" 4y Desired Test$. Internal Lab Code: . TKN P K S Ca ma 1Fe Al 01. cu ti zn NH -N NOU x x x x x x x Caco Volatile C.rl Cr Ni Pb . As ft Se H Eq. % Solids °!o Org-N Mo Ci B Ba X. ... x O4 Ag Sb Co Sit Ti. tt Be ALK. SS Avail P Sal K Cond WIN .. SOL 8 JL A : O�G SP,OR. TSS 5' I�2tt- SteveM S1 1Ra ASH Ca0 CaCO3 M 3 M94 GIN TOC Env OTAL. TOTAL '2C}S K2O TN TKNW idH41W- NO.3W ORGU-W PA CERT AZ CER'T BTU.= PCBS REACT. CN FECAL_., . TCLP ICR , p R� NORTH � /gyAROLINA �"qw"� .sV�� .'�rir`•�"'. f e-"' - >ar �Cwiu_:,i�e''N ' �+F�, jt'��? }:Y '`-y m' � Y, n?M����Yy' Z, .'rJr� -`Y+�'.. . A �'+'ra: v4[x-it�'•F �1'i t'iFn.�''. i� �- •'r.': ;'r.' �'��rw :WJ�Y�.�-C•^ .tip �^• - - • 4�f •a'i�. PI�C€'PER'SAMPC E>= -.�� ,�srr n AD m m w Lo Facility: Source: Location: Type of Anualysis: Report No.: Date Sampled: Date Reported: Reporting Period: Quarterly Sludge Summary Campbell Soup Supply Company DAF Sludge Maxton, North Carolina Quarterly Sludge - DAF 14-059-0205 2/27/2014 3/7/2014 1st Quarter - 2014 Parameter % PPM Dry Weight EPA Monthly Limits Solids 4.34 43,400.00 Nitrogen (TKN) 0.67 6,680.00 Phosphorus 0.07 744.00 Potassium 0.11 1,080.00 Sulfur -------- -------- Calcium 0.15 1,510.00 _ Magnesium 0.02 194.00 Sodium 0.08 814.00 Iron -------- -------- Aluminum -------- 600.00 Manganese -------- -------- Copper -------- 7.00 1,500.00 Zinc -------- 141.00 2,800.00 Ammonia Nitrogen 0.05 461.00 -------- Nitrate N/Nitrite N -------- 134.00 -------- Cadmium -------- 2.00 39.00 Chromium -------- 1,200.00 Nickel -------- 7.00 420.00 Lead -------- 5.00 300.00 Arsenic -------- -------- 41.00 Mercury -------- -------- 17.00 Selenium -------- -------- 100.00 pH3.7 -------- -------- Calcium Carbonate eq. (est) -------- -------- Organic Nitrogen 0.62 6,219.00 -------- Molybdenum -------- -------- 75.00 Chloride -------- -------- -------- Boron -------- -------- -------- Available P2O5 -------- -------- -------- Specific Gravity -------- 1 8.34 1 -------- Page: 3 of 2 Report Number: 14-092-0202 ��. A&L. Easters Laboratories, Inc._ Account Number: 00327 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 2114M Submitted By: GRADY DOBSON . WWUaleastem.com Send To: EHC Inc. Project: DAF-2ND QTR SLUDGE GRADY DOBSON NC CERT#257 PO Box 902 RED SPRINGS ; NC 28377 REPORT OF ANALYSIS Date Sampled:.4/1/2014 10:00:00 Lab Number: 98717 Date Received; 04/02/2014 00:00 Sample Id : DAF-2ND QTR SLUDGE Date Reported: 04/07/2014 Total Solids 0.93. 9300 100.0 JM 04/02/2014 14:39 SM-2540G Moisture" 99.07 100.0 JM 04/02/201414:39 SM-2540G Total Kjeldahl Nitrogen 2.47 24700 10.0 . JM. 04/03/2014 08:24 SM .4500-NH3C-TKN Total Phosphorus 0.11 1090 100 KM 04/04/2014 09:04 SW 601OC Total Potassium 0.42 4220 100 KM 04/04/2014 09:04 SW 601 OC Total Calcium 0.47 4690 100 KM 04%04/2014 09:04 SW 601 OC Total Magnesium 0.05 469 100 KM 04/04/2014 09:04 SW 601 OC Total Sodium 0:36 3620 100 KM 04/04/2014 09:04 SW 601.10C Total Aluminum_ 400 100 KM 04/04/2014 09:04 SW 601 OC Total Copper 25 5 KM 04/04/2014 09:04 SW 601 OC, Total Zinc 364 5 KM 04/04/2014 09:04 SW 601 OC Ammonia Nitrogen 0.97 9680 10.0 JM 04/03/2014 08:24 SM-4500-NH3C Organic N 1.50 15020 10.0 04/03/2014 08:24 CALCULATION Nitrate+Nitrite-N 53.8. 2.00 JM .04/03/2014 08:25 .: SM-450ONO3F Total Cadmium <2.0 2.0 KM 04/04/2014 09:04 SW 601 OC Total Nickel 21 5 KM 04/04/2014,09:04 , : SW 601 OC Total Lead <5 5 KM 04/04/2014 09:04 SW 60:1 OC. pH (Standard Units) * 4.40 2.00 JM 04/03/2014 08:24 SW-9045D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 bf. 2 Report Number: 14-092-0202 Account Number: 00327 Submitted By: GRADY DOBSON Send To: EHC Inc. GRADY DOBSON PO Box 902 RED.SPRINGS NC 28377 Lab Number :: 98717 . Sample Id : DAF-2ND QTR SLUDGE RESULT PARAMETER Comments:- ORGANIC.NITROGEN NOT FOR COMPLIANCE PURPOSES. A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743,9401 Fax (ew) 271=6446 www.aleastern.com Project : DAF-2ND QTR SLUDGE NC CERT#257 .REPORT OF ANALYSIS Date Sampled:.4/1/2014 10:00:00 Date Received: 04/02/2014 00:00 Date Reported: 04/07/2014 RESULT QUANTITATION DATEITIME All values are cin.a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLE. TRANS-Ml . TTAL A&L Eaftim 14,092-mO; O�-Q2-201 DAF­2JNb dm SLUDGE 12,41-09 - ­ =_ . . SkjhrAidpd By T --'GRADY DOBSON EMC,,,VNC POR 902 Email 6GrRA RED -SPRING.t KC. iO# -grad bsoneheiftmail.Dorn 9 n I ab Rurn . bdf,(Leab Usip, Only), "so male W� c;0tamer — Sbhnpj0q30Q* qhfml�,- Date Reed: PAP-- . $/a d-O Glass (yWor No). Samoled TVm&jj-,,6l6 Tints ReOd: emtic fy ar Na) Sam Reed �Xw Relkicpj Date, Is nature rlifid, R6&ClV0d 13pl(Signature)- me_ I Ti__ A__A roC V Place;� 'X ''by sts- Intemal L4b Code: Des Tests Ads: TKN P K CA - mg, A] Un NH4-N x X X X X X x X x Cd Cr Ni Pb Pb As Fig So- PH 5a�e_ CaCO3 E ofids 0/6 cl Sa x SDI —Ag, Sb__ Co Ti V_ SS _S61.K Cand WIN iiOL 13, 'OL NA O&G SPiGR TSS Sievd#20: SievoM SlevdfHQD ASH CaO 06CO3 _:_mgcoa. _ Moo. am TOG Er t FGTAL p2G5 TOTAL K2O' TN TK I NW N H4W NO3W ORGM-VU PAGER1 AZ'CERTI-1. BTU PCBS. REACT CN FECAL TGLP ICR iill M - . . . . . . 4,4- 10,4611 ROW, WON MUM- NORTH CAROLINA: - 1''.. It— W ,f - lmxaml: i !� M, Facility: Source: Location: Type of Anualysis: Report No.: Date Sampled: Date Reported: Reporting Period: Quarterly Sludge Summary Campbell Soup Supply Company DAF Sludge Maxton, North Carolina Quarterly Sludge - DAF 14-092-0202 4/1/2014 4/7/2014 2nd Quarter - 2014 Parameter % PPM Dry Weight EPA Monthly Limits Solids 0.93 9,300.00 Nitrogen (TKN) 2.47 24,700.00 Phosphorus 0.11 1,090.00 Potassium 0.42 4,220.00 Sulfur Calcium 0.47 4,690.00 Magnesium 0.05 469.00 Sodium 0.36 3,620.00 Iron -------- -------- Aluminum -------- 400.00 Manganese -------- -------- Copper -------- 25.00 1,500.00 Zinc -------- 364.0. 2,800.00 Ammonia Nitrogen 0.97 9,680.00 -------- Nitrate N/Nitrite N -------- 53.80 -------- Cadmium -------- 2.00 39.00 Chromium -------- -------- 1,200.00 Nickel -------- 21.00 420.00 Lead -------- 5.00 300.00 Arsenic -------- -------- 41.00 Mercury -------- -------- 17.00 Selenium -------- -------- 100.00 pH 4.4 -------- -------- Calcium Carbonate eq. (est) -------- 0.00 -------- Organic Nitrogen 1.5 15,020.00 -------- Molybdenum -------- -------- 75.00 Chloride -------- -------- -------- Boron-------- -------- -------- Available P205 -------- -------- -------- Specific Gravity -------- 8.34 -------- - Page: 1 of 2 - - - Report Number: 14-1,90-0216 A&L Eastern Laboratories, Inc. Account Number: 00327 7621 Whitepina Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 Submitted By: GRADY DOBSON www.aleastem.com Send To: EHC Inc. Project: DAF 3RD QTR PO Box 902 NC CERT#257 RED SPRINGS, NC 28377 Lab Number: 56375 Sample Id : DAF 3RD QTR REPORT OF ANALYSIS Date Sampled: 7/7/2014 08:30:00 Date Received: 07/09/2014 00:00 Date Reported: 07/14/2014. Total Solids * 1.39 13900 100.0 JM 07/09/2014 16:29 SM-2540G Moisture * 98.61 100.0 JM 07/09/2014 15:29 SM-2540G Total Kjeldahl Nitrogen 1.22 12200 10.0 JM 07/10/2014 08:50 SM-4500-NH3C-TKN Total Phosphorus 0.20 1970 100 KM 07/10/2014 14:12 SW 6010C Total Potassium 0.19 1850 100 KM 07/10/2014 14:12 SW 6010C . Total Calcium 4.42 44200 100 KM 07/10/2014 14:12 SW 6010C Total Magnesium 0.18 1760 100 KM 07/10/2014 14:12 SW 6010C Total Sodium 0.43 4300 100 KM 07/10/2014 14:12 SW 6010C Total Aluminum 2000 100 KM 07/10/2014 14:12 SW 6010C Total Copper 50 5 KM 07/10/2014 14:12 SW 6010C Total Zinc 236 5 KM 07/10/2014 14:12 SW 6010C Ammonia Nitrogen 0.22 2160 10.0 JM 07/10/2014 08:50 SM-4500-NH3C Organic N 1.00 10040 10.0 07/10/2014 08:50 CALCULATION Nitrate+Nitrite-N 14.4 2.00 JM 07/10/2014 08:50 SM-450ONO3F Total Cadmium <2,0 2.0 KM 07/10/2014 14:12 