WQ0003824_Residual Annual Report 2014_20150225

CITY OF GRAHAM
LAND APPLICATION
2014 ANNUAL REPORT
'REMIMIDENROV
FEB �,� 2015
P rmto 1
�tio0

Cott# of *a4am
P.O. Drawer 357
201 South Main Street
Graham, North Carolina 27253
Tel: [phone] / Fax: [phone]
DENR/DWQ/WATER QUALITY SECTION
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, N.C. 27699-1617
February 23, 2015
Dear Sirs:
The following data and report are for the City of Graham's land application
program:
Permit Number
Period Covered
Sources of Sludge
Method of Application
WQ0003824
Jan.1, 2014 thru Dec.31, 2014
City of Graham WWTP,
City of Graham Water Plant
Surface Applied
Bio-solids from the City of Graham Wastewater Treatment Plant were land
applied in eleven months during 2014; sludge application did not occur in
September. Ferric sludge from the City of Graham Water Treatment Plant was land
applied during May of 2014. Synagro Southeast, Inc. of Clemmons, NC, provides
alum sludge records and data. Applied metal calculations reflect the totals of both
sources of sludge. The metal loadings (ending 12/31/2013) were added to the 2014
WWTP bio-solids and then added to the 2014 Ferric sludge totals to arrive at the
ending 2014 accumulated metal totals.
Soil samples were reported in September 2014 and are attached.
The TCLP Analysis sample was collected on October 16, 2014 and is
attached.

Quarterly Sludge Analysis was performed during March, May, July, and
October of 2014.
The City met the 40 CFR 503(B) rules for Pathogen Reduction (Class B,
Alternative 1 for Fecal Coliform and Vector Attraction Rate by Specific Oxygen
Uptake Rate. The City of Graham uses the North Carolina Department of
Environmental and Natural Resources method developed by them for the US EPA.
If any additional information or explanation is needed, please, contact me at
[phone].
Sincerely;
Crispian T. Routh
Plant Superintendent
City of Graham
1

ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0003824 County: ALAMANCE Year: 2014
Facility Name (as shown on permit): CITY OF GRAHAM
Land Application Operator: Crispian T. Routh Phone: [phone]
Land application of residual solids as allowed by the permit -occurred during the past calendar year?
■ Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit: 9
Total number of fields land application occurred durine the vear: 9
Total amount of dry tons applied during the year for all application sites: 248.315
Total number of acres land application occurred during the year: 89.4
Part B:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. ❑ Yes No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that'there-are significant -penalties -for submitting false information,
' including the possibility of fines and imprisonment for knowing violations."
Victor R. Quick / Utilities Director ` u /S . � Z3 1
Permittee Name and Title .(type or print) Signature of Permittee Date
Signature of Preparer*
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r)
f _1
Date Signature of Land Applier Date
(if different from Permittee and Preparer)

The City of Graham received a `Notice of Violation' concerning its Land Application Permit
WQ0003824 for the following buffer zone violations as determined by DWR staff during its annual
Compliance Inspection on July 10, 2014:
Condition II.5. a. Buffer zone of 400 feet from residences
Residuals had recently been applied within two house buffers. on Field 2.
Condition II.5. d. Buffer zone of 100 feet from any streams classified as WS
Permanent stakes used to mark setbacks on Field 10 were approximately 50 feet, which was less
than the required 100 feet, from Haw Creek, which is classified as a water supply stream.
Corrective actions taken for each of the violations were as follows:
Re: Condition II.5. a. Buffer zone of 400 feet from residences
The City of Graham contracted a local engineering firm to re-establish the correct residency buffers
on Field 2. No biosolids were applied on Field 2 until the correct residency buffers in place.
Re: Condition II.5. d. Buffer zone of 100 feet from any streams classified as WS.
The City of Graham relocated setbacks from Haw Creek to 100 feet on Field 10. However, in our
new Land Application permit which went into effect on December 1, 2014, surface application of
biosolids on Field 10 is prohibited due to being located within the 100 year flood plain. Setbacks
were returned to their original 50 feet which meets subsurface application guidelines. At this time,
The City of Graham has suspended all land application on this field.
Victor Quick / Utilities Director �cc Z Z3
Permittee Name and Title (type or print) Signature of Permittee D6

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: CITY OF GRAHAM Permit Number:
WWTP Name: CITY OF GRAHAM NPDES Number:
Monitoring Period: From 1/1/2014 1 - To 3/31/2014
WQ0003824
NCO021211
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ElHeat
Treatment ❑
Thermophilic ❑
::
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1 ET
Alternative 2 77T
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"!
Lime Stabilization MT
Air Drying ❑
I Composting ❑
jAerobic Digestion ❑
Anaerobic Digestion i n
g
...................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number of
Excee-
d n
Frequency
of
AnalysisType
Sample
Analytical
Tech -
ni aue
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
2
26
199
MPN
0
QTRLY
GRAB
9221 B
_ 1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry wei ht
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ Option 3 ❑ I Option 4 0 1 Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ I Option 10 ❑
No vector attraction reduction
were options performed
p
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the -requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Crispian T. Routh / Plant Superintendent C2.lSPIAN ! 120U T P I PANT SCAPT.
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
-F, 2 -12- 3/IS'
Signature of Preparer Date Signature of Land Applier (if applicable) Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: CITY OF GRAHAM Permit Number: WQ0003824
WWTP Name: CITY OF'GRAHAM NPDES Number: NCO021211
Monitoring Period: From 4/l/2014 To 6/30/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3E1:1
Alternative 4 ❑
Alternative 5 ❑
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ElHeat
Treatment ❑
Thermophilic El::
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1
Alternative 2 ❑
Alternative 3 El::
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
I Aerobic Digestion ❑
Anaerobic Di estion
g
............................................................................................
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number ot
Excee-
n
Prequency
of
Analysis
Sample
Type
Analytical
Tech -
niaue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
2
5
11
MPN
0
QTRLY
GRAB
9221 B
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option, performed:
Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 0 Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑
P were ons No vector attraction reduction o tirformed
P
e ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an.explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and. supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Crispian T. Routh / Plant Superintendent
Preparer Name and Title (type or print)
Z,Itw�T 4-4(
Signature of Preparer Date
C2►setAN T. PouTN I PLANT APT.
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: CITY OF GRAHAM Permit Number: WQ0003824
WWTP Name: CITY OF GRAHAM NPDES Number: NCO021211
Monitoring Period: From 7/1/2014 To 9/30/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost El
Heat Drying El
Heat Treatment ElThermophilic
El::
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1
Alternative 2 ❑
Alternative 3 El:;:
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑
I Aerobic Digestion ❑
Anaerobic Di estion
g
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of
Sample
Type
Analytical
Tech -
ni oue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
1
2
3
MPN
0
QTRLY
GRAB
9221 B
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 0 1 Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ 1 Option 10 ❑
No vector attraction reduction
were options performed
P
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
l
this statement attach. an explanation_ why you -have not met.one or- both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment,"
Crispian T. Routh / Plant Superintendent
Preparer Name -and Title (type or print)
eRISP/AN T 120147N % (SLANT, 5"19r
Land Applier Name and Title (if applicable)(type or print)
Z 23 l5
Signature of Preparer Date
Signature of Land Applier (if applicable) Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: CITY OF GRAHAM
WWTP Name: CITY OF GRAHAM
Monitoring Period: From 10/1/2014
Permit Number:
NPDES Number:
To 12/31/2014
WQ0003824
NCO021211
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3
Alternative 4 ❑
Alternative 5 ❑
Alternative 6 ❑
..........
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ElHeat
Drying ❑
I Heat Treatment ElThermophilic
El::
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1
Alternative 2 Ll
Alternative 3
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑
jAerobic Digestion ❑
n r A ae obtc Digestion estion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
n
Frequency
An 1 i
Sample
Type
na yica
Tech -
n iaue
inimu
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
1
4
7
MPN
0
QTRLY
GRAB
9221 B/
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 LJ Option 2 ❑ 1.0ption 3 ❑ Option 4 0 10ption 5 I -I
Option 6 ❑ Option 7 ❑Option 8 ❑ 1 Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Crispian T. Routh / Plant Superintendent
Preparer Name and Title (type or print)
&G,w%% ! ` fiw 2 23 1 S
Signature of Preparer Date
C215PiAN -r (20ttlrl-1 / PLANT s14PT,
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date

r01
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003824 Laboratory:
Facility Name:
NPDES # or
WQ#:
WWTP Name:
Residual Analvsis Data
CITY OF GRAHAM
NCO021211
CITY OF GRAHAM
1) MERITECH, INC.
2)
3)
4)
5)
Sample or
Composite Date
3/19/14
5/7/14
7/9/14
10/16/14
Percent Solids
1.83
1.89
1.73
1.33
Arsenic
<2.78
<2.63
<2.89
<0.752
Cadmium
3.78
3.89
3.7
4.81
Chromium
88
88.4
77.5
88
,b
Copper
438
455
431
502
Lead
35.9
32.7
30.1
43.8
Mercury
0.25
0.4760
0.462
0.226
Molybdenum
6.94
9.26
7.3
5.19
Nickel
15.6
16.6
16.5
17.9
Selenium
<2.78
5.89
5.09
<0.752
Zinc
861
700
665
1,170
Total Phosphorus
19,944
22,736
24,600
30,200
TKN
55,200
60,800
59,500
35,300
Ammonia -Nitrogen
3,730
7,410
10,800
15,500
Nitrate and Nitrite
<546
<529
<578
1 <752
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature o Preparer Date
DENR FORM RSSF (5/2003)

w
City of &a4at t
P.O. Drawer 357
201 South Main Street
Graham, North Carolina 27253
Tel: [phone] / Fax: [phone]
Ed Hardee
NCDENR/Aquifer Protection Section
1636 Mail Service Center
Raleigh, NC 27699-1636
February 27, 2015
Subject: 2014 Annual Report Correction
Dear Mr. Hardee,
Enclosed is a corrected copy of the Annual Residual Sampling
Summary Form for the City of Graham's 2014 Land Application Annual
Report., .A typographical error resulted in the October 16, 2014 data for Lead
to incorrectly -read "4308 mg/kg". The correct result is "43.8 mg/kg". Two
additional corrected copies are also enclosed.
If you need any additional information regarding our 2014 Annual
Report, please contact me at 336.570.6721 or email at
[e-mail].
Sincerely,
Crispian T. Routh
Plant, Superintendent
City: of Graham
Cc: Victor Quick, Utilities Director
'REGEeVEDIDENRIDINR
MAR - 2 2015
WeltorQuality
Permifflng Section

k
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003824 Laboratory: 1) MERITECH, INC.
Facility Name: CITY OF GRAHAM 2)
NPDES # or NCO021211 3) yr
WQ#:
4)
WWTP Name: CITY OF GRAHAM 5)
Residual Analvsis Data
Sample or
Composite Date
3/19/14
5/7/14
7/9/14
10/16/14
Percent Solids
1.83
1.89
1.73
1.33
Arsenic
<2.78
<2.63
<2.89
<0.752
Cadmium
3.78
3.89
3.7
4.81
Chromium
88
88.4
77.5
88
,b
Copper
438
455
431
502
Lead
35.9
32.7
30.1
4308
4 3 ®$ _mv,
-
Mercury
0.25
0.4760
0.462
0.226
Molybdenum
6.94
9.26
7.3
5.19
rA
Nickel
15.6
16.6
16.5
17.9
Selenium
<2.78
5.89
5.09
<0.752
x
Zinc
861
700
665
1,170
Total Phosphorus
19,944
22,736
24,600
30,200
TKN
55,200
60,800
59,500
35,300
Ammonia-Nitroge
3,730
7,410
10,800
15,500
Nitrate and Nitrite
<546
<529
<578
<752
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
.� 2Z31S
Signature of Preparer Date
DENR FORM RSSF (5/2003)

M
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003824 Laboratory: 1) MERITECH, INC.
Facility Name: CITY OF GRAHAM 2) CITY OF GRAHAM (pH only)
NPDES # or NCO021211 3)
WQ#:
WWTP Name:
Residual Analvsis Data
CITY OF GRAHAM
4)
5)
Sample or
Composite Date
3/19/14
5/7/14
7/9/14
10/16/14
Aluminum
8,222
932
8,790
10,200
pH
7.2
7.5
1.2
7.5
Potassium
5,383
5,947
6,360
8,420
P.A.N.
17,852
20,251
20,588
14,442.0
,b
TSS
10,500
13,020
11,940
12,280
Calcium
10,944
11,736
11,100
15,100
Magnesium
4,988
5,157
5,510
-6,720
CD
Sodium
12,055
12,473
13,200
22,300
01
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
"-I/��2�r
Signature of Preparer Date
DENR FORM RSSF-B (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
CITY OF, GRAHAM Total Dry Tons Applied (Annual):
26.342
NCO021211 Cation Exchange Capacity (non 503 only): 43.1
CRISPIAN T. ROUTH
15.2 Acres Permitted:
_ Owner: CITY OF GRAHAM
15.2 Site #: 1 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
Com-
orite
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/1410/16/14
% Solids
1.83
1.83
1 1.83
1.89
1.89
1.89
1.73
1.73
1.73
1.33
1.33
1.33
Arsenic
2.78
2.78
2.78
2.63
2.63
2.63
2.89
2.89
2.89
0.752
0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
3.89
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
431
431
431
502
502
502
Lead
35.9
35.9
1 35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25
0.25
0.25
0.476
0.476
0.476
A462
0.462
0.462
0.226
0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
1 2.78
5.89
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
700
700
665
665
665
1170
1 1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Co
co
o'
0.225
0.211
0.141
0.595
0.348
0.000
0.213
0.000
0.000
0.000
0.000
0.000
Arsenic
0.001
0.001
0.001
0.003
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.008
Cadmium
0.002
0.002
0.001
0.005
0.003
0.000
0.002
0.000
0.000
0.000
0.000
0.000
0.013
Chromiurr
0.040
0.037
0.025
0.105
0.062
0.000
0.033
0.000
0.000
0.000
0.000
0.000
0.301
Copper
0.197
0.185
0.124
0.541
0.317
0.000
0.184
0.000
0.000
0.000
0.000
0.000
1.547
Lead
0.016
0.015
0.010
0.039
0.023
0.000
0.013
0.000
0.000
0.000
0.000
0.000
0.116
Mercury 1
0.000
0.000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.003
0.003
0.002
0.011
0.006
0.000
0.003
0.000
0.000
0.000
0.000
0.000
0.029
Nickel
0.007
0.007
0.004
0.020
0.012
0.000
0.007
0.000
0.000
0.000
0.000
0.000
0.056
Selenium
0.001
0.001
0.001
1 0.007
0.004
0.000
0.002
0.000
0.000
0.000
0.000
0.000
0.016
Zinc
0.387
0.363
. 0.243
0.833
0.487
0.000
0.283
0.000
0.000
0.000
0.000
0.000
2.597
Total
-
Phos-
8.975
8.416
5.624
27.056
15.824
0.000
10.480
0.000
0.000
0.000
0.000
0.000
76.375
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
1 is %LoK01,73115
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 1.733
Owner: CITY OF GRAHAM Operator: CRISPIAN T. ROUTH Cation Exchange Capacity (non 503): 43.1
Site #: 1 Field #: 1 Acres Utilized: 15.2 Acres Permitted: 15.2
o
0
Specify
Totals
Acre
I
%
s
Dry Tons Per
Acre
Residual
(Summarize)
ite
Cond .
,
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
nation
Rate
TKN
Ammo
nia-
Ni-
trogen
. Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 C
p or Crop
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
JAN
44800
2947.4
1.83
0.225
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
8.030
#######
FESCUE
1
FEB
42000
2763.2
1.83
0.211
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
7.529
#######
FESCUE
2
MAR
28000
1842.1
1.83
0.141
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
5.019
#######
FESCUE
3
APR
114800
7552.6
1.89
0.595
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
24.109
#######
FESCUE
4
MAY
67200
4421.1
1.89
0.348
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
14.112
:#######
FESCUE
5
JUN
0
0
1.89
0.000
0.000
#######
FESCUE
6
JUL
44800
2947.4
1.73
0.213
WWTP
N/A
N/A
S.
0.5
30%
59500
10800
578
8.755
#######
FESCUE
7
AUG
0
0
1.73
0.000
0.000
#######
FESCUE
8
SEP
0
0
1.73
0.000
0.000
#######
FESCUE
9
OCT
0
0
1.33
0.000
0.000
#######
FESCUE
#
NOV
0
0
1.33
0.000
0.000
#######
FESCUEl
#
DEC
0
0
1.33
0.000
0
#######
FESCUE
#
TOTALS:
22474
..>:
As
Cd
I Cr
Cu
Pb
Hg
Mo
Ni'
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.008
0.013
0.301
1.547
0.116
0.001
0.029
0.0564
0.016
2.597
76.375
67.554
0
Date
lbs/ac
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 1 2677 1 1338 1 267 15 1 NA 1 374 89 2498 :
2 50
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 t/2nd Cro
p o
P
• 1. certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties/for submitting false information, including the possibility of fines and imprisonment for knowing violations."
6 C���j�,A.� ! • 2 Z 3 /S *Application Method: S - Surface, IN -Injection, INC -Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loadina Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual .Report
Facility Name:
Permit #:
Operator:
Acres Used:
CITY OF GRAHAM Total Dry Tons Applied (Annual): 13.032
NCO021211 Cation Exchange Capacity (non 503 only): 26.4
CRISMAN T. ROUTH Owner: CITY OF GRAHAM
12.4 Acres Permitted: 12.4 Site #: 1 Field #:
Residual Analysis Data (Heavy Metals and Total Phosphorus use mu/kg, % Solids use Raw Percent #):
Sample
Com-
orite
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/14
10/16/14
% Solids
1.83
1.83
1.83
1.89
1.89
1.89
1.73
1.73
1.73
1.33
1.33
1.33
Arsenic
1 2.78
2.78
2.78
2.63
1 2.63
2.63
2.89
1 2.89
2:89
0.752
0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
189
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
431
431
431
502
502
502
Lead
35.9
35.9
35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25
0.25
0.25
0.476
0.476
0.476
0.462'
0.462
0.462
0.226
0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
2.78
5.89
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
700
700
665
665
665
1170.
1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual Heavy 1Vletal Field Loadings (Calculated in lbs/acre):
01
� o
y
o• !0-_
0.000
0.000
0.138
0.481
0.000
0.285
0.147
0.000
0.000
0.000
0.000
0.000
Arsenic
0.000
0.000
0.001
0.003
0.000
0.001
0.001
0.000
0.000
0.000
0.000
0.000
0.006
Cadmium
0.000
0.000
0.001
0.004
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.008
Chromiurr
0.000
0.000
0.024
0.085
0.000
0.050
0.023 -
'0.000
0.000
0.000
0.000
0.000
0.182
Copper
0.000
0.000
0.121
0.438
0.000
0.259
0.127
0.000
0.000
0.000
0.000
0.000
0.945
Lead
0.000
0.000
0.010
0.031
0.000
0.019
0.009
0.000
0.000
0.000
0.000
0.000
0.069
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.000
0.000
0.002
0.009
0.000
0.005
0.002
0.000
0.000
0.000
0.000
0.000
0.018
Nickel
0.000
0.000
0.004
0.016
0.000
0.009
0.005
0.000
0.000
0.000
0.000
0.000
0.035
Selenium
0.000
0.000
0.001
0.006
0.000
0.003
0.001
0.000
0.000
0.000
0.000
0.000
0.011
Zinc
0.000
0.000
0.238
0.673
0.000
0.399
0.196
0.000
0.'000
0.000
0.000
0.000
1.506
Total
Phos-
0.000
0.000
5.505
21.872
0.000
12.960
7.232
0.000
0.000
0.000
0.000
0.000
47.568
horus
1 certlly, unaer penalty of law, tnat tors aocument was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
�� z Z3 /S
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 1.050
Owner: CITY OF GRAHAM Operator: CRISPIAN T. ROUTH Cation Exchange Capacity (non 503): 26.4
Site #: 1 Field #: 2 Acres Utilized: 12.4 - Acres Permitted: 12.4
o
0
� o
S eci
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
i e
Cond.
Dry,
Wet'
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
.Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
Gal.
Cu.Yd.
::
77
Report
Totals
in Gal.
Crop 1
Crop 2
JAN
0
0
1.83
0.000
0
#######
FESCUE
1
FEB
0
0
1.83
0.000
0
#######
FESCUE
2
MAR
22400
1806.5
1.83
0.138
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
4.92187
#######
FESCUE
3
APR
75600
6096.8
1.89
1 0.481
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
19.4614
#######
FESCUE
4
MAY
0
0
1.89
0.000
1
0
#######
FESCUE
5
JUN
44800
3612.9
1.89
0.285
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
11.5327
#######
FESCUE
6
JUL
25200
2032.3
1.73
0.147
WWTP
N/A
N/A
S
0.5
30%
59500
10800
578
6.03678
#######
FESCUE
7
AUG
0
0
1.73
0.000
0
#######
FESCUE
8
SEP
0
0 .
1.73
0.000
0
#######
FESCUE'
9
OCT
0
0
1.33
0.000
1
0
#######
FESCUE
#
NOV
0
0
1.33
0.000
0
#######
FESCUE
#
DEC
0
0
1.33
0.000
0
#######
FESCUEJ
#
TOTALS:
13548
:::::::::::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0.006
0.008
0.182
0.945
0.069
0.001
0.018
0.035
0.011
1.506
47.568
41.953
0
Date
lbs/ac
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
4 26771338 267 15 NA 374
250
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"1 certily, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing, violations."
ef4f' 7i2-3 /S *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: CITY OF GRAHAM Total Dry Tons Applied (Annual): 25.044
Permit #: NCO021211 Cation Exchange Capacity (non 503 only): 70
Operator: CRISPIAN T. ROUT14 Owner: CITY OF GRAHAM
Acres Used: 6.8 Acres Permitted: 6.8 Site #: 1 Field #: 3
Residual Analvsis Data (Heave Metals and Total Phosphorus use mg/kg. % Solids use Raw Percent #):
Sample
or Com-
posite
Date
3/19/14
3/19/14
5/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/14
10/16/14
% Solids
1.83
1.83
1.83
1.89
1.89
1.89
1.73
1.73
1.73
1.33
1 1.33
1.33
Arsenic
2.78
2.78
2.78
2.63
2.63
2.63
2.89
2.89
2.89
0.752
0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
3.89
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
431
431
431
502
502
502
Lead
35.9
35.9
1 35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25
0.25
0.25
0.476
0.476
0.476
1 0.462
0.462
0.462
0.226
0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
1 2.78
2.78
5.89
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
700
700
1 665
665
665
1170
1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual rieavv iwetal viela Loadings malculatecl to ins/acre):
►�
o
0
co -- y
o'
0.597
0.628
0.283
1.201
0.000
0.974
0.000
0.000
0.000
0.000
0.000
0.000
Arsenic
0.003
0.003
0.002
0.006
0.000
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.020
Cadmium
0.005
0.005
0.002
0.009
0.000
0.008
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Chromiurr
0.105
0.110
0.050
0.212
0.000
0.172
0.000
0.000
0.000
0.000
0.000
0.000
0.649
Copper
0.523
0.550
0.248
1.093
0.000
0.886
0.000
0.000
0.000
0.000
0.000
0.000
3.300
Lead
0.043
0.045
0.020
0.079
0.000
0.064
0.000
0.000
0.000
0.000
0.000
0.000
0.251
Mercury
0.000
0.000
0.000
0.001
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
denum
0.008
0.009
0.004
0.022
0.000
0.018
0.000
0.000
0.000
0.000
0.000
0.000
0.061
Nickel
0.019
0.020
0.009
0.040
0.000
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.119
Selenium
0.003
0.003
0.002
0.014
0.000
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Zinc
1.028
1.081
0.487
1.681
0.000
1.364
0.000
0.000
0.000
0.000
0.000
0.000
5.642
Total
Phos-
23.813
25.050
11.288
54.612
0.000
44.290
0.000
0.000
0.000
0.000
0.000
0.000
159.053
horus
l certuy, under penalty of law, tnat tnis document was prepares under my clirection or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines nd imprisonment for knowing violations"
Signaturef Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK_ OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 3.683
Owner: CITY OF GRAHAM
Site #:
Field #:
Operator: CRISPIAN T. ROUTH Cation Exchange Capacity (non 503): 70
Acres Utilized: 6.8
Acres Permitted: 6.8
o y
o
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
i e
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN I
PAN 2
Must Select
Crop I or Crop
p p
2
*
Gal.
Cu.Yd.
::
Report
Totals
in Gal.
Crop 1
Crop 2
JAN
53200
7823.5
1.83
0.597
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
21.3161
#######
FESCUE
1
FEB
56000
8235.3
1.83
0.628
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
22.43795
#######
FESCUE
2
MAR
25200
3705.9
1.83
0.283
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
10.0971
#######
FESCUE
3
APR
103600
15235
1.89
1.201
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
48.6323
#######
FESCUE
4
MAY
1 0
0
1.89
0.000
1
0
#######
FESCUEl
5
JUN
84000
12353
1.89
0.974
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
39.4316
#######
FESCUE
6
JUL
0
0
1.73
0.000
0
#######
FESCUE
7
AUG
0
0
1.73
0.000
0
#######
FESCUE
8
SEP
0
0:
1.73
0.000
0
#######
FESCUE
9
OCT
0
0
1.33
1 0.000
0
#######
FESCUEl
10
NOV
0
0
1.33
0.000
0
#######
FESCUE
11
DEC
0
0
1.33
0.000
0
#######
FESCUEJ
12
TOTALS:
47353
:::::::::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime A
lied
Annuallbs/acre
0.020
0.028
0.649
3.300
0.251
0.003
0.061
0.119
0.034
5.642
159.053
141.915
0
Date
. lbs/ac
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 2677 3338, 267 15 NA 374 89 2498 .................
................................................................................................................................................................::::::::::.. .
250
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified -personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Z• Z/Z3 IS *Application Method: S - Surface, IN - Injection, INC --Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
' Permit #:
? - Operator:
Acres Used:
CITY OF GRAHAM Total Dry Tons Applied (Annual): _
NCO021211 Cation Exchange Capacity (non 503 only):
CRISMAN T. ROUTH Owner: CITY OF GRAHAM
8.8 Acres Permitted: 8.8 Site #: 1 Field #:
16.377
62.9
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
oreCom-
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/14
10/16/14
% Solids
1.83 1
1.83
1.83
1.89
1 1.89
1.89
1.73
1 1.73
1.73
1.33
1 1.33
1.33
Arsenic
2.78
2.78
2.78
2.63
2.63
2.63
2.89
1 2.89
2.89
0.752
0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
3.89
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
431
431
431
502
502
502
Lead
35.9
35.9
35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25
0.25
0.25
0.476
0.476
0.476
0.462
0.462
0.462
0.226
0.226
' 0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
2.78
5.89
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
700
700
665
665
665
1170
1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
4
�C y
+ o
C7
MCD
0
:v
W Y
o
0.000
0.194
0.194
0.201
0.176
0.000
0.390
0.000
0.000
0.424
0.141
0.141
Arsenic
0.000
0.001
0.001
0.0.01
0.001
0.000
0.002
0.000
0.000
0.001
0.000
0.000
0.007
Cadmium
0.000
0.001
0.001
0.002
0.001
0.000
0.003
0.000
0.000
0.004
0.001
0.001
0.016
Chromiurr
0.000
0.034
0.034
00036
0.031
0.000
0.060
0.000
0.000
0.075,
0.625
0.025
0.319
Copper
0.000
0.170
0.170
0.183
0.160
0.000
0.336
0.000
0.000
0.426
0.142
0.142
1.728
Lead
0.000
0.014
0.014
0.013
0.012
0.000
0.023
0.000
0.000
0.037
0.012
0.012
0.138
Mercury
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0.000
0.003
0.003
0.004
0.003
0.000
0.006
0.000
0.000
0.004
0.001
0.001
0.025
denum
Nickel
0.000
0.006
0.006
0.007
0.006
-0.000
0.013
0.000
0,000
0.015
0.005
0.005
1 0.063
Selenium
0.000
0.001
0.001
0.002
0.002
0.000
0.004
0.000
0.000
0.001
0.000
0.000
0.012
Zinc
0.000
0.334
0.334
0.281
0.246
0.000
0.519
0.000
0.000
0.992
0.330
0.330
3.367
Total
Phos-
0.000
7.738
7.738
9.140
8.003
0.000
19.188
0.000
0.000
25.610
8.516
8.516
94.450
horus
-i certuy, under penalty of law, that this aocument was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, .
including the possibility of fimes and imprisonment for knowing violations"
z Z3 �S
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 1.861
Owner: CITY OF GRAHAM Operator: CRISPIAN T. ROUTH Cation Exchange Capacity (non 503)• 629
Site #:
1 Field #: 4 Acres Utilized: 8.8 Acres Permitted: 8.8
o �
o
Specify-
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
*
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
JAN
0
0
1.83
0.000
0.000
#######
FESCUE
1
FEB
22400
2545.5
1.83
0.194
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
6.935
#######
FESCUE
2
MAR
22400
2545.5
1.83
0.194
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
6.935
#######
FESCUE
3
APR
22400
2545.5
1.89
0.201
WWTP
N/A
I N/A
S
0.5
30%
60800
7410
529
8.125
#######
FESCUE
4
MAY
1 19600
2227.3
1.89
0.176
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
7.110
#######
FESCUE
5
JUN
0
0
1.89
0.000
0.000
#######
FESCUE
6
JUL
47600
5409.1
1.73
0.390
WWTP
N/A
N/A
S
0.5
30%
59500
10800
578
16.068
#######
FESCUE
7
AUG
0
0
1.73
0.000
0.000
#######
FESCUEl
8
SEP
0
0
1.73
0.000
0.000
#######
FESCUE
9
OCT
67200
7636.4
1.33
1 0.424
WWTP
N/A
N/A
S
0.5
30%
35300
15500
752
12.233
#######
FESCUE
10
NOV 1
22400
2545.5
1.33
0.141
WWTP
N/A
N/A
S
0.5
30%
35300
15500
752
4.078
#######
FESCUE
11
DEC 1
22400
2545.5
1.33
0.141
WWTP
N/A
N/A
S
0.5
300/c
353001
15500
752
4.078
#######
FESCUE
12
TOTALS:
28000
:::::::::::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0.007 1
0.016
1 0.319
1 1.728
0.138
1 0.001
0.025
1 0.063
0.012
1 3.367
94.450 1
65.562 1
0
Date
lbs/ac
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 2677 1338 267 15 NA 374 89 2-1
250
p
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I ani aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
' 2-Z3 I S *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
CITY OF GRAHAM Total Dry Tons Applied (Annual): 15.766
NCO021211 Cation Exchange Capacity (non 503 only): 1 59.5
CRISMAN T. ROUTH Owner: CITY OF GRAHAM
10.4 Acres Permitted: 10.4 Site #: 1 Field #:
Residual Analvsis Data (Heavv Metals and Total Phosnhorus use mu/ku- % Solids use Raw Percent M!
Sample
or Com-
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
16/16/14
10/16/14
% Solids
1 1.83
1.83
1 1.83
1.89
1.89
1.89
1.73
1.73
1 1.73
1.33
1.33
1.33
Arsenic
2.78
2.78
2.78
2.63
2.63
2.63
2.89
2.89
2.89
0.752
0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
3.89
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
431
431
431
502
502
502
Lead
35.9
35.9
1 35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25 _
0.25
0.25
0.476
0.476
0.476
0.462
0.462
0.462_
0.226
0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6.
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
2.78
5.89
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
700
700
665
665
665
1170
1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22;736
24,600
24,600
24,600
30200
30200
30200
Annual itieavv lvletal riela Loaclin2s (Ualculatecl in Ibs/acre):
►C H
-o
< t7
CD
o
0.000
0.308
0.205
0.446
0.000
0.382
0.175
0.000
0.000
0.000
0.000
0.000
Arsenic
0.000
0.002
0.001
0.002
0.000
0.002
0.001
0.000
0.000
0.000
0.000
0.000
0.008
Cadmium
0.000
0.002
0.002
0.003
0.000
0.003
0.001
0.000
0.000
0.000
0.000-
0.000
0.012
Chromiurr
0.000
0.054
0.036
0.079
0.000
0.068
0.027
0.000
0.000
0.000
0.000
0.000
0.264
Copper
0.000
0.270
0.180
0.406
0.000
0.348
0.151
0.000
0.000
0.000
0.000
0.000
1.354
Lead
0.000
0.022
0.015
0.029
0.000
0.025
0.011
0.000
0.000
0.000
.0.000
0.000
0.102
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.000
0.004
0.003
0.008
0.000
0.007
0.003
0.000
0.000
0.000
0.000
0.000
0.025
Nickel
0.000
0.010
0.006
0.015
0:000
0.013
0.006
0.000
0.000
0.000
0.000
0.000
0.049
Selenium
0.000
0.002
0.001
0.005
0.000
0.004
0.002
0.000
0.000
0.000
0.000
0.000
0.014
Zinc
0.000
0.530
0.353
0.624
0.000
0.535
0.233
0.000
0.000
0.000
0.000
0.000
2.275
Total
Phos-
0.000
12.286
8.177
20.281
0.000
17.370
8.610
0.000
0.000
0.000
0.000
0.000
66.723
horus
-1 ceruly, unuer penalty or law, inar tms aocument was prepares under my airection or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fitand imprisonment for knowing violations"
?i/Z3 !S
Signature of Land Applier Date
* See bottom of FSF Form for Helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 1.516
Owner: CITY OF GRAHAM
Site #:
Field #:
Operator:
5
CRISPIAN T. ROUTH Cation Exchange Capacity (non 503): 59.5
Acres Utilized: 10.4 Acres Permitted: 10.4
o ZV
r.
r oPer
�
>:
Specify
Totals
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
i e
Cond.
Dry,
Wet,
Inches
Precip.
Past24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN I
PAN 2
Must Select
Crop 1 or Crop
p p
2
Gal.
Crop 1
Crop 2
JAN
0
0
1.83
0.000
0.000
#######
FESCUE
1
FEB
42000
4038.5
1.83
0.308
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
11.003
#######
FESCUE
2
MAR
28000
2692.3
1.83
0.205
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
7.335
#######
FESCUE
3,
APR
58800
5653.8
1.89
0.446
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
18.048
#######
FESCUE
4
MAY
0
0
1.89
0.000 _
0.000
#######
FESCUE
5
JUN
50400
4846.2
1.89
0.382
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
15.469
#######
FESCUE
6
JUL
25200
2423.1
1.73
0.175
WWTP
N/A
N/A
S
0.5
30%
59500
10800
578
7.198
#######
FESCUE
7
AUG
0
0
1.73
0.000
0.000
#######
FESCUE
8
SEP
0
0
1.73
0.000
0.000
#######
FESCUE
9
OCT
0
0
1.33
0.000
0.000
#######
FESCUE
10
NOV
0
0
1.33
0.000
0.000
#######
FESCUE
11
DEC
0
0
1.33
0.000
0.000
#######
FESCUE
12
TOTALS:
19654
:::::::::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0.008
0.012
0.264
1.354
0.102
0.001
0.025
0.049
0.014
2.275
66.723
59.053
0
Date
lbs/ac
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 2677 1338 267 15 NA 374 89 2498
� 50
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
15 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: CITY_ OF GRAHAM Total Dry Tons Applied (Annual):
Permit #: NC0021211. Cation Exchange Capacity (non 503 only):
Operator: CRISMAN T. ROUTH
Acres Used: 12 Acres Permitted:
18.324
62.6
Owner: CITY OF GRAHAM
12 Site #: 1 Field #: 6
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft
Sample
or Com-
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/14
10/16/14
% Solids
1 1.83
1.83
1.83
1.89
1.89
1.89
1.73
1.73
1 1.73
1.33
1.33
1.33
Arsenic
2.78
2.78
1 2.78
2.63
2.63
1 2.63
2.89
2.89
2.89
0.752
1 0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
3.89
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
431
431
431
502
502
502
Lead
1 35.9
35.9
35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25
0.25
1 0.25
0.476
0.476
0.476
0.462
0.462
0.462
0.226
1 0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
2.78
5.89
5.89
1 5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
1 861
700
700
700
665
665
665
1170
1170
1170
Total
Phos-
horus
'
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�c y
o
rn y
A�
o
0.000
0.267
0.142
0.000
0.000
0.294
0.488
0.000
0.000
0.336
0.000
0.000
Arsenic
0.000
0.001
0.001
0.000
0.000
0.002
0.003
0.000
0.000
0.001
0.000
0.000
0.007
Cadmium
0.000
0.002
0.001
0.000
0.000
0.002
0.004
0.000
0.000
0.003
0.000
0.000
0.012
Chromiury
0.000
0.047
0.025
0.000
0.000
0.052
0.076
0.000
0.000
0.059
0.000
0.000
0.259
Copper
0.000.
0.234
0.124
0.000
0.000
0.268
0.421
0.000
0.000
0.337
0.000
0.000
1.384
Lead
0.000
0.019
0.010
0.000
0.000
0.019
0.029
0.000
0.000 _
0.029
0.000
0.000
0.107
Mercury
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
denum
0.000
0.004
0.002
0.000
0.000
0.005
0.007
0.000
0.000
0.003
0.000
0.000
0.022
Nickel
0.000
0.008
0.004
0.000
0.000
0.010
0.016
0.000
0.000
0.012
0.000
0.000
0.051
Selenium
0.000
0.001
0.001
0.000
0.000
0.003
0.005
0.000
0.000
0.001
0.000
0.000
0.011
Zinc
0.000
0.460
0.245
0.000
0.000
0.412
0.649
0.000
0.000
0.786
0.000
0.000
2.551
Total
Phos-
0.000
10.650
5.664
0.000
0.000
13.369
24.010
0.000
0.000
20.294
0.000
0.000
73.987
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
x See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 1.528
Owner: CITY OF GRAHAM Operator: CRISPIAN T. ROUTH Cation Exchange Capacity (non 503): 62.6
Site #: 1 Field #: 6 Acres Utilized: 12 Acres Permitted: 12
o
Y o
Q
S eci
Totals
Per
Acre
%
Solid
s
Acre
Residual
Sources
(Summarize)
ite
Cond.
Dry,
Wet,
Moist
Inches .Must
Past.24
Hrs.
A li
PP
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Select
P orro p
Crop 1 Ccation
2
Gal.
:<
Report
Totals
in Gal.
Crop 1
Crop 2
JAN
0
0
1.83
0.000
0.000
#######
FESCUE
1
FEB
42000
3500
1.83
0.267
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
9.536
#######
FESCUE
2
MAR
22400
1866.7
1.83
0.142
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
5.086
#######
FESCUE
3
APR
0
0
1.89
0.000
0.000
#######
FESCUE
4
MAY
0
0
1.89
0.000
0.000
#######
FESCUE
5
JUN
44800
3733.3
1.89
0.294
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
11.917
#######
FESCUE
6
JUL
81200
6766.7
1.73
0.488
WWTP
N/A
N/A'
S
0.5
30%
59500
10800
578
20.100
#######
FESCUE
7
AUG
0
0
1.73
0.000
0.000
#######
FESCUE
8
SEP
0
0
1.73
0.000
0.000
#######
FESCUE
9
OCT
72800
6066.7
1.33
0.336
WWTP
N/A
N/A
S
0.5
30%
35300
15500
752
9.718
#######
FESCUE
10
NOV
0
0
1 1.33
0.000
0.000
#######
FESCUE
11
DEC
0
0
1.33
0.000
0.000 1
#######
FESCUE
12
TOTALS:
21933
::::::::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.007
0.012
0.259
1.384
0.107
0.001
0.022
0.051
0.011
2.551
74.0 1
56.358
0
Date
lbs/ac
:::"
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2009 REPORT OF ANNUAL -SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 2677 1338 267 15 NA 374 89 2498 >:
.......................................
250
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
4?e Z 2.3 5. *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Ini ection/Inco rpo ration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column 9 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: CITY OF GRAHAM Total Dry Tons Applied (Annual):
Permit #: NC0021211 Cation Exchange Capacity (non 503 only):
Operator: CRISMAN T. ROUTH Owner:
Acres Used: 8.8 Acres Permitted: 8.8
Site #:
CITY OF GRAHAM
18.577
47.5
Field #: 7
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
Com-
orite
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/14
10/16/14
% Solids
1.83
1.83
1.83
1.89
1.89
1..89
1.73
1 1.73
1.73
1.33
1 1.33
1.33
Arsenic
2.78
1 2.78
2.78
2.63
2.63
2.63
2.89
2.89
2.89
0.752
0.752
0.752
Cadmium
3.78
3.78,
3.78
3.89
3.89
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
1 88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
431
431
431
502
502
502
Lead
35.9
35.9
1 35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
1 43.8
43.8
Mercury
0.25
0.25
0.25
0.476
0.476
0.476
0.462
1 0.462
0.462
0.226
0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
2.78
5.89
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
700
700
665
665
665
1170
1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
0
+ o
a�
y
CD d_
y
o
0.000
0.461
0.413
0.000
0.000
0.752
0.000
0.344
0.000
0.000
0.000
0.141
Arsenic
0.000
0.003
0.002
0.000
0.000
0.004
0.000
0.002
0.000
0.000
0.000
0.000
0.011
Cadmium
0.000
0.003
0.003
0.000
0.000
0.006
0.000
0.003
0.000
0.000
0.000
0.001
0.016
Chromiurr
0.000
0.081
0.073
0.000
0.000
0.133
0.000
0.053
0.000
0.000
0.000
0.025
0.365
Copper
0.000
0.404
1 0.362
0.000
0.000
0.684
0.000
0.297
0.000
0.000
0.000
0.142
1.888
Lead
0.000
0.033
0.030
0.000
0.000
0.049
0.000
0.021
0.000
0.000
0.000
0.012
0.145
Mercury
0.000
0.000
0.000
0.000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.000
0.006
0.006
0.000
0.000
0.014
0.000
0.005
0.000
0.000
0.000
0.001
0.033
Nickel
0.000
0.014
0.013
0.000
0.000
0.025
0.000
0.011
0.000
0.000
0.000
0.005
0.069
Selenium
0.000
0.003
0.002
0.000
0.000
0.009
0.000
0.004
0.000
0.000
0.000
0.000
0.017
Zinc
0.000
0.794
0.711
0.000
0.000
1.053
0.000
0.458
0.000
0.000
0.000
0.330
3.345
Total
Phos-
0.000
18.388
16.474
0.000
0:000
34.195
0.000
16.925
0.000
0.000
0.000
8.516
94.498
_horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and im risonment for knowing violations"
21Z3 /S
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 2.112
Owner: CITY OF GRAHAM Operator: CRISPIAN T. ROUTH Cation Exchange Capacity (non 503): 47.5
Site #:
1 Field #: 7 Acres Utilized: 8.8 Acres Permitted: 8.8
o
o
Q
S eci
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
ma-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
Gal.
Cu.Yd.
Report
Totals
:: in Gal.
Crop 1
Crop 2
JAN
0
0
1.83
0.000
0.000
#######
FESCUE
1
FEB
53200
6045.5
1.83
0.461
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
16.471
#######
FESCUE
2
MAR
47600
5409.1
1.83
0.413
WWTP
N/A
N/A
S
0.5
30%
55200
3730
546
14.738
#######
FESCUE
3
APR
0
0
1.89
0.000
0.000
#######
FESCUE
4
MAY
0
0
1.89
0.000
0.000
#######
FESCUE
5
JUN
84000
9545.5
1.89
0.752
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
30.470
#######
FESCUE
6
JUL
1 0
0
1.73
0.000
0.000
#######
FESCUE
7
AUG
42000
4772.7
1.73
0.344
WWTP
N/A
N/A
S
0.5
30%
59500
10800
578
14.177
#######
FESCUE
8
SEP
0
0
1.73
0.000
1
0.000
#######
FESCUE
9
OCT
0
0
1.33
0.000
0.000
#######
FESCUE
10
NOV
0
0
1.33
0.000
0.000
#######
FESCUE
11
DEC
1 22400
1 2545.5
1.33
0.141
WWTP
N/A
N/A
S
0.5
30%
0.000
#######
FESCUE
12
TOTALS:
28318
::::::::
As
Cd
I Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annual lbs/acre
0.011
0.016
1 0.365
1.888
0.145
0.002
0.033
0.069
1 0.017
3.345
94.50
1 75.856
0
Date
lbs/ac
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 2677 1338 267 15 NA 374 89 2498......................................
250
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit Ist/2nd Crop
PFil
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting alse information, including the possibility of fines and imprisonment for knowing violations."
Z7 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5. Iniection/Incori)oration -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: CITY OF GRAHAM Total Dry Tons Applied (Annual): .14.706
Permit #: NCO021211 Cation Exchange Capacity (non 503 only): 1 32.1
Operator:
Acres Used:
CRISMAN T. ROUTH Owner: CITY_ OF GRAHAM
Acres Permitted: 6 Site #: 1 Field #: 8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/14
10/16/14
% Solids
1 1.83
1.83
1 1.83
1.89
1.89
1 1.89
1.73
1.73
1 1.73
1.33
1.33
133
Arsenic
2.78
2.78
2.78
2.63
2.63
2.63
2.89
2.89
2.89
0.752
0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
3.89
3.89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4 _
77.5
77.5
77.5
88
88
88
Copper
438
438
438
455
455
455
1 431
431
431
1 502
502
502
Lead
35.9
35.9
1 35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25
0.25
0.25
0.476
0.476
0.476
0.462
0.462
0.462
0.226
0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
2.78
5.89
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
'700
700
665
665
665
1170
1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
�C
�+ o
0
C7
CD y
o !C_1
0.000
0.000
0.000
0.294
0.736
0.000
0.269
0.505
0.000
0.078
0.569
0.000
Arsenic
0.000
0.000
0.000
0.002
0.004
0.000
0.002
0.003
0.000
0.000
0.001
0.000
0.011
Cadmium
0.000
0.000
0.000
0.002
0.006
0.000
0.002
0.004
0.000
0.001
0.005
0.000
0.020
Chromiurr
0.000
0.000
0.000
0.052
0.130
0.000
0.042
0.078
0.000
0.014
0.100
0.000
0.416
Copper
0.000
0.000
0.000
0.268
0.670
0.000
0.232
0.435
0.000
0.078
0.571
0.000
2.254
Lead
' 0.000
0.000
0.000
0.019
0.048
0.000
0.016
0.030
0.000
0.007
0.050
0.000
0.171
Mercury
0.000
0.000
0:000
0.000
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.000
0.000
0.000
0.005
0.014
0.000
0.004
0.007
0.000
0.001
0.006
0.000
0.037
Nickel
0.000
0.000
0.000
0.010
0.024
1 0.000
0.009
0.017
0.000
0.003
0.'020
0.000
0.083
Selenium
0.000
0.000
0.000
0.003
0.009
0.000
0.003
0.005
0.000 1
0.000
0.001
0.000
0.021
Zinc
0.000
0.000
0.000
0.412
1.030
0.000
0.358
0.672
0.000
0.183
1.331
0.000
3.985
Total
Phos-
0.000
0.000
0.000
13.369
33.467
0.000
13.235
24.846
0.000
4.711
34.368
0.000
123.996
horus
"1 certily, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fin and imprisonment for knowing violations"
Z Z3 (S
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: CITY OF GRAHAM WWTP Permit #: WQ0003824 Annual Dry Tons Applied: 2A51
Owner: CITY OF GRAHAM Operator: CRISPIAN T. ROUTH Cation Exchange Capacity (non 503): 32.1
Site #: 1 Field #: 8 Acres Utilized: 6 Acres Permitted: 6.0
o
o
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
1 e
Cond.
Dry,
Wet,
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 Crop
p or p
2
Gal.
Cu.Yd.
Report
Totals
F1 in Gal.
Crop 1
Crop 2
JAN
0
0
1.83
0.000
0.000
#######
FESCUE
1
FEB
0
0
1.83
0.000
0.000
#######
FESCUE
2
MAR
0
0
1.83
0.000
0.000
#######
FESCUE
3
APR
22400
3733.3
1.89
0.294
WWTP
N/A
N/A
S
0.5
30%
60800
7410
529
11.917
#######
FESCUE
4
MAY
1 56000
9333.3
1.89
0.736
WWTP
N/A
N/A
S
0.5
30%
60800
1 7410
529
29.793
#######
FESCUE
5
JUN
0
0
1.89
0.000
0.000
#######
FESCUE
6
JUL
22400
3733.3
1.73'
0.269
WWTP
N/A
N/A
S
0.5
30%
59500
10800
578
11.090
#######
FESCUE
7
AUG
42000
7000
1.73
0.505
WWTP
N/A
N/A
S
0.5
30%
59500
10800
578
20.793
1 #######
FESCUE
8
SEP
0
0
1.73
1 0.000
0.000
#######
FESCUE
19
OCT
1 8400
1400
1.33
0.078
WWTP
N/A
N/A
S
0.5
30%
35300
15500
752
2.243
#######
FESCUE
10
NOV
61600
10267
1.33
0.569
WWTP
N/A
N/A
S
0.5
30%
35300
15500
752
16.447
#######
FESCUE
11
DEC
0
0
1.33
0.000
1
0.000
#######
FESCUE
12
TOTALS:
35467
:::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.011
0.020
0.416
2.254
0.171
0.002
0.037
0.083
0.021
3.985
124.00
0
Date
lbs/ac
Current Cumulative lbs/ac
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
:.:.......... ::::::
SEE 2009 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 2677 1338 267 15 NA 374 89 2498 ......................
250
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penaltiesforsu mittin false information, including the possibility of fines and imprisonment for'knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorvoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
1
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: CITY OF GRAHAM Total Dry Tons Applied (Annual): 6.984
Permit #: NCO021211 Cation Exchange Capacity (non 503 only): 37.8
Operator: CRISMAN T. ROUTH Owner: CITY OF GRAHAM
Acres Used: 9 Acres Permitted: 9 Site #: 1 Field #: 10
Residual Analvsis Data (Heavv Metals and Total Phosphorus use mg/kg. %► Solids use Raw Percent #):
Sample
or Com'-
posite
Date
3/19/14
3/19/14
3/19/14
5/7/14
5/7/14
5/7/14
7/9/14
7/9/14
7/9/14
10/16/14
10/16/14
10/16/14
% Solids
1.83
1.83
1 1.83
1.89
1.89
1 1.89
1.73
1.73
1.73
1.33
1.33
1.33
Arsenic
2.78
2.78
2.78
2.63
2.63
2.63
2.89
2.89
2.89
0.752
0.752
0.752
Cadmium
3.78
3.78
3.78
3.89
3.89
3:89
3.7
3.7
3.7
4.81
4.81
4.81
Chromium
87.8
87.8
87.8
88.4
88.4
88.4
77.5
77.5
77.5
88
88
88
Copper
1 438
438
438
455
455
455
431
431
1 431
502
502
1 502
Lead
35.9
35.9
35.9
32.7
32.7
32.7
30.1
30.1
30.1
43.8
43.8
43.8
Mercury
0.25
0.25
0.25
0.476
0.476
0.476
0.462
0.462
0.462
0.226
0.226
0.226
Molyb-
denum
6.94
6.94
6.94
9.26
9.26
9.26
7.28
7.28
7.28
5.19
5.19
5.19
Nickel
15.6
15.6
15.6
16.6
16.6
16.6
16.5
16.5
16.5
17.9
17.9
17.9
Selenium
2.78
2.78
2.78
5.89 '
5.89
5.89
5.09
5.09
5.09
0.752
0.752
0.752
Zinc
861
861
861
700
700
700
665
665
665
1170
1170
1170
Total
Phos-
horus
19944
19944
19944
22,736
22,736
22,736
24,600
24,600
24,600
30200
30200
30200
Annual neavv Ivietal tielcl Loaclin2s (Ualculatetl in lbs/acre):
1-M0111
M1111111100111
limit
1 ell
M
1 111
1 111
1 111
1 111
1 111
1 101
1 111
1 111
1111
1 11
1 111
1 111
1 11
1 111
1 111
KIT, el
1 111
on 037111
111
1 111
1 111
1 111
1 11
1 11
1 111
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1 •
1 111
•••
WIT, Me
1111
I ell
1 111
1 111
1 111
1 111
1 111
ffTITI1
1 1:
1 111
1 •
1 111
1 111
1 111I
1 Ile
1 111
1 I11
1 ell
1 111
1 111
1 1 1
1 1 :
1 111
1 1•:
1111
1 111
1 ell
MITI I
I M eel
1 III
1 III
1 111
1 III
1 111
1 111
1 111
1 111
.-• •
1 111
1 111
1 111
1 111
1 ell
1 III
1 111
1 111
1 lee
1 11.
III
1 III
1 11:
1 111
1 III
1 111
1 III
1 ell
1 111
1 111
MITI M,
1 I11
1 1 1
1 11
1 111
1 1
WIT, M,
1 111
IIII
1 111
loll
IIII
1 111
1 111
1 111
1 11
IIII
IIII
III
®
1 111
MITI M,
1 111
1 Ill
1 111
1 111
1 III
1 ell
1 III
®
1 �:�
1 III
IIII
1 eel
1 111
1 111
1 111
IIII
1 Ill
1 111
1 111
� .:
1
1 111
�.: 1
I ceruly, unuer penalty of iaw, inat tnis aocument was preparea under my alrectlon or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fi ies and imprisonment for knowing violations"
�5
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form

