HomeMy WebLinkAboutWQ0004893_Residual Annual Report 2014_20150219�� o 60 Z, 7
CAMPBELL SOUP SUPPLY COMPANY, LLC
LAN® APPLICATION ANNUAL REPORT 2014
PERMIT #WQ0004693
2120 NC 71 Highway North 3iE'
Maxton, NC 28364
February 16, 2015
North Carolina Department of Environment and Natural Resources
Aquifer Protection Section
1617 Mail Service Center
Raleigh, NC 27699-1617
Reference: 2014 Land Application Annual Report
Campbell Soup Supply Company
Maxton, North Carolina
Permit No. WQ0004893
Information Processing Unit:
Enclosed Campbell Soup Supply Company is submitting all monitoring and reporting
mo information as required in the referenced permit'for the facility in Maxton, North Carolina. This
report includes: 1) Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual
Metals Field Loading Summary Forms, 4) Annual Land Application Field Summary Form, 5)
Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen and Vector Attraction Form,
8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data, 10) 2014
Application Summary Table, and 11) Application Condition Summaries. This is a non-503
permit that is not required to have pathogen reduction or vector attraction reduction requirements
to be met.
A total of 686,740 gallons (89.9357 dry tons) of industrial residuals were land applied to 56.8
acres.
If any further information is required regarding this land application program, please do not
hesitate to contact me at (910) 844-1654.
Sincerely,
amie C. Collins
Environmental & Facilities Manager
TABLE OF CONTENTS
I Certification Form
II Annual Residual Sampling Summary Form
III Annual Metals Field Loading Summary Forms
IV Annual Land Application Field Summary
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction Form
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Report
X 2014 Application Summary Table
XI 2014 Application Condition Summaries
Certification Form
ANNUAL LAND.APPLICATION CERTIFICATION FORM
Permrt#: WQ0004893 County: Robeson Year: 2014 .
Facility Name (as shown on permit): Campbell Soup Supply Company
-Land Application'Operator: -Campbell Soup.Supply Company Phone:. (910) 844-5.631 •-.
PP. Y P g.• P
and a hcation.of residual.sohds as allowed b the ermit occurred- the ast:ca . - " lendaryear? ..'.
RI, .Yes ❑ No If No,'skip Part A; and Part B and proceed to`the certification. Also., if.residuals were. .
generated but not land applied; please -attach an explanation on how the residuals were handled.
Part'Ac:
Total number. of application fields in permit: 7 .
Total number of acres land.application occurred during the year':. 56.8:
Part B:
Facility. was compliant during:calendaryear .2014 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water-Resources.0 Yes ❑ No'.
If no please, provide a written description why the facility was. not compliant, the dates, and explain .
corrective action taken. .
1. Only'residuals approvedfor this permit were applied to .the permitted sites..
2. Soil pH was adjusted as specified in the permit. and, lime was applied (if. needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils -analysis were performed on each site receiving residuals during.the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed -and three (3) copies of certified.laboratory results are attached..
` All other monitoring was performed in. accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not, exceed any of the Pollutant Concentration Limits in Table 1- of.40 CFR Part 503.13 or the
Pollutant Loading.Rates in Table 2 of 40 CFR part 503.13. (applicable to 40 CFR Part 503 regulated facilities)..
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part. 503.14 were
complied 'with.(applicable. to 40 CFR Part 503 regulated:'facilities).
8. All operations and maintenance requirements .in. the permit were complied with or, in the' case of a deviation,
prior authorization was received from the Divisio"n of Water Resources.
9. No contravention. of Ground Water.'Quality Standards occurred at a'monitoririg well or explanations .of .
violations are attached to include appropriate actions and remediations.
10..Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan-:
:11.. No runoff of residuals from the application.sites onto adjacent property ornearby,surface-waters has occurred::
12. All.buffer'regpirements as specified on,.the.permit were maintained during each application. of residuals:
"I certify 'under penalty of law, that the above information is, to the best of my knowledge and belief, true,.,
accurate; and complete. I am .aware, that there, are significant penalties for submitting false information; -
including the possibility of fines and imprisonment for knowing vio ati s
"Michael G:Miller - Sr..Dir. Of Operation_ s 2 1��
Permittee Name and Title (type or print) . � . - Signature of Pen'nittee Date
-4.
-
Si nature of Preparer* Date Signature of. -Land Applier - Date
.(if different from Permittee) ; (if different from Permittee and Preparer)
* Preparer is defined in 40 CFI .Part'503 9'(r)
DENR FORM ACF (5i2003)
Annual Residual Sampling Summary Form
ANNUAL RESIDUAL SAM LTG SUMMARY FORM
Attach this form to the corresponding Annual.Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0004893- Laboratory: 1) A & L Eastern Laboratories, Inc. -
Facility Name: Campbell Soup Supply Company 2)
NPDES # or WQ0003.626 3)
WQ#:
4)
WWTP Name: Campbell Soup Supply Company - DAF 5)
R.,Qidnal Ana1v6.c data
Sample or
Composite Date
2/27/14
4/1/2014
7/7/2014
10%6/2014
Percent Solids
4.34
0.93
1.39
4.76
Arsenic
NR
NR
NR
NR
Cadmium
2
2
2
2
Chromium
NR
NR
NR
NR
Copper
7
25.
50
23.
Lead
5
5
5
5..'
Mercury
NR
NR
NR
NR
Molybdenum'
NR
NR
NR
NR
y
Nickel'
7
21
45 .
28
Selenium
NR
NR
NR,
NR
Zinc
141
364
236
284.
Total Phosphorus
744
1090
1970
1400
TKN
6680
24700
12200
27100
Ammonia -Nitrogen
461
9680
2160
2310
Nitrate and Nitrite
134
53.8
14.4
2
"I certify, .under penalty of law, that this document was prepared under my direction or -supervision in' accordance. with a system.
designed to. assure that qualified personnel properly gathered and evaluated, the, information submitted. I.am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Si1rhature. of Preparer Date
DENR.FORM RSSF.(5/2003),
ANNUAL RESIDUAL -SAN.. SING SUMMARY FORM
Attach this form to the corresponding Annual Report,
Please note that your permit may contain additional parameters to be analyzed than those required to, be summarized on this form.
Permit Number: WQ0004893 Laboratory: 1) A & L Eastern Laboratories, Inc.
Facility Name: Campbell Soup Supply Company 2)
NPDES # or 3)
WQ#.. WQ0003626
4)
WWTP Name:, Campbell Soup Supply Company- DAF 5)
RPcirinal Analveic data
Co I• •site • , I
®
, ,
®®®
, ' I
®.®®®'
I
®
•'
®
,• •1
•
� •
�
11
®
III
S�-®
"I certify, .under penalty of law, that this document was prepared under my direction or supervision in accordance with 'a system .
designed to assure that, qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Si nature of Preparer
12 - /d - iS
Date
DENR FORM RSSF-B-(5/2003)
Annual Metals Field Loading Summary Forms
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 11.84628
Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0
1' ator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company
acres Used: 5.1 Acres Permitted: 5.1 Site #: S Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
Ill
2/27/14
_2j
4/1/14
3
7/7/14
4
10/6/14
5
6
7
8
9
10
11
12
% Solids
4.34
0.93
1.39
1 4.76
Arsenic
0
0
0
0
Cadmium
2
2
2
2
Chromium
0
0
0
0
Copper
7
25
50
23
Lead
5
5
5
5
Mercury
0
0
0
0
Molyb-
denum
0
0
0
0
Nickel
7
21
45
28
Selenium
0
0
0
0
Zinc
141
364
236
284
Total
Phos-
nhn,.ug
744
1090
1970
1400
-
ial Heavy Metal Field Loadings (Calculated in lbs/acre):
0
1
L 2
3L_j
L4J
5j
6j
L7J_8
9j
10
11
12
•`,
d--
o
0.369
0.2642
0.137
1.5526
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0.0015
0.0011
0.0005
0.0062
0
0
0
0
0
0
0
0
0.0093
hromi
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0.0052
0.0132
0.0137
0.0714
0
0
0
0
0
0
0
0
0.1035
0.0037
0.0026
0.0014
0.0155
0
0
0
0
0
0
0
0
0.0232
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0.0052
0.0111
0.0123
0.0869
0
0
0
0
0
0
0
0
0.1155
I
0
0
0
0
0
0
0
0
0
0
0
0
0
0.1041
0.1923
0.0647
0.8819
0
0
0
0
0
0
0
0
1.2429
0.5491
0.576
0.5398
4.3473
0
0
0
0
0
0
0
0
6.0121
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
i d " mation submitted. I am aware that there are significant penalties for submitting false information,
i ding the possibility of fines and imprisonment for knowing violations"
s .2-/G-/�
Sigdture of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
�. Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 19.67364
Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0
Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company
Acres Used: 8.4 Acres Permitted: 8.4 Site #: S Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
2/27/14
2/27/14
4/1/14
4/1/14
10/6/14
% Solids
4.34
4.34
0.93
0.93
4.76
Arsenic
0
0
0
0
0
Cadmium
2
2
2
2
2
Chromium
0
0
0
0
0
Copper
7
7
25
25
23
Lead
5
5
5
5
5
Mercury
1 0
0
0
0
0
Molyb-
denum
0
0
0
0
0
Nickel
7
7
21
21
28
Selenium
0
0
0
0
0
Zinc. _
_ 141 __.
141.
3M4
364
284,
L
744
744
1090
1090
1400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
� o
o "
0.293
0.3269
0.18
0.0418
1.5004
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0.0012
0.0013
0.0007
0.0002
0.006
0
0
0
0
0
0
0
0.0094
Chromiurr
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0.0041
0.0046
0.009
0.0021
0.069
0
0
0
0
0
0
0
0.0888
Lead
0.0029
0.0033
0.0018
0.0004
1 0.015
0
0
1 0
0
1 0
0
0
10.0234
Mercury.
0
0
0
0
0
0
0
0
0
0
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0041
0.0046
0.0076
0.0018
0.084
0
0
0
0
0
0
0
0.102
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
0.0826
0.0922
0.131
0.0304
0.8522
0
0
0
0
0
0
0
1.1885
Total
Phos-
0.436
0.4864
0.3924
0.0911
4.2011
0
0
0
0
0
0
0
5.6071
horns
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
S gnature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 19.6352
Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0
Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company
Acres Used: 26 Acres Permitted: 26 Site #: S Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
2/27/14
2/27/14
2/27/14
4/1/14
7/7/14
7/7/14
10/6/14
% Solids
4.34
4.34
4.34
0.93
1.39
1.39
4.76
Arsenic
0
0
0
0
0
0
0
Cadmium
2
2
2
2
2
2
2
Chromium
0
0
0
0
0
0
0
Copper
7
7
7
25
50
50
23
Lead
5
5
5
5
5
5
5
Mercury
1 0
0
1 0
0
1 0
0
1 0
Molyb-
denum
0
0
0
0
0
0
0
Nickel
7
7
7
21
45
45
28
Selenium
0
0
0
0
0
0
0
Zinc
141
141
141
364
236
236
284
Total
Phos-
horus
744
744
744
1090
1970
1970
1400
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
C o
�a�
y
CD d
o
0.0949
0.0739
0.2948
0.0486
0.0371
0.0684
0.1375
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0.0004
0.0003
0.0012
0.0002
0.0001
0.0003
0.0006
0
0
0
0
0
0.003
Chromiurr
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0.0013
0.001
0.0041
0.0024
0.0037
0.0068
0.0063
0
0
0
0
0
0.0258
Lead
0.0009
0.0007
0.0029
0.0005
0.0004
0.0007
0.0014
0
0
0
0
0
0.0076
Mercury
1 0
0
0
0
0
1 0
0
1 0
0
0
0
0
1 0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0013
0.001
0.0041
0.002
0.0033
0.0062
0.0077
0
0
0
0
0
0.0257
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
0.0268
0.0208
0.0831
0.0354
0.0175
0.0323
0.0781
0
0
0
0
0
0.294
Total
Phos-
0.1412
0.11
0.4387
0.1059
0.1462
0.2695
0.385
0
0
0
0
0
1.5965
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, '
including the possibility of fines and imprisonment for knowing violations"
-2-Id - /.S
Si ature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 16.21347
Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0
Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company
Acres Used: 9.1 Acres Permitted: 9.1 Site #: S Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
2/27/14
2/27/14
7/7/14
7/7/14
10/6/14
% Solids
4.34
4.34
1.39
1.39
4.76
Arsenic
0
0
0
0
0
Cadmium
2
2
2
2
2
Chromium
0
0
0
0
0
Copper
7
7
50
50
23
Lead
5
5
5
5
5
Mercury
1 0
0
0
0
0
Molyb-
denum
0
0
0
0
0
Nickel
7
7
45
45
28
Selenium
0
0
0
0
0
Zinc
141
141
236
236
284
Total
Phos-
horus
744
744
1970
1970
1400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
o
� t7
o "
0.3215
0.485
0.1149
0.1994
0.6609
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0.0013
0.0019
0.0005
0.0008
0.0026
0
0
0
0
0
0
0
0.0071
hromiu
0
0
0
� 0
0
0
0
0
0
0
0
0
0
Copper
0.0045
0.0068
0.0115
0.0199
0.0304
0
0
0
0
0
0
0
0.0731
Lead
0.0032
0.0049
0.0011
0.002
0.0066
0
0
0
0
0
0
0
0.0178
Mercury
0
0
0
0
0
0
0
0
0
0
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0045
0.0068
0.0103
0.0179
0.037
0
0
0
0
0
0
0
0.0766
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
0.0907
0.1368
0.0542
0.0941
0.3754
0
0
0
0
0
0
0
0.7512
Total
Phos-
0.4784
0.7217
0.4527
0.7856
1.8505
0
0
0
0
0
0
0
4.2889
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
SiiKature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 10.00416
Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0
Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company
Acres Used: 3.4 Acres Permitted: 3.4 Site #: S Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
2/27/14
4/1/14
7/7/14
10/6/14
% Solids
4.34
0.93
1.39
4.76
Arsenic
0
0
0
0
Cadmium
2
2
2
2
Chromium
0
0
0
0
Copper
7
25
50
23
Lead
5
5
5
5
Mercury
0
0
1 0
0
Molyb-
denum
0
0
0
0
Nickel
7
21
45
28
Selenium
0
0
0
0
Zinc
141
364
236
284
-Total
Phos-
horus
744
1090
1970
1400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
ti o
a�
o
CD
��a
o �
0.8455
0.08
0.2869
1.73
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0.0034
0.0003
0.0011
0.0069
0
0
0
0
0
0
0
0
0.0118
Chromiun
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0.0118
0.004
0.0287
0.0796
0
0
0
0
0
0
0
0
0.1241
Lead
0.0085
0.0008
0.0029
0.0173
0
0
0
0
0
0
0
0
0.0294
Mercury
1 0
0
1 0
0
0
0
0
1 0
0
0
0
0
1 0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0118
0.0034
0.0258
0.0969
0
0
0
0
0
0
0
0
0.1379
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
0.2384
0.0582
0.1354
0.9826
0
0
0
0
0
0
0
0
1.4147
Total
Phos-
1.2581
0.1744
1.1304
4.844
0
0
0
0
0
0
0
0
7.4069
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 0.73554
Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0
Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company
Acres Used: 2.3 Acres Permitted: 2.3 Site #: S Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
o
�a�
y
0
o
0.3198
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0.0013
0
0
0
0
0
0
0
0
0
0
0
0.0013
Chromiun
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0.016
0
0
0
0
0
0
0
0
0
0
0
0.016
Lead
0.0032
0
0
0
0
0
0
0
0
1 0
0
0
0.0032
Mercury
0
0
1 0
0
0
1 0
0
0
0
0
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0134
0
0
0
0
0
0
0
0
0
0
0
0.0134
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
0.2328
0
0
0
0
0
0
0
0
0
0
0
0.2328
Total
Phos-
0.6972
0
0
0
0
0
0
0
0
0
0
0
0.6972
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
2:2 � V -/14-/S
Si ature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 3.322
Permit #: WQ0004893 Cation Exchange Capacity (non 503 only): >5.0
Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company
Acres Used: 2.5 Acres Permitted: 2.5 Site #: S Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Rase Percent #):
Sample
or Com-
posite
Date
4/1/14
10/6/14
10/6/14
% Solids
0.93
4.76
4.76
Arsenic
0
0
0
Cadmium
2
2
2
Chromium
0
0
0
Copper
25
23
23
Lead
5
5
5
Mercury
1 0
0
1 0
Molyb-
denum
0
0
0
Nickel
21
28
28
Selenium
0
0
0
Zinc
364
284
284
Total
Phos-
horus
1090
1400
1400
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�o
�J y w
H
0
o
0.3229
0.7921
0.2138
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0.0013
0.0032
0.0009
0
0
0
0
0
0
0
0
0
0.0053
Chromiutr
0
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0.0161
0.0364
0.0098
0
0
0
0
0
0
0
0
0
0.0624
Lead
0.0032
0.0079
0.0021
0
0
0
0
0
0
0
0
0
0.0133
Mercury
1 0
0
0
0
0
0
0
0
0
0
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0.0136
0.0444
0.012
0
0
0
0
0
0
0
0
0
0.0699
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
0
0.2351
0.4499
0.1214
0
0
0
0
0
0
0
0
0
0.8064
LPhorus
0.7039
2.2179
0.5986
0
0
0
0
0
0
0
0
0
3.5204
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
Annual Land Application Field Summary
ANNUAL LAND APPLICATIOT ELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX_ WHEN NOT APPLICABLE.