SW 6010C Total Nickel 45 5 KM 07/10/2014 14:12 SW 6010C Total Lead <5 5 KM 07/10/2014 14:12 SW 6010C pH (Standard Units) * 5.07 2.00 RJN 07/10/2014 08:50 SW-9045D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our orior written authorization. Debbie Holt SAMPLE TRANSMITTAI A&L Eas 'O91OU2014 ,M EHC Inc_3:19: DAF 3RD QTR 7621 Whi!mine Road Richn Offcce Information R'qAA# Submitted By 'Charge. To Copy To Project GRADY DOBSON EHC INC Awl -9 POB 902 Er ual� RED SPRINGS WC 28377 ab Nri�ber (Lab Use, Only) Sample ID Qalas iner Tan -0,0UYe or Na) Sam Jed Data: e: Sam ifn - pled time: Date R Time Recd. Plastic (7 e—s. or -No). Sampled By Re1incjtAerk13y_-^gnature) Date Time Received gy: (Signature) Date Time !2 Rease Place'a"X' by Desired Tes6i_ Intemal Lab Code: Ads WI TKN p K Ca Rflg Ma Fe Mn CanZn N"4-N NO3-N x x x x x x x x x x x x cd Cr Pli Pb As Hg— Se PH CaCO& Eq. % Volatile Sogids olrg-w too IfyD sa x x x x x 904 tag Sb co So Ti V Be ALK SS Aval I P Sol K' Cond MIN WIL ff oL NA '0&0 SP-GR. TSS 8tavc#20 Sieve-960 Sieve#100 ASK 'CaO cacO3 4_pO3 Mgo rim TOG Env i V TOTAL P205 TOTAL uo TN TKNW W1 4W NO3W .OFZGN-W PACERT,A-7CF-RT, BTU PCBS REACT CN FEGAL TCLP ICR MORTH CAROLINA A Z PFUCE PER SAMPLE -J (.n Lq rn F- on Facility: Source: Location: Type of Anualysis: Report No.: Date Sampled: Date Reported: Reporting Period: Quarterly Sludge Summary Campbell Soup Supply Company DAF Sludge Maxton, North Carolina Quarterly Sludge - DAF 14-19070216 7/7/2014 7/24/2014 3rd Quarter - 2014 Parameter % PPM Dry Weight EPA Monthly Limits Solids 1.39 13,900.00 Nitrogen (TKN) 1.22 12,200.00 Phosphorus 0.2 1,970.00 Potassium 0.19 1,850.00 Sulfur -------- -------- Calcium _ 4.42 44,200.00 Magnesium 0.18 1,760.00 Sodium 0.43 4,300.00 Iron -------- -------- Aluminum -------- 2,000.00 Manganese -------- -------- Copper -------- 50.00 1,500.00 Zinc -------- 236.00 2,800.00 Ammonia Nitrogen 0.22 2,160.00 -------- Nitrate N/Nitrite N -------- 14.40 -------- Cadmium -------- 2.00 39.00 Chromium -------- -------- 1,200.00 Nickel -------- 45.00 420.00 Lead -------- 5.00 300.00 Arsenic -------- -------- 41.00 Mercury -------- -------- 17.00 Selenium -------- -------- 100.00 pH 5.07 -------- -------- Calcium Carbonate eq. (est) -------- 0.00 -------- Organic Nitrogen 1 10,040.00 -------- Molybdenum -------- -------- 75.00 Chloride -------- -------- -------- Boron -------- -------- -------- Available P2O5 -------- -------- -------- Specific Gravity -------- 8.34 -------- Page: 1 of 2 Report Number: 14-280-0207 Account Number: 00327 Submitted By: GRADY DOBSON Send To: EHC Inc. PO Box 902 RED SPRINGS, NC 28377 L A &L Eastern Laboratories, into. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-401 Fax (804) 271.6446 wwmaleastern.com Project: CAMPBELL SOUP 4TH QTR SLUDGE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 10/6/2014 09:30:00 Lab Number: 57974 Date Received: 10/07/2014 00:00 Sample Id : DAF/CAMPBELL SOUP Date Reported: 10/17/2014 PARAMETER RESULT RESULT 'QUANTITATION LIMIT ANALYSIS (%.. ANALYST �, Total Solids * 4.76 47600 100.0 JM 10/07/2014 13:59 SM-2540G Moisture * 95.24 100.0 JM 10/07/2014 13:59 SM-2540G Total Kjeldahi Nitrogen 2.71 27100 10.0 JM 10/08/2014 08:44 SM-4500-NH3C-TKN Total Phosphorus 0.14 1400 100 KM 10/16/2014 18:38 SW 6010C Total Potassium 0.12 1160 100 KM 10/16/2014 18.38 SW 6010C Total Calcium 0.90 9030 100 KM 10/16/2014 18:38 SW 6010C Total Magnesium 0.06 614 100 KM 10/16/2014 18:38 _ SW 6010C Total Sodium 0.13 1340 100 KM 10/16/2014 18:38 SW 6010C Total Aluminum 1200 100 KM '10/161201418:38 SW 6010C Total Copper 23 5 KM 10/16/2014 18:38 SW 6010C Total Zinc 284 5 KM 10/16/2014 18:38 SW 6010C Ammonia Nitrogen 0.23 2310 10.0 JM 10/08/2014 08:44 SM-4500-NH3C Organic N 2.48 24790 10.0 10/08/2014 08:44 CALCULATION Nitrate+Nitrite-N <100 2.00 JM 10/08/2014 08:45 SM-450ONO3F Total Cadmium <2.0 2.0 KM 10/16/2014 18:38 SW 6010C Total Nickel 28 5 KM 10116/201418:38 SW 6010C Total Lead <5 5 KM 10/16/2014 18:38 SW 6010C pH (Standard Units) * 4.42 2.00 MW 10/08/2014 09:20 SW 9045D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Debbie Holt Facility: Source: Location: Type of Anualysis: Report No.: Date Sampled: Date Reported: Reporting Period: Quarterly Sludge Summary Campbell Soup Supply Company DAF Sludge Maxton, North Carolina Quarterly Sludge - DAF 14-280-0207 10/6/2014 10/17/2014 4th Quarter - 2014 Parameter % PPM Dry Weight EPA Monthly Limits Solids 4.76 47,600.00 Nitrogen (TKN) 2.71 27,100.00 Phosphorus 0.14 1,400.00 Potassium 0.12 1,160.00 Sulfur -------- -------- Calcium 0.9 9,030.00 Magnesium 0.06 614.00 Sodium 0.13 1,340.00 Iron -------- -------- Aluminum -------- 1,200.00 Manganese -------- -------- Copper -------- 23.00 1,500.00 Zinc -------- 284.00 2,800.00 Ammonia Nitrogen 0.23 2,310.00 -------- Nitrate N/Nitrite N -------- 2.00 -------- Cadmium -------- 2.00 39.00 Chromium -------- -------- 1,200.00 Nickel -------- 28.00 420.00 Lead -------- 5.00 300.00 Arsenic -------- -------- 41.00 Mercury -------- -------- 17.00 Selenium -------- -------- 100.00 pH 4.42 -------- -------- Calcium Carbonate eq. (est) -------- 0.00 -------- Organic Nitrogen 2.48 24,790.00 -------- Molybdenum -------- -------- 75.00 Chloride -------- -------- -------- Boron -------- -------- -------- Available P2O5 -------- -------- -------- Specific Gravity -------- 8.34 -------- Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report = K SC L•A•B S•C•1•E•N-C•E•S Mr. Thomas Ammons EHC, Inc. PO Box 902 Red Springs, NC 28377 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Report Summary Thursday June 19, 2014 Report Number: L703709 Samples Received: 06/10/14 Client Project: 14-MI0602-3 Description: Campbell Soup DAF Sludge (Annual TCLP Sludge) The analytical results, in this report are based upon information supplied by you, the -client, and are for your exclusive use. If you -have any questions regarding this data package, please -do not hesitate to call. %% II11 Entire Report Reviewed By: JimW Hunt , ESC Representative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BI0041, ND'- R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, ' MN 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3,'OK - 9915, PA - 68-02979, IA Lab #364, EPA - TN002 Accreditation is only applicable tb the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 13 ESC L-A-8 REPORT OF ANALYSIS Mr. Thomas Ammons EHC, Inc. PO Box 902 Red Springs, NC 28377 June 19,2014 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-600-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Date Received June 10, Description Campbell Soup Sample ID DAF SLUDGE Collected By Grady Dobson Collection Date 06/09/14 11:00 Parameter 2014 DAF Sludge Result (Annual TCLP Det. Limit Sludge) Units ESC Sample Site ID Project Limit Method # L703709-01 MAXTON, NC 14-MI0602-3 Date/Time By Dil Corrosivity Non-Corrosiv 9045D 06/13/14 1032 SDC 1 Ignitability See Footnote Deg. F D93/101 06/14/14 1215 AS 1 pH 4.5 su 9045D 06/11/14 1125 KBC 1 Reactive CN (SW846 7.3.3.2) BDL 0.125 mg/kg 9012B 06/12/14 1003 MCG 1 Reactive Sulf.