970043_Report of Analysis_20180624

0
RESEARCh&ANA1YT*1CA1
..O,
For: NC DENR DWQ
450 W. Hanes Mill Rd. Suite 300
Winston-Salem, NC 27105
Attn: Melissa Rosebrock
Client Sample ID: Downstream Harper
Site: NC DEQ
Report of Analysis
6/24/2018
s ptt•:zerr+'�+
NC ti34 z
M NC 937701
% r
Lab Sample ID: 52312-01
Collection Date: 6/20/2018 10:57
Fra
ameter Method Result Units Rep Limit Analyst Analysis Date/Time
Fec Coli-MF SM 9222 D-1997 >12000 col/100 ml 1 8J 6/20/20i8 1645
Client Sample ID: Upstream Harper Lab Sample ID: 52312-02
Site: NC DEQ Collection Date: 6/20/2018 11:30
Parameter Method Result Units Rep Limit Analyst Analysis DatelTime
Fec Cali-MF SM 9222 D-1997 >12000 col/100 inl 1 BJ 6/20/2018 1650
Client Sample ID: Upstream McGinnis Lab Sample ID: 52312-03
Site: NC DEQ Collection Date: 6/20/2018 12:10
I Parameter Method Result Units Rep Limit Analyst Analysis Date/Time
t_ ,. __.. �................ .... . _ .. __ _ ._...-_ ........... _.._ _ ._ _ ___-- ___ _ _ _ _ __. _._._ _.___... ......... ..... ... ........ _...____._ _ _.._ ..W ._ _ __._ ____.._.._ .. _ ... _....... .....
Fec Cali-MF SM 9222 D-1997 >12000 col/100 ml 1 BJ 6/20/2018 1700
NA = not analyzed
P.O. Box 473 106 Short Street Kemersville, North Carolina 27284 Tel: [phone] Fax. [phone] www,randalabs.com Page 1

AC51732 North Carolina Division of Water Resources Water Sciences
Loc. Descr.:
HARPER DOWNSTREAM `/
County:
Wilkes
Collector:
M ROSEBROCK
VisitlD
Region:
WSRO
Report To
WSRO
Location ID:
WSRO NLC
River Basin
YAD01
Collect Date:
06/2012018
Priority
COC
Emergency
Collect Time:
10_67
Sample Matrix:
SURFACEWATER
COC Yes/No
Yes
Sample Depth
Loc. Type:
River/Stream
Final Report
Sample ID:
AC51732
PO Number #
Date Received:
06/2112018
Time Received:
08:16
Labworks LoginlD
TASCENZ01
Delivery Method
NC Courier
Final Report Date:
7110118
Report Print Date:
07/1012018
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/
Method
Analysis
CAS # Analyte Name
PQL
Qualifier
Units
Reference
Date
Validated by
LAB
Sample temperature at receipt by lab
2.4
°C
6/21/18
RBYRD
MIC ,
BOD, 5-Day in liquid
2.0
12
mg/L
SM 5210 B-2001
6/21/18
ESTAFFORDI
Turbidity
1.0
34
NTU
SM 2130 B-2001
6/21/18
RBYRD
NUT
NH3 as N in liquid
0.02
7.0
mg/L as N
EPA 350.1 REV 2
6/21/18
CGREEN
NO2+NO3 as N in liquid
0.02
0.66
mg/L as N
EPA 353.2 REV 2
6/21/18
CGREEN
Phosphorus —total as P in liquid 0.02 0.57 mg/L as P EPA 365.1 REV 2 6/29/18 CGREEN
Total Kjeldahl N as N in liquid 0.2 8.6 mg/L as N EPA 351.2 REV 2 6/28/18 CGREEN
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

AC51733 North Carolina Division of Water Resources Water Sciences
Loc. Descr.:
UPSTREAM HARPER
County:
Wilkes
Collector:
M ROSEBROCK
VisitlD
Region:
WSRO
Report To
WSRO
Location ID:
WSRO NLC
River Basin
YAD01
Collect Date:
06/20/2018
Priority
COC
Emergency
Collect Time:
11_30
Sample Matrix:
SURFACEWATER
COC Yes/No
Yes
Sample Depth
Loc. Type:
River/Stream
Final Report
Sample ID:
AC61733
PO Number #
Date Received:
06/21/2018
Time Received:
08:15
Labworks LoginlD
TASCENZ01
Delivery Method
NC Courier
Final Report Date:
7/10/18
Report Print Date:
07/10/2018
if this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/
Method
Analysis
CAS # Analyte Name
P L
Qualifier
Units
Reference
Date
Validated by
LAB
Sample temperature at receipt by lab
2.4
°C
6/21/18
RBYRD
MIC
BOD, 5-Day in liquid
2.0
9.8
mg/L
SM 5210 B-2001
6/21118
ESTAFFORDI
Turbidity
1.0
37
NTU
SM 2130 B-2001
6/21/18
RBYRD
NUT
NH3 as N in liquid 0.02 7.0 mg/Las N EPA 350.1 REV 2 6/21/18 CGREEN
NO2+NO3 as N in liquid 0.02 0.74 mg/L as N EPA 353.2 REV 2 6/21/18 CGREEN
Phosphorus —total as P in liquid 0.02 0.36 mg/L as P EPA 365.1 REV 2 6/29/18 CGREEN
Total Kjeldahl N as N in liquid 0.2 8.2 mg/L as N EPA 351.2 REV 2 6/28/18 CGREEN
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL.
Page 1 of 1

AC51734
North Carol'Carolista Division of Water Resources Water Sciences
Loc. Descr.:
UPSTREAM MCGILLIS
County:
Wilkes
Collector:
M ROSEBROCK
VisitlD
Region:
WSRO
Report To
WSRO
Location ID:
WSRO NLC
River Basin
YAD01
Collect Date:
06/20/2018
Priority
COC
Emergency
Collect Time:
12_10
Sample Matrix:
SURFACEWATER
COC Yes/No
Yes
Sample Depth
Loc. Type:
River/Stream
Final Report
Sample ID:
AC51734
PO Number #
Date Received:
06/21/2018
Time Received:
08_16
Labworks LoginlD
TASCENZ01
Delivery Method
NC Courier
Final Report Date:
7/10118
Report Print Date:
07/10/2018
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result/
Method
Analysis
CAS # Analyte Name
PQL
Qualifier
Units
Reference
Date
Validated by
LAB
Sample temperature at receipt by lab
2.4
°C
6/21/18
RBYRD
MIC
BOD, 5-Day in liquid
2.0
64
mg/L
SM 5210 B-2001
6/21/18
ESTAFFORDI
Turbidity 0 kj-r-tj1.0
380 Vr
NTU
SM 2130 B-2001
6/21/18
RBYRD
NUT
NH3 as N in liquid
0.02
2.5
mg/L as N
EPA 350.1 REV 2
6/21/18
CGREEN
NO2+NO3 as N in liquid
0.02
2.2
mg/L as N
EPA 353.2 REV 2
6/21/18
CGREEN
Phosphorus —total as P in liquid
0.02
0.94
mg/L as P
EPA 365.1 REV 2
6/29/18
CGREEN
Total Kjeldahl N as N in liquid
0.2
7.1
mg/L as N
EPA 351.2 REV 2
6/28/18
CGREEN
WSS Chemistry Laboratory>> 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 7333908
"Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the POL.
Page 1 of 1