r- - ,
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
Owner:
Site #:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
CITY OF GRAHAM WWTP
CITY OF GRAHAM
Field #:
Operator:
10
Permit #: WQ0003824
CRISPIAN T. ROUTH
Acres Utilized: 9
Annual Dry Tons Applied: 0.776
Cation Exchange Capacity (non 503): 37.8
Acres Permitted: 9.0
o �
0
o
Q
::.
Specif7
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
*
Gal.
Cu.Yd.
>
Report
Totals
in Gal.
Crop 1
Crop 2
JAN
0
0
1.83
0.000
0.000
#######
FESCUE
1
FEB
0
0
1.83
0.000
0.000
#######
FESCUE
2
MAR
0
0
1.83
0.000
0.000
#######
FESCUE
3
APR
0
0
1.89
0.000
0.000
#######
FESCUE
4
MAY
0
0
1.89
0.000
0.000
#######
FESCUE
5
JUN
0
0
1.89
0.000
0.000
#######
FESCUE
6
JUL
0
0
1.73
0.000
0.000
#######
FESCUE
7
AUG
0
0
1.73
0.000
0.000
#######
FESCUE
8
SEP
0
0
1.73
0.000
0.000
#######
FESCUE
9
OCT
92400
10267
1.33
0.569
WWTP
N/A
N/A
S
0.5
30%
35300
15500
1 752
16.447
#######
FESCUE
10
NOV
33600
3733.3
1.33
0.207
WWTP
N/A
N/A
S
0.5
30%
35300
15500
752
5.981
#######
FESCUE
11
DEC
0
0
1.33
0.000
0.000
#######
FESCUE
12
TOTALS:
14000
::::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
iplied
Annual lbs/acre
0.001
0.007
1 0.137 1
0.779
0.068
0.000 1
0.008 1
0.028 1
0.001 1
1.816
46.87 1
22.427 1
0
Date
lbs/ac
Current Cumulative lbs/ac
SEE 2008 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
SEE 2008 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
36 34 1 2677 1 1338 1 267 15 NA 1 374 89 1 24 88
250
p.
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for s=ittingIseinformation, including the possibility of fines and imprisonment for knowing violations."
Application Method: S -Surface, IN -Injection, INC -Incorporation
Signature of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.

2014 REPORT OF ANNUAL SLUDGE APPLIED TO FARM FROM WWTP AND WTP
GALLONS
WET
DRY TONS
DRY TONS
FIELD
SOURCE
ACRES
APPLIED PER ACRE
PER ACRE
FIELD
PAN
P
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
1
12/31/2013
METALS DATA
.
. . .
0.567
2.118
8.881
93.411
39.331
0.090
1.349
8.536
0.665
153.607
1
wwtp
422,800
27816
1.733
26.342
67.554.
76.375
0.008
0.013
0.301
1.547
0.116
0.001
0.029
0.056
0.016
.2.597
1
wtp
0
0
0.000
.0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
TOTALS
15.2
422800
27816
1.733
26.342
67.554
76.375
0.575
2.131
9.182
94.958
39.447
0.091
1.378
8.592
0.681
156.204
2/31/2013
METALS DATA
.....
_ ....
..
...
0.439
1.930
7.806
81.041
38.772
0.059
1.297
7.217
0.485
136.894
2
wwtp
369,600
29806
1.050
13.032
41.953
47.568
0.006
0.008
0.182
0.945
0.069
0.001
0.018
0.035
0.011
1.506
2
wtp
0
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2
TOTALS
12.4
369600
29806
1.050
13.020
41.953
47.568
0.445
1.938
7.988
81.986
' 38.841
0.060
1.315
7.252
0.496
138.400
3 ..
12/31/201 3
METALS DATA
_
.
1.503
3.450
24.172
190.003.
86.445
0.209
..
3.913
...
17.300
1.823
315.217
3
wwtp
420,000
61765
3.683
.25.044
141.915'
159.053
0.020
0.028
0.649
3.300
0.251
0.003
0.061
0.119
0.034
5.642
3
wtp
0
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3
TOTALS
6.8
420000
61765
3.683
26.044
141.915
159.053
1.523
3.478
24.821
193.303
86.696
0.212
3.974
17.419
1.857
320.859
12/31/2013
METALS DATA
0.787
2.305
12.563
101.638
38.874
0.120
2.077
10.829
0.917
175.640
4
wwtp
386,400
43909
1.861
16.377
65.562
94.450
0.007
0.016
0.319
1.728
0.138
0.001
0.025
0.063
0.012
3.367
4
wtp
0
0
4.891
43.041
39.000
9.980
0.039
0.020
0.342
0.372
0.215
0.004
0.049
0.460
0.049
0.646
4
TOTALS
8.8
386400
43909
6.752
59.418
104.562
104.430
0.833
2.341
13.224
103.738
39.227
0.125
2.151
11.352
0.978
179.653
5•.•.•
12131/2013
METALS
A S DATA
. . . . .
'
••1.057
2.253
15.832
105.185
.53.309
0.1.1.3
•2.259
9.5 1 �""• 8
•0.878
168.800
5
wwtp
215,600
20731
1.516.
15.766'
59.053
66.723
0.008
0.012
0.264
1.354
0.102
0.001
0.025
0.049
0.014
2.275
5
wtp
0
0
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5
TOTALS
10.4
215600
20731
1.516
15.766
69.053
66.723
1.065
2:265
16.096
106.539
53.411
0.114
2.284
9.630
0.892
171.075
_ 5
12/31/2013
METALS DATA
,....
...
.,
..
0.565 '
...• 2.1 .4....
8
8.319
2.....
101.15
4" . 74
6 8
0 092
.1.707.••
.•11•.64•�
6
0.727
173.213
6
wwtp
414,400
34533
1.528
18.324
56.358
74.000
0.007
0.012
0.259
1.384
0.107
0.001
0.022
0.051
0.011
2.551
6
wtp
0
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6
TOTALS
12
414400
34533
1.528
18.336
56.358
74.000
0.572
2.196
8.578
102.536
46.981
0.093
1.729
11.697
0.738
175.764
7...
12/31/2013
METAL D• •
S DATA
0.992
3.131
17.792
125.427
58.129
.....
0.118
2.806
13.193
1.042
206.927
7
wwtp
313,600
35636
2.112
...... 18.577
75.856
94.500
0.011
0.016
0.365
1.888
0.145
0.002
0.033
0.069
0.017
3.345
7
wtp
0
0
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7
TOTALS
8.8
313600
35636
2.112
18.586
75.856
94.500
1.003
3.147
18.157
127.315
58.274
0.120
2.839
13.262
1.059
210.272
8....
12/3112 013
METALS DATA
................................................................•.......•._
0.711 ........
.....2:::;:;
0.375
11. 318
5.530
1:7;;.;.
053
7;:;;.
••0.55
1.853•4.11••
5
0.600
38.744
8
wwtp
232,400
38733
2.451
14.706
13.000
124.000
0.011
0.020
0.416
2.254
0.171
0.002
0.037
0.083
0.021
3.985
8
wtp
136,400
22733
1.981
11.886
33.000
4.360
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8
TOTALS
6.0
368800
61467
4.432
26.592
46900
128.360
0.722
0.395
11.734
27.784
10.708
0.577
1.890
4.198
0.621
42.729
.....................
.................................................................................................
10
12/ 31/2013
METALS DATA
.'�.� '� � �."'
.'�." .�.'.
o.. ...
.. ..............
.......
0.669
0.288
15.223
27.407
13.733
0.074
2.856
4.654
0.659
40.894
10
wwtp
184,800
20533
0.776
6.984
22.427
46.870
0.001
0.007
0.137
0.779
0.068
0.000
0.008
0.028
0.001
1.816
10
wtp
111,600
12400
5.707
9.729
18.000
11.640
0.046
0.023
0.400
0.434
0.251
0.005
0.057
0.537
0.057
0.753
10
TOTALS
9.0
296400
32933
6.483
58.347
40.427
58.510
"F" "
0.716
0.318
15.760
28.620
14.052
"
0.079
" "1s
2.921
..
5.219
.
0.717
43.463
Permitted
C. P. L. R.
from NCDENR
Form F S
3s
3a
2677
1338
267
NA
374
8 9
2 498
Signature of Land Applier Date

eritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 4/1/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 PO#: 2014000785
Graham, NC 27253 Date Sample Rcvd: 3/19/2014
Meritech Work Order # 0319.14145 Sample: Sludge Storage Grab 3/19/14
Parameters Results Analysis Date Reporting rting limit Method
% Total Solids
1.83 %
3/20/14
0-100 %
SM 2540B
Total Suspended Solids
10,500 mg/L
3/20/14
2.5 mg/L
SM 2540 D
Ammonia, Nitrogen
3,730 mg/kg
3/24/14
10 mg/kg
EPA 350.1.
TKN
55,200 mg/kg
3/31/14
20 mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
< 546 mg/kg
3/19/14
546 mg/kg
EPA 353.2
Nitrogen, total
55,200 mg/kg
3/31/14
20 mg/kg
EPA 353.2
Aluminum, total
8,222 mg/kg
3/24/14
2.50 mg/kg
EPA 200.7
Arsenic, total
< 2.78 mg/kg
3/24/14
2.78 mg/kg
EPA 200.7
Cadmium, total
3.78 mg/kg
3/24/14
0.200 mg/kg
EPA 200.7
Calcium, total
10,944 mg/kg
3/24/14
10.0 mg/kg
EPA 200.7
Chromium, total
87.8 mg/kg
3/24/14
0.250 mg/kg
EPA 200.7
Copper, total
438 mg/kg
3/24/14
1.00 mg/kg
EPA 200.7
Lead, total
35.9 mg/kg
3/24/14
0.500 mg/kg
EPA 200.7
Magnesium, total
4,988 mg/kg
3/24/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.25 mg/kg
3/25/14
0.10 mg/kg
EPA 245.1
Molybdenum, total
6.94 mg/kg
3/24/14
0.500 mg/kg
EPA 200.7
Nickel, total
15.6 mg/kg
3/24/14
0.500 mg/kg
EPA 200.7
Phosphorus, total
19,944 mg/kg
3/24/14
2.00 mg/kg
EPA 200.7
Potassium, total
5,383 mg/kg
3/24/14
20.0 mg/kg
EPA 200.7
Selenium, total
< 2.78 mg/kg
3/24/14
2,78 mg/kg
EPA 200.7
Sodium, total
12,055 mg/kg
3/24/14
20.0. mg/kg
EPA 200.7
Zinc, total
861 mg/kg
3/24/14
0.500 mg/kg
EPA 200.7
�J
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
Client: of Cvr�
MERITECH9
' ENVIRONMENTAL LABORATORIES Address: �� `��0✓w�
<..
P A Division of Water Technology and Controls, Inc.
:} Phone: [phone] a
642 Tamco Rd. Fax: [phone]
Reidsville, NC 27320 Email: [e-mail] t'{ �
Web Site: vrvimmeritech-labs.com Attention: ((}}
Sample Sampling Dates & Times Person Takin Sample Si nature : �hX -e— G11.4
Location/ID # START END Comp? #oi Tests Required
Date Time Date Time Grab? Conls.
NPDES#
Phone: a56 20
Fax: ( -5 j.3 - fio .L
Email:
Project #
P o. # O y ba© -7,95
-Turn Around Time"
'RUSH work must have prior approval
-. -
Sid (10 d3 - 5�Day 24 _48 Hr
-t
Required
Method
Llaab. Use
Only
200.8 / 200.7
PH OK?
C120K?
for« 19 a09 13 o l'z,�,��:�b�,s�� �i �3
NI (N A-s. a.
1. Cam._
1"Dechlorination (<0.5 ppin) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation.`
Compositor # —
Jug #
Comments:
Method of Shipment:
UPS
Are these msulls r regulatorypurposes?
YES NO ❑
Report results in
mg/L ❑ mg/Kg
On Ice?
'
t
Temperature On ReceiptIJ t
Fed Ex��
❑ and Delivery
' Other
RLOquished by
D to Time
Receive
Date Time
Relinquis Date Time / f�j
Received by
Date Time
c
Relinquished 4
Date Time
R ed at-la'by ,
11}, "
Date j Time
� i �., j � r

Date:
Grab Sample
Collected By:
Time Collected: �� % "i 2, {\�1
S TE - -- - _R I_ pH : 0+0 10 (Ai s)
CERTIFICATION NO. 240 U DO SM 4500-0 G-2001 (Aqueous)
TEMPERATURE, D.O., pH, Cl2 TEMP. SM 2550 B-2000 (Aqueous)
TOTAL RESIDUAL CHLORINE SM 4500 CI G-2000 (Aqueous)
TEMPERATURE
GRAB
SAMPLE
TEMP.
READING
TIME OF
READING
READ
BY
RESULTS
REPORTED ° C
rDUP
Relative Absolute % Difference (Effluent)
2 ( —1�'\: N- )
+ X100= %
i
PH
SAMPLE
pH
READING
TIME OF
READING
READ
BY
REPORTED
in Std. Units.
EFF
EFF DUP
-7 . �L
Relative Absolute % Difference (Effluent)
+ �� X 100 = _%
L1_"
D.O.
TIME OF
READ
RESULTS
SAMPLE
READING
READING
BY
REPORTED mg/L
EFF
EFF DUP
U
DISSOLVED OXYGEN
TIME DO METER CALIBRATED BY
SLOPE DO READING AT CALIBRATION mglL
Relative Absolute % Differen a Effluent
2( - i )
+ x 100 = %
LOW LEVEL CHLORINE RESIDUAL
LL CLz RES. AVERAGE BLANK Mn RESULTS
SAMPLE ANALYST ANALYSIS READING EFFLUENT CORRECTION CORRECTION REPORTED
TIME ppb ppb ppb ppb
EFF \
EFF DUPL. i
Results Reported Average Effluent Minus Blank Correction Minus Mn Correction
CURVE DATE: CORR.COEFF:
DAILY CHLORINE RESIQUAL STANDARDS
QC RESULT DATE RUN TIME ANALYZED ANALYST
CHLORINE QC VALUE IS
ACCEPTABLE RANGE IS TO _
HACH LOW RANGE CHLORINE STD. I
OPENED EXP. DATE `\ z LOT#
Relative Absolute % Difference (Effluent)
2( - /)
+ x� %

Meritech, Inc.
n. Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Report Date: 5/21/2014
NPDES#: WQ0003824
P.O.#: 2014001004
Date Sample Rcvd: 5/7/2014
Meritech Work Order # 05071436 Sample: Sludge Storage Grab
5/7/14•
Parameters
Result
Analysis Date
Reporting Limit
Method
% Total Solids
1.09 %
5/7/14
0-100 %
SM 2540B
Total Suspended Solids
13,020 nig/L
5/8/14
2.5 mg/L
SM 2540 D
Ammonia, Nitrogen
7,410 mg/kg
5/7/14
10 rng/lcg
EPA 350.1
TKN
60,800 mg/kg
5/13/14
20 rng/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
< 529 mg/kg
5/9/14
529 mg/kg
EPA 353.2
Nitrogen, total
60,800 mg/kg
5/15/14
20 mg/kg
EPA 353.2
Aluminum, total
932 mg/lcg
5/21/14
2.50 mg/kg
EPA 200.7
Arsenic, total
< 2.63 mg/kg
5/21/14
2.63 mg/kg
EPA 200.7
Cadmium, total
3,89 mg/kg
5/21/14
0.200 mg/kg
EPA 200.7
Calcium, total
11,736 mg/kg
5/21/14
10.0 mg/kg
EPA 200.7
Chromium, total
88.4 mg/kg
5/21/14
0.250 mg/kg
EPA 200.7
Copper, total
455 mg/kg
5/21/14
1.00 mg/kg
EPA 200.7
Lead, total
32.7 mg/kg
5/21/14
0.500 mg/kg
EPA 200.7
Magnesium, total
5,157 mg/kg
5/21/14
10.0 mg/kg
EPA 200.7
Mercury, total
0.476 mg/kg
5/12/14
0.02 mg/kg
EPA 245.1
Molybdenum, total
9.26 mg/kg
5/21/14
0.500 mg/kg
EPA 200.7
Nickel, total
16.6 mg/kg
5/21/14
2.0 mg/kg
EPA 200.7
Phosphorus, total
22,736 mg/kg
5/21/14
2.00 mg/kg
EPA 200.7
Potassium, total
5,947 mg/kg
5/21/14
20.0 mg/kg
EPA 200.7
Selenium, total
5.89 mg/l(g
5/21/14
0.50 mg/kg
EPA 200.7
Sodium, total
12,473 mg/kg
5/21/14
20.0 mg/kg
EPA 200.7
Zinc, total
700 mg/kg
5/21/14
0.500 mg/kg
EPA 200.7
I hereby certify that I have reviewed and approve these data.
c< <
Laboratory Representative
642 'Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-2a-zo2 Chain of Custody Record (COC)
NPDES#: I�,� C� OC� c -�7
Client: �t n� C--/` . �,�� Phone: ��� ^ �5 2 / 2�
E 9 �, INC.
Address: C ,'a.w'Q1_ ��% Fax:
'
ENVIRONMENTAL LABORATORIES
�S7iY
r
.r-r ,,ink C �7
�` Email:
642 TamcoRd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
�
P.O.#:__ a3 19 � C) to OL1
Email: [e-mail]
Attention: C-,> 3 s Turn Around Time*
p �r�
www.meritechdabs.cb
How would you like your report sent? "RUSH work needs prior approval.
t I
Circle all that apply:(preferred)Fax, Mail Std 10 s) 3 5 Da 5 �4-48Hrs
CEmail
lip Dates &times
P sonTakingSample(Sign/Print):Sam
aG
Lab:Use Only..
:
Sample Location and/or ID #
Start
End
,
Comp.
r:
#o,
tes/t(s)
Required,
Yes/:.._=pFfOK.
�-
Date
Time
Date
Time
Grab?
Cont.
Yes /;No
CI OK?
C.»
-Q-
/0
Temperature Upon`
Receipt::.
a p
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO samples must be done in the field prior to preservation. ***
Comments:
Compositor #,-
Shipment:
❑ UPS
Jug•#
Fed Ex
Are these results for regulatory purposes? Yes s No
Report results in: mg/C [ mg/kgf ug/L=
4 Delivery
nd Delive
Relinquished b1��i� _�� V mate: Time: C
C t,cJ
Rec4 d by: Time:
,f
Sather
Relin fished by: � .�gatR Time: �—�.—,
J i/
Received by: Date- Time:
Relinquished by: Date: Time:
Received by: ab: Dale: Time`
( ..�yi
15
L ) l

), : -.'7. 00
Date:
Grab Sample t
Collected By:
Time Collected: 5 —7:� 1C`\
STE R L J - >H E o-H+ 0 (A( s)
CERTIFICATION NO. 240 DO SM 4500-0 G-2UO1 (Aqueous)
TEMPERATURE, D.O., pH, Cl2 TEMP. SM 2550 B-2000 (Aqueous)
TOTAL RESIDUAL CHLORINE SM 4500 Cl G-2000 (Aqueous)
TEMPERATURE
GRAB
SAMPLE
TEMP.
READING
TIME OF
READING
READ
BY
RESULTS
REPORTED ° C
EFF
EFF DUP
Relative Absolute % Difference (Effluent)
2( r )
+ 1 X100=
{
pH
SAMPLE
pH
READING
TIME OF
READING
READ
BY
REPORTED
in Std. Units.
EFF
EFF DUP
Relative Absolute % Difference (Effluent)
2( Nj 11�-'- )
+ X100= %
SAMPLE
D.O.
READING
TIME OF
READING
READ
BY
RESULTS
REPORTED mg/L
DISSOLVED OXYGEN
TIME DO METER CALIBRATED BY
SLOPE DO READING AT CALIBRATION mg/L
Relative Absolute % Difference (Effluent)
2( - )
+ X100= %
LOW LEVEL CHLORINE RESIDUAL
LL CL2 RES. AVERAGE BLANK Mn RESULTS
SAMPLE ANALYST ANALYSIS READING EFFLUENT CORRECTIONCORRECTIONREPORTED
TIME ppb ppb ppb ppb
EFF
EFF DUPL.
Results Reported = Average'Effluent Minus Blank Correction Minus Mn Correction
CURVE DATE: CORR.COEFF:
DAILY CHLORINE RESIDUAL STANDARDS
QC RESULT DATE RUN TIME ANALYZED ANALYST
CHLORINE QC VALUE IS
ACCEPTABLE RANGE IS TO
HACH LOW RANGE CHLORINE STD.
OPENED EXP. DATE LOT #
Relative Absolute % Difference (Effluent)
+ X100= %