(SW846 7.3.4.1) BDL 25. mg/kg 9034/90 06/12/14 0505 AS 1 TCLP Extraction - 1311 06/13/14 0817 CCS 1 Mercury BDL 0.010 mg/1 0.20 7470A 06/14/14 1707 CCE 1 Arsenic BDL 0.45 mg/1 5.0 6010C 06/14/14 0126 WBD 1 Barium BDL 1.4 mg/1 100 6010C 06/14/14 0126 WBD 1 Cadmium BDL 0.45 mg/l 1.0 6010C 06/14/14 0126 WBD 1 Chromium BDL 0.45 mg/l 5.0 6010C 06/14/14 0126 WBD 1 Lead BDL 0.45 mg/l 5.0 6010C 06/14/14 0126 WBD 1 -Selenium BDL 0.45 mg/l 1.0 6010C 06/14/14 0126 WBD 1 Silver BDL 0.45 mg/1 5.0 6010C 06/14/14 0126 WBD 1 TCLP ZHE Extraction - 1311 06/12/14 0832 CCS 1 TCLP Volatiles Benzene BDL 0.050 mg/l 0.50 8260B 06/12/14 2202 JC 1 Carbon tetrachloride BDL 0.050 mg/l 0.50 8260B 06/12/14 2202 JC 1 Chlorobenzene BDL 0.050 mg/l 100 8260B 06/12/14 2202 JC 1 Chloroform BDL 0.25 mg/l 6.0 8260B 06/12/14 2202 JC 1 1,2-Dichloroethane BDL 0.050 mg/l 0.50 8260B 06/12/14 2202 JC 1 1,1-Dichloroethene BDL 0.050 mg/1 0.70 8260B 06/12/14 2202 JC 1 2-Butanone (MEK) BDL 0.50 mg/1 200 826013 06/12/14 2202 JC 1 Tetrachloroethene BDL 0.050 mg/1 0.70 8260B 06/12/14 2202 JC 1 Trichloroethene BDL 0.050 mg/l 0.50 8260B 06/12/14 2202 JC 1 Vinyl chloride BDL 0.050 mg/l 0.20 8260B 06/12/14 2202 JC 1 Surrogate Recovery Toluene-d8 106.s Rec. 114. 8260B 06/12/14 2202 JC 1 Dibromofluoromethane 99.8 a Rec. 125. 8260B 06/12/14 2202 JC 1 a,a,a-Trifluorotoluene 99.3 e Rec. 114. 8260B. 06/12/14 2202 JC 1 4-Bromofluorobenzene 102. % Rec. 128. 8260B 06/12/14 2202 JC 1 TCLP Pesticides Chlordane BDL 0.0050 mg/l 0.030 8081A 06/18/14 1132 CBB 1 L703709-01 (IGNITABILITY) - did not ignite at 170F L703709-01 (PH) - 4.5@21.4c Page 2 of 13 *ESC I C C 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 )1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Thomas Ammons June 19,2014 EHC, Inc. PO Box 902 Red Springs, NC 28377 - ESC Sample # : L703709-01 Date Received June 10, 2014 Description Campbell Soup DAF Sludge (Annual TCLP Sludge) Site ID MAXTON, NC. Sample ID DAF SLUDGE Project 14-MI0602-3 Collected By Grady Dobson Collection Date 06/09/14 11:00 Parameter Result Det. Limit Units Limit Method Date/Time By Dil Endrin BDL 0.0050 mg/l 0.020 8081A 06/18/14 1132 CBB 1 Heptachlor BDL 0.0050 mg/1 0.0080 8081A 06/18/14 1132 CBB 1 Lindane BDL 0.0050 mg/l 0.40 8081A 06/18/14 1132 CBB 1 Methoxychlor BDL 0.0050 mg/l 10. 8081A 06/18/14 1132 CBB 1 Toxaphene BDL 0.010 mg/l 0.50 8081A 06/18/14 1132 CBB 1 Surrogate Recovery Decachlorobiphenyl 106. °s Rec. 123. 8081A 06/18/14 1132 CBB 1 Tetrachloro-m-xylene 66.8 o Rec. 114. 8081A 06/16/14 1132 CBE 1 TCLP Herbicides 2,4,5-TP (Silvex) BDL 0.0020 mg/1 1.0 8151A 06/16/14 1951 KLM 1 2,4-D BDL 0.0020 mg/l 10. 8151A 06/16/14 1951 KLM 1 Surrogate Recovery 2,4-Dichlorophenyl Acetic Acid 73.7 °s Rec. 8151A 06/16/14 1951 KLM 1 TCLP Semi-Volatiles 1,4-Dichlorobenzene BDL 0.10 mg/l 7.5 8270D 06/17/14 1704 KMF 1 2,4-Dinitrotoluene BDL 0.10 mg/1 0.13 8270D 06/17/14 1704 KMF 1 Hexachlorobenzene BDL 0.10 mg/1 0.13 B270D 06/17/14 1704 KMF 1 Hexachloro-1,3-butadiene BDL 0.10 mg/l 0.50 8270D 06/17/14 1704 KMF 1 Hexachloroethane BDL 0.10 mg/1 3.0 8270D 06/17/14 1704 KMF 1 Nitrobenzene BDL 0.10 mg/l 2.0 8270D 06/17/14 1704 KMF 1 Pyridine BDL 0.10 mg/l 5.0 8270D 06/17/14 1704 KMF 1 3&4-Methyl Phenol BDL 0.10 mg/1 400 8270D 06/17/14 1704 KMF 1 2-Methylphenol BDL 0.10 mg/l 200 8270D 06/17/14 1704 KMF 1 Pentachlorophenol BDL 0.10 mg/l 100 8270D 06/17/14 1704 KMF 1 2,4,5-Trichlorophenol BDL 0.10 mg/l 400 8270D 06/17/14 1704 KMF 1 2,4,6-Trichlorophenol BDL 0.10 mg/1 2.0 8270D 06/17/14 1704 KMF 1 Surrogate Recovery 2-Fluorophenol 45.2 °s Rec. 67.0 8270D 06/17/14 1704 KMF 1 Phenol-d5 32.3 "s Rec. 67.0 8270D _ 06/17/14 1704 KMF 1 Nitrobenzene-d5 61.1s Rec. 120. 8270D 06/17/14 1704 KMF 1 2-Fluorobiphenyl 61.4 o Rec. 122. 8270D 06/17/14 1704 KMF 1 2,4,6-Tribromophenol 68.7 °s Rec. 148. 8270D 06/17/14 1704 KMF 1 p-Terphenyl-dl4 51.6 °s Rec. 149. 8270D 06/17/14 1704 KMF 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Limit - Maximum Contaminant Level as established by the US EPA Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/19/14 12:10 Printed: 06/19/14 13:55 L703709-01 (IGNITABILITY) - did not ignite at 170F L703709-01 (PH) - 4.5@21.4c Page 3 of 13 Attachment A List of Analytes with QC Qualifiers Sample Work Sample Run Number Group Type Analyte ID Qualifier L703709-01 WG726036 SAMP 2-Sutanone (MEK) R293999G J3 WG72GS82 SAMP Heptachlor R2943611 J3 Page 4 of 13 C Attachment B Explanation of QC Qualifier Codes Qualifier Meaning J3 The associated batch QC was outside the established quality control range for precision. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected)." Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. r' TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 5 of 13 Summary of Remarks For Samples Printed 06/19/14 at 13:55:31 TSR Signing Reports: 350 R5 - Desired TAT Report GW in ppb except Campbell Soup; 6010C Sample: L703709-01 Account: ENVHYD Received: 06/10/14 09:00 Due Date: 06/17/14 00:00 RPT Date: 06/19/14 12:10 I ( ` _ _ SC✓ L•A•B 5•C•I•E-N•C•E•S • c • EHC, Inc. Mr. Thomas Ammons - PO Box 902 Red Springs, NC 28377 - Quality Assurance Report Level II L703709 - 12065 Lebanon Rd. Mt. Juliet, TN 37122 ' (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 June 19, 2014 Laboratory= B3'ank; ;• Analyte Result Units s Rec Limit Batch Date Analyzed Reactive Sulf;(SW846- 7.3.4.1) < 25_ mg/kg- .WG725665,06/12/-14 ",05:05 Reactive CN (SW846 7.3.3.2) < .125 mg/kg WG725666 06/12/14 09:58 1,1-Dichloroethene < .05 mg/1 WG726036 06/12/14 14:09 1,2-Dichloroethane < .05 mg/l WG726036 06/12/14 14:09 2-Butarione '(MEK) < .5- mg/1 WG726036; 06%12/14 -14:09 Benzene < .05 mg/1 WG726036 06/12/14 14:09 Carbon tetrachloride < .05 mg/1 WG726036 06/12/14 14:09 Chl6robenzene < .05_ mg/1 WG726036'06112`114 '14:09 Chloroform < .25 mg/1 WG726036 06/12/14 14,09 Tetrachlorcethene < .05 mg/1 WG726036 06/12/14 14:09 Triahloroethene' < .05 mg/l WG726036"--06/12%,14 14:09 vinyl chloride < .05 mg/1 WG726036 06/12/14 14:09 4-Bromofluorobenzene o Rec. 101.0 71-126 WG726036 06/12/14 14:09 DibroTdQfiuOromethane %- Rec. 99.40 78.3'121 WG726036`-06/12/14-14:09 Toluene-d8 % Rec. 103.0 88.5-111 WG726036 06/12/14 14:09 a,a,a-Trifluorotoluene o Rec. 100.0 85-114 WG726036 06/12/14 14:09 Arsenic < .45 mg/l WG726279 06/14/14 01:12 Barium < 1.35 mg/1 WG726279 06/14/14 01:12 ^admium. < .45 mg/1 WG726279"06/14/14 01:12 ftromium < .45 mg/1 WG726279 06/14/14 01:12 gad < .45 mg/l WG726279 06/14/14 01:12 Selenium < .45 mg/l WG726279. 08/14/14 01:12 Silver < .45 mg/1 WG726279 06/14/14 01:12 Mercury < .01 mg/1 WG.726271 06/14/14,16:39 2,4,5-TP (Silvex) < .002 mg/1 WG726590 06/16/14 17:31 2,4-D_ - < .002 mg/l. WG726590-06/16/14,17:31 2,4-Dichlorophenyl Acetic Acid o Rec. 66.00 22.9-153 WG726590 06/16/14 17:31 1,4-Dichlorobenzene < .1 mg/1 WG726366 06/17414 02:18 2,4,5-Trichlorophenol < .1 mg/1 WG726366 06/17/14 02:18 2,4,6-Trichlorophenol < .1 mg/1 WG726366 06/17/14 02:18 2,_4-Dinitrotoluene _ < .1 -- .mg/1_.., . .. ."*.- . _ .. ... .. -.WG726366- 06/17/14-,02:18 2-Methylphenol < .1 mg/l WG726366 06/17/14 02:18 3&4-Methyl Phenol <".1 mg/l WG726366 06/17/14 02:18 Hexachloro-1,3-butadiene < .1 mg/1 WG726366.06/17/.14 02:18 Hexachlorobenzene c .1 mg/l WG726366 06/17/14 02:18 Hexachloroethane < .1 mg/1 WG726366 06/17/14 02:18 Nitrobenzene < .1 mg/1 - WG726366 06/17/14 02:18 Pentachlorophenol < .1 mg/l WG726366 06/17/14 02:18 Pyridine < .1 mg/l WG726366 06/17/14 02:18 2,4,6-Tribromophenol a Rec. 60.40 11.2-130 WG7263,66 06/17/14 02:18 2-Fluorobiphenyl o Rec. 52.80 29.5-131 WG726366 06/17/14 02:18 2-Fluorophenol o Rec. 42.30 10-77.9 WG726366 06/17/14 02:18 Nitrobenzene-d5 % Rec. 51.00 21.8-123 WG726366 06/17/14 02:18 Phenol-d5 °s Rec. 32.70 5-70.1 WG726366 06/17/14 02:18 p-Terphenyl-d14 o Rec. 56.50 29.3-137 WG726366 06/17/14 02:18 * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 6 of 13 12065 Lebanon Rd. _ - Mt. Juliet, TN 37122 ESC C (615) 758-5858 .1-800-767-5859 Fax (615) 758-5859 L-A-8 S•C•I•E•[d-C•E•S Tax I.