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HomeMy WebLinkAbout970040_Chain of custody_20180620DIVISION OF WATER QUALITY Chemistry Laboratory Report / Water Quality Lab Number -0 SAMPLE TYPE Date Received: COUNTY RIVER BASIN: \ A( v')'11/4,0-S V D PRIORITY AMBIENT 0 QA �TREAM EFFLUENT Time Received: Received By REPORT TO yJ Cl IZ Regional Office COMPLIANCEXIA CHAIN OF CUSTODY LAKE INFLUENT Other EMERGENCY VISIT ID ESTUARY Data Released COLLECTOR(S) 6G v— ❑ Date Reported: Estimated BOD Range: Station Location: d 0-, R •-T D wV15+ re-ra vvq Seed: Chlorinated: Remarks: Station #/Location Code Date Begin (yy/mm/dd) Date End (yylm /dd) Ti a Begin Time End Depth - DM, DB, DBM Value Type - A, H, L Composite-T, S, B Sample Type lg o� 2C� t8 0�� zo 16; s 6'.5- 7 BOD 310 mg/L COD High 340 mgtL COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /10021 Coliform: tube Fecal 31615 /100ml Coliform: Fecal Strep 31673 /loom] Residue: Total 500 mg/L Volatile 505 mg/L Fixed 510 mg1L Residue: Suspended 530 mg/L Volatile 535 mg/L Fixed 540 mg/L PH 403 units Acidity to pH 4.5 436 mg/L Acidity to pH 8.3 435 mg/L Alkalinity to pH 8.3 415 mgtL Alkalinity to pH 4.5 410 mgtL TOC 680 mg/L Turbidity 76 NTU Coliform Total Tube /100 nil COMMENTS : Chloride 940 mg1L Chlorophyll a EPA 445.0 modified option ug/L Color: True 80 C.U.— Color:(pH) 83 pH= C.U. Color: pH7.6 82 c.u. Cyanide 720 mg/L Fluoride 951 mg/L Formaldehyde 71880 me/L Grease and Oils 556 mg/L Hardness Total 900 mv-/L Specific Cond. 95 umhos/cm MBAS 38260 mg1L Phenols 32730 ug/L Sulfate 945 mg/L Sulfide 745 mg/L Boron Tannin & Lignin ug/L Hexavalent Chromium ug(L Bicarbonate mg/L Carbonate mg/L Total Dissolved Solids mg/L NH3 as N 610 mg/L TKN an N 625 mg/L NO2 plus NO3 as N 630 mg/L P: Total as P 665 mg/L PO4 as P 70507 mg/L P: Dissolved as P 666 mg/L K-Potassium mg/L Cd- Cadmium 1027 ugtL Cr-Chromium:Total 1034 ug/L Cu- Copper 1042 ug/L Ni-Nickel 1067 ug/L Pb- Lead 1051 ug/L Zn- Zinc 1092 ugtL IV -Vanadium ug(L Ag- Silver 1077 ugtL Al- Aluminum 1105 ug/L Be- Beryllium 1012 ug/L Ca- Calcium 916 mg/L Co- Cobalt 1037 ug/L Fe- Iron 1045 ugtL Mo-Molybdenum ug/L Sb-Antimony ug/L Sn-Tin ug/L TI-Thallium ug/L Ti-Titanium ug/L Hg-1631 ng/L P = 7toz- Obbo - 43r _I �ll✓ Li -Lithium 1132 ug/L Mg- Magnesium 927 mg/L Mn-Manganese 1055 ug/L Na- Sodium 929 mg/L Arsenic:Total1002 ug(L Se- Selenium 1147 ug/L Hg- Mercury 71900 ug/L Ba-Barium ug/L Organochlorine Pesticides Organophosphorus Pesticides Organonitrogen Pesticides Acid Herbicides Base/Neutral&Acid Extractable Organics TPH Diesel Range Purgeable Organics (VOA bottle req'd) TPH Gasoline Range TPH/BTEX Gasoline Range Phytoplankton Temperature on arrival (°C): C COUNTY R[VER BASIN : Sa Ki j' REPORT TO W 5 R © Regional Office Other : COLLECTOR(S) :— P- Estimated BOD Range: DIVISION OF WATER QUALITY Chemistry Laboratory Report / Water Quality SAMPLETYPE PRIORITY AMBIENT Ej QA "tREAM IN: EFFLUENT COMPLIANCE PI -CHAIN OF CUSTODY [—] LAKE 0 INFLUENT El EMERGENCY VISIT ID EJ ESTUARY Station Location: Lab Number Date Received Time Received: Received By : Data Released : Date Reported Seed: Chlorinated: Remarks: Station #/Location Code Da a Begi (yy/mm/dd) Date End (yy/mm/dd) Time Begin Time End Depth - DM, DB, DBM Value Type - A, }I, L Composite-T, S, B Sam Type 06 zoI I (Y) BOD 310 mg/L COD High 340 mg/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 /100ml Coliform: tube Fecal 31615 /100ml Coliform: Fecal Strep 31673 1100ml Residue: Total 500 mg/L Volatile 505 mg/L Fixed 510 mg(L Residue: Suspended 530 mg/L Volatile 535 mg/L Fixed 540 mg/L pH 403 units Acidity to pH 4.5 436 mg/L Acidity to pH 8.3 435 mg/L Alkalinity to pH 8.3 415 mg/L Alkalinity to pH 4.5 410 mg/L OC 680 mg/L Turbidity 76 NTU Califomt Total Tube /100 ml Chloride 940 mg/L Chlorophyll a EPA 445.0 modified option ug/L Color: True 80 C.U. Color: (pH) 83 pH= C.U. Color: pH 7.6 82 C.U. Cyanide 720 mg/L Fluoride 951 mg/L Formaldehyde 71880 mg/L Grease and Oils 556 mg/L Hardness Total900 mg/L Specific Cond. 95 umhos/cm MBAS 38260 mg/L Phenols 32730 ug/L Sulfate 945 mg1L .Sulfide 745 mg/L Boron Tannin & Lignin ug/L Hexavalent Chromium ug/L Bicarbonate mg/L Carbonate mg/L. Total Dissolved Solids mg/l, COMMENTS: L NH3 as N 610 mg/L TKN an N 625 mg/L 'NO2 plus NO3 as N 630 mg/L P: Total as P 665 me/L PO4 as P 70507 mg/L P: Dissolved as P 666 mg/L K-Potassium mg/L Cd- Cadmium 1027 ug/L Cr-Chromium:Total 1034 ug/L Cu- Copper 1042 ug/L Ni-Nickel 1067 uafL Pb- Lead 1051 ug/L Zn- Zinc 1092 ug/L V-Vanadium u_WL Ag- Silver 1077 ug/L Al- Aluminum 1105 ug/L Be- Beryllium 1012 ug/L Ca- Calcium 916 mg/L Co- Cobalt 1037 ug/L Fe- Iron 1045 ug/L Mo-Molybdenum ug/L Sb-Antimony ug/L Sn-Tin ug/L TI-Thallium ug L Ti-Titanium ug/L Hg-1631 ng/L Li -Lithium 1132 ug/L Mg- Magnesium 927 mg/L Mn-Manganese 1055 ug/L Na- Sodium 929 mtf� L Arsenic:Total1002 ug/L Se- Selenium 1147 ug/L Hg- Mercury 71900 ug/L Ba-Barium ug/l. Organochlorine Pesticides Organophosphorus Pesticides Organonitrogen Pesticides Acid Herbicides Base/Neutral&Acid Extractable Organics TPH Diesel Range Purgeable Organics (VOA bottle req'd) TPH Gasoline Range TPH/BTEX Gasoline Range Phytoplankton Temperature on arrival (°C): C, DIVISION OF WATER QUALITY Chemistry Laboratory Report / Water Quality Lab Number ❑ SAMPLE TYPE Date Received y COUNTY V v : ` Pi PRIORITY Time Received: RIVERBASIN:Ck9j AMBIENT QA �t STREAM 5�/ '�C EFFLUENT Received By REPORT TO G (J Regional Office COMPLIANCE CHAIN OF CUSTODY LAKE INFLUENT Other : EMERGENCY VISIT ID ESTUARY Data Released COLLECTOR(S) C- L" ❑ Date Reported ( Station Location: U 5- C' Estimated BOD Range: I {i n V Seed: Chlorinated: Remarks: Station N/Location Code Dat Begin (yy/mm/dd) Date End (yy/mm/dd) Time Begin I Time End Depth - DM, DB, DBM Value Type - A, H, L Composite-T, S, B Sample Type Ola Z, tb l2 l 0 a BOD 310 - mg/L COD High 340 nw/L COD Low 335 mg/L Coliform: MF Fecal 31616 /100ml Coliform: MF Total 31504 1100H Coliform: tube Fecal 31615 /100ml Coliform: Fecal Strep 