Facility Name:'. ..Campbell Soup Supply Company Permit #: WQ0004893 Annual Dry Tons Applied: 11:84540458
Owner: Campbell. Soup Supply Company ..'Operator: Campbell Soup Supply Company Cation Exchange Capacity (non 503): >5.0.
Site #:. S. Field #: 1 AcresUtilized: 5.1. Acres Permitted: 5.1
o"
0
o
A
>:
Specify,
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Sources
(Summarize)
site
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
- tili-
zation
Rate* *
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
-Must Select
Cro 1 or Crop
p p
2
*=
Gal.:
Cu.Yd.
. .
Report
Totals
in Gal.
crop 1
"Crop 2
Jan 14.
10398 -
2038.8-
4.34
0.368982205
DAF. -
Dry
.0
S
0.5
0.4
6680
461
134
#######
2.10475
Rye
1
May 14
. 34736.
6811
0.93
0.264136631
DAF
Dry
0
S
.0.5
0.4-
24700
9680
53.8
5.75913
#######
Bermuda
2
.Sep 14.
12050 ..2362.7
L39
0.136951794
DAF
Dry
0
S
0.5
0.4
12200
2160
14.4
1.39976
#######
Bermuda
3
Oct 14
" 39,891
1821.8
4.76
1.55255772
DAF
Dry
0
S
0.5
0.4-
27100
2310
2
34.3829
#######
Bermuda
4
0
0
0
0
5
0
.0
0
0
-
6-
0
0
0
0.
7
0
0
0
0
8
0
0
0
0.
9
0
0.
-0
0
=
10
0 :
0
0
0
11
0
0
0
0
12
TOTALS:
19034
::::::::::::::::
As
Cd '
Cr
Cu
Pb
Hg
Mo
Ni
Se'
Zn
P
-PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0
0.00929
0
0.1035
9.02323
0
0
0.11554
0
1.24294
6.01209.
41.5418
2.10475
Date
lbs/ac
Current Cumulative lbs/ac
0 0.00929 0 0.1035 0.02323 0 0 0.11554 0 1:24294:'.'•.'•>.'•.'•::::::::`::':::.'::'::::::::::`:::::::::
............
100 50
Prior. Years Cumulative lbs/ac .
Permitted C. P. L. R.
Permit PAN Limit l st/2nd Crop
"I certify, under. penalty of law, that this document was prepared.under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I.am aware that there are
significant penalties for submitting false information; including the possibility of fines'and imprisonment_ for: knowing violations."
-2 -1d - i-s *Application Method: S - Surface, IN --Injection, INC - Incorporation
Signature of Land Applier Date *.*Volatilization Rate: Surface - 0.5. Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate.
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be -entered into
the same numbered column. on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column #.1.
DENR FORM FSF (5/2003):
ANNUALLAND APPLICATIOP ' 'ELD SUMMARY FORM
.
PLEA, . • iVIAKE A COPY OF THIS BLANK FORM TO BE COMP: 'ED AND SUBMITTED FOR EACH APPLICATION FIE] -
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: - Campbell Soup Supply Company . Permit #: WQ000493 Annual Dry Tons Applied: 19.67388361
Owner: -Campbell. Soup Supply Company Operator: Campbell Soup Supply Company 'Cation Exchange Capacity (non 503): >5.0
Site #:.: S Field #: 2 Acres Utilized: 8.4 Acres Permitted: 8.4.
o
Specify
Totals
Per
Acre
% :
Solid
s
Dry- Tons Per
.Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
nation
Rate* *
Miner-
ali-
nation
Rate
TKN
Ammo
nia-
Ni-
trogeri
= Ni-
trate
and
Nitrite
PAN 1
PAN -2
Must Select
Crop 1.or Crop
2
*:
*.
Gat.
Cu.Yd.
Report
Totals
in Gal.
Crop i
rCrop 2
Jau.14
13600
1619
4.34
0.293012 -
DAF.
Dry
0
S
6.5
0.4
6680
461
134
#######
1.6714
Rye
1
Feb 14
15173
1806.3
4.34
0.326902285
DAF
Dry
0
S
0.5
0.4
6680
461
134
#######
1.86472
Rye .
2
May 14
38995
4642.3
0.93
0.180031559
DAF
Dry
0
S
0.5
0.4.
24700
9680
53.8
3.92534
#######
Bermuda
3
Jun 14
9048
1077.1
0.93
0.041772677:
DAF.
Dry
0
S
0.5
0.4
24700
9680
53.8
0.91079
#######
Bermuda
4
Nov 14
. 63496
7559
4.76
1.50041048
DAF
Dry
0 -
S
0.5
0.4
27100
2310
2.
1#######
33.2291
Rye.
5
0
0 ..
0
0
6
0
0
0
0
7
0
0
0
0
8.
a..
0
-0
0
0
9
0
0
0
1 0
10
'0
0
„
0
0
11
0..
0
0
0
12
TOTALS:
16704
:::::::::::`::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
R
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0
0.00937
0
0.08879
0.02342
0
0
0.10202
0
1.18851
5.60706
14.83613
36.7642
Date
lbs/ac
Current Cumulative lbs/ac .
0 0.00937 0 0.08879 0.02342 0 0 0.10202 0 1.18851 ::::'? : »»:::::: »>:
299 50
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
it PAN Limit 1 st/2nd Crop
Perm L p
"I certify, under penalty of law, that this document was prepared under my direction or supervision'm accordance with a system .
designed to -assure that qualified personnel properly gathered. and evaluated the information submitted. I am aware that there are
-significant penalties for submitting false information, including the possibility of fines 'and imprisonment for knowing violations."
*Application Method: S - Surface, IN Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation -,1.0.
* * * C.P.L.R.: Cumulative Pollutant Loading Rate
- . The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this informationneeds to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF.row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
ANNUAL LAND APPLICATIOT . ELD SUMMARY FORM
PLEASE.MAKE,A COPY. OF -THIS BLANK FORM TO BE COMPLETED AND SUBMITTED•FOR EACH APPLICATION'FIELD.
PLACE A "N/A". IN A BLANK OR BOX WHEN NOT APPLICABLE. .
Facility Name: Campbell Soup Supply Company. ' _ Permit #: WQ0004893 Annual Dry Tons Applied: 28.1415
Owner: Campbell Soup Supply Company Operator: Campbell. Soup Supply Company Cation Exchange Capacity (non.503):
Site #: -S Field #: 3 Acres Utilized: 26. Acres Permitted: 26
�
4.
A
Specify
Totals-
-.
Per
.Acre.
%
Solid
s
- -
Dry Tons Per
:
Acre
Residual
Sources
(Summarize}
Site
Cond.
Dry,
Wet
Moist
Inches-
Precip.
Past 24
Hrs:
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
T&N
Ammo
ma-
Ni-
trogen
Ni--
trate
and
Nitrite
PAN 1
PAN 2
Must Select ..
Crop 1 Qr..Crop
2
*:
.
Gal.
CuNd.
. •
Report
Totals
in Gal.
Crop T
.Crop 2
Jan 14
13631
52421
4.34 -
0.094881197
DAF
:Dry
0
S
0.5
0.4
6680
461 '
134
0.54122
#######
Pines
1
Fe1i'14
10616
40831
4:34
0.07389471
DAF
Dry
0
S
0.5
0.4
6-
461
134
0.42151
#######
. Pines
2.
ivlai 14
42356
1629.,1
: 4.34 .
0.294827083
DAF,
Dry
0.
S
0.5
0.4.
6680
461.
134.
1.68175
#######
. Pines:
3'
Apr 14
32549
1251.9-
0.93
0.048549337,
DAF .
Dry
0
S-
0.5
0.4
24700
9680
53.8
1.05.855
#######
. Pines
4
Aug 14_
'1663.1
'639.65
1.39 :
_ 0.037076256
DAF.
Dry
0
S .
0.5.
0.4 ,
12200
2160
14A_
0.37895
#######
Pines-
5
Sep 14.
30695
.1.180.6
1.39.
°0.06842978.
DAF
Dry,
0
S
-0.5, :
0.4
1.2200..
2160 . _
14.4
0.69941
.#######
' Pines
6
Oct 14
18017
692.96
- 4.76
0.137547322
DAF
'Dry
0
S
1 0.5
0.4
27100
2310
2
3,04612
#######
Pines
7
Nov 14
2105.0
809.62
4.76 .
0A6070207.DAF
Dry .
0
S
0.5
0.4
27100
2310
2
3.55891
#######.
' Pines
'
8
Dec 14
21804
83 $.62
4.76,
6.1664H445 :
• • DAF
Dry
0
S
0.5
.0.4 '
27100
2310
2
:3.68639
1 #######
: Pines'
9
1Q
..
11
12
TOTALS:
7975
`:: °'::`:
As
Cd
Cr
Cu
Pb
H
Mo
Ni.
Se.
' Zn
P
PAN.1
PAN 2
Lime A
lied .
Annual.lbs/acre,.
0. -
0.00302
0.
0.0258
0.00755
0_ •
b .
0.02573
0 ,:.
0.29401
1.59645
15.07281
0
Date.
lbs/ac.
Current Cumulative lbs/ac
0 0.06302 0 . - 0.0258 0.00755 0' 0 0.02573' 0 0.29401 '
60.
Prior Years Cumulative lbs/ac
Pemitted C. P. L. R.
2 r
Permit PAN Limit 1st/ nd C o Perm L x P
"I certify, under penalty:of law, that -this document was prepared under my direction or supervision in accordance with a system.
designed to assure that.qualifed personnelproperly gathered and'evaluated the information submitted. I am aware that there are:
significant penalties for. submitting false information, including: the possibility of fines and imprisonment for knowing violations."
*Application.Method: S - Surface: -Injection, INC -Incorporation
Signature of Land Applies Date . **Volatilization Rate: Surface 7-0.5, Iniection/Incorporation - 1:0
***C.P.L.R.: Cumulative Pollutant Loading Rate .
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered.into -
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column #.1.
PLEA:..,-. `,MAKE A COPY OF THIS BLANK FORM TO BE COMP__ _'ED AND. SUBMITTED FOR EACH APPLICATION FIEL_:
PLACE A -"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Campbell Soup Supply Company . Permit #:. WQ0004893
Owner:
Site #:
Campbell Soup Supply Company Operator: Campbell Soup Supply Company
S Field #:. 4 Acres Utilized: 9.1.
Annual Dry Tons Applied: 16.2.1309719
Cation Exchange Capacity (non 503): >5.0
Acres Permitted: 9.1
o °
�,
0 o
Specify
Totals
Per
'Acre..:
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
1 e .
Cond.
Dry,
Wet,
-Inches
Precip.
Past 24
Hr8.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
. zation
Rate
TKN
Ammo
ma-
Ni-
trogen
Ni-
trate
and .
Nitrite
PAN 1
PAN2
1Vlust Select
Crop 1 or Crop'
p
2
Gal..
..
Cu.Yd.
1:1Jan
Report
Totals .
in Gal.
Crop 1
Crop 2
14
16165
1776.4
4.34
0.321484546
DAF
Dry
0
S
0.5
0.4
6680
461
134
#######
1.8338.1
Rye
.1
Feb 14
24388 -
2680
4.34
0.48502104
DAF
Dry
0
S
0.5
0.4
6680
461
134
#######
2.76666
Rye .
2
Jul 14
18038
-1982.2
1.39
0.114894131
DAF
Dry
0
S
0.5
0.4
12200
2160
14.4
1.17431
#######
Bermuda
3
Aug 14
31307
3440.3
1.39;
0.199411829_
DAF
Dry.
01.
S
0.5
.0.4
12200
2160
14.4
2.03815
#######
Bermuda
.
4'
Dec 14
30297
3329J
4.76
0.660847486
DAF
Dry
0
S
0.5
0.4
27100
2310
2
#######
' 14.6351
1 Rye
5
0
0
0
0
6
0
0
0
0
7.
0
0
0.
0
$
0
0
0
0
9
0
0
0
0
10
0..
0
0
0
11
0
p
0*.
0 ..
12
TOTALS:
13208
:::"
As
Cd
Cr
Cu
Pb.
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN
Lime'A
lied
Annual lbs/acre
0
0.00713
0
0.07312
0.01782
0
0
0.07659
0
0.75117
4.28893
3.21246
19.2356
. Date
lbs/ac
Current Cumulative lbs/ac.-
0 0.007.13 0 . 0.07312 0.01782 0 0 0.07659 0 0.75.117..............:::.......:....:.:.:.:::.:....
1 10 50
Prior Years Cumulative lbs/ac
Permitted C. P. L: R.
2 r
Perm Permit PAN Limit 1st/ nd Crop p
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system .
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that thereare
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application. Method: S -Surface, IN Injection,. INC -Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorooration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered: on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the'MFLSF as is. entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF 'row # 1 to MFLSF column # 1.
ANNUAL LAND APPLICATIOr rAELD SUMMARY FORM
-PLEASE MAKE.A COPY_ - OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Campbell Soup Supply Company Permit #: WQ0004893 Annual Dry Tons Applied: - 10.-00412107
Owner: Campbell .Soup Supply Company Operator:. Campbell Soup Supply Company Cation Exchange Capacity (non 503): ->5.0.
Site #: .S.:Field #: 5 Acres Utilized: 3.4. Acres Permitted: 3.4
o-
„ �
o ..
Specify--
Totals
Per
Acre
. %
Solid
s
Dry Tons Per
Acre
Residual .
Sources .
(Summarize)
i e
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-'
trogen
Ni-
trate -
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop.
p p.
2 _
Gal.
CuNd.
Report
Totals
in Gal.
Crop 1
Crop 2
Jan 14
.15885
4672.1
4.34
0.845539862
DAF - -
Dry
0 ..
S
0.5
0.4
6680
461
134
#######
.4.82313
-
Rye
1
Jun 14.
7010
2061.8
0.93
0.079957297
DAF
Dry
0
S
0.5
0A
24700
_ 9680
53.8
1.74336
#######
Bermuda
2
Jul 14
-168-30.
4950
.1.39-
0.28691685.
DAF
Dry.
0
S
0.5
0.4
12200.
2160
14.4 .
2.93252
#######
Bermuda
3•
Dec 14
: 29633
8715.6
4.76
1.72997454
DAF
Dry
0 •
S
0.5
0.4
27100
2310
.2:
#######
38.312
Rye: -
4
p..
0
0
-0
5
0--
0
•0'
0
6:
0
0
0
0
7.
0
p
0
0
8
0
0..
0
0
9
O..
0
0
10
0
0
0..
.0.
11
0
0
0.
0
12
TOTALS:
20399
::::::::::::::::
As
Cd
Cr
..Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
.0
0.01177
0
0.12411
0.02942
0
0
0.1379
0
1.41473
7.40689
4.67588.
43.1351
Date
lbs/ac
Current Cumulative lbs/ac
0 = 0.01177 0 0.12411 0.02942 0 0 0.1379 0.. 1.41473::::::::::::::::::::
50
Prior. Years Cumulative lbs%ac
Permitted C. P. L. R.
i Limit lst/2nd Cropllb
Perm t PAN
" I certify, under. penalty of law, that this document was prepared under my direction ,or supervision in accordance with a system
designed to assure that qualif ed personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including'the possibility of fines'and imprisonment for knowing violations." .
-16 -%S' *Application Method: S - Surface, IN --Injection, INC = Incorporation
Signature of Land Applies Date **.Volatilization Rate: Surface - 0,5; Iniection/Incorporation - 1.0 -
* * * C.P.L.R.: Cumulative Pollutant Loadinz Rate. : .