-D. 62-0814289 Est. 1970 EHC, Inc. Mr. Thomas Ammons PO Box 902 Quality Assurance Report Level II Red Springs, NC 28377 - June 19, 2014 L703709 Lab oratory=El-4 .1. Analyte Result Units % Rec Limit Batch Date Analyzed Chlordane .. .. < '.005 mg/1, . �• � - W6726582 06/,18%1`4'10:55 Endrin < .005 mg/1 WG726582 06/18/14 10:55 Lindane < .005 mg/1 WG726582 06/18/14 10:55 Heptachlor < .005 - mg/1= WG726582;1.06/281,14=10:55 Methoxychlor < .005 mg/l WG726582 06/18/14 10:55 Toxaphene < .01 mg/1 WG726582 06/18/14 10:55 Decachlorobiphenyl % Rec. _ 115d0.. 10.-156 WG726582' 06/18'/.14r10:55 Tetrachloro-m-xylene % Rec. 87.30 13.9-137 WG726582 06/18/14 10:55 Duplicate Analyte Units Result Duplicate RPD Limit Ref Samp Batch pH'- stir 7.10 7.'10 0.0' 1 1,703420=4 7 WG725694 pH su 7.20 7.20 0.278 1 L703730-07 WG725694 Reactive Sulf.(SW846 7.3.4.1) mg/kg 0.0 0.0 '0.0 20 L703664-01 WG725665 Reactive CN (SW846 7.3.3.2) mg/kg 0.0 0.0 0.0 20 L703664-01 WG725666 Corrosivity 0.0 0.0 0.0 10 L703374-01 WG726094 •.:rcury mg/l 0.0 0.000234 2.00 20 L704070-02 WG726271 jnitability Deg. F 0.00 0.00 0.00 10 L703664-01 WG726283 Ignitability Deg. F 0.00 0.00 0.00 10 L704505-01 WG726283 Laboratory Control Sample Analyte Units Known Val Result % Rec Limit Batch pH su - 6.33 6.30 99.5 98.3-101.7 WG725694 Reactive Sulf.(SW846 7.3.4.1) mg/kg 100 110. 110. 70-130 WG725665 Reactive CN (SW846 7.3.3.2) mg/kg .1 0.0933 93.3 50-150 WG725666 1,-1-Dichloroethene% - --mg/1- ----- -.025 .0.0209- - 83..7 .67.8-129 WG726036 1,2-Dichloroethane mg/1 .025 0.0207 82.9 68.8-124 WG726036 2-Butanone (MEK) mg/1 .125 0.0961 76.9 55-149 WG726036 Benzene;. .. - mg/l ...025. 0..0213 85.3.. .. 74.8-121 ,--WG726036 Carbon tetrachloride mg/1 .025 0.0211 84.3 70.2-123 WG726036 Chlorobenzene mg/l .025 0.0214 85.5 78.1-119 WG726036 Chloroform mg/l :025 0.0207 83.0 76-121 WG726036 Tetrachloroethene mg/l .025 0.0212 84.7 72.6-126 WG726036 Trichloroethene mg/l .025 0.0211 84.5 77.7-118 WG726036 Vinyl chloride mg/l .025 0.0226 90.2 65.9-128 WG726036 4-13romofluorobenzene 102.0 71-126 WG726036 Dibromofluoromethane 102.0 78.3-121 WG726036 Toluene-dS 104.o 88.5-111 W6726036 a,a,a-Trifluorotoluene 101.0 85-114 WG726036 * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 7 of 13 I *-,-ESC L•A•B S•C•f•E•N•C-E•S EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Corrosipi'ty.': Arsenic Baiium.;: Cadmium Chromium Selenium Silver Mercury Ignitability 2,4,5-TP (Silvex) 2',4-D` 2,4-Dichlorophenyl Acetic Aci 1,4-Di'chlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2-4-Dinitrotolu_ene Methylphenol 4-Methyl Phenol n.xachloro-1,3-butadiene Hexachlorobenzene Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine 2,4,,6--Tribromophenol 2-Fluorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-d5 p-Terphenyl-d14 Endrin Lindane Heptachlor Methoxychlor Decachlorobiphenyl Quality Assurance Report Level II L703709 d taboratory,5eoiitrol' Sample Units Known Val Result - - 6.33 .� - :. .6 3,0- mg/l 9 9.53 mg/l 9 9.54 mg/1 9 9.56 .. .. mg/I 9" - - 9. 68. . mg/l 9 9.44 mg/1 9 9.20 mg/1 .03 0.0283 ' -Deg.- F " 82 - - 84': 0 mg/l .005 0.00397 -mg/l .005 0:00382 mg/1 .025 0-.0106- mg/1 .025 0.0171 mg/1 .025 0.0149 mg/l .625 0.0168 mg/1 .025 0.0131 mg/l .025 0.0155 mg/1 .025 0.0127 mg/l .025 0.0157 mg/l .025 0.0118 mg/l .025 0.0174 mg/l .025 0.0120 mg/1 .025 0.0104 mg/1 .0002 0.000149 mg/l .0002 0.000140 mg/1 .0002 0.0000701 mg/1 .0002 0.000175 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 June 19, 2014 Rec Limit Batch .98:3-1'01.-7 .. WG726094 106. 80-120 WG726279 .106'. .•- 80-.120c icWG726279 106. 80-120 WG726279 106. 80-120 WG726279 108". _ 60-120,� '- WG726279 105. 80-120 W6726279 102. BO-120 WG726279 94.0 85-115 WG726271 " 102: 93-107- 'WG726283 79.4 57.6-129 WG726590 76.5 43.9-115 WG726590 68.50 22.9-153 WG726590 42-.6 21-89.4 WG726366 68.6 34.9-112 WG726366 59.4 29.8-107 WG726366 6.7..2 31.2-iO5 WG726366 52.4 26.4-86.9 WG726366 61.9 27.9-92 WG726366 50.9 16.1-104 WG726366 62.9 38.5-116 WG726366 47.4 16.5-89.8 WG726366 69:5 31.4-106 WG726366 47.9 10-97.4 WG726366 41.8 13.5-58.9 WG726366 60.20 11.2-130 WG726366 58.40 29.5-131 WG726366 47.10 10-77.9 WG726366 '72.80 21.8-123 WG726366 33.00 5-70.1 WG726366 54.00 29.3-137 WG726366 74.7 50.1-131 WG726582 69.9 54.7-125 WG726582 35.1 20.7-127 WG726582 87.6 48.2-144 WG726582 100.0 10-156 WG726582 72.20 13-9-137 WG726582 Laboratory Control Sample Duplicate Analyte Units Result Ref %Rec Limit RPD Limit Batch PH su 6.30 6.30 100. 98.3-101.7 0.0 20 WG725694 Reactive Sulf.(SW846 7.3.4.1) mg/kg 120. 110. 120. 70-130 8.70 20 WG725665 * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 8 of 13 'JOESC L-A-B S•C•I•E•N-C E•S EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Analyte Reactive';,.CN� ;(SW8,46..-.71'3-.3,.2) 1,1-Dichloroethene ,=Dichl`oroethane'-' 2-Butanone (MEK) Benzene Carbop,tetirachloride- Chlorobenzene Chloroform Tetrachloroethene Trichloroethene Vinyl chloride 4-Broin6fluorobenzene` Dibromofluoromethane Toluene-d8 a,a,a-Trifluorotoluene 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 Quality Assurance Report Level II L703709 June 19, 2014 `.,�Laborat"ory` Control* Sample``Duplicate, Units Result Ref %Rec Limit RPD Limit Batch ;mg/kg, 0.._0935` „, A,0933•- �94',0 _ '50-150_. , 0_:214s.. ,_ '.20'Y: .. .WG725666 mg/l 0.0254 0.0209 102. 67.8-129 19.3 20 WG726036 • mg, /1'..0':,0252.": :0.02,07--- �101--. .• - �-68..8-124_-.19-4.;:- �`20, =. ,.WG726036 mg/l 0.118 0.0961 94.0 55-149 20.1* 20 WG726036 mg/1 0.0256 0.0213 102. 74.8-121 1B.2 20 WG726036 mg/1` .6.02$Z- '0:021't,. .101. 70�:2-123.- 17':.7 20�- WG726036 mg/1 0.0243 0.0214 97.0 78.1-119 12.8 20 WG726036 mg/l 0.0250 0.0207 100. 76-121 18.5 20 WG726036 i6/l 6'.0238 0. 0212• 95'.0 72.6"126 ll.5 '20 -WG726036 mg/l 0.0253 0.0211 101. 77.7-118 18.0 20 WG726036 mg/l 0.0272 0.0226 109. 65.9-128 18.7 20 WG726036 _ � � - `98r30 ''71-126" WG726036 102.0 78.3-121 WG726036 104.0 88.5-111 WG726036 - - 99:7065-114 WG726036 Corrosivity 6.30 6.30 100. 98.3-101.7 0.0 10 WG726094 Arsenic mg/l 9.62 9.53 107. 80-120 1.00 20 WG726279 Barium mg/l 9.61 9.50 107. 80-120 1.00 20 WG726279 -Amium mg/l 9.65 9-54 107. 80-120 1.00 20 'WG726279 iromium mg/1 9.67 9.56 107. 80-120 1.00 20 WG726279 :ad mg/l 9.78 9.68 109. 80-120 1.00 20 WG726279 Selenium - m4/1 9.53 9.44 106: 80-120 1.00 20 WG726279 Silver mg/1 9.31 9.20 103. 80-120 1.00 20 WG726279 Ignitability Deg.-F 84.0 84=0 102: 93-107 0.00 20 •WG72G283 2,4,5-TP (Silvex) mg/l 0.00334 0.00397 67.0 57.6-129 17.3 20.7 WG72GS90 2;. 4-D, . mg/l. 0.00483 0.00382 97:0 43.9-115 23.3 28 WG726590 2,4-Dichlorophenyl Acetic Acid 66.40 22.9-153 WG726590 1,4-Dichlorobenzene mg/l -0.0114 0.0106 45'.0 21-89.4 6.51 32.6 WG726366 2,4,5-Trichlorophenol mg/l 0.0172 0.0171 69.0 34.9-112 0.110 23.9 WG726366 2,4,6-Trichlorophenol mg/l 0.0157 0.0149 63.0 29.8-107 5.25 24.1 WG726366 2-,4-Dinitrotoluene.. .- ... .. .. mg/1... .0169_ _ 0.0168- _ 67_0." ._" 31-2-105 0..300 22 WG726366 2-Methylphenol �mg/l 0.0133 0.0131 53.0 26.4-86.9 1.07 26.5 WG726366 3&4-Methyl Phenol mg/l 0.0157 0.0155 63.0 27.9-92 1.64 27 WG726366 Hexachloro-1,3-butadiene mg/l 0.0125 0:0127 50.0 16.1-104 1.67 31.2 WG726366 Hexachlorobenzene mg/1 0.0170 0.0157 68.0 38.5-116 7.60 20.1 WG726366 Hexachloroethane mg/l 0.0128 0.0118 51.0 16.5-89.8 7.B6 30.7 WG726366 Nitrobenzene' mg/1 _ 0.0164 0.0174- 66.0 31.4=106 5.80, 25.7 WG726366 ' Pentachlorophenol mg/l 0.0128 0.0120 51.0 10-97.4 6.25 35.1 WG726366 Pyridine mg/l 0.0105 0.0104 42.0 13.5-58.9 0.990 32.5 WG726366 2,4;6-Tribromophenol 63.90 11.2-130 WG726366 2-Flucrobiphenyl - 54.60 29.5-131 WG726366 2-Fluorophenol 41.50 10-77.9 WG726366 Nitrobenzene-d5 69.40 21.8-123 - WG726366 Phenol-d5 33.50 5-70.1 WG726366 p-Terphenyl-dl4 52.70 29.3-137 WG726366 * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 9 of 13 12065 Lebanon Rd. Mt. Juliet,TN 37122 (615) 758-5858 1-800-767-5859OESC Fax (615) 758-5859 L•A•B S. C•I•E•N•C•E•S - Tax I.D. 62-0814289 • e • Est. 1970 EHC, Inc. Mr. Thomas Ammons PO Box 902 Quality Assurance Report ' Level II Red Springs, NC 28377 June 19, 2014 L703709 :'LaliO`ratory{Pont=ol. Sample";Dup, licate Analyte Units Result Ref %Rec Limit RPD Limit Batch Eiidrin4.. . _ mg/1 . 