31673 /100ml Residue: Total 500 mg/L Volatile 505 mg/L Fixed 510 mg/L Residue: Suspended 530 mg/L. Volatile 535 mg/L Fixed 540 mg/L pH 403 units Acidity to pH 4.5 436 mg/L Acidity to pH 8.3 435 mg/L Alkalinity to pH 8.3 415 mg/L Alkalinity to pH 4.5 410 mg/L TOC 680 mg/L Turbidity 76 - NTU Coliform Total Tube /100 ml COMMENTS: Chloride 940 . mg/L Chlorophyll a EPA 445.0 modified option ug/L Color: True 80 c.u. Color: (pH) 83 pH= au. Color: pH 7.6 82 c.u. Cyanide 720 mg/L Fluoride 951 mg/L Formaldehyde 71880 mall, Grease and Oils 556 mg/L Hardness Total900 mg/L Specific Cond. 95 umhos/cm MBAS 38260 mg/L Phenols 32730 ug/L Sulfate 945 mg/L Sulfide 745 mgfL Boron Tannin & Lignin ug/L Hexavalent Chromium ug/L Bicarbonate mg/L Carbonate mg/L Total Dissolved Solids mgtL NH3 as N 610 tj" mg/L an N 625 mg/L NO2 plus NO3 as N 630 mg/L P: Total as P 665 mg/L PO4 as P 70507 mg/L P: Dissolved as P 666 mg/L K-Potassium mg/L Cd- Cadmium 1027 ug/L Cr-Chromium:Total 1034 ug/I. Cu- Copper 1042 ug/L Ni-Nickel 1067 ug/L Pb- Lead 1051 ug/L Zn- Zinc 1092 ug/L V-Vanadium ug/L Ag- Silver 1077 ug/L Al- Aluminum 1105 ug/L Be- Beryllium 1012 ug/L Ca- Calcium 916 mg/L Co- Cobalt 1037 ug/L Fe- Iron 1045 ug/L Mo-Molybdenum ug/L Sb-Antimony ug/L Sn-Tin ue-/L TI-Thallium ug/L Ti-Titanium ug/L Hg-1631 ng/L Li -Lithium 1132 ug/L Mg- Magnesium 927 mg/L Mn-Manganese 1055 ug/L Na- Sodium 929 mg/L Arsenic-Total1002 ug/L Se -Selenium 1147 ug/L Hg- Mercury 71900 ug/L Ba-Barium ug/L Organochlorine Pesticides Organophosphorus Pesticides Organonitrogen Pesticides Acid Herbicides Base/Neutral&Acid Extractable Organics TPH Diesel Range Purgeable Organics (VOA bottle req'd) TPH Gasoline Range TPH/BTEX Gasoline Range Phytoplankton Temperature on arrival (°C): _5 17 Z) = 15 r Report to: W/ 5j p,C) WATER QUALITY SECTION Page of! CHAIN OF CUSTODY (COC) RECORD NC DENR/DWQ LABORATORY (check one): CENTRAL [I ARO [I WaRO For Investigation of: C VZ n L e-- Sample collector (print name) and DM-1 forms completed by: tvlv-OU1SSGQ P-pSEbroc-y- Sample collector'ssignatm, Field storage conditions and location (when ap licable): Dut'jfo,-•{e— ve�hi,cl-e— L�6>Use Only NUMBER DATE TIME OF z . .Li1B NO�fi. ,` STATION NO. STATION LOCATION SAMPLED SAMPLED CONTAINERS ^ DlY eta 1>0VQ4- J5+rt° a- brv�2c-2e18 fp.7 HOL yr �i,- zo- �� ► l 3 6 3 fteii. U 5 4-r m. c G c6 -aa[ Z U l l i rl R t5 �x pir, :st= n.. k *� -- +p. G e � quished by signature): Date Time Received by (signature): Date Time 06-z0-;Zo F l b-3 hr s Relinquished by (signature): Date Time Received by (signature): Date Time Relinquished by (signature): Date Time Received by (signature): Date Time Method of Shipment (circle one): a Cowrie Hand -delivered Federal Express UPS Other: Sealed by: keA j S, S e- I0� L jL $token by - Security Type and Conditions: S r LAG E d K C.ou :" i er- bo K UP LUJ1L)VT - LaD use QA\Forms\Sample Receiving\COC form WQ 4/10/01dbs Water Quality Monitoring Field Meter Calibration Sheet Collector(s): Study: Meter Model: J1 Meter / Sonde