***.* The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and. MFLSF are mathematically linked so'this information needs to be entered into
the same numbered column, on=the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF. row # 1. to MFLSF column # 1.
ANNUAL. LAND APPLICATIOT ., ,, _ELD SUMMARY FORM
PLEASE MAKE A COPS. OF.THIS BLANK FORM TO. BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A". IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name:- Campbell Soup Supply Company. 'Permit #: WQ0004893 Annual Dry Tons Applied: 0.735559227
Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Cation Exchange Capacity (non.505): >5.0
-Site #: S Field #: 6 Acres Utilized: 13. Acres Permitted:. 23
o
o
A
s eci
Totals.
- Per
Acre
%_
Solid
-s:
Dry Tons Per
-
Acre'
Residual
Sources
(Summarize) .
i e
Cond.
Dry,
= � Wet, :
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od *
Vola-
tili-
zation
Rate *�
Miner-
ali- ,
zation
Rate
TKN
Ammo
nia-
Ni-
trogen"
Ni-
trate
-
and
Nitrite
:.
PAN .1
PAN 2
Must Select . .
Crop 1 or Crop
p p
2
* ,
* .
1.
Gal.
Cu.Yd.
..
:::
Report
Totals
in Gal.:
Crop 1
Crop 2
Jun 14
18967 � �.
8246.5'
0.93.
-0.31980836
DAF .
Dry
0
S
0.5
0.4
24700
•9680
53.8
16,97297
#######
Bermuda
.
1
0
0
'0
2
0:
0
0
0.
3'
0.
0
0
0 ..
4.
0-
0. ..
0
0
5
0
0
0
6
0
0 -
0:.
.0-
7
0
0
0 ..
0
8.
0.,
0
0
0..
9
0 .
0.
0
0
10
0.
.0.
0' .
0 ,
11
0.
-0
0
0
12
TOTALS:.
8247
:::.......
As
Cd
Cr
:Cu.
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annual lbs/acre
0
0.00128
0
.0.01599
. 0.0032
0
0
0:01343
0
0.23281-
0.69716.
6.97297.1
0
Date
- lbs/ac
Current Cumulative lbs/ac
0 0.00128 0 0.01599 0.'0032 0. 0. 0.01343 0,. 0.23281:::::::::::::..........::::`:::::::::::::::::
224 50
Prior. Years Cumulative lbs/ac
Permitted C. P: L. R.
i • it 'Ts 2nd Cro
L Permit PAN m t1 p .
"I certify, under. penalty of -lawthat this document was prepared.under,my direction.br_supervision.in accordance with a system
designed to assure that qualified personnel properly gathered and. evaluated the information submitted. I.am aware :that there are
significant penalties -for submitting. false Information, including the possibility of fines'and imprisonment, for knowing violations."-
/� -/� *Application Method:. S -Surface, IN - Injection, INC - Incorporation
Signature of Land Applies Date **.Volatilization Rate: Surface - 0.5, Iniection/Incorporation
* * * C.P.L:R.: Cumulative Pollutant Loading Rate
The RSSF Data and the Dry- Tons.Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are, mathematically linked so this information needs to be -entered into
the same numbered. column. on the MFLSF as is entered on the identically numbered FSF row to. properly complete the metals equations: ie. FSF row #.1 to MFLSF-column.# 1.
ANNUAL LAND APPLICATIO1', _ _ZELD SUMMARY FORM
PLEASE, MAKE A COPY OF THIS BLANK FORM, TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A". IN A•BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name:. Campbell Soup Supply Company Permit #: WQ0004893 . Annual Dry Tons Applied: 3.321921663 '
Owner: Campbell Soup Supply Company Operator: Campbell. Soup Supply Company Cation Exchange Capacity (non 503): >5.0
Site #: S Field #: 7 Acres Utilized:, 2.5 Acres Permitted: 2.5.,
o .
Q
-Specify
Totals
Per
Acre
• %
. Solid
a
Dry Tons Per
Acre
Residual
- Sources
(Suminarize)
.61 e
Cond.
Dry,
- Wet,
Inches
Precip:
Past 24
I
Appli-
-cation
Meth-
*
odist.
Vola-
tili- .
zation
Rate **
Miner-
ali-
zation
Rate
TKN
Amino
nia-
Ni---
trogen
Ni-
trate
and-
Nitrite_
PAN .l
T
PAN 2
Must Select '
Crop 1 or Crop
2
Gal. Gal.
Cu.Yd.
Report
- .Totals
in Gal. -
Crop l
_Crop 2
Jun-14
- - 20815.
8326
0.93
0.322890606
DAF
Dry
0
S
0.5
0.4' -
24700
9680
- 53.8
7;04018
#######
Bermuda-
1
Oct 14:
9976 :
3990.4
4.76
0.792062477
DAF
Dry
0
S -
0.5
0.4 -
27100
2310
2.
17.541
#######
Bermuda
2
Nov 14,
2693 .
1077.2
.4.76
0.213815582
DAF
Dry.
0
S - .
0.5 ..
0.4 ..
'27100,
2-310
:2
#######
4.73516
Rye
3
0
0
.0
4
0
0.
0
0
5
0.:0
'
.0
0
6
0
0.
0:
0.-
7
0
p
0
0
8
0
p
0.
0
9
p
0
0
10
__..:
0.
:'
0.
0.
0
11
0..
0
0
.0
12
TOTALS-...
13394
::::::::::::::::
.,As.:
Cd
Cr
Cu
Pb"
Hg
Mo
Ni
Se •
. Zn
P
PAN'1
I PAN 2
Lime Applied
Annual lbs/acre
.0
0.00532
0
-0.06242
.0.01329
0
0
0:06989
0 :
0.80642
3.52044.
24:58I2
4.73516
' Date
lbs/ac
Current'Cumulative lbs/ac
0' 0:00532 0 0.06242 0.01329 0 0 0.06989 0:0:80642 ::::::::::::::::: `
............................................................•.•........•. .
2 4 50
2
Prior. Years Cumulative lbs%ac
Permitted C.T. L. R. * *
1 t/2nd Crop
rmit PAN Limrt s Pe P
"I certify, under penalty, of law; that this document -was prepared under my direction or supervision in accordance witn a system
designed to assure that qualified -personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false.information; including the possibility of fines: and imprisonment for: knowing violations."
�-14 _/jC- *Application Method: S - Surface, IN --Injection, INC : Incorporation
Signature of Land Applier Date "volatilization Rate: Surface - 0.5,- Iniection/Incorvoration =1.0.
***C.P.L:R.: Cumulative -Pollutant Loading Rate:
* * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically -linked so this information needs to be entered into
the same numbered.column on:the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1-to MFLSF colurun.# 1.
Residual Analysis Lab Sheets
t
Page: 1-of 2
Report Number: 14-059-0205L
A&L Eastern Laboratories, Inc..,
Account Number: 00327
7621 Whitepine Road Richmond, Virginia 23237,
(804) 743-9401 Fax (804) 271-WS
Submitted By: GRADY DOBSON
www.aleastern.com
Send Tor EHC Inca
Project: CAMPBELL SOUP DAF
PO, Box 902
NC CERT#257
RED SPRINGS , 'NC 28.377
REPORT OF ANALYSIS
Date Sampled: 2/27/2014 11:30:00
Lab Number: 98171
,Date Received: 02/28/2014 00:00
Sample Id : DAF 1ST QTR A
Date Reported: 03/07/2014
..
PARAMETER
.
QUANTITATION
LIMITANALYSIS
D.
•.
Total Solids
4.34
43400
100.0
JM
03/04/2014 09:20
SM-2540G
Moisture "
95.66.
100.0
JM
03/04/2014 09:20
SM-2540G
Total Kjeldahl Nitrogen
0.67
6680
10.0
JM
03/03/2014 07:54 SM-4500-NH3C-TKN
Total Phosphorus
007
744
100
KM
03/03/2014 12:51
SW 6010C
Total Potassium
0.11
1080
100
KM
03/03/2014 12:51
SW 6010C
Total Calcium
0.15
1510
100
KM
03/03/2014-12:51 .
SW 6010C
Total Magnesium
0.02
194
100
KM
03/03/2014 12:51
SW 6010C
Total. Sodium
0.08
814 .
100
KM
03/03/2014 12:51
SW 6010C
Total Aluminum
600
100
KM
03/03/2014 12:51
SW 6010C
Total Copper
7
5
KM
03/03/2014 12:51
SW 601 OC
Total Zinc
141
5
KM
03/03/2014 12:51
SW 6010C
Ammonia Nitrogen
0.05
461
10.0
JM
03/03/2014 07:54
SM-4500-NH3C
Organic N
0.62
6219
10.0
03/03/2014 07:54
CALCULATION
Nitrate+Nitrite-N
134.
2.00
JM
03/03/2014 07:55
SM-4500NO3F
.Total Cadmium
<2.0
.2.0
KM
03/03/2014 12:51
SW 6010C
Total Nickel
7
5
KM
03/03/2014 12:51
SW 6010C
Total Lead
<5
5
KM
03/03/2014 12:51
SW 6610C
PH (Standard Units) *
3.70
2.00
JM
03/03/2014 09:09
SW-9045D
All values are on_ a dry weight basis except as noted by asterisk. Detection limit on all N
series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients,
and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our
prior written authorization.
Debbie Holt
i
Page: 2 of 2 Report Number: 14-059-0205 w A&L. EaStel71 Laboratofies, Inc.
Account Number: 00327 � � 7621 Whitepine Road Richmond, Virginia23237 (804)743.9401 Fax (B04)271.6446
Submitted By:: GRADY DOBSON wll uleastemcom
Send To: EHC Inc. Project: CAMPBELL SOUP DAF .
PO Box 902 NC CERT#257
RED SPRINGS NC 28377
REPORT OF ANALYSIS Date Sampled: 2/27/201411:30:00
Lab Number.: 98171 'Date Received: 02/28/2014 00:00
Sample Id : DAF 1 ST QTR A Date Reported: 03/07/2014
Comments:
ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al"., "CA", AND "NO3/NO2=N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N".
ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.-�
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SAMPLE TRANSNIITTA
A&L E step
7621_ WWWDim Read Rich
1oil il i lii1 l 1,11, 1 o 14
ENC lqc. 1
GAF 1ST QTR A
f3fHoe
SUbr�iiRte�t3
..To
CopY To
Ptaed
RADY DOBSON
ApotRem!
9
!onj-
POS 902
Esiail
RED SPRING$ NC 29S.77ab
1�9tttttDer (t,ab USo._...
a ID_ ._
_ .1909 -._.... 53rrt _%d Dab,AA7/
i3a>g: find:
`i� 1
: r�o� s, .�d �rfts«
T,
Is._c�.
:►: I
Rai'
i• d
.:' tt'atut+e
Dale
Tinia Rc�eiu04 BY: Slgnatur� .
Date
Time
..E49i
F0c,
IH
I J -:
Please
P[a.ce a- "X"
4y
Desired Test$.
Internal
Lab Code:
.
TKN
P
K
S Ca
ma 1Fe Al 01.
cu ti zn
NH -N
NOU
x
x
x
x
x
x
x
Caco
Volatile
C.rl
Cr
Ni
Pb
. As
ft
Se
H
Eq. %
Solids °!o
Org-N
Mo
Ci
B
Ba
X. ...
x
O4
Ag
Sb
Co
Sit
Ti.
tt
Be
ALK.
SS
Avail P
Sal K
Cond
WIN ..
SOL 8
JL A
: O�G
SP,OR.
TSS
5' I�2tt-
SteveM
S1 1Ra
ASH
Ca0
CaCO3
M 3
M94
GIN
TOC
Env
OTAL.
TOTAL
'2C}S
K2O
TN
TKNW
idH41W-
NO.3W
ORGU-W
PA CERT
AZ CER'T
BTU.=
PCBS
REACT.
CN
FECAL_., .
TCLP
ICR
,
p R�
NORTH � /gyAROLINA
�"qw"� .sV�� .'�rir`•�"'.
f e-"' - >ar �Cwiu_:,i�e''N ' �+F�, jt'��? }:Y
'`-y m' � Y, n?M����Yy' Z, .'rJr�
-`Y+�'.. . A �'+'ra: v4[x-it�'•F �1'i t'iFn.�''. i� �- •'r.': ;'r.'
�'��rw
:WJ�Y�.�-C•^ .tip �^•
-
-
• 4�f
•a'i�.
PI�C€'PER'SAMPC E>=
-.��
,�srr
n
AD
m
m
w
Lo
Facility:
Source:
Location:
Type of Anualysis:
Report No.:
Date Sampled:
Date Reported:
Reporting Period:
Quarterly Sludge Summary
Campbell Soup Supply Company
DAF Sludge
Maxton, North Carolina
Quarterly Sludge - DAF
14-059-0205
2/27/2014
3/7/2014
1st Quarter - 2014
Parameter
%
PPM
Dry Weight
EPA
Monthly
Limits
Solids
4.34
43,400.00
Nitrogen (TKN)
0.67
6,680.00
Phosphorus
0.07
744.00
Potassium
0.11
1,080.00
Sulfur
--------
--------
Calcium
0.15
1,510.00 _
Magnesium
0.02
194.00
Sodium
0.08
814.00
Iron
--------
--------
Aluminum
--------
600.00
Manganese
--------
--------
Copper
--------
7.00
1,500.00
Zinc
--------
141.00
2,800.00
Ammonia Nitrogen
0.05
461.00
--------
Nitrate N/Nitrite N
--------
134.00
--------
Cadmium
--------
2.00
39.00
Chromium
--------
1,200.00
Nickel
--------
7.00
420.00
Lead
--------
5.00
300.00
Arsenic
--------
--------
41.00
Mercury
--------
--------
17.00
Selenium
--------
--------
100.00
pH3.7
--------
--------
Calcium Carbonate eq. (est)
--------
--------
Organic Nitrogen
0.62
6,219.00
--------
Molybdenum
--------
--------
75.00
Chloride
--------
--------
--------
Boron
--------
--------
--------
Available P2O5
--------
--------
--------
Specific Gravity
--------
1 8.34
1 --------
Page: 3 of 2
Report Number: 14-092-0202 ��. A&L. Easters Laboratories, Inc._
Account Number: 00327 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 2114M
Submitted By: GRADY DOBSON . WWUaleastem.com
Send To: EHC Inc. Project: DAF-2ND QTR SLUDGE
GRADY DOBSON NC CERT#257
PO Box 902
RED SPRINGS ; NC 28377
REPORT OF ANALYSIS Date Sampled:.4/1/2014 10:00:00
Lab Number: 98717 Date Received; 04/02/2014 00:00
Sample Id : DAF-2ND QTR SLUDGE Date Reported: 04/07/2014
Total Solids
0.93.
9300
100.0
JM
04/02/2014 14:39
SM-2540G
Moisture"
99.07
100.0
JM
04/02/201414:39
SM-2540G
Total Kjeldahl Nitrogen
2.47
24700
10.0 .
JM.
04/03/2014 08:24
SM .4500-NH3C-TKN
Total Phosphorus
0.11
1090
100
KM
04/04/2014 09:04
SW 601OC
Total Potassium
0.42
4220
100
KM
04/04/2014 09:04
SW 601 OC
Total Calcium
0.47
4690
100
KM
04%04/2014 09:04
SW 601 OC
Total Magnesium
0.05
469
100
KM
04/04/2014 09:04
SW 601 OC
Total Sodium
0:36
3620
100
KM
04/04/2014 09:04
SW 601.10C
Total Aluminum_
400
100
KM
04/04/2014 09:04
SW 601 OC
Total Copper
25
5
KM
04/04/2014 09:04
SW 601 OC,
Total Zinc
364
5
KM
04/04/2014 09:04
SW 601 OC
Ammonia Nitrogen
0.97
9680
10.0
JM
04/03/2014 08:24
SM-4500-NH3C
Organic N
1.50
15020
10.0
04/03/2014 08:24
CALCULATION
Nitrate+Nitrite-N
53.8.
2.00
JM .04/03/2014
08:25 .:
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
04/04/2014 09:04
SW 601 OC
Total Nickel
21
5
KM
04/04/2014,09:04 ,
: SW 601 OC
Total Lead
<5
5
KM
04/04/2014 09:04
SW 60:1 OC.
pH (Standard Units) *
4.40
2.00
JM
04/03/2014 08:24
SW-9045D
All values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced
in whole or part, nor may
any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 bf. 2
Report Number: 14-092-0202
Account Number: 00327
Submitted By: GRADY DOBSON
Send To: EHC Inc.