0:.001'84 ."i. 0.,000149 92:0.,, _ 50:1-131- ,- �.2i:0 � ;29:1 _W . G726582 Lindane mg/1 0.000166 0.000140 83.0 54.7-125 17.1 21.1 WG726582 Heptachlor mg/l 0.000117 0.0000701 59.0 20.7-127 50.4* 30.5 WG726582 Me"-hoxycHlor= mg/1 -0-:'00,0212, -j,O:.000175 ''106.' - : 48:2-.144., ; 18':9• 27.8:. ;WG726582 Decachlorobiphenyl _111.0 10-156 WG726582 Tetrachloro-m-xylene 73.80 13.9-137 WG726582 Matrix.Spike Analyte Units MS Res Ref Res TV o Rec Limit Ref Samp Batch 1,77Dichl6roethene mg/1 1.16 0:0-' •1.25' 92.0 51.1-140 L702695-01 WG726036 1,2-Dichloroethane mg/1 1.28 0.0 1.25 100. 60-126 L702695-01 WG726036 2-13utanone (MEK) mg/l 6.51 0.0599 6.25 100. 22.4-138 L702695-01 WG726036 Benzene'".." - 64/1 1.26, 0:00271 1.25 100. "54:,3=-133 L762695-01 WG726036 Carbon tetrachloride mg/1 1.27 0.0 1.25 100. 55.7-134 L702695-01 WG726036 Chlorobenzene mg/1 1.36 0.0 1.25 110. 67-125 L702695-01 WG726036 Chloroform, mg/1 1.30 0.0 1.25 100'. 63=129 L702695=01 WG726036 Tetrachloroethene mg/1 1.23 0.0 1.25 98.0 53-139 L702695-01 WG726036 Trichloroethene mg/1 1.25 0.0 1.25 100. 44.1-149 L702695-01 WG726036 Vinyl chloride mg/1 1.13 0.0 1.25 90.01 47.8-137 L702695-01 WG726036 4-Bromofluorobenzene 103.0 71-126 WG726036 ^ibromofluoromethane 102.0 78.3-121 WG726036 ��-- oluene-d8 104.0 88.5-111 WG726036 ,a,a-Trifluorotoluene 101.0 85-114 WG726036 Arsenic mg/1 9.88 70.0344 9 110. 75-125 L703709-01 WG726279 Barium mg/1 9.77 0.108 9 110. 75-125 L703709-01 WG726279 Cadmium mg/1 9.89, 0.00598 9 110. 75-125 L703709-01 WG726279 Chromium mg/1 9.84 0.:0488- 9 110. -75-125 L703-709-01 W6726279 Lead mg/1 9.83 0.0196 9 110. 75-125 L703709-01 WG726279 Selenium mg/1 10.0 0.0599 9 110. 75-125 L703709-01 WG726279 Silver mg/1 9.44 0:00566 9 100. 75-125 L703709-01 WG726279 Mercury mg/1 0.0306 0.000234 .03 100. 80-120 L704070-02 WG726271 Mercury mg/1' 0.0302 0.000261 .03 100. 80-120 L704028-01 WG726271 2,4,5-TP (Silvex) mg/l 0.0329 0.0 .05 66.0 57.6-129 L703709-01 WG726590 2,4-D mg/l 0:0391 0.0 .05 - 78. 0, 43.9-115 L703709-01 WG726590 2,4-Dichlorophenyl Acetic Acid 72.50 22.9-153 WG726590 Endrin mg/1 0.00195 -0.0 .002" - 97..0 50.1-131 L703709-01 WG726582 Lindane mg/1 0.00164 0.0 .002 82.0 54.7-125 L703709-01 WG726582 Heptachlor mg/1 0.00131 0.0 .002 65.0 20.7-127 L703709-01 WG726582 Methoxychlor-" mg/1 0.00215 0.0 .002- 110. 48.2-144 L703709-01 WG726582 Decachlorobiphenyl 123.0 10-156 WG726582 Tetrachloro-m-xylene 76.60 13.9-137 WG726582 1,4-Dichlorobenzene mg/l 0.123 0.0 .25 49.0 14-104 L703833-02 WG726366 2,4,5-Trichlorophenol mg/l 0.173 0.0 .25 70.0 30.6-120 L703833-02 WG726366 2,4,6-Trichlorophenol mg/l 0.152 0.0. .25 61.6 19.1-114 L703833-02 WG726366 2,4-Dinitrotoluene mg/1 0.174 0.0 .25 70.0 16.2-135 L703833-02 WG726366_ 2-Methylphenol mg/1 0.133 0.0 .25 53.0 10-133 L703833-02 WG726366 3&4-Methyl Phenol mg/l 0.142 0.0 .25 57.0 17.4-100 L703833-02 WG726366 Hexachloro-1,3-butadiene mg/1 0.138 0.0 .25 55.0 15.7-109 L703833-02 WG726366 * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' . Page 10 of 13 12065 Lebanon Rd. *-ESC' - Mt. (615) Juliet, TN 758-5858 37122 1-800-767-5859 Fax (615) 758-5859 L•fr9 S•C•I•E•N•C•E'S Tax I.D. 62-0814289 _ • • Est. 1970 EHC, Inc. _ Mr. Thomas Ammons PO Box 902 Quality Assurance Report Level II Red Springs, NC 28377 June 19, 2014 L703709 ;Matrz,,$pke:; Analyte Units MS Res Ref Res TV % Rec Limit Ref Samp Batch Hezachlorobenzene::' ,. '.:- -, mg/1�•-_O i177_ 0::0; -;'.25:„�,":Zl>0..,.;': .;31.•9-135:, L703833.-.02' .WG726366 Hexachloroethane mg/1 0.149 0.0 .25 60.0 10.4-105 L703833-02 WG726366 Nitrobenzene mg/l 0.176 0.0 .25 70.0 23.1-121 L703833-02 WG726366 Pentachlo`r'opheiiol- mg/1 bi153;,;'''' ? 0't'0 25n'Y!,`- 61-V - 1-0; 108 L703833-02 WG126366 Pyridine mg/l 0.0966 0.0 .25 39.0 10-77.8 L703833-02 WG726366 2,4,6-Tribromophenol 68.00 11.2-130 WG726366 2-FluorobiphenyL - -,..60:50 29'.5-131, _ . - . :WG726366 2-Fluorophenol 41.40 10-77.9 WG726366 Nitrobenzene-d5 72.70 21.8-123 WG726366 Phenol-d5 29. 50- 5-70.1 WG726366 p-Terphenyl-d14 51. 90 29.3-137 WG726366 Matrix Spike Duplicate Analyte - Units MSD Ref %Rec Limit RPD Limit Ref Samp Batch 1,1-Dichlofoethene mg/1 1.06 1.16 84:8 51.1-140- 8.67 20.2 L70269.5-61 WG726036 1,2-Dichloroethane mg/1 1.20 1.28 96.1 60-126 6.38 20 L702695-01 WG726036 2-Butanone (MEK) mg/l 6.23 6.51 98.6 22.4-138 4.50 27 L702695-01 WG726036 Benzene mg/l 1.16 1.26 92.2 541.3-133 8.26 20 L702695-'01 WG726036 Carbon tetrachloride mg/1 1.17 1.27 93.4 55.7-134 8.51 20 L702695-01 WG726036 Chlorobenzene mg/l 1.24 1.36 98.9 67-125 9.23 20.3 L702695-01 WG726036 i -'ilorof orm mg/1 1.22 1.30 98.0 63'-.129 6.2.7 20 L702695-01 WG.72603G {` :trachloroethene mg/l 1.11 1.23 89.0 53-139 9.76 20 L702695-01 WG726036 :ichloroethene mg/1 1.14 1.25 91.3 44.1-149 9.37 20 L702695-01 WG726036 vinyl chloride mg/l 1.04 1.13 83.0 47'..8-137 8.39 20 L702695-01 WG726036 4-Bromofluorobenzene 103.0 71-126 WG726036 Dibromofluoromethane 103.0 78.3-121 WG726036 Toluene=d8_ _ _ 103.0 88:_5-111 WG726036 a,a,a-Trifluorotoluene 99.30 85-114 WG726036 Arsenic mg/-1 9.68.- 9.88 108. 75„125 2-00 20 L703709-01 WG726279 Barium mg/1 9.69 9.77 106. 75-125 1.00 20 L703709-01 WG726279 Cadmium mg/l 9.72 9.89 108. 75-125 2.00 20 L703709-01 WG726279 Chromium mg/1 9.73 9.84 108. 75-125 1.00 20 L703.709-01 WG726279 Lead mg/l 9.72 9.83 _ 10B. 75-125 1.00 20 L703709-01 WG726279 Selenium mg/l 9.72 10.0 107. 75-125 3.00 20 L703709-01 WG726279 Silver.. _. _ _. .. mg/l .9.39 .. .9.44,., .104. .357125". 1.00 20 L703709-01 WG726279 Mercury mg/1 0.0306 0.0306 101. 80-120 0.0 20 L704070-02 WG726271 Mercury mg/1 0.0304 0.0302 100. - 80-120 1.00 20 L704028-01 WG726271 2,4,5-TP (Silvex) m9/1 0.0326 0.0329 65.2 57.6-129 0.910 20.7 L703709-01 WG726590 2,4=D mg/1 0:0392 0.'0391 78.4 43.9-115 0.330 28 L703709-01 WG726590 2,4-Dichlorophenyl Acetic Acid 71.10 22.9-153 WG726590 Endrin mg/l 0.00178 0.00195' 89.2: 50'.1-131 8.82 29.1 L703109-01 WG726582 Lindane mg/l 0.00165 0.00164 82.6 54.7-125 0.980 21.1 L703709-01 WG726582 Heptachlor - mg/1 0.00137 0.00131 68.3 20.7-127 4.40 30.5 L703709-01 WG726582 Methoxychlor mg/1 0.00233 0:00215 li6. 48:2-144 8:01 -27.8 L703709-01 WG726582 Decachlorobiphenyl 100.0 10-156 WG726582 Tetrachloro-m-xylene 81.60 13.9-137 WG726582 1,4-Dichlorobenzene mg/1 0.135 0.123 53.9 14-104 8.91 36.4 L703833-02 WG726366 2,4,5-Trichlorophenol mg/1 0.185 0.175 74.1 30.6-120, 5.80 33.8 L703833-02 WG726366 * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 11 of 13 EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality"Assurance Report Level II L703709 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 - Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970. June 19, 2014 ,Matrix,Spike _ Duplicat`e. ' analvha Units MSD Ref 'Rec Limit _ RPD Limit Ref Samp Batch 2,.4, 6,_Trichlorophenol . .. m g/1 0.171 0{152 -'68.2._`.. • 19..T-114" -,'li703833-02'..•WGZ26366 2,4-Dinitrotoluene mg/l 0.185 0.174 73.8 16.2-135 5.98 20.6 L703833-02 WG726366 2-Methylphenol mg/l 0.137 0.133 54.7 10-133 2:47 40 L703833-02 WG726366 3&4=Methyl,-,Phenol-` '- mg/1; 0..143 O'.142;'^_ {57'4.^ •: .. 17,=i00 :;4 A,,6 -40s ': 2Z.7 r L703833-02 ..',WG726366 Hexachloro-1,3-butadiene mg/l 0.145 0.138 58.0 15.7-109 4.83 37.6 L703833-02 WG726366 Hexachlorobenzene mg/l 0.190 0.177 76.0 31.9-135 7.03 20 L703833-02 WG726366 Hexachlor6ethane mg/1' 0.