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Meritech Work Order # 07091472 Sample: Sludge Storage Grab
Parameters
Results Analysis Date
Revised Date: 712912014
Report Date: 7/23/2014
NPDES#: WQ0003824
Date Sample Rcvd: 7/9/2014
7/9/14
Reporting Limit Method
% Total Solids
1.73 %
7/10/14
0-100 %
SM 2540B
Total Suspended Solids
11,940
mg/L
7/15/14
2.5
mg/L
SM 2540 D
Ammonia, Nitrogen
10,800
mg/kg
7/10/14
10
tnglkg
EPA 350.1
TKN
59,500
mg/kg
7/21/14
20
mglk�
EPA 351.1
Nitrate/Nitrite, Nitrogen
<578
rrrg/kg
7/9/14
578
mg/kg
EPA 353.2
Nitrogen, total
59,500
mg/kg
7/21/14
20
mg/ltg
EPA 353.2
Aluminum, total
8,790
mg/kg
7/21/14
2,50
mg/loc
EPA 200.7
Arsenic, total
<2.89
mg/kg
7/21/14
2.89
mg/Icg
EPA 200.7
Cadmium, total
3.70
mg/kg
7/21/14
0.200
mg/l(g
EPA 200.7
Calcium, total
11,100
mg/kg
7/21/14
10.0
mg/1W
EPA 200.7
Chromium, total
77.5
nzg/l,(,q
7/21/14
0.005
mg/1,
EPA 200.7
Copper, total
431
mg/kg
7/21/14
0.250
mg/kg
EPA 200.7
Lead, total
30.1
mg/kg
7/21/14
0.500
mg/kg
EPA 200.7
Magnesium, total
5,510
mg/kg
7/21/14
10.0
mg/kg
EPA 200.7
Mec•cury, total
0.462
mg/1cg
7/14/14
0.02
mg/kg
EPA 245.1
Molybdenum, total
7.28
mg1kg
7/21/14
0.500
mg/kg
EPA 200.7
Nickel, total
16.5
mg/1{q
7/21/14
2.0
mg/kg
EPA 200.7
Phosphorus, total
24,600
mg/kg
7/21/14
2.00
Iltgll{g
EPA 200.7
Potassium, total
6,360
mg/kg
7/21/14
20.0
mg1kg
EPA 200.7
Selenium, total
5.09
mg/Irg
7/21/14
0.50
mglkg
EPA 200.7
Sodium, total
13,200
mg/lcg
7/21/14
20.0
mg/lrg
EPA 200.7
Zinc, total
665
mg/kg
7/21/14
0.500
mg/Itg
EPA 200.7
I hereby certify that 1 have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-20-201 Chain of Custody Record (COC)
��`/�� NPDES#: Q G oe� y
� n� d i l3� W W—►y' Phorte:a3(z ! S %O — 6 ?21
Address: i - �'� a ,Q^Gtn�rzT % Fax:
ctX\ C G -% 3 Email:
Project:
P_O.#:
Attention: ,`,� Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: mail(preferred), ax, Mail Std 10 s) 3--5 Days z�s
MERClient:
ITINC.
.., ENVIRONMENTAL LABORATORIES
Irk 642TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
�-y�
www.meritech-labs.com I
Sample Location and/or ID #
Sampling ®aces Times
P s n Taking Sample Sign Print):
�� �� e ��
Lab Us dy
Start
End
comp?
Grab?
# of
Cont.
_
Tests) Required
On Ice?
Yes No
pH OK -?*'
Cl OK?
Date
Time
Date
Time
ND
n.
3¢ 3
Tern perature. Upon
Receipt:
Method of
Shipment:
"" Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. "*
Comments:
Compositor;
Jug #
Q' UPS
Fed Ex
Are these results for regulatory purposes? Yes No
Report results in: mg/L [ m k ug/L 13,-
d Delivery
Relinq by:
ate: Time:
1'.'Z� Or1
Rec " ed by. � � Time:
�t�'� 7 � Z
Other
Ck _ n
""S
ReLiiiquished by: Date: Ti
Received by: D e: Time:
^ *
Relin ished y: Date: Time:
Receive
1
� b: 3� Da� I I Time: .,1

1 , G0
a� caz l i O c
Date: /
Grab Sample
Collected By:
Time Collected: -�
iTEI R Li v Fl S )-H•1- J (Aq >)
CERTIFICATION NO. 240 `c DO SM 4900 0-Zw1 (Aqueous)
TEMPERATURE, D.O., pH, Cl2 TEMP. SM 2550 B-2000 (Aqueous)
TOTAL RESIDUAL CHLORINE SM 4500 Cl G-2000 (Aqueous)
TEMPERATURE
GRAB
SAMPLE
TEMP.
READING
TIME OF
READING
READ
BY
RESULTS
REPORTED' C
EFF
EFF DUP
')5w)
f6
� c) c..
Relative Absolute % Difference (Effluent)
+ X100= %
pH
;-SAMPLE
pH
READING
TIME OF
READING
READ
BY
REPORTED
in Sid. Units.
FF
3 EFF DUP
Relative Absolute % Difference (Effluent)
2( +X100=
DISSOLVED OXYGEN
SAMPLE
D.O.
READING
TIME OF
READING
READ
BY
RESULTS
REPORTED mg/L
EFF
EFF DUP
TIME DO METER CALIBRATED
SLOPE DO READING AT CALIBRATION mg/L
Relative Absolute % Difference (Effluent)
2( - )
+ X 100 = %
'LOW LEVEL CHLORINE RESIDUAL
LL CL2 RES.
AVERAGE
BLANK
Mn
RESULTS
SAMPLE
ANALYST
ANALYSIS
READING
EFFLUENT
CORRECTIO
CORRECTIONREPORTED
TIME
ppb
ppb
ppb
ppb
EFF
EFF DUPL.
Results Reported = Average Effluent Minus Blank Correction Minus Mn Correction
CURVE DATE: CORR.COEFF:
DAILY CHLORINE RESIDUAL STANDARDS
QC RESULT
DATE RUN
TIME ANALYZED
ANALYST
CHLORINE QC VALUE IS
ACCEPTABLE RANGE IS TO _
HACH LOW RANGE CHLORINE STD.
OPENED EXP. DATE LOT #
Relative Absolute % Difference (Effluent)
2( - )
+ X100= %

Meritech, Inc,
Environinental Laboratory
- Laboratory Certification No. 165
Contact: Cris Routh Report Date: 10/28/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 PO#: 2015000236
Graham, NC 27253 Date Sample Rcvd: 10/16/2014
Meritech Work Order # 10161440 Sample: Sludge Storage Grab 10/16/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
1.33 %
10/17/14
0-100 %
SM 2540B
Total Suspended Solids
12,280 mg/l.
10/21/14
2.5 mg/L
SM 2540 D
Ammonia, Nitrogen
15,500 mg/kg
10/21/14
10 mg/kg
EPA 350.1
TKN
35,300 mg/kg
10/20/14
20 mg/lcg
EPA 351.1
Nitrate/Nitrite, Nitrogen
< 752 mg/kg
10/17/14
752 mg/lcg
EPA 353.2
Nitrogen, total
35,300 mg/kg
10/23/14
20 mg/kg
EPA 353.2
Aluminum, total
10,200 mg/kg
10/24/14
2.50 mg/Icg
EPA 200,7
Arsenic, total
< 0.752 mg/kg
10/24/14
0.752 mg/kg
EPA 200.7
Cadmium, total
4.81 mg/kg
10/24/14
0.200 mg/kg
EPA 200.7
Calcium, total
15,100 mg/kg
10/24/14
10.0 nlg/kg
EPA 200.7
Chromium, total
88.0 mg/kg
10/24/14
0.250 mg/kg
EPA 200.7
Cropper, total
502 mg/kg
10/24/14
1.00 mg/kg
EPA 200.7
Lead, total.
43.8 mg/kg
10/24/14
0.500 mg/1%
EPA 200.7
Magnesium, total ......................
6,7.20 111 Ic
�.....
10 24....1.4 .
/ /
....,.10.O.ilii/I�,� ..............rPA.200,7.......
...
Mercury total
.......,...�.:..�......
0.226 �mg/Icg
1Cl%17/14
0.10 mg/kg
EPA 245.1
Molybdenum, total
5.19 mlg/Icg
10/24/14
0.500 mg/kg
EPA 200.7
Nickel, total
17.9 mg/kg
10/24/14
0.500 mg/kg
EPA 200.7
PhOSp110111S, total
30,200 ing/Icg
10/24/14
2.00 mg/Icg
EPA 200.7
Potassium, total
8,420 mg/kg
10/24/1.4
20.0 mg/kg
EPA 200.7
Selenium, total
< 0.752 mg/lcg
10/24/14
0.752 mg/kg
EPA 200.7
Sodium, total
22,300 mg/lcg
10/24/14
20.0 ing/kg
EPA 200.7
Zinc, total
1,170 mg/kg
10/24/14
0.500 mg/kg
EPA 200.7
1 hereby certify that I have reviewed and approve these data. ce , k"_(i1
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3=0-201; Chairs. of Custody Record (COC)
NPDES#:_ Q D Oo$
Client: ' '-r. 0-1'10M1A>WV Phorie:�36-57c—�72SMERITECH,
INC.
—
Address: Rn _ �� ; � � Fax: �36-S�-ss
d 2.
ENVIRONMENTAL LABORATORIES
(r^ x Email:
_-
642 TamcoRd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
! P O #: j S C,,=g �fa
Email: [e-mail]
iAttention: s'S `'
Turn Around Time'
`�,'� s r,� r "' (` I �rw'
V� �r�, i �" � h—y � �O
l How would you;Dike your report sent? "RUSH work needs prior approval.
Std io d (s)
° v °�S .
Circle all that apply .Email (preferred) , Fax, Mail
3 -5 Da Ys 24 - 48 Hrs
Sampling Dates & Times
P n TakinpSample (Sign Print): ��
(L I `� �' � w4 v .L . �z -i .
b y
��S� ®�,
Sample Location and/or !D # Start
_End
Date Time
Comp.
:of
�st(s) Required
On Ice?
pH OK?
Date Time
Grab?
Cont.
Yes / No
Cl OK?
Woo
�LX'2 t 9�7 Y • �e
C//0'•
N! —T,
0 C
1
Temperature Upon
i
j
�R i .
-
Method of: "* Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
:;c :rments:
Shipment:.
Compositor#
UPS
Jug#
:. Fed Ex Are these results for regulatory purposes? Yes
Not: Report r 5 in: m L [)
p g/
mg/kg Q ug/L
I--� nd Delivers el G d by: Date:
lJ � e
Tim �Rec
D e • �,] Time:
Ea Other l ,•�i'°� ° v Date:
T'me: > �' 3 eceived by:
i
Date: Time:
shed by: Date:
Time: rved by C•, -
Q�te `i Ci Timed^� -
�,'�i ! ` )

-j , - „ - L{ . U i
Date:
Grab Sample
Collected By:
Time Collected: 10:O L N �1
STE --R l_ t pH ; 10-H-1 10 (Ai s)
CERTIFICATION NO. 240 ��
LL<< ,� DO SM 4500-0 G-2001 (Aqueous)
TEMPERATURE, D.O., pH, Cl2 TEMP. SM 2550 B-2000 (Aqueous)
TOTAL RESIDUAL CHLORINE SM 4500 Cl G-2000 (Aqueous)
TEMPERATURE
GRAB
SAMPLE
TEMP.
READING
TIME OF
READING
READ
BY
RESULTS
REPORTED ° C
EFF
EFF DUP
Relative Absolute % Difference (Effluent)
2 )
+ X100= %
--
C�J . Iv.1-2C
pH
SAMPLE
PHTIME
READING
OF
READING
READ
BY
REPORTED
in Std. Units.
EFF
EFF DUP
Relative Absolute % Difference (Effluent)
2
+ �_ X 100 m _%
DISSOLVED OXYGEN
D.O.
TIME OF
READ
RESULTS
SAMPLE
READING
READING
BY
REPORTED mg/L
EFF
\'
EFF DUP
TIME DO METER CALIBRATED �� BY_
SLOPE DO READING AT CALIBRATIO
Relative Absolute % Difference (Effluent)
2( - )
+ X100=
LOW LEVEL CHLORINE RESIDUAL
LL CLz RES.
AVERAGE
BLANK
Mn
RESULTS
SAMP
ANALYST
ANALYSIS
READING
EFFLUENT
CORRECTIONCORRECTION
REPORTED
\
TIME
PPb
PPb
PPb
PPb
`\
EFF
\
EFF DUPL.
Results Reported = Average Effluent Minus Blank Correction Minus Mn Correction
CURVE DATE: CORK COEFF:
DAILY CHLORINE RESIDUAL STANDARDS
QC RESULT
DATE RUN
TIME ANALYZED --,,I
ANALYST
CHLORINE QC VALUE IS
ACCEPTABLE RANGE IS —TO _
HACH LOW RANGE CHLORINE STD.
OPENED EXP. DATE LOT #
Relative Absolute % Difference (Effluent)
2 ( ^- )
+ X100=

�I
meritech, Inc.
Environmental. Laboratory
" Laboratory Certification No.165
_t„" _
'.k:". .. .. ... ..
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Meritech Work Order # 10161441 Sample: Sludge Storage Grab
1311- TCLP Metals
Report Date: 11/4/2014
Date Sample Rcvd: 10/16/2014
Collection Date:, 10/16/2014
Parameter
Results
Analysis
Det. Limi
Reg. Limit
Method
Arsenic
< 0.010 mg/l,
10/27/14
0.100
5.0
EPA 200.7
Barium
0.061 mg/L
10/27/14
0,050
100.0
EPA 200.7
Cadmium
< 0.002 mg/L
10/27/14
0.020
1.0
EPA 200.7
Chi•oI11iUn1
< 0.005 mg/L
10/27/14
0:050
5.0
EPA 200.7
Lead
< 0.010 mg/L
10/27/14
0.100
5.0
EPA 200.7
Mercury
< 0.02 mg/L
10/24/14
0.02
0:2
EPA 245.1
Selenium
< 0,010 ing/L
10/27/14
0.100
1.0
EPA 200.7
Silver
< 0.005 mg/L
10/27/14
0.050
5.0
EPA 200.7
TCLP.Organics
Parametc r ...
Results
Analysis
Method
Pesticides 8080
Attached
.... ....
10/30/14 r.
8080
Volatiles..826.0
Attached ......
.. 10/22/14......:..............:....:..:....:........:.:8260
.:...............::........
Semi Vol. 8270
Attached
10/22/14
8270
Her icides 8150
Attacled
10/30/14
8150
Other Tests
Parameter Results Analysis Reporting Limit Method
Cyanide, total
< 0.500 mg/kg
10/22/14
0.5 mg/kg EPA 335.4
'Hash Point
> 140 '°r
10/18/14
EPA 1020B
lgnitability
Will not ignite
10/18/14
= = EPA 103G
pH
6.8 S.U.
10/27/14
1.0 -14.0 S.U. SM 4500 HB
j Sulfide, total
1
< 10 mg/kg
10/21/14
10 mg/kg SM 4560 SD
642 Tameo Road, Reidsville, North Carolina 27320
teI.[phone] fax.[phone]
i

Merilech, Inc.
Environmental Laboratory
x
Laboratory Certification No.165
Contact: Cris Routh
Report Date:
11/4/2014
Client: Graham, City of
P.O. Drawer 357
Date Sample Rcvd:
10/16/2014
Graham, NC 27253
Meritech Work Order # 10161441 Sample: Sludge Storage Grab.
Collection Date:
10/16/2014
1311- TCLP Pesticides & Herbicides
Pesticide - SW-846 8081A
Analyst: Summit
Analysis Date:
10/30/14
Parameter
Results Det. Limit
Reg. Limit imit Dilution Factor
Heptachlor Epoxide
< 0.002 mg/L 0.002
0.008
1
Endrin
< 0.002 mg/L 0.002
0.02
1
Chlordane
< 0.010 mg/L 0.01
0.03
1
Gamma - BHC
< 0.002 mg/L 0.002
0.4
1
Toxaphene
< 0.10 mg/l., 0.1
0.5
1
Methoxychlor.......................................
<...0,002...mg/L..........-....... -_........ ....... ...... 0.002... ...... .... .......... ...-.......10.0.
.... .......... ......... .... ..................._._1............................._.:..::::...
I-leptachlor
< 0.002 mg/l. ....0.002
....0.008 ..........1
......:...:............
Lindane ................. .:.:.::.:.<.0.002
mg/L . 0.002
.0.4 . _ .
1 .., . ..... ........,
Herbicides - SW-846 8151A
Analyst: Summit ..
....Analysis Date:...........10/31/14
............
Parameter
Results Det. Limit
Reg. Limit Dilution Factor
2,4-D
< 5.0 mg/L 5.0
10.0
1
2,4,5-1'P (Silvex)
< 0.5 mg/L 0.5
1.0
1
I hereby certify that I have reviewed and approve these data.
if.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.
Environmental Laboratories
Laboratory Certificate d#165
Client:, �' . City of Graham Wb� TP
Project: TCI.,P
Client Sample ID: Sludge Storage
Sample Collection: 10/16/14
Meritech Sample ID: 10161441
1311 - TCLP ®raanics
Volnti_I_es: SW-846 8260-
Analysis: 10/22/ 14
Extracted:
10/ 16/ 14
Analyst: VwV
Parameter
Result
Units
Det. Limit
Reg. Limit
Dilution Factor
Benzene
< 0.0100
mg/L
0.0100
5.00
10
Carbon Tetrachloride
< 0.0100
mg/L
0.0100
5.00
10
Chlorobenzene
< 0.0100
mg/L.
0.0100
100
10
Chloroform
< 0.0100
mg/L
0.0100
6.0
10
1,2-Dichloroetltahe
<0.0100
mg/L
0.0100
0.50
10
l,l-Dichtoroethene
<0.0100
mg/L
0.0100
0,70
10
Methyl Ethyl Ketone
< 0.100
mg/1,
0.100
200
10
Tetrachlorocthylcne
< 0.0100
mg/L
0.0100
0.70
10
Trlclzloroetliene
< 0.0100
mg/L
0.0100
0.50
10
Vinyl Chloride
< 0.0200
mg/L
0.020
0.20
10
Semi-Volatiles: SW-846 8270
............. .....
..... ......._........................................................................_
............................. _...................
Analysis: 10/28114
Extracted:
10/22/14
Analyst: PM
Parameter
Result
Units
Det, Limit
Reg. Limit
Dilution Factor
1,4>Dichlorobcnzene
<0.100
mg/L
0.100
7.5
10
I-Icxachlorobenzene
<0.100
mg/L
0.100
0.13
10
Hexachloro-1,3-butadiene
<0.100
mg/L
0.100
0.5
10
I-lexachloroctlianc
<0.100
mg/L
0.100
3.00
10
o-cresol
<0.100
mg/L
0.100
200
10
ni&p-cresol
<0.200
mg/L
0.200
200
10
Total cresols
<0.300
mg/L
0.300
200
10
Nitrobenzene
<0.100
mg/L
0.100
2.00
t0
Pentactilorophenol
<0.500
11101,
0.500
100
10
Pyridine
<0.100
mg/L
0.100
5.0
10
2,4,5- frichlorophenol.
<0.100
mg/L
0.100
400
10
2,4,6-Trichlorophenot
<0.100
mg/L
0.100
2.00
10
2,4-Dinitrotoluene
<0.100
mg/L
0.100
0.13
10
I hereby ceilify that I have reviewed and approve these data.
(�r
Laboralory Representative
642 Tamco Road * Reidsville, NC 27320
[phone]
Ph *
(336) 3424622
Fax

—'— ---' --- ��N�� ---/ --- ---` '---'
---~
�
-
Address: 4
ENVIRONMENTAL LABORATORIES
C_r'k Email:
Reidsville NC 27320 Fax- 336-342-1522
P.O.#: Turn Around Tirrie*
Email- [e-mail]
Attention: *RUSH work needs prior approval.
How would you like your report sent?
www,medtechdabs.com
Circle all that apply: CEm7il (prefe-ed_)',,,, Fax, Mail C=,
Sampling Dates & Times
CQ:
:,Lab: Use Onl
Sta rt
End
Comp?
# of
X A
Test(s) Required
Ice..:
Ye No:
p
Sample Location and/or ID #
— ___7
Date
Time
Date
Time
Grab?
Cont.
Cl OK?
Temperature Upon
Method of
Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO samples must be done in the f4ld prior to preservation.'
Compositor #'
UPS
Pugg.
Q:Fed Ex
Are these results for regulatory purposes? Yes
E�r Report results in: mg/L mg/kg
Datey
/'

CITY OF GRAHAM, WASTEWATER TREATMENT PLANT
1 q-Mar-14
Sodium Absorption Ratio Calculation (SAR)
% Solids
1.83
Na (mg/kg)
12055
Ca (mg/kg)
10944
Mg (mg/kg)
4988
Na (mg/L)
220.61
Ca (mg/L)
200.28
Mg (mg/L)
91.28
Na (meq)
9.60
Ca (meq)
9.99
Mg (meq)
7.51
SAR =
LEGEND
Fill in this area with data from the analysis sheets
<. This area is calculated automatically
NOTE: NOTIFY WSRO, AQUAFER PROTECTION, IF SAR IS GREATER THAN 5.0
Prepared by Cris Routh 1/26/2015
Page 1

CITY OF GRAHAM, WASTEWATER TREATMENT PLANT
7-May-14
Sodium Absorption Ratio Calculation (SAR)
% Solids
1.89
Na (mg/kg)
12473
Ca (mg/kg)
11736
Mg (mg/kg)
5157
Na (mg/L)
235.74
Ca (mg/L)
221.81
Mg (mg/L)
97.47
Na (meq) 10.25
Ca (meq) 11.07
Mg (meq) 8.02
SAR =
LEGEND
Fill in this area with data from the analysis sheets
This area is calculated automatically
NOTE: NOTIFY WSRO, AQUAFER PROTECTION, IF SAR IS GREATER THAN 5.0

CITY OF GRAHAM, WASTEWATER TREATMENT PLANT
9-Jul-14
Sodium Absorption Ratio Calculation (SAR)
% Solids
1.73
Na (mg/kg)
13200
Ca (mg/kg)
11100
Mg (mg/kg)
5510
Na (mg/L) 228.36
Ca (mg/L) 192.03
Mg (mg/L) 95.32
Na (meq)
9.93
Ca (meq)
9.58
Mg (meq)
7.84
SAR =
LEGEND
Fill in this area with data from the analysis sheets
This area is calculated automatically
NOTE: NOTIFY WSRO, AQUAFER PROTECTION, IF SAR IS GREATER THAN 5.0

CITY OF GRAHAM, WASTEWATER TREATMENT PLANT
1 F-nest-14
Sodium Absorption Ratio Calculation (SAR)
% Solids
1.33
Na (mg/kg)
22300
Ca (mg/kg)
15100
Mg (mg/kg)
6720
Na (mg/L)
296.59
Ca (mg/L)
200.83
Mg (mg/L)
89.38
Na (meq)
12.90
Ca (meq)
10.02
Mg (meq)
7.35
SAR =
LEGEND
Fill in this area with data from the analysis sheets
.. a
This area is calculated automatically
NOTE: NOTIFY WSRO, AQUAFER PROTECTION, IF SAR IS GREATER THAN 5.0

(2) Primary Clarifiers
IPS to Aeration
(2) Aeration Basins
WAS to Digestion
'Al
I (a E Y ijnH( �inv t
y,- �..vv
'
it
art
C hi,, e,
(4) Final Clarifiers Digester No. 1 Digester No. 2 Digester No. 3
114,000 gallons —� 196,000 gallons —� 750,000 gallons
Sludge Storage (2) Silo Sludge'" ��, a
750,000 gallons � Storage Tanks —� —� Farm Site
50,000 gallons each

CITY OF GRAHAM
WASTEWATER TREATMENT PLANT
GEOMETRIC MEAN CALCULATIONS FOR SLUDGE
503 B
FIRST QUARTER - 2014
DATE
RESULTS
UNITS
% DRY SOLIDS
March 18, 2014
56524
MPN/g.dry
1.93
March 19, 2014
33843
MPN/g.dry
1..89
March 20, 2014
117318
MPN/g.dry
1.79
March 25, 2014
55556
MPN/g.dry
1.80
March 26, 2014
2333
MPN/g.dry
1.80
March 27, 2014
198895
MPN/g.dry
1.81
March 31, 2014
1536
MPN/g.dry
1.76
GEOMETRIC MEAN =
26378
MPN/g.dry
1.83

_J
Meritech, Inc.
Environmental Laboratory
r- - Laboratory Certification No.165
Contact: Cris Routh
Report bate:
3/26/2014
Client: Graham, City of
NPDES#:
WQ0003824
P.O. Drawer 357
P.O.#:
2014000785
Graham, NC 27253
Date Sample Rcvd:
3/18/2014
Meritech Work Order # 03181427 Sample: Sludge Storage Grab
3/18/14
Parameters
Resul ,Analysis Date
Reporting Limit
Method
% Total Solids
1.93 % 3/19/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
56,524 col/g drywt 3/18/14
130 col/g diywt
SM 9222D
y
4
I hereby certify that I have reviewed and approve these data.
&&a, e -
Laboratory Represe tative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
�1�Phone:
Client:C;4n ►.�iFax:
Address: d •*2�`
����- � Iy C a Z
C�-
Attention: I S G
NPDEs# WQ Z500
� -S7o-� 6 %2 f
Z-36-313 -.SS02ITC
Project#
PO. # &110p a
9I .Email:
ENVIRONMENTAL LABORATORIES
r /tin
• A Division of Water Technoioyy and ControiS, in_C.
Phone: [phone]
642 Tamco Rd. Fax: [phone]
Reidsville, NC 27320 Email: srmrtechCbellsouth.net
Web Site: www.meritech-labs.com
Turn Around Time*
*RUSH work must have prior approval.
Std (10 d
3 - 5Day
2�r
Sample
Location/ID #
Sam lin Dates & Times
p �
" n�
PersonTakin Sam le Si nature : �i3Qlot� �
Required
Method
Lab Use
Only,
START
END
Comp?
Grab?
#oi
Coots.
Tests Required
_ Q
zoos 1zoo.7
pH OK?
C12 OK?
Date
Time
Date
Time
t�3�cQ4
Compositor #
Jug #
***Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation*"
Comments:
Method of Shipment:
UPS
❑ Fed Ex
brand Delivery
Other
Are these results ,! regulatory purposes? Report results in
YES NO Lk 0 mg/Kg ❑ ixg2 ❑
On lee? Temperature On Receipt (
ReG shed by Date Time
3 db
Receive by Date Tim
Relinquish Date } Time
Received by Date Time
Relinquished by Date Time
Received at by Date, Time

Meritech, Inc.
. Environmental Laboratory
Laboratory Certification No.165
j Revised Date: 312712014
Contact: Cris Routh Report Date: 3/26/2014
Client: Graham, City of - NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2014000785
Graham, NC 27253 Date Sample Rcvd: 3/19/2014
Meritech Work Order # 031914144 Sample: Sludge Storage Grab 3/19/14
Parameters Result Analysis Date Reporting Limit Method Oualif ,
% Total Solids 1.89 % 3/21/14 0-100 % SM 2540E
Fecal Coliform (Sludge) 33,843 cal/g dry wt 3/19/14 130 col/g dry wt SM 9222D B3
B3 Countable membranes with more than 60 colonies. The value reported is calculated using the count
from the smallest volume filtered.
I hereby certify that I have'reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of CUstody� Record (COC)
a
CEI@rit: -�i4-Q 1 a'V t/V t11
NPDES# Q�130. -
Phone: - %
Fax:%
E .: �, INC.
" ENVIRONMENTAL LABORATORIES
g A DIv1sio17 of WaferTeC/jno% and Controls, r /nc.
Phone:, 1-336-342-4746
642'Tamco Rd. Fax: 1-336-3,42-1522
Reid_ sville; NC 2732T Email: srmrtech@belisouth:net
Web Sltes vivivrmeritech-labs.co"m
Q
Address: n Q0"'t'T�+�
'
Attentlon: 1 � A-"-
Email:
Project #•
Turn tround,Time*
*RUSH work rnusl have prlorapproval.
Std (tio d
3 - 5`Day
24 = 48 Hr
Sample
'Lopation/ID #
Sampling .Dates &Times
s
Person Takin Sam le Si nature: vQ
�eqiyired
Method
Lab Use
only
START
END
comp?
Grab?
# of
eoms.
Tests. Required
2oo:ai2oo:�
pH OK?
C120K?
Date
Time
Dale
Time
to
1
Imo,
L'
.S'A"J4
W! , � Is ° C,
Compositor,
Jug #
'"-•Deohiorination (<0.5 ppm) of. Ammonia,
Cyanide, Phenol or TKN samples must be done in the field prior to preservation.**k
Comments:
Method of Shipment:
ups
❑ Fed Ex
U nd Delivery
t9aTime
.Other
/'''� '^1 ,-^n
Are these results f egutatory purposes?
YES No
Report tesults In
mgtL LI mg/Kg LI µ92
.On ice?
c1
Temperature.On Receipt. e
Rei" fished by Date Time
Receiv y Date, Time
R he 144 Dale Time
Received by bate
Relinquished by Date time
at fa y D e Tune

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Report Date:
3/26/2014
NPDES#:
WQ0003824
ROA
2014000785
Date Sample Rcvd:
3/20/2014
Meritech Work Order # 03201432 Sample: Sludge Storage Grab 3/20/14
Parameters Resul Analysis Date Re oU rting Limit Method
% Total Solids 1.79 % 3/21/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 117,318 col/g dry wt 3/20/14 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. 6 _ �&�
Laboratory Representative
642 Tainco Road, Reidsville, forth Carolina 27320
tel.[phone] fax.[phone]

--
Chain of Custody Record (COC)
o
Client: c� r r. YV J
,- ���
Address:
�,�„ Jy G 2 %,2.
Attention: ��iil s S G
Phone �S o - b 2-11
Fax:_a- y� B
MERI �"EC�1, INC.
ENVIRONMENTAL LABORATORIES
.m
A Division of Water Techno%gyand Contro/s, 7nc.�
Phone: [phone]
642 Tamco Rd. Fax: [phone]
Reidsville, NC 27320 Email: [e-mail]
Web Site: www.meritech-labs.com
Email:
Project#
P.O. # O O
Turn Around Time*
*RUSH work must have prior approval.
Std (10 da
3 -5 Day
24 -48 Hr
Sample
Location/ID #
Sampling Dates & Times
p g
Person Takin Sam le (Signature):
Required
�`'o Use
START
END
Comp?
Grab?
#of
Conts.
Tests Required
2D08/20�7
pH OK?
C120K7
Date
Time
Date
Time
•
3 19
4.
Gt7`�
Compositor #
Jug #
***Dech[orination (<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation.***
Comments:
Method of Shipment:
❑ UPS
❑ Fed Ex
❑; nd Delivery
Other
L
Are these results regulatory purposes?
YES NO ❑
Report results in
mg/L ❑ mg/Kg ❑ µ9/L ❑
On Ice?
ti
Temperature On Receipt _L
ReI- ished by Date Time
O
Received b Date Time
�- 3 .ZO /
Relinquished Date Time
3 �� 3 O
Received by Date Time
Relinquished by Date Time
Received t lab by Date Time
+�

Meritech, Inc,
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 4/4/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2014000785
Graham, NC 27253 Date Sample Rcvd: 3/25/2014
Meritech Work Order # 03251446 Sample: Sludge Storage Grab 3/25/14
Parameters Result Analysis Date Reporting Limit Mhod
% Total Solids 1.80 % 3/26/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 55,556 col/g dry wt 3/25/14 130 col/g dry wt SM 9222D
h
I hereby certify that I have reviewed and approve these data. k . Az, z Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Cheitl'of'Custody Record (COG)
s 1
Client: } 1
NPCES
Phone:.aSf�.-670 - 6,121
Fax:
ENVIRCINMENTAL LABORATORIES
A Diflision ofWaler Technology, and Controls, %nc.
Phone: [phone]=474W
642 Tarnco. Rd. Fax: [phone]-
Reielsville,.NC27320 Email: srmrtet:hQbeHsouth;net
Web Site: wvv%v;meritech-labs.com
Address:
AttentiOtl
Email:, Z
Project:#
p O. #
Turn -Around Time*
'RUSH work must have�piiar approval,
std(10. s}
3-5-Day
24-48,He
Sample_
Location/10i
Sampling Datos & Times
Person Takin Sa6 le- Si' nature :. t.c?2r` -_
Required
Meihod
Lab Use
Only,
START
END
Comp?
Grab?
# of
Copts..
TeSt8, RegUIP£d.
20Q'8J200'7
pH pK?
C12,OK?
Date
Time.
Daie.,
Time
rql W'Q(790f�
xs
� ,.
to 1'7
G e �`
t
Compositor #'
jtig
***Dechlorination (<015-pprn) of`Aimmonia, Cyanide, Phenol or TKN satrtples.must be done in the field prior to preservation.***
Comments:
Method of Shipnlerit,'
u UPS
❑'.Fed Ex
_❑ 'and DeliV81 y'
I-Qther
ry p " poses.
Are theY�rsesuits r'regulalloO ur Report resiitts in
F—Ig/L ❑ mg7Kg i1wL ❑
On lee.?
Temperature_On Receipt, , ti
Reuished by Dat Time.
t`
Re by 'date Time
' 2 ''n / �" 4
Retie" ed b Date Time
- �f+ �- -
by date' me
Rec ed Time,
Relinquished by Date Time-
ed at lab Date Time`
7

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh
Report Date:
4/4/2014
Client: Graham, City of
NPDES#:
WQ0003824
P.O. Drawer 357
P.O.#:
2014000785
Graham, NC 27253
Date Sample Rcvd:
3/26/2014
Meritech Work Order # 032614101 Sample: Sludge Storage Grab
3/26/14
Parameters
Results Analysis Date
Reporting Limit
Method
% Total Solids
1.80 % 3/27/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,333 col/g dry wt 3/26/14
130 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. CCU/'L
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

4,4 Email:
Chain of Custody ROOM (COC) - AA
Client: • Phone:, 6?'�/ 7i
Fax:
MERITECH. INC.,
ENVIAO, -AL LABORATORIES C, NMENT Addiress: Project#
J A D Usion of. wwar Toofinolooy and Controls, .1hb. � C_ 0­7*1P. 6.-J 600j3
Phtthe: 114-36-342-4740 Turn Around Tfind*
642 TAffoo Rd. Fax: [phone] *RUSH work mu _$t have pri fapproval.
. ... . ...... .
Relds,viile,'_N­C 27320 Email: srmrtech(Pbellsouth. et Std 5 nay 11 24as Hr
Web Site: vmmmetitech-iabs.com Attention. " Xw-
,
uired. Use
Sample. $ampiing t�ates-& Times Per�onTakihcjSa Rio (§igr1Atur6)**w'E:P_0_ ReqMethod Lab only
START END POMP? # of 2oo.8 2&� pH OK?
Location/IQ # Tests Requited,
C12,01(?
odle Time: D Time Grab?
!Zkta
-3/ P
Compositor "Techlo-driat ionj<0.5- lipm)of 'AmMon ia, Cyanide, P.. h6noi or TKWtiampl,60 niu'stbe done In the -field prior to preservation:'"*preservation:'"*-
Jlug Comrribrits:
Method of Shipment:, _Awthise rpsyfts,JK feguldt6ry._ purposes? Reportresults in Temperature On Receipt
Oups YES NO rng/L L) md/Kg IJ Itg/L L
Refl4g-vishied by fDate Time Received by Date Time
L) Fed Ek
- -) 1,!j / �''3 -57
Ll�a.&A:e
U"Wrid- Delivery Relinquished` Dat3 Time Received by Date 'rime -
,Other
Relinquished by Date Time Received at lab y Date Time