GRADY DOBSON
PO Box 902
RED.SPRINGS NC 28377
Lab Number :: 98717 .
Sample Id : DAF-2ND QTR SLUDGE
RESULT
PARAMETER
Comments:-
ORGANIC.NITROGEN NOT FOR COMPLIANCE PURPOSES.
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743,9401 Fax (ew) 271=6446
www.aleastern.com
Project : DAF-2ND QTR SLUDGE
NC CERT#257
.REPORT OF ANALYSIS Date Sampled:.4/1/2014 10:00:00
Date Received: 04/02/2014 00:00
Date Reported: 04/07/2014
RESULT QUANTITATION
DATEITIME
All values are cin.a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SAMPLE. TRANS-Ml . TTAL
A&L Eaftim
14,092-mO;
O�-Q2-201
DAF2JNb dm SLUDGE 12,41-09
- =_ . .
SkjhrAidpd By
T
--'GRADY DOBSON EMC,,,VNC
POR 902
Email
6GrRA
RED -SPRING.t KC. iO#
-grad bsoneheiftmail.Dorn
9 n I
ab Rurn . bdf,(Leab Usip, Only), "so male W�
c;0tamer —
Sbhnpj0q30Q* qhfml�,-
Date Reed:
PAP-- . $/a d-O
Glass (yWor No).
Samoled TVm&jj-,,6l6
Tints ReOd:
emtic fy ar Na)
Sam
Reed �Xw
Relkicpj Date,
Is nature
rlifid,
R6&ClV0d 13pl(Signature)-
me_ I
Ti__
A__A
roC
V
Place;� 'X ''by
sts- Intemal L4b Code:
Des Tests
Ads:
TKN
P
K
CA
- mg,
A]
Un
NH4-N
x
X
X
X
X
X
x
X
x
Cd
Cr
Ni
Pb
Pb
As
Fig
So-
PH
5a�e_
CaCO3
E
ofids 0/6
cl
Sa
x
SDI
—Ag,
Sb__
Co
Ti
V_
SS
_S61.K
Cand
WIN
iiOL 13,
'OL NA
O&G
SPiGR
TSS
Sievd#20:
SievoM
SlevdfHQD
ASH
CaO
06CO3
_:_mgcoa.
_ Moo.
am
TOG
Er t
FGTAL
p2G5
TOTAL
K2O'
TN
TK I NW
N H4W
NO3W
ORGM-VU
PAGER1
AZ'CERTI-1.
BTU
PCBS.
REACT
CN
FECAL
TGLP
ICR
iill M
- . . . . . . 4,4-
10,4611
ROW,
WON
MUM-
NORTH CAROLINA:
- 1''.. It— W
,f -
lmxaml:
i !� M,
Facility:
Source:
Location:
Type of Anualysis:
Report No.:
Date Sampled:
Date Reported:
Reporting Period:
Quarterly Sludge Summary
Campbell Soup Supply Company
DAF Sludge
Maxton, North Carolina
Quarterly Sludge - DAF
14-092-0202
4/1/2014
4/7/2014
2nd Quarter - 2014
Parameter
%
PPM
Dry Weight
EPA
Monthly
Limits
Solids
0.93
9,300.00
Nitrogen (TKN)
2.47
24,700.00
Phosphorus
0.11
1,090.00
Potassium
0.42
4,220.00
Sulfur
Calcium
0.47
4,690.00
Magnesium
0.05
469.00
Sodium
0.36
3,620.00
Iron
--------
--------
Aluminum
--------
400.00
Manganese
--------
--------
Copper
--------
25.00
1,500.00
Zinc
--------
364.0.
2,800.00
Ammonia Nitrogen
0.97
9,680.00
--------
Nitrate N/Nitrite N
--------
53.80
--------
Cadmium
--------
2.00
39.00
Chromium
--------
--------
1,200.00
Nickel
--------
21.00
420.00
Lead
--------
5.00
300.00
Arsenic
--------
--------
41.00
Mercury
--------
--------
17.00
Selenium
--------
--------
100.00
pH
4.4
--------
--------
Calcium Carbonate eq. (est)
--------
0.00
--------
Organic Nitrogen
1.5
15,020.00
--------
Molybdenum
--------
--------
75.00
Chloride
--------
--------
--------
Boron--------
--------
--------
Available P205
--------
--------
--------
Specific Gravity
--------
8.34
--------
- Page: 1 of 2 - - -
Report Number: 14-1,90-0216 A&L Eastern Laboratories, Inc.
Account Number: 00327 7621 Whitepina Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446
Submitted By: GRADY DOBSON www.aleastem.com
Send To: EHC Inc. Project: DAF 3RD QTR
PO Box 902 NC CERT#257
RED SPRINGS, NC 28377
Lab Number: 56375
Sample Id : DAF 3RD QTR
REPORT OF ANALYSIS Date Sampled: 7/7/2014 08:30:00
Date Received: 07/09/2014 00:00
Date Reported: 07/14/2014.
Total Solids *
1.39
13900
100.0
JM
07/09/2014 16:29
SM-2540G
Moisture *
98.61
100.0
JM
07/09/2014 15:29
SM-2540G
Total Kjeldahl Nitrogen
1.22
12200
10.0
JM
07/10/2014 08:50
SM-4500-NH3C-TKN
Total Phosphorus
0.20
1970
100
KM
07/10/2014 14:12
SW 6010C
Total Potassium
0.19
1850
100
KM
07/10/2014 14:12
SW 6010C .
Total Calcium
4.42
44200
100
KM
07/10/2014 14:12
SW 6010C
Total Magnesium
0.18
1760
100
KM
07/10/2014 14:12
SW 6010C
Total Sodium
0.43
4300
100
KM
07/10/2014 14:12
SW 6010C
Total Aluminum
2000
100
KM
07/10/2014 14:12
SW 6010C
Total Copper
50
5
KM
07/10/2014 14:12
SW 6010C
Total Zinc
236
5
KM
07/10/2014 14:12
SW 6010C
Ammonia Nitrogen
0.22
2160
10.0
JM
07/10/2014 08:50
SM-4500-NH3C
Organic N
1.00
10040
10.0
07/10/2014 08:50
CALCULATION
Nitrate+Nitrite-N
14.4
2.00
JM
07/10/2014 08:50
SM-450ONO3F
Total Cadmium
<2,0
2.0
KM
07/10/2014 14:12
SW 6010C
Total Nickel
45
5
KM
07/10/2014 14:12
SW 6010C
Total Lead
<5
5
KM
07/10/2014 14:12
SW 6010C
pH (Standard Units) *
5.07
2.00
RJN
07/10/2014 08:50
SW-9045D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our orior written authorization.
Debbie Holt
SAMPLE TRANSMITTAI
A&L Eas 'O91OU2014
,M EHC Inc_3:19:
DAF 3RD QTR
7621 Whi!mine Road Richn
Offcce Information
R'qAA# Submitted By 'Charge. To Copy To Project
GRADY DOBSON EHC INC
Awl -9
POB 902
Er ual�
RED SPRINGS WC 28377
ab Nri�ber (Lab Use, Only)
Sample ID
Qalas
iner Tan
-0,0UYe or Na)
Sam Jed Data:
e:
Sam ifn - pled time:
Date R
Time Recd.
Plastic (7 e—s. or -No).
Sampled By
Re1incjtAerk13y_-^gnature)
Date Time
Received gy: (Signature)
Date
Time
!2
Rease Place'a"X' by Desired Tes6i_
Intemal Lab Code:
Ads WI
TKN
p
K
Ca
Rflg
Ma
Fe
Mn
CanZn
N"4-N
NO3-N
x
x
x
x
x
x
x
x
x
x
x
x
cd
Cr
Pli
Pb
As
Hg—
Se
PH
CaCO&
Eq. %
Volatile
Sogids
olrg-w
too
IfyD
sa
x
x
x
x
x
904
tag
Sb
co
So
Ti
V
Be
ALK
SS
Aval I P
Sol K'
Cond
MIN
WIL ff
oL NA
'0&0
SP-GR.
TSS
8tavc#20
Sieve-960
Sieve#100
ASK
'CaO
cacO3
4_pO3
Mgo
rim
TOG
Env
i V
TOTAL
P205
TOTAL
uo
TN
TKNW
W1 4W
NO3W
.OFZGN-W
PACERT,A-7CF-RT,
BTU
PCBS
REACT
CN
FEGAL
TCLP
ICR
MORTH CAROLINA
A Z
PFUCE PER SAMPLE
-J
(.n
Lq
rn
F-
on
Facility:
Source:
Location:
Type of Anualysis:
Report No.:
Date Sampled:
Date Reported:
Reporting Period:
Quarterly Sludge Summary
Campbell Soup Supply Company
DAF Sludge
Maxton, North Carolina
Quarterly Sludge - DAF
14-19070216
7/7/2014
7/24/2014
3rd Quarter - 2014
Parameter
%
PPM
Dry Weight
EPA
Monthly
Limits
Solids
1.39
13,900.00
Nitrogen (TKN)
1.22
12,200.00
Phosphorus
0.2
1,970.00
Potassium
0.19
1,850.00
Sulfur
--------
--------
Calcium _
4.42
44,200.00
Magnesium
0.18
1,760.00
Sodium
0.43
4,300.00
Iron
--------
--------
Aluminum
--------
2,000.00
Manganese
--------
--------
Copper
--------
50.00
1,500.00
Zinc
--------
236.00
2,800.00
Ammonia Nitrogen
0.22
2,160.00
--------
Nitrate N/Nitrite N
--------
14.40
--------
Cadmium
--------
2.00
39.00
Chromium
--------
--------
1,200.00
Nickel
--------
45.00
420.00
Lead
--------
5.00
300.00
Arsenic
--------
--------
41.00
Mercury
--------
--------
17.00
Selenium
--------
--------
100.00
pH
5.07
--------
--------
Calcium Carbonate eq. (est)
--------
0.00
--------
Organic Nitrogen
1
10,040.00
--------
Molybdenum
--------
--------
75.00
Chloride
--------
--------
--------
Boron
--------
--------
--------
Available P2O5
--------
--------
--------
Specific Gravity
--------
8.34
--------
Page: 1 of 2
Report Number: 14-280-0207
Account Number: 00327
Submitted By: GRADY DOBSON
Send To: EHC Inc.
PO Box 902
RED SPRINGS, NC 28377
L A &L Eastern Laboratories, into.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-401 Fax (804) 271.6446
wwmaleastern.com
Project: CAMPBELL SOUP 4TH QTR SLUDGE
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 10/6/2014 09:30:00
Lab Number: 57974
Date Received: 10/07/2014 00:00
Sample Id : DAF/CAMPBELL SOUP
Date Reported: 10/17/2014
PARAMETER
RESULT
RESULT
'QUANTITATION LIMIT
ANALYSIS
(%..
ANALYST
�,
Total Solids *
4.76
47600
100.0
JM
10/07/2014 13:59 SM-2540G
Moisture *
95.24
100.0
JM
10/07/2014 13:59 SM-2540G
Total Kjeldahi Nitrogen
2.71
27100
10.0
JM
10/08/2014 08:44 SM-4500-NH3C-TKN
Total Phosphorus
0.14
1400
100
KM
10/16/2014 18:38 SW 6010C
Total Potassium
0.12
1160
100
KM
10/16/2014 18.38 SW 6010C
Total Calcium
0.90
9030
100
KM
10/16/2014 18:38 SW 6010C
Total Magnesium
0.06
614
100
KM
10/16/2014 18:38 _ SW 6010C
Total Sodium
0.13
1340
100
KM
10/16/2014 18:38 SW 6010C
Total Aluminum
1200
100
KM
'10/161201418:38 SW 6010C
Total Copper
23
5
KM
10/16/2014 18:38 SW 6010C
Total Zinc
284
5
KM
10/16/2014 18:38 SW 6010C
Ammonia Nitrogen
0.23
2310
10.0
JM
10/08/2014 08:44 SM-4500-NH3C
Organic N
2.48
24790
10.0
10/08/2014 08:44 CALCULATION
Nitrate+Nitrite-N
<100
2.00
JM
10/08/2014 08:45 SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
10/16/2014 18:38 SW 6010C
Total Nickel
28
5
KM
10116/201418:38 SW 6010C
Total Lead
<5
5
KM
10/16/2014 18:38 SW 6010C
pH (Standard Units) *
4.42
2.00
MW
10/08/2014 09:20 SW 9045D
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet
basis.
Debbie Holt
Facility:
Source:
Location:
Type of Anualysis:
Report No.:
Date Sampled:
Date Reported:
Reporting Period:
Quarterly Sludge Summary
Campbell Soup Supply Company
DAF Sludge
Maxton, North Carolina
Quarterly Sludge - DAF
14-280-0207
10/6/2014
10/17/2014
4th Quarter - 2014
Parameter
%
PPM
Dry Weight
EPA
Monthly
Limits
Solids
4.76
47,600.00
Nitrogen (TKN)
2.71
27,100.00
Phosphorus
0.14
1,400.00
Potassium
0.12
1,160.00
Sulfur
--------
--------
Calcium
0.9
9,030.00
Magnesium
0.06
614.00
Sodium
0.13
1,340.00
Iron
--------
--------
Aluminum
--------
1,200.00
Manganese
--------
--------
Copper
--------
23.00
1,500.00
Zinc
--------
284.00
2,800.00
Ammonia Nitrogen
0.23
2,310.00
--------
Nitrate N/Nitrite N
--------
2.00
--------
Cadmium
--------
2.00
39.00
Chromium
--------
--------
1,200.00
Nickel
--------
28.00
420.00
Lead
--------
5.00
300.00
Arsenic
--------
--------
41.00
Mercury
--------
--------
17.00
Selenium
--------
--------
100.00
pH
4.42
--------
--------
Calcium Carbonate eq. (est)
--------
0.00
--------
Organic Nitrogen
2.48
24,790.00
--------
Molybdenum
--------
--------
75.00
Chloride
--------
--------
--------
Boron
--------
--------
--------
Available P2O5
--------
--------
--------
Specific Gravity
--------
8.34
--------
Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
= K
SC
L•A•B S•C•1•E•N-C•E•S
Mr. Thomas Ammons
EHC, Inc.
PO Box 902
Red Springs, NC 28377
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
Report Summary
Thursday June 19, 2014
Report Number: L703709
Samples Received: 06/10/14
Client Project: 14-MI0602-3
Description: Campbell Soup DAF Sludge (Annual TCLP Sludge)
The analytical results, in this report are based upon information supplied
by you, the -client, and are for your exclusive use. If you -have any
questions regarding this data package, please -do not hesitate to call.
%% II11
Entire Report Reviewed By:
JimW Hunt , ESC Representative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND'- R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, '
MN 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3,'OK - 9915, PA - 68-02979, IA Lab #364, EPA - TN002
Accreditation is only applicable tb the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 13
ESC
L-A-8
REPORT OF ANALYSIS
Mr. Thomas Ammons
EHC, Inc.