-i52,: 0:149'-...�:60:'8'' 10:4=105 Li78 4d li703833'=02 •",WG726366 Nitrobenzene mg/1 0.178 0.176 71.3 23.1-121 1.45 29 L703833-02 WG726366 Pentachlorophenol mg/1 0.152 0.153 60.8 10-108 0-540 40 L703833-02 WG726366 Pyridine,``' mg/1 d'.i06 0°0966 _41.5' 10-77.8 9.59-,:':38.8 L703833-02 WG7.26366 2,4,6-Tribromophenol 70.30 11.2-130 WG726366 2-Fluorobiphenyl 65.60 29.5-131 WG726366 2-Fluorophenol- - 36 40 ' 10'77'.9 '•',WGI,26366 Nitrobenzene-d5 77.00 21.8-123 WG726366 Phenol-d5 25.10 5-70.1 WG726366 `WG726366 p-Tefpheriyl-d14 -59:80 29.3=137 Post. Spike . Serial Dilution Batch number /Run number / Sample number cross reference WG725694: R2938690: L703709-01 WG725665: R2939454: L703709-01 WG725666: R2939553: L703709-01 WG725842: R2939690: L703709-01 WG726036: R2939996: L703709-01 WG726052: R2940465: L703709-01 WG726094: R2940669: L703709-01 WG726279: R2941106: L703709-01 WG726271: R2941405: L703709-01 WG726283: R2941687: L703709-01 WG726590: R2942385: L703709-01 WG726366: R2942889: L703709-01 WG726582: R2943611: L703709-01 * * Calculations are performed prior to rounding of reported values. * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 12 of 13 F �_,,,OESC L-A-B S-C-I•E•N•C•E-B EHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L703709 The data package includes a summary of the analytic results of the quality control samples required by the SW-846 or CWA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. If a target parameter is outside the method limits, every sample that is effected is flagged .with the appropriate qualifier in Appendix B of the analytic report. Method Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytes above the reporting limit in the method blank are qualified with the "B" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control". If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "J4" qualifier for all effected samples. Matrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spiked with known concentrations of target analytes. The percent recovery of the target analytes also has statistical control limits. If any recoveries that are outside the method control limits, the sample that was selected for matrix spike/matrix spike duplicate analysis is flagged with either a "J5" or a "J6". The relative percent difference (%RPD) between the matrix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. i - Page 13 of 13 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-600-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 June 19, 2014 Company I Address: E�lll!ri6 Informationro five 10 of Otis" EEC, Inc. " Mr. Thomas Ammon s El L PO Bpi 902 ,P2 <S Red Springs PQ Box,? ings,NC 28377 -orihas.NC 28377 Red S ;f 4. Report to1/1 L F122', 1.11;1'�e I �* k) malts:'' j A7, Project city/satr 41300)". D riplion "YV c 6so 56' "N Phone: 14� -91 ft E .,ESC. Ke�, il"S' 250ti SitelFac lit cted by. (print) /1' - ,, '4 L .:,y P.Q.# Collected bY(,s 4tliately Pocked on Ice IN Y Sample ID (LaP MUST Be Noti.fied) Some Day... , .. 200% Next Day ........ 100% Two Day. , , . , ...50% Three Day ....... 25% Date Results Neede Email? No Yes FAX? _No�__Yes Comp/Grab I Matrle I Do pth Date Time No. of 0, Remat3fContaminant I 'Sanl'plasthbaw "PMMMMMMMM 14AM11-- I.- :14trix SS- So!VSolid GW - Groundwater VVW - WasteWater DW - DrinkIng Water OT - Other 7e*V d.0-7(. /39T Rerh2rks, r7 kt T "T TIN PH Temp Flow odder qUisl�b b Relln ipRture) Relli Date. Time: • Z ,7—t 4' Received by: Si nature IK Recived p molts returried via: DUPS FedEx ElCourier D aes A Dates Time: 0 list '11M N, Date: Time: Ti Rellnciulshed by: 4 a Pathogen and Vector Attraction Reduction Form PATHOGEN REDUCTION AND VECTOR ATTRACTION DEDUCTION The current permit, WQ0004893 does not have vector or pathogen requirements. This is a non- biological wastewater treatment plant and will not require vector attraction reduction. Pathogen certification will be included as soon as it is required by the permit. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Campbell Soup Supply Company Permit Number: WQ0004893 WWTP Name: Campbell Soup Supply Company NPDES Number: WQ0003626 Monitoring Period: .'From . 1/1/2014. To 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and. alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4❑ Alternative 5 0 Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Y Gamma Ra Y ❑ Pasteurization ❑ Class B: Alternative 1❑ Alternative-2 ❑ Alternative 3 ❑ If applicable to alternative performed (Class'B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting El7 Aerobic Digestion ❑ e ® . Anaerobic Dt soon g If applicable to alternative performed (Class A.or Class B) complete the following monitoring data: Parameter*' Allowable Level in Sludge Pathogen Density Number of Exccc= deuces Frequency of Anal 'sis Sample Typie Analytical Tech - niame .m Geo. Mean Maximuty Units Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of Current permit WQ000489.3 does not have Vector or Pathogen requirements. 1000 mpn per, gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ I Option 2 ❑ Option 3 ® joption 4 ❑ Option 5., ❑ Option 6 _ ❑ Option 7 ❑ Option 8 ❑ I Option 9 ❑ loption 10 ❑ No vector attraction re duction options ❑ s were performed p P CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR_ 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify; under penalty of law, that the pathogen requirements in 40 CFR 503.32'and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction ,and supervision in accordance with the system designed to ensure that qualified personnel properly gather, and evaluate the information used to. determine that the. pathogen. and vector attraction reduction requirements have been met.. I. am aware; that there are significant penalties for false certification including fine and imprisonment."' Al 64 riarer Name and Title (type or print) /,4ignature of Preparer Date a Land Applier Name and Title. (if applicable)(tyl% or print) ignature of Land Applier (if applicable) Date 4 � 4 DENR FORM RF (5/2003) Pathogen and Vector Attraction Reduction Documentation PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The current permit, WQ0004893 does not have vector or pathogen requirements. This is a non - biological wastewater treatment plant and will not require vector attraction reduction. Pathogen certification will be included as soon as it is required by the permit. Soil Analysis Report Page 1 of 5 Report Numbil"� '.:If-302-0766 Account Num�_.. _ J0327 0 Send To: EHC Inc. wwwaleastem.com PO Box 902 RED SPRINGS NC 28377 Date Received: 10/29/2014 Date Of Analysis: 10/30/2014 A&L( 7-astern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 Grower: SLUDGE SITES SOIL ANALYSIS REPORT Date Of Report: 10/30/2014 Analytical Method(s): Mehlich 3 Farm ID: Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g SITE 1 05639 3.6 M 113' 169 VH 131 VH 75 M 323 L 21 VL 4.8 6.70 2.3 5.0 NC=141 NC=67 SITE 2 05640 1.6 L 73 64 H 90 M 169 H 808 M 13 VL 6.4 0.6 6.3 NC=53 NC=46 SITE 3 05641 3.2 M 109 65 H 50 L 37 L 255 L 13 VL 4.7 6.75 1.8 3.5 NC=54 NC=26 SITE 4 05642 1.3 L 73 61 H 22 VL 33 M 216 L 14 L 5.2 6.85 0.8 2.2 NC=51 NC=11 SITE 5 05643 6.2 H 150 187 VH 129 H 216 H 823 M 18 VL 5.8 6.78 1.5 7.8 NC=156 NC=66 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI Field ID % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm SITE 1 20 M 11.3 VH 13 M 174 VH 1.3 M 0.3 VL 0.2 VL 6.7 12.5 32.3 1.8 46.5 NC=42 NC=282.5 NC=81 NC=65.0 SITE 2 12 L 3.4 M 33 H 106 VH 1.4 M 0.3 VL 0.1 VL 3.7 22.4 64.1 0.9 8.9 NC=25 NC=85.0 NC=206 NC=70.0 SITE 3 L 2.2 L 8 L 64 VH 1.1 M VL 0.11 VL 3.7 8.8 36.4 1.6 50.5 �13 10.1 NC=27 NC5.0 NC=50 NC=55.0 SITE 4 L 2.6 M 14 M 91 VH 0.9 M 0.1 VL 0.07 VL 2.6 12.5 49.1 2.8 34.7 �12 NC=25 NC=65.0 NC=88 NC=45.0 SITE 5 L H ' VH VH 1.6 H 0.2 VL VL 4.2 23.0 52.8 1.0 19.0 �14 �4.7 �,79 1159 10.16 NC=29 NC=117.5 NC=494 NC=80.0 Values on this report represent the plant available nutrients in the . Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: q�Aytia me Gp�� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. TT C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 5 Report Numb. '4-302-0766 Account Number 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received: 10/29/2014 ❑atp of Rpnnrt- 1n/3n/2n14 �y Ak :astern Laboratories ;. A� 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastem.com Grower: SLUDGE SITES Farm ID: SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P z O s Kz O M g S Zn Mn Fe Cu. B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A SITE 1 Bermuda, Coastal 5 1.8 75 0 224 5 14 0 2 0 0 0.5 SITE 1 Grass(Small Grain) 5 1.8 100 0 174, 5 8 0 2 0 0 0 SITE 2 Grass(Small Grain) 5 0.0 100 30 200 0 17 0 0 0 0 0 SITE 2 Bermuda, Coastal 5 0.0 75 30 338 0 23 0 0 0 0 0.5 SITE 3 Grass(Small Grain) 5 1.5 100 30 200 43 -T 16 0.9 3 0 0 0 SITE 3 Bermuda, Coastal 5 1.5 75 30 400 43 22 0 3 0 0 0.5 SITE 4 Bermuda, Coastal 5 0.8 75 30 452 47 23 0 2 0 0 0.5 SITE 4 Grass(Small Grain) 5 0.8 100 30 200 47 17 0.7 2 0 0 0 SITE 5 Grass(Small Grain) 5 0.8 100 0 200 0 15 0 0 0 0 0 SITE 5 Bermuda, Coastal 5 0.8 75 0 262 0 21 0 0 0 0 0.5 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Paudc McGroary Page 3 of 5 - --- - Report Numb �'-4-302-0766 v Account NUrriRiVu 00327 � wnMnraleastem,com Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Sample(s) : SITE 2,SITE 3,SITE 4,SITE 5 Crop: Bermuda, Coastal Apply additional 65 pounds of nitrogen after every Cutting and harvest of hay. Boron recommendations are on a broadcast basis. AEI ---astern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 Grower: SLUDGE SITES Farm ID: The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. Sample(s) : SITE 3,SITE 4 Crop: Bermuda, Coastal Apply dolomitic lime to raise pH and improve the magnesium level. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." fl M Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 Gam« OF work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 4 of 5 Report Numb' l`4-302-0766 Account Num.- . J0327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Ne wwwaleastem.com Date Received: 10/29/2014 Date Of Analysis: 10130/2014 A&I _. `=astern Laboratories 7621 Whitepine Road Richmond, Virginia.23237 (804) 743-9401 Fax (804) 271.8446 Grower: SLUDGE SITES SOIL ANALYSIS REPORT Date Of Report: 10/30/2014 Analytical Method(s): Mehlich 3 Farm, ID: Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number o ENR /o Rate Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g SITE 6 82 H 42 L 103 H 456 M 17 VL 05645 1.9 L 82 5.7 6.84 0.9 4.2 NC=68 NC=21 SITE 7 151 VH 75 M 93 VH 337 M 19 LF6 05646 1.5 L 76 0.2 2.9 NC=126 NC=38 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample Field ID ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm SITE 6 L4.5 H 36 H 132 VH 1.1 M 0.2 VL 0.1 VL 2.6 20.4 54.3 1.8 21.123 7NC NC=112.5 1 NC=225 NC=55.0 SITE 7 9 VL 2.5 M 25 H 113 VH 1.1 M VL 0.06 VL 6.6 26.7 58.1 2.8 5.9 �0.1 - NC=19 NC=62.5 NC=156 NC=55.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A, This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. �« me �� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories,, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 5 of 5 Report Numb 4-302-0766 Account Numper: 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received: 10/29/2014 Date Of Report: 10/30/2014 At A& --astern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 0 www.aleastem,com Grower: SLUDGE SITES Farm ID: SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A lb/A lb/A Ib/A Ib/A lb/A Ib/A ib/A lb/A Ib/A Ib/A SITE 6 Bermuda, Coastal 5 0.8 75 30 428 0 24 0 0 0 0 0.5 SITE 6 Grass(Small Grain) 5 0.8 100 30 200 0 18 0 0 0 0 0 SITE 7 Bermuda, Coastal 5 0.0 75 0 333 0 26 0 0 0 0 0.5 SITE 7 Grass(Small Grain) 5 0.0 100 0 200 0 20 0.8 0 0 0 0 Comments: Sample(s) : SITE 7 Crop: Bermuda, Coastal Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. Boron recommendations are on a broadcast basis. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary 2014 Application Summary Table Campbell Soup Supply Company Land Applicat ' rogram Permit #WQ0004893 2014 Appf i n Summary Farmer Tract/S_ ite Field Acres Date Spread Gallons Pounds Dry Tons/Acre Dry Tons % Solids Crop PAN Dry Tons/Acre Dry Tons Campbell Soup Supply Company S 1 5.1 1/28/14 10,398 86,720 ' 0.3690 1.8818 4.34 Rye Grass 43.65 2.3227 11.8457 5/5/14 18,748 156,360 ' 0.1426 0.7271 0.93 Bermuda 5/19/14 15,988 133,340 0.1216 0.6200 0.93 Bermuda 9/3/14 12,050 1 100,500 ,, 0.1370 0.6985 1.39 1 Bermuda 10/14/14 17,746 148,000 0.6907 3.5224 4.76 Bermuda 10/21/2014 5,004 41,740 0.1948 0.9934 4.76 Bermuda 10/28/2014 17,141 142,960 0.6671 3.4024 4.76 Bermuda Campbell Soup Supply Company S 2 8.4 1/20/14 13,600 113,420 0.2930 2.4612 4.34 Rye Grass 41.60 2.3421 19.6738 2/7/14 15,173 126,540 0.3269 2.7459 4.34 Rye Grass 5/9/14 17,333 144,560 0.0800 0.6722 0.93 Bermuda 5/29/14 13,691 114,180 0:0632 0.5309 1 0.93 Bermuda 5/30/14 7,971 66,480 0.0368 0.3091 0.93 Bermuda 6/9/14 9,048 75,460 0.0418 0.3509 0.93 Bermuda 11/4/14 18,501 154,300 0.4372 3.6723 4.76 Rye Grass 11/11/14 12,909 107,660 0.3050 2.5623 4.76 Rye Grass 11/15/14 15,343 127,960 0.3626 3.0454 4.76 Rye Grass 11/19/14 16,743 139,640 0.3956 3.3234 4.76 Rye Grass Campbell Soup Supply Company S 3 26 1/2/14 13,631 113,680 0.0949 2.4669 4.34 Pine Trees 15.07 1.0824 28.1412 2/28/14 10,616 88,540 0.0739 1.9213 4.34, Pine Trees 3/3/14 9,600_ _ 80,060 0.0668 1.7373 4.34 Pine Trees 3/13/14 17,758 148,100 0.1236 3.2138 4.34 Pine Trees 3/25/14 14,998 125,080 0.1044 2.7142 4.34 Pine Trees 4/3/14 14,863 123,960 0.0222 0.5764 0.93 Pine Trees 4/17/14 17,686 147,500 - 0.0264 U859 0.93 Pine Trees 8/22/2014 16,631 138,700 0.0371 0.9640 1.39 Pine Trees 9/16/2014 15,309 127,680 0.0341 0.8874 1.39 Pine Trees 9/30/2014 15,386 128,320 0.0343 0.8918 1.39 Pine Trees 10/8/2014 18,017 150,260 ; 0.1375 3.5762 4.76 Pine Trees 11/28/2014 21,050 175,560 0.1607 4.1783 4.76 Pine Trees 12/10/2014 7,950 66,300 0.0607 1.5779 4.76 Pine Trees 12/31/2015 13,854 115,540 : 0.1058 2.7499 4.76 Pine Trees Campbell Soup Supply Company S 4 9.1 1/14/14 16,165 134,820 ; 0.3215 2.9256 4.34 Rye Grass 22.45 1.7817 16.2134 2/18/14 24,388 203,400 0.4860 4.4138 4.34 Rye Grass 7/14/14 18,038 150,440 0.1149 1.0456 1.39 Bermuda 8/5/14 16,058 133,920. 