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 4/4/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2014000785
Graham, NC 27253 Date Sample Rcvd: 3/27/2014
Meritech Work Order # 03271428 Sample: Sludge Storage Grab 3/27/14
Parameters Result Analysis pate Reporting Limit Method
% Total Solids 1.81 % 3/28/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 198,895 col/g dry wt 3/27/14 130 col/g dry wt SM 9222D
1 hereby certify that 1 have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (POC)
-Plone
Client: w
NPDES#WQ�g_382;q
: - -76 -035,2a1
Fax:, )J3. 2
-
A4Email:
,QI0MERITECH'INC
ENVIRONVENTAL LABORATORIES
A Diksion.of Water TOC17nologyanof Con/rots, Inc
Phone; 1 -M-349-4748.
042.'TemaQ Rd; Fax: [phone]
Reidsville__,. NC 27320 -Email: stmr1ech0bellsouth.net
Web Site: www.meritech-labsecom
3IM S
A,7!
ddress
NC. 227;M
Attention:
Project #.
P. 0;4 Q-0146c>6-7
Turn Around. Time*
'RUSH. work must have prior 6ppraiial.
Sid (10 dayor
3 - 5'Day
24 - 48 Hr
Sample
Location/ID #
Sampling DatesTimes
Person Taking sample (Sidnature ): 'L-, w a,.Cc gat4=LMethod
Required
Lab Use
.Only
START
Comp?
Grab?-
of
:Copts.
Tests Required
H OK
P '?
G12OK?
DaW
Time
Date
Time
Lt L2 5
(zi-I
Compositor #
*"Dedhiorinatioln (.e,0.5 p0m) of Ammonia,
Cyanide,, Phenol .or TKN samples Must be -done In'the field prior to pregervati6n.***
Comments:
.Method, of Shipment;
LNOS
U Fed Ex
Q I nd Delivery
th
Me these r& gpjatbry�,Ourposos?.
YES No Q
9!gpbrt results in
=,gA- U mg/Kg U. Pg/LQ
On Ice?
Temperature On Receipt
Re' ished.by Date Time
2, t7 )I L1
R65Vdy- Date Time
�2
Rel nqui Oy pate, Time
Received by Date Time
Relinquishedby Date.
LI/
hme Received at b by Date Time
M

f Meritech, Inc.
Environmental Laboratory
.` Laboratory Certification No.165
Contact: Cris Routh Report Date: 4/4/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2014000785
Graham, NC 27253 Date Sample Rcvd: 3/31/2014
Meritech Work Order # 03311409 Sample: Sludge Storage Grab 3/31/14 -
% Total Solids 1.76 % 4/1/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 1,536 col/g dry wt 3/31/14 130 col/g dry wt SM 9222D B1
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
all filters reported per 100 ml.
0
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-iQ•2013 Chain of Custody Record (COC)
NPDES#: d00 cs,-y
1
Client: 11 Bpi � c; Phone:336 -590 •-
Address: T r� a Y1 pT 35? Fax: I3
G2.��r . 7 Email:
Project:
P.O.#: �� �t✓-'
Attention: � It �C'L Turn -Around Time*
How would you like your report sent? *RUSH.work needs prior,approval.
3 - 5 Days 24 -A8 Hrs
Circle all that apply: Email , , Mail =,
pMERITECH INC
ENVIRONMENTAL LABORATORIES
642 Tamco.Rcl. Phone: [phone]
Reidsville NC 27320 Fax: [phone];522
Email:'[e-mail]
w erip h®ac hy
Sam" .le Location and or ID #
.Sam ili1 Dates & Times
gxPwat'
P { on Taking Sample SignJPri t): II
Lab Use Only
Start
End
Comp?
Grab?
# of
Cont.
�es�t(s)
(� (�
Required
On Ice?
Yp� µs �O
pH"OK.
Cl OK?
Date`
Time
Date
Time
Temperature Upon
Receipt:
Method of
Shipment:
* g* De -chlorination (<0.5 pprn) of ia, Cyanide, Phenol and TKN-samples must be done in the field prior to preservation.
Ammon
Comments:
Compositor #
[] UPS
lug #
Fed Ex
Are these results for regulatory purposes? Yes- No
Report results in: mg/L E{ mg/kg Q: ug/L Q
nd Delivery
R to fished by: Da
ii�.c w�.
e: Time:
h :
Received _by ��= 1 =--� ate: Time:
�y� ! gat/ %3' 3.�
Other
Relinquis / D Tune
Received by: n Date: Time:
Relinquished by: Dater Time:
Received-W La Date Time: � 9

CITY OF GRAHAM
WASTEWATER TREATMENT PLANT
GEOMETRIC MEAN CALCULATIONS FOR SLUDGE
503 B
SECOND QUARTER - 2014
DATE
RESULTS
UNITS
% DRY SOLIDS
May 6,.2014
10660
MPN/g.dry
1.97
May 7, 2014
10204
MPN/g.dry
1.96
May 8, 2014
1877
MPN/g.dry
1.92
May 13, 2014
4995
MPN/g.dry
1.84
May 14, 2014
4896
MPN/g.dry
1.84
May 15, 2014
4431
MPN/g.dry
1.83
May 19, 2014
2059
MPN/g.dry
1.75
GEOMETRIC MEAN =
4629
MPN/g.dry
1.87

:w
ate..
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Meraitech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date: 5/16/2014
NPDES#: WQ0003824
P.O.#: 2014001004
Date Sample Rcvd: 5/6/2014
Meritech Work Order # 05061456 Sample: Sludge Storage Grab 5/6/14
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.97 % 5/7/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 10,660 col/g dry wt 5/6/14 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
oratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3Q0-2013 Chain of Custody Record (COC)
NPDES#: G Ooe-_!:-�18 2
Client: of ���ahcy", YV Phone: �3 "S 70 - ^7 2.1
Addresses: �. ©. �1'" �S% Fax:_ 'S1 -.� d2.
(S{+'c l �J C o272,S� Email:
Project:
P.O.#:_ ao 1- 7 00 ) OO V
Turn Around Time*
Attention: l 1,- , ,� 4�iT1'\
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Emal (preferred}, Fax, Mail Std 1od 3-s ays 2�S
�'
MERITC C®
ENVIRONMENTAL LABORATORIES
642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or ID #
.Sampling ®ate58cT1I11eS
gd�wa
Person TakingSample(Sign/Print):
L. � d
Lab. Only
Start
End
Comp?
Crab?
# of
Cont.
�����5� Req r��
:.
On Ice? :•
xes
;pH OK?
Cl OK?
Date
Time
Date
Time
7.
Temperature Upon:
Receipt:
,l
Method of
Shipment:
*** Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field priorto preservation. ***
Comments:
Compositor #: ':
Jug#':
UPS
< Fed Ex
Are these results for regulatory purposes? Yes �.v% No
Rep results in: mg/L [ mg/kg U ug/L
Relinquished b Da
Time:
R by. DTime:a
-Other
`
quish b Da Time: .,�
'ZIr
Received by: Date: Time:
elinquished by: Date: Time:
Received by La Da Time:

Merxtech, Inc.
:, .. Environmental Laboratory
:. Laboratory Certification No.165
Contact: Cris Routh Report Date: 5/16/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2014001004
Graham, NC 27253 Date Sample Rcvd: 5/7/2014
Meritech Work Order # 05071435 Sample: Sludge Storage Grab 5/7/14
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
1.96 %
5/7/14
0-100 % ,
SM 2540B
Fecal Coliform (Sludge)
10,204 col/g dry wt
5/7/14
130 col/g dry wt
SM 9222D
I hereby certify that'l have reviewed and approve these data. ox�x
aboratoty Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-20-2013 Chain of Custody Record (COC)
��''•• 1_ ], p NPDES#: W 0 000 3RZ9
Client-fa.n Y�W�� Phone:,-5�76—�or%Z[
Address: _ u-2T � Fax: 33(. -- 5 f3 -S"e'6 2
,",JC Email:
Project:
I bc� r3o L J
P.O.#: � / � 1
l', �^ Turn Around Time*
Attention: � c�.� r `
*RUSH work needs prior approval.
How would you like your report sent?
Circle all that apply: Cma�il{preferred), Fax, Mail Std 10 s) 3-5 Da s 24-4sHrs
0=
MERITECH9 C'
ENVIRONMENTAL LABORATORIES
642 TamcoRd. Phone: [phone]
u
Reidsville NC 27320 Fax: 336=342-1522
Email: [e-mail]
�y C 1�-Y�1
WWW.r�2ritech-I�..1��7.c�1 1 1
Sample Location and/or ID #
Sampling Dates & Times
P g
Person Taking S p e (Si n/ rin :
C' 1r
I. "
Lab Use:O'raly
.. _
Start
End
Comp?
Grab?
#of
cost,
e5+(
Skequired
\ }
t. 0nIce?-
:Yes -:No
pH:OK?Date
t O
CIK?
Time
Date
Time
.Temperature,upon ,
Receipt.
Method of
Shipment:
*`* Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO samples
must be done in the field prior to preservation.'
Comments:
Compositor:#:-:." .
.. .. .
Jug #
[3: UPS
Q; Fed Ex
Are these results for regulatory purposes? Yes No
Report results in: mg/L [] mg/kg ug/L
% nd Delivery
Relirt i ed a
_
e Time:
So
Receiv by at� Time:
Other
C
Relin shed by: � D Time:
Received y: Date: Time:
Reihd bDTi h qusey: ate: me:
Received b DaTime:
b: te: Y i L

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 5/16/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2014001004
Graham, NC 27253 Date Sample Rcvd: 5/8/2014
Meritech Work Order # 05081446 Sample: Sludge Storage Grab 5/8/14
Parameters Result Analysis Date Reporting Limit Metho Qualifie
% Total Solids
1..92 %
5/9/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
1,877 col/g dry wt
5/9/14
130 col/g dry wt
SM 9222D B1
B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on
all filters reported per 100 in].
I hereby certify that I have reviewed and approve these data.
La oratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-=a2013
Chain of Custody Record (COC)
NPDES#: Q 0 63-39274
Client: a oT Q3fMhaA% YV +' i Phone: �3 L 570— 6 72i
Address:_ D o �c�f �� Fax: ��t�— 5 ��
3 Email:
Project:
P.0•#:� 00 GO- � I 1 LI
Attention: TumAroundTime*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email (preferred), Fax, Mail Std 10 s) 3-s Da s 124-48 Hrs
ME 1 1 �.
ENVIRONMENTAL LABORATORIES
* 642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-i(:ibs.coi I m 1
Sample Location and/or ID #
Dates 8c Times
-Sampling�.
Person Taking Sample Sign/Print):
Qwa : C(*
` e
:Lab. Us '.Only
Start
End
,
Comp.
Drab?
#of
Cont.
test(s) Required
'Ce'
o
p"°K 7
C1:OK?
Date
Time
Date
Time
o
Temperature Upon
Recei4ZIpt:.
Method of
Shipment:
* "* Dechlonnation (<0.5 ppm) of Ammonia, Cyanide, Phenol
and TO samples must be done in the field prior to preservation. **'
Comments:
Compositor.#;
[: UPS
Jug #
!: Fed Ex
Are these results for regulatory purposes? Yes
No
Report results in: m L
p g/ �r
m k u L (,
g/ g g/
;. and Delivery
Relinquished
Da
e: Ti
,
Rec 'v C
Date
Time: t
,
-Other
.,
P Qate: — i Time I *
V
Received by: Date:
Time:
Relinquished by: Date: Time:
Receivedy lab: �t�g:
) l Time,
i.3

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Report Date: 5/28/2014
NPDES#: WQ0003824
P.O.#: 2014001004
Date Sample Rcvd: 5/13/2014
Meritech Work Order # 05131450 Sample: Sludge Storage Grab 5/13/14
Parameters Result Analysis Date Reporting Lill Method
% Total Solids 1.84 % 5/15/14 0-100 % SM 2540B
Fecal Coliform (Sludge) .4,995 col/g dry wt 5/14/14 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
&ei�c
Laboratory Represe itative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COQ
//'�� aa NPDES#: 0 OOsS
Client: ' "� of(T3'ahan WdrP Phone: 336 -5 70 r C7 21
Address: 3S7 Fax: 3 "5 J 3 -550.-
cn1 Email:
Project:
P.O.#: �r' 1 `! 0,3
Attention: i�5 P-0 Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Emaii(preferred), Fax, Mail Std soda 3j-S�Da�js zra-a�sHrs
MERITECH, INC.
"` ENVIRONMENTAL LABORATORIES
642 TamcoAd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.col I �n !
Sample Location and/or ID #
Sampling Dates &TimesaroQ
P on Taking Sam le (Sign/Print):
Lab U.se:Q.nly
Start
End
Comp?
Grab.
ont
Cont.T6st(s)
Required
.Yes � No
C OK .
Date
Time
Date
Time
Temperature Upon
Receipt: "
Method of
Shipment:
*** Dechlorination (<0.5 ppm) ofAmmonia, Cyanide,
Phenol and TKN samples
must be done in the field prior to preservation.
Comments:
compositor #
#
UPS
Fed Ex
Are these results for regulatory purposes? Yes
No l
II��Jug
Report results in: mg/L mg/kg a ,F ug/L=
Q Delivery
and Delive
Relinquished
`
,Dat :,
Time: U
Received � %3 Time: / l /o
7
.... Other
Relinquis
� te3
Time: / 5•-/ O
Received by: Date: Time:
Relinquished by: Date:
Time:
Received by Lab f Date: Time:

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Report Date: 5/28/2014
NPDES#: WQ0003824
P.O.#: 2014001004
Date Sample Rcvd: 5/14/2014
Meritech Work Order # 05141409 Sample: Sludge Storage Grab 5/14/14
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.84 % 5/15/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 4,896 col/g dry wt 5/14/14 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data. �{
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-2a2023 Chain of Custody Record (COC)
NPDES#: W 0 b b p382`f
}
Client: D iz&10 ?lam ki k� Phone: �✓�� - �5 70- G 2 Z �
Address: i - �. Qs? 2i S5% Fax: .3��rs)3 55�2.
C3T^Olt) IJ C X22 Email:
Project: 11 �/
P.O.#: O 1 �� 1
s Turn Around Time*
Attention: ►S
How would you like
Email{preferred}, ayour report sent? *RUSH work needs prior approval.
Circle all that apply x, Mail Std l0 3-5 Da s za -aaHrs
INC.
ENVIRONMENTAL LABORATORIES
642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
a A p-�-�
VV W YV .rneritech-Iabs.C®1 i 1
Sample Location and/or ID #
_Sampling Dates & Times
Per,Taking Sample (Sign/Print): tea C ,
6a r�
Lab Use PIPIN
Start
End
?
Camp.
Grab?
ont
Cont.Test(s)
Required
ice? :`:pH.OK?.
Yes- No:
;'-.Cl OK?
Date
Time
Date
Time
j
3®
-kcA o &1 '
d
Temperature,Upon.
Receipt
Method of
Shipment:
* "` Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.***
Comments:
Compositor #.::.: .
Jug#
[ UPS
Fed Ex
? No �
Are these results for regulatory purposes. Yes
Report results in: m L ( mg/kg e ug/L
p g/
`
nd Delivery
Relinquished
Dat I Time
Received . � te:�i /i Time:
/ l
Other
_°��
Cam-
Relinquishe ate Time� 0:
� C;�
Received by: Date: Time:
,.
Relinquished by: Date: Time:
Received by ' _, " Date: Time:
Gv" � Z 1.3 Cc,

Meritech, Inc.
Environmental Laboratory
:.. Laboratory Certification No.165
7
Contact: Cris Routh Report Date: 5/28/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2014001004
Graham, NC 27253 Date Sample Rcvd: 5/15/2014
Meritech Work Order # 05151476 Sample: Sludge Storage Grab 5/15/14
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.83 % 5/19/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 4,431 col/g dry wt 5/16/14 130 col/g dry wt SM 9222D
0
I hereby certify that I have reviewed and approve these data. &OW
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax,[phone]

320--2013 Chain of Custody Record (COC)
NPDES#:_W Q 6 a 6�g,2�
Client: �' ��� ( �',°`f� ` Phorre: �34� - _ D— F,-72J
Address: �, 0 . z-a^, Y')-- �� Fax: 3-3(� - S 13 -. -70 2-
6-IT-011ko'n G 272-:�s Email:
Project: �
P:O.#:_ao J � 60) 0 er�!
r Turn Around Time*
Attention: l � �"
How would you like your report sent? *RUSH work needs prior approval.
5td iod 3-S Da s �a-a8Hrs
Circle all that apply: Email(preferred) Fax, Mail
MERITECH1 INC.
ENVIRONMENTAL LABORATORIES
- 642TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
e
WW Vv .meretech-labs.co 9 �Y1 1
Sample Location and/or ID #
Sampling ®ates &Times
Pe on Taking Sample (Si n/Pri t):
lab. Use: ®nly
Start
End
Comp?
Grab?
#of
Cont.
+0111Ce?
S 1(S)
Required
Ye Nol
Cl; OK?
Date
Time
Date
Time
✓ '� O
_
..
CA46Y
Temperature: Upon
Receipt::
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO samples must be done in the field priorto preservation. ***
Comments:
Compositor;#:.;
Jug #
UPS
Fed Ex
I Are these results for regulatory purposes? Yes =' No
Report results in: mg/L [ mg/kg ug/L �.
nd Delivery
Relinquished ate" Time: ; y.,
Reeeiv y: t¢-• Time:
Other
Relin b : ' / tej Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Received b La : Date: 11Tinei
R r' ��j{

Meritech, Inc.
aI<: Environmental Laboratory
Laboratory Certification No.165
I
Contact: Cris Routh Report Date: 5/28/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O*: 2014001004
Graham, NC 27253 Date Sample Rcvd: 5/19/2014
Meritech Work Order # 05191423 Sample: Sludge Storage Grab 5/19/14
Parameters
Result
Analysi�Date
Reporting Limit
Method
% Total Solids
1.75 %
5/21/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
2,059 col/g dry wt
5/20/14
130 col/g dry wt
SM 9222D
I
I hereby certify that I have reviewed and approve these data.
&' 62V(;
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
teI.(336)342-44748 fax.[phone]

Chain of Custody Record (COC)
NPDES,#:
0 .
Client- � w�& 6A)
chPhone, 57 0 6 2
'Address: S2 F..: 3-3f. SO 1
� Email:
Project:
P.'O,#: 00 00Y
Attention: Cr)"'s -JAk Turn Around Time*
*RUSH %voik needs prior approval.
How would you like your report sent?
'Circle all that apply: t7d11:0:d];?6) 3-5 Days 2s 4--kgHr
mail (preferred)Fax, Mail S=
MERITECH p INC.
ENVIRONMENTAL LABORATORIES
642 Tamco -Rd. Phone: .[phone]
Reidsville NC 27320 Fax:'336w3424522
Email: info@m'eritech-labs.com
www.meritech-tabs.com
Sample Location and/or ID #
sampling Dates & Times
i ign/ rint)-
P n Taking sample
to cGt,?tVc
. ........... ....
LaP USA Only
Start
End
COMP7
Grab?
It of
Cont.
e �t
(s)
R d
-equire
Ice?
Ye 0
OH OK?
CI OK?
----TTime
--Date
Date
Time
-qkA 6112. S-A 0 MA 2
67
R44 swoom— 27u+A-- &CILIA
Temperature upon
Receipt':
Method of
Shipment:
***.Dechlorination (<0.5 ppm) of Arnmonia,,Cyahide, Phenol and TKN samples must be done in the field prior to preservation.
Comments:
Compositor It
Jug it
Eli UPS
Fed Ex
Are these results. for regulatory purposes? Yes: Er No
Report results in: mg/L EJ, mg/kg ❑ uL
10nd Delivery
h
Relinquish
aReceived
3.0
a „Time:
4
Other
�-t ZZ !z
Received by: Date: Time:
relinquished by: Date: Time:
d Zb/i/l� <�-h

CITY OF GRAHAM
WASTEWATER TREATMENT PLANT
GEOMETRIC MEAN CALCULATIONS FOR SLUDGE
503 B
THIRD QUARTER - 2014
DATE
RESULTS
UNITS
July 8, 2014
1036
MPN/g.dry
July 9, 2014
3161
MPN/g.dry
July 10, 2014
1553
MPN/g.dry
July 15, 2014
1112
MPN/g.dry
July 16, 2014
3316
MPN/g.dry
July 17, 2014
1092
MPN/g.dry
July 21, 2014
2158
MPN/g.dry
% DRY SOLIDS
1.74
1.71
1.74
1.62
1.63
1.65
1.67
GEOMETRIC MEAN = 1718 MPN/g.dry 1.68

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 7/14/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357
Graham, NC 27253 Date Sample Rcvd: 7/8/2014
Meritech Work Order # 07081448 Sample: Sludge Storage Grab 7/8/14
Parameters Rgsults Analysis Date Reporting Limit Method
% Total Solids
1.74 %
7/9/14
0-100 %
SM 2540B
Fecal Coliform
1036 col/100 ml
7/8/14
1 col/100 ml
SM 9222 D
I hereby certify that I have reviewed and approve these data. it, &=C=
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
a
pWV)NPDEStt: W g
Client: l Of Phone: - —,:5,70 6
Address:f-,,-b 0,�, Fax.- 33� SO 2�
Email:
Project:
P.O.#:
Attention: CP it -S Turn Around Time"
*
How, would you like your report sent? RUSH. work needs prior approval,
48,Hrs
Circle all that apply. �Ernil (p�Wermd � Fax, Mail
MERITECH', INC.
ENVIRONMENTAL LABORATORIES
6423a�rncoRd. Phone: [phone]!
Reidsville NC 27M Fax: [phone]
Email: [e-mail]
www.meriteh-labs.com
Sarn'plb Location and/or ID #
Sampling Gates & Times
P M�on TakingSample(��' �n,/Pr�int)
AJ\CA ( n--, /E�Aw ckv--p
Lab Use Qnly
-
—— Start
End
Comp?
Grab?
N'of
Cont
R,eq u i redCge
on IcO
No
pH OK?.
Cl OK?
DateTTime
Date
Time
to-
f e-6 Soi'm— t —Ar� S6('4CL
—
-
J
Temperature Upon
Rly%eipt:
Method of
Shipment:
Dechlorination
(<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Comments:
Conioositor#
Jug ft.
EJ UPS
Fed Ex
Are these results for regulatory purposes? Yes, EK No�
p
Report results in: mg/L ug/L
mg/kg
_q'-HJ,'n'-dq [Delivery
Reli I nquishe Time:
QJ C
Recei y: All, Time:
Other
Relinquish Y! Time:
Received by. Date: Time:
Telhnquf�h—ed by�' /Dat—e Time:
71

Meritech, Inc.
Environmental Laboratory
::. Laboratory Certification No.165
Contact: Cris Routh Report Date: 7/17/2014
Client: Graham, Cityof NPDBS#: WQ0003824
P.O. Drawer 357
Graham, NC 27253 Date Sample Rcvd: 7/9/2014
Meritech Work Order # 07091471 Sample: Sludge Storage Grab 7/9/14
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 1.71 % 7/10/14 0-100 % SM 2540B
Fecal Coliforin 3,161 col/100 ml 7/9/14 1 col/100 ml SM 9222 D
I hereby certify that I have reviewed and approve these data, la
Laboratory Representative
1
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

-124=013 Chain of Custody Record (COC)
/r NPDES#: 0 O a
Client: "k e-F GAS W WV PhoneMERITECH%b- f
Address: U 3S-7 Fax: 336 -S /3 - SSO 2
�2- Email:
Project:
P.O.#:
Time*
Attention: Turn Around a 5 � .
How would you like your report sent? "RUSH work needs prior approval.
Circle all that apply. Email{preferred Fax, Mail Std 10 s) 3 5 Days 24-4SHrs
1 INC.
=' ENVIRONMENTALLABORATORIES6-A
642 TamcoAd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com m I
Sample Location and/or ID #
:Samp9ir>sg Dates &Times
Per n
akingSample Si Prin-p^.d
=gwa;r L.Ca� ; Q��
Lab..EDse only
Start
End
comp?
Grab?
#of
Cont.
Te t(S) Required
onace?
ye No
pH OK?
CI OK?.
Date
Time
Date
Time
0�0A '"-30.5
,
Temperature Upon
Receipt:
aA `,. -
Method of
Shipment:
"" Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field priorto preservation. * "*
Comments-
Compositor .#
} UPS
Jug #
Fed Ex
Are these results for regulatory purposes?. Yes 41, No Q
Report results in: mg/L [ g/ Q: ug/L Q'
Q; and Delivery
Reli u ed � • ate: Time:
l� e 9 �7 (`
Rec ' ed by: Time:
Z
Other
Reli wished by: e/
Receive by: D e: Time:
Relinqui ed by: Date: Time:
Received by 4 b: Date;, Ti

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Cris Routh Report Date: 7/17/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357
Graham, NC 27253 Date Sample Rcvd: 7/10/2014
Meritech Work Order # 07101410 Sample: Sludge Storage Grab 7/10/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
1.74 %
7/11/14
0-100 %
SM 2540B
Fecal Coliforin
1,553 col/ g dry
7/10/14
1 cal/100 ml
SM 9222 D
I hereby certify that I have I•eviewed and approve these data,
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-20-2013 Chain of Custody Record (COC)
NPDES#: ..7
Client. a . "s�-�, w WTf Phone: -S,3� -�%O - 6 7Z11
Address: o • �y'C }� _ Fax: �1 " 5)3 - S-S02
�'j`� a, �i C 27 Email:
Project:
P.O.#:
Turn Around Time*
Attention: t .5
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email(preferred Fax, Mail Std lOd 3 3-5 Dates 2�s
INC.
ENVIRONMENTAL LABORATORIES
' 642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.co 1 1
Sample Location and/or ID #
.Sampling Dates &Timesi��wq�r�P
P son Taking Sample Sign/Print): i ``
L. �a� i°e d
Lab Use: Only
Start
End
comp?
Grab?
#of
Cont.
tes"t(s) Required
Ice?
y / No.
..
pH OK?
Cl OK?
Date
Time
Date
Time
da 4�"
1iC
o U ap
Temperature Upon
Receipt:
Method of
Shipment:
*** Dechiorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO samples must be done in the field prior to preservation. ***
Comments:
-
Compositor #
Jug#
D UPS
Fed Ex
Are these results for regulatory purposes? Yes No D:
Report results in: mg/t mg/kg ug/L>
talid Delivery
Relinquishe y: Dat
%(7Ca Z O
Time
f �� .
Re ed r Date; Ti e:
M Other
R Ch by ✓ w f �Dat� Time:�.��
Received by: Date: Time:
Relinquished by: Date: Time:
eived 7-1 Aate
Tim
i

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh
Client: Graham, City of
P.O. Drawer 357
Graham, NC 27253
Meritech Work Order # 07151414 Sample: Sludge Storage Grab
Report Date: 7/22/2014
NPDES#: WQ0003824
Date Sample Rcvd: 7/15/2014
7/ib/ i4
Parameters
suits
Analysis Date
ReportingLimit
Method
%Total Solids
Fecal Coliform (Sludge)
1.62 %
1,112 col dry wt
/g y
7/16/14
7/15/14
0-100 %
130 col/g dty wt
SM 2540B.
SM 9222D
I hereby certify that I have reviewed and approve these data,
Laborato►y Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

}zo-zo,3 Chain of Custody Record (COC)
NPDES#: W Q 0o/)_3 9Z14
l� ` �j-�`Q L-1 Jb
Client: i t�� � �'`� Phone:
Address aap ^a.u-erS� Fax:
� � Email:
Project:
P.O.#:
�'� D _ Turn Around Time*
Attention: T-,E� *RUSH work needs prior approval.
How would you like your report sent?
Circle all that a 1 Email (preerre Fax, Mail Std 10 s} 3-5 Da s 24-asHrs
apply:(
MERITECH, INC,
y E14VIRONMENTAL LABORATORIES
642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
e !, /
W VV �!V .r�eriteeh-9abs�C�l 1 l
Sample Location and/or ID #
.Sampling ®aces & Times
Pers akingSamp (S /Pri t}�
j
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
T sts)
Required
on Ice?
Yes / Na
pH OK?
Cl OK?
Date
Time
Date
Time
1' ©C_
Temperature Upon
R eiot:
Method of
Shipment:
*** Dechlorination (<O.S ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field priorto preservation. **'ii
Comments:
Compositor #
lJUg#
D UPS
Fed Ex
Are these results for regulatory purposes? Yes NoQ_
Report results In: mg/L [ mg/kg ug/L Lam.
Q d Delivery
(Relinquished ^�
d(
e: `� Time: �D
a —1
Received by: D te- Time: 'moo
Other
'
Relinquishe D S Time: / / 3 O
eceived by: Date: Time:
Re inquished by: Date: Time:
I W66NvelLab• r c 11 91te: 1 1� to )

Meritech, Inc.
y Environmental Laboratory
Laboratory Certification No.165
r � d
Contact: Cris Routh Report Date: 7/22/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 Date Sample Rcvd: 7/16/2014
Graham, NC 27253
Meritech Work Order # 07161492 Sample: Sludge Storage Grab
7/16/14
Parameters Results Analysis Date Reporting Limit Methi2d
% Total Solids 1.63 % 7/18/14 0-100 % SM 2540E
/g d
Fecal Coliforrn (Sludge) 3,316 cotr 7 16 14 130 col/g dry wt SM 9222D
Y wt //
1 hereby certify that 1 have reviewed and approve these data. A ' A /
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

o-zo�
Chain of Custody Record (COC)
NPDES#: W Q06031929
Client: r"a a Phone:33� —� 7�
Address: . Fax: 3�(� 5 '-�55O
co, C 7 Email:
Project:
P.O.#:
Attention: �,' i k Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply Email {preferred}) Fax, Mail Std 10 d s 3 - 5 Da 5 24-48 Hrs
Pe n Taking Sample (Sign/Print}: • t
Lab lJse ®a31y
MERITE ! INC.
ENVIRONMENTAL LABORATORIES
642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email:'[e-mail]
r
www. a 11 e itec h—labs - C o m
Sample Location and/or ID #
.Sampling Dates & Tamales
Start
End
Comp.
?
Grab?
#of
Cont.
test(S)
p g r
Required
n Ice?
Yes No
pH OK?
Cl OK?
Date
Time
Date
Time
r
Temperature Upon
Receipt:.
'! .
Method of
Shipment:
** Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples
must be done in the field prior to preservation. ***
Comments:
Compositor#
Jug#
[�. UPS
Fed Ex
Are these results for regulatorypurposes? Yes
No C
Report results in: mg/L [ ." mg/kg ug/L
2. and Delivery
Relinquished
i �t
:�
Time: /�R
�C/YA
Received b-- t�
Time: 3 O
Other
Relinquish Date: /
T17e z O
R ceived by: Date: Time:
Relinquished by: Date: Time:
Received by._L_ab_ 1 Time:
a_

Mer. iteclh, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 7/29/2014
Client; Graham, City of NPDES#: WQ0003824
P.O. Drawer 357
Graham, NC 27253 Date Sample Rcvd: 7/17/2014
Meritech Work Order # 07171423 Sample: Sludge Storage Grab 7/17/14
Parameters Results Analysis Date Reporting Limit Method
Total Solids 1.65 % 7/18/14 0-100 % SM 2540B
Fecal Coliform 1,092 col/ g dry 7/17/14 1 col/ g dry SM 9222 D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-:0-:013 Chain of Custody Record (COC)
! NPDES#: OUD ' 2 1
Client: � C.vr% tI^►W Phone:: � /6 ' �7� — 7Z1
Address: �py w 1 37 Fax:S1�—�So2-
�•siraj-�a.� c 2�3 Email:
Project:
P.O.#:
Attention: Cr, s S Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply Email (preferred) Fax, Mail St d 7Oda 3-5 Da s 24-48Hrs
�`
ITEM +®
"u'i"" ENVIRONMENTAL LABORATORIES
" 642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates & Times
`
p� T king �ample (Si n�Print. cc� �wav� �. ^, � �
Lab Use `Qply
Start
End
comp?
Grab?
#of
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® �j
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on Ice?
Yes No
pH OK?
G.0K.'
Date
Time
Date
Time
1
Cagy 4-
J^ O
o
Temperature. Upon
Receipt
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in thefield priorto preservation. ***
Comments:
Compositor #....:.
JJug#
[] UPS
Q` Fed Ex
Are these results for regulatory purposes? Yes No Q
Report results in: mg/L [:J-: mg/kg Q ug/L
nd Delivery
Relinquis /•
ie: Time: 1ya
eve
Reteiv te: Time:
�t%2�
- ` Other
C�-r
Relin ash Date: ime: s /y
! / "
Received by: Date: Time:
Relinquished by: Date: Time:
Received by Lab: Date: Time:

Meritech, Inc.
:..: Environmental Laboratory
s Laboratory Certification No.165
Contact: Cris Routh Report Date: 7/29/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2015000016
Graham, NC 27253 Date Sample Rcvd: 7/21/2014
Meritech Work Order # 07211425 Sample: Sludge Storage Grab 7/21/14
Parameters
Results Analysis Date Reporting Limit Method
% Total Solids
1.67 %
7/22/14
0-100 %
SM 2540B
Fecal Coliform
2,158 col'/ g dry
7/21/14
1 col/ g dry
SM 9222 D
I hereby certify that I have reviewed and approve these data. (C. &&2
Laborato►y Repre entative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Chain of Custody Record (COC)
( NPDES#: Q D oO 3 2
Client: , of �TS`c�o�n iJ W J !p Phone:MERITECH,
Address: O S% F2X: J� �3 --'\So�2-
l 01-, C- �7 3 Email:
Project: t
P.O.#:
Attention: & ►s Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Email (preferred), Fax, Mail std 1od 3-5 Da s 24-48xrs
INC.
ENVIRONMENTAL LABORATORIES�
642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com 1
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign Print):
,2co C�'s �du?,/a�
Lab.Use Only
Start
End 'Comp?
Grab?
#of
Cont.
1 eSt(S) Required
Ice?
No
pH OK?
tIOK?
Date
Time
Date
Time
Li
T--T
Temperature Upon
Receipt:
Method of
Shipment:
*'* Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO samples
must be done in the field prior to preservation.
Comments:
Compositor #:
Jug#
UPS
Fed Ex
Are .these results for regulatory purposes? Yes No ice:
Report results in: mg/L mg/kg Q� ug/t
d Delivery
Relinquished by: �� D te: Time:
I Received by: Date: Time:
Other
iNA
Relinquished by: Da'e: Tide:' .
�n"�L Z / �Y
Received b . e j Time:
Relinquished-� +� ate: Ti
27/1
Receiv y b a Tim

CITY OF GRAHAM
WASTEWATER TREATMENT PLANT
GEOMETRIC MEAN CALCULATIONS FOR SLUDGE
503 B
FOURTH QUARTER - 2014
DATE
RESULTS
UNITS
% DRY SOLIDS
October 7, 2014
6696
MPN/g.dry
1.48
October 8, 2014
2792
MPN/g.dry
1.55
October 9, 2014
6902
MPN/g.dry
1.55
October 14, 2014
2403
MPN/g.dry
1.50
October 15, 2014
<699
MPN/g.dry
1.43
October 16, 2014
4412
MPN/g.dry
1.36
October 20, 2014
1945
MPN/g.dry
1.39
GEOMETRIC MEAN =
3723
MPN/g.dry
1.47