Serial No: 1-�, —,� � V--) Date yy/mm/dd Time 24hr hh:mm Initials Pre -Sampling Calibration Post -Sampling Check Miscellaneous (Does not apply to YSI or Accumet Meters) Battery Level M Stirrer Working? Pre -Sampling Calibration / / N Post -Sampling Check Battery Ranges = Surveyor: Internal- r.2-/.bv, external- 11-13V; uuanta: 4.u-4.bv rlissnlvprt CfYvnPn /mn/L► Barometer Calibration (mmHg) 'YSI Pro Plus Meters Only - Initial Reading Calibrated Value 3atg 133 Initial % Barometric Pressure D.O. Table Initial Meter Calibrated Meter Calibrated % Temp. °C Saturation mmH Altitude (ft.) Value Reading (mg/L) Reading (mg/L) Saturation Pre -Sampling Calibration n �r� wv C` Jt Post -Sampling Check aa`� y2 Za r Within c Conductance (NS/cm at 25°C) Lot #: Lot #: I k U '6 U. Dry Air 1.2 Conductive Standard 3 Calibration Check Zero (0) value: `0�� Value: lz_,�` Initial Meter Calibrated 4 Initial Meter Calibrated 4 Initial Meter ±10% Ranges for Sp: Cond. Reading Meter Reading Reading Meter Reading Reading of Standard Rance 100.., 90to116 . piing Calibration p g --� ` ` \oo\ 500 :' 450 to 550.: 1 000 . 90o to 1;100 npling Check Wit 1090 - Wi hin ±10% 10;OO6 %000 to 11.,000. - Y / Y / N 7W N 13,500 to 18 500 15,0.00 NOTE: Quanta reads in mS/cm; move deimal 3 places right for pS/cm. 5%:0011 . 45,000 to 55,000 1 Dry Air CALIBRATIONS are conducted for 4a and M55 Hydrolabs only. Z Dry Air CHECKS (confirmation of zero in dry air) are conducted for YSI 85, YSI 6920, YSI Pro Plus & Quanta meters. J Conductivity standards are used to CHECK the YSI 85 meter and to CALIBRATE all Hydrolab meters and the YSI 6920 & YSI Pro Plus. 4 Does not apply to Dry Air. CHECKS or Conductivity Standard CHECKS (leave blank).( (� pH (SU) Lot #: a��o�� Lot #: Buffer #1 BuffeLU confirmation 70 ++ 10.0 Buffer Buffer Temp: �h sp Buffer Temp: �b,'R Slope Efficiency' 7.0 Initial Meter Calibrated Meter Initial Meter Calibrated Meter Meter Reading Reading Reading Reading Reading Pre -Sampling Calibration -ul,\ `lt�a, a ,®�QCj I,�>,.? Post -Sampling Check �t�S \ `0.:........ Within ?? Y / N .................... ± 0.2? Within ± 0.2? MVVi Y N Y N 5 Slope efficiency applies to Accumet meters only (does not apply to Hydrolab or YSI meters). Comments: Keep original on file for 5 years Ver. 0610512012 LAbORATORiES, INC. Analytical / Process Consultations Phone (336) 996-2841 (.Umpapy ,In]) No. .�' G bL i .N Jcz)rejf Street Address proojecl D W . 44 tll i; S t � Q . Rol City, Slate, Zip Sampler Name (Please ['rinl� V'J I n 5-k-ci� ti��t�Q_-m L-JC_. contact. l'IltRit Sampler Siguatore 1` dv)sg� Ro.-'Arcc� .33� 1'16.�tatj� Sample. NIluber Date FI Time IC'onlp. Crab TCnlp ���'� ]teS. Cl. Cidol'ine Itemuvc'I cSFn11pIC Matrix (t.Ttt tjsC t)Iltt'I VorN (SorW, 0 li'ttr;ii [IV 1)a(cJ1'irrlc Relinquished BY Uatefi'ime Rectived B Iji6vived By Water / Wasteivater 1 Misc. Y L! ja o p is J Sample I atcution ! ].]). O o U o E c a� U 0, a v c T C Ca Y u'vJ 615 �rctss, n 1tr+ Remarks Ice ' Sample Temperature at receipt '- I 1c,