PO Box 902
Red Springs, NC 28377
June 19,2014
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-600-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
Date Received June 10,
Description Campbell Soup
Sample ID DAF SLUDGE
Collected By Grady Dobson
Collection Date 06/09/14 11:00
Parameter
2014
DAF Sludge
Result
(Annual TCLP
Det. Limit
Sludge)
Units
ESC Sample
Site ID
Project
Limit Method
# L703709-01
MAXTON, NC
14-MI0602-3
Date/Time By
Dil
Corrosivity
Non-Corrosiv
9045D
06/13/14
1032 SDC
1
Ignitability
See Footnote
Deg. F
D93/101
06/14/14
1215 AS
1
pH
4.5
su
9045D
06/11/14
1125 KBC
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
06/12/14
1003 MCG
1
Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
06/12/14
0505 AS
1
TCLP Extraction
-
1311
06/13/14
0817 CCS
1
Mercury
BDL
0.010
mg/1
0.20 7470A
06/14/14
1707 CCE
1
Arsenic
BDL
0.45
mg/1
5.0 6010C
06/14/14
0126 WBD
1
Barium
BDL
1.4
mg/1
100 6010C
06/14/14
0126 WBD
1
Cadmium
BDL
0.45
mg/l
1.0 6010C
06/14/14
0126 WBD
1
Chromium
BDL
0.45
mg/l
5.0 6010C
06/14/14
0126 WBD
1
Lead
BDL
0.45
mg/l
5.0 6010C
06/14/14
0126 WBD
1
-Selenium
BDL
0.45
mg/l
1.0 6010C
06/14/14
0126 WBD
1
Silver
BDL
0.45
mg/1
5.0 6010C
06/14/14
0126 WBD
1
TCLP ZHE Extraction
-
1311
06/12/14
0832 CCS
1
TCLP Volatiles
Benzene
BDL
0.050
mg/l
0.50
8260B
06/12/14
2202
JC 1
Carbon tetrachloride
BDL
0.050
mg/l
0.50
8260B
06/12/14
2202
JC 1
Chlorobenzene
BDL
0.050
mg/l
100
8260B
06/12/14
2202
JC 1
Chloroform
BDL
0.25
mg/l
6.0
8260B
06/12/14
2202
JC 1
1,2-Dichloroethane
BDL
0.050
mg/l
0.50
8260B
06/12/14
2202
JC 1
1,1-Dichloroethene
BDL
0.050
mg/1
0.70
8260B
06/12/14
2202
JC 1
2-Butanone (MEK)
BDL
0.50
mg/1
200
826013
06/12/14
2202
JC 1
Tetrachloroethene
BDL
0.050
mg/1
0.70
8260B
06/12/14
2202
JC 1
Trichloroethene
BDL
0.050
mg/l
0.50
8260B
06/12/14
2202
JC 1
Vinyl chloride
BDL
0.050
mg/l
0.20
8260B
06/12/14
2202
JC 1
Surrogate Recovery
Toluene-d8
106.s
Rec.
114.
8260B
06/12/14
2202
JC 1
Dibromofluoromethane
99.8
a Rec.
125.
8260B
06/12/14
2202
JC 1
a,a,a-Trifluorotoluene
99.3
e Rec.
114.
8260B.
06/12/14
2202
JC 1
4-Bromofluorobenzene
102.
% Rec.
128.
8260B
06/12/14
2202
JC 1
TCLP Pesticides
Chlordane
BDL
0.0050
mg/l
0.030
8081A
06/18/14
1132
CBB 1
L703709-01 (IGNITABILITY) -
did not ignite at
170F
L703709-01 (PH) - 4.5@21.4c
Page 2 of
13
*ESC
I
C
C
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
)1-800-767-5859
Fax (615) 758-5859
Tax I.D.
62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Thomas Ammons
June 19,2014
EHC, Inc.
PO Box 902
Red Springs, NC 28377
-
ESC Sample
# : L703709-01
Date Received June 10,
2014
Description Campbell Soup
DAF Sludge
(Annual TCLP
Sludge)
Site ID
MAXTON,
NC.
Sample ID DAF SLUDGE
Project
14-MI0602-3
Collected By Grady Dobson
Collection Date 06/09/14 11:00
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time By
Dil
Endrin
BDL
0.0050
mg/l
0.020
8081A
06/18/14
1132 CBB
1
Heptachlor
BDL
0.0050
mg/1
0.0080
8081A
06/18/14
1132 CBB
1
Lindane
BDL
0.0050
mg/l
0.40
8081A
06/18/14
1132 CBB
1
Methoxychlor
BDL
0.0050
mg/l
10.
8081A
06/18/14
1132 CBB
1
Toxaphene
BDL
0.010
mg/l
0.50
8081A
06/18/14
1132 CBB
1
Surrogate Recovery
Decachlorobiphenyl
106.
°s Rec.
123.
8081A
06/18/14
1132 CBB
1
Tetrachloro-m-xylene
66.8
o Rec.
114.
8081A
06/16/14
1132 CBE
1
TCLP Herbicides
2,4,5-TP (Silvex)
BDL
0.0020
mg/1
1.0
8151A
06/16/14
1951 KLM
1
2,4-D
BDL
0.0020
mg/l
10.
8151A
06/16/14
1951 KLM
1
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
73.7
°s Rec.
8151A
06/16/14
1951 KLM
1
TCLP Semi-Volatiles
1,4-Dichlorobenzene
BDL
0.10
mg/l
7.5
8270D
06/17/14
1704 KMF
1
2,4-Dinitrotoluene
BDL
0.10
mg/1
0.13
8270D
06/17/14
1704 KMF
1
Hexachlorobenzene
BDL
0.10
mg/1
0.13
B270D
06/17/14
1704 KMF
1
Hexachloro-1,3-butadiene
BDL
0.10
mg/l
0.50
8270D
06/17/14
1704 KMF
1
Hexachloroethane
BDL
0.10
mg/1
3.0
8270D
06/17/14
1704 KMF
1
Nitrobenzene
BDL
0.10
mg/l
2.0
8270D
06/17/14
1704 KMF
1
Pyridine
BDL
0.10
mg/l
5.0
8270D
06/17/14
1704 KMF
1
3&4-Methyl Phenol
BDL
0.10
mg/1
400
8270D
06/17/14
1704 KMF
1
2-Methylphenol
BDL
0.10
mg/l
200
8270D
06/17/14
1704 KMF
1
Pentachlorophenol
BDL
0.10
mg/l
100
8270D
06/17/14
1704 KMF
1
2,4,5-Trichlorophenol
BDL
0.10
mg/l
400
8270D
06/17/14
1704 KMF
1
2,4,6-Trichlorophenol
BDL
0.10
mg/1
2.0
8270D
06/17/14
1704 KMF
1
Surrogate Recovery
2-Fluorophenol
45.2
°s Rec.
67.0
8270D
06/17/14
1704 KMF
1
Phenol-d5
32.3
"s Rec.
67.0
8270D _
06/17/14
1704 KMF
1
Nitrobenzene-d5
61.1s
Rec.
120.
8270D
06/17/14
1704 KMF
1
2-Fluorobiphenyl
61.4
o Rec.
122.
8270D
06/17/14
1704 KMF
1
2,4,6-Tribromophenol
68.7
°s Rec.
148.
8270D
06/17/14
1704 KMF
1
p-Terphenyl-dl4
51.6
°s Rec.
149.
8270D
06/17/14
1704 KMF
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 06/19/14 12:10 Printed: 06/19/14 13:55
L703709-01 (IGNITABILITY) - did not ignite at 170F
L703709-01 (PH) - 4.5@21.4c
Page 3 of 13
Attachment A
List of Analytes with QC Qualifiers
Sample Work Sample Run
Number Group Type Analyte ID Qualifier
L703709-01 WG726036 SAMP 2-Sutanone (MEK) R293999G J3
WG72GS82 SAMP Heptachlor R2943611 J3
Page 4 of 13
C
Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
J3 The associated batch QC was outside the established quality control range
for precision.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
"unless qualified as 'R' (Rejected)."
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
r'
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
Page 5 of 13
Summary of Remarks For Samples Printed
06/19/14 at 13:55:31
TSR Signing Reports: 350
R5 - Desired TAT
Report GW in ppb except Campbell Soup; 6010C
Sample: L703709-01 Account: ENVHYD Received: 06/10/14 09:00 Due Date: 06/17/14 00:00 RPT Date: 06/19/14 12:10
I
(
`
_
_
SC✓
L•A•B 5•C•I•E-N•C•E•S
• c •
EHC, Inc.
Mr. Thomas Ammons -
PO Box 902
Red Springs, NC 28377
-
Quality Assurance Report
Level II
L703709
-
12065 Lebanon Rd.
Mt. Juliet, TN 37122 '
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
June 19, 2014
Laboratory= B3'ank; ;•
Analyte
Result
Units s Rec
Limit
Batch Date Analyzed
Reactive Sulf;(SW846- 7.3.4.1)
<
25_
mg/kg-
.WG725665,06/12/-14
",05:05
Reactive CN (SW846 7.3.3.2)
<
.125
mg/kg
WG725666 06/12/14
09:58
1,1-Dichloroethene
<
.05
mg/1
WG726036 06/12/14
14:09
1,2-Dichloroethane
<
.05
mg/l
WG726036 06/12/14
14:09
2-Butarione '(MEK)
<
.5-
mg/1
WG726036; 06%12/14
-14:09
Benzene
<
.05
mg/1
WG726036 06/12/14
14:09
Carbon tetrachloride
<
.05
mg/1
WG726036 06/12/14
14:09
Chl6robenzene
<
.05_
mg/1
WG726036'06112`114
'14:09
Chloroform
<
.25
mg/1
WG726036 06/12/14
14,09
Tetrachlorcethene
<
.05
mg/1
WG726036 06/12/14
14:09
Triahloroethene'
<
.05
mg/l
WG726036"--06/12%,14
14:09
vinyl chloride
<
.05
mg/1
WG726036 06/12/14
14:09
4-Bromofluorobenzene
o Rec. 101.0
71-126
WG726036 06/12/14
14:09
DibroTdQfiuOromethane
%- Rec. 99.40
78.3'121
WG726036`-06/12/14-14:09
Toluene-d8
% Rec. 103.0
88.5-111
WG726036 06/12/14
14:09
a,a,a-Trifluorotoluene
o Rec. 100.0
85-114
WG726036 06/12/14
14:09
Arsenic
<
.45
mg/l
WG726279 06/14/14
01:12
Barium
<
1.35
mg/1
WG726279 06/14/14
01:12
^admium.
<
.45
mg/1
WG726279"06/14/14
01:12
ftromium
<
.45
mg/1
WG726279 06/14/14
01:12
gad
<
.45
mg/l
WG726279 06/14/14
01:12
Selenium
<
.45
mg/l
WG726279. 08/14/14
01:12
Silver
<
.45
mg/1
WG726279 06/14/14
01:12
Mercury
<
.01
mg/1
WG.726271 06/14/14,16:39
2,4,5-TP (Silvex)
<
.002
mg/1
WG726590 06/16/14
17:31
2,4-D_ -
<
.002
mg/l.
WG726590-06/16/14,17:31
2,4-Dichlorophenyl Acetic Acid
o Rec. 66.00
22.9-153
WG726590 06/16/14
17:31
1,4-Dichlorobenzene
<
.1
mg/1
WG726366 06/17414
02:18
2,4,5-Trichlorophenol
<
.1
mg/1
WG726366 06/17/14
02:18
2,4,6-Trichlorophenol
<
.1
mg/1
WG726366 06/17/14
02:18
2,_4-Dinitrotoluene _
<
.1
-- .mg/1_.., . .. ."*.- . _ ..
... ..
-.WG726366- 06/17/14-,02:18
2-Methylphenol
<
.1
mg/l
WG726366 06/17/14
02:18
3&4-Methyl Phenol
<".1
mg/l
WG726366 06/17/14
02:18
Hexachloro-1,3-butadiene
<
.1
mg/1
WG726366.06/17/.14
02:18
Hexachlorobenzene
c
.1
mg/l
WG726366 06/17/14
02:18
Hexachloroethane
<
.1
mg/1
WG726366 06/17/14
02:18
Nitrobenzene
<
.1
mg/1
-
WG726366 06/17/14
02:18
Pentachlorophenol
<
.1
mg/l
WG726366 06/17/14
02:18
Pyridine
<
.1
mg/l
WG726366 06/17/14
02:18
2,4,6-Tribromophenol
a Rec. 60.40
11.2-130
WG7263,66 06/17/14
02:18
2-Fluorobiphenyl
o Rec. 52.80
29.5-131
WG726366 06/17/14
02:18
2-Fluorophenol
o Rec. 42.30
10-77.9
WG726366 06/17/14
02:18
Nitrobenzene-d5
% Rec. 51.00
21.8-123
WG726366 06/17/14
02:18
Phenol-d5
°s Rec. 32.70
5-70.1
WG726366 06/17/14
02:18
p-Terphenyl-d14
o Rec. 56.50
29.3-137
WG726366 06/17/14
02:18
* Performance of this Analyte
is outside
of
established criteria.
For additional information,
please
see Attachment A 'List of Analytes with QC
Qualifiers.'
Page 6 of 13
12065 Lebanon Rd.
_ - Mt. Juliet, TN 37122
ESC
C (615) 758-5858
.1-800-767-5859
Fax (615) 758-5859
L-A-8 S•C•I•E•[d-C•E•S
Tax I.-D. 62-0814289
Est. 1970
EHC, Inc.
Mr. Thomas Ammons
PO Box 902 Quality Assurance Report
Level II
Red Springs, NC 28377 - June 19, 2014
L703709
Lab oratory=El-4 .1.
Analyte
Result
Units % Rec
Limit
Batch Date Analyzed
Chlordane .. ..
< '.005
mg/1, . �•
� -
W6726582 06/,18%1`4'10:55
Endrin
< .005
mg/1
WG726582 06/18/14 10:55
Lindane
< .005
mg/1
WG726582 06/18/14 10:55
Heptachlor
< .005 -
mg/1=
WG726582;1.06/281,14=10:55
Methoxychlor
< .005
mg/l
WG726582 06/18/14 10:55
Toxaphene
< .01
mg/1
WG726582 06/18/14 10:55
Decachlorobiphenyl
% Rec. _ 115d0..
10.-156
WG726582' 06/18'/.14r10:55
Tetrachloro-m-xylene
% Rec. 87.30
13.9-137
WG726582 06/18/14 10:55
Duplicate
Analyte
Units
Result Duplicate RPD
Limit
Ref Samp Batch
pH'-
stir
7.10 7.'10 0.0'
1
1,703420=4 7 WG725694
pH
su
7.20 7.20 0.278
1
L703730-07 WG725694
Reactive Sulf.(SW846 7.3.4.1)
mg/kg
0.0 0.0 '0.0
20
L703664-01 WG725665
Reactive CN (SW846 7.3.3.2)
mg/kg
0.0 0.0 0.0
20
L703664-01 WG725666
Corrosivity
0.0 0.0 0.0
10
L703374-01 WG726094
•.:rcury
mg/l
0.0 0.000234 2.00
20
L704070-02 WG726271
jnitability
Deg. F
0.00 0.00 0.00
10
L703664-01 WG726283
Ignitability
Deg. F
0.00 0.00 0.00
10
L704505-01 WG726283
Laboratory Control Sample
Analyte
Units
Known Val Result
% Rec
Limit Batch
pH
su
- 6.33 6.30
99.5
98.3-101.7 WG725694
Reactive Sulf.(SW846 7.3.4.1)
mg/kg
100 110.
110.
70-130 WG725665
Reactive CN (SW846 7.3.3.2)
mg/kg
.1 0.0933
93.3
50-150 WG725666
1,-1-Dichloroethene% -
--mg/1- -----
-.025 .0.0209- -
83..7
.67.8-129 WG726036
1,2-Dichloroethane
mg/1
.025 0.0207
82.9
68.8-124 WG726036
2-Butanone (MEK)
mg/1
.125 0.0961
76.9
55-149 WG726036
Benzene;. .. -
mg/l
...025. 0..0213
85.3.. ..
74.8-121 ,--WG726036
Carbon tetrachloride
mg/1
.025 0.0211
84.3
70.2-123 WG726036
Chlorobenzene
mg/l
.025 0.0214
85.5
78.1-119 WG726036
Chloroform
mg/l
:025 0.0207
83.0
76-121 WG726036
Tetrachloroethene
mg/l
.025 0.0212
84.7
72.6-126 WG726036
Trichloroethene
mg/l
.025 0.0211
84.5
77.7-118 WG726036
Vinyl chloride
mg/l
.025 0.0226
90.2
65.9-128 WG726036
4-13romofluorobenzene
102.0
71-126 WG726036
Dibromofluoromethane
102.0
78.3-121 WG726036
Toluene-dS
104.o
88.5-111 W6726036
a,a,a-Trifluorotoluene
101.0
85-114 WG726036
* Performance of this Analyte
is outside of
established criteria.
For additional information,
please see Attachment A 'List of Analytes with
QC Qualifiers.'
Page 7 of 13
I
*-,-ESC
L•A•B S•C•f•E•N•C-E•S
EHC, Inc.