Meritech, Inc.
-; 4= Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 10/22/2014
Client: Graliam, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 201500236
Graham, NC 27253 Date Sample Rcvd: 10/7/2014
Meritech Work Order # 10071473 Sample: Sludge Storage Grab 10/7/14
Parameters
Results
Analysis Date
Reporting Limit
Method
%Total Solids
1.48 %
10/8/14
0-100 %
SM 2540B
Fecal Coliform
6,696 col/ g diy
10/7/14
1 col/ g dry
SM 9222 D
I hereby certify that I have reviewed and approve these data.
LaboratmyRepresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-21 2013
Chain of Custody Record (COC)
,gip NPDES#: ifs Qa00�$� 1
Client: ia� . = ,G-"��°4`'3y Phone: �36v SZO-G72f
Address: - ar' w-R i ---sS 7 Fax:
�-r�`�1Cv�^, iV� %372,� Email:
Project:
P.O.#: 15 06 O
Attention: ^:`s —p'--u r, Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent?
Circle all that applyStcl. Email (preferred), Fax, Mail io 3-5 Da s 24-48Hrs
; o
ENVIRONMENTAL LABORATORIES
'' •. 642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: info>ameritech-labs.com
� p �` � p , �+ ,
V!/ �Jl� �° ,meritech-labs.co !
Sample Location: and/or ID #
.Sampling Dates & Times
P on Takin SamplQ (Sign/Print):
l '�' t,vc �.. �4.�.
Lab Use ®n[y
Start
End
?
Comp.
Grab?
.. of
+
Cont.
..
Required
7
ceTest(s)
Yes: No
?
pH OK.
CI OK?
Date
Time
Date
Time
,y
C�
Cak.� t
I
i
f
E
1
Temperature Upon
Receic�t ,
Method ©f
Shipment:
( *** Dechlorination (<o.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples must be done in the field priorto preservation.
[Comments:
-
Compositor #
Jug #
UPS
Fed Ex
Are these results for regulatory purposes? Yes
` No Report results in:
mg/L [ mg/kg ❑ ug/L
nd Delivery
Re?' ettShed by r Date:
{�LdX�- -i
Time:, ,_ 1Re iv Dy:
.�' .t �.-�i.v
-- Dale Time-
✓ '/ ,
Other
�.
Reim isp' d by: Date:
�V ..2�-�` �/ /�
iime• Received by: /
/ e
Date: Time:
Relinquished by: Date: lime: •Received b b:
,t te: Lf Ti7. 1 `

Merltech, Inc.
_.- Environmental Laboratory
Laboratory Certification No..165
:y
Contact: Cris Routh Report Date: 10/14/2014
Client: Graham, City of NPDCS#: WQ0003824
P.O. Drawer 357 P.O.#: 2015000236
Graham, NC 27253 Date Sample Rcvd: 10/8/2014
Meritech Work Order # 10081453 Sample: Sludge Storage Grab 10/8/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.55 % 10/10/14 0-100 % SM 2540B
Fecal Coliform 2,792 col/ g dry 10/8/14 1 col/ g dry SM 9222 D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel:[phone] fax.[phone]

320.202 Chain of Custody Record (COC)
NPDES#: W'Q 000 SUI
Client: C:41 d r�M Vic.Phone: 33C — 570— b, 211
Address: 3S� Fax:
Gb'GZ.bC, ! \;• C. --7 . '�3 Email:
Project:
P.O.#: 0 06 a-3�
.� ` Turn Around Time*
Attention: ��
*RUSH work needs prior approval.
How:would you like your report sent?
^�- , Sid 10 s) 3 - 5 Da s 24 - 48 H rs
Circle all that apply, Email (preferred �, Fax, Mail
INC,
ENVIRONMENTAL L6ai3®RA.TOk36ES
642 Tamco.Rd. Phone: [phone]
` ReWsvifle NC27320 Fax:336-342-'!522
Email: [e-mail]
@
�A� / , {� c
VW w y e t N e ec1 -lab 3, C®m
Sample Location and/or ID #
.SarnpSing.Dates arc Tirnes
Pt on Taking Sample
ign/Print):
•0 a �' � � �. 'c` e�
�.
Lab Use Only
Start
End
Comp?
Crab?
# of
Cont.
�S.(S)
.Req I Y �d
Ice?
Yes o
pH OK?
Cl: OK?
Date
Time
Date
Time
C -- �-- :-J R
Temperature Upon
Receipt:
Meth©d of *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO samples must be done in the field prior to preservation.
;Comments:
Shipment:
UPS
Compositor #
Jug# `
Fed Ex Are these results for regulatory purposes? Yes � No L,r
:Re port ,esuIts in: m g/L rri /kg [�` u g/L
G� g
Reli u ed by: t ate: Tme:
q Nand Delivery �p
Re e ���� Dates Time: ,,1
,
�j.4 G — d'-% d'
Other $Relic uis., " by ) i G} �Da*pG/ Time:
r''�^ . quished by Date: Time:
DA tom+` c �r
Received by: Date: Time:
Reteiv�) ^y ;L Da e 11 Time:

-Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Cris Routh Report Date: 10/13/2014
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O.#: 2015000236
Graham, NC 27253 Date Sample Rcvd: 10/9/2014
Meritech Work Order # 10091432 Sample: Sludge Storage Grab 10/9/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.55 % 10/10/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 6,902 col/g dry wt 10/9/14 130 col/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
i
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax,[phone]

3.20-201
Chain of Custody Record (COC)
NPDES#:
Client: Phone:_ 3� S r �7f6 —
__�
Address: 5 357 Fax: —.s —_s5(32
�� 4`C�'1 t?��e �} �. �� 2Q Email:
Project:
P.O.#: 500o
Turn Around Time*
Attention: *RUSH work needs prior approval.
How would you like your report sent?
Circle all that apply=(pref�,red),,%Fax, Mail Sid 10 s) 3-5 Da s 24-48Hrs
-
®
ENVIRONMENTAL LABORATORIES
" 642TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
wA=��eritec—ab�7=c®
Sample Location and/or 1D #
Sams➢ink ®ales Times
Pe n
Taking SampI ign/Print):
��V
Lab Use Only
Start
End
Comp.
Grab?
, cn
*o,
Cont.
tes't'(s)- Required
lce?:
ye No
:pH OK?
Cl OK?
Date
Time
Date
Time
7.
i
Temperature Upon
Receipt
, .
MethOC� O )
Shipment:
" "* Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples must be done in the field prior to preservation. ***
Com ments:
,
Compositor #
[]: lJ PS
Jug #
Fed Ex
Are these results for regulatory purposes? Yes
" ND 0Report
results in: mg/L [ mg/kg ug/Li
and Delivery
Reanquishe ay: , Dale,
/ `' j
Time:
3 ®
Received by: Da Time:
�-- /p /z �33e7
Other
-
RelinGuis; �/ /�>D a e
Time ,
Received by: Date: Time:
�.36incaished by: Date:
Time:
. 4 oy b j _
�y

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 16 5
............ ............
Contact: Cris Routh Report Date: 10/22/2014
Client: Graham, City of NPDESft: WQ0003824
P.O. Drawer 357 P.OA 2015000236
Graham, NC 27253 Date Sample Rcvd: 10/14/2014
Meritech Work Order# 10141491 Sample: Sludge Storage Grab 10/14/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
1.50 %
10/15/14
0-100 %
SM 2540B
Fecal Coliform
2,403 col/ g di'y
10/14/14
1 col/ g dry
SM 9222 D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3*0-2033 Chain of Custody Record (COQ
NPDES#-0,003S;t
'W 0 -4
W W1
-72 Client: Phone: a3G 570 - ra1
V
Address: Fax: 336 5
Email:
Project:
P.O.#:
Attention: Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Fax, Mail StAL10 -�K 3-5 Da S 24 - 42 Hrs
M mr. p INC.
ERITECH
ENVIRONMENTAL LABORATORIES
642 T a mco -Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or!D #
sampling Dates & Times
Pe Taking Sample (Si Pri
caw 4;\d
Lab Use O.nly
Start
End
Comp?
Grab?
Hof
Cont.
Test(s) Required (..Lesy
On Ice?
No
pH OK?
C1 OK?
--D—a—te-7
Time
Date
Time
0
Temperature Upon
method of
Shipment:
Dechlorination (<03 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Comments:
Compositor #
IjLlg#
El:% UPS
Fed EX
Are these results for regulatory purposes? Yes V No
Report results in: mg/L [ l- mg/kg ug/L
and Delh,
R e! ir nq 'P"h P d b Y: e 71 ,
C Da 7� _3 o,
--dL '2 AN
R Date- Time
/0 -741-19
Dther
'C�
Relinq�,-��d by: 1<7 aj!� Tirne:-.1
R _ / 6"
Received by: Date: Time:
Rclinquishd by: Date: Time:
Rec Tim

Meritech, Inc.
:y. Environmental Laboratory
Laboratory Certification No. 165
Contact: Cris Routh Report Date: 10/22/2014
Client: Graham, City of NPDCS#: WQ0003824
P.O. Drawer 357 P.O.#: 2015000236
Graham, NC 27253 Date Sample Rcvd: 10/15/2014
Meritech Work Order # 10151465 Sample: Sludge Storage Grab 10/15/14
Parameters
Results Analysis Date Reporting Mini Method
% Total Solids
1.43 %
10/16/14
0-100 %
SM 2540B
Fecal Coliform
< 699 COI/ g dry wt
10/15/14
699 col/ g dry wt
SM 9222 D
I herebycer•ti that I have reviewed and approve these data. et, f-al-�
fY Np
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

'-- '---- --- r------ --
C' Email:
Attention: C-r 3,"5 0A Turn Around Time*
*RUSH work needs prior approval.
How would you like your report sent? - .
Circle all that apply:(�-:r7Ya-il—(p,,—fe-,-e-d')"4, Fax, Mail
ENVIRONMENTAL LABORATORIES
Email: [e-mail]
www.meritech-labs.com
Sample Location and/or ID #
Sampling Dates & Times
P T;'King S mple
n dA
Lab Use Only
Grab?
Cont.
e'stf(s) Required
Cl OK?
Date
I Time
Date
-rime
Temperature Upon
Dechlorination (<0.5 ppm) of Amry henol andTKN samples must be done inthefield priorto preservation.
Fornments:
Compositor
Fed Ex A re these results for regulatory purposes? Yes N o ED,
Report results in: -g/L mg/kg ug/L
by: Date:" Tirne
Recelv me
Other ICI Timevz
Relinquished by: Date: Time:
Received by: Date, Time:
Received by Lab: i� ate, Time-

Meriiech, Inc.
Environmental Laboratory
Laboratory Certification No.165
3
M1 .:ar
Contact: Cris Routh Report Date: 10/28/2014
Client: Graham, City of NPDCS#: WQ0003824
P.O. Drawer 357 P.O.#: 2015000236
Graham, NC 27253 Date Sample Rcvd: 10/16/2014
Meritech Work Order # 10161428 Sample: Sludge Storage Grab 10/16/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
1.36 %
10/17/14
0-100 %
SM 2540B
Fecal Coliform
4,412 col/ g dry
10/16/14
1 col/ g dry
SM 9222 D
I hereby certify that I have 1•eviewed and approve these data. (41 mt-�a
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
i tel.[phone] fax.[phone]
I

3-20-=W
Chain of Custody Record (COC)
NPDES#: (. ' oao 3924
Client: Cl 4 - L rur) '" Phone: 336 - 70 - (97,2-f
INC.
Address: 9, D , Fax: S�Z
'
ENVIRONMENTAL LABORATORIES
�`c�1Q� N' d 27253 Email:
642 TamcoRd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#: 15 Cd(3,236
Email: [e-mail]
AttentionJ k Turn Around Time*
gY ti �f��`���, mer,itech-f abs. co
*RUSH work needs prior approval.
How would you JiiCe your report sent?
I 1
Circle all that appl .Email (preferred} Fax, Mail Std 10 d `) 3- 5 Da 5 24-48 Hrs
Sampling Dates & Times
PTaking Sample n/PrintL.
AFA Lab 11se-Only
Sample Location
and/or ifs #
Start End
.
pH OK?
comp? #of s� s) Required
Grab? Cont. i red
Date
Time
Date
Time
No CI OK.
Gd
t`c r
OG I6 j
%7 i+!Gc.,ta
ctb
t
i
1
1 Temperature upon
1
Method of :
3 _ jY' Rc
i *** Dechlorination (<0.5 ppm) of�mmonia, Cyanide, Phenol and T(N samples must be dorie in thefield prior to preservation. t
*** S
a
Shipment:
? comments:
I
Compositor #
1:5. u as
Q- Fed Ex'i
,are these results for regulatory purposes? Yes
Jug #
No � � Repo lilts in: mg/L [� mg/kg ug/L
nj &RR�kJtYCi `• Da •e: Ti
,Uand Delive. �� f3 �R" e Time:
Other
sSe!in Date -,(4 Ji e:
-� ceived by: .. Date: Time:
_
�e!inquished b .
i Y' Date: Time:
eoved� 1 —

Meritech, Inc.
_-
Environmental Laboratory
Laborator Certification No.165
Contact: Cris Routh
Report Date:
10/28/2014
Client: Graliam, City of
NPDCS#:
WQ0003824
P.O. Drawer 357
ROA
2015000216
Graham, NC 27253
Date Sample Rcvcl:
10/20/2014
Meritech Work Order # 10201413 Sample: Sludge Storage Grab
10/20/14
Parameters
Results Analysis Date Reporting Limit
Method
%Total Solids
1.39 %
10/21/14
0-100 %
SM 2540B
Fecal Coliform
1,945 col/ g dry
10/20/14
1 col/ g dry
SM 9222 D
1 hereby certify that 1 have reviewed and approve these data. t X
- Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-20-2033 Chain of Custody Record (COC)
NPDES#: � © 6CL3&2L1
Client: y ' ' �`�+^ Phone:—:;-570 - 72 i
Address: .. 0 . c�sN�c'T 3 Fax: 33b --5S3- sSQ2
�^>-+``�,-, § a 7253 Email:
s.''
Project:
P.O.#: v'C S DOo�
Attention: �`+� �C Turn Around Time*
How would.you Nke your report sent? *RUSH work needs prior approval.
''�..
Circle all that apply: xmaiitpreferred)q Fax, Mail Std 10 s) 3-5 Days 24�48Hirs
MERITECH1
,.: ENVIRONMENTAL LABORATORIES
° 642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
��p�� ,,++ �y r'Y�
V°f 'V!J;'�` . _ eritech-labs.co ! !
Sample Location and/or ID #
Sacr>Ig�llrag ®ayes Times
Pei Taking Simple (Si n/Pr', ):
� �
Lab Use Only
Y
Start
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,
Comp.
Grab?
# of
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Y No
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Date
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s G
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
lCorm-nents:
1
Compositor #
lug #
❑: UPS
Fed Ex Are these results for regulatory purposes? Yes No
Report results in: mg/L ing/kg ug/L<
l�l Rebv: Date Time:
li .ed
` ` and Delivers -a` D ZO I ���3
Sy. a T• e:
eceived bD
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t^elinGnishedby: Date: Time:
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�: 6
Receiv vLaba: Date: Time:

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Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.38
9.38
9.30
9.13
9.10
8.84
8.69
8.53
8.21
8.02
7.58
7.32
7.11
6.91
GRAHAM WWTP
W00003824
3/23/14
11.1
3/23/14 1435
SS
3/23/14 1443
SS
1.6
12.3
15.1
Yo Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.17
Intercept: 9.7
i Correlation Coefficient: 0.98
Oxygen Uptake Rate: 10.40 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.65 mg Oxygen/hr/g
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.50
Temperature Corrected Specific Oxygen Uptake Rate: 0.98 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

12
10
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E
0
0
0
Lh
0 4
K
N
Oxygen Uptake Rate Chart
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Time (minutes)
12 13 14 15 16

Vector Attraction Reduction
Option 4 - SOUR
GRAHAM WWT
DIGESTER:
DATE:
P SOUR TEST
TEMPERATURE AT COLLECTION: I i I �- j C4, q I
j �rl
DATE/TIME COLLECTED: 1I�� I i L� �,(� '
SAMPLED BY: �~ -
ANALYSIS BEGAN DATE/TIME:-
ANAI Y71=n RY-
� I -, r
ANAYLSIS ENDED DATE/TIME; ``�`
o ;
BEGINNING SOUR TEST TEMPERATURE: ' 3 C _
ENDING SOUR TEST TEMPERATURE: I C'
Time in Minutes
D.O. mg/L
0
9,.a19
1
2�
3
4
a
5a
6
�A
7-6
8
�3
9
9.11
10
11
12
7
13
b,
14
15
6 ae��

SAMPLE DATE- ��-� -- �. I c r-ck - J Lf
DIGESTER DATA
,.�.�E..,.,,..,,,,..,,..,.,,..,,.,,.,,,..,......,,,.,,,,,.,.,......,....,,,,.%
„DIGESTED #1,.,,..., SAMPLE
AIR:
TEMP. -
° CELSIUS
PH
DO-
mg/L
ALKALINITY - mg/L
NH3N-
mg/L i
TSS -
�� mg/L
VSS -
�` mg/L
DIGESTER #2
SAMPLE TIME: I
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
°`CELSIUS
mg/L
DIGESTER #3 SAMPLE TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
mg/L
_mg/L
_mg/L
_mg/L
mg/L
Sample Date-
DIGESTER # 3
Volume Used - 25 mi. n
Date In Oven- %') ) m'V'Gk - Date Out of Oven-
Time In- L) 0 -P t" , Time Out- 7 -
Weight of Dish- LI , ) 3 �), 0 gm. (B)
Weight of Wet Solids + Dish- �� 0 b gm. (C)
Weight of Dry Solids + Dish- 9 i - D gni. (A)
Calculations:
(A) 9 � , 1 % -dill. - (B) . J�1 gm.
% Dry solids= ---------------------Divided By------------- ---------- x 100
(C) 6 S 7 90� gm.- (B) N I l gm.
® -3(Z,5 7 gin.
DIVIDED BY-------)X 100 = ) ^ % TOTAL DRY SOLIDS
PI -I-) , Do cS( gin.
Sant I Date -
DIGEST R #
Volume Used - 25 mi.
Date In Oven-� Date Out of Oven -
Time In- Time Out -
Weight of Dish- giu.(B)
Weight of Wet Solids + Dish- gin.
Weight of Dry Solids + Dish- gm.
Calculations:
(A) gm. - (B)
% Dry solids= ---------------------Divided By ------------
(C) gin - (B)
(---------- DIVIDED BY-------)X 100 =
gin.
(C)
(A)
x 100
% TOTAL DRY

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature:
Dissolved Oxygen Level
8.671
8.25
8.04
7.76
7.54
7.28
7.03
6.74
6.51
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
W00003824
3/29/14
10.5
3/29/14 1112
SS
3/29/14 1120
SS
1.6
13.0
15.1
0.21
9.5
0.99
o Dry Solids
degrees Celsius
Degrees Celsius
12.47 mg Oxygen/hr
0.78 mg Oxygen/hr/g
14 degrees Celsius
1.50
Temperature Corrected Specific Oxygen Uptake Ratej 1.17 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

12
10
2
I
Oxygen Uptake Rate Chart
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V
Mv
IF
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ES
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1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16

Vector Attraction Reduction
Option 4 - SOUR
DATE: 0'- 1 I OU`CY1 ' 1 1
GRAHAM WWTP SOUR TEST
DIGESTER: 3
a °
TEMPERATURE AT COLLECTION:
DATE/TIME COLLECTED:31 ' -1 h 4 —
SAMPLED BY: S
ANALYSIS BEGAN DATE/TIME:
ANAI Y7_ED BY: �S
c".:3 j 2q ), y
�,;t I f I. I7 fl�
ANAYLSIS ENDED DATE/TIME: <3). ) 4
° s5
BEGINNING SOUR TEST TEMPERATURE: 1.2- i ) ILI
o
ENDING SOUR TEST TEMPERATURE: C
Time in Minutes
D.O. mg/L
0
i�rJ
1
_I o alG
2
3
4
,g
5
6
g, Lia
7
gaX-s
s,U
9
, "� 6
10
r 5
11
12
13
14
15
��

SAMPLE DAT E-
0� I
DIGESTED #1 SAMPLE TIME:
AIR:
TEMP. -
° CELSIUS
PH -
DO-
mg/L
ALKALINIT -
mg/L
NH3N-
mg/L
TSS -
mg/L
VSS -
mg/L
DIGESTER #2 SAMPLE TIME:
AIR:
TEMP. -
° CELSIUS
PH -
DO-
mg/L
ALKALINITY -
mg/L
NH3N-
mg/L
TSS -
mg/L
VSS -
mg/L
DIGESTER #3
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
Sample Date-`% ' �� l cJY
DIGESTER # 3
Volume Used - 25 mi. 1
Date In Oven- �� r I, \c',ItW 4 Date Out of Oven- �� I -
Time In- 1 f ' ),5 Time Out-
Weight of Dish- 9 ) , S3 gm.(B)
Weight of Wet Solids + Dish- (o y� - �S? g gm.(C)
Weight of Dry Solids + Dish- I qI gm. (A)
Calculations:
(A) �, I j gm. - (B) 1 gm.
% Dry solids= ------------ -------Divided By------------------------ x 100
(C) 6 -5 , S 78 gm.- (B) 9 f , S,31 Z gin.
3 S03 gm.
(---------- DIVIDED BY-------)X 100 = 1 d % TOTAL DRY SOLIDS
1.1_I , S X� (� gin.
Sample Dat -
DIGESTER
Volume Used - 2 mI
Date In Oven- Date Out of Oven -
Time In -
Time Out -
TIME: Weight of Dish- gm.(B)
CELSIUS
_mg/L,
_mg/L
mg/L
Weight of Wet Solids + Dish -
Weight of Dry Solids + Dish -
Calculations:
(A) gin. - (B
% Dry solids= ---------------------Divided B,
(C) gm.- (B)
s (---------- DIVIDED BY-------)X 100 =
n. (C)
n. (A)
gm.
-------------- x 100
gill.
% TOT\ALIDRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.1
7
7.67
7.42
7.25
7.04
6.4
6.2
6.0
58
5.5
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
3/29/14
11.5
3/29/14 1501
SS
3/29/14 1505
SS
1.6
13.4
16.4
0.23
8.8
0.99
Dry Solids
legrees Celsius
legrees Celsius
13.95 mg Oxygen/hr
0.87 mg Oxygen/hr/g
15 degrees Celsius
1.40
Temperature Corrected Specific Oxygen Uptake Rate:1 1.22 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
F-11
FA
�
�
4
3
2
1
Oxygen Uptake Rate Chart
IM
V
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WE
ISM
WAS
Mr
wt
WASS
El -
IF
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1 2 3 .4 5 8 7 8 Q 10 11 12 13 14 15 18
Time (minutes)

�-
Vector Attraction Reduction t
Option 4 - SOUR DATE: �'� _ GLrG
- 1
GRAHAM VI WTP SOUR TEST
DIGESTER: �
` o '
TEMPERATURE AT COLLECTION: l C 3)19 j 11 --t
DATE/TIME COLLECTED: 3�
SAMPLED BY: I L
ANALYSIS BEGAN DATE/TIME: -3 5 P
ANALYZED BY: S�
ANAYLSIS ENDED DATE/TIME: a- `' 3 - 2'
0
BEGINNING SOUR TEST TEMPERATURE: 13 - 4 C'
ENDING SOUR TEST TEMPERATURE: b ` q o C'
Time in Minutes
D.O. mg/L
0
o
1
2
3
r0
4
% �g
5
a W%
6
.9 a
7
-a-
8
.>
9
��g5
10
6 ct
11
12
13
14
�a
53
15^��

SAMPLE DATE- I ►
DIGESTER DATA
DIGS ffER #1 SAMPLE TIME:
AIR:
TEMP. - ° CELSIUS
PH -
DO- mg/I,
NH3N-
TSS -
VSS -
mg/L
mg/L,
mg/L
mg/L
DIGESTER #2 SAMPLE, TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
—mg/L
�mg/L
_mg/L
mg/L
DIGESTER #3 SAMPLE TL
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
mg/L
Mn
tng/L
mg/L
mg/L
ipp,
....................................._.----- --------
Sample Date- 0 - m � c' \
DIGESTER # 35,
Volume Used - 25 ml.
Date In Oven- 29 - ney r-ol Date Out of Oven-
Time In- 73 b -q(-'\q Time Out- I
Weight of Dish- 3 1 I gm. (B)
Weight of Wet Solids + Dish-�;� gill. (C)
Weight of Dry Solids + Dish- �'t►gm. (A)
Calculations: _ p
(A) 9 7 - % ci � � grit. - (B) � . gin.
% My solids= ---------------------Divided By------------ --------- x 100
y
(C) 7.2 , 0 (Q 1 gm.- (B) ? --9 11 gin.
gm.
(---------- DIVIDED BY-------)X 100 = _� % TOTAL DRY SOLIDS
'1� , c, 03 gnr.
Sample Date
DIGESTER #
Volume Used - 2 I.
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish- gnr.(B)
Weight of Wet Solids + Dish -
Weight of Dry Solids + Dish -
Calculations:
(A) gin. - (B
% Dry solids= ---------------------Divided B,
(C) gm.- (B)
gm.
(---------- DIVIDED BY-------)X 100 = _
gm.
n. (C)
a. (A)
gin.
------------- x 100
gilt.
TOT DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By
Analysis Date/Time.
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.14
9.19
9.14
9.08
9.00
8.87
8.72
8.55
8.32
8.22
8.02
7.82
7.62
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
3/30/14
10.1
3/30/14 1117
SS
3/30/14 1122
SS
1.6
12.1
14.3
0.12
9.5
0.94
�/0 Dry Solids
degrees Celsius
degrees Celsius
7.14 mg Oxygen/hr
0.45 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate:1 0.72 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

y='0110x+9.5Q18
Oxygen Uptake Rate Chart
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1 2 3 4 5 S 7 8 Q 10 11 12 13 14 15 15
Time (minutes)

Vector Attraction Reduction DATE:
Option 4 - SOUR
GRAHAM WWTP SOUR TEST
DIGESTER: 3
TEMPERATURE AT COLLECTION: A/k
� 6
DATEITIME COLLECTED: j 1 13 0 I �i ' 0 A/k
r`� 1
SAMPLED BY: 5 S
ANALYSIS BEGAN DATE/TIME: 3)I
ANALYZED BY: S SS
ANAYLSIS ENDED DATE/TIME: 3 3.
j,S 3�4 i 4
BEGINNING SOUR TEST TEMPERATURE: Ia 1 C.
ENDING SOUR TEST TEMPERATURE: I �C-
Time in Minutes I.
D.O. mg/L
0
2
�I
3
4
�)
5
,08
6
, D�
7
8
s
< 5J
10
- 3
11
12
13
�'D.Z
14
b 2--
15
i

SAMPLE DATE- --� `� � � Q-j-(,)N
DIGES R #1 SAMPLE TIME:
AIR: 0 CELSIUS
T-
EEMP.
i
DO- ` mg/L
ALKALINITY,.,- mg/L
i
NH3N- mg/L
TSS - t mg/L
i
VSS - mg/L ,
DIGESTER #2 SAMPLE TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
DIGESTER #3
AIR:
TEMP. -
PH-_
DO-_
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
nig/L
_mg/L
mg/L
mg/L
�mg/L
PLE TIME:
° CELSIUS
_mg/L
mg/L
E
--rlez/v
Sample Date --
DIGESTER #
Volume Used - 25 ml. m
Date In Oven- 3 �1 -PCIk Date Out of Oven- SS ' I "ILA\ - � 1-1
Time In- W. 2-- F1-'\jn Time Out- 1 ��
Weight of Dish- S ' �0 I gm•(B)
Weight of Wet Solids + Dish- �© 0 gm.(C)
Weight of Dry Solids + Dish�J
- 7 6 . '12 3 6 gm, (A)
Calculation (A) w 6 . 323 � gm. - (B) 5 19 C � g
In.
% Drv_ solids=
(------ -- --- ---Divided By------------------------ x 100
c�gm.--G
.� D ��� gm.
(---------- DIVIDED BY-------)X 100 = % TOTAL DRY SOLIDS
`l
DIGESTER #
Volume U�ed - 25 ml.
Date In Over+
Time In -
Weight of Dish -
Weight of Wet Solids
Weight of Dry Solids +
Calculations:
(A)
% Dry solids=
Date Out of Oven-,
_ Time Out-
giii.(B)
(C) gm.
(---------- DIVIDED BY-------)X 100 =
gm. (C)
gni. (A)
- (B) gm.
;d Bv------------------------ x 100
gm.
% TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date.
Digester Temperature.
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By.
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.311
9.23
9.16
8.94
8.74
8.57
8.35
8.11
7.85
7.69
7.51
7.28
7.05
6.86
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
3/30/14
10.0
3/30/14 1456
SS
3/30/14 1500
SS
1.6
11.9
14.9
0.17
9.6
0.99
'/o Dry Solids
legrees Celsius
legrees Celsius
10.50 mg Oxygen/hr
0.66 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate:�� 1.05 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

12 -
10
I
Oxygen Uptake Rate Chart
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1 2 3 4 5 6 7 - 8 9 10 11 12 13 14 15 16
Time (minutes)

Vector Attraction Reduction DATE: 1 1 a 14
Option 4 - SOUR
GRAHAM WWTP SOUR TEST
DIGESTER: 3
TEMPERATURE AT COLLECTION: 0,0eC
DATE/TIME COLLECTED: 3
SAMPLED BY: 5S
ANALYSIS BEGAN DATE/TIME: )"� - ' o 0 P
ANALYZED BY: :J S
ANAYLSIS ENDED DATE/TIME: 5 130.. j 9 3 . � G r
BEGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE: I 1 • 1 OC
Time in Minutes
D.O. mg/L
o
`l 3
1
2
3
3
4
5
6
y
7s57
s
n� S
9
10
11
�5
12
13
14
pz

SAMPLE DATE- d
DIGESTER DATA PERCENT DRY SOLIDS J
�Dr'�U
DIGESTER 01 SAMPLE TIME: Sam1e ate- _ 1
17>
AIR:_ DIGESTER
TEMP. °CELSIUS ,Voume used - 25 mt. �
1
PH - �i Date In Oven- Zz. • nw•ck-) l Date Out of Oven- 3 ) - 1 m ' �J- ck—
DO- tng/L I Time In- ' O �j P F\ Time Out-
ALKALINIT - mg/L Weight of Dish- �l I , ��� gm.(B)
NH3N- mg/L Weight of Wet Solids + Dish- g 9111. (C)
TS S - \ mg/L Weight of Diy Solids -+- Dish- % gm.(A)
VSS - mg/L Calculations: ' I 4 �' g O
(A) `1 gm.
% D1), solids=-------e---------- -Divided By------------------------ x 100
DIGESTER #2 SAMPLE TIME: (C2c d gin.- (B) H 11 gm.
AIR: �p
TEMP. - \° CELSIUS O G gm.
PH - \ j (---------- DIVIDED BY-------)X 100 = I % TOTAL DRY SOLIDS
DO- mg/ _ � j , gill.
ALKALINITY - mg/L `\
NH3N- mg/LS�►mple late-
TSS - rlig/L DIGESTED#
VSS - mL %Volume Used,,r25 mi. Date In Oven -
Date Out of Oven-
\
%Time In- \N Time O (B)
DIGESTER #3 SAMPLE TIME-\ _ Weight ofDisll- g
/o/Weight of WeSolids + Di:
AIR: °IN
TEMP. - CELSIUS n L IUS Weight of ct Solids +Dish- \l g to (A)
PH - Calculations:
0/11
DO- mg/L \ (A) gm. - B) gin.
In L % D1y solids= -------- Divided B} x 100
ALKALINITY - g/------------------------------------ .
NH3N- Ing/L (C) gm.- (B) gm.
TSS - m Yg/L j(---------- DIVIDED BY--------)X 100 = % TAL DRY SOLIDS
VSS - g/

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.06
8.42
7.81
7.67
7.54
7.50
7.41
7.24
7.07
6.94
6.78
6.54
6.41
g
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
3/31/14
10
3/31/14 1133
SS
3/31/14 1139
SS
1.6
11.9
14.4
0.18
8.5
0.97
Yo Dry Solids
legrees Celsius
degrees Celsius
10.54 mg Oxygen/hr
0.66 mg Oxygen/hr/g
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate: I1.06 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
9
8
7
G
4
3
2
1
D
Oxygen Uptake Rate Chart
56,
;S
777
TTM
31
PMW
Willl -Si,
VNWO
100,
In
50
Am
-01
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16

Vector Attraction Reduction DATE: I ` I -c, -�
Option 4 - SOUR
GRAHAM WWTP SOUR TEST
DIGESTER:
g�o
TEMPERATURE AT COLLECTION:
DATE/TIME COLLECTED:
SAMPLED BY: f�C
ANALYSIS BEGAN DATE/TIME:
oNAI Y7F1) BY: �Ss
ANAYLSIS ENDED DATE/TIME:.
BEGINNING SOUR TEST TEMPERATURE: t ` ' C"
ENDING SOUR TEST TEMPERATURE: 1 q cC
Time in Minutes
D.O. mg/L
0
R OuCo
1Iz-
2
3
�• �%
4
�5
5
C �®
6
•9 1
7
o �`{
8 -
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g
- I
10
6•i�3
11
12
13
14
15
5
rO 23
5,95

SAMPLE DATE -
]DIGESTER #
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
DIGESTER DAT.
SAMPLE TIME:
° CELSIUS
mg/L
mg/L
mg/L
_mg/L
—�mg/L
DIGESTER #2 SAMPL
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
mg/L
— 9/1-
DIGESTER #3 SAMPLE TIME.-,
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
mg/L
_mg/L,
_mg/L
_mg/L
mg/L
Sample Date- >) - � '` I'cll - )I
DIGESTER # 3
Volume Used - 25 mi.
Date In Oven- cJ-(A1 _ y Date Out of Oven-
Time In-
`"1 C"M Time Out-
Weight of Dish- `-� 36 -� gm.(B)
Weight of Wet Solids + Dish- )3 J gm. (C)
Weight of Dry Solids + Dish- J 2 9 0 2 gm. (A)
Calculations: ` �y
(A) Lj 5 , d gm. - (B) I w gm.
%Dry solid (C) -��-` a�J--J-- -Divided By--� � ;-g-C�--�-�--- x 100
gm. (B) g
I a gm.
DIVIDED BY-------)X 100 = J % TOTAL DRY SOLIDS
`I . 31 O gm.
Sample te-
DIGESTE #
Volume Use - 25 mi.
Date In Oven-�
Time In -
Weight of Dish -
Weight of Wet Solids
Weight of Dry Solids +
Calculations:
(A)
% Dry solids=---------
(C)
Date Out of Oven-,
_ Time Out -
gm. (B)
Dish- gm. (C)
Gish- gm. (A)
(---------- DIVIDED BY ------
gm.
- (B) gin.
dBy------------------------ x 100
(B) gm.
)X 100 = \ % TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.07
8.37
8.25
8.15
8.01
7.69
7.47
6.931
d
GRAHAM WWTP
WQ0003824
3/31/14
10.1
3/31/14 1507
SS
3/31/14 1512
SS
1.6
13.0
15.7
)o Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.19
Intercept: 8.8
Correlation Coefficient: 0.99
Oxygen Uptake Rate: 11.42 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.71 mg Oxygen/hr/g
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.50
Temperature Corrected Specific Oxygen Uptake Ratef 1.07 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
Oxygen Uptake Rate Chart
M
I to al
IN
fi
us
g
MzV
If
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MW
-
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PAM
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1 2 3 4 5 G 7 8 A 10 11 12 13 14 15 18
Time (minutes)

'D
Vector Attraction Reduction
Option 4 - SOUR DATE: - C G"k
GRAHAM WWTP SOUR TEST
DIGESTER:
TEMPERATURE AT COLLECTION: �.0 I "C
DATE/TIME COLLECTED:
SAMPLED BY: ,-53
ANALYSIS BEGAN DATE/TIME:
nniol v7Fr1 RY• <�
ANAYLSIS ENDED DATE/TIME: �3 3i P (Y\
BEGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
2j��
3
g.1Ls
4
'.A
5
cg
6
�' 6
7
g
9
a FZ
10
11
12
13
14
15
/6 ' T3.
s, g$
13o c--
i �)."�
'313 I) i Ll
3A
C'l