0.1023 0.9307 1.39 Bermuda 8/15/14 15,249 127,180 0.0971 0.8839 1.39 Bermuda 12/16/14 12,993 108,360 -: 0.2834 2.5790 4.76 Rye Grass 12/26/14 17,304 144,320 0.3775 3.4348 4.76 Rye Grass Campbell Soup Supply Company S 5 3.4 1/6/14 15,885 132,480 0.8455 2.8748 4.34 Rye Grass 47.81 2.9424 10.0041 6/26/14 7,010 58,460 0.0800 0.2718 0.93 Bermuda 7/24/14 16,830 140,360 0.2869 0.9755 1.39 Bermuda 12/4/14 15,988 133,340 0.9334 3.1735 4.76 Bermuda 12/10/14 13,645 113,800 : 0.7966 2.7084 4.76 Bermuda Campbell Soup Supply Company S 6 2.3 6/24/14 8,185 68,260 0.1380 0.3174 0.93 Bermuda 6.97 0.3198 0.7355 6/26/14 10,782 89,920 0.1818 0.4181 0.93 Bermuda Campbell Soup Supply Company S 7 2.5 1 6/9/14 6,374 53,160 0.0989 0.2472 0.93 Bermuda 29.32 1.3288 3.3219 6/17114 14,441 120,440 0.2240 0.5600 0.93 Bermuda 10/21/2014 9,976 83,200 0.7921 1 1.9802 1 4.76 Bermuda 11/4/2014 2,693 22,460 0.2138 1 0.5345 1 4.76 Rye Grass Number of Field Applied to: 56.8 686,740 5,727,420 89.9357 Campbell Soup Supply Company DAF Sludge, Maxton , NC I Gallons I Pounds . Dry Tons 2014 Application Condition Summaries Campbell Soup Supply Company Maxton, North Carolina Farmer: Campbell Soup Supply Company Site/Tract: S Field: 1 Residual Report No: 14-059-0205 WQ0004893 1st Quarter DAF Residuals 5.1 Application Method: Surface Percent Solids: 4.34 Crop: Winter Rye Grass Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 1/28/2014 1 1 10,398 Dry Clear 0 I Total Gallons 1 1 10,398 1 1 1 1 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter ®AF Residuals Farmer: Campbell Soup Supply Company 5.1 Site/Tract: S Application Method: Surface Field: 1 Percent Solids: 0.93 Residual Report No: 14-092-0202 Crop: Winter Rye Grass Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 5/5/2014 1 18,748 Dry Clear 0 5/19/2014 1 15,988 Dry Clear 0 Total Gallons 1 1 34,736 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company 5.1 Site/Tract: S Application Method: Surface Field: 1 Percent Solids: 1.39 Residual Report No: 14-190-0216 Crop: Bermuda Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 9/3/2014 1 12,050 Dry Clear 0 Total Gallons 12,050 M Campbell Soup Supply Company Maxton, North Carolina WQ0004893 4th Quarter DAF Residuals Farmer: Campbell Soup Supply Company 5.1 Site/Tract: S Application Method: Surface Field: 1 Percent Solids: 4.76 Residual Report No: 14-280-0207 Crop: Bermuda Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 10/14/2014 1 17,746 Dry Rain 0.2 10/21/2014 1 5,004 Dry Clear 0 10/28/2014 1 17,141 Dry Clear 0 Total Gallons 39,891 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 1st Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 8.4 Site/Tract: S Application Method: Surface Field : 2 Percent Solids: 4.34 Residual Report No: 14-059-0205 Crop: Winter Rye Grass Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 1/20/2014 2 13,600 Dry Clear 0 2/7/2014 2 15,173 Dry Clear 0 Total Gallons 28,773 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company 8.4 Site/Tract: S Application Method: Surface Field : 2 Percent Solids: 0.93 Residual Report No: 14-090-0202 Crop: Winter Rye/Bermuda Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 5/9/2014 2 17,333 Dry Clear 0 5/29/2014 2 13,691 Dry Clear 0 5/30/2014 2 7,971 Dry Rain 0.1 6/9/2014 2 9048 Dry Cloudy 0 Total Gallons 1 48,043 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 4th Quarter DAF Residuals Farmer: Campbell Soup Supply Company 8.4 Site/Tract: S Application Method: Surface Field: 2 Percent Solids: 4.76 Residual Report No: 14-280-0207 Crop: Bermuda Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 11/4/2014 2 18,501 Dry Clear 0 11/11/2014 2 12,909 Dry Clear 0 11/15/2014 2 15,343 Dry Cloudy 0 11/19/2014 2 16,743 Dry Clear 0 Total Gallons 63,496 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 1st Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 26 Site/Tract: S Application Method: Surface Field: 3 Percent Solids: 4.34 Residual Report No: 14-059-0205 Crop: Pine Trees Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 1/2/2014 3 13,631 Dry Rain 0.4 2/28/2014 3 10,616 Dry Clear 0 3/3/2014 3 9,600 Dry Rain 0.4 3/13/2014 3 17,758 Dry Clear 0 3/25/2014 3 14,998 Dry Rain 0.1 Total Gallons 66,603 --'s Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 26 Site/Tract: S Application Method: Surface Field: 3 Percent Solids: 0.93 Residual Report No: 14-092-0202 Crop: Pine Trees Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 4/3/2014 3 14,863 Dry Clear 0 4/17/2014 3 17,686 Dry Cloudy 0 Total Gallons 32,549 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 26 Site/Tract: S Application Method: Surface Field: 3 Percent Solids: 1.39 Residual Report No: 14-190-0216 Crop: Pine Trees Weather Date Field No. Gallons Soil Conditions Conditions 8/22/2014 3 16,631 Dry Clear Prev. 24 Hour Rainfall 0 9/16/2014 3 15,309 Dry Cloudy 0 9/30/2014 3 15,386 Dry Rain 0.3 Total Gallons 47,326 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 4th Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 26 Site/Tract: S Application Method: Surface Field: 3 Percent Solids: 4.76 Residual Report No: 14-280-0207 Crop: Pine Trees Weather Date Field No. Gallons Soil Conditions Conditions 10/8/2014 3 18,017 Dry Clear Prev. 24 Hour Rainfall 0 11/28/2014 3 21,050 Dry Clear 0 12/10/2014 3 7,950 Dry Clear 0 12/31/2014 3 13,854 Dry Cloudy 0 Total Gallons 60,871 Campbell Soup Supply Company Maxton, North Carolina Farmer: Campbell Soup Supply Company Site/Tract: S Field: 4 Residual Report No: 14-059-0205 WQ0004893 1st Quarter DAF Residuals Acres: 9.1 Application Method: Surface Percent Solids: 4.34 Crop: Winter Rye Grass Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 1/14/2014 4 16,165 Dry Rain 0.1 2/18/2014 4 24,388 Dry Clear 0 Total Gallons Campbell Soup Supply Company Maxton, North Carolina Farmer: Campbell Soup Supply Company Site/Tract: S Field: 4 Residual Report No: 14-190-0216 WQ0004893 3rd Quarter DAF Residuals Acres: 9.1 Application Method: Surface Percent Solids: 1.39 Crop: Bermuda Date Field No. Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 7/14/2014 4 18,038 Dry Clear 0 8/5/2014 4 16,058 Dry Cloudy 0 8/15/2014 4 15,249 Dry Clear 0 Total Gallons Campbell Soup Supply Company Maxton, North Carolina WQ0004893 1st Quarter ®AF Residuals Farmer: Campbell Soup Supply Company Acres: 3.4 Site/Tract: S Application Method: Surface Field : 5 Percent Solids: 4.34 Residual Report No: 14-059-0205 Crop: Pine Trees Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 1/6/2014 5 15,885 Dry Rain 0.1 Total Gallons 15,885 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 3.4 Site/Tract: S Application Method: Surface Field : 5 Percent Solids: 0.93 Residual Report No: 14-092-0202 Crop: Bermuda Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 6/26/2014 5 7,010 Dry Clear 0 Total Gallons 7,010 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Site/Tract: S Field: 5 Residual Report No: 14-190-0216 Date Field No. Gallons 7/24/2014 5 16,830 Total Gallons Acres: 3.4 Application Method: Surface Percent Solids: 1.39 Crop: Bermuda Weather Prev. 24 Hi Soil Conditions Conditions Rainfall Dry Cloudv 0 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 4th Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 3.4 Site/Tract: S Application Method: Surface Field: 5 Percent Solids: 4.76 Residual Report No: 14-280-0207 Crop: Bermuda Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 12/4/2014 5 15,988 Dry Cloudy 0 12/10/2014 5 13,645 Dry Rain 0.1 Total Gallons 29,633 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 2.3 Site/Tract: S Application Method: Surface Field : 6 Percent Solids: 0.93 Residual Report No: 14-092-0202 Crop: Bermuda Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 6/24/2014 6 8,185 Dry Cloudy 0 6/26/2014 6 10,782 Dry Clear 0 Total Gallons 18,967 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 2.5 Site/Tract: S Application Method: Surface Field: 7 Percent Solids: 0.93 Residual Report No: 14-092-0202 Crop: Bermuda Grass Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 6/9/2014 7 6,374 Dry Clear 0 6/17/2014 7 14,441 Dry Cloudy 0 Total Gallons 20,815 Campbell Soup Supply Company Maxton, North Carolina Farmer: Campbell Soup Supply Company Site/Tract: S Field: 7 Residual Report No: 14-280-0207 WQ0004893 4th Quarter DAF Residuals Acres: 2.5 Application Method: Surface Percent Solids: 4.76 Crop: Bermuda Grass Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 10/21/2014 7 9,976 Dry Clear 0 11/4/2014 7 2,693 Dry Clear 0 I Total Gallons 1 1 12,669 1 1 1 1