Mr. Thomas Ammons
PO Box 902
Red Springs, NC 28377
Corrosipi'ty.':
Arsenic
Baiium.;:
Cadmium
Chromium
Selenium
Silver
Mercury
Ignitability
2,4,5-TP (Silvex)
2',4-D`
2,4-Dichlorophenyl Acetic Aci
1,4-Di'chlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2-4-Dinitrotolu_ene
Methylphenol
4-Methyl Phenol
n.xachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,,6--Tribromophenol
2-Fluorobiphenyl
2-Fluorophenol
Nitrobenzene-d5
Phenol-d5
p-Terphenyl-d14
Endrin
Lindane
Heptachlor
Methoxychlor
Decachlorobiphenyl
Quality Assurance Report
Level II
L703709
d
taboratory,5eoiitrol' Sample
Units
Known Val
Result
- -
6.33 .�
- :. .6 3,0-
mg/l
9
9.53
mg/l
9
9.54
mg/1
9
9.56
.. .. mg/I
9"
- - 9. 68. .
mg/l
9
9.44
mg/1
9
9.20
mg/1
.03
0.0283
' -Deg.- F
" 82 - -
84': 0
mg/l
.005
0.00397
-mg/l
.005
0:00382
mg/1
.025
0-.0106-
mg/1
.025
0.0171
mg/1
.025
0.0149
mg/l
.625
0.0168
mg/1
.025
0.0131
mg/l
.025
0.0155
mg/1
.025
0.0127
mg/l
.025
0.0157
mg/l
.025
0.0118
mg/l
.025
0.0174
mg/l
.025
0.0120
mg/1
.025
0.0104
mg/1
.0002
0.000149
mg/l
.0002
0.000140
mg/1
.0002
0.0000701
mg/1
.0002
0.000175
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
June 19, 2014
Rec
Limit
Batch
.98:3-1'01.-7
.. WG726094
106.
80-120
WG726279
.106'. .•-
80-.120c
icWG726279
106.
80-120
WG726279
106.
80-120
WG726279
108".
_ 60-120,�
'- WG726279
105.
80-120
W6726279
102.
BO-120
WG726279
94.0
85-115
WG726271
" 102:
93-107-
'WG726283
79.4
57.6-129
WG726590
76.5
43.9-115
WG726590
68.50
22.9-153
WG726590
42-.6
21-89.4
WG726366
68.6
34.9-112
WG726366
59.4
29.8-107
WG726366
6.7..2
31.2-iO5
WG726366
52.4
26.4-86.9
WG726366
61.9
27.9-92
WG726366
50.9
16.1-104
WG726366
62.9
38.5-116
WG726366
47.4
16.5-89.8
WG726366
69:5
31.4-106
WG726366
47.9
10-97.4
WG726366
41.8
13.5-58.9
WG726366
60.20
11.2-130
WG726366
58.40
29.5-131
WG726366
47.10
10-77.9
WG726366
'72.80
21.8-123
WG726366
33.00
5-70.1
WG726366
54.00
29.3-137
WG726366
74.7
50.1-131
WG726582
69.9
54.7-125
WG726582
35.1
20.7-127
WG726582
87.6
48.2-144
WG726582
100.0
10-156
WG726582
72.20
13-9-137
WG726582
Laboratory Control Sample Duplicate
Analyte
Units
Result Ref %Rec
Limit RPD Limit Batch
PH
su
6.30 6.30 100.
98.3-101.7 0.0 20 WG725694
Reactive Sulf.(SW846 7.3.4.1)
mg/kg
120. 110. 120.
70-130 8.70 20 WG725665
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment A 'List of Analytes
with QC Qualifiers.'
Page 8 of 13
'JOESC
L-A-B S•C•I•E•N-C E•S
EHC, Inc.
Mr. Thomas Ammons
PO Box 902
Red Springs, NC 28377
Analyte
Reactive';,.CN� ;(SW8,46..-.71'3-.3,.2)
1,1-Dichloroethene
,=Dichl`oroethane'-'
2-Butanone (MEK)
Benzene
Carbop,tetirachloride-
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
4-Broin6fluorobenzene`
Dibromofluoromethane
Toluene-d8
a,a,a-Trifluorotoluene
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
Quality Assurance Report
Level II
L703709
June 19, 2014
`.,�Laborat"ory` Control* Sample``Duplicate,
Units Result Ref %Rec
Limit
RPD
Limit
Batch
;mg/kg,
0.._0935`
„, A,0933•-
�94',0 _
'50-150_.
, 0_:214s..
,_ '.20'Y: ..
.WG725666
mg/l
0.0254
0.0209
102.
67.8-129
19.3
20
WG726036
• mg, /1'..0':,0252.":
:0.02,07---
�101--. .• -
�-68..8-124_-.19-4.;:-
�`20, =.
,.WG726036
mg/l
0.118
0.0961
94.0
55-149
20.1*
20
WG726036
mg/1
0.0256
0.0213
102.
74.8-121
1B.2
20
WG726036
mg/1`
.6.02$Z-
'0:021't,.
.101.
70�:2-123.-
17':.7
20�-
WG726036
mg/1
0.0243
0.0214
97.0
78.1-119
12.8
20
WG726036
mg/l
0.0250
0.0207
100.
76-121
18.5
20
WG726036
i6/l
6'.0238
0. 0212•
95'.0
72.6"126
ll.5
'20
-WG726036
mg/l
0.0253
0.0211
101.
77.7-118
18.0
20
WG726036
mg/l
0.0272
0.0226
109.
65.9-128
18.7
20
WG726036
_
� � -
`98r30
''71-126"
WG726036
102.0
78.3-121
WG726036
104.0
88.5-111
WG726036
-
-
99:7065-114
WG726036
Corrosivity
6.30
6.30
100.
98.3-101.7
0.0
10
WG726094
Arsenic
mg/l
9.62
9.53
107.
80-120
1.00
20
WG726279
Barium
mg/l
9.61
9.50
107.
80-120
1.00
20
WG726279
-Amium
mg/l
9.65
9-54
107.
80-120
1.00
20
'WG726279
iromium
mg/1
9.67
9.56
107.
80-120
1.00
20
WG726279
:ad
mg/l
9.78
9.68
109.
80-120
1.00
20
WG726279
Selenium -
m4/1
9.53
9.44
106:
80-120
1.00
20
WG726279
Silver
mg/1
9.31
9.20
103.
80-120
1.00
20
WG726279
Ignitability
Deg.-F
84.0
84=0
102:
93-107
0.00
20
•WG72G283
2,4,5-TP (Silvex)
mg/l
0.00334
0.00397
67.0
57.6-129
17.3
20.7
WG72GS90
2;. 4-D, .
mg/l.
0.00483
0.00382
97:0
43.9-115
23.3
28
WG726590
2,4-Dichlorophenyl Acetic Acid
66.40
22.9-153
WG726590
1,4-Dichlorobenzene
mg/l
-0.0114
0.0106
45'.0
21-89.4
6.51
32.6
WG726366
2,4,5-Trichlorophenol
mg/l
0.0172
0.0171
69.0
34.9-112
0.110
23.9
WG726366
2,4,6-Trichlorophenol
mg/l
0.0157
0.0149
63.0
29.8-107
5.25
24.1
WG726366
2-,4-Dinitrotoluene.. .- ... ..
.. mg/1...
.0169_ _
0.0168-
_ 67_0." ._"
31-2-105
0..300
22
WG726366
2-Methylphenol
�mg/l
0.0133
0.0131
53.0
26.4-86.9
1.07
26.5
WG726366
3&4-Methyl Phenol
mg/l
0.0157
0.0155
63.0
27.9-92
1.64
27
WG726366
Hexachloro-1,3-butadiene
mg/l
0.0125
0:0127
50.0
16.1-104
1.67
31.2
WG726366
Hexachlorobenzene
mg/1
0.0170
0.0157
68.0
38.5-116
7.60
20.1
WG726366
Hexachloroethane
mg/l
0.0128
0.0118
51.0
16.5-89.8
7.B6
30.7
WG726366
Nitrobenzene'
mg/1
_ 0.0164
0.0174-
66.0
31.4=106
5.80,
25.7
WG726366
' Pentachlorophenol
mg/l
0.0128
0.0120
51.0
10-97.4
6.25
35.1
WG726366
Pyridine
mg/l
0.0105
0.0104
42.0
13.5-58.9
0.990
32.5
WG726366
2,4;6-Tribromophenol
63.90
11.2-130
WG726366
2-Flucrobiphenyl
-
54.60
29.5-131
WG726366
2-Fluorophenol
41.50
10-77.9
WG726366
Nitrobenzene-d5
69.40
21.8-123
-
WG726366
Phenol-d5
33.50
5-70.1
WG726366
p-Terphenyl-dl4
52.70
29.3-137
WG726366
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment
A 'List
of Analytes
with QC Qualifiers.'
Page 9 of 13
12065 Lebanon Rd.
Mt. Juliet,TN 37122
(615) 758-5858
1-800-767-5859OESC
Fax (615) 758-5859
L•A•B S. C•I•E•N•C•E•S
-
Tax I.D. 62-0814289
• e •
Est. 1970
EHC, Inc.
Mr. Thomas Ammons
PO Box 902
Quality Assurance Report '
Level II
Red Springs, NC 28377
June 19, 2014
L703709
:'LaliO`ratory{Pont=ol.
Sample";Dup, licate
Analyte
Units
Result
Ref
%Rec
Limit RPD
Limit
Batch
Eiidrin4.. .
_ mg/1 .
0:.001'84
."i. 0.,000149
92:0.,,
_
50:1-131- ,- �.2i:0 �
;29:1
_W
. G726582
Lindane
mg/1
0.000166
0.000140
83.0
54.7-125 17.1
21.1
WG726582
Heptachlor
mg/l
0.000117
0.0000701
59.0
20.7-127 50.4*
30.5
WG726582
Me"-hoxycHlor=
mg/1
-0-:'00,0212,
-j,O:.000175
''106.' - :
48:2-.144., ; 18':9•
27.8:.
;WG726582
Decachlorobiphenyl
_111.0
10-156
WG726582
Tetrachloro-m-xylene
73.80
13.9-137
WG726582
Matrix.Spike
Analyte
Units
MS Res
Ref Res
TV
o Rec
Limit
Ref Samp
Batch
1,77Dichl6roethene
mg/1
1.16
0:0-'
•1.25'
92.0
51.1-140
L702695-01
WG726036
1,2-Dichloroethane
mg/1
1.28
0.0
1.25
100.
60-126
L702695-01
WG726036
2-13utanone (MEK)
mg/l
6.51
0.0599
6.25
100.
22.4-138
L702695-01
WG726036
Benzene'".."
- 64/1
1.26,
0:00271
1.25
100.
"54:,3=-133
L762695-01
WG726036
Carbon tetrachloride
mg/1
1.27
0.0
1.25
100.
55.7-134
L702695-01
WG726036
Chlorobenzene
mg/1
1.36
0.0
1.25
110.
67-125
L702695-01
WG726036
Chloroform,
mg/1
1.30
0.0
1.25
100'.
63=129
L702695=01
WG726036
Tetrachloroethene
mg/1
1.23
0.0
1.25
98.0
53-139
L702695-01
WG726036
Trichloroethene
mg/1
1.25
0.0
1.25
100.
44.1-149
L702695-01
WG726036
Vinyl chloride
mg/1
1.13
0.0
1.25
90.01
47.8-137
L702695-01
WG726036
4-Bromofluorobenzene
103.0
71-126
WG726036
^ibromofluoromethane
102.0
78.3-121
WG726036
��--
oluene-d8
104.0
88.5-111
WG726036
,a,a-Trifluorotoluene
101.0
85-114
WG726036
Arsenic
mg/1
9.88
70.0344
9
110.
75-125
L703709-01
WG726279
Barium
mg/1
9.77
0.108
9
110.
75-125
L703709-01
WG726279
Cadmium
mg/1
9.89,
0.00598
9
110.
75-125
L703709-01
WG726279
Chromium
mg/1
9.84
0.:0488-
9
110.
-75-125
L703-709-01
W6726279
Lead
mg/1
9.83
0.0196
9
110.
75-125
L703709-01
WG726279
Selenium
mg/1
10.0
0.0599
9
110.
75-125
L703709-01
WG726279
Silver
mg/1
9.44
0:00566
9
100.
75-125
L703709-01
WG726279
Mercury
mg/1
0.0306
0.000234
.03
100.
80-120
L704070-02
WG726271
Mercury
mg/1'
0.0302
0.000261
.03
100.
80-120
L704028-01
WG726271
2,4,5-TP (Silvex)
mg/l
0.0329
0.0
.05
66.0
57.6-129
L703709-01
WG726590
2,4-D
mg/l
0:0391
0.0
.05 -
78. 0,
43.9-115
L703709-01
WG726590
2,4-Dichlorophenyl Acetic Acid
72.50
22.9-153
WG726590
Endrin
mg/1
0.00195
-0.0
.002" -
97..0
50.1-131
L703709-01
WG726582
Lindane
mg/1
0.00164
0.0
.002
82.0
54.7-125
L703709-01
WG726582
Heptachlor
mg/1
0.00131
0.0
.002
65.0
20.7-127
L703709-01
WG726582
Methoxychlor-"
mg/1
0.00215
0.0
.002-
110.
48.2-144
L703709-01
WG726582
Decachlorobiphenyl
123.0
10-156
WG726582
Tetrachloro-m-xylene
76.60
13.9-137
WG726582
1,4-Dichlorobenzene
mg/l
0.123
0.0
.25
49.0
14-104
L703833-02
WG726366
2,4,5-Trichlorophenol
mg/l
0.173
0.0
.25
70.0
30.6-120
L703833-02
WG726366
2,4,6-Trichlorophenol
mg/l
0.152
0.0.
.25
61.6
19.1-114
L703833-02
WG726366
2,4-Dinitrotoluene
mg/1
0.174
0.0
.25
70.0
16.2-135
L703833-02
WG726366_
2-Methylphenol
mg/1
0.133
0.0
.25
53.0
10-133
L703833-02
WG726366
3&4-Methyl Phenol
mg/l
0.142
0.0
.25
57.0
17.4-100
L703833-02
WG726366
Hexachloro-1,3-butadiene
mg/1
0.138
0.0
.25
55.0
15.7-109
L703833-02
WG726366
* Performance of this Analyte
is outside
of established criteria.
For additional information,
please see
Attachment
A 'List of Analytes
with QC
Qualifiers.' .
Page 10 of 13
12065 Lebanon
Rd.
*-ESC'
-
Mt.
(615)
Juliet, TN
758-5858
37122
1-800-767-5859
Fax (615) 758-5859
L•fr9 S•C•I•E•N•C•E'S
Tax I.D. 62-0814289
_ • •
Est.
1970
EHC, Inc.
_
Mr. Thomas Ammons
PO Box 902
Quality Assurance Report
Level II
Red Springs, NC 28377
June
19, 2014
L703709
;Matrz,,$pke:;
Analyte
Units
MS Res
Ref Res TV
% Rec
Limit
Ref Samp
Batch
Hezachlorobenzene::' ,. '.:-
-, mg/1�•-_O
i177_
0::0;
-;'.25:„�,":Zl>0..,.;':
.;31.•9-135:,
L703833.-.02'
.WG726366
Hexachloroethane
mg/1
0.149
0.0
.25
60.0
10.4-105
L703833-02
WG726366
Nitrobenzene
mg/l
0.176
0.0
.25
70.0
23.1-121
L703833-02
WG726366
Pentachlo`r'opheiiol-
mg/1
bi153;,;''''
? 0't'0
25n'Y!,`-
61-V -
1-0; 108
L703833-02
WG126366
Pyridine
mg/l
0.0966
0.0
.25
39.0
10-77.8
L703833-02
WG726366
2,4,6-Tribromophenol
68.00
11.2-130
WG726366
2-FluorobiphenyL -
-,..60:50
29'.5-131, _
. - .
:WG726366
2-Fluorophenol
41.40
10-77.9
WG726366
Nitrobenzene-d5
72.70
21.8-123
WG726366
Phenol-d5
29. 50-
5-70.1
WG726366
p-Terphenyl-d14
51. 90
29.3-137
WG726366
Matrix Spike
Duplicate
Analyte -
Units
MSD
Ref
%Rec
Limit
RPD
Limit
Ref Samp
Batch
1,1-Dichlofoethene
mg/1
1.06
1.16
84:8
51.1-140-
8.67
20.2
L70269.5-61
WG726036
1,2-Dichloroethane
mg/1
1.20
1.28
96.1
60-126
6.38
20
L702695-01
WG726036
2-Butanone (MEK)
mg/l
6.23
6.51
98.6
22.4-138
4.50
27
L702695-01
WG726036
Benzene
mg/l
1.16
1.26
92.2
541.3-133
8.26
20
L702695-'01
WG726036
Carbon tetrachloride
mg/1
1.17
1.27
93.4
55.7-134
8.51
20
L702695-01
WG726036
Chlorobenzene
mg/l
1.24
1.36
98.9
67-125
9.23
20.3
L702695-01
WG726036
i
-'ilorof orm
mg/1
1.22
1.30
98.0
63'-.129
6.2.7
20
L702695-01
WG.72603G
{`
:trachloroethene
mg/l
1.11
1.23
89.0
53-139
9.76
20
L702695-01
WG726036
:ichloroethene
mg/1
1.14
1.25
91.3
44.1-149
9.37
20
L702695-01
WG726036
vinyl chloride
mg/l
1.04
1.13
83.0
47'..8-137
8.39
20
L702695-01
WG726036
4-Bromofluorobenzene
103.0
71-126
WG726036
Dibromofluoromethane
103.0
78.3-121
WG726036
Toluene=d8_ _
_
103.0
88:_5-111
WG726036
a,a,a-Trifluorotoluene
99.30
85-114
WG726036
Arsenic
mg/-1
9.68.-
9.88
108.