SAMPLE DATE -
DIGESTER DATi
i)IGESTER #� SAMPLE TIME:
AIR: \
TEMP. - ° CELSIUS
PH -
DO- mg/L
ALKALINITY- mg/L
NH3N- mg/L
TS S - mg/L
VSS - ' mg/L
I)MFSTER 92 SAMPLE TIME:
AIR:
TEMP. -
PH-_
DO --
ALKALINITY -
NH3N-
TS'S -
VSS -
IDIGESTER #3
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
°'CELSIUS
mg/L
mg/L
SAMPLE TIME:
° CELSIU�
mg/L
mo
mg/L
mg/L
mg/L
Sample Date-
DIGESTER #
Volume Used - 25 mi.
C\j'\G 1 Date Out of Oven -
Date In Oven-�J� -in
Time In- �` �� Time Out- g�
Weight of Dish- 9 :5 - '�-- gnl•(B)
Weight of Wet Solids + Dish- '� O - 96 5 gm.(C)
Weight of Dry Solids + Dish- t / gm.(A)
;Calculations: 5 �� T; g S 2 Z
(A) - gm. - (B) J gm.
% Dry solids= ---------------------Divided By------------------7-- x 100
(C) c, 5�'� gm.- (B) S Z gm.
l� J gm.
(----------DIVIDED BY-------)X 100 = % TOTAL DRY SOLIDS
, 511..E RM.
Sample Dal -
DIGESTER
;Volume Used - 5 mi.
Date In Oven -
Time I
Weiglt of Dish -
Weight of Wet Solids + Dish
Weight of Dry Solids + Dish -
I Calculations:
Date Out of Oven -
Time Out-
% Dry solids= ------------ Divide
(C) gm.-
(---------- DIVIDED BY -gn i-)X 100 =
C)
-- (B) gm.
cKRv------------------------ x 100
% TOTAL DRY SOLIDS

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Time
(minutes)
0
1
2
3
4
5
6
7
8
0
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.79
7.58
7.38
7.18
6.89
6.61
6.33
5.70
5.39
4.76
4.48
4.14
3.79
GRAHAM WWTP
WQ0003824
5/6/14
17.5
5/6/14 0952
EC
5/6/14 1013
SS
1.6
18.3
18.9
Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.29
Intercept: 8.3
Correlation Coefficient: 1.00
Oxygen Uptake Rate: 17.38 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.09 mg Oxygen/hr/g
Average Temperature: 19 degrees Celsius
Temperature Correction Factor: 1.07
Temperature Corrected Specific Oxygen Uptake Rate: 1.16 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

0
li
Al
tM
E
r-
5
X
0
4
0
W
I
Oxygen Uptake Rate Chart
�A-IMI';�
51
R
VS
3"
ow ii V,
xiw 0�3,
R
A
P k P
Z.
ZIP la,"
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R�
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A
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V
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MAW
�%k
'Y
. . ....
XMI, X
2
3
4
5
6
7 8 9 10 11 12 13 14 15 16
Time (minutes)

Lector Attraction Reduction
Option 4 - SOUR DATE: t ' a -'
GRAHAM WWTP SOUR TES
DIGESTER: 3
1 ss SJct �y
,-EMPERATURE AT COLLECTION: I - 5 DO METER CALIBRATED: ATI ��t-��
)ATE/TIME COLLECTED: 51 � I i q — • 52 6 2 • 3 t %- S • 5 mg/L
SAMPLED BY: C-
ANALYSIS BEGAN DATE/TIME:
ANALYZED BY: ss
kNAYLSIS ENDED DATE/TIME: 5 16 1 )9 - [o ` �3Q�
3EGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE: JS') oC
Time in Minutes
D.O. mg/L
0
2
% 5 Cl-)
3
4
—7.4Q
5
6
7
r6�
8
1 O
9
10
5F 39
11
12
�%O
13
91419
14
15
3b

SAMPLE Dj ME-
#1 SAMPLE TIME:
AIR:
TEMP. -
PH -
DO-
NH3N-
TSS -
VSS -
DIGESTER 02 SAJ
AIR:
TEMP. -
PH
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
ing/L
tng/L
mg/L
mg/L
mg/L
PLE TIME:
° CELSIUS
DIGESTER #3 SAMPLE "
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
_mg/L
_mg/L
_mg/L
mg/L
° CE SIUS
mg/L
ing/L
Sample Date- % , 4Y) 2-2 - )')
DIGESTER # 3
Volume Used - 25 mi.
Date In Oven- b - M �- ) 9. Date Out of Oven- I w
Time In- 5 C Pr N Time Out- 6 AN A
Weight of Dish- 1 , () 0 3 C) gm.(B)
Weight of Wet Solids + Dish- b 5 , -) )- '2— gin. (C)
Weight of Dry Solids + Dish- y 13 71-3 gm.(A)
Calculations:
(A) ) r B gin. - (B) © �() gin.
% Dry solids= ---------------------Divided By------------------------ x 100
(C) C 5, � ),2>1 gin.- (B) 9) , 0 a � gin.
o 3 16 .,.� _- gm.
(---------- DIVIDED BY ---
)X 100 = 1 ' (e % TOTAL DRY SOLIDS
Sample Dil e-
DIGESTER
Volume Used - 5 mi.
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish-
Weight of Wet Solids + Dish gin,
Weight of Dry Solids + Dish- gin.
Calculations:
(A) \-
%Dii! solids=-----------------------------
(C)
(---------- DIVIDED BY-------)X 100 =
2111.
(C)
(A)
x 100
Al, DRY SOLIDS

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.
7.
7
7.08
6,.85
6.51
6.36
6.04
5.76
5.49
4.89
4.63
4.33
4.05
GRAHAM WWTP
WO0003824
5/5/14
17.5
5/5/14 1005
EC
5/5/14 1010
SS
1.6
18.3
19.3
'/0 Dry Solids
degrees Celsius
degrees Celsius
Slope: . 0.27
Intercept: 8.2
Correlation Coefficient: 1.00
Oxygen Uptake Rate: 16.22 •mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.01 mg Oxygen/hr/g
Average Temperature: 19 degrees Celsius
Temperature Correction Factor: 1.07
Temperature Corrected Specific Oxygen Uptake Rate: 1.08 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

RM
n.
7
5"R
E
c
X
0
'a
(D 4
A2
0 3
I
no
Oxygen Uptake Rate Chart
"!S
Y'
Tpol'
W
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ok
1 2 3 4 5 6
8 9 10 11 12 13 14 15 I b
Time (minutes)

_,'ector Attraction Reduction
Option 4 - SOUR DATE: S
GRAHAM WWTP SOUR TEST
DIGESTER: 3
EMPERATURE AT COLLECTION: Jr C- DO METER CALIBRATED: 5I 5 AT
)ATE/TIME COLLECTED: 5 -� %- Z ' mg,L
SAMPLED BY: EC
ANALYSIS BEGAN DATE/TIME:
►NALYZED BY:
�NAYLSIS ENDED DATE/TIME: � - �� - � � f � "2- 5 Afk
o
3EGINNING SOUR TEST TEMPERATURE: C-
o
NDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
0
i3
1
% • T% �
2
�? - 5q I
3
7W 3
4
).C)8
5
g�
6
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5, 76
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11
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12
13
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14
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15
. 0 5

SAMPLE DATE -
DIG
DIG
TEMP. -
PH -
DO-
NH3N-
TSS -
VSS -
DIGESTER D
#1 SAMPLE TIME:
DIGESTER #2 SAI,
AIR:
TEMP. -
PH-_
DO --
ALKALINITY -
NH3N-
TSS -
VSS -
DIGESTER #3.
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
CELSIUS
mg/L
mg/L
mg/L
mg/L
mg/L
PLE TIME:
° CELSIUS
mg/L
tng/L
mg/L
mg/L
SAMPLE IME:
° CE SIUS
mg/L
t g/I
in L
Mg/L
- — - ing L,
Sample Date- .5 `
DIGESTER # 3
Volume Used - 25 mi. /
Date In Oven-5 - Date Out of Oren- tOM
Time In- ( U Time Out- (� SS P(
Weight of Dish- H L+ gni•(B)
Weight of Wet Solids + Dish- 4 gm.(C)
Weight of Dry Solids + Dish- gm,(A)
:Calculations:
(A) in. - (B) gm.
% Dn, solids= ---------------------Divided By----LL-,,------------------ x 100
(C) -�) , 9D a y gym.- (B) `7 13 gm.
q
I gm.
(---------- DIVIDED BY-------)X 100 = I ° % TOTAL DRY SOLIDS
gm.
Sampl Date-
DIGES R #
Volume ed - 25 ml.
Date In Ove
Time In -
Weight of Dish -
Weight of Wet Soli
Weight of Dry Solids
Calculations:
% Dry solids=
Date Out of Oven -
Time Out-
gm.(B)
+ Dish- glll.(C)
+,Dish- gm.(A)
- (B) gm.
2dBv------------------------ x 100
- (B) gm.
(---------- DIVIDED BY-------)X 100 =� _ % TOTAL DRY SOLIDS

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
. Facility.Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
m
7.33
7.05
6:64
6.05
5.74
5.15
4.81
4.50
4.19
3.86
3.55
2.951
GRAHAM WWTP
WQ0003824
5/8/14
19.8
5/8/14 0950
EC
5/8/14 0959
SS
1.6
19.8
19.7
o Dry Solids
legrees Celsius
legrees Celsius
Slope: 0.33
Intercept: 7.8
Correlation Coefficient: 0.99
Oxygen Uptake Rate: 19.68 mg"Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.23 ,mg Oxygen/hr/g
Average Temperature: 20 degrees Celsius
Temperature Correction Factor: 1.00
Temperature Corrected Specific Oxygen Uptake Rate: 1.23 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

M
7
Al,
2
1
Oxygen Uptake Rate Chart
NOW affl-
gg
211
1 2 3 4 5 6 7 8 Q 10 11 12 13 14 15 16
Time (minutes)

Vector Attraction ReductionM
Option 4 - SOUR DATE: o -�
GRAHAM WWTP SOUR TEST
DIGESTER:
C� o
TEMPERATURE AT COLLECTION: I I f C
DATE/TIME COLLECTED:
SAMPLED BY:
DO METER CALIBRATED: J' j q AT fl11�
10,q . 3 I'l
ANALYSIS BEGAN DATE/TIME: J I S I J'I
ANALYZED BY: 15s
ANAYLSIS ENDED DATE/TIME-. I `� I 0 ` f A�
O _
BEGINNING SOUR TEST TEMPERATURE: I �"
ENDING SOUR TEST TEMPERATURE: 9.
Time in Minutes
D.O. mg/L
0•
35
1
3
2
�. O
3
4
5
.QJ
6
7
8
5 �5
9
10
11
r ��
12
3 P SG
13
= 55
14
38� -7
15
2. 9s

SAMPLE DATE -
-- � , ) GLL1 1
DIGESTER #1
AIR:
SAMPLE TIME:
TEMP. -°CELSIUS
PH - C
DO- 0, mg/L
ALKALINITY - Z5 mg/L
NH3N- tng/L
TSS - Q mg/
L
VSS - ) L) _ 690 tng/L
DIGESTER #2
AIR:
SAMPLE TIME:
TEMP. - �') ° CELSIUS
PH -
DO- 3 mg/L
ALKALINITY - mg/L
NH3N- mg/L
TSS - i g 5 0 mg/L
VSS -
DIGESTER #3
AIR: D
SAMPLE TIME:
TEMP. -
° CELSIUS
-
PH
��3 >
DO-
mg/L
ALKALINITY - �w c ing/L
NH3N-
mg/L
TSS -
, E, U nig/L
VSS -
1 "so
Sample Date- -N - 1 I Q2�
DIGESTER # �-
Volume Used - 25 mi. )
Date In Oven- - �)a4- Date Out of Oven- CI
Time In- Iy : q0 Ny" Time Out- 6 i o
Weight of Dish-_ ' I 763 6 gnl. (B)
Weight of Wet Solids + Dish- 7y 3 gill. (C)
Weightof Dry Solids A- Dish- � S , 0 972 V gnr.(A)
Calculations:
(A) q 3 , 016a gm. - (B) , i � gill.
l % Dry solids= ---------------------Divided By------------------------ x 100
1 (C) 6 7, 63ZZ- gm.- (B) 112. f Z3� gm.
a 3 I gill.
i
j(-------- -- DIVIDED BY-------)X 100 = I ' %'TOTAL DRY SOLIDS
Lj . � (o) gill.
i
Sample Date- I I w, - _
DIGESTER #
%Volume Used - 25 m�c
iDate In Oven- 14 Date Out of Oven-
� Time In- 'I'imc Out- ) 0 s Wa
s D Weight of Dish- gill.(B)
ht of
101
Weight of Dry Solids + Dishl- i -O 9 5 giu,(A)
g _1 b
Calculations:
(A) s S O &D gin. - (B) 9'1_ ) Z 1 i gill.
% Dry solids= --------------------Divided By --I- �-L--j--/-------I-------- x 100
(c)6 O--< q?22- gill.- (B) I I 1 LJ gill.
_ a_ 3911 a gill.
DIVIDED BY-------)X 100 = %'TOTAL DRY SOLIDS

Facility Name
Biosolids Permit Number.
Date.
jDigester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By.
Total Solids
Beginning Temperature
End Temperature
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
8.82
5.44
4.99
4.83
4.65
4.48
4.32
4.12
3.92
3.51
3.29
2.54
2.23
GRAHAM WWTP
WO0003824
5/13/14
22.1
5/13/14 1001
EC
5/13/14 1009
SS
1.6
22.6
22.5
% Dry Solids
Degrees Celsius
degrees Celsius
Slope: 0.28
Intercept: 6.3
Correlation Coefficient: 0.88
Oxygen Uptake Rate: 17.03 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.06 mg Oxygen/hr/g
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.86
Temperature Corrected Specific Oxygen Uptake Ratel 0.92 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
O
8
7
G
4
3
2
1
O
Oxygen Uptake Rate Chart
iL
IP
WON
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0111
1 2 3 4 5 G 7 8 Q 10 11 12 13 14 15 10
Time (minutes)

ector Attraction Reduction l >�
Option 4 - SOUR DATE: _ M q
GRAHAM WWTP SOUR TEST
DIGESTER: 13
`o
EMPERATURE AT COLLECTION: ` C"
,ATE/TIME COLLECTED: --�
SAMPLED BY: G
ANALYSIS BEGAN DATE/TIME:
NALYZED BY: sl S
,NAYLSIS ENDED DATE/TIME:
-1EGINNING SOUR TEST TEMPERATURE
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
0
`b���)-
1
9
2
3
p
, 03
4
J
5
6
-32
7
, tit
s
.9; .
9
3
10
3 e
11
3
12
13
14
15
c a3
DO METER CALIBRATED: 5) AT l) ' 0� �
(
j •� S-96
I � � � `� % — mg/L
a16"C-
/a`a • 5°c-

-SAMYLE IAA I L-
DIGESTER #1
AIR:
--._--- .-----------
SAMPLE
TEMP. - 5S ° CELSIUS
PH-. 9,7
DO- O l (--mg/L
ALKALINITY- `� �) mg/L
NH3N- mg/L
TSS-_ 1 -:3� 9 410 mg/L
VSS_ to , .`j Q_Cj mg/L
DIGESTER #2 SAMPLE TIME:
TEMP. - - ;k S- ° CELSIUS
PH-- 6.60
DO- ©. %.2- ma
ALKALINITY - mg/L
NH3N- mg/L
TSS - .a , a 8 b mg/L.
VSS - ! 3 J 0 mg/L
DIGESTER #3 SAMPLE TIME:
/ TEMP. - V { o2 a' I ° CELSIUS
PH - 1�2
DO- . 6), 1 mg/L
ALKALINITY - P-C) 6
mg/L
NH3N- mg/L
TSS - I H� S GO mg/L
VSS - t._Q.
Sample Date- ) 3 (D
DIGESTER # :2
Volume Used - 25 mi.
Date In Oven- 3- c Z " )'� Date Out of Oven- l y - N 0- '_ 1 V
Time In- Time Out- + '-J 2PJY
Weight of Dish- �{ - U� 2 gm.(B)
Weight of Wet Solids + Dish- �J - 3k 7gm.(C)
Weight of Dry Solids + Dish- H 0= gin.(A)
Calculations:
(A) q 0 - _535.5 gm. - (B) j e, .2c, C L gm.
% Dry solids= ---------------------Divided Bv----------------------- x 100
r 3293
(---------- DIVIDED BY ------)X 100 = ) ,,3 % TOTAL DRY SOLIDS
_. % / 25 gm.
Sample Date-
DIGESTER #
Volume Used - 25 mi.
Date In Oven- )3 -- Date Out of Oven- - )
Time In- )Q I_S PEA Time Out- �� Z ��("V
Weight of Dish- � 9, `'1 `% S 6 gm.(B)
Weight of Wet Solids + Dish- . 9_% 7 gm.(C)
Weight of Dry Solids + Dish- Lj , �_�� c� grn.(A)
Calculations: o u
(A) y 6 g gm. - (B) I �i y gin.
% Dry solids= ---------------------Divided By------------------------ x 100
(C)) gm.- (B) y , y L� gru.
G� gm.
(-------- `DIVIDE,D BY-------)X 100 = I d _ % TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.93
7.43
7.12
6.17
5.97
5.80
5.41
5.21
4.87
4.69
GRAHAM WWTP
WO0003824
5/19/14
16.8
5/19/14 0940
EC
5/19/14 0946
SS
1.6
18
19
0 Dry Solids
legrees Celsius
legrees Celsius
Slope: 0.21
Intercept: 7.9
Correlation Coefficient: 0:95
Oxygen Uptake Rate: 12.83 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.80 mg Oxygen/hr/g
Average Temperature: 19 degrees Celsius
Temperature Correction Factor: 1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.86 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
L-11
7
8
4
Mo
2
Oxygen Uptake Rate Chart
van 1
INS
Elliot
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MWIM20
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1 2 3 4 5 6 7 8 9 10 11 lz �15 /,4 /n m

ector Attraction Reduction q (�
Option 4 - SOUR DATE:
GRAHAM WWTP SOUR TEST
DIGESTER:
!
0
S
EMPERATURE AT COLLECTION: 1 �' 00 C DO METER CALIBRATED: `� AT Gl - i3 v�-
: 1h(YL iATE/TIME COLLECTED
,NALYSIS BEGAN DATE/TIME: JI 1 9 j 9
,NALYZED BY: 5 -s
�NAYLSIS ENDED DATE/TIME:
'BEGINNING SOUR TEST TEMPERATURE
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L.
0
`- , '?3
1
), LB
2
i. �Z
3
6,�O
4
61,91
5
6161
6
. S2
7
639
8
6,»
9
15J9
10
;5, 8o
11
5. 63
12•
13
JAzI
14
15
�� ��

.....................
DIGESTER #1
AIR: _
TEMP
SAMPLE TIME:
CELSIUS
PH - —0-
DO-- 0 Z mg/.L
ALKALINITY - i 0 mg/L
NH3N- mg/L
TSS - �_�� mg/L
VSS - 2,0 mg/L
DIGESTER #2
AIR:
TEMP. -
PH -
SAMPLE TIME:
3 ' Z ° CELSIUS
DO- --- ��—_mg/L
ALKALINITY - — 'A 0
mg/L
NH3N- d 63
mg/L,
_
TSS - I r F2 0
—mg/L
VSS - .`—_--- 12c—mg/L
Sample Date-
DIGESTER # _
lVolume Used - 26 mi.
I Date In Oven- 9 _ -� y Date Out of Oven- 2-0 trn
CL-)
% Time In- )0', 13 A"� Time Out- 3
%Weight of Dish- t1 2Z� c-gin.(B)
Weight of Wet Solids -+- Dish- OQ giu.(C)
Weight of Dry Solids + Dish- b • 7 y 6 7 giit.(A)
Calculations.
(A) .7 gin. - (B) Z Z y gm.
% Du solids= - --------- ---------Divided By------------------ -- - x 100
`� ----- (c)_ 7 D .�OG� 1 gin.- (B) q . "j Zz I gin.
DIGESTER #3 SAMPLE TIME: 1_ I q 0
AIR: LV 1
TENI.P. -
° CELSIUS
ALKALINITY
TSS - - ---
`_�.. a 10
uig/L
VSS ...
. - . 1 � 'D, 5o ....
mg/L.
3 `i
---------- DIVIDED BY-------)X 100 = %, TOTAL DRY SOLIDS
9,V777 gnl.
Sample Date -
DIGESTER #
;Volume Used - 25 mi.
-Date In Oven- g _g'7 Date Out of Oven-�'`�
s Thile In- � `� r Time Out- '• Li
Weight of Dish-_ 91L LO5
Weight of Wet Solids A- Dish- Z3. cgs 6 � gm.(C)
;Weight of Dry Solids +Dish- i e s ��� gnl.(A)
%calculations: �y
(A) 1 cS L -5 9 gill. - (B). ____-gut.
% Dry solids= ------------- - ------Divided BN----------- --------------
_ x 100
(Q u -- --
2 C `� gill.- (B) � 05
(___.___..... DIVIDED BY -_ )X. 100 - --- e __-- °/,) TOTAL, L)RY SOLIDS
y �•i 6 l?Ill.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name.
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.82
5.23
5.14
5.05
4.96
4.76
4.67
4.56
4.47
4.37
4.22
4.01
3.89
3.78
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
5/20/14
16.7
5/20/14 0938
CR
5/20/14 0944
SS
1.5
17.7
18.6
0.18
6.2
0.74
36 Dry Solids
degrees Celsius
degrees Celsius
10.80 mg Oxygen/hr
0.72 mg Oxygen/hr/g
18 degrees Celsius
1.14
Temperature Corrected Specific Oxygen Uptake Rate: 0.82 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
E;
FA
CO 4
m
,W
3
2
1
Oxygen Uptake Rate Chart
0
V 4�
,J�
2 3 4 5 8 7 8 A 10 11 12 13 14 15 16
Time (minutes)

-actor Attraction Reduction
Option 4 - SOUR DATE: - aw - 1
GRAHAM WWTP SOUR TEST
DIGESTER: 3
i EMPERATURE AT COLLECTION:
ATE/TIME COLLECTED: 51
OAMPLED BY: U,
ANALYSIS BEGAN DATE/TIME:
,NALYZED BY: SS
,NAYLSIS ENDED DATE/TIME:
\ o
1EGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
o�-
1
�3
2
SO
3
4
_I
b
5
L
6
`
7
/
8
9
10
, 3�
11
0 ��-
12
1 l
13
L , 01
14
15
• ��
DO METER CALIBRATED: 5 I y AT 35i

SAPUi DAA-L''-
M
DIGESTER #1
AIR:
TEMP.
PH -
DO-
DIGESTER DAT
SAMPLE TIME:
° CELSIUS
mg/L,
ALKAL114, TY - mg/L
NH3N- nig/L
TSS - mg/L
VSS - mg/L
DIGESTER 4 SAMPLE TIME:
TEMP. -
° CELSIUS
PH--
DO-AN
g/L
ALK—_mg/L
NH3mg/L,
TSS---mg/L
VSSmg/L
DIGLE
TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
CELSIUS
_mg/L
mg/L
[&L.
Sample Date- 'aLa - I' I � - 11..
DIGESTER #
Volume Used - 25 mi.
Date In Oven- 0-b , (`)a`�' Date Out of Oven-
Time In- 9 9 I Time Out- g ��
Weight of Dish- � 9 . � I � C� q gtii•(B)
Weight of Wet Solids + Dish- I y gul.(C)
Weight of Dry Solids + Dish- gm.(A)
Calculations:/
(A) U gill. - (B) ! L) b) gill.
% Dry solids= ---------------------Divided By----------------------- x 100
i q
(C) ©y 3 gm.- (B) �O , 1 gm.
i 0 _gin.
(---------- DIVIDED BY ------- )X 100 = % TOTAL DRY SOLIDS
Sample Ib te-
DIGESTER
Volume Used - 5 ml.
Date In Oven- Date Out of Oven -
Time In- _ Time Out-
Weigllt of Dish- _gm.(B)
Weight of Wet Solids + Dish-
i Wcight of Disc Solids + Dish -
calculations:
(A) gin. -
% Dne solids= ---------------------Divided B
(B)
_gin.
(----------- DIVIDED BY-------)X 100 = --
gill.
v----------------------- x 100
% TOTAL DRY SOLIDS

H
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
11
7.91
6.40
5.74
5.47
5.36
5.05
4.87
4.77
4.77
4.62
4.45
4.26
4.12
3.95
3.79
3.62
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
5/21 /14
18
5/21 /14 0927
SS
5/21/14 0935
SS
1.6
18.9
19.5
0.21
6.5
0.91
Yo Dry Solids
legrees Celsius
legrees Celsius
12.49 mg Oxygen/hr
0.78 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: 0.84 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Ee
N.
7
6
5
4
cn
1
0
Oxygen Uptake Rate Chart
Vo
311
gllpu
gp-
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16

ector Attraction Reduction -
Option 4 - SOUR DATE: -
GRAHAM WWTP SOUR TES
DIGESTER: 3
_ EMPERATURE AT COLLECTION:
ATE/TIME COLLECTED:
SAMPLED BY: �sSS
.NALYSIS BEGAN DATE/TIME:
NALYZED BY: 5 S S
,NAYLSIS ENDED DATE/TIME: -S 0 (Ary�
BEGINNING SOUR TEST TE
MPERATURE: o C
0
ENDING SOUR TEST TEMPERATURE: 5 C'
i ime in Minutes
D.O. mg/L
0
---).91
1
�
2
5 `�
3
5ay7
4
5�
5
0IT 5
s
8.7
8
9�-
10
�,45
11
12
13
3 0 15Q
14
16
�J 2-
DO METER CALIBRATED: I I AT
16,�,, 3 %_ ' 1 © mg/L

SAMPLE DA I E-
L
.............................
DIGESTER#I SAMPLE TIME.
AIR: _ TEMP ` ° CELSIUS
PH -
DO- mg/L
ALKALINITY - ` nlg/L
NH3N- mg/L
TSS - mg/L
VSS - tng/L
7
DIGESTER #2 SAl PLE TIME:
AIR:
TEMP. PH -
DO -
ALKALINITY -
NH3N-
TSS - _
VSS -
Sample Date-
DIGESTER # 3
Volume Used - 26 ml.
Date In Oven- ' -�M Date Out of Oven-
q, )
Time In- 6 Time Out- 9 9 ca pr�
Weight of Dish- 7 gtli.(B)
Weight of Wet Solids i+ Dish- 6 g-T_gni,(C)
Weight of Dry Solids -+- Dish- 19 F ,5 gni. (A)
;Calculation (A) g� gin. - (B) � .�� I I gill.
% Dry solids= - -------------------Divided By----------------- ----- x 100
(C) G 6. 089 9 gin.- (B) H ) • �? ) ) gnl.
° CELSIUS_ gm.
P (---------- DIVIDED BY ------
,..,r
__ ng/L
_tng/L,
_mg/L
mg/L
DIGESTER #3 SAMPLE TIME:
AIR:
TEMP. - ° CELLSIUS
PH -
DO- mg/I,
ALKALINITY - D
NH3N- II r
I S S - _^- ---- m
VSS - -Mg/L.
)X 100 = _ �' % TOTAL DRY SOLIDS
Sample` aate-
DIGESTER
Volume Use 26 ml.
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish- gm.(B)
Weight of Wet Solids -+- Disli
Weight of Dry Solids -+- Dish -
Calculations:
(A) gtn. - B
Dry solids= ---------------------Divided B,
(C) ----gut.- (B)
---------_ DIVIDED BY---_---)X 100 =
n.(C)
i.(A)
gill.
-------------- x 100
_gilt.
°in - TAL DRY SOLIDS

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Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7.68
6.32
6.06
5.99
5.93
5.85
5.80
5.71
5.66
5.59
5.53
5.45
5.37
g5.2
GRAHAM WWTP
WO0003824
7/7/14
22.3
7/7/14 1040
CR
7/7/14 1048
SS
1.5
22.6
21.8
Yo Dry Solids
legrees Celsius
legrees Celsius
Slope: 0.11
Intercept: 6.6
Correlation Coefficient: 0.84
Oxygen Uptake Rate: 6.39 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.43 mg Oxygen/hr/g
Average Temperature: 22 degrees Celsius
Temperature Correction Factor: 0.91
Temperature Corrected Specific Oxygen Uptake Rate: 0.39 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

!11
M
Lw-,
M
E
X
0
4
0
3
1
I
Oxygen Uptake Rate Chart
et
k
v
77
. . . . . . . . . .
.... .. ...ns
tiv
-f,
"JV
77
X
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

✓ector Attraction Reduction -7
Option 4 - SOUR DATE: /
G rlp% AM WWTP SOUR TEST
DIGESTER: 3
0
-i EMPERATURE AT COLLECTION: C DO METER CALIBRATED: % I I AT 0
)ATE/TIME COLLECTED: I — `� `�O R►'� Q a a 3 %- mg/L
iAMPLED BY:
ANALYSIS BEGAN DATE/TIME: - �
kNALYZED BY
ss
kNAYLSIS ENDED DATE/TIME:
3EGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mggy/L
Q
2
.
3
q�
S
4
5.93
5
5. &5
g
e ��
7
8
59��
s
10
- 53
11
12
13
a
14
15
1

i
,,,,,,,,,,,,,.......................................................................... ........... ....------- .......................-- .
DIGESTER #1 SAMPLE TIME:
AIR:
i
TEMP. - ° CELSIUS
PH -
DO- mg/L
ALKALINITY - nig/L
10/1
NH3N- mg/L
TSS - mg/L
VSS - ' mg/L
i
ii
DIGESTER #2 S MPLE TIME:
AIR: TEMP, -
° CELSIUS
PH -
DO- mg/L
ALKALINITY - mg/L
NH3N- mg/L
TSS - ` mg/L
ii
VSS - `�mg/L
DIGESTER #3 SAMPLE = ICE'.
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS - _
° CELS US
mg/L
m
_ mg/
mg/L
mg/L
PERCENT DRY
Sample Date- _/ - - lq - -
DIGESTER # __75
Volume Used - 25 mi. Date In Oven- 7 Date Out of Oven U—� 7
Time In- I I A!°\ Time Out -
Weight of Dish- _oZ9 31 gm.(B)
Weight of Wet Solids + Dish- - O 7 gill. (C)
Weight of Dry Solids + Dish- I I I S gill. (A)
Calculations: 1.j i
(A) I 1 . 5i c0 gm. - (B) I I - 2-c) 3 1 gm.
% Dry solids= ---------------------Divided By------------------------- x 100
(C) 6 J - 90 /i t;m.- (B) 9 1 , ;02 I gm.
_gin.
(---------- DIVIDED BY --- ---- )X 100 = I ' % TOTAL DRY SOLIDS
Lj , 6 O % 6 gm.
Sample Dal -
DIGESTER
Volume Used - 5 mi.
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish- gm.(B)
Weight of Wet Solids + Dish gm.(C)
Weight of Dry Solids + Dish-\Divided
_gm.(A)
Calculations:
(A) gin.
% Dry solids=---------------------------------------x 100
(---------- DIVIDED BY-------)X 100 = \ % TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name'.
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
I
8.98
7.88
7.69
7.53
7.3
7.13
7.15
7.02
6.87
6.65
6.46
6.34
6.18
6.02
5.9
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
7/8/14
23.3
7/8/14 0935
EC
7/8/14 0945
SS
1.5
23.2
22.2
0.16
8.2
0.95
Yo Dry Solids
legrees Celsius
legrees Celsius
9.47 mg Oxygen/hr
0.63 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature'Corrected Specific Oxygen Uptake Rate: 0.55 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Oxygen Uptake Rate Chart
10
,
f'
-
"
x
r
z
-
i .
n
6
,
o
}
t•
S,
0
4
-
LA
O
,
-.s
_
4,�_.
7 $ 9 10
11 12
13 14
15 16
�1
2', 3 5».»
6
Time (minutes)

vector Attraction Reduction Q 1
Option 4- SOUR DATE: y r I - f
GRAHAM WWTP SOUR T S
DIGESTER:
o �`
TEMPERATURE AT COLLECTION: 23 3 C" DO METER CALIBRATED: AT 7 $�
ATE/TIME COLLECTED: -� 1 S ' 3 S PA ! mg/L
-AMPLED BY:C
ANALYSIS BEGAN DATE/TIME:
_ .NALYZED BY: Ss
,NAYLSIS ENDED DATE/TIME:
'EGINNING SOUR TEST TEMPERATURE
rNDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
0
• °QQ) 8
2
"7 , G22
3
�J
4
5
6
7
D n2—
s
og%
9
10
11
�O l
12
3
13
14
b ��
15
�,
d

SAMPLE DATE-
S
\if AA k/VN - I
L1
.,,,,,
DIGESTER #1 SAMPLE TIME:
AIR: ,__._&___._
TEMP, - _ 2_�, l• °CELSIUS
PH-_ " 6 �z .
DO- C0, 0_2 tng/L
ALKALINITY - 02 0qo ing/L
NH3N-_mg/L
TSS - _ a.3 0 _inga,
VSS - 5 210. mg/L
DIGESTER #2 SAMPLE TIME:
AIR:
TEMP. - ' j °CELSIUS
PH
DO- ,� mg/L
ALKALINITY - U mg/L
NH3N- a 3 % tng/L
TSS - �q 00 mg/L
VSS - ")E) o mg/L
DIGESTER #3 SAMPLE TIME:
AIR: U G�
TEMP. - ° CELSIUS
PH - CI _
DO- S , 1�4 mg/L
ALKALINITY - n0 _tng/L
NH3N- _ � O� ( 5 �2_ _mg/L
TSS-----°�-, '-�' _— zng/L
VSS -.— —� `�'-°—�G _mg/L
Sample Date -
DIGESTER #
Volume Used - 25 mi. q u
Date In Oven- -) i Date Out of Oven-
Time In- I °o. Ar Time Out-
Weigh; of Dish -
Weight of Wet Solids + Dish - 0 . 7 y gnr. (C)
Weight of Dry Solids -+- Dish- . 9 6 1 �_gnr.(A)
IN
ON
Calculations: y U
(A) 115, bogut. - (B) IJ , 7 y L , gin.
% Dry solids= ---------------------Divided By------------------------ x 100
5 1
01, (C) 70. 7 E 1 w gym.- (B) 9 .S .-7 J J V gm.
. ,zo 6 o
(---------- DIVIDED BY ------
:z-s , O o ,?(o grn.
)X 100 = . 0 v 8 Z % TOTAL DRY SOLIDS
Sample Date- (�
DIGESTER # 3
iVolume Used - 26 mi. ---�� -- ' `J �
:Date In Oven- - f Date Out of Oven.
Time In- f ; Time Out- 7 3)
Weight of Dish-_ 5309 g�nr. (B)
Weight of Wet Solids + Dish-
Weight of Dry Solids + Dish- grn.(A)
Calculations:
(A) gru. - (B) I� S / gm.
° ------ --Divided B x 100
/o Dr} solids- ------------ y------------------------ ,.
gm.- (B) q) 1 530% gilt.
OIL- sin.
DIVIDED BY-------)X 100 = I. ` ,-5% TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By.
Total Solids
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.90
7.16
4.75
6.35
6.05
5.72
5.04
4.83
4.51
4.40
4.20
4.04
3.93
t3.71
GRAHAM WWTP
WQ0003824
7/9/14
23.8
7/9/14 0928
EC
7/9/14 0939
SS
1.5
23.4
22.3
lo Dry Solids
legrees Celsius
degrees Celsius
Slope: 0.25
Intercept: 7.1
Correlation Coefficient: 0.86
Oxygen Uptake Rate: 14.75 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.98 mg Oxygen/hr/g
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.86
Temperature Corrected Specific Oxygen Uptake Rate: 0.85 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
9
8
7
6
c
x 5
O
0 4
N
N
3
2
1
0
Oxygen Uptake Rate Chart
ar
•
_
„
,
f-
�y.
3
.2458
x
Ya
•
-a
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iY^
va
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r
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v
e
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,
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s
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1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

lector Attraction Reduction
Option 4 - SOUR DATE: ! 1
GRAHAM WWTP SOUR T`ES
DIGESTER: s
TEMPERATURE AT COLLECTION: a5,2 eC-
)ATE/TIME COLLECTED:-%) �) I 1 `1 - l �g A
✓-� `y,�
SAMPLED BY: q
ANALYSIS BEGAN DATE/TIME: i 9 ) 4 -
ANALYZED BY:
5S
DO METER CALIBRATED: _)I 1)) LjAT U O
% - 1 , mg/L
kNAYLSIS ENDED DATE/TIME: I 9 - q 5 � Pm
3EGINNING SOUR TEST.TEMPERATURE: ' "C'
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
0
90
1
16
2
b- -75
3
4
5
5.
6
5.91
DI
a
�1,83
9
f 3
10
51
11
12
u��D
13
Ll
14
3-9.
15

z5AMa-I-.,E DA i E-
#1 SAMPLE TIME:
AIR:
TEMP, -
PH-_
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
DIGESTER #2 SA
AIR:
TEMP. - —
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
mg/L
ing/L
mg/L
tng/L
_mg/L
'LE TIME:
Sample Date- - )
DIGESTER #
Volume Used - 26nm11.
Date In Oven- (9 `, - i Date Out of Oven-) O " -) 4
Time In- I `) o p Time Out- g' �i' 3 wn,
Weight of Dish �- . 1 �g gm.(B)
Weight of Wet Solids + Dish- �' - 5 S 7 3 gni. (C)
Weight of Dry Solids + Dish- �) , i3�i gm.(A)
Calculations:
(A)_!� ' �3�f gin, - (B) 8g gin.
% Dry solids= ---------------------Divided By------------------------ x 1o0
(C) (' S P 5S7.3�in. - (B) ), M 5 2 K gin.
° CELSIUS �y gin.
(---------- DIVIDED BY ------
1 L j aM S &S gni.
mg/L
DIGESTER 93 SAMPT,F,
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
mg/L
-mg/L
tng/L
;IME:
L
mg/L
Samplell le-
DIGESTE\\ #
Volume Use- 26 ml.
Date hi Oven -
Time In -
Weight of Dish
Weight of Wet Solids +I
Weight of Dry Solids + I
Calculations:
)X 100 = 1 " '5 % TOTAL DRY SOLIDS
Date Out of Oven -
Time Out-
% Dry solids=---------------------Did{d
(C) gm,
gin.
(---------- DIVIDED BY-------)X 100 =
-------- ----gin.
gill.(B)
gm. (C)
gin. (A)
- (B) gin.
d By------------------------ x loo
% TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.75
6.34
6.06
5.90
5.81
5.74
5.69
5.65
5.52
5.43
5.34
5.25
5.19
5.11
GRAHAM WWTP
WO0003824
7/10/14
23.3
7/10/14 0938
EC
7/10/14 0947
SS
1.5
23.4
22.3
Slope: 0.13
Intercept: 6.8
Correlation Coefficient: 0.73
3o DrySolids
degrees Celsius
degrees Celsius
Oxygen Uptake Rate: 7.86 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.52 mg Oxygen/hr/g
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.86
Temperature Corrected Specific Oxygen Uptake Rate: 0.45 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
9
8
7
6
c
m
rn
Ox 5
m
0 4
n
0
3
2
1
0
Oxygen Uptake Rate Chart
`A
Y`
-77 c
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

ector Attraction Reduction
Option 4 - SOUR DATE: --
GRAHAM WWTP SOUR T ST
DIGESTER: 3
. EMPERATURE AT COLLECTION: 93,3 oC
ATE/TIME COLLECTED: .� i I°� �i —' J 38 NM
SAMPLED BY: F C
r%NALYSIS BEGAN DATE/TIME:� I° 1H
,NALYZED BY: S S
�NAYLSIS ENDED DATE/TIME: -7 10 I
'IEGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
0
-�
2
�.06
3
5.90
4
ag
5
7�
6
�� 6
7
�3F 65
s
5-go
9
32
10J
r
11
5, Sl
12-32
13
�a5
14
5-
15
DO METER CALIBRATED: AT 1
t 0� r 3 %- ,�- g mg/L
�\'j,-� ()L
Q-1.30C—

�!iAM.ri�j.? LEA 1lE-
,,,,,,,,,,,,,,
AIGESTE #1
AIR:
TEMP. -
PH
DO- _
ALKALINITY -
NH3N-
TSS -
VSS -
SAMPLE TIME-
0
CELSIUS
nig/L
_mg/L
mg/L
mg/L
mg/L
DIGESTER #2 SAMPLE TIME:
AIR:
TEMP. - ° CELSIUS
PH -
ISO- mg/L
ALKALINITY - mg/L
NH3N- tng/L
TSS - mg/L
VSS - mg/L
DIGESTER #3
AIR: --- _
TEMP. -
PH -
DO -
ALKALINITY -
NH3N- _
TSS -
VSS -
ILEI TIME:
° C LSIUS
mg/L
mg/L
_ rng/L
Sample Date- 16 -1'�
DIGESTER # 3
Volume Used - 25 ml.
Date In Oven- - v -k -) Date Out of Oven-)
Time In- O Time Out- (o ss P
Weight of Dish- % 1q� gm.(B)
Weight of Wet Solids + Dish- ! -)C 12, gill, (C)
Weight of Dry Solids + Dish- L) • 9? gm. (A)
Calculations: U
(A) I L) % d S gym. - (B) gm.
% Dry solids= -------- -------------Divided By ------------------------
- --------------. x 100
(C) 61, )w I 2 b;rn.- (B) 11 1 . 6 I ) 9 gm.
o 3 J 9 I gm.
(---------- DIVIDED BY-------)X 100 = 5 % TOTAL DRY SOLIDS
a t ,'J. � 9 9 gm.
Sample D te-
DIGESTE
Volume Use 26 mi.
Date In Oven -
Time Li -
Weight of Dislr-
Weight of Wet Solids + DiS -
Weight of Dry Solids + Dish -
Calculations:
(A)
Date Out of Oven -
Time Out-
(B) gm.
Dry solids= - -Divided - x 100
(C) gin.- (B) g111.
_gin.
------__-_ °
�( DIVIDED BY--••----)X 100 = o TOTAL DRY SOLIDS
__gin.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
9.131
6.26
6.05
5.90
5.
5.
5.39
5.28
5.21
5.12
4.99
4.90
4.79
GRAHAM WWTP
WO0003824
7/11/14
23.7
7/11/14 0848
EC
7/11/14 0909
SS
1.4
23.5
22.0
Yo Dry Solids
legrees Celsius
legrees Celsius
Slope: 0.18
Intercept: 7.1
Correlation Coefficient: 0.81
Oxygen Uptake Rate: 10.57 mg Oxygen/hr.
Ambient Specific Oxygen Uptake Rate: 0.75 mg Oxygen/hr/g
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.86
Temperature Corrected Specific Oxygen Uptake .Rate: 0.65 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
g
8
7
8
4
3
2
1
O
Oxygen Uptake Rate Chart
1 2 3 4 5 8 7 8 A 10 11 12 13 14 15 16
Time (minutes)

Vector Attraction Reduction DATE:
Option 4 - SOUR LL
GRAHAM WWTP SOUR TS
DIGESTER:
J„ � � 8' � �1 i r�►1
i EMPERATURE AT COLLECTION: �� C. DO METER CALIBRATED: 7AT
IATE/TIME COLLECTED: 11 ) `� �% C� 2.3 %- `' a15 mg/L
AMPLED BY: i` C
ANALYSIS BEGAN DATE/TIME: I I ) i - 2 % SDI hm—
LNALYZED BY: 55
,NAYLSIS ENDED DATE/TIME: )) ) 4 — f ' (-) 9 Am-
IEGINNING SOUR TEST TEMPERATURE:
-NDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
0
)3
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S MFLE DA I j.-
DIGESTER DAI
DIGE�TER #1 SAMPLE TIME:
AIR:
TEMP. -
° CELSIUS
PH -
DO-
mg/L
ALKALINI Y - —
tng/L
NH3N-
mg/L
TSS -
mg/L
VSS -
mg/L
DIGESTER 02
\ SAMPLE TIME:
TEMP. -
° CELSIUS
PH -
--
mg/L
ALKALINITY -
tng/L,
i
NH3N-
mg/L
TSS
g/L
Ttmng/L
VSS =
i
DIGESTER #3
SAMPL + TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
0
mg/L
mg/L,
Sample Date- (9 ' `? - ) I
DIGESTER # 3
Volume Used - 26 mi. Q
Date In Oven- Date Out of Oven-
Time In- t� J� Time Out- (D/Y\
�7
Weight of Dish- 5 . 9 a O gm.(B)
Weight of Wet Solids + Dish- �u0. q 5_3 gIll.(C)
16 Weight of Dry Solids + Dish- °'A193 gm,(A)
Calculations: p
(A) 4 �3 $m. - (B) � -5c1C� i)Q O gin.
% Diy solids= ----------------------Divided By------------ ------ x 100
(C) �� ° I3,53 gmg
.- (B) I� QS m.
0 �52� gm.
L
---------- DIVIDED BY ------- )X 100 = r % TOTAL DRY SOLIDS
aLl . q qi W _5 fZ111.
Sample Date -
DIGESTER #
Volume Used - 26 I.
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish- gm.(B)
Weight of Wet Solids + Disli-
Weight of Dry Solids + Dish -
Calculations:
(A) gn
% Dry solids= ---------------------Divide
(C)__ gm.
gm.
----------- DIVIDED BY-------)X 100 =
MM
x 100
% TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.7
6.60
6.48
6.42
6.35
6.34
6.26
6.22
6.18
6.11
5.9
5.9
58
5_8
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
7/12/14
24.5
7/12/14 1353
SS
7/12/14 1356
SS
1.4
24.1
22.3
0.10
7.2
0.73
Yo Dry Solids
legrees Celsius
legrees Celsius
6.29 mg Oxygen/hr
0.45 mg Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate: 0.39 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
D
8
FA
�
E
`~ 8
CO 4
w
o
3
2
1
0
Oxygen Uptake Rate Chart
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16

Vector Attraction Reduction
Option 4 - SOUR DATE:
/
GRAHAM WWTP SOUR TES 4
DIGESTER:
TEMPERATURE AT COLLECTION: 9-1 , j a<--
DATE/TIME COLLECTED: LI I-A-)l`I
SAMPLED BY: S S
ANALYSIS BEGAN DATE/TIME: -) i 1 - 1, 5C- fc-N
ANALYZED BY: !,S S
%NAYLSIS ENDED DATE/TIME. 7 00 ► -• a. • I a P m
3EGINNING SOUR TEST TEMPERATURE
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
TD.O. mg/L
0
4
1
��I
2
, 60
3
c�
4
5
6
6 2) L-1
7
-
8
.1L2
9
In U
10
p I
11
• 0 5
12J
v
13
14
A r�
15
5.
9-1 Y3 C.
c
a'A . 3 c
DO METER CALIBRATED: / %� j I AT�

SAMPLE DATE- I oL
DIGES ER #1 SAMPLE TIME:
AIR:
TEMP. - ° CELSIUS
PH -
DO- mg/L
NH3N-
TSS - _
VSS -
DIGESTER #2
AIR:
TEMP. -
PH --
DO- _
ALKAL11,IITY -
NH3N-
TSS -
VSS -
_mg/L
mg/L
ing/L
mg/L
TIME:
I d FBI fro
Sample Date- I
DIGESTER #
Volume Used - 25 mi.
Date In Oven- a - ) Date Out of Oven- a -
Time In- ) 'f :� % P (y\ Time Out- % �J tD
Weight of Dish- �') 9 S ) Sc, gm.(B)
Weight of Wet Solids + Dish- 1 - 16 7 gill. (C)
Weight of Dry Solids + Dish- _ 337-?m.(A)
Calculations: y
(A) 5 . 3 % wni. - (B) 1 �i . gm.
% Dry solids= ---------------------Divided By--- ------------ x 100
(C) 6 J . 6 6 gill.- (B) gill.
° CELSIUS a '�3 5 5 1 gill.
i
---------- DIVIDED BY ------- ° j ( )X 100 /o = I � TOTAL DRY SOLIDS
ig/L ZI . � 3 � 9 gill.
DIGESTER #3 SAMPLE
AIR: - TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
°
mg/L
_mg/L
_mg/L
mg/L,
E:
US
_mg/L
mg/L
Sample Date -
DIGESTER #
Volume Used - 2b I.
(Date In Oven- Date Out of Oven -
Time In- Time out -
Weight of Dish-_ giu.(B)
Weight of Wet Solids + Dish -
Weight of Dry Solids + Dish -
Calculations:
(A) gill
Dry solids= ---------------------Divided B,
(C) gm.- (B)
gin.
(---------- DIVIDED BY-------)X 100 = _—
(C)
(A)
x 100
%'DOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date.
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
6.47
6.13
6.00
5.90
5.82
51 5
5.
5.
5
5.11
5.08'
GRAHAM WWTP
W00003824
7/14/14
25
7/14/14 1035
EC
7/14/14 1038
EC
1.4
25.1
24.2
Slope: 0.12
Intercept: 6.7
Correlation Coefficient: 0.81
Dry Solids
Degrees Celsius
Degrees Celsius
Oxygen Uptake Rate: 7.49 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.53 mg Oxygen/hr/g
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.78
Temperature Corrected Specific Oxygen Uptake Rate: 0.42 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Q
8
7
S
5
CD 4
— 3
2
1
O
Oxygen Uptake Rate Chart
77,
1 2 3 4 5 G 7 8 0 10 11 12 13 14 15 16
Time (minutes)

Vector Attraction Reduction I. -"
Option 4 - SOUR DATE: Q
GRAHAM WWTP SOUR fET
DIGESTER: 3
TEMPERATURE AT COLLECTION: S
ATE/TIME COLLECTED: 7�/ f 103S-APK
-AMPLED BY: -cc,
ANALYSIS BEGAN DATE/TIME: 7 .'`f D3P>�
ANALYZED BY: -�
�NAYLSIS ENDED DATE/TIME: .711 - 105-3 4M
0
IEGINNING SOUR TEST TEMPERATURE: r
rNDING SOUR TEST TEMPERATURE: ' Z �c'-
Time in Minutes
D.O. mg/L
0
�a
1
'
2
3
3
.00
4
, 01d
5
5, 6 7
6
/
7 lD
7
�S
8
Sr�f
S
10
Sr
11
Sid
12
13
jam, -21�
14
1 9_2
15
rob
DO METER CALIBRATED: r AT
ZO G ' 3� % - r mg/L

SAMPLE DA 1E-
a —ICA_ Ll
DIGESTER DATA
DIGESTER 91
SAMPLE TIME:
AIR:
-
° CELSIUS
PH -
i
DO-
mg/L
ALKALINITY -
tng/L
NH3N- _
mg/
TSS -
mg/L
VSS -
mg/L
i
DIGESTER #2
S MPLE TIME:
i
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIUS
_mg/L
_mg/L
_mg/L
mg/L
DIGESTER #3 SAMPLE T!
AIR: -
TEMP. -
PH-
DO- _-
ALKALINITY -
NH3N-
TSS -
VSS -
° CF
mg/L
W
IUS
_mg/L
mg/L
Sample Date- J Ll
DIGESTER # 3
Volume Used - 25 mi. .
Date In Oven- 7 1 `� / Y Date Out of Oven- 1 l S
Time In- /a 3 / Time Out- G 0 4Aj
Weight of Disli-_gm.(B)
Weight of Wet Solids + Dish- 0 6 2-cl0 gm.(C)
Weight of Dry Solids + Dish- 'IC, J/d Y3 gni.(A)
Calculations:
(A) . `1a`� gm. - (B) 9 gm.
% Dry solids= ---------------------Divided Bv------------------------ x 100
(C) 70, (..2,Gi 0 gm.- (B) 0 SS % gin.
(---------- DIVIDED BY ---
Sample Date
DIGESTER #
Volume Used - 25
)X 100 = 1 0 � % TOTAL DRY SOLIDS
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish- gm.(B)
Weight of Wet Solids + Dish- gill
Weight of Dry Solids + Dish- .gm.
Calculations:
(A) gm. - (B)
% Dry solids= --------------------- Divided By ------------
(c) gin.- (B)
x 100
(---------- DIVIDED BY-------)X 100 = _ % TOTAL DRY SOLIDS

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Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14'
15
Facility Name:
Biosolids Permit Number:
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.9
7.1
7.01
7.18
7.17
7.08
7.06
6.6 J
6.61
GRAHAM WWTP
WQ0003824
10/1/14
19.1
10/1 /14 0938
EC
10/1 /14 0945
SSS
1.4
19.5
20.1
Slope: 0.08
Intercept: 7.6
Correlation Coefficient: 0.69
Dry Solids
legrees Celsius
legrees Celsius
Oxygen Uptake Rate: 4.70 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.34 mg Oxygen/hr/g
Average Temperature: 20 degrees Celsius
Temperature Correction Factor: 1.00
Temperature Corrected Specific Oxygen Uptake Rate: 0.34 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Oxygen Uptake Rate Chart
y =-0.0783x + 7.7095
10
:3
-
-
9
A a
n.,
-a,
z .
< a
xv
n
a�
i
f'
5
�.
I
a
-
Q
m
s
—
r
,
2
- ,
p
< ,
0
6 7 8 9 10 11 12 13 14 15 16
1
2 3 4 5
Time (minutes)

_ctor Attraction Reduction
Dption 4 - SOUR DATE: 1 - D� r -'
GRAHAM WWTP SOUR TEST
DIGESTER: 3
�MPERATURE AT COLLECTION: l I oC'
1 kTE/TIME COLLECTED: )OWN
�A,MPLED BY: ��-
ANALYSIS BEGAN DATE/TIME: W))
4ALYZED BY: 'S
DO METER CALIBRATED: AT 1 1 7-'
J 0 2, 3 %- �, J)� mg/L
qAYLSIS ENDED DATE/TIME: I� I ICI
EGINNING SOUR TEST TEMPERATURE: C_
FNDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L
0
3
3
�� D
4
s�v
7
Dfo
8
�.DJ
9
10
11
12'
b
13
_
14
6 •6%
15
6

SAMPLE DATE -
I - UC-7�
DIGESTER #1 SAMPLE TIME:
AIR:
TEMP. ° CEL SIUS
PH -
DO- mg/L
ALKALINI' Y - mg/L
NH3N- \ mg/L
TSS - mg/L
VSS - , mg/L
DIGESTER #2 AMPLE TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
CELSIUS
mg/L
mg/L
� mg
/L
\\ —mg/L
mg/L,
DIGESTER #3 SAMPLE TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS ..
° CELSIUS
mg/L
mg/L,
mg/L
mg/L
mg/L
Sample Date-
DIGESTER #
Volume Used - 25 mi.
Date In Oven- — � '- Date Out of Oven- J } V
Time In - ---I. 3Time Out- - j KM
Weight of Dish- H H - S-35 1 c�gm•(B)
Weight of Wet Solids + Dish- �u 9 3 1 ) 2— gm. (C)
Weight of Dry Solids + Dish- ) g� �� gm.(A)
Calculations: V
(A) q ii,i 6 D gm. - (B) gm.
% Dry solids= ------------------- -Divided By----------------------- x 100
(C) �' 1 12 gm.- (B) � . Jr� gm.
.13906 gm.
DIVIDED BY-------)X 100 = _ % TOTAL DRY SOLIDS
Sample Date -
DIGESTER #�
Volume Used -\25 mi.
Bate In Oven- Date Out of Oven -
Time hi- Time Out -
Weight of Dish- gm.(B)
Weight of Wet Solids + Disci- gm.(C)
Weight of Dry Solids +Dish\-\ _gm.(A)
!Calculations:
(A) In.
%Dry solids=---------------------Divlt,
(C) gin.-
(---------- DIVIDED BY-------)X 100 =
- (B) gin.
edBy------------------------ x 100
gm.
% TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
l
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.94
8.38
8.25
8.23
8.17
8.16
7.92
7.93
7.86
7.70
7.63
7.68
7.54
7.42
7.32
7.16
GRAHAM WWTP
WO0003824
10/2/14
19.4
10/2/14 0928
EC
10/2/14 0935
SSS
1.4
19.7
20.2
Yo Dry Solids
degrees Celsius
degrees Celsius
Slope:
0.09
Intercept:
8.6
Correlation Coefficient:
0.97
Oxygen Uptake Rate:
5.53 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.39 mg Oxygen/hr/g
Average Temperature:
20 degrees Celsius
Temperature Correction Factor:
1.00
Temperature Corrected Specific Oxygen Uptake Rate: 0.39 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

10
9
8
7
8
~ 5
�
UO 4
m
3
2
1
0
y =-U.0Q21x+ 8.076
Oxygen Uptake Rate Chart
1 2 3 4 5 G 7 O Q 10 11 lZ 13 14
Time (minutes)

actor Attraction Reduction - c3o l
Option 4 - SOUR DATE: C
GRAHAM WWTP SOUR TEST
DIGESTER:
_MPERATURE AT COLLECTION: C DO METER CALIBRATED: C I AT
Y
T
C� r
\TE/TIME COLLECTED: Ia �� 14 I j � � %- ( mg/L
SAMPLED BY:
tANALYSIS BEGAN DATE/TIME: i 1 � 90.3
4ALYZED BY: `J S
14AYLSIS ENDED DATE/TIME: 10 5 1 NX\
"EGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE: ' �c
Time in Minutes
D.O. mg/L
- 0
g qli
- 1
2
I `�
3
4
`
5aq�
6
—1
7
8
vg
9
10
4�<
11
12
13
14
Z,
15

SAMPLE DATE-
DIGEqER #1
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
DIGESTER #2
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
SAMPLE TIME
° CELSIUS
mg/L
mg/L
mg/L
mg/L
mg/L
SAMP E TIME:
° ELSIUS
mg/L
Sample Date- c*ob f.L - H
DIGESTER #
Volume Used - 25 ml.
LA P -� -
Date In Oven- �(]� �r' Date Out of Oven-
dz 4
Time In- "I r 6 �� Time Out- -7
Weight of Dish- 26 gm.(B)
Weight of Wet Solids + Dish--% 6. O 3 9 f gni.(C)
Weight of Dry Solids + Dish- 9.5. 13 &5 gm.(A)
Calculations: IJ
(A)
% Dry solids= ---------------------Divided By------------------------ x 100
(C) 70 , o `3 91 gym. - (B) � J , S276, gin.
DIVIDED BY-------)X 100 = Z % TOTAL DRY SOLIDS
'JL-5.1 S ), 5 em.
mg/L
mg/L
%Sample D e-
ig/L
Vo�ume Used - S mi.
DIGESTED #3 SAMPLE TIME
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
° CELSIU
mg/L
m6
mg/L
mg/L
mg/L
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish- gm.(B)
Weight of Wet Solids + Dish- gm,
Weight of Dry Solids + Dish -gin.
Calculations:
(A) gm. - )
% Dry solids= ---------------------Divided By ----------
(C) gin.- (B)
gin.
(---------- DIVIDED BY-------)X 100 = °/
gin.
(C)
(A)
x 100
AL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
8.89
7.98
7.84
7.74
7.79
7.70
7.65
7.57
7.55
7.54
7.44
7.39
7.32
7.22
7.16
7.15
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
W00003824
10/3/14
20.1
10/3/14 1000
SP
10/3/14 1008
SSS
1.4
20.4
20.8
0.08
8.2
0.87
Yo Dry Solids
legrees Celsius
legrees Celsius
4.57 mg Oxygen/hr
0.33 mg Oxygen/hr/g
21 degrees Celsius
0.95
Temperature Corrected Specific Oxygen Uptake Rate: 0.31 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

o
10
Q
8
7
3
2
1
O
Oxygen Uptake Rate Chart
1 2 3 4 5 8 7 8 Q 10 11 12 13 14 15 16
Time (minutes)

�, _ ctor Attraction Reduction V LQ J_ P
Dption 4 - SOUR DATE: 6
GRAHAM WWTP SOUR TEST
DIGESTER: .3
0
'MPERATURE AT COLLECTION: ac , c
JE/TIME COLLECTED: W `3 ) m- J o. o o
F'\MPLED BY: j
RNALYSIS BEGAN DATE/TIME: (3 13 14
4ALYZED BY: 153
DO METER CALIBRATED: j AT .O
G,D. .o_ g • )­mg/L
4AYLSIS ENDED DATEITIME: l0 131 )4 a- 1 0 : ✓` I hn
GINNING SOUR TEST TEMPERATURE:
%) , '-I �3 c_
u
PNDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mg/L.
0
2
3
7 `�
4
%•��
5
g
7, G ,J
7
�
8
7 �� • ` s
9
10
11
12
13
14
d �• (o
15
�'�

SAIL _3 DA 11C- _ ") -- k-.; I
Qz" - I
Q'
PH -
DO-
DIGESTER D.
TER #1 SAMPLE TEAE:
° CELSIUS
mg/L
fil
ALKAL ITY - mg/L,
NH3N-
mg/L
TSS -
mg/L
V S S -
_ mg/L
DIGESTER #2
SAMPLE TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
_° CELSIUS
mg/L
mg/L
_mg/L
\ mg/L
T Mg/L
DIGESTER #3 SAMPLE TIME:
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
_° CEISIU4
mg/L
I g/
mg
mg/L
mg/L
Sample Date- .5 -- O C;)-o bQT -) `i
DIGESTER # —3
Volume Used - 25 mi.
Date In Oven- 3 - O G�ZL2r-)! Date Out of Oven- 3
Time In- 1O `. �� 9 wm Time Out- m
Weight of Dish- H (, S 9 ),5` gm.(B)
Weight of Wet Solids + Dish-'? I 70 gm.(C)
Weight of Dry Solids + Dish- 1"� r) '1,5 gm.(A)
Calculations:
(A) L} % ) 6 S gm. - (B) y (. `� 1 S gm.
% Div solids= ---------------------Divided By------------------------ x _gin.
(C) 7Q gm.- (B) I-) LI , 9Ll )s
1 3 t'1 3c) gm.
(---------- DIVIDED BY-------)X 100 = ' % TOTAL DRY SOLIDS
a. , 6 J z gin.
Sample te-
DIGESTE
Volume Use - 25 mi.
Date In Oven -
Time In -
Weight of Dish -
Weight of Wet Solids +
Weight of Dry Solids + I
Calculations:
(A)
% Dry solids= -----------
Date Out of Oven -
Time Out -
gm. (B)
(C)
(A)
- (B) gm.
ed By------------------------ x 100
- (B) gall.
gm.
(---------- DIVIDED BY-------)X 100 =
gm.
% TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
(mg/1)
8.34
10.13
9.67
9.49
9.41
9.32
9.25
9.17
9.17
9.15
8.89
9.04
9.02
8.99
8.98
8.96
GRAHAM WWTP
WQ0003824
10/6/14
14.9
10/6/14 0957
EC
10/6/14 1001
EC
1.4
16.0
.17.5
o Dry Solids
iegrees Celsius
tegrees Celsius
Slope:
0.03
Intercept:
9.4
Correlation Coefficient:
0.40
Oxygen Uptake Rate:
1.98 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate:
0.14 mg Oxygen/hr/g
Average Temperature:
17 degrees Celsius
Temperature Correction Factor:
1.23
Temperature Corrected Specific Oxygen Uptake Rate: 0.17 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes.
The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

12
10
8
, 2
0
Oxygen Uptake Rate Chart
. ..... .
.. ......
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16

actor Attraction Reduction t 1
Option 4 - SOUR DATE:
RAi;AM WWTP SOUR PEST
DIGESTER: 3
EMPERATURE AT COLLECTION:
ATE/TIME COLLECTED: Ia�
-qgMPLED BY: I �c--
/ANALYSIS BEGAN DATE/TIME: (0 1 6� I j — 10 � F �oy\
14ALYZED BY: L
JAYLSIS ENDED DATE/TIME: b )1y ` vv�
—EGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE: 1 7' c�
Time in Minutes
D.O. mg/I_
0
2
e 7
a
3
clr41
4
7
5
9.,32
s
q, zs
7
C'
$
Cl Er
9
.
10�
8
11
+
12
:cc) z
13
8 199
14
0 , 9
15
/6
8,9 /
c
DO METER CALIBRATED: AT
I � �

DIGESTER DATA PERCENT DRY SOLIDS
DIGESTER #1 SAMPLE TIME: Sample Date-
TEM� ° CELSIUS VoGume Used - 25 mi.
PH - � ^. I Date In Oven- - d c)O�U-)9 Date Out of Oven- % C C-
i
DC)- ,; mg/L Time In- Ar') Time Out-
ALKALII CITY - mg/L Weight of Dish- 9 0 . x c� L . gm.(B)
N143N- mg/L Weight of Wet Solids + Dish- b "S • L I gm, (C)
TSS - mg/L Weight of Dry Solids + Dish- q o -5 9 % 2 gm.(A)
VSS - , mg/L Calculations: _ 1
(A) 22- gm. - (B) 1 Z gin.
%Dry solids= ----------------- Divided By - -- ------ x 100
DIGESTER #A SAMPLE TIME: � (C)_ 6,� S x )3,5 gm.- (B) 3 ��t� � � _gm.
AIR;
TEMP. - ° CELSIUS gm.
PH - _ j (---------- DIVIDED BY - )X 100 - I /o TOTAL DRY SOLIDS
DO- mg/L IN��...�i � � � 13 gm.
ALKAL
NH N- II�IITY _ mg/L ;Sample Date-
---!`—
TSS - t mg/L IDIGESTEli\#
VSS - mg/L Date In Oven- mi.Date Out of Oven-,
i
i
Time In -
Time Out -
DIGESTER #3 SA.MP E TIME: Weight of Dish- gm.(B)
AIR, Weight of Wet Solids + Di-—gm.(C)
TEMP. - ` ELSIUS Weight of Dry Solids + Disll,� _gm.(A)
i
PH- Calculations:
ALKALINITY - tng/L % Dry solids=---------------------Divi B x 100
g/
NH3N- mg/L (C) gin.- ) __ gin.
TSS - m L -- __gm.
i
VSS - ____ _ _ Ma(---_______ DIVIDED BY-------)X 100 = % TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name;
Biosolids Permit Number:
Date;
Digester Temperature;
Sampling Date/Time:
Sampled By:
Analysis Date/Time-
Analyzed By:
Total Solids;
Beginning Temperature
End Temperature
Dissolved Oxygen Level
i.92
.69
8.62
8.25
8.19
8.13
LA
GRAHAM WWTP
WQ0003824
10/7/14
15.2
10/7/14 1110
EC
10/7/14 1117
SS
1.4
17.2
18.4
% Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.05
Intercept: 8.7
Correlation Coefficient: 0.96
Oxygen Uptake Rate: 3.08 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.22 mg Oxygen/hr/g
Average Temperature: 18 degrees Celsius
Temperature Correction Factor: 1.14
Temperature Corrected Specific Oxygen Uptake Rate: 0.25 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

a
8.4
X
8
D .2
o
8
7.8
7.6
7.4
Oxygen Uptake Rate Chart
1 2 3 4 5 8 7 8 0 10 /6 /14 o m
Time (minutes)

I- -tor Attraction Reduction 7 _ oc- p )ption 4 - SOUR DATE. 1
GRAHAM WWTP SOUR TEST
DIGESTER: 3
cMPERATURE AT COLLECTION:
TE/TIME COLLECTED:
A,MPLED BY: 1 �C
%NALYSIS BEGAN DATE/TIME:
IALYZED BY: SS
dAYLSIS ENDED DATE/TIME:
GINNING SOUR TEST TEMPERATURE
ENDING SOUR TEST TEMPERATURE:
Time in Minutes D.O. mg/L
o
2
3
A
5
1
6
�0•�0
DO METER CALIBRATED: d 1.� AT )G
mg/L

', l
SAMPLE DTrE- � - U
DIGESTER #1
AIR: n )__
TEMP. - 02 °CELSIUS
PH-
DO- 4 tng/L
ALKALINITY - a3(� mg/L
NH3N- 1. nlg/.L
TSS - 15 o 3o mg/L
VSS- mg/L
DIGESTER #2
AIR:
SAMPLE TIME:
SAMPLE TIME:
TEMP. - oZ 3 ° CELSIUS
PH
DO- nig/L
ALKALINITY - 9,t mg/L
NH3N- U - �j mg/L
TSS - b / mg/L
VSS - mg/L
Sample Date -
DIGESTER #
Volume Used - 25 mi.
Date In Oven-
Date Out of Oven- O - 0 4- 1 q
Time In- 37 on Time Out-
Weight of Dish- ) - � q gm. (B)
Weight of Wet Solids + Dish- E . ') 2-20 gm.(C)
Weight of Dry Solids + Dish- �) • %U 2� gm.(A)
Calculations:
(A) I 70gm. - (B) �) y 50 gill.
/ % Dry solids= ---------------------Divided By--C-�---------------------- x 100
l 2 j (C) u 0 gin.- (B) 1 / _gm.
#3 SAMPLE TAmE: 0 -A�vv\
AIR:: Cry'( /
'S Z °
TEMP. - / CELSIUS
PH - °/b
DO- l3 • i S mg/L
ALKALINITY -
tng/L
NH3N-
tng/L
TSS - , U
mg/L,
VSS -
gill.
(---------- DIVIDED BY-------)X 100 = U 9 �� % TOTAL DRY SOLIDS
al. cjz7a gill.
Sample Date- 7- o U6i�,zr-- L 1
DIGESTER # 3
;Volume Used - 25 mi.
7;
;Date In Oven- �� � (.;��.''�`,_ Date Out of Oven- 'XK `"
Time ICI- i :1 .RM Time Out- 2,5 II P nl
%Weight of Dish- `�) • `�`f gm.(B)
Weight of Wet Solids + Dish- cl 2J 2-- gm.(C)
Weight of Dry Solids + Dish- L- � ZI _gm.(A)
Calculations:
(A) ) 1 gnl. - (B) gm.
% Dry solids= ---------------------Divided By----------------------- x 100
(C) gin.- (B) gin.
(---- __�. DIV�I?DED BY-------)X 100 = °io TOTAL DRY SOLIDS

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By.
Analysis Date/Time
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9.03
8.54
8.45
8.56
8.49
8.42
8.31
8.07
7.85
7.95
7.73
7.69
1 t 7.67
7.67
GRAHAM WWTP
WO0003824
10/8/14
16.8
10/8/14 0925
SP
10/8/14 0930
SS
1.4
17.5
18.7
Slope: 0.08
Intercept: 8.8
Correlation Coefficient: 0.95
o Dry Solids
Degrees Celsius
legrees Celsius
Oxygen Uptake Rate: 4.82 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.34 mg Oxygen/hr/g
Average Temperature: 18 degrees Celsius
Temperature Correction Factor: 1.14
Temperature Corrected Specific Oxygen Uptake Rate: 0.39 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

9.5
7.1
8.5
8
cn
— 7.5
7
6.5
Oxygen Uptake Rate Chart
1 2 3 4 5 0 7 8 Q 10 11 12 13 14 15 10
Time (minutes)

ector Attraction Reduction�,r_
Option 4 - SOUR DATE:
GRAHAM WWTP SOUR TEST
DIGESTER:
EMPERATURE AT COLLECTION: J �L
,ATE/TIME COLLECTED: I� ��� ►`� - �� ; �� Ate.
'AMPLED BY:��
,-,NALYSIS BEGAN DATE/TIME: �� 1`i - �'• 3e A
NALYZED BY: S
io [s! )q
DO METER CALIBRATED: AT
C O -1. 3 % - mg/L
,NAYLSIS ENDED DATE/TIME: 10 L ) `i - 9 - 4 s W\
IEGINNING SOUR TEST TEMPERATURE
ENDING SOUR TEST TEMPERATURE:
Time in Minutes
D.O. mpg/L
0
q .o3
1
1� 0 59
2�
/
3
4
5.
6
{U o
7
V
8
S � 0 S
9
�. 9�
10�
11
�7
12
13
�•�
14
(o
0 15
7.67

L
SAMPLE DA'111- 6 — u �J 0 I
DIGESTS #1
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
SAMPLE TIME:
° CELSIUS
mg/L
Jng/L
mg/L
mg/L,
mg/L
DIGESTER #2 SAMP E TIME:
AIR: --
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
PERCENT DRY SOLIDS
Sample
i
DIGESTER # -
Date In Oven- S- 0c)mS-14 Date O ut Oven -
Time
o f n- - Time In- `"I ). �\ "Y� Time Out- -7 S P(,\
Weight of Dish-_ y U gm.(B)
Weight of Wet Solids + Dish- 6 Iq . �9 8G gm.(C)
g ��•� 2 Weight of Dry Solids +Dish- gill, (A)
�i u
Calculations:
A) gm. - (B) �
1 ,.l9() m. g
% Dry solids= ---------------------Divided By------------------------ x 100
--- -- % (C)- 0 - 6 9 90 gym.- (B) gm.
° C;ELSIUS % `� gm.
(---------- DIVIDED BY ------
1
DIGESTER #3 SAMPLE
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
mg/L
mg/L
° CELSIUS
mg/L
—mg/L
,mg/L
_mg/L
mg/L
)X 100 = Lj % TOTAL DRY SOLIDS
Sample Dat -
DIGESTER
Volume UsedT-5el.
Date In Oven- Date Out of Oven -
Time In- Time Out -
Weight of Dish- gm.(B)
Weight of Wet Solids + Di 1- gm.(C)
Weight of Dry Solids + Dish- gm.(A)
Calculations:
(A) nI B) gm.
% Dry solids=---------------------Divi By------------------------ x 100
(C) _gm.- ( gm.
(---------- DIVIDED BY-------)X 100 = \ % TOTAL DRY SOLIDS