75„125
2-00
20
L703709-01
WG726279
Barium
mg/1
9.69
9.77
106.
75-125
1.00
20
L703709-01
WG726279
Cadmium
mg/l
9.72
9.89
108.
75-125
2.00
20
L703709-01
WG726279
Chromium
mg/1
9.73
9.84
108.
75-125
1.00
20
L703.709-01
WG726279
Lead
mg/l
9.72
9.83 _
10B.
75-125
1.00
20
L703709-01
WG726279
Selenium
mg/l
9.72
10.0
107.
75-125
3.00
20
L703709-01
WG726279
Silver.. _. _ _.
.. mg/l
.9.39 ..
.9.44,.,
.104.
.357125".
1.00
20
L703709-01
WG726279
Mercury
mg/1
0.0306
0.0306
101.
80-120
0.0
20
L704070-02
WG726271
Mercury
mg/1
0.0304
0.0302
100. -
80-120
1.00
20
L704028-01
WG726271
2,4,5-TP (Silvex)
m9/1
0.0326
0.0329
65.2
57.6-129
0.910
20.7
L703709-01
WG726590
2,4=D
mg/1
0:0392
0.'0391
78.4
43.9-115
0.330
28
L703709-01
WG726590
2,4-Dichlorophenyl Acetic Acid
71.10
22.9-153
WG726590
Endrin
mg/l
0.00178
0.00195'
89.2:
50'.1-131
8.82
29.1
L703109-01
WG726582
Lindane
mg/l
0.00165
0.00164
82.6
54.7-125
0.980
21.1
L703709-01
WG726582
Heptachlor
- mg/1
0.00137
0.00131
68.3
20.7-127
4.40
30.5
L703709-01
WG726582
Methoxychlor
mg/1
0.00233
0:00215
li6.
48:2-144
8:01 -27.8
L703709-01
WG726582
Decachlorobiphenyl
100.0
10-156
WG726582
Tetrachloro-m-xylene
81.60
13.9-137
WG726582
1,4-Dichlorobenzene
mg/1
0.135
0.123
53.9
14-104
8.91
36.4
L703833-02
WG726366
2,4,5-Trichlorophenol
mg/1
0.185
0.175
74.1
30.6-120,
5.80
33.8
L703833-02
WG726366
* Performance of this Analyte
is outside
of established
criteria.
For additional information,
please see
Attachment
A 'List
of Analytes
with QC Qualifiers.'
Page 11 of 13
EHC, Inc.
Mr. Thomas Ammons
PO Box 902
Red Springs, NC 28377
Quality"Assurance Report
Level II
L703709
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859 -
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970.
June 19, 2014
,Matrix,Spike _ Duplicat`e. '
analvha Units MSD Ref 'Rec Limit _ RPD Limit Ref Samp Batch
2,.4, 6,_Trichlorophenol . ..
m g/1
0.171
0{152
-'68.2._`.. •
19..T-114"
-,'li703833-02'..•WGZ26366
2,4-Dinitrotoluene
mg/l
0.185
0.174
73.8
16.2-135
5.98
20.6
L703833-02
WG726366
2-Methylphenol
mg/l
0.137
0.133
54.7
10-133
2:47
40
L703833-02
WG726366
3&4=Methyl,-,Phenol-` '-
mg/1;
0..143
O'.142;'^_
{57'4.^ •: ..
17,=i00
:;4
A,,6 -40s ':
2Z.7 r
L703833-02
..',WG726366
Hexachloro-1,3-butadiene
mg/l
0.145
0.138
58.0
15.7-109
4.83
37.6
L703833-02
WG726366
Hexachlorobenzene
mg/l
0.190
0.177
76.0
31.9-135
7.03
20
L703833-02
WG726366
Hexachlor6ethane
mg/1'
0.-i52,:
0:149'-...�:60:'8''
10:4=105
Li78
4d
li703833'=02
•",WG726366
Nitrobenzene
mg/1
0.178
0.176
71.3
23.1-121
1.45
29
L703833-02
WG726366
Pentachlorophenol
mg/1
0.152
0.153
60.8
10-108
0-540
40
L703833-02
WG726366
Pyridine,``'
mg/1
d'.i06
0°0966
_41.5'
10-77.8
9.59-,:':38.8
L703833-02
WG7.26366
2,4,6-Tribromophenol
70.30
11.2-130
WG726366
2-Fluorobiphenyl
65.60
29.5-131
WG726366
2-Fluorophenol-
- 36 40 '
10'77'.9
'•',WGI,26366
Nitrobenzene-d5
77.00
21.8-123
WG726366
Phenol-d5
25.10
5-70.1
WG726366
`WG726366
p-Tefpheriyl-d14
-59:80
29.3=137
Post.
Spike .
Serial Dilution
Batch number /Run number / Sample number cross reference
WG725694: R2938690: L703709-01
WG725665: R2939454: L703709-01
WG725666: R2939553: L703709-01
WG725842: R2939690: L703709-01
WG726036: R2939996: L703709-01
WG726052: R2940465: L703709-01
WG726094: R2940669: L703709-01
WG726279: R2941106: L703709-01
WG726271: R2941405: L703709-01
WG726283: R2941687: L703709-01
WG726590: R2942385: L703709-01
WG726366: R2942889: L703709-01
WG726582: R2943611: L703709-01
* * Calculations are performed prior to rounding of reported values.
* Performance of this Analyte is outside of established criteria.
For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.'
Page 12 of 13
F
�_,,,OESC
L-A-B S-C-I•E•N•C•E-B
EHC, Inc.
Mr. Thomas Ammons
PO Box 902
Red Springs, NC 28377
Quality Assurance Report
Level II
L703709
The data package includes a summary of the analytic results of the quality
control samples required by the SW-846 or CWA methods. The quality control
samples include a method blank, a laboratory control sample, and the matrix
spike/matrix spike duplicate analysis. If a target parameter is outside
the method limits, every sample that is effected is flagged .with the
appropriate qualifier in Appendix B of the analytic report.
Method Blank - an aliquot of reagent water carried through the
entire analytic process. The method blank results indicate if
any possible contamination exposure during the sample handling,
digestion or extraction process, and analysis. Concentrations of
target analytes above the reporting limit in the method blank are
qualified with the "B" qualifier.
Laboratory Control Sample - is a sample of known concentration
that is carried through the digestion/extraction and analysis
process. The percent recovery, expressed as a percentage of the
theoretical concentration, has statistical control limits
indicating that the analytic process is "in control". If a
target analyte is outside the control limits for the laboratory
control sample or any other control sample, the parameter is
flagged with a "J4" qualifier for all effected samples.
Matrix Spike and Matrix Spike Duplicate - is two aliquots of an
environmental sample that is spiked with known concentrations of
target analytes. The percent recovery of the target analytes
also has statistical control limits. If any recoveries that are
outside the method control limits, the sample that was selected
for matrix spike/matrix spike duplicate analysis is flagged with
either a "J5" or a "J6". The relative percent difference (%RPD)
between the matrix spike and the matrix spike duplicate
recoveries is all calculated. If the RPD is above the method
limit, the effected samples are flagged with a "J3" qualifier.
i - Page 13 of 13
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-600-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
June 19, 2014
Company I Address: E�lll!ri6 Informationro five 10 of Otis"
EEC, Inc.
"
Mr. Thomas Ammon
s El
L
PO Bpi 902
,P2
<S Red Springs PQ Box,?
ings,NC 28377
-orihas.NC 28377 Red S
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Phone: 14�
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Collected bY(,s
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Sample ID
(LaP MUST Be Noti.fied)
Some Day... , .. 200%
Next Day ........ 100%
Two Day. , , . , ...50%
Three Day ....... 25%
Date Results Neede
Email? No Yes
FAX? _No�__Yes
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a
Pathogen and Vector Attraction Reduction Form
PATHOGEN REDUCTION AND VECTOR ATTRACTION DEDUCTION
The current permit, WQ0004893 does not have vector or pathogen requirements. This is a non-
biological wastewater treatment plant and will not require vector attraction reduction. Pathogen
certification will be included as soon as it is required by the permit.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Campbell Soup Supply Company Permit Number: WQ0004893
WWTP Name: Campbell Soup Supply Company NPDES Number: WQ0003626
Monitoring Period: .'From . 1/1/2014. To 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and. alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4❑
Alternative 5 0
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ra ❑
Y
Gamma Ra Y ❑
Pasteurization ❑
Class B:
Alternative 1❑
Alternative-2 ❑
Alternative 3 ❑
If applicable to alternative performed (Class'B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting El7
Aerobic Digestion ❑
e ® .
Anaerobic Dt soon
g
If applicable to alternative performed (Class A.or Class B) complete the following monitoring data:
Parameter*'
Allowable Level
in Sludge
Pathogen Density
Number of
Exccc=
deuces
Frequency
of
Anal 'sis
Sample
Typie
Analytical
Tech -
niame
.m
Geo. Mean
Maximuty
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
Current permit WQ000489.3 does not have Vector or Pathogen requirements.
1000 mpn per,
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ I Option 2 ❑ Option 3 ® joption 4 ❑ Option 5., ❑
Option 6 _ ❑ Option 7 ❑ Option 8 ❑ I Option 9 ❑ loption 10 ❑
No vector attraction re duction options ❑ s were performed p P
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR_ 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify; under penalty of law, that the pathogen requirements in 40 CFR 503.32'and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction ,and supervision in accordance with the
system designed to ensure that qualified personnel properly gather, and evaluate the information
used to. determine that the. pathogen. and vector attraction reduction requirements have been met.. I.
am aware; that there are significant penalties for false certification including fine and imprisonment."'
Al 64
riarer Name and Title (type or print)
/,4ignature of Preparer Date
a
Land Applier Name and Title. (if applicable)(tyl% or print)
ignature of Land Applier (if applicable) Date
4 � 4
DENR FORM RF (5/2003)
Pathogen and Vector Attraction Reduction Documentation
PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The current permit, WQ0004893 does not have vector or pathogen requirements. This is a non -
biological wastewater treatment plant and will not require vector attraction reduction. Pathogen
certification will be included as soon as it is required by the permit.
Soil Analysis Report
Page 1 of 5
Report Numbil"� '.:If-302-0766
Account Num�_.. _ J0327
0
Send To: EHC Inc. wwwaleastem.com
PO Box 902
RED SPRINGS NC 28377
Date Received: 10/29/2014 Date Of Analysis: 10/30/2014
A&L( 7-astern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446
Grower:
SLUDGE SITES
SOIL ANALYSIS REPORT
Date Of Report: 10/30/2014
Analytical Method(s):
Mehlich 3
Farm ID:
Organic
Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm
Rate
pH
Index
meq/100g
meq/100g
SITE 1
05639
3.6 M 113'
169 VH
131 VH
75
M
323
L
21
VL
4.8
6.70
2.3
5.0
NC=141
NC=67
SITE 2
05640
1.6 L 73
64 H
90 M
169
H
808
M
13
VL
6.4
0.6
6.3
NC=53
NC=46
SITE 3
05641
3.2 M 109
65 H
50 L
37
L
255
L
13
VL
4.7
6.75
1.8
3.5
NC=54
NC=26
SITE 4
05642
1.3 L 73
61 H
22 VL
33
M
216
L
14
L
5.2
6.85
0.8
2.2
NC=51
NC=11
SITE 5
05643
6.2 H 150
187 VH
129 H
216
H
823
M
18
VL
5.8
6.78
1.5
7.8
NC=156
NC=66
Percent
Base
Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble
Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
AI
Field ID
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm
Rate
ms/cm Rate
ppm Rate
ppm
SITE 1
20 M
11.3 VH
13 M
174
VH
1.3 M
0.3
VL
0.2
VL
6.7
12.5
32.3
1.8
46.5
NC=42
NC=282.5
NC=81
NC=65.0
SITE 2
12 L
3.4 M
33 H
106
VH
1.4 M
0.3
VL
0.1
VL
3.7
22.4
64.1
0.9
8.9
NC=25
NC=85.0
NC=206
NC=70.0
SITE 3
L
2.2 L
8 L
64
VH
1.1 M
VL
0.11
VL
3.7
8.8
36.4
1.6
50.5
�13
10.1
NC=27
NC5.0
NC=50
NC=55.0
SITE 4
L
2.6 M
14 M
91
VH
0.9 M
0.1
VL
0.07
VL
2.6
12.5
49.1
2.8
34.7
�12
NC=25
NC=65.0
NC=88
NC=45.0
SITE 5
L
H
' VH
VH
1.6 H
0.2
VL
VL
4.2
23.0
52.8
1.0
19.0
�14
�4.7
�,79
1159
10.16
NC=29
NC=117.5
NC=494
NC=80.0
Values on this report represent the plant available nutrients in the . Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: q�Aytia me Gp��
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. TT
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
Page 2 of 5
Report Numb. '4-302-0766
Account Number 00327
Send To: EHC Inc.
PO Box 902
RED SPRINGS NC 28377
Date Received: 10/29/2014
❑atp of Rpnnrt- 1n/3n/2n14
�y Ak :astern Laboratories ;.
A� 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
wwwaleastem.com
Grower:
SLUDGE SITES Farm ID:
SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P z O s
Kz O
M g
S
Zn
Mn
Fe
Cu.
B
Field ID
Tons
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
SITE 1
Bermuda, Coastal
5
1.8
75
0
224
5
14
0
2
0
0
0.5
SITE 1
Grass(Small Grain)
5
1.8
100
0
174,
5
8
0
2
0
0
0
SITE 2
Grass(Small Grain)
5
0.0
100
30
200
0
17
0
0
0
0
0
SITE 2
Bermuda, Coastal
5
0.0
75
30
338
0
23
0
0
0
0
0.5
SITE 3
Grass(Small Grain)
5
1.5
100
30
200
43 -T
16
0.9
3
0
0
0
SITE 3
Bermuda, Coastal
5
1.5
75
30
400
43
22
0
3
0
0
0.5
SITE 4
Bermuda, Coastal
5
0.8
75
30
452
47
23
0
2
0
0
0.5
SITE 4
Grass(Small Grain)
5
0.8
100
30
200
47
17
0.7
2
0
0
0
SITE 5
Grass(Small Grain)
5
0.8
100
0
200
0
15
0
0
0
0
0
SITE 5
Bermuda, Coastal
5
0.8
75
0
262
0
21
0
0
0
0
0.5
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Paudc McGroary
Page 3 of 5 - --- -
Report Numb �'-4-302-0766 v
Account NUrriRiVu 00327 �
wnMnraleastem,com
Send To: EHC Inc.
PO Box 902
RED SPRINGS NC 28377
Sample(s) : SITE 2,SITE 3,SITE 4,SITE 5 Crop: Bermuda, Coastal
Apply additional 65 pounds of nitrogen after every Cutting and harvest of hay.
Boron recommendations are on a broadcast basis.
AEI ---astern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446
Grower:
SLUDGE SITES
Farm ID:
The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in
spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield
is low the following applications should be reduced or eliminated.
Sample(s) : SITE 3,SITE 4 Crop: Bermuda, Coastal
Apply dolomitic lime to raise pH and improve the magnesium level.
If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." fl M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 Gam« OF
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary
Page 4 of 5
Report Numb' l`4-302-0766
Account Num.- . J0327
Send To: EHC Inc.
PO Box 902
RED SPRINGS NC 28377
Ne
wwwaleastem.com
Date Received: 10/29/2014 Date Of Analysis: 10130/2014
A&I _. `=astern Laboratories
7621 Whitepine Road Richmond, Virginia.23237 (804) 743-9401 Fax (804) 271.8446
Grower:
SLUDGE SITES
SOIL ANALYSIS REPORT
Date Of Report: 10/30/2014
Analytical Method(s):
Mehlich 3
Farm, ID:
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
o ENR
/o Rate
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm Rate
pH
Index
meq/100g
meq/100g
SITE 6
82 H
42 L
103
H
456
M
17 VL
05645
1.9 L 82
5.7
6.84
0.9
4.2
NC=68
NC=21
SITE 7
151 VH
75 M
93
VH
337
M
19 LF6
05646
1.5 L 76
0.2
2.9
NC=126
NC=38
Percent
Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble
Salts
Chloride
Aluminum
Sample
Field ID ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
AI
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm Rate
ms/cm
Rate
ppm Rate
ppm
SITE 6
L4.5
H
36 H
132
VH
1.1 M
0.2 VL
0.1
VL
2.6
20.4
54.3
1.8
21.123
7NC
NC=112.5
1 NC=225
NC=55.0
SITE 7
9 VL
2.5 M
25 H
113
VH
1.1 M
VL
0.06
VL
6.6
26.7
58.1
2.8
5.9
�0.1
-
NC=19
NC=62.5
NC=156
NC=55.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A, This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. �« me ��
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories,, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
Page 5 of 5
Report Numb 4-302-0766
Account Numper: 00327
Send To: EHC Inc.
PO Box 902
RED SPRINGS NC 28377
Date Received: 10/29/2014
Date Of Report: 10/30/2014
At
A& --astern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446
0
www.aleastem,com
Grower:
SLUDGE SITES Farm ID:
SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons
Tons/A
lb/A
lb/A
Ib/A
Ib/A
lb/A
Ib/A
ib/A
lb/A
Ib/A
Ib/A
SITE 6
Bermuda, Coastal
5
0.8
75
30
428
0
24
0
0
0
0
0.5
SITE 6
Grass(Small Grain)
5
0.8
100
30
200
0
18
0
0
0
0
0
SITE 7
Bermuda, Coastal
5
0.0
75
0
333
0
26
0
0
0
0
0.5
SITE 7
Grass(Small Grain)
5
0.0
100
0
200
0
20
0.8
0
0
0
0
Comments:
Sample(s) : SITE 7 Crop: Bermuda, Coastal
Apply additional 65 pounds of nitrogen after every cutting and harvest of hay.
Boron recommendations are on a broadcast basis.
The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in
spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield
is low the following applications should be reduced or eliminated.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary
2014 Application Summary Table
Campbell Soup Supply Company Land Applicat ' rogram Permit #WQ0004893
2014 Appf i n Summary
Farmer
Tract/S_ ite
Field
Acres
Date Spread
Gallons
Pounds
Dry Tons/Acre
Dry Tons
% Solids
Crop
PAN
Dry
Tons/Acre
Dry Tons
Campbell Soup Supply Company
S
1
5.1
1/28/14
10,398
86,720 '
0.3690
1.8818
4.34
Rye Grass
43.65
2.3227
11.8457
5/5/14
18,748
156,360 '
0.1426
0.7271
0.93
Bermuda
5/19/14
15,988
133,340
0.1216
0.6200
0.93
Bermuda
9/3/14
12,050 1
100,500 ,,
0.1370
0.6985
1.39
1 Bermuda
10/14/14
17,746
148,000
0.6907
3.5224
4.76
Bermuda
10/21/2014
5,004
41,740
0.1948
0.9934
4.76
Bermuda
10/28/2014
17,141
142,960
0.6671
3.4024
4.76
Bermuda
Campbell Soup Supply Company
S
2
8.4
1/20/14
13,600
113,420
0.2930
2.4612
4.34
Rye Grass
41.60
2.3421
19.6738
2/7/14
15,173
126,540
0.3269
2.7459
4.34
Rye Grass
5/9/14
17,333
144,560
0.0800
0.6722
0.93
Bermuda
5/29/14
13,691
114,180
0:0632
0.5309 1
0.93
Bermuda
5/30/14
7,971
66,480
0.0368
0.3091
0.93
Bermuda
6/9/14
9,048
75,460
0.0418
0.3509
0.93
Bermuda
11/4/14
18,501
154,300
0.4372
3.6723
4.76
Rye Grass
11/11/14
12,909
107,660
0.3050
2.5623
4.76
Rye Grass
11/15/14
15,343
127,960
0.3626
3.0454
4.76
Rye Grass
11/19/14
16,743
139,640
0.3956
3.3234
4.76
Rye Grass
Campbell Soup Supply Company
S
3
26
1/2/14
13,631
113,680
0.0949
2.4669
4.34
Pine Trees
15.07
1.0824
28.1412
2/28/14
10,616
88,540
0.0739
1.9213
4.34,
Pine Trees
3/3/14
9,600_ _
80,060
0.0668
1.7373
4.34
Pine Trees
3/13/14
17,758
148,100
0.1236
3.2138
4.34
Pine Trees
3/25/14
14,998
125,080
0.1044
2.7142
4.34
Pine Trees
4/3/14
14,863
123,960
0.0222
0.5764
0.93
Pine Trees
4/17/14
17,686
147,500 -
0.0264
U859
0.93
Pine Trees
8/22/2014
16,631
138,700
0.0371
0.9640
1.39
Pine Trees
9/16/2014
15,309
127,680
0.0341
0.8874
1.39
Pine Trees
9/30/2014
15,386
128,320
0.0343
0.8918
1.39
Pine Trees
10/8/2014
18,017
150,260 ;
0.1375
3.5762
4.76
Pine Trees
11/28/2014
21,050
175,560
0.1607
4.1783
4.76
Pine Trees
12/10/2014
7,950
66,300
0.0607
1.5779
4.76
Pine Trees
12/31/2015
13,854
115,540 :
0.1058
2.7499
4.76
Pine Trees
Campbell Soup Supply Company
S
4
9.1
1/14/14
16,165
134,820 ;
0.3215
2.9256
4.34
Rye Grass
22.45
1.7817
16.2134
2/18/14
24,388
203,400
0.4860
4.4138
4.34
Rye Grass
7/14/14
18,038
150,440
0.1149
1.0456
1.39
Bermuda
8/5/14
16,058
133,920.
0.1023
0.9307
1.39
Bermuda
8/15/14
15,249
127,180
0.0971
0.8839
1.39
Bermuda
12/16/14
12,993
108,360 -:
0.2834
2.5790
4.76
Rye Grass
12/26/14
17,304
144,320
0.3775
3.4348
4.76
Rye Grass
Campbell Soup Supply Company
S
5
3.4
1/6/14
15,885
132,480
0.8455
2.8748
4.34
Rye Grass
47.81
2.9424
10.0041
6/26/14
7,010
58,460
0.0800
0.2718
0.93
Bermuda
7/24/14
16,830
140,360
0.2869
0.9755
1.39
Bermuda
12/4/14
15,988
133,340
0.9334
3.1735
4.76
Bermuda
12/10/14
13,645
113,800 :
0.7966
2.7084
4.76
Bermuda
Campbell Soup Supply Company
S
6
2.3
6/24/14
8,185
68,260
0.1380
0.3174
0.93
Bermuda
6.97
0.3198
0.7355
6/26/14
10,782
89,920
0.1818
0.4181
0.93
Bermuda
Campbell Soup Supply Company
S
7
2.5
1 6/9/14
6,374
53,160
0.0989
0.2472
0.93
Bermuda
29.32
1.3288
3.3219
6/17114
14,441
120,440
0.2240
0.5600
0.93
Bermuda
10/21/2014
9,976
83,200
0.7921
1 1.9802
1 4.76
Bermuda
11/4/2014
2,693
22,460
0.2138
1 0.5345
1 4.76
Rye Grass
Number of Field Applied to:
56.8
686,740 5,727,420
89.9357
Campbell Soup Supply Company DAF Sludge, Maxton , NC I Gallons I Pounds . Dry Tons
2014 Application Condition Summaries
Campbell Soup Supply Company
Maxton, North Carolina
Farmer: Campbell Soup Supply Company
Site/Tract: S
Field: 1
Residual Report No: 14-059-0205
WQ0004893
1st Quarter
DAF Residuals
5.1
Application Method: Surface
Percent Solids: 4.34
Crop: Winter Rye Grass
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
1/28/2014 1 1 10,398 Dry Clear 0
I Total Gallons 1 1 10,398 1 1 1 1
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
2nd Quarter
®AF Residuals
Farmer: Campbell Soup Supply Company 5.1
Site/Tract: S Application Method: Surface
Field: 1 Percent Solids: 0.93
Residual Report No: 14-092-0202 Crop: Winter Rye Grass
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
5/5/2014
1
18,748
Dry
Clear
0
5/19/2014
1
15,988
Dry
Clear
0
Total Gallons
1
1 34,736
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
3rd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company 5.1
Site/Tract: S Application Method: Surface
Field: 1 Percent Solids: 1.39
Residual Report No: 14-190-0216 Crop: Bermuda
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
9/3/2014
1
12,050
Dry
Clear
0
Total Gallons
12,050
M
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
4th Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company 5.1
Site/Tract: S Application Method: Surface
Field: 1 Percent Solids: 4.76
Residual Report No: 14-280-0207 Crop: Bermuda
Weather
Date Field No. Gallons Soil Conditions Conditions
Prev. 24 Hour
Rainfall
10/14/2014
1
17,746
Dry
Rain
0.2
10/21/2014
1
5,004
Dry
Clear
0
10/28/2014
1
17,141
Dry
Clear
0
Total Gallons
39,891
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
1st Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 8.4
Site/Tract: S Application Method: Surface
Field : 2 Percent Solids: 4.34
Residual Report No: 14-059-0205 Crop: Winter Rye Grass
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
1/20/2014
2
13,600
Dry
Clear
0
2/7/2014
2
15,173
Dry
Clear
0
Total Gallons
28,773
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
2nd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company 8.4
Site/Tract: S Application Method: Surface
Field : 2 Percent Solids: 0.93
Residual Report No: 14-090-0202 Crop: Winter Rye/Bermuda
Weather
Date Field No. Gallons Soil Conditions Conditions
Prev. 24 Hour
Rainfall
5/9/2014
2
17,333
Dry
Clear
0
5/29/2014
2
13,691
Dry
Clear
0
5/30/2014
2
7,971
Dry
Rain
0.1
6/9/2014
2
9048
Dry
Cloudy
0
Total Gallons
1
48,043
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
4th Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company 8.4
Site/Tract: S Application Method: Surface
Field: 2 Percent Solids: 4.76
Residual Report No: 14-280-0207 Crop: Bermuda
Weather
Date Field No. Gallons Soil Conditions Conditions
Prev. 24 Hour
Rainfall
11/4/2014
2
18,501
Dry
Clear
0
11/11/2014
2
12,909
Dry
Clear
0
11/15/2014
2
15,343
Dry
Cloudy
0
11/19/2014
2
16,743
Dry
Clear
0
Total Gallons
63,496
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
1st Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 26
Site/Tract: S Application Method: Surface
Field: 3 Percent Solids: 4.34
Residual Report No: 14-059-0205 Crop: Pine Trees
Weather
Date Field No. Gallons Soil Conditions Conditions
Prev. 24 Hour
Rainfall
1/2/2014
3
13,631
Dry
Rain
0.4
2/28/2014
3
10,616
Dry
Clear
0
3/3/2014
3
9,600
Dry
Rain
0.4
3/13/2014
3
17,758
Dry
Clear
0
3/25/2014
3
14,998
Dry
Rain
0.1
Total Gallons
66,603
--'s
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
2nd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 26
Site/Tract: S Application Method: Surface
Field: 3 Percent Solids: 0.93
Residual Report No: 14-092-0202 Crop: Pine Trees
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
4/3/2014
3
14,863
Dry
Clear
0
4/17/2014
3
17,686
Dry
Cloudy
0
Total Gallons
32,549
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
3rd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 26
Site/Tract: S Application Method: Surface
Field: 3 Percent Solids: 1.39
Residual Report No: 14-190-0216 Crop: Pine Trees
Weather
Date Field No. Gallons Soil Conditions Conditions
8/22/2014 3 16,631 Dry Clear
Prev. 24 Hour
Rainfall
0
9/16/2014
3
15,309
Dry
Cloudy
0
9/30/2014
3
15,386
Dry
Rain
0.3
Total Gallons
47,326
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
4th Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 26
Site/Tract: S Application Method: Surface
Field: 3 Percent Solids: 4.76
Residual Report No: 14-280-0207 Crop: Pine Trees
Weather
Date Field No. Gallons Soil Conditions Conditions
10/8/2014 3 18,017 Dry Clear
Prev. 24 Hour
Rainfall
0
11/28/2014
3
21,050
Dry
Clear
0
12/10/2014
3
7,950
Dry
Clear
0
12/31/2014
3
13,854
Dry
Cloudy
0
Total Gallons
60,871
Campbell Soup Supply Company
Maxton, North Carolina
Farmer: Campbell Soup Supply Company
Site/Tract: S
Field: 4
Residual Report No: 14-059-0205
WQ0004893
1st Quarter
DAF Residuals
Acres: 9.1
Application Method: Surface
Percent Solids: 4.34
Crop: Winter Rye Grass
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
1/14/2014 4 16,165 Dry Rain 0.1
2/18/2014 4 24,388 Dry Clear 0
Total Gallons
Campbell Soup Supply Company
Maxton, North Carolina
Farmer: Campbell Soup Supply Company
Site/Tract: S
Field: 4
Residual Report No: 14-190-0216
WQ0004893
3rd Quarter
DAF Residuals
Acres: 9.1
Application Method: Surface
Percent Solids: 1.39
Crop: Bermuda
Date
Field No.
Gallons
Soil Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
7/14/2014
4
18,038
Dry
Clear
0
8/5/2014
4
16,058
Dry
Cloudy
0
8/15/2014
4
15,249
Dry
Clear
0
Total Gallons
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
1st Quarter
®AF Residuals
Farmer: Campbell Soup Supply Company Acres: 3.4
Site/Tract: S Application Method: Surface
Field : 5 Percent Solids: 4.34
Residual Report No: 14-059-0205 Crop: Pine Trees
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
1/6/2014
5
15,885
Dry
Rain
0.1
Total Gallons
15,885
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
2nd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 3.4
Site/Tract: S Application Method: Surface
Field : 5 Percent Solids: 0.93
Residual Report No: 14-092-0202 Crop: Bermuda
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
6/26/2014
5
7,010
Dry
Clear
0
Total Gallons
7,010
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
3rd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company
Site/Tract: S
Field: 5
Residual Report No: 14-190-0216
Date Field No. Gallons
7/24/2014 5 16,830
Total Gallons
Acres: 3.4
Application Method: Surface
Percent Solids: 1.39
Crop: Bermuda
Weather Prev. 24 Hi
Soil Conditions Conditions Rainfall
Dry Cloudv 0
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
4th Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 3.4
Site/Tract: S Application Method: Surface
Field: 5 Percent Solids: 4.76
Residual Report No: 14-280-0207 Crop: Bermuda
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
12/4/2014
5
15,988
Dry
Cloudy
0
12/10/2014
5
13,645
Dry
Rain
0.1
Total Gallons
29,633
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
2nd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 2.3
Site/Tract: S Application Method: Surface
Field : 6 Percent Solids: 0.93
Residual Report No: 14-092-0202 Crop: Bermuda
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
6/24/2014
6
8,185
Dry
Cloudy
0
6/26/2014
6
10,782
Dry
Clear
0
Total Gallons
18,967
Campbell Soup Supply Company
Maxton, North Carolina
WQ0004893
2nd Quarter
DAF Residuals
Farmer: Campbell Soup Supply Company Acres: 2.5
Site/Tract: S Application Method: Surface
Field: 7 Percent Solids: 0.93
Residual Report No: 14-092-0202 Crop: Bermuda Grass
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
6/9/2014
7
6,374
Dry
Clear
0
6/17/2014
7
14,441
Dry
Cloudy
0
Total Gallons
20,815
Campbell Soup Supply Company
Maxton, North Carolina
Farmer: Campbell Soup Supply Company
Site/Tract: S
Field: 7
Residual Report No: 14-280-0207
WQ0004893
4th Quarter
DAF Residuals
Acres: 2.5
Application Method: Surface
Percent Solids: 4.76
Crop: Bermuda Grass
Weather Prev. 24 Hour
Date Field No. Gallons Soil Conditions Conditions Rainfall
10/21/2014 7 9,976 Dry Clear 0
11/4/2014 7 2,693 Dry Clear 0
I Total Gallons 1 1 12,669 1 1 1 1