Facility Name,
I_ Biosolids Permit Number:
Date:
1 Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time',
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Time
(minutes)
0
1
2
3
,4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
101
8.62
8.56
8.51
8.37
8.31
8.24
8.18
8.20
8.13
7.93
7.93
7.87
7.85
GRAHAM WWTP
WQ0003824
10/9/14
19.8
10/9/14 1039
EC
10/9/14 1043
SS
1.4
18.0
18.9
Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.07
Intercept: 8.8
Correlation Coefficient: 0.96
Oxygen Uptake Rate: 4.16 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.30 mg Oxygen/hr/g
Average Temperature: 18 degrees Celsius
Temperature Correction Factor: 1.14
Temperature Corrected Specific Oxygen Uptake Rate:L 0.34 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically
Updated 10/23/2013

9.5
IN
8.5
0
UO 8
7.5
7
Oxygen Uptake Rate Chart I
... ...... .
T5,
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16
Time (minutes)

_ actor Attraction Reduction C� j
Option 4 - SOUR DATE: I - 0
GRAHAM WWTP SOUR TEST
,A
DIGESTER. � C c toig hl
EMPERATURE AT COLLECTION: 1 �G DO METER CALIBRATED: •-� �IQ)m (a 35 F
ATE/TIME COLLECTED: )0 19119 O 39 4M
SAMPLED BY:�
ANALYSIS BEGAN DATE/TIME: Jo 19 I`i
NALYZED BY:
NAYLSIS ENDED DATE/TIME: �� 9 1 10 • I ��
IEGINNING SOUR TEST TEMPERATURE:
ENDING SOUR TEST TEMPERATURE: _
Time in Minutes
D.O. mg/L
0
�ml�
2
3
4
5�51
6
-3
7
9..
s
9
10
2�
IT
� 1
12
., 93
13
14
gi
15
1b-�. %- '61 �, mg/L

SAMPLE DATE- _ I - C-A o 6-�) M—) 1
DIGESTER #1 SAMPLE TIME:
AIR:
0"
TEMP.
°CELSIUS '
PH -
DO-
ALKAL Y -
tng/
NH3N-
m
TSS -
mg/L
VSS -
mg/L
DIGESTER #2 SAMPLE
TIME:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
DIGESTER #3
AIR:
TEMP. -
PH -
DO -
ALKALINITY -
NH3N-
TSS -
VSS -
CELSIUS
mg/L
mg/L
mg/L,
mg/L
mg/L
SAMPLE T E:
° CEL IUS
mg/L
m L
m L
mg/L
mg/L
Sample Date- - C)wba-r-
DIGESTER # 3
!Volume Used - 25 mi.
Date In Oven- - Oc; uc6 T-H Date Out of Oven-,o _ oc-a�-r- 4 -{
Time In- 10 Pin Time Out- I a�
Weight of Dish- H 2-5 gm.(B)
Weight of Wet Solids + Dish- �J,� I . �� �Z-7 gm.(C)
Weight of Dry Solids + Dish- I •5 3 ,5gm.(A)
Calculations: U
(A) 9 9 • 5 3J m. - (B) 1 ) gJJ gm.
% Dry solids= ---------------------Divided By------------------------ x 100
(C) 69. C S )J gm.- (B) 19 . 1 S -cSS gm.
2-5C)`I
(--------••- DIVIDED BY ------
0 I - 909 ) oL gm.
)X 100 = ) ' I % TOTAL DRY SOLIDS
Sample Dat�-
DIGESTER \\
Volume Used - 2 ml.
Date In Oven- Date Out of Oven -
Time In- Time But -
Weight of Dish- gm.(B)
Weight of Wet Solids + Dis - gm.(C)
Weight of Dry Solids + Dish- gm.(A)
Calculations:
(A) i7-(B)_ gin.
% Dry solids= ---------------------Div �ed By------------------------ x 100
(C) gmB) gm.
(---------- DIVIDED BY-------)X 100 = \ % TOTAL DRY SOLIDS

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY15-SL005194
Client: City of Graham-VVVVTP
Advisor: NC DENR/WSRO
¢tia,uiu��,
Predictive PO Drawer 357
3503 Swepsonville-Saxapahaw Rd
585 Waughtown St.
Winston Salem, NC
a t Graham, NC 27253
}g, Soil Report Mehlich-3 Extraction
..
27107
Sampled County: Alamance
Sampled: 06/30/2014 Received: 09/11/2014 Completed: 09/22/2014 Farm:
Links to Helpful Information
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or 7" to alert you that copper and/or zinc have accumulated in the soil and are approaching
a level that could be detrimental to
crop production. The C and Z symbols are printed on your report for soil test index levels of 2000 or more; for peanuts with zinc, the level is 300. This note is designed to be a "trigger"
that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu &amp; Zn has
been set at 3000 index; for peanuts with zinc, the level is 500. These levels are used by DENR as a benchmark to determine when application of
waste products should be stopped.
The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field.
Sample ID: 001
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6 K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0 120-200 0 60 0 0 pH$ 0
0 0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0 120-200 0 60 0 0 pH$ 0
0 0
Note: 12 Note:
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral
HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.66 1.02 43.1 100 0.0 7.2 444 40 94 6 134 463 276 276 1502 1502
1043 0.3 1
Sample ID: 002
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0 120-200 0 100 0 0 pH$ 0
0 0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0 120-200 0 100 0 0 pH$ 0
0 0
Note: 12 Note:
Test Results [units - WIV in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral
HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI
Cu-1 Na ESP SS -I NO3-N
0.46 1.09 26.4 100 0.0 7.3 346 21 92 7 54 552 329 329 1097 1097
1007 0.3 1
North Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: vv ivw.ncagr.gov/agrohomi/
Report No..
FY15-SL0051,94
Page 2 of 4
Sample ID: 02C
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1
0.0
120-200 0
70
0
0
pH$
0
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim,
0.0
120-200 0
70
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WN in
g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.60 1.03 28.1
99 0.3 7.1
397 33
88 10 66
371
223
223
1293
1293
1044
0.3
1
.Sample ID: 003
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1
0.0
120-200 0
70
0
0
pH$
0
0
0
Note: 12 Note:
2 - Fescue/OGrass/Tim,
0.0
120-200 0
70
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WN in
g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/drr?]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg% 8-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.60 0.88 70.0
100 0.0 7.2
320 32
96 _ 3 221
447
267
267
1383
1383
1042
0.3
0
Sample ID: -004
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1
0.0
120-200 0
90
0
0
pH$
0
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim,
0.0
120-200 0
90
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - W/V in
g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dO]:
Soil Class:
Mineral
HM%1 WN CEC BS% Ac pH
P-I, K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.41 0.92 62.9 100 0.0 7.3
452 25
96 4 169
379
224
224
1874
1874
1356
0.6
1
Sample ID: 005
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1
0.0
120-200 0
80
0
0
pH$
0
0
0
Note: 12 Note:
2 - Fescue/OGrass/Tim,
0.0
120-200 0
80
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WN in
g/cnf; CEC and Na in meq/100 crrr3;. NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 0.93 59.5 100 0.0 7.1
347 29
97 3 179
299
179
179
1423
1423
1166.
0.3
1

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY15-SL005194
Page 3 of 4
Sample ID: 006
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1
0.0
120-200 0
80
0
0
pH$
Z
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim,
0.0
120-200 0
80
0
0
pH$
Z
0
0
Note: 12 Note:
Test Results [units - WIV in
g/crrP; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.56 0.96 62.6
100 0.0 7.3
587 31
95 4
136
222
130
130
2033
2033
1270
0.4
1
Sample ID: 007
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1
0.0
120-200 0
100
0
0
pH$
0
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim,
0.0
120-200 0
100
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WIV in
g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
0.51 1.01 47.5
100 0.0 7.5
415 20
96 4
108
224
128
128
1172
1172
1075
0.2
0
Sample ID: 008
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1
0.0
120-200 0
90
0
0
pH$
0
0
0
Note: 12 Note:
2 - Fescue/OGrass/Tim,
0.0
120-200 0
90
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WIV in g/crrP; CEC and Na in meq/100 crrr3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.32 1.06 32.1
100 0.0 7.7
136 24
96 4
75
673
396
396
352
352
490
0.2
1
Sample ID: 010
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K20
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1
0.0
120-200 0
110
0
0
pH$
0
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim,
0.0
120-200 0
110
0
0
pH$
0
0
0
Note: 12 Note:
Test Results [units - W/V in
glcnf; CEC and Na in meq/100 ed; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 1.09 37.8
100 0.0 7.7
155 17
96 4
93
855
505
505
360
360
430
0.3
1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY15-SL005194'
Page 4 of 4
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%.
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-AI1
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-n- I
manganese index
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncagr.pov/agronomi/obpart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS-1, Na, ESP, SS -I, NO3-N (not
Zn-I
zinc index
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrst.htm
for more information.

February 12, 2015
Mr. Victor Quick
City Manager
P.O. Drawer 357
Graham, NC 27253
Dear Mr. Quick:
Enclosed is the information for your use in completing your 2014 NCDENR Annual
Report.
If you have any questions or comments, please contact me at [phone] x14.
Sincerely,
1
Nate Roth
Synagro
Enclosures
284 Boger Road, Mocksville, NC 27028
Phone [phone] • Fax: [phone] e [phone]

CITY OF GRAHAM, NC
MEBANE, WTP
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003824
2014 ANNUAL REPORT
INFORMATION

City of Graham, NC
Mebane WTP
Residuals Land Application Program
2014 Annual Report
Information
TABLE OF CONTENTS
Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Page
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
1 5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORfllll
Permit Number W00003824 County Alamance Year 2014
Facility Name (as shown on permit) City of Graham -Mebane WTP NPDES No. NCO045292
Land Application Operator SynaQro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A and Part Band proceed to the certification. Also, if residuals were generated
but not land applied, please attach an explanation on how the residuals were handled.
PART A
Total number of application fields in permit: 9
Total number of fields land application occurred during the year: 2
Total amount of dry tons applied during the year for all application sites: 94.41
Total number of acres land application occurred during the year: 17.8
PART B
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not
limited to items 1-12 below) issued by the Division of Water Quality X YES NO.
If no, Please provide a written description why the Facility was not compliant, the dates, and explain corrective action
taken.
1.
Only residuals approved for this permit were applied to the permitted sites.
2.
Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least
6.0 or the limit specified in the permit.
3.
Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3)
copies of laboratory results are attached.
4.
Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5.
All other monitoring was performed in accordance with the permit and reported during the year as required and
three (3) copies of certified laboratory results are attached.
6.
The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (Applicable to 40 CFR Part 503 regulated
facilities).
7.
All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (Applicable to 40 CFR Part 503 regulated facilities).
8.
All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
'
prior authorization was received from the Division of Water Quality.
9.
No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10.
Vegetative cover as specified in the permit was maintained on this site and crops grown were removed in
accordance with the crop management plan.
11.
No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12.
All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Victor Quick, Utilities Director Jb-�
Pennittee Name and Title (type or print) na re f Date _
gnatur of Preparer* Date Signature of Land Applier Date
(if different fiom Pernittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9(r) DENR FORM ACF (5/2003)

2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
GRAHAM, NC
GRAHAM, NC MEBANE WTP LIQUID
MONTHNEAR
May 2014
YEARLY TOTAL
AMOUNT UNIT
421,600.00 G
421,600.00 G
DRY METRIC
DRY TONS UNIT TONS
94.41 D 85.62
94.41 D 85.62
1 /2812015

2014 ANNUAL REPORT
PROJECT:
FACILITY:
WTP NPDES:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Graham
Graham, NC
Graham WTP
P.O. Drawer 357
Graham, NC 27253
336-578-3264
NCO045292
Victor Quick, Utilities Director
P.O. Drawer 357
Graham, NC 27253
336-578-3264
James Carson, Supervisor
P.O. Drawer 357
Graham, NC 27253
336-578-3264
Synagro Central, LLC
Contact: Marshall Puryear
[phone] ext. 17

M
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003824
Facility Name: GRAHAM, NC
NPDES# : NCO045292
or WQ# (residual only)
WWTP Name: GRAHAM/MEBANE WTP
Residuals Analysis Data
Product Type
WPL
Date Sampled (grab) or 05/08/14
Date Composited
Percent Solids
5.37
PARAMETERS (mg/kg dry weight)
Arsenic
4
Cadmium
<2
Mercury
<0.4
Chromium
35
Copper
38
Lead
22
Molybdenum
<5
Nickel
47
Selenium
<5
Zinc
66
Total Phosphorus
1020
TKN
9310
Ammonia -Nitrogen
1860
Nitrate and Nitrite
55.9
Laboratory
A&L Eastern Laboratories Inc.
"I certify, under,penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information 'submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
TU OF PREPARER)
Date P-qr/S
DENR FORM RSSF (5/2003) Printed: Wednesday - January 28 2015 at 14:39:47 for: 2036 01

M
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003824
Facility Name: GRAHAM, NC
NPDES# : NCO045292
or WQ# (residual only)
WWTP Name: .GRAHAM/MEBANE WTP
Residuals Analysis Data
Product Type WPL
Date Sampled (grab) or 05/08J14
Date Composited
Percent Solids 5.37
PARAMETERS (mg/kg dry weight)
Aluminum
22000
Calcium
2490
Magnesium
1080
pH
6.82
Potassium
622
Sodium
2720
Laboratory
A&L Eastern Laboratories Inc.
I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(S[G- ATU M O
NR - Data Not Reported or Data Not Required
Date a- —/
DENR FORM RSSF-B (7/2002) Printed: Wednesday - January 28 2015 at 14:40:07 for: 2086 01

Page: 1 of 2
Report Number: 14-129-0209
Account Number: 46457
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/GRAHAM
MARY BREWER #51-0025
284 BOGER RD
MOCKSVILLE , NC 27028
p A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond Virginia 23237 [phone] Fax [phone]
www,aleastern.com
Project: GRAHAM WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 5/8/2014 09:15:00
Lab Number: 55276 Date Received: 05/09/2014 00:00
Sample Id: GRAHAM WTP Date Reported: 05/15/2014
Total Solids
5.37
b3/UU
iw.0
JIVE
-,..
Moisture *
94.63
100.0
JM
05/09/2014 13:59
SM-2540G
Total Kjeldahl Nitrogen
Total Phosphorus
0.93
0.10
9310
1020
10.0
100
JM
KM
05/12/2014 08:39
05/12/2014 13:47
SM-4500-NH3C-TKN
SW 6010C
Total Potassium
0.06
622
100
KM
05/12/2014 13:47
SW 6010C
Total Sulfur
0.39
3940
100
KM
05/12/2014 13:47
SW 6010C
Total Calcium
0.25
2490
100
KM
05/12/2014 13:47
SW 6010C
Total Magnesium
0.11
1080
100
KM
05/12/2014 13:47.
SW 6010C
Total Sodium
0.27
2720
100
KM
05/12/2014 13:47
SW 6010C
Total Iron
330000
100
KM
05/12/2014 13:47
SW 6010C
Total Aluminum
22000
100
KM
05/12/2014 13:47
SW 6010C
Total Manganese
3850
5
KM
05/12/2014 13:47
SW 6010C
Total Copper
38
5
KM
05/12/2014 13:47
SW 6010C
Total Zinc
66
5
KM
05/12/2014 13:47
SW 6010C
Ammonia Nitrogen
0.19
1860
10.0
JM
05/12/2014 08:39
SM-4500-NH3C
Organic N
Nitrate+Nitrite-N
0.74
7450
55.9
10.0
2.00
JM
05/12/2014 08:39
05/12/2014 08:40
CALCULATION
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
05/12/2014 13:47
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and Letters are for the exclusive andconfidential use of our clients, and may not be reproduced in whole or part: nor may any reference be ;Wade
to the work, the results. or the company in any advertising. ,news release, or other public announcements without obtaining our prior ivritten authorization.
Debbie Holt

Page: 2 of 2
Report,Number: 14-129-0209 R z A&L Eastern Laboratories, Inc.
Account Number: 46457"� 7621 WhiteP ine Road Richmond, Virginia 23237 [phone] Fax [phone]
Submitted By: MARSHALL PURYEAR www.aleastern.com
Send To: SYNAGRO CENTRAL LLC/GRAHAM Project: GRAHAM WTP
MARY BREWER #51-0025 NC CERT#257
284 BOGER RD
MOCKSVILLE , NC 27028
REPORT OF ANALYSIS Date Sampled: 5/8/2014 09:15:00
Lab Number: 55276 Date Received: 05/09/2014 00:00
Sample Id: GRAHAM WTP Date Reported: 05/15/2014
Total Chromium
�J5
b
NIVI
UU/ I414V IY IJ.`tr
. Vr —.—
Total Nickel
47
5
KM
05/12/2014 13:47
SW 6010C
Total Lead
22
5
KM
05/12/2014 13:47
SW 6010C
Total Arsenic
4.0
3.0
KM
05/12/2014 13:47
SW 6010C
Total Mercury
<0.4
0.4
KM
05/14/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
05/12/2014 13:47
SW 6010C
pH (Standard Units) 6.82
2.00
JM
05/12/2014.08:39
SW-9045D
Total Molybdenum
<5
5
KM
05/12/2014 13:47
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr", "Ni",
AND "Pb".
ALL OTHER QC
DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, -and may not be reproduced in whole or part, nor may any reference be macle
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

,IN OF CUSTGDV
SAMPLING LOGII ` P&A Ri II111111111111111111111111111111Jill111111%ill11111111JillJill 5-0�2o,°J RECORD ANALYS11S
CUSTOMER: SYNAGRO SOUTHEAST SYNAGROCENTRAL LLCiGRAHAM 12:34:53
GRAHAM WTP
�c ^ sampling procedures
PRUJEUT MANAGER: fII/I ,'Lr�r1L.1 � � /c`7rr —..--tion of these samples.
Phone: 1 3
SAMPLER
A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD
LAS # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED
f7tj L (ii L G. YJ A —/III
Relinquished by Sampl�r: _
Date f
Time
Recieved by: REMARKS:
'� l�i.-•-�- J ( `��l L�J: i" `-1 ,�n'1�::
ll �'�! uc��% i-i
1 �! S ��
V (? � G (b'CX�/) f i ti•�
Relinquished by: /
Date
Time
Recieved by:
R nqu�g ed by:
ate
Time
Recieved by: r-
SPECIAL INSTRUCTIONS:
t�f�� �,
> For
monitoring purposes.
�
ryrn c;
ANALYSIS REQUEST
SAMPLE
---I.D.
So--
SL2
NH, -N
r
I N0 -N
a
Organic{
N I
Cd
Cr
Ni
Pb�
As �
Hg �
Se
py
CaCO,
egU1V. i
volatile e
SOIIdS—pw
Mo
CI
NO, N
—pop
I
SL7: Total Solids (Moisture), Total Kjeldahl Nitrogen. Phosphorus, and Potassium
31-2, Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc
White - A & L Canary - MANAGER COPY

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2036-01-WPL-NC GRAHAM, NC MEBANE WTP LIQUID 5/8/2014 5/1/2014-12/31/2014 2.6462
Na mg/I = (IJa mg/kg x % Solids) + 100 = (2720 x 5.3700) + 100 = 146.064
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (2490 x 5.3700) + 100 = 133.713
Mg mg/I = (mg mg/kg x % Solids) = 100 = (1080 x 5.3700) + 100 = 57.996
Na meq = Na mg/I _ Molec.Wgt.Na = 146.064 + 23 = 6.35061
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 133.713 + 20 = 6.68565
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 57.996 + 12 = 4.833
SAR = Na meq = SgrRo6t[0.5 x (Ca meq + Mg` meq)] = 6.35061 = SgrRoot[0.5(6.68565+4.833)] = 2.64624
1
Page 1
Printed: 1 /28/2015
14:40

FACILITY NAME: GRAHAM, NC
OWNER: CITY OF GRAHAM
SITE #: NC AM 00001 FIELD# : AM 00001 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Page: I
Lime Applied ***
PERMIT #: W00003824 ANNUAL DRY TONS APPLIED: 43.04 Date Lbs/Ac
OPERATOR: CITY OF GRAHAM CAT10N EXCHANGE CAPACITY (NON'503):
OLD FIELD #: 4 ACRES UTILIZED: 8.80 ACRES PERMITTED: 8.80
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry,
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
till-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
5/9/14
62,000.00 (G)
7045.455
5.37
1.578
GRWPL
DRY
0-<1/2"
SUR
0.5
0.40
9,310.0 p
1,860.00 p
55.90 p
73966
( FESCUE
5/12114
130,200.00 (G)
14795.455
5.37
3.313
GRWPL
DRY
0-<1/2"
SUR
0.5
0.40
9,310.0 p
1,860.00 p
55.90 p
3966
FESCUE
May-14
1 192,200.00 (G)
21,840.910
1
rotas %.rauons/Ac: 1.r,awv.Yr
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
39
0.039
0.020
0.342
0.372
0.215
0.004
0.049
0.460
0.049
0.646
9.98
Cumulative Ibs/acre
0.234
0.065
5.151
1.952
1.165
0.020
0.520
1.360
0.196
2.298
Permit PAN Limit (lbs/acre) Ist Crop/2nd Cro p
' s
y-
z rc
?
° ' ,
250
`
iFD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
2679
15.0 375.0
89.0
2500.0
r
z
GRWPL = GRAHAM, NC MEBANE WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
°1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/l g ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, 1NJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
r

FACILITY NAME: GRAHAM, NC
OWNER: CITY OF GRAHAM
SITE #: NC AM 00001 FIELD# : AM 00001 0010
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PERMIT #: W00003824 ANNUAL DRY TONS APPLIED: 51.37
OPERATOR: CITY OF GRAHAM CATION EXCHANGE CAPACITY (NON-503):
OLD FIELD #: 10 ACRES UTILIZED: 9.00 ACRES PERMITTED: 9.00
Page
Lime Applied ***
Date
Lbs/Ac
DATE or
MONTH
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Solids
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
A li-
pp
cation
Method
Vola-
till-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
Total
Per Acre
5/8/14
124,000.00 (0)
13777.778
5.37
3.085
GRWPL
DRY
0-<1/2"
SUR
0.5
0.40
9,310.0 p
1,860.00 p
55.90
3966
I FESCUE
5/9/14
105,400.00 (G)
11711.111
5.37
2.622
GRWPL
DRY
0-<1/2"
SUR
0.5
0.40
9,310.0p
1,860.00 p
p
55.90
3966
FESCUE
iMay-14
T..
229,400.00 (G)
1
25,488.389
p
1
TOTALS:
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
Annuallbs/acre
0.046
0.023
0.400
0.434
0.251
0.005
0.057
0537
0.057
0.753
11.64
45
CLm1UIatiVe Ibs/acre
0.461
0.125
13.062
5.907
8.423
0.045
2.253
3.573
0.217
8.397
-
. -
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
250
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
'.
1339.0
2679
15.0 375.0
89.0
2500.0
M1.�• ±i,:
GRWPL = GRAHAM, NC MEBANE WTP LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
.evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of lines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5. Injection/Incorporation 1.0
* Application Method: SUR-Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

",(y:� ..11
i c ai3'
a3..�.:-ric..-2;-�'�, v.n'I�Cirii}1_r747 `J237O21x?J
May 19, 2014
Marshall Puryear
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Graham
Dear Marshall Puryear:
Summit Envii-onmenial Technologies, Inc.
3310 Win St.
Cuyahoga Falls. Ohio 44223
TEL [phone] Pi1,Y.• [phone]
Wehsite.' hHoVivivin.seffek.conr
Order No.: 14050938
Summit Environmental Technologies, Inc. received I sample(s) on 5/9/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
"10 Win St.
Cuyahoga Falls, Ohio 44223
A21-A 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut P11-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho 01-100923, Illinois 200061 and Reg.5, Indiana C-011-13, Kansas F.-10347, Kentucky (underground Storago'I'ank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPI-I923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
01-12O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas 1'I04704466-11-5, Region 8 STMS-
L, USDA/APHIS P330-11-00244, Utah 01-1009232011-I, Vermont VT-87688, Virginia 00440 and 1531, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 8

sumonflu
Summit Environmental Technologies, Inc.
Workorder
3310 I�I'in St.4c,L!Sample
Summary
Fts1tlROhIFo1Eld'fAL'tt'Cl��itiL��:Gt=:>, t�zr,
Cuyahoga Falls, Ohio 44223
Lzboralos*0:
TFL: [phone] FA,r: [phone]
W04: 14050938
I4rebrite: hnn://ivww.seltek.cont
20-May-14
CLIENT: Synagro
Project: Graham
Lab SampleID Client Sample ID 'rag No
14050938-001 Graham WIT
Date Collected
5/8/2014 9:10:00 AM
Date Received Matrix
5/0/2014 11:00:00 AM Sludge
Page 2 of 8

Smnnrit Environmental Technologies, Inc. Case Narrative
3310 Win St.
I L .: a Cry ho a Falls, Ohio 44223
4;<ti;iotat��Fr.rai-32��:t:r��aa;es;+ Cuyahoga WO#: 14050938
"!r t,fir>..i Libarayorms TIiL: [phone] /rAX: [phone] Dale: i/]I12014
Website: hitn://iririv.s•ellek.com
CLIENT: Synagro
Project: Graham
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 8

SuunrfEnvironmental Technologies, Inc.
[Yin Sr.
WO#:
140i0938OUMRRO�-u3310
'
Date
Re ported:
I
5/19/2014
G'itili;nhlLfE!;'I',i.L :EC}SA:rlL��u!c S; i?dC
Cu} alroo-nFa(Is, Olrio=l=l77j
I1i1: [phone] FAX: [phone]
Company:
Synagro
Wcbsile: hun://ivtiviv.seilek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
5/9/2014
Project#:
Graham
TCLP Metals Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt
Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Graham WTP
001
5/8/2014
TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
5/14/2014
VVK
Graham WTP
001
5/8/2014
TCLP Barium(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
5/14/2014
VVK
Graham WTP
001
5/8/2014
TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
5/14/2014
VVK
Graham WTP
001
5/8/2014
TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
5/14/2014
VVK
Graham WTP
001
5/8/2014
TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
5/14/2014
VVK
Graham WTP
001
5/8/2014
TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
5/14/2014
VVK
Graham WTP
001
5/8/2014
TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
5/14/2014
VVK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Graham WTP 001 5/8/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 5/14/2014 ALJ
SVOC SW-846: 8081 Pesticides-TCLP
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Graham WTP
001
5/8/2014
Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
5/14/2014
JBN
Graham WTP
001
5/8/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
5/14/2014
JBN
Graham WTP
001
5/8/2014
Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
5/14/2014
JBN
Graham WTP
001
5/8/2014
gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
5/14/2014
JBN
Graham WTP
001
5/8/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
5/14/2014
JBN
Graham WTP
001
5/8/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
5/14/2014
JBN
Graham WTP
001
5/8/2014
Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
5/14/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab lD#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Graham WTP
001
5/8/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
5/14/2014
MES
Graham WTP
001
5/8/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
5/14/2014
MES
Graham WTP
001
5/8/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
5/14/2014
MES
Graham WTP
001
5/8/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
5/14/2014
MES
Graham WTP
001
5/8/2014
Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
5/14/2014
MES
'Graham
WTP
001
5/8/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
5/14/2014
MES
Graham WTP
001
5/8/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
5/14/2014
MES
Graham WTP
001
5/8/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
5/14/2014
MES
Graham WTP
001
5/8/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
5/14/2014
MES
Graham WTP
001
5/8/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
5/14/2014
MES
Page 4 of 8

,
t�- � "I
f,�1 lairs 1 I {
Simunit Environmental Technologies, Inc.
3310 ruin St.
WO#:
14050938
�y Jlyt r., 1J
Date Reported:
5l19/2014
'Gehl FMEP!'('i1.L -1 EC?iNOLOGIES. ;Nc.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Company:
Synagro
Wehsiie: Iruo://,vw,v.seriek.com
Address:
284 Boger Rd.
Mocksvillc NC 27028
Received:
5/9/2014
Project#:
Graham
SVOC 8270 TCLP BNA List
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Graham WTP
001
5/8/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
5/14/2014
AKE
Graham WTP
001
5/8/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
5/14/2014
AKE
Graham WTP
001
5/8/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
5/14/2014
AKE
Graham WTP
001
5/8/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
5/14/2014
AKE
Graham WTP
001
5/8/2014
Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
5/14/2014
AKE
Graham WTP
001
5/8/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
5/14/2014
AKE
butadiene
Graham WTP
001
5/8/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
5/14/2014
AKE
Graham WTP
001
5/8/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
5/14/2014
AKE
Graham WTP
001
5/8/2014
Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
5/14/2014
AKE
Graham WTP
001
5/8/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
5/14/2014
AKE
Graham WTP
001
5/8/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
5/14/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
Graham WTP 001 5/8/2014 2,4-D 5.0 ND mg/L Sludge EPA 8321 A 1 10 5/14/2014 AMZ
Graham WTP 001 5/8/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 5/14/2014 AMZ
Page 5 of 8

I�
S11n1111if Fnl•ironlnewal Technologies, hic.
Wp{/.
14050938
r
=--•-- - �.-1 14
rar
3310 Win St.
��
=l=1__; Cllyuhognhnlls.Ohio3
Date Reported:
5/19/2014
j
_r
1r,Bit+t! 1.3t t.,ltrcrar �r!e;
TEL: [phone] lA,r: [phone]
Company:
Synagro
Wehsite: hmr.//ivinv.sellek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 5/9/2014
Project;'#: Graham
Client ID#
Lab ID#
Collected Analyte
Result Units
Matrix
Method
DF
RL Run
Analyst
Graham WTP
001
5/8/2014
Flashpoint (140T)
>140 T
Sludge
EPA 1010
1
5/9/2014
TAH
Graham WTP
001
5/8/2014
Cyanide, Reactive
ND mg/Kg
Sludge
EPA 9014
1
0.50 5/12/2014
TIR
Graham WTP
001
5/8/2014
pH
6.4 s.u.
Sludge
EPA 9045 D
1
5/9/2014
AYS
Graham WTP
001
5/8/2014
Sulfide, Reactive
ND mg/L
Sludge
EPA 9034
1
25 5/12/2014
TIR
Page 6 of 8

Summit Environmental Technolokiies, Inc.
3110 10 W-i n Strat Analysis Request/Chain of Custody
For Sunignif 11w. 11,;e olliv
01
Mall,,rlr,:r:l' hl,,itc:
l'r, i 4s V.-.n3r
Amd)-fical
Parameter:~
and Methods
L
-14 0 ev 5'L/ I ,,j,,- -z
Oweil Mill w No
q 3 y
T'liciii Fu\ No Ej
2r
-
it
Cliew Fln;J! ✓ D
Q11ow No.
it
J
Owch O'Ohio VAP vamplt, ✓El
A
oil
Daw
Thliv
ri
i Dale
Tillits
Received be:
17
LO sr
A /W
Received ill hit. by: D.1tv
h,-,pp(o,oJ
Ljticsted I.Y:
(D
--A
0
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Date: 07/27/13
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Page 8 of 8

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name . City of Graham Permit # WQ0003824
WWTP Name Graham — Mebane WTP NPDES # NCO045292
Monitoring Period: From 01/01/14 To 12/31/]4
Pathogen Reduction (40CFR 503.32) - Please indicate level achieved and alternative performed
Class A
Alternative I
Alternative 4
Class B
Alternative I
Alternative 2
Alternative 5
Alternative 2
Alternative 3
Alternative 6
Alternative 3
If applicable to altcNOIT
'(C ss n-i-7) ' al t P s I' fro i rr-n-iL to IZec B
yens";
Aerobic Dig. R,E �� 7� I) ■� `rE ie p' ab.
If applicable to alternative performed (Cla i� 1 r;rts_ � ii nMR
6wim, monitorinn data.
f� Yl _ ITM1 a O
Parameter
AllowableF Pathogen Densitv No. of I Freq.
�
Sample
Analytical
t i— ! —� f r--� ;,M7E1TTech.
T,)"of
i y E
WF—t-uAl- .-
Pi11 PE
�vl ca',
.Fecal
Coliform
2x 1O6
MI'N.:g or
w--LU'7
(`j"'2Y
f
106J
CFt.J/z
t'y"t -
1000
M PN/g
M PN
Salmonella
3 MPN/
bacteria
4 g
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed
Option I Option 2 Option 3 Option 4 Option 5_
Option 6 Option 7 Option 8 Option 9 Option 10
No vector attraction options were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
X "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law that the pathogen requirements In 40 CFR 503.32 and the vector attraction
reduction requirement in 40 Cff 503.33 have not been met." (Please note if you check this statement
attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and
vector attraction reduction requirements Tave been met. I am aware that there are significant penalties for false
certification including fine and imprisonment."
Preparer Name and Title
Land Applier Name and Title (if applicable)
Signature of Preparer Date Signature of Land Applier (if applicable) Date

Agricultural Lime Application Log
Year: 2014
Project: Graham
FieldI Soil Lime Requirement Tons/Acre Date Applied
(state -county -site -field) pH (from soil analysis) Applied
NC-AM-1-4 6.9 0.OT/Ac.
NC-AM-1-10 7.8 O.OT/Ac.

Page 1 of 2 — -
Report Number: 15-023-0632'
Account Number: 46457
Send To: SYNAGRO CENTRAL LLC/GRAHAM www.aleastern.com
MARY BREWER #51-0025
284 BOGER RD
MOCKSVILLE NC 27028
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower:
GRAHAM WTP
SOI L ANN UAL
SOIL ANALYSIS REPORT
Date Received: 01/23/2015 Date Of Analvsis- n1 i9w9o1 s n.ro of po ..• M »ar')n, r
Submitted By: NATE ROTH
Farm ID: GRAHAM
Analytical Method(s):
Mehlich 3
Sample ID
Lab
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Field ID
Number
ENR
% Rate
Mehlich 3
Reserve
K
M g
Ca
Na
Soil
Buffer
H
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
pH
Index
meq/100g
meq/100g
AM-1-4
09635
18.1 VH 150
642 VH
56 VL
296 L
7166
VH
99
VL
NC = 535
NC = 29
6.9
0.5
39.4
AM-1-10
09637
8.0 VH 150F
234 VH
36 VL
129 VL
5126
" VH
VL
NC=195
NC=18
149
.8
0.0
27.0
Sample ID
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
I Boron
Soluble Salts
Chloride
Aluminum
Field ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
CI
Al
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
m Rate pp
ppm
Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
AM-1-4
0.4
6.3
90.9
1.1
1.4
61 VH
59.7 VH
52 VH
233
VH
27.5 VH
1.9 H
0.3 VL
NC = 127
NC = 1492.5
NC = 325
NC = 1375.0
AM-1-10
0.3
4.0
94.9
0.8
0.0=77
I
VH
�qc
13.4 VH
149 VH
163
VH
7.6 VH
0.9 M
0.22 VL
.
NC=335.0
NC=931
NC=380.0
-- --- - -•• - •-r�• • •..r....... •r�^ u.�^u..� ��� � cnNidiiduuii of by[ oois: vo (percent), ppm (pans per million), Ibs/A This report applies to samples) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. c H (High), VH (Very High). ENR - Estimated Nitrogen Release, (milli -equivalent per 100 grams). Conversions: e-r
( q p g ) ppm x 2 =Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc, by. ��� m i1
C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm.
Pauric McGroary

Page 2 of 2
Report Number: 15-023-0632
Account Number:46457
Send To: SYNAGRO CENTRAL LLC/GRAHAM
MARY BREWER #51-0025
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 01/23/2015
Date Of Report: 01/26/2015
z A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 804 743-9401 Fax [phone]
www.aleastern.com
Grower: Submitted By: NATE ROTH
GRAHAM WTP Farm ID: GRAHAM
SOIL ANNUAL
SOIL FERTILITY RECOMMENDATIONS
Sample ID
Yield Goal
Lime
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Field ID
Intended Crop
Tons
Tons/A
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
AM-1-4
Fescue Hay
4
0.0
50
0
250
0
0
0
0
0
0
0
AM-1-10
Fescue Hay
4
0.0
50
0
250
0
0
0
0
0
0
0
Comments
Sample(s) : AM-1-10 Crop: Fescue Hay
Apply additional 50 pounds of nitrogen after every cutting and harvest of hay.
Cation Exchange Capacity may be over -estimated due to high pH and free lime in the soil.
The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in
spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield
is low the following applications should be reduced or eliminated.
Use ammonium sulfate as all or portion of the N requirement to reduce pH.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary