WQ0013982_Renewal Application_20190705

APPLICATION FOR
PERMIT RENEWAL / MODIFICATION
NON -DISCHARGE PERMIT
WQ0013982
Prepared for:
Duvaltex (US), Inc.
304 Fast Main Street
Elkin, North Carolina 28621
Prepared by:
Willcox & Mahe Soil Solutions, PLLC
7231B Summerfield Road
Summerfield, North Carolina 27358
� � a
willcox&mabe
SOIL SOLUI IONS
June - 2019

willcox&mabe
SO 1 L SOL U T I ON S
July 1, 2019
NCDEQ/DWR
Water Quality Permitting Section
Non -Discharge Permitting Unit
512 N. Salisbury Street,
9th Floor, Office# 942X
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
Reference: Application For Permit Renewal
Permit No. WQ0013982
WMSS Job No. 19-02
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting; the Permit Renewal
application on behalf of Duvaltex (US), Inc. (Duvaltex). Duvaltex is not requesting to
change anything in the existing permit: Duvaltex WWTP (520 Dry Tons annually) and
renewing four fields (CR-3, GH-1, GH-2, GH-3) totaling 80.6 net acres. Duvaltex also
wanted to note that they are currently leasing the WWTP.
If there is any further information required or questions regarding this application please do
not hesitate to contact WMSS, Mr. Martin Mabe at 336-312-1396 or Duvaltex, Mr. Keith
Ogden at 336-526-0503 for further assistance.
Sincerely,
WMSS, PLLC
10��LA01�4
Martin Mabe
Partner
cc: Greg Kanellis, Hart & Hickman
Keith Ogden, Duvaltex
Shared\WMSS ProjecW2019119-02 Hart & Hickman, PC1Renewai AppticatbnOuvaltex 2019 Permit Renewal Pkg.doc
Willcox & Mabe Soil Solutions, PLLC 17231 B Summerfield Road / Summerfield, NC 273581 Rob 336.339.9128 or
Martin 336.312.13961www.willcoxmabesoil.com

TABLE OF CONTENTS
APPENDIX: TITLE
RLAP - APPL,ICATION FORM
II RSC - SOURCE ADDITIONS
III LASC - APPLICATION FORM
IV UPDATED SITE MAPS

Inn
MOST RECENT PERMIT
O&M PLAN

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two conies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -.Discharge Permuting Unit
General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that
are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under
15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages):
• Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please
do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
• The Applicant's CerliGcation on Pagc 5 of this form shall be signed in accordance with 15A NCAC 02T .0106 b . An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
Q If this project is for a modification of an existing permit, submit one copy of the existing permit.
;J Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification New Permit F Major Modification'
Major (land are permitted for > 300 acres) ( $1,310 I $395
Minor (land are permitted for < 300 acres) $810 $245
- A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional land application areas not previously approved for that particular program [including transferring of field(s) from
one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not
previously permitted. There is no fee for minor modifications to a permit.
C. Cover Letter (All Application Packages)
0 List all items included in the application package, as well as a brief description of the requested permitting action.
D. Environmental Assessments (May be Required — See 15A NCAC IC .0300)
El Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: RLAP 06-16 Page I of 3

E. Operation and Maintenance flan (New and Renewal Application Packages)
❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
® Submit the O&M Plan in accordance will) 15A NCAC 021 ._I 1_I_0 and include at a minimum:
® Operational functions; describe the operation of the program to show what operations are necessary for the program to
function and by whom the functions are to be conducted.
® Maintenance schedules; may include equipment calibration, maintenance of signs, etc.
® Safety measures; may include safety training program, manuals, signs, etc.
® Spill response plan; including control, containment, rerrediation, emergency contact information, etc.
® Inspection plan including the following information;
® Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the
selected location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
® Sampling and monitoring plan including the following information;
® Names and titles of personnel responsible for conducting the sampling and monitoring.
® Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature,
flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The
sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for
residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per
year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most
likely to be negatively affected by cold temperatures.
THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY.
F. Program Determination
❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T
1102(12). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable:
0 Any land application site certified for the residuals land application program that receives residuals at rates or frequencies
greater than agronomic rates.
❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal,
and agricultural crop production is of secondary importance.
❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation
facilities or irrigation facilities fed through a fixed supply system,
❑ Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program
falls under the dedicated program definitions.
G. Program Information
❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system.
❑ Provide an explanation of the dedicated system and its operation.
H. Detailed Site Maps (All New or Modification Application Packages)
❑ Submit three (3) sets of standard size plans and two (2) sets of I I" by 17" plans (electronic format is acceptable - Adobe PDF
only). For Modifications, submit plans specific to the nnodiftcation(s) only.
❑ Plans must include the following minimum items:
❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site
relief and showing all facility related structures and fences within the land application area.
❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and
perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s).
❑ Delineation of the review and compliance boundaries
❑ Setbacks as required by 15A NCAC 02T .1 108
❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s).
❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's
evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray
irrigation zones as they will be operated.
❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY. NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with
the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION
INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3

1. Project Evaluation and Receiver Site Management Plan (AII New Application Packages or Modifications that include new sites)
❑ Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops
and their ability to accept the proposed application rates.
J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity)
❑ Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 023'
_.1104(d)(4) and current Division Policy
available at: littp.//www,ncwatcr.org/Rules Policies and, Regulations/. The document shall be signed, sealed and dated by a
qualified professional.
K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation
facilities fed through fixed supply system)
❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or
Professional Land Surveyor in accordance with 15A NCAC 02T .1104(d)(2). For Modifications, submit an updated site map
specific to the modification(s) only.
❑ The design documents must include the following minimum items:
❑ Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new
units or are critical to the understanding of the complete process;
❑ Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the
finished product including leaking testing; and
❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head
cut e analysis for each pump, and irrigation design.
❑ Soil mapping units shown on all disposal sites.
L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or
irrigation facilities fed through fixed supply systems)
❑ Submit a completed and accurate water balance in accordance with 15A NCAC 02T 1104(d)(5) and current Division Policy
availableat:littp://www.licwaterorgRulcs Policies,and Regulations/,
M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment
or irrigation components)
❑ Property ownership documentation shall consist of one of the following:
❑ Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or
❑ Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or
❑ An easement running with the land specifically indicating the intended use of the property and meeting the requirements of
15A NCAC 021, .0107(0, or
❑ A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or
survey map.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of

State of North Carolina
Department of Environmental Quality
s Division of Water Resources
Division of Water Resources 15A NCAC 02T.1100— RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 06-16
1. APPLICANT INFORMATION:
1. Applicant's name: Duvaltex US), hic.
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per ISA NCAC 02"1 Q1Q6; Keith Ogden Title::fextile Engineering No Director
Applicant's mailing address: 304 East Main Street
City: Elkin State: NC Zip: 28621-_
Telephone number: [phone] Email Address: keith.ogden@,duvaltex.com
2. Consultant's name: Willcox & Mahe Soil Solutions. PLLC License Number (for P.F.): _
Affiliation: ❑ On Staff ® Retained (Firm: WMSS. PLLC)
Consultant's mailing address: 7231 B Summerlield Road
City: Summerfield State: NC Zip: 27358-__
Telephone number: (336) 312-13966 Email Address: martink(Dwilleoxniabesoil.com
3. Agronomist's name: Martin Mahe License Number: _
Affiliation: ❑ N/A ❑ On Staff ® Retained (Firm: WMSS, PLI.C)
Agronomist's mailing address: 723IB SUtnnlerfleld Road
City: Summerfield State: NC Zip: 27358-_
Telephone number: [phone] Email Address: martin r willcoxmabcsoii con
4. Soil Scientist's name: License Number: _
Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: )
Soil Scientist's mailing address: __
City: __ State: Zip:
Telephone number: (_) _- Email Address:
5. Fee submitted: N/A (See Instruction B) *RENEWAL ONLY
It. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W 00 013982 Date of most -recently issued permit: August 30,.2018
Date of most -recently certified Attachment A (if different than the permit): August 30 2018
Date of most -recently certified Attachment B (if different than the permit): Au20t 30. 2018
FORM: RLAP 06-16 Page 1 of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 175 Fabric Lane
City: Elkin State: NC Zip: 28621-
Coordinates: Latitude: 36' 14' 41.51" Longitude: 80' 50' 29.49"
Datum: NAD83 Level of accuracy: Nearest hundredth of second
Method of measurement: MAP
2. County where residuals land application program is headquartered: Surr -
List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Glen Gary
Duvaltex
994475
Back -Up ORC
Billy Stone
Duvaltex
997291
- Additional Back -Up---
ORCs
(ifa licable) -.__--
—__—
-- --
_-- ----
_---
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test:
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 520 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
1 Surface
Incorporation
or Injection
First -Year
4.80
4.81
2,496
2,501
Five -Year Maximum Adjusted
7.91
7.92
4,113
4,118
b. Land Application Site Use Summarr: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
-----
--Row Crops --_
-
-------
--- flay -
- ----
-----
---- Pasture
80.6 -
--
----
80.6
--_ ---- --�
Methods
-------Total:
Surface
80.6
Incorporation or Injection
Total:
80.6
FORM: RLAP 06-16 Page 2 of 5

c. Residuals Land Application Sunnnarr: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Acres Required Using
Acres Required Using
Application Rate
First -Year PAN Concentrations
Five -Year Maximum Adjusted PAN
(Ibs PAN/ac-yr)
Concentrations
Surface Incorporation or
Surface Incorporation or
Injection
Injection
50
50
50
83
83
100 - _
25 ----- -
— -- 29---
----- 42
42
150
17
17
28
28
200-----
--13 --
-- 13
21
21
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation ofNo th Carolina Administrative Code (e.g, not enough storage, not enough land, vector reduction
practices not in place, etc.): Ultimate cleanout of the W W"I'P and lagoon will require additional land to handle the anticipated
increase in dry tonnaee not accounted for in this renewal application.
7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals program contains any land application site(s) that receives residuals at rates Or frequencies greater than agronomic
rates, explain; _
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain; —
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain; _
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
llf
Residua IsSource
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land ApplicalionS Site Certification and all associated documentation.
t
Land Application Siite
Certification.doc
FORM: RLAP 06-16 Page 3 of 5

Note: Item VI. Applicable to Dedicated Program with.fixed- irrigation Vstem onl -.
VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM
1. The irrigation system is: ❑ Spray ❑ Drip
2. Disposal system is: ❑ existing ❑ proposed.
3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: _ feet
below ground surface. Rules 15A NCAC 02T 0505(p) requires at least one -foot vertical separation between SH WT and ground
surface.
4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area?
❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if
structures are to be maintained or modified:
5. Loading rates recommended by the Soil Scientist Evaluation:
Soil Series
TRecommended
1 Fields within Soil Area
Loading Rate
_..._(in/hr).
Recommended
Loading Rate
..__ in/ r .-
6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist?
❑ Yes or ❑ No If No, explain why 15A NCAC 02 f 0505(n) is not met:
7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system):
Field Zone
Design Area
z
Ott)
Number of
Nozzles
Maximum Application
/h Rate (gallonsr) —_—
Design Annual Loading
_ Rate �galr)—.,
Toial
—�
Spray Irrigation Design Clement
Plan Sheet
Number
Specification
Page Number
Wetted diameter of nozzles
It
Wetted area of nozzles
ft2
Nozzle capacity
gpm
—_
Nozzle manufacturer / model
Elevation of highest nozzle
ft
FORM: RLAP 06-16 Page 4 of 5

Applicant's Certification (signing authority must be in compliance with 15A NWAC 021" ,0106):
The applicant or any affiliate has not been convicted of an environmental Crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes E] No, Explain; _
Keith Ogden Textile Eneineerine Project Director
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Duvaltex (US) Inc_____ —___....
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. t will make no claim against the Division of Water
Resources should a condition of this permit be violated. 1 also undersland that if all required parts of this application are not completed
and that if all required supporting information and attachments ere not included, this application package will be retwned io me as
incomplete.
Note: In accordance with North Carolina General Statutes § I43-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil perallics up to $25,000 per violation.
Signature: /�K Dare: -- —G/?
FORA: RL.AP 06-16 Page 5 of 5

ROY COO R
Grrrrvvt�'
NNAIC CAE L S. lZEC AN
'cr£.!m'y
I.IND A CULPEITER.
In lenhx Girer:o,
NOR'I'Fl CAROLINA
F.'izvir'c�nrnt�r<s27Cjeaffi'Fy'
August 30, 2018
KEIT i OGDEN— DIRECTOR OF OPERATIONS
DIJVALTEX (US), INC.
304 EAST MAIN STREET
ELKIN, NORTII CAROLINA 28621
Dear Nh. Ogden:
Subject: Permit No. W00013982
Duvaltex RLAP
Land Application of
Class B Residuals
Surry County
In accordance with your permit change of ownership request
forwarding herewith Permit No. W00013982 dated August 30, 2018.
continued operation of the subject residuals management program.
received June 20, 2018, we are
to Duvaltex (US), Inc. for the
Please note the Pei mince has been changed from True Textiles, Inc. to Duvaltex (tIS), Inc.
This permit shall be effective from the date of issuance until July 31, 2019, shall void Permit No.
W00013982 issued March 13, 2014, and shall be subject to the conditions and limitations as specified
therein. Please pay particular attention to the monitoring requirements listed in Attachment A for they may
differ from the previous penuit issuance. Failure to establish an adequate system for collecting and
maintaining the required operational information shall result in future compliance problems.
If any parts, requirements or limitations contained in this permit are unacceptable, the Penniace
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding.
� xn
of AIR!
3.54

Mr, Keith Ogden
August 30, 2018
Page 2 of 2
If you need additional information concerning this permit, please contact "'Troy Doby at (919) 707-
3655 orgr,e_ciow_{a)r
Sincerely,
^Linda Culpepper, Interim Director
Division of Water Resources
cc: Surry County Health Department (F,lectronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Seth Buffington -- Protection and Enforcement Branch (Electronic Copy)
Digital Pennit Archive (Electronic Copy)
Central Piles

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
LAND APPLICATION OF CLASS 13 RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes ofNorth Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION 1S HEREBY GRANTEE) TO
Duvaltex (US), lake
Surry County
FOR THE
continued operation of a residuals management program for Duvaltex (US), Inc. and consisting of the land
application of Class B residuals generated by the approved facility listed in Attachment A to the approved
fields listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application
received June 20, 2018, and in conformity with other supporting data subsequently tiled and approved by
the Department of Environmental Quality and considered a part of this permit. 'The use and disposal of
residuals are regulated under Title 40 Code of Federal Regulations Part 257. This pennit does not cxempt
the Permittee from complying with the federal regulations'.
This permit shall be eftedive from the date of issuance until July 31. 2019, shall void Pennit No.
W00013982 issued March 13, 2014, and shall be subject to the following specified conditions and
limitations:
SCHEDULES
No later than six months prior to the expiration of this permit, the Permittee shall request renewal of
this permit on official Division forms. Upon receipt of the request, the Division will review the
adequacy of the facilities described therein, and if warranted, will renC�s the permit for such period of
time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A
NCAC 02'T .0105(d) requires an updated site map to be submitted with the permit renewal application.
[15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109]
it. PERFORMANCE. STANDARDS
'File subject residuals management program shall be effectively maintained and operated at all times so
there is no discharge to surface waters, nor any contravention of groundwater or surface water
standards. In the event the facilities fait to perform satisfactorily, including the creation of prolonged
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
land applying residuals, contact the Winston-Salem Regional Office super,isor, and take: any
mmediate corrective actions. [G.S. 143 215.1 ]
VVQo013982.Vcrsiou:,.1 Shell Version I71103 Page; of I=

2. This permit shall not relieve the Permitter of responsibility lot damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 0213 .0200,
02L.0100]
3. Only residuals generated by the facility listed in Attachment A me aPlnoved for land application in
accordance with this permit. [G.S. 143-215.1 ]
4. Only the fields listed in Attachment 13 are approved for residuals land application. [G.S. 143 215.11
5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not
exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant
Loading Rates (CPLRs):
-----.
Ceiling Concentration
Parameter ,_"Y.,
Arsenic j
75
Cadmium
85
Copper
4,300
Lead
840
C1' LR
Mercun
57
15
Molybdenum
75
n/a
Nickel
420
374
Selenium
100
89
Zinc
7,500
2,498
The Pennittecshall determine compliance with the CPLRs using on, ofthe following methods:
a. By calculating file existing canurlative level of pollutants using actual analytical data from all
historical land application events of residuals, or
b. For land where residuals application has not occurred or is which the required data is incomplete,
by determining background concentrations through representative soil sampling.
[ 15A NCAC 02T .l 105]
6. Residuals that arc land applied shall meet Class B pathogan reduction requirements in 15A NCAC 02'1
.1106 (a) and (c). Fxceptionsto this requirement shall be specified in Attachment A. [15A NCAC 021-
11061
7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing
wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A)
that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 021
.1 107(a). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 021' .11071
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8. Setbacks for treatment aid storaae facilities shall be as follows
Setback
Setback Duscriptilm
(feet) '
I tabita )le residence or place of public assembly under
separate ownership
or not to
100
be maintained as part of the project site
Property lines
50
Private or public ater supply
; too
Surface eaters (streams— intermittent and perennial, perennial waterbodies,
and
50
wetlands)
_-_----_
Wells with exception to monitoring wells
too
All treatment and storage facilities were originally permitted
prior to September L 2006.
[15A NCAC 02T .1 1081
4. for Class B land application sites shall be as follows:
(Setbacks
I Setback
by application
type
(feet)
Setback Description
Vchiculu I
Legation
Injection /
Surface.
Sin face
Incorporation
Application
Application
habitable residence or place of public assembly under
i
separate ownership or not to be maintained as part of
f 400
do0
1 200
the )i'O e,(.t site
f__. I
i
Habitable residence or places of public assembly
;
owned by the Permittee, the owner of the land, or the
0
200
0
lessee/operator of the land to be maintained as part of
the project site
Properly ]me's
50
50
50
Public right of Way
�-
50
50
50
Pr ivate or public waver supply
100
100
too
Surface waters (sticams - intermittent and perennial,
100
100
50
perennial waterbodies, and wetlands)
Surface water diversions (ephemeral streams,
25
00
25
waterwoos ditches)
_
Groundwater losveun ditches( wherethe bottom of
��
00
25
r
the ditch intersects the SIIW f)
Subsurface groundwater lowering system
0
100
0
Wells with exception to monitoring wells
too
100
( 100
Bedrock outcrops
25 )
�5
25
Top of slope of embankments or cuts of two feet or
15
S
15
mote in vertical her -lit
Building foundations or basements
0
—----
5
------
0
Water lines
( 0
10
0
Swimming pools
100 i
100
too
Vitrification Lclds
1 0
20
0
[ 15A NCAC 02T .I 108]
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10. Land application areas shall he clearly marked o❑ each site prior to and during any residuals application
event. [15ANCACO2'r.0108(b)(I)]
11. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance
of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen
requirements based on the determined Realistic Yield Expectations (RYE) using any of the following
methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina I Iistorical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (httly-/lnuutt,nts_soil uc,u.eduhialds/index 1hp). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any ofthe following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter I
(hnn:!/uti .>+ n ai_i. >l SWC`/tech d<i ui tents ei(II_.Guidance Doc_100109._0di).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services ('NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(irp/htp_f�:sccgosusdt \1_i��t>>3cticr;slands�ds/;,trnducl_s/590.pdt).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessaryaction.
15A NCAC 02T.1109(b)(I)(k)]
12. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by
25% in accordance will) the USDA-NRCS 590 Nutrient Management Standards. [15A NCAC 02T
.0108(b)(1)]
13. If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer
and rye grass in the winter with both crops to receive residuals), then the second crop can receive an
application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may
be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted
for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. [15A
NCAC 02T.0108(b)(1)]
14. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office-, the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments {e.g., grypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall
maintain written records of these recommendations and details of their implementation. [15A NCAC
02T .0108(b)(I )]
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1.5. These residuals land application sites were individually pennitted on or after 1Dcembcr 30, 1983;
therefore, the compliance boundary is established at either 250 feet from the residual land application
area, or 50 feet within the property boundary, whichever is closest to the residual land application area.
An excecdanco of groundwater standards at or beyond the compliance boundary is subject to
remediation action according to ISA NCAC 021..0106(d)(2) as well as enforcement actions in
accordance with North Carolina General Statute 143 215.6A through 143-215.6C. Any approved
relocation of the COMPLIANCF BOUNDARY will be; noted in Attachment 13. 115A NCAC 021,
.0107(a)]
16, The review boundary shell be established midway between the compliance boundary and the residual
land application area. Any exceedance of groundwater standards at the review boundary shall require
action in accordance with 15A NCAC 02t..0106. [15A NCAC 021- 0108]
III, OPERATION AND MAINTENANCE RLQUIRI,.MjgNTS
1. The residuals management program shall be properly maintained and operated in all times. The
program shall be effectively maintained and operated as a non -discharge system to prevent any
contravention of surface water or groundwater standards. 115A NCAC 021.I 110]
2. The Winston-Salem Regional Office, telephone number [phone], and the appropriate local
government official (i.e., county manager, city manager, or health director) shall be notified at least 48
hours prior to the initial residuals land application to any new land application site. Notification to the
regional supervisor shall be made from 8:00 8.111. until 5:00 p.m. on Monday through Friday, excluding
Statc Holidays. [ 15A NCAC 02T .0108(b)(1)]
3. The Winston-Salem Regional Office shall be notified via email or telephone, (336) 776-98007 at least
24 hours prior to conducting any land application activity. Such notification shall indicate; at a
minimum, the anticipated application times, field IDs, and location of land application activities. If it
becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be
notified prior to commencing the application to those fields. [15 A NCAC 02 1 .0108(b)(1)]
ft. The Pernnittec shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications
to the OFzM Plan shall be approved by the Division prior to utilization of the r,ew plan. The O�@M Plan,
at the minimum. shall include:
a. Operational functions;
b. Maintenance schedules;
C. Safety measures;
d. Spill response plan;
c. Inspection plan including the following information:
I. Names and/or titles of personnel responsible for conducting the inspections;
ii. Frequency and location of inspections, including those to be conducted by the ORC. and
procedures to assure that the selected location(s) and inspection frequency are representative
of the residuals management program;
iii. Detailed description of inspection procedures including record keeping and actions tone taken
by the inspector in the event that noncompliance is observed pursuant to the noncompliance
noti ication requirements under the monitoring and reporting section of the permit:
f. Sampling and irienitoring plan including the following information:
i. Nantes and/or titles of personnel responsible for conducting the sampling and Ilion itorin ;
ii. Detailed description of monitoring procedures including parameters to be monitored;
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iii. Sampling frequency and procedures to assure that i-aprescntativc samples are being collected.
Fluctuation in temperature, llow, and other operating conditions can affect the quality of' the
residuals gathered during a particular sampling event. 'The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
nreei pathogen and vector attraction reduction requirements (e.g. facilities that land apply
multiple times per year but have an annual sampling frequency, may need to sample during
winter months when pathogen reduction is most likely to be negatively affected by cold
temperatures).
115A NCAC. 021' . 1100]
Upon the Water Pollution Control System Operators Certification Cmmission'S (WPCSOCC)
classification ofthe facility, the Permittee shall designate and employ if certified operator in responsible
charge (ORC) and one o+' more certified operators as back-up ORCs in accordance with 15A NCAC
08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204,
or as specified in the most recently approved O&M plan (i,e., see Condition II1.4.), and shall comply
with all other conditions of 15A NCAC; 08G. 0204. For more information regarding classification and
designation requirements, please contact the Division of Water Resources' Protection and Enforcement
Branch at [phone]. 115A NCAC 02T .01 1'7]
6. When the Permittee land applies bulk residuals, a copy ofthis permit and a copy of O&M Plan shall be
maintained at the land application sites during Land application activities. [ISA NCAC 02T
0108(b)(1)]
7. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be
maintained in all residuals transport and application vehicles. [ 15A NCAC 021'.1 1 101
8. Residuals shall not be stored at any land application site, unless written approval has been requested
and received from the Division. [G.S. 143-215.1]
9. When the R°rmittee land applies bulk residuals, adequate measures shall be laken to preveni wind
erosion and surface runoff from conveying residuals from the and application sites onto adjacent
properties or into .surface waters. [G.S. 1,13.215.1 ]
10. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land
application sites onto which residuals are applied, or application shall be in accordance with the crop
manaeemeni plan outlhted by the local Cooperative Extension Office, the Pepimment of Agricultne
and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved
by the Division. 115A NCAC 021' .1 109(b)(I )]
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11. Bulk residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangcred species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes prolonged nuisance conditions;
c. If the Land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the
residuals would occur;
e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a
24-hour period following a residuals land application event;
f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours
following a rainfall event of 0.5 inches or greater in a 24-hour period;
g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than
18% for injected or incorporated bulk liquid residuals;
h. If the land does not have an established vegetative cover unless the residuals are incorporated or
injected within a 24-hour period following a residuals land application event. Any field that is in a
USDA no -till program shall be exempted from meeting this vegetative cover requirement;
i. if the vertical separation between the seasonal high water table and the depth of residuals
application is less than one foot;
j. If the vertical separation of bedrock and the depth of residuals application is less than one toot;
k. Application exceeds agronomic rates.
[15A NCAC 02T .1109]
12. The following public access restrictions apply to residual land application sites:
a. Public access to public contact sites (e.g.. golf courses, parks, ball fields, etc.) shall be restricted
for 365 days after a residuals land application event:
b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land
application event.
[15A NCAC 02T .1 109(b)(2)]
13. Public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g.,
1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and
contact information, including the Pertnittee or applicator's telephone number. Signs shall be posted
in a clearly visible and conspicuous manner at the entrance to each land application site during a land
application event, and for as long as the public access restrictions required under Condition II1.12.
apply. [15A NCAC 02T .0108(b)(1)]
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14 The following harvesting and grazing restrictions apply to residual land application sites after each
land application event:
i Restricted
Harvesting and Grazing Description Duration
Animals shall not be allowed to graze during land application activities and
restricted period. Sites that are to be used for grazing shall have fencing to
prevent access after each land application event.
_ __.....
Food crops, feed crops and fiber crops shall not be harvested for:
Turf grown on land where residuals have been applied shall not be harvested lot-:
Food crops with harvested parts that touch the residual/soil mixture and are
totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.)
shall not be harvested for:
30 days
30 days
12 months
14 months
When the residuals remain on the land sin face for four months or longer prior to
incorporation into the soil, food crops with harvested parts below the land 20 months
surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be
harvested for.
When the residuals remain on the land surface for less than four months prior to
l incorporation into the soil, food crops with harvested parts below the land 38 mmu9ts
surface shall not be harvested for:
[15A NCAC 02T .l 109(b)(3)]
15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume
of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that
have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those
operations where a NMP is required by the US Department of Agriculture — National Resources
Conservation Service (NRCS) or other State Agencies. The Pennittee shall calculate allowable nutrient
loading rates based on the provided information and use appropriate reductions.
For the purpose of this permit condition, a Crop Management plan (CMP), Waste Utilization Plan
(WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient
Management Plan, [15A NCAC 02T .0108(b)(I ), 02T .1104(c)(3)]
16. No residuals shall be land applied unless the submitted Land Owner Agreement between the Permittee
and landowners or lessees/operators of the land application site is in full force and effect. These
agreements shalt be considered expired concurrent with the permit expiration date, and shall be renewed
during the permit renewal process. [I SA NCAC 021' .l 104(c)(4)]
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IV
MONITORING AND REPORTING REQUIREMt_i 'I_S
1. Any Division -required monitoring (including groundwater; plant tissue, soil and surface water
analyses) necessary to ensure groundwater and surface water protection shall be established, and an
acceptable sample reporting schedule shall be followed. [I5A NCAC 02T .0108(c)]
2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation
and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40
CFR Part 261 shall not be used or disposed under this permit The analyses [corrosivity, ignitability,
reactivity, and toxicity characteristic leaching procedure (TCLP)J shall be performed at the
frequency specified in Attachment A. and the Pennittee shall maintain these results for a minimum of
five years. Any exceptions from the requirements in this condition shall be specified in Attachment A.
The TCLP analysis shall include the following parameters (the regntatory level in milligrams per liter
is in parentheses):
Arsenic (5.0) 1,,1 Dichlorobenzene (7.5) Nitrobenzene (2.0)
Barium (100.0) 1,2 Dichloroethane (0.5) Pentzchloropheuol (100.0)
Beuzene(05) 1, 1 -Dichlorocthylene (0.7) Pyridine(5.0)
Cadmium (1 0) 2,4-Dinitzotoluonc (0.13) Selenium (1.0)
Carbon tetrachlor ide (0.5) Inds in (0.02) Silver (5.0)
Chlordane (0.03) Hexachlorobenzene (0.13) 1 etrachlomethylene (0.7)
14cptachlot (and ds hydroxide)
Chlmohencene(100.0) (0.008) Toxaphene(0.>)
Chloroform (6,0) Nexachloio 1,3-butadicne (0,5) 1 richloroethylene (0.5)
Cluornium (5.0) Ilexachloroethane (3.0) 2,d 5 "frichlorophenol (400,0)
m Cresol (200.0) Lead (5.0) 1 2,4 6-1-1i, hlorophenol (2.0)
o-C-resol (200,0) 1Jndauc (0.4) 2A.5-TP (Silvex) (1.0)
u-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2)
Cresol (200.0) hiethoxyehlor (10.0)
- _
2,d D (10.0) Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittec may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitorinn, frequency be less than once per permit cycle.
[ I5A NCAC 13A .0102(b), 021- .1101, 021- .11051
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An analysis shall be conducted on residuals front each source generating facility at the frequency
specified in Attachment A, and the Perntitlee shall maintain the results I'or a minimum of live )cars.
The analysis shall include the following parameters:
Aluminum Mercury Potassium
Ammonia -Nitrogen Molybdenum I Selenium
Arsenic Nickel Sodium
Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio
(SAR) —
Calcium I Percent Total Solids TKN
Copper pll 'Zinc
Lead , Phosphorus
Magnesium I Plant Available, Nitrogen (by calculation)
[15A NCAC 029' .1101]
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A, and at the tittle indicated in the sampling and
monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization
process utilized, and sufficient to demonstrate compliance with the Class B pathogen reduction
requirements in 15A NCAC 02T .1106 (a) and (c), and one vector attraction reduction requirement in
15A NCAC 021- .1107 (a) shall be met. Any exceptions from the requirements in this condition shall
be specified in Attachment A. [15A NCAC 021 .1 106, 02T .1 107, 02'f .l 1 11(c)]
5. Au annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on
each land application site listed in Attachment B on which a residuals land application event will occur
in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil
Sampling" located in the Sampling Instructions section of the NC Department of Agriculture &
Consumer Services' website (imp /,»,-eti n �_ i..�u��/ r.. r iipni/I r r� Itu�t). The Permittec shall maintain
these results and a description of the sampling methodologies used to detennine soil fertility fora period
of no less than five years, and shall be made available to the Division upon request. At a mininunn, the
Standard Soil Fertility Analysis shall include the following parameters:
AcidityExchangeable
angeable Sodium Percentage Phosphorus
Base Saturation (by calculation) Magnesium Potassium
Calcium Manganese Sodium
Cation Exchange Capacity Percent Humic Matter Zinc
__ ______ . ______
Copper pH
[15A NCAC 02T .0108(c), 15A NCAC 02T .1 111(d)]
6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall
be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC, 02B .05051
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The Permittee shall maintain records fl residual land application ev-nts. At a minimum, these
records shall include the followin-�
a Source of residuals;
b. Date of land application;
c. Location of land application (i.e., site, field, or zone number as listed in Attachment B);
d. Approximate areas applied to (acres);
c. Method of land application;
f. Weather conditions (e.g., sunny, cloudy, raining, etc.):.
g. Predominant Soil Mapping Unit (e.g., CW32);
h. Soil conditions (e.g., (try, wet, frozen, etc.):
i. Type ofcrop or crops to be grown on field;
j. Nitrogen Application Rate based oil RYFs (if using data obtained from the North Carolina State
University Department of Soil Science Website, the printout page shall be kept oil (-tic and reprinted
every five years);
k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet
ton per acre;
I, Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre. or
wet tons per acre;
In, Volume of soil amendments (e.g., lime, gypsum, etc.) applied in gallons per acre, dry ton per acre,
or wet tons per acre; and
❑. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other
sources of nutrients (e.g., ifapplicable), annual and cumulative pounds per acre ofeach heavy metal
(e.g.: shall inchide,. but shall not be limited to, arsenic, cadmium, copper, lead, mercur,Y,
molybdenum, nickel, selenium, and zin(:), annual pounds per acre of PAN. and annual 1:,ounds per
acre of phosphorus applied to each field.
15A NCAC 02T .0109(a)]
8. Three copies of an annual report shall be submitted on or before March I ". "hlre annual report shall
meet the requirements described in the Instructions_ for Residuals Appltcation Annual Reporting Forms.
hrsiruc6ons for reporting and annual report forms are available at
lutp Ntl�q n� otla;aou,.liv.lion i_e uurcts/jcai i i_�0iouv,pr!rartxv b�rualt>»pi�-
di�_nt rr i .tin_, tn.i+'r�,roirin u nm_, or can be obtained by contacting the Non -Discharge
Permitting Unit directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing t'nit
1617 Mail Service Center
Raleigh; North Carolina 27699-1617
j 15A NCAC 02T .I I I I(a)]
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9. Noncompliance Notification
The Permittee shall report by telephone to the Winston-Salem Regional Office, telephone number (336)
776-9800, as soon as possible, but in no case more than 24 hours or on the next working day following
the occurrence or fist knowledge of the occurrence of any of the following:
a. Land application of residuals abnormal in quantity or characteristic.
b. Any failure of the land application program resulting in a release of material to surface waters.
c. Any time self -monitoring indicates the facility has gone out of compliance with its permit
limitations.
d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of
adequate residual treatment.
c. Any spill or discharge from a vehicle or piping system during residuals transportation.
Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of
a storage structure, etc.) outside normal business homy shall be repotted to the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone].Persons
reporting such occurrences by telephone shall also File a written report in letter form within five days
following first knowledge of the occurrence. This report shall outline the actions taken or proposed to
be taken to ensure that the problem does not recur. 115A NCAC 02T .0105(1), 02T .0108(b)(1)]
V. INSPECTIONS
The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the
subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)]
Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the
residuals storage, transport and application facilities to identify malfunctions, facility deterioration and
operator errors that could result in discharges to the environment, a threat to human health or a public
nuisance. The Pcrmittee shall maintain an inspection log that includes, at a minimum, the date and time
of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The
Permittee shall maintain this inspection log for a period of five years from the date of inspection, and
this log shall be made available to the Division upon request. [ 15A NCAC 021.0108(b)]
3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect
any property, premises or place on or related to the land application sites or facilities permitted herein
at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy
any records required to be maintained under the terms and conditions of this permit; and may collect
groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)]
VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an
enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to
143-215.6C. [G.S. 143-215.6A to 143-215.6C]
2. This permit shall become voidable if the residuals laud application events are not carried out in
accordance with the conditions of this permit. [15A NCAC 02T .0110]
3. This permit is effective only with respect to the nature and volume of residuals described in the permit
application and other supporting documentation. [G.S. 143-215.1 ]
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4. The issuance of this permit does not exempt the Permittce Flom complying with any and all statutes,
rules, regulations, or ordinances, which may be imposed by ober,jurisdictional government agencies
(e.g., local, slate, and federal). OI'pwHmlar concern to the Division are applicable river buffer rules in
15A NCAC 0213 .0200, erosion and sedimentation control requirements in 15A NCAC Chapter 4 and
under the Division's General Permit WOO 10000; any requirements pertaining to wetlands undea 15A
NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter
143 of the General Statutes. [ 15A NCAC 02T .0105(c)(6)]
5. In the event the residuals program changes ownership or the Permittec changes his name, a format
permit modification request shall be submitted to the Division. "Phis request shall be made on official
Division forms, and shall include appropriate documentation front the parties involved and other
supporting documentation as necessary. The Permittce of record shall remain fully responsible for
maintaining and operating the residuals program permitted herein until a permit is issued to the new
ovIncr. [ 15A NCAC 021' .01041
6. This permit is subject to revocation or unilateral modification upon 60-day notice fiom the Division
Director, in whole or part for the requirements listed in 15A NCAC 07r .0I A. [ 15A NCAC 02T .01 101
7. Unlass the Division Dbeetor grants a variance, expansion of the permitted residuals program contained
herein shall not be granted if the Permittec exemplifies any of the a iterin in 15A NCAC 02'l .0120(b).
[ 15A NCAC 021' .0120]
& The Permittce shall pay the annual fee tvWn 30 days afler being billed b} the Division, failure to pay
the annual fee accordingly shall be cause for the Division to revoke this permit [I5A NCAC 02'f
.0105(eXQ
Pennit issued this the W day of August 2018
NORTH (AROIANA E NVIRONMIAIAL NIANAGL II N"1 CO\9;\'II)'SION
� 7
Linda Culpepper, Interim Director
Division of Water Resources
By Authority of the Environmental Mmagement Commission
Pennit Number W00013982
W00013982 Version 3.1 Shell Version 171103 Page 13 of 13

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AT'rAC'HMENT A -Approved Residual Sources
Duvaltes (US), Ltc.
Certification Data: August 30, 2018
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1A'Q001398_ Version 3A Allaehmem A rage 1 or I

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A'I"rACli iVtF.N 1'13 - Approved Land Application Sites
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ATTACHMENT
OPERATION AND MAINTENANCE PLAN

Table of Contents
PAGE #(s)
1. Introduction
WASTEWATER FLOWS
REGULATORY REQUIREMENTS SATISFIED BY O & M
MANUAL REVISIONS AND DOCUMENT CONTROL
2. Facility Description
FACILITY LOCATION 2
SITL; DESCRIPTION 2
INDUSTRIAL PROCESSES 2
WASTEWATER TREATMENT 3
UTILITIES 3
ISO 14001 ENVIRONMENTAL MANAGEMENT SYSTEM
SITE SECURITY 3
3. PERMITS AND REGULATIONS
LEGAL REQUIREMENTS 4
RECORDKEEPING AND REPORTING 4
4. DESCRIPTION OF TREATMENT FACILITY
GENERAL
5
BASIC DESCRIPTION OF TREATMENT FACILITY
5
LIQUID PROCESS FLOW
Lift Station
5
Screen Room
6
Equalization Basin
6
Aeration Basin
7
Sedimentation
7-8
Chlorination
9
Post Aeration
9
Dechlorination
9
Secondary Solids Storage
9
Sludge Dewatering
10
Sludge Drying Beds
10
Land Application Site
10

5. UNIT OPERATIONS — EQUIPMENT DESCRIPTION
LIFT STATION
11-13
INFLUENT LIFT SCREENS
14-15
EQUALIZATION BASIN
15
AERATION LIFT STATION
16-17
AERATION BASIN
17
CLARIFIERS
18
EFFLUENT FLOW METER
19
SLUDGE HANDLING FACILITIES
Sludge and Scum Pumps
19-20
Aerobic Digester (Sludge Storage Tank)
20-21
Sand Drying Bed
21
Sludge Disposal
22
Sampling and Monitoring
22
Pathogen Reduction Requirement
22
Vector Attraction Requirement
23
Land Application Site Inspection
23
Spill Control Plan
23
6. OPERATIONAL CONTROL OF ACTIVATED SLUDGE:
Process Theory and Performance
MIXED LIQUOR SUSPENDED SOLIDS
25
RETURN SLUDGE RATE CONTROL
25
WASTE SLUDGE RATE CONTROL
26
DISSOLVED OXYGEN CONTROL
26
NUTRIENTS
26
PRODUCTION FLUCTUATIONS
27
PHOSPHORUS REMOVAL
27
TROUBLESHOOTING
27
SETTLEABILITY TEST
27
MICROSCOPIC EXAMINATION
28
7. PERSONNEL
STAFFING PLAN 29
LICENSING and CONTINUING EDUCATION 29

8. SAMPLING AND LABORATORY ANALYSIS
SAMPLING POINTS AND REPRESENTATIVE SAMPLING
GRAB SAMPLES
COMPOSITE SAMPLES
FLOW -PROPORTIONAL COMPOSITE
SAMPLING FREQUENCY
COLLECTION and ANALYSIS of SAMPLES for NPDES FREQUENCY
IN HOUSE TESTING
QUALITY ASSURANCE
EPA QA/QC TESTING
CHAIN OF CUSTODY
9. RECORDS AND RECORDKEEPING
OPERATIONS RECORDS
30
30
30
31
31
31
33
33
34
GENERAL 35
DAILY LOG 35
RECORDS STORAGE 35
MONTHLY DISCHARGE MONITORING REPORTS (DMRs) 35
10. MAINTENANCE
ROUTINE MAINTENANCE
37
PREVENTATIVE MAINTENANCE
37
CORRECTIVE/BREAK DOWN MAINTENANCE
37
11. EMERGENCY RESPONSE PROGRAM
EMERGENCY RESPONSE (ICP) 39
CRITICAL. EQUIPMENT FAILURE (TREATMENT PROCESS BYPASS) 39
12. SAFETY
LOCKOUT /TAGOUT 40
CONFINED SPACE ENTRY PROGRAM 40
HAZARD COMMUNICATION PROGRAM 40
PPE PROGRAM 41
WELDING, CUTTING, and BRAZING POLICY 41
HEARING CONSERVATION PROGRAM 41

1. INTRODUCTION
1.1 WASTEWATER FLOWS
The wastewater treatment facility at the Duvaltex US Inc. (Elkin) Facility treats
wastewater from the finishing process, as well as domestic wastewater, and
stormwater. However, the textile plant is in the process of closing.
The wastewater treatment facility typically treats 0.05 million gallons per
day (MGD) to 1.0 million gallons per day and has an historic maximum per day
flow of approximately 1.8 million gallons per day. The facility's effluent
discharge permit limits daily flow to a maximum of 4.0 million gallons per day
(monthly average maximum).
1.2 REGULATORY REQUIREMENTS SATISFIED BY O & M
The Operation and Maintenance Manual satisfies the requirements of the North
Carolina Department of Enviromuent and Natural Resources (NCDEQ) based
on the regulation 15A NCAC 02T.1007, which requires all wastewater
treatment facilities to prepare. adopt. and keep current an operation and
maintenance manual that contains information necessary for all wastewater
treatment facility operators to properly operate and maintain the facility.
1.3 MANUAL REVISIONS AND DOCUMENT CONTROL
This Operations and Maintenance Manual (O & M Manual) is a controlled
document. The Environmental Manager will administer all revisions to this
Manual. Controlled copies of this Operations and Maintenance Manual are
distributed as follows:
- Glen Gary, Wastewater Treatment Plant Manager (ORC)
- Environmental Manager Office
- Corporate Environmental Manager

2. FACILITY DESCRIPTION
2.1 FACILITY LOCATION
Duvaltex US Inc. is located at 304 East Main Street, Elkin, North Carolina
28621, which is in Surry County. The wastewater treatment facility is located
on the southeast side of the property, south of the facility. The address for the
WWTP is 175 Fabric Lane, Elkin, North Carolina 28621. The WWTP is
adjacent to the Yadkin River.
2.2 SITE DESCRIPTION
Duvaltex US Inc. is a textile finishing and fiber production facility that
manufactures high quality yarns and finished fabric for commercial, automotive,
and residential interiors. These fabrics are primarily made from synthetic fibers.
The textiles facility is located within the town limits of Elkin, North
Carolina, and occupies approximately 77 acres. The facility consists of 12
buildings which encompass approximately one and a half million square feet of
manufacturing space. The site includes several paved roadways; paved access
areas, parking areas, and loading and unloading areas. Landscaped vegetated
areas consisting of grass, shrubs and trees exist throughout the facility grounds.
The site is accessible from Highway 268.
2.3 INDUSTRIAL PROCESSES
The Elkin facility performs fiber manufacturing and fabric finishing. Finishing
includes final washing, heat setting, and application of coating and/or surface
treatments necessary to meet specific customer satisfactions. The average
annual production of the facility is approximately 13 million linear yards.
There are three major wet processes: wet finishing, back coating, and raw
water filtration. The woven fabric components are dried in finishing. In the wet
finish areas, the material is fed through rolls into washers, where a detergent
and/or coating are applied to the fabric. This fabric is then dried, decanted,
inspected, and prepared for shipment,
2.4 WASTEWATER TREATMENT
The Elkin facility's industrial activity requires on -site treatment of the facility's
wastewater. The facility's cooling water, process water, boiler blow down, non -
contact cooling water, and domestic sewage are treated at the on -site treatment
facility. All floor drains located throughout the facility are connected to the
wastewater treatment facility. All discharges to the Yadkin River are limited
and monitored by the Elkin facility pursuant to the requirements of the facility's
National Pollutant Discharge Elimination System (NPDES) permit. [The
NPDES Permit number is NC0005312.]
The flows from the three wet processes are combined with wastewater
generated from the boiler blow down, filter backwash, and cooling waters at the
2

lift station. These wastewater discharges reach the treatment facility via a series
of collection drains gravity -fed to the plant. The wastewater is screened and
biologically treated by conventional aeration. The final effluent from the
secondary wastewater treatment process is chlorinated, then dechlorinated prior
to discharge to the Yadkin River.
Waste sludge generated from the secondary treatment system is thickened
and dewatered through polymer application. The residuals are applied to sand
drying beds and disposed via the requirements of the land application permit.
(The NPDES permit number for the land application program is WQ0013982).
2.5 UTILITIES
Drinking water services for the manufacturing plant and W WTP are supplied by
the Town of Elkin. Electrical services for both are provided by Duke Power.
No known leach fields, septic system, water wells, cisterns, or burn pits are
located at the site.
2.6 SITE SECURITY
Plant personnel are continuously present at the facility. Plant personnel
maintain security during hours of operation.
Once plant personnel (i.e. W WTP operators) leave the facility, the outside
gate is locked. Keys for this lock are kept by the following individuals:
- Glen Gary, Wastewater Treatment Plant Manager (ORC)
- Environmental Manager's Office
- Billy Stone, Wastewater Treatment Plant Operator

3. PERMITS AND REGULATIONS
3.1 LEGAL REQUIREMENTS
All wastewater treatment plants operating under the NPDES program are
required to conduct a sampling and analysis program. This program focuses
primarily on monitoring effluent quality for evaluation of plant compliance
with the permit's effluent limits. Elkin's NPDES permit specifies sampling
location, sample type, sampling frequency, analyses to be performed at each
sampling location and the frequency of reporting the analytical results to the
regulatory agencies.
3.2 RECORDKEEPING AND REPORTING
Based on 15 A NCAC 02B.0502, the Elkin facility is required to monitor and
report the quantity and quality of wastewater discharges to the water resources
of the state. DMR's (Discharge monitoring reports) are due to NCDEQ by the
30"' day of the following month for the current month.

4. DESCRIPTION OF TREATMENT FACILITY
4.1 GENERAL
A schematic of the W WTP has been provided for your convenience. The
schematic was created by John Duncan, Draftsman for Duvaltex US Inc.
4.2 BASIC DESCRIPTION OF TREATMENT FACILITY
The wastewater treatment plant (W WTP) at Elkin, North Carolina is leased
and operated by Duvaltex US Inc. The W WTP is an activated sludge plant
designed and permitted to discharge up to four million gallons per day (MGD)
of wastewater. The facility is designated by North Carolina DEQ as a Grade
IV wastewater treatment facility.
The current NPDES permit contains specific effluent characteristic
limitations and monitoring requirements for various pollutants. The permit
authorizes treated wastewater to discharge from the treatment works to
receiving waters designated at the Yadkin River.
4.3 LIQUID PROCESS FLOW
4.3.,1 Lift Station
The influent wet well is approximately 12,000 gallons. The wet well
contains a manually operated course bar screen to protect the influent
pumps from large debris. Screenings are manually racked onto a landing
and placed in a container. The containers are carried manually or lifted
via a hoist assembly to the floor level of the screen house. Debris from
course screens are combined with fine screens in a collection dumpster.
The influent wet well level is controlled by an ultrasonic level
sensing system, which consists of three 20hp self -priming centrifugal
pumps (P-101, P-102, and P-103). Each pump has a capacity to pump
1500 gallons per minute. All three pumps are equipped with a variable
frequency drive (VPD). Any of the three pumps can operate in the lead
position by adjusting the control panel HOA (Hand/Off/Auto) switch. All
three pumps discharge to a common 14-inch header pipe.
4.3.2 Screen Room

4.3.2 Screen Room
Wastewater from the lift station enters the screen room from a 14-inch
force main that separates into two headers. Each header directs flow to
two sets of static arc -type fine screens. individual valves installed in the
header can divert flow to a single screen if necessary. The west header
has a bypass valve installed to divert flow directly to the intermediate
channel. The east header has a bypass valve installed to direct flow
directly to the aeration basin lift station.
Each fine screen has the capacity to handle up to 450 gallons per
minute. As the wastewater passes over the screens, the fibers and other
large particulate solids are trapped on the metal mesh and are carried by
gravity down the sides of the screens. The solids are manually scrapped to
a drain plate and further moved to a collection drum. The collection drum
contents are then disposed of to a collection dumpster. Furthermore, we
have four other screens also capable of handling 700 gallons per minute,
which provides enough ability to handle the required capacity for the
plant.
The filtered wastewater passes through each screen unit to a
gravity drain system. The fine screened effluent is directed to the
intermediate channel. From the intermediate channel, the flow is directed
to the equalization basin but can be bypassed to the aeration lift station by
a manually -operated slide gate valve.
4.3.3 Equalization Basin
The equalization (EQ) basin is 2.9 million gallons; it has an unlined clay
bottom and a concrete apron. It is equipped with a bubbler level
indicating system. The EQ basin helps with the stabilization of influent
flow through the W WTP. Loading on the secondary system can be
controlled by utilizing the EQ basin to handle peak flows that occur
throughout the day. The EQ basin can also be used as an emergency spill
basin. An accidental spill or toxic dump can be neutralized or isolated in
this area.
The equalization basin is currently equipped with two 30-hp Aqua -
Aerobic surface aerators. The aerators add dissolved oxygen to the raw
wastewater while maintaining the solids in suspension. A pneumatically
actuated flow control valve, installed in a concrete vault (adjacent to the
EQ basin), is designed to throttle flow from the equalization basin to the
aeration basin.

4.3.4 Aeration Basin
The aeration basin is 2.1 million gallons. The basin was constructed with
an earthen basin and a concrete apron. Oxygen is added by mechanical
means to supply dissolved oxygen to the bacteria system. The activated
sludge aeration basin functions are the following: to transfer oxygen,
promote mixing, suspend the solids, and promote flocculation.
The aeration basin is designed with two manifolds to distribute the
return activated sludge and the primary effluent wastewater to six injection
ports. The wastewater treatment of activated sludge of this type is defined
as a complete mix activated sludge treatment process. Complete Mix
aeration ensures equal distribution of applied waste load, dissolved
oxygen, and return sludge throughout the aeration basin.
The design operating water depth in the basin is approximately 10
feet. The aeration basin contains three surface 30-hp mechanical Oxy-
Gun aerators (A/B aer-230, 231, 232) and one surface 30-hp mechanical
Aqua -Aerobic aerator (A/B aer-233). The basin also has four surface 10-
lip Aqua -Aerobic mixers (A/B mix-220, 221, 222, 223). The surface
aerators and mixers provide dissolved oxygen and uniform mixing.
The treatment plant can expect a hydraulic detention time for the
aeration basin of about two days with an average flow of 1.0 million
gallons per day.
4.3.5 Sedimentation
After the aeration basin, the wastewater flows to a splitter box with two
slide gates. The splitter box directs flow to two circular clarifiers. The
splitter box is designed with an adjustable slotted pipe to remove floating
scum exiting the aeration basin. The wastewater is routed to the
secondary settling tank where water solids separation is performed
(sedimentation).
The clarifiers are 80 feet in diameter and have a capacity of 0.376
million gallons each. The clarifier weir and center well is 9 feet and 11
feet in vertical height, respectively. Both clarifiers utilize the original
Envirex drive and scum rakes. In each clarifier, the Envirex drive is
assembled with a motor, gear reducer, and gear assembly. The sloped
tank floor allows the sludge scrapper assembly to efficiently collect the
sludge to the center well where the sludge is returned to the aeration basin.
The scum layer is collected by a skimmer assembly directing the flow to a
manhole. The biomasses are stabilized from previous aerobic conditions
and are in a form that can be easily settled and removed during
sedimentation.
Each clarifier has its own dedicated return activated sludge pump.
Both clarifiers share a third pump that is used as a back-up pump during
repairs to one of the other normal pumps. All three RAS pumps share a
common discharge header that transfers the RAS flow to the aeration
basin at 6 different injection points. The clarifier effluent from both tanks
gravity drain to a common drain where chlorination is next in the waste
7

treatment sequence. The settled biomass is returned to the aeration basin
to maintain appropriate solids inventories to speed up decomposition of
incoming waste.
The table below shows the typical design values for secondary
clarifiers. The peak flow rate used for design basis analysis is 2.4 MGD,
which corresponds to the maximum daily design Mow. A BOD of 15mg/I,
and a TSS of 33mg/L leaving the secondary clarifiers was used in
calculating the table below:
Both
Clarifiers On- One Clarifier
Parameter Line On -Line Typical Design
Average Hydraulic
Overflow
Rate(gal/ft2-day)
100
199
200-400
Maximum
Hydraulic
Overflow Rate
(gal/ft2-day)
239
477
600-800
Solids Loading
Rate (Ibs/ft2 -hr)
0.12
0.24
0.2-1
Peak Solids
Loading
(Ibs/ft2-hr)
0.29
0.58
1.4
Average Blanket
Depth (ft)
<5.0 ft
<5.0 ft
<3.0 it
Process control changes or adjustment typically originate from the
clarifier. Flow rates from the return activated sludge (RAS) pumps (P-
501, P-502, P-503), and from the waste activated sludge (WAS) pumps (P-
504, P-505) play a dominate role in the activated sludge treatment process.
All pumps are constant speed, Gorman -Rupp self priming pumps that are
housed in the sludge pump building adjacent to the secondary clarifiers.
Proper depths of the sludge blanket in the secondary clarifier along with
mixed liquor concentrations in the aeration basin also very important
control parameters. Sludge blanket depths are inspected daily by the plant
operator with the use of a mechanical devise called a "sludge judge."
Concentrations for mixed liquor suspended solids and mixed liquor
volatile suspended solids are also analyzed daily by the plant operator.
The clarifiers mechanically remove the settled sludge by use of a
sludge collector on the bottom of the tank. This collector moves the
settled solids to the center of the clarifier to a sludge hopper where they
are returned back to the aeration basin. Also, floatable and scum solids
are collected by the scum skimmer arm. The skimmer arm has a blade
that pushes the scum to a collection ramp where it gravity flows to a
collection manhole (Manhole 47). The scum pumps draw from this
manhole and pump to either the head end of the plant (Intermediate Pump
Station) or to the sludge holding tank.

4.3.6 Chlorination
Chlorination is performed to disinfect the treated effluent that flows to the
stream. Solid calcium hypochlorite pellets are dissolved with water to
produce a liquid form of calcium hypochlorite. The chlorinator is
designed to automatically prepare and deliver a consistent and accurate
dose of available chlorine for disinfection. The solid calcium hypochlorite
pellets are added manually to the chlorination unit.
The metering pump injects the chlorine solution to the chlorine
contact chamber. The pump is wired to the effluent flow controller using
a 4-20 mA signal. The control wire allows the chlorine injection to be
injected based on flow. [The metering pump is a positive displacement
pump manufactured by desco, Inc.]
4.3.7 Post Aeration
The post aeration tank adds dissolved oxygen concentration to the final
effluent with a 7.5-hp Aqua -Aerobic surface mechanical aerator.
Increasing the oxygen concentration encourages the growth of aquatic life
downstream of the plant.
4.3.8 Dechlorination
The dechlorination system neutralizes the excess chlorine residual
produced in the disinfection process. The system uses liquid sodium
bisulfite as the dechlorination agent. The design includes a dual metering
pump system that incorporates two positive displacement pumps for
injection. The system has a sulfite controller to monitor the sulfite
concentration of the dechlorinated solution. This system operates
continuously and is programmed to notify the operator when the residual
reaches a low level set point through the remote paging system. This
notifies the operator to replace the dechlorination drum.
The dechlorination system is equipped with a pH -monitoring
system to measure any change in pH that may affect the final effluent.
Any observable changes that may affect the process can by altered by
addition of pI I amendment.
4.3.9 Secondary Solids Storage
Waste sludge from the north and south clarifiers are directed to the aerobic
digester. [If process demands, the scum pump wet well (Manhole #7) can
be directed to the aerobic digester.] After wasting, the sludge can be
thickened by a settling and decanting process. After settling, the clear
supernatant lying above the sludge is directed back to Manhole #7 by a
manually operated decanting boom. The sludge storage tank is aerated
with course bubble diffusers powered by two Universal mechanical
blowers. Once the sludge has reached the desired concentration (2-4%),
the sludge transfer pump directs the flow to the sand drying beds.

4.3.10. Sludge Dewatering
Polymer PT-1644 is stored in 55-gallon drums and mixed with makeup
water in a 1500 gallon make down tank. Five gallons of polymer is added
to 1500 gallons of makeup water to make a batch of dilute polymer for use
in the sludge dewatering process. The make down tank is automatically
filled using chlorine contact chamber reuse water. The reuse water pump
will fill the make down tank and automatically shut off with a mechanical
float device (switch). Sludge from the storage tank is pumped to one of six
sand drying beds. While the sludge is transferred to the drying bed the
operator may enhance the sludge drying time by the addition of a polymer.
The operator starts the sludge transfer pump and the polymer pump
simultaneously to process the sludge with polymer. Once the treatment is
started the best method to achieve good solids separation is to adjust the
polymer pump speed knob. The goal is to produce a sludge cake on the
sand bed that will dewater and dry the fastest.
4.3.11 Sludge Drying Beds
Sludge from the storage tank is pumped to one of six sand drying beds.
The dimensions of each of the six sludge drying beds are 35 feet by 82
feet (2870 square feet). The sand drying beds are not covered, and thus,
they are subject to precipitation, cloud coverage, etc. The climatic
changes produced by the four seasons may cause the sludge concentration
to vary 18% up to 75%. Water drained from the sludge cake is collected
in a wet well manhole and is pumped to Manhole #7. Once the sand beds
are sufficiently dried, the biosolids are transferred to a collection bed (one
of the sand drying beds) and stockpiled. From the collection bed the
biosolids are loaded onto trucks for land application disposal.
4.3.12 Land Application Site
Sludge disposal from the sand drying beds is performed through the land
application program. There are 520 dry tons per year of residuals
(biosolids) allowed to land apply according to NPDES Permit Number
WQ0013982. The operator must read and understand the parameters of
the land application permit. The operator is subject to the conditions and
limitations that are specified in the permit.
The preferred disposal method for biosolids is farmland application
of dry solids. During suitable weather (i.e, no precipitation and the
ground is not be frozen), the biosolids are transferred by a contractor from
the stockpile into a dump truck and applied to permitted farmland.
An alternate method that can be utilized for residual disposal
consists of the following: Liquid land application is treated in the aerobic
digester tank through a lime stabilization process to meet Pathogen
Reduction Requirements set forth in the Land Application Permit
WQ0013982.
10

5. UNIT OPERATIONS -EQUIPMENT DESCRIPTION
5.1 LIFT STATION
The influent lift station is equipped with three vertical dry pit non -clog
pumps with two section shafting. The influent pumps (P-101, 102, 103)
are controlled from a control panel based on the wet well level monitored
by a submersible pressure transducer. The signal from the pressure
transducer is converted to a 4-20 milliamp signal from an inline converter.
The converter is connected to the Hydro Ranger, whereas the signal is
connected to the pump control panel. The Hydro Ranger control panel is
located on the left side of the screening wet.
All three pumps are equipped with variable frequency drive
(VFD). However, only two pumps are operated by the VFD while the third
pump is operated by the high level float. Any of the three pumps can
operate in the lead position by adjusting the control panel three-way
switch. Pump No. 1 is the dedicated lead pump. The lead pump is
operated by the VFD to provide uniform flow to the screening room.
Pumping rates increase as the liquid level increases to maintain water
levels at a desired range. If necessary, all three pumps will operate at the
same time. Under normal conditions, the control panel switches will be in
the Auto Mode position. All valves should be in the full open position.
The level control system must be functioning properly. The influent
pumps can be operated in the manual position in the event of an
Emergency or if the level -control system should fail. Plant staff will check
the magnetic flow meter and record cumulative flow reading on a daily
basis.
When the water level in the wet well reaches a vertical height (VH)
of 3.9 feet, the Lead Pump will start. The lead pump motor Frequency will
stay at 56.7 Hz and pump 1,000 gallons per minute unless the liquid level
rises. If the liquid level increases the Frequency of the lead pump will
increase proportionally for a max of 1,500 gallons per minute at
Frequency of 63.0 Hz. If the liquid level decreases, the pump motor
Frequency decrease in proportion to the level in the sump.

Table 5.1 Influent Litt Station Equipment List
Description Rated Capacity Driver Data Notes
(HI) -RPM -
Volts)
Coarse Bar Rack 13R-101 100 Coarse Screen - Influent Lilt station
Influent Pump 13-101 1500 GPM (D, 33 Fl- 20-880-208
Influent Pump P-102 1500 GPM (a;33 FT 20-880-208
Influent Pump 11-103 1500 GPM a) 33 F I 20-880-208
Table 5.2 Influent PumD Control Levels
Influent Wet Well
Pump On
Pump Off
Pumps
Lead Pump
3.9 feet
3A feet
Secondary Pump
6.3 feet
4.8 feet
Third Pump
8.3 feet
7.9 feel
(Backup pump)
The Secondary pump operates when the liquid level reaches 6.3
feet. The Lead and Secondary pump motor Frequency will stay at 56.7 I Iz
or increase to a max of 63.0 Hz as the liquid level continues to rise. If the
liquid level continues to rise, the third pump will operate. The Third pump
operates from a float positioned inside the wet well. The liquid level turns
the float upright actuating the pump motor. The Third pump turns off
when the float returns to its original stationary position.
Table 5.3 Influent Pump Control Setting
Influent Wet Well VFll Frequency Flz Approximate Plow Rate
Pumps (gPtn)
56.7 1-Iz 1000
Lead Pump
63.01 Iz 1500
Lead Pump
1900
Lead -Secondary Pump 56.7 Iiz
2400
bead -Secondary Pump 63.0 1-lz
3000
Lead-Second,tay- hh(l 63.01Iz.
12

An ultrasonic level sensor has been installed to provide a high
level alarm signal that initiates an auto -dialer to alert the operator on duty.
The Prosonic FMU 860 ultrasonic transmitter controller is wall mounted
in the screen house laboratory. The Prosonic transmitter and sensor
provides continuous level measurements in the wet well. The high level
alarm is programmed to relay the paging system at 12.5 feet of liquid level
depth.
All three influent pumps can operate in the Lead -Secondary -Third
Pump Position. The control panel has a three position switch to manually
position the pump sequence.
"Fable 5.4_Three Position PnM-P Control Switch
Three Position Pump Control
Lead Pump
Secondary
Third Point)
Switch
Pump
(Backup)
ill pump
43 Pump
#2 Pump
1 Pump Position
# 2 Pump
ill Pump
#3 Pump
2 Pump Position
43 Pump
#2 Pump
#t Pump
3 Pump Position
The lift station may also be manually operated. This may be
required during maintenance or repair of the VFD, level sensors, or
individual pumps. There is a manual/auto control switch located on the
control panel. Also, each individual pump has a manual/auto control
switch. When a pump is out of service or under repair, the other two
pumps operate in the lead and secondary pump positions. With the pumps
operating in the manual mode, the liquid level requires constant
monitoring and pump setting adjustments to prevent sump overflow.
Additionally, care must be taken to prevent liquid levels from falling
below the minimum of 36 inches to prevent the pumps from rwming dry,
which can damage the pumps. Upon completion of maintenance or repairs
activities, the lift station should be placed back into automatic position.
13

5.2 INFLUENT LIFT SCREENS
The influent pumps feed a series of fine and mechanical screens
for large particulate and lint removal. The Hydro and/or Syncro-Matic
Separator screen units provide liquid/solids separation from the combined
textile process waste and domestic waste lines. The static screen is
comprised of two basic elements, a cabinet and a screen panel. The
curved screen panel is comprised of wedge shaped wires that are coined
and wrapped around support rods which are placed perpendicular to the
support wire. Welded to the bottom of the screen panel is a catch tray.
The catch tray is designed to capture accumulated solids built up on the
screen. The cabinet is designed to receive the incoming flow and
distribute the flow across the width of the screen. The influent stream is
directed to and flows evenly over a weir onto the screen surface. The
solids are manually scrapped daily (more if necessary) to a catch tray and
further moved to a collection drum. The collection drum contents are then
disposed of to a collection dumpster.
Table 5.5 Hydro Fine Screen Equipment List
Description
Rated Capacity
Driver Data (HP-
Notes
RPM -Volts)
Fine Screen FS-201
200 Fine Screen
450 GPM
Replaced 2002
Fine Screen FS-202
200 Fine Screen
450 GPM
Replaced 2002
Fine Screen FS-203
200 Fine Screen
450 GPM
Replaced 2002
Fine Screen FS-204
200 Fine Screen
450 GPM
Replaced 2002
The four screens are equipped with individual valves to divert flow
to another screen or direct flow to the intermediate channel. There are few
instances where the bypass of all four screens is desired. This can be
accomplished in two ways. Close the valve to each individual screen or
close the header valve to close two screens on each train. The result is the
same as the wastewater is feeding directly into the intermediate channel.
Each train is also equipped with an isolation valve. This is to
isolate one train while the other is down or under mechanical repair.
Make sure the isolation valves are open to allow flow to pass through
when the screen valve or the train valves are closed. Damage can occur to
the influent pumps if all the discharge valving is closed off.
Bypassing the fine screens occurs a few times throughout the year and is
always coordinated with the Maintenance/Engineering Department
➢ Draining or cleaning of the water treatment settling tank;
Draining and cleaning of the water treatment contact chamber;
Y Draining and cleaning of the holding ponds and reservoirs
14

Table 5.5 (continued Mechanical Precision Sereener E ui . ment List
Description
Rated Capacity
Driver Data (HP-
Notes
12PM-Volts)
Mechanical Screen MS-201
100 Coarse Screen
700 GPM
NA
Mechanical Screen MS-202
100 Coarse Screen
700 GPM
NA
Mechanical Screen MS-203
100 Coarse Screen
700 GPM
NA
Mechanical Screen MS-204
100 Coarse Screen
700 GPM
NA
5.3 EQUALIZATION BASIN
Wastewater flows to the equalization basin (EQ) from the
intermediate channel. A pneumatically actuated flow control valve,
installed in a concrete vault adjacent to the EQ basin, is designed to
throttle flow from the equalization basin to the aeration lift station. The
valve control panel is located in the aeration lift station on the left side as
you walk into the building entrance. The panel is equipped with air
regulators to adjust the amount of air pressure applied to the valve unit.
The air pressure gauges are used to adjust the valve open, partially open,
and closed position.
The EQ basin level indicator is located in the plant office and is
controlled by a bubbler system. Air to the bubbler system is feed from an
air compressor unit located in the screen house. Forced air from the
compressor enters a bubble tube submerged in the liquid wet well. The
depth of the liquid is determined by measuring the pressure needed to
force the bubbles out of the line. The pressure required is converted to
depth in feet.
The Intermediate Channel is equipped with a slide gate valve to
direct flow to the EQ Basin or the Aeration Lift Station. Directing flow to
the equalization basin dampens instantaneous peak flows that occur
throughout the day and reduce loading spikes on the secondary system.
The basin can also be used as an emergency spill basin. An accidental
spill or toxic dump can be neutralized or isolated in the equalization basin.
Toxicity causes severe reduction or death of the microorganisms and
produce system and effluent upsets. Mill latex dumps are currently
isolated utilizing the equalization basin. Mill operators call treatment
plant staff with specific information when latex solution is discharge from
their process lines. This allows plant staff time to close the intermediate
channel gate valve to the aeration lift station, directing flow to the EQ
Basin.
15

.uff a. yR7cNIVEIRM111mIi. -M.1011112
The aeration lift station incorporates three Gorman -Rupp suction
lift pumps (13-401, P-402, and P-403), to pump the EQ basin or
Intermediate channel to the aeration basin. The lift station is equipped
with continuous level indication provided by a transducer. The level
control system is located in the plant office adjacent to the EQ level
indicating system. The aeration lift station system is equipped with a
Dwyer pressure transmitter that converts the line pressure to a 4-20
milliamp output signal. "The analog signal operates the aeration lift pump
controls based on the level in the lift station wet well. All three pumps are
equipped with variable fi•equency drive (VFD). However, only one pump
is operated by the VFD while the other two pumps are in standby mode.
Any of the three pumps can operate in the lead position by adjusting the
control panel pump selection. Pump Number 1 is the dedicated lead pump.
The lead pump is operated by the VFD to provide uniform flow to the
aeration basin. Pumping rates increase as the liquid level increases to
maintain water levels at a desired range.
Table 5.6 Aeration Lift Station Equipment List
Description
Rated Capacity
Driver Data
Notes
(IIP-RPM-Volts)
Wet Well T-401
14 Pi' x 22 PT x 12.5
Intermediate Wet
f'I'
Well
Aeration Lift Pump P-401
20-1180-208
20-880-208
11'1-0 Drive
Aeration Lift Pump P-402
20-1180-208
20-880-208
PTO Drive
Aeration Lift Pump 1`403
20-1180-208
20-880-208
PTO Drive
Table 5.7 Aeration Lift Station Control Settings
Aeration Lift Station
Pumps
Lead Pump
Lead Pump
Lead and Secondary Pump
VFD Frequency Hz
46.4 1 lz
46.1 1lz
46.1 1lz
Table 5.8_ "Three Position Pum) Control Switch
Approximate Plow Rate
(gpm)
1640
2132
3000
Three Position Pump Control Switch Lead Pump Secondary Pump
I Pump Position #1 pump #3 Pump
2 Pump Position f7 2 Pump # I Pump
3 Pump Position #3 Pump #2 Pump
16

There is a manual/auto control switch located on the control panel. Also,
each individual pump has a manual/auto control button. When one pump
is out of service or under repair, one of the two other pumps can operate in
the lead position. With any pump operating in the manual mode, the
liquid level requires constant monitoring to prevent the pump from
running dry. Upon completion of maintenance or repairs activities, the lift
station should be placed back into automatic position.
5.5 AERATION BASIN
The aeration basin contains four surface 30 hp mechanical aerators (A/B
aer-230, 231, 232, 233) and four surface 7.5-15 hp mechanical mixers
(A/B mix-220, 221, 222, 223). Under the original design, the wastewater
discharges from the aeration lift station to seven locations in the aeration
basin.
Table 5.9 Aeration Basin Equipment List
Description
Rated Capacity
Driver Data
Notes
(HP -RPM -Volts)
Aeration Basin T-402
2.1 MGAL
215 ft DIA. 12 ft TD
Aerator A-230
NA
30-1170-460
ABS Oxygun Aerator
Aerator A-231
NA
30-1170-460
ABS Oxygu❑ Aerator
Aerator A-232
NA
30-1170-460
ABS Oxyguo Aerator
Aerator A-233
NA
30-1170-460
Aqua -Aerobic aerator
Mixer A-220
NA
10111,
Aqua -Aerobic mixer
Mixer A-221
NA
10111,
Aqua -Aerobic mixer
MixerA-222
NA
10 HP
Aqua -Aerobic mixer
MixerA-233
NA
IOHP
Aqua -Aerobic mixer
Three of the four 30 HP aerators are manufactured by ABS Inc.
These Oxygun aerators are positioned at near equal distanced fi•om one
another in the aeration basin. The Oxygun aerators disperse atmospheric
air below the water surface using a unique impeller and diffuser system.
Atmospheric air is aspirated down the hollow shaft, through the ports, and
into the wastewater. The motor /shaft assemble tilt angle can be adjusted
by the position in the frame assemble. This allows for unique adjustment
in the aeration zone of influence towards the tank bottom, side walls, and
horizontal surface. The float assemble consists of three polyethylene shell
pontoons, with UV inhibitors, that resist water and wastewater. The
remaining surface aerator and mixers are manufactured by Aqua -Aerobic
Systems. The 30 HP aqua -jet aerator is a direct drive aerator. The
diffusion head design changes the direction of the fluid, flowing at high
velocity, from vertical to horizontal. This feature of the Aqua -jet aerator
and mixers dilutes and blends influent wastewater and return activated
sludge material and maintains uniform dispersion of the treatment
solution. All aerators and mixers use polypropylene rope to secure the
units in place of operation.
17

5.6 CLARIFIERS
The aeration basin effluent flows to a splitter box where the flow is
directed to two secondary clarifiers. The splitter box is designed with an
adjustable slotted pipe to remove floating scum exiting the aeration basin.
Each clarifier is equipped with a lateral slide gate valve to open, partially
open, or close the direction of flow to the clarifier. The gate valve is
closed to isolate the clarifier for maintenance repair and inspections. The
sluice gate valves are self contained manually operated with a hand wheel
lift mounted directly over the head angle. Under normal operating
conditions the slide gate valves are in the open position.
The two clarifiers are identified by name of North and South
clarifiers. The local controls for the clarifier unit are located near the
center well. The clarifier control panels are located in the RAS building
located adjacent between the two clarifiers.
The clarifiers are sedimentation tanks with circular configuration.
The clarifier is center feed with a scrapper sludge removal system. Plow
enters the center well and liquid solids separation takes effect. The radial
effluent flows past v-notch weir plates to a collection drain system
(effluent trough). The flow from the effluent trough is directed to chlorine
contact chamber for disinfection. The solids settle to the bottom of the
tank where the scrapper assembly collects the sludge to the conical base.
From the cone shaped center, the sludge is returned back to the aeration
tank as activated sludge or it is wasted to the digester tank as waste
activated sludge. Oil and scum are skimmed by a radial arm at the surface
of the water which deposits the material into a sump. The sump contents
are directed to a collection wet well. Scum sump contents can be directed
to the aeration lift station or the digester tank.
Table 5.10 Equipment List
Description
Secondary Clarifier T-501
Secondary Clarifica T-502
Splitter 130x T-503
Sludge Rake SR-501
Rated Capacity
0.376 MGM.
0,376 WAL
Driver Data (HP -
RPM -Volts)
1-1750-208
Notes
80 FF DIA- 9 FT SWD
80 FT DIA, 9 FT SWD
Limit Switch OL
18

5.7 EFFLUENT FLOW METER
Effluent flow is recorded continuously as it passes through a 3 foot
rectangular weir. The Isco 4210 flow meter monitors and records the
liquid level with an ultrasonic level sensing devise. The ultrasonic sensor
is mounted above the flow stream measuring the level and converting into
flow rate. The meter is equipped with a printer that records flow and other
level monitoring parameters. The printer paper is easily replaced by the
plant operator. The 4210 flow meter is equipped to collect effluent
composite samples flow proportioned. Also, the 4210 flow meter is
equipped to disinfect the wastewater using flow proportion.
In the event of a failure of the flow meter, the influent flow meter
can be utilized as a flow measuring instrument.
5.8 SLUDGE HANDLING FACILITIES
5.8.1 Sludge and Scum Pumps
The control panels and pumps for the scum pumps are all housed in the
RAS Building. The sump pumps draw from #7 manhole and pump to
either the head end of the plant (Intermediate Pump Station) or to the
sludge holding tank. Under normal operation, the scum pump discharge
line is valves to the Intermediate Pump Station. There are two centrifugal
200gpm Gorman -Rupp pumps that operate off a bubbler level control
system. The scum discharge line is equipped with an electromagnetic
flow meter to digitally record and verify flow rates.
Table 5. I1.1 Equipment List
Description Rated Capacity
Driver Data (HP- Notes
RPM -Volts)
Scum Pumps P-506 200 gpm (%26 ft
7.5-1760-208 Scum
Scum Pumps P-507 200 gpm C 26 ft
7.5-1760-208 Scum
The RAS pumps are operated continuously with a maximum flow rate of
1400 GPM. There is a dedicated RAS pump for the north and south
clarifiers. There is a backup RAS pump that can be used to return sludge
from both the north and south clarifiers. This pump also acts as an
emergency pump when one of the primary pumps fail or is under repair.
There are manual throttle valves located on the discharge plumbing.
19

Table 5_1 ].2 Ed_uipn�ent List
Description Rated Capacity
RAS Pump P-501 1400 gpm (ii; 32 tt
RAS Pump 11-502 1400 gpm a 32 11
RAS Pump P-503 1400 gpm !a) 32 fl
Driver Data (HP- Notes
RPM -Volts)
20-1760.208 RAS
20-1760-208 RAS
20-1760-208 RAS
The waste pump is typically operated on a time basis and determined by
process control conditions. Under normal conditions the operator
determines the volume of sludge that needs to be wasted and manually
operates the WAS pump for the time required to waste that volume. To
operate the pump, open the discharge valve and place the switch to the
"on" position. There is a WAS pump dedicated specifically for the north
and south clarifiers. The WAS pumps discharges to the aerobic digester
tank. The WAS discharge line is equipped with an electromagnetic flow
meter to digitally record and verify flow rates.
Table 5.11,3 rquument List
Description Rated Capacity Driver Data (HP- Notes
RPM -Volts)
WAS Pump 11-504 100 gpm g 15 n 3-1745-208 WAS
WAS Pump P-505 100 gpm ((�, 15 ft 3-1745-208 WAS
5.8.2 Aerobic Digester (Sludge Storage Tank)
Waste sludge from the north and south clarifiers are directed specifically
to the aerobic digester. Scum pumps can be directed to the aerobic
digester or the intermediate lift station. After wasting, the sludge is
allowed to settle in the tank for 24 hours. After settling, the clear
supernatant lying above the sludge is directed back to #i7 manhole by a
manually operated decanting boom. The sludge storage tank is aerated
with course bubble diffusers powered by two mechanical blowers. Once
the sludge storage tank is decanted the tank can be filled by wasting back
and the settle and decant process can be completed again. Once the sludge
has reached the desired concentration the sludge Transfer Pump directs the
flow to the sand drying beds.
20

Table 5..11.4 Equiiament List
Description
Rated Capacity
Driver Data (HI'-
Notes
RPM -Volts)
Blower I3-801
NA
10-1755-208
NA
Blower B-802
NA
10-1755-208
NA
Sludge Storage Tank T-801
26 PT DIAMETER;
NA
1 I PT DETTI-I
Sludge Transfer Pump P-901
NA
7.5-1160-208
NA
Under drain pump 11-902
NA
7.5-208
NA
Sludge Drying Bed 1'-901
35P"1-x821'T
NA
NA
Sludge Drying Bed T-902
35PTx82F1'
NA
NA
Sludge Diving Bed T-903
35PTx82T
NA
NA
Sludge Drying Bed '1'-904
35PTx821-1'
NA
NA
Sludge Drying Bed T-905
351-Tx82FT
NA
NA
Sludge Drying Bed T-906
35PTx821'7
NA
NA
Polymer Pump P-1001
NA
NA
NA
Polymer Mixing Tank T-1001
NA
NA
NA
Polymer Mixer M-1001
NA
NA
NA
5.8.3 Sand Drying Bed
Sludge from the storage tank is pumped to one of six sand drying beds.
While the sludge is transferred to the drying bed the operator may enhance
the sludge drying time by the addition of a polymer. To process the
sludge with polymer, the operator starts the sludge transfer pump and the
polymer pump simultaneously. The operator needs to determine the
correct polymer makeup, polymer pump speed to achieve the best sludge
dewatering as it is applied to the sand drying bed. Once the treatment is
started the best method to achieve good solids separation is to adjust the
polymer pump speed knob. The goal is to produce a sludge cake on the
sand bed that will dewater and dry the quickest.
Polymer PT-1644 is stored in 55-gallon drums and mixed with
makeup water in a 1500 gallon mix tank. To make a batch of dilute
polymer for use in the sludge dewatering process, ten gallons of polymer
is added to 1500 gallons of makeup water. The makeup tank is manually
21

filled and the operator must be cautious not to overfill the polymer
makeup tank.
5.8.4 Sludge Disposal
Sludge disposal from the sand drying beds is performed through the land
application program. There are 520 dry tons per year of residuals allowed
to land apply according to the Permit No. WQ0013982. The operate] -
must read and understand the parameters of the land application permit.
The operator is subject to the conditions and limitations that are specified
in the permit. The operator must also pay particular attention to the
monitoring and reporting requirements as specified in the permit.
Notification of a Land Application Event must be made to the Regional
Office — Aquifer Protection Section at least 48 hours prior to conducting
any land application. Such notification shall indicate the anticipated time
land application activities will commence, field ID, and its location. If
changes to the application schedule are necessary, the Regional Aquifer
Protection Supervisor shall be notified at least 24 hours prior to the new
commencing schedule or as soon as possible if changes are due to
unforeseen weather.
When residuals are applied to grazed pasture, hay crop nutrient rates shall
be reduced by 25% in accordance with the USDA-NRCS 590 Nutrient
Management Standards.
5.8.5 Sampling and Monitoring
All sampling and monitoring of the Land Application Program must at a
minimum comply with Attachment A of the Land Application Permit
number WQ0013982.
All sampling will be conducted by the Operator in Responsible Charge or
the Back-up Operator in Responsible Charge. This includes:
Condition IV.2 Annually
Condition IV.3 Condition IVA Dry'Fons <319 1/year
Condition IV.3 Condition IVA Dry Tons >319-<1,650 4/year
Condition IV.3 Condition IVA Dry Tons>1,650 -<6/year
Condition IV.3 Condition IVA Dry Tons>16,500 monthly
Condition IV.5 Annual Solis Analysis (i.e. Standard Soil Fertility
Analysis)
15A NCAC 02T .1106 (c) Pathogen Reduction Requirements
For biological residuals to be classified as Class B with respect to
pathogens one of the following shall be met:
(1) Fecal Coliform Density Demonstration. Seven samples of the
biological residuals are collected at the time the residuals are used or
22

disposed, and the geometric mean of the density of the fecal Coliform
in the samples collected is less than either 2,000,000 Most Probable
Number per gram of total solids (i.e. dry weight) or 2,000,000 Colony
Forming Units per gram of total solids(i.e. dry weight basis)
(2) (B) Air Drying, Biological residuals are dried on sand beds or on
paved or unpaved basins for a minimum of three months. During two
of the three months, the ambient average daily temperature is above
zero degrees Celsius.
15A NCAC 02T .1107 Vector Attraction Requirements
In order to meet the Vector Attraction Requirement the bio-solids must
meet one of the following conditions from 15A NCAC 02T .1 107 (a)
(6) Alkaline Stabilization. The pI-I of the bio-solids residuals shall be
raised to 12 or higher by alkali addition and, without the addition of more
alkali remain at 12 or higher for two hours and then at 11.5 or higher for
an additional 22 hours.
(7) Drying of Stabilized Residuals. The biological residuals shall be dried
to 75 % total solids if the biological residuals contain no unstabilized
solids from a primary treatment process. Mixing of the biological residuals
with other materials shall not be used to meet this alternative.
5.8.6 Land Application Site Inspection
The land application site must be inspected by the Operator in Responsible
Charge (ORC) or Back-up Operator in Responsible Charge at least once
per week after the initial Bio-Solids have been applied to a field for a
period of thirty days (30) after application.
ORC Glen Gary
Back-up ORC Billy Stone
Site inspection report must include:
Date, Time and Inspector
Visually inspect for no animal grazing during the 30 day period.
Inspect cattle fence and perimeter fence for breeches.
Insure all setbacks were observed during spreading of bio-solids.
Complete Duvaltex US Inc., Inc. Land Application Site Inspection Form
Any Non Compliance must be reported by telephone to the Winston-
Salem Regional Office telephone [phone] as soon as possible, but
no later than 24 hours or the next business day. Any emergency requiring
immediate reporting outside of business hours must be reported to the
Division's Emergency Response personnel at telephone [phone]
[phone] or [phone]
23

5.8.7 Spill Control Plan
In the unlikely event of a spill, the following action shall be taken
immediately:
Spill prevention. Liquid Land Application:
Project Manager shall take the immediate following steps:
• Ensure personnel monitor tanker while loading.
• Ensure valves and lids are closed and latched while transporting.
2. Halt source of the spill- overturned truck, leaking valve, ruptured tank.
Contain spill. Use straw bales and absorbents to form a barrier. In
addition to straw bales, use shovels to form an earthen barrier to
augment straw bales.
Cleanup. Employ vacuum equipment to remove as much spill material
as possible. Complete clean up by scattering straw from bales, soaking
up remaining materials. Pick up straw manually, and dispose in
landfill.
5. Final cleanup. Plush roadways with water as necessary to clean.
Allow to dry and incorporate if a spill occurs on a non -paved and
tillable area. In the event, a spill occurs on private property, final
cleanup should be completed immediately to the satisfaction of the
owner.
6. Notification. As soon as possible after the spill occurs, notify:
• Glen Gary, WWTP Manager [phone]
• NC DENR field office [phone]
• County Sheriff Dept. 911
• Fire Dept. — if assistance is required for wash down, etc. 911
7. Management of cleanup efforts. The project manager shall take
immediate charge and initiate cleanup activities. Additional labor
shall be requested from the plant as needed. The project manager shall
also communicate with the public on the scene answering and advising
of cleanup activity.
Reporting. Any emergency that requires immediate reporting (e.g.,
discharges to surface waters, imminent failure of a storage structure,
etc.) outside of normal hours must be reported to the Division's
Emergency response personnel at telephone number [phone],
[phone], or [phone]. Duvaltex US Inc. COO will
review this report before being sent to NCDENR within five days.
24

6. OPERATIONAL CONTROL OF ACTIVATED SLUDGE:
Process Theory and Performance
6.1 MIXED LIQUOR SUSPENDED SOLIDS
The MLSS concentration is used as a measure of the amount of
microorganisms available in the biological system for treatment. The
Duvaltex US Inc. Wastewater "Treatment Facility currently targets a MLSS
concentration of 3,500 mg/L to 5,000 mg/L, which is within the typical
range of MLSS for an extended aeration facility. Maintaining this MLSS
concentration is achieved by returning settled sludge from the secondary
clarifiers at a constant rate of 500-700gpi-n and wasting sludge as required.
These two parameters are also used to control the depth of the sludge
blanket in the secondary clarifier.
6.2 RETURN SLUDGE RATE CONTROL
The objective of return sludge rate control is to optimize the distribution of
solids between the aeration basins and the clarifiers. An appropriate
amount of solids needs to be returned to the aeration basins to provide
proper biological treatment, to allow proper settling and thickening in the
secondary clarifier, and to prevent the sludge blanket in the clarifier from
rising which could result in solids being washed out of the clarifier in the
plant effluent.
If return rates are too low:
1. The sludge blanket in the clarifier could rise, potentially resulting in
solids being carried out of the clarifier in the plant effluent.
2. The aeration basis MLSS concentration could decrease, resulting in an
insufficient mass of microorganisms to treat the incoming BOD.
3. The solids in the clarifier could become anaerobic (septic) which
would result in floating solids, sludge bulking (sludge not settling in
the clarifier), and odors.
If return rates are too high:
1. The solids would not be able to properly thicken in the clarifier, which
can be identified by low solids concentrations in the return
sludge/waste sludge.
2. The increased return rate would increase the hydraulic loading on the
clarifier which could result in solids washout due to inadequate settling
time.
The W WTP typically runs the return sludge pumps at a constant rate of
approximately 500-700 gpm when the MLSS concentration is at the target
of 3,500 mg/L to 5,000 mg/L. If MLSS concentration is below the target
level the RAS rate should be increased to approximately 75 — 100 gpm
until the target value is reached, thereafter the RAS rate should be returned
to the constant rate setting.
25

6.3 WASTE SLUDGE RATE CONTROL
As the microorganisms degrade the organic matter in the waste stream,
more microorganisms are created. If no sludge wasting was performed
this process would lead to continually increasing MLSS concentrations.
Eventually this should lead to too many microorganisms for the food
available and/or an overload of solids to the clarifiers resulting in reduced
treatment efficiency. Wasting sludge provides control of the solids
inventory in the system to ensure proper system performance.
Additionally, as the microorganism's age they become less
effective and eventually die. These old, ineffective and dead
microorganisms must be removed from the system to maintain proper
system performance. Wasting sludge also removes inert solids from the
system.
Sludge wasting is currently done on a time basis. The operator
measures the MLSS concentration and determines if it is within the target
range. If MLSS levels are higher than the target value, the operator must
calculate how much sludge need to be wasted and how long the sludge
wasting pumps will need to be run to waste the appropriate volume.
6.4 DISSOLVED OXYGEN CONTROL
Activated sludge microorganisms need oxygen to break down the organic
matter and grow new cells. The oxygen must be dissolved in the mixed
liquor to be useful. It is measured in the field as dissolved oxygen, or DO.
The target value for DO at the Duvaltex US Inc. Treatment Plant is 1.5
mg/L. The DO levels in the basin should be checked on a daily basis to
ensure proper DO levels are being maintained. Insufficient oxygen will
create an unfavorable environment for the organisms and possibly
encourage the growth of filamentous organisms, which can cause foaming
and sludge settling problems.
6.5 NUTRIENTS
Organic nitrogen and phosphorus -containing compounds are essential to
the growth of microorganisms in the activated sludge system. The
generally recommended ration of BODs-to-nitrogen-to phosphorus is
100:5:1 (lbs). Since influent BOD is not measured a direct dosage
requirement cannot be calculated. Ammonia, if not converted through
nitrification to nitrite and nitrates, can cause acute (lethal) toxicity to
aquatic life such as macro invertebrates and fish species.
26

6.6 PRODUCTION FLUCTUATIONS
Decreases or increases in production rates can affect the treatment plant
performance if sustained for long periods of time. During temporary plant
shutdowns or holidays lasting up to one or two weeks, hydraulic
equalization tank levels should be managed to allow for consistent flow
rates into the system. The MLSS concentrations may also need to be
reduced prior to shutdown to compensate for reductions in food -to -mass
ratios. Aeration rates may also be reduced to avoid over -aeration and
super saturation which could cause hindered solids settling.
Significant increases in flows and loading due to sustained production
increases or changes may require the following:
■ Increase aeration rates (oxygen supply) as necessary to maintain
adequate DO:
• hicrease RAS and WAS rates as necessary to maintain manageable
solids concentrations and mass in the system; and
■ Increase solids dewatering to allow for increased wasting as necessary.
6.7 SETTLING AGENT
The Duvaltex US Inc. Wastewater Treatment Facility currently uses PT-
318 as a coagulant to aid in settling in secondary clarifiers. The dosage of
PT-318 (if needed) is set at 40 percent stroke and 20 percent seed on the
60 gpd metering pump. Then adjusted as needed for aid in settling of
solids.
6.8 TROUBLESHOOTING
Operational problems can be grouped by conditions that the operator can
observe in the aeration basins and the secondary clarifier. Aeration tank
problems include low DO, odor, inadequate mixing, color changes,
turbulence, surging, and foaming.
Clarifier problems include solids washout, bulking sludge,
clumping or rising sludge, cloudy effluent, pin floc, and straggler floc.
6.9 SETTLEABILITY TEST
The settlability test is a qualitative test that shows the settling
characteristics of the mixed liquor cinder controlled conditions. The
following is a brief description of the settlability test:
The test is performed by taking a sample from the aeration basin
after the aeration system has been running for ten to fifteen minutes. Use
this sample to fill a settleometer, an open jar typically about 2 liters in
volume. Let the sample stand and watch the formation and settling of the
floe. At the end of thirty minutes the settleometer should be about half
full of settled solids with clear water above. The solids should have a
chocolate brown color and should appear granular.
If the solids do not settle half way and the water above them is
cloudy or murky a longer aeration time, or solids wasting is needed. If the
solids settle to less than a quarter of the settleometer depth and the water
27

above the solids is cloudy or murky, no wasting of solids should be done
and the solids level in the aeration basins should be allowed to increase. If
the solids settle to the bottom of the jar with a clear liquid on top and stay
down for one hour and come up in two howl, this is an indication of good
operation. If the solids should rise in only one hour, this is usually an
indication of too much air or too many solids.
Another possible reason for solids rising in one hour could be that
there are not enough solids under aeration. When this happens the sludge
will rise because of the high respiration rate (breathing) of the overtaxed
organisms and the rapid DO depletion caused by these organisms in the
settling compartment. Under these circumstances the operator should try
to increase the mixed liquor suspended solids concentration.
6.10 MICROSCOPIC EVALUATION
Microscopic evaluation of the mixed liquor can give an indication of the
health of the biomass and can be used as a predictive and diagnostic tool
for the treatment process. Microscopic evaluation should be performed on
a regular (daily) basis so that changes in the relative quantities of different
organisms can be trended.

7.0 PERSONNEL
7.1 STAFFING PLAN
The organizational staffing for the Elkin plant consists of the below
listed positions and responsibilities that are listed below. The normal staff
schedule is Monday through Friday from 7:00 to 4:00pm. All normal
operations, maintenance, and in-house laboratory testing is expected to be
accomplished during the normal work week.
o Wastewater Treatment Plant Manager, Grade IV Operator
(Operator Responsible in Charge -> ORC)
The plant operator is responsible for the proper operation of the
mechanical, electrical, hydraulic, and biological processes to
ensure they perform as intended in the treatment of wastewater
from the Duvaltex US Inc. Manufacturing. The Plant Operator is
responsible for reporting and record keeping at the plant.
o Backup Operators: There is I backup operator at the Duvaltex US
Inc. facility that works for the Maintenance department, and has
his operator license. He fills in for the ORC at the WWTP when
needed. He also is on weekend call duty for the W WIP.
o Environmental Manager. Responsible for maintaining adequate
resources for plant operations.
o Chief Operating Officer or Environmental Coodinator,
Responsible for signing monthly DMR's
7.2 LICENSING and CONTINUING EDUCATION
The wastewater treatment facility must be operated by a Grade IV
wastewater treatment facility operator licensed in the state of North
Carolina. Furthermore, the ORC along with all back-up operators must
keep their license active by receiving training of at least 6 training contact
hours per year.
29

8.0 SAMPLING AND LABORATORY ANALYSIS
8.1. SAMPLING POINTS AND REPRESENTATIVE SAMPLING
The primary goal of sampling is to ensure that the sample obtained
will be representative of the wastewater to be analyzed. Because the
sample represents only a small portion of the flow both sample site
selection and techniques are crucial.
Several guidelines to ensure representative sampling include the
following.
• Collect sample at points where the sample stream is well mixed, such
as in aerated channels or at a location of hydraulic turbulence.
• Avoid taking samples where settling occurs or where large chunks of
floating debris exist.
• Avoid areas with non -representative deposits or solids accumulated on
channel walls.
• After choosing the sample sites, mark them with paint or some other
means and always sample at those locations.
• Clearly mark sample containers for each sample location. Do not
rotate containers fi-om site to site.
• Keep samples thoroughly mixed throughout the collection and
measuring procedure to prevent settling.
• After collection, store the samples either in ice or in the sample
refrigerator so that their composition will not change before testing.
Refrigeration at 4°C or less is required.
The rnost widely used identified locations for sampling are the following:
Influent: Screen outlet
Mixed Liquor: Aeration Tank effluent weirs
Effluent: Post Aeration Weir Prior to Outfall Pipe
8.2. GRAB SAMPLES
A grab sample is a discrete sample that is collected manually. Grab
samples are used if the operator must know the characteristics of the
process stream soon after the sample's collection. Examples of such
parameters include pH, DO, temperature, low level residual chlorine,
Fecal Coliform, and soluble sulfide.
8.3. COMPOSITE SAMPLES
A composite sample is a single sample prepared by combining or
composting a number of grab samples during a specific period, usually 24
hours. The plant's NPDES permit requires collection of composite
samples for BOD, COD, TSS, Total Nitrogen, etc.
30

8.4. FLOW -PROPORTIONAL COMPOSITE
A flow -proportional composite requires varying either the volumes among
the grab samples or the sampling frequency, to weight the final sample in
proportion to the several flow rates measured during the composite sample
period. Such a composite contains wastewater reasonably equivalent to
the flow -weighted average composition of the process stream during the
composite sampling period. In effect, the total composite volume
collected is proportional to the total flow volume past the sampling point.
Accordingly, flow -proportioned composite sampling demands accurate
measurements of the varying flow rates of the process stream.
8.5. SAMPLING FREQUENCY
Grab samples are collected for process control testing and pH tests on a
daily basis. Both grab and composite samples are required for effluent
reporting, depending on the parameter to be analyzed.
8.6. COLLECTION and ANALYSIS of SAMPLES for NPDES
FREQUENCY
Duvaltex US Inc. is required to collect and analyze a composite sample as
defined in the NPDES discharge permit (Part II of the NPDES Permit). At
Duvaltex US Inc. W WTP, the recommended sampling procedure is a
sample taken using an ISCO refrigerated sampler for effluent NPDES
reporting, which keeps the samples at 6°C as required for sample
preservations.
Please refer to the "EFFLUENT LIMITATIONS AND
MONITORING REQUIREMENTS" page of the permit for the required
samples needed.
Table 8-1 (below) summarizes the testing frequencies, sample
volumes, container types, preservation techniques and maximum
allowable holding times for the effluent sampling and analysis required by
the NPDES permit. Note that all analysis, except for pH, required for
effluent reporting is performed by outside laboratories.
31

Table 8-1-Effluent Testing Frequencies*, Sample Volumes, Containers, Preservation Techniques and Ma)
Hol Ing Times - ------ -
---
- �
Container
--
Sample
(P=Plastic)
Analysis
Frequency
Volume
Glass
Preservation
- -
Maximum Holding Tin'
BOD
Dail_ -
500mL
P,G
Cool 4°C
48 Hours
Cool 4°C
0.5 mL H2SO4
COD
Weekly
250mL
P,G
(PH<2)_
28days _
TSS
Daiy-_
500mL
P,G
Cool, 4°C
Cool, 4°C
2mL,2N
Zn acetate
Sulfides
2/Month
500mL
P,G
NaOH to pH>2
7 days .........
-- --
-- --
-
-------
Cool, 4°C
1mL H2SO4
Phenols
2/Month
1 L
G
�pH <2) _
28 days
1mL1HNO3
Chromium
2/Month
500mL
P,G
__ (pH<2�_—
6Months�180d�
Fecal-
--
---....-
Coliform
Cool, 4°C
(geometric
Add sodium
mean _
2/Month
250 ml
P -
thiosulfate
8 hours
Total
Residual
Analyze Immediately (withi
Chlorine
Daily-
1 L
G
None
minutes)____
Analyze Immediately (with)
250mL
P,G
None
minutes)
Analyze Immediately (with!
Temperature
Dail_
250 ml
P, G
None
minutes _ __
Total
Nitrogen
Cool, 4°C
(NO2+ NO3+
1mL H2SO4
TKJ_
Monthly
250 ml
P, G
(pH <2)-._...-
_ __- 28 days
Cool, 4°C
Total
1mL H2SO4
_Phosphorus_
____ Months
250ml
P, G
_ _pH <� ___ __
_28 days
Chronic
_ Toxici�_
_ Quarterly___
1.0 liter
-_ P _-_
Cool, 4°C
_ 36 Hours__ _
32

Flow I Continuous
NA I Influent or
* Frequencies reflect the NPDES permit issued November 51h, 2008 to
Duvaltex US Inc. WWTP.
8.7. IN HOUSE TESTING
In-house testing is performed to allow the operator to evaluate the
treatment process and make adjustments as required. The following are
analysis performed by the operator for process control. In addition to the
process control testing, the operator also performs daily p1l, temperature,
and low level chlorine analysis for NPDES reporting. Procedures for
these analyses are located in Appendix B.
8.8. QUALITY ASSURANCE
8.8.1 EPA QA/QC TESTING
An annual DMRQA or PE sampling must be completed by the Duvaltex
US Inc. Wastewater treatment plant. This QA/QC testing must be
performed for all parameters that are performed in-house that are
reportable compliance parameters for the Daily Monitoring Report
(currently pH and Total Residual Chlorine), The EPA letter instructs
treatment plant employees to purchase samples from certain suppliers,
analyze the samples, and return the results of the analysis to the vendor
and the state. For all parameters analyzed by outside laboratories, the
laboratory is responsible for performing their own QA/QC testing.
In order to be compliant with all parameters on the permit, Pace
supplies the W WTP personnel with their QA/QC results, which are sent to
their vendor and NCDENR with the results of testing.
8.8.2 CHAIN OF CUSTODY
A Chain -of -Custody form is a legal term for an unbroken sequence of
possession from sampling through analysis. 'phis type of form is
completed when sending out samples to an outside laboratory certified for
33

performing analyses for North Carolina. In order to prevent any
possibility of confusion regarding the sampling location, type, etc., the
following items for chain -of -custody need to be completed:
• Sample source/location;
• Sample date and time;
• Sample type (grab or composite);
• Preservative(s) (if any) added;
• Required analyses;
• Date submitted to the laboratory; and
• Signature of the person collecting the sample.
In order to verify that the chain-of'custody form is complete, the necessary
information listed above should also be correctly labeled for the specific
sample bottle using a waterproof marker.
All of the above data is needed for samples transported off -site to an
outside analytical laboratory. For routine samples collected and analyzed
on the site, the data may be limited to the first three items on the list, but
only if there is no possibility of confusion.
34

9.0 RECORDS AND REPORTING
9.1 OPERATIONS RECORDS
9.1.1 GENERAL
For the successful and efficient operation of the wastewater treatment
system, all operation, maintenance, and laboratory data shall be recorded
in a neat, orderly manner. Daily bench sheets and a monthly operating
log are stored in the wastewater treatment plant laboratory. These are
maintained as an initial method for recording key information. It is
reasonable to expect that changes in the recording format may take place
as the plant operator becomes more experienced with the treatment
system.
Some recording practices are common to both the daily bench sheets and
the monthly log. These practices include:
I. All entries in the logs should be made clearly in pen.
2. If an error is made in an entry, a line should be drawn through the
entry and the correct entry made. Furthermore, the entry should be
initialed by the analyst. Never erase or white -out entries.
3. Folders are used for storing laboratory bench sheets. All supporting
daily operations entries are made in the operations log.
9.1.2 DAILY LOG
The following guidelines should be used when keeping the daily log:
1. Entries to the log should be made daily.
2. Every operational day should have a corresponding bench sheet.
3. In using the "remarks' sections, do not be lengthy in your comments.
4. Use the daily log as a reminder for the month. This will provide
important information for reference. At the end of each week, check
back through the daily operations log to be sure that all important
items have been completed and entered on the appropriate
documentation.
9.1.3 RECORDS STORAGE
The graphs are filed in their own binder located in the Wastewater
Treatment Office and kept current. Records must be stored for at least 5
years according to NCDENR regulations.
9.2 MONTHLY DISCHARGE MONITORING REPORTS (DMR's)
hn accordance with certain provisions contained in the 1974 Clean Water
Act, the United States Environmental Protection Agency (USEPA)
requires that all permitted wastewater facilities submit DMRs on a
monthly basis to NCDENR. [Reporting forms are forwarded by the
USEPA to address all permit monitoring requirements.] The DMR must
be submitted via the NC DENR DWQ eDMR website and regular mail by
the 30"' day of the following month. All effluent parameters and limits are
imprinted on the DMRs. The information collected from a contracted
35

outside laboratory as well as parameter recorded in the daily log and bench
sheets (i.e. pH, low level chlorine, and temperature are used to complete
these forms.
The NCDENR also requires that a monthly O&M Report
accompany the DMR form. 'The O&M report contains key details with
regard to daily operations and laboratory results. Plant personnel use an
electronic version of the O&M Form maintained on the laboratory
computer and enter the relevant data to produce the report form each
month for submission to NCDENR.
Additionally, when Whole Effluent Toxicity Testing is performed,
the test results must be sent to the Environmental Sciences Branch of
DWQ by the 30"' day of the following month.
36

10.0 MAINTENANCE
10.1 ROUTINE MAINTENANCE
Routine maintenance (or plant housekeeping) involves the care of the
overall facility, mainly including mechanical equipment. Walks and
stairways within the plant should be kept clear of debris and should be
washed down often for reasons of health and safety. .
10.2 PREVENTATIVE MAINTENANCI;
Preventative maintenance is the practice of doing maintenance on a
schedule tailored to pre -specified equipment requirements. Examples of
preventative maintenance are lubrication programs and filter changes.
Preventative maintenance is done to prevent breakdown, reduce wear on
equipment, improve efficiency and extend the life of the equipment and
facilities. A copy of the Preventative Maintenance program is attached in
Appendix C.
10.3 CORRECTIVE/BREAK DOWN MAINTENANCE
Corrective maintenance consists of work that must be performed due to a
decline in the efficiency or breakdown of the equipment, such as major
overhauls and emergency repairs. Maintenance personnel should be ready
to handle this type of work at all times to assure that the plant continues to
function within the parameters of its design.
When major tasks are to be completed in-house, the following steps
should be considered:
• Determine the effects of isolating the equipment in question, including
a reasonable estimate for the number of days and/or hours the
component may be out of service.
• Evaluate the staff commitments available to perform the task.
• Review the manufacturer's guidelines to determine parts and tools
needed, number of personnel needed, the completeness of the
instructions and plant personnel's understanding of same, any safety
precautions and questions you may wish to direct to the equipment
manufacturer.
• Discuss problems with equipment representatives, generally questions
can be answered on the phone. Operators should note that the better
the equipment functions, manufacturers receive increased references
and repeat sales, so manufacturers are normally quite helpful in these
situations.
• Take manufacturer's guidelines of the equipment site and manually
disassemble the unit. Personnel should determine and record all
potential problems in performing the task before initiating the
assignment.
• When possible, initiate repairs at the beginning of the week. More
supplies are available and there will be a greater possibility of
37

scheduling outside aid if needed. Adequate lifting equipment and
special tools must be scheduled.
• After disassembling a unit, manually add missing (if any) instructions
to the manufacturer's guidelines. This information should be
recorded in the equipment files.
Although the preceding steps may seem to be unimportant, experience
indicates that, by conducting maintenance tasks in this fashion, treatment
plants have reduced maintenance expenditures in addition to providing a
training mechanism for personnel and keeping plant operations stable.
W

11. EMERGENCY RESPONSE PROGRAM
11.1 EMERGENCY RESPONSE (ICP)
Duvaltex US Inc. has a comprehensive emergency response plan. This
plan is contained within the document titled "Integrated Contingency
Plan" (ICP) for Duvaltex US Inc. A copy of the ICP is kept at the W WTP
Office in the case of the following emergencies:
• Chemical Spill Emergency
• Medical Emergency
• Fire/Explosion Emergency
• Gas Release Emergency
• Weather Emergencies
11.2 CRITICAL EQUIPMENT FAILURE (TREATMENT
PROCESS BYPASS)
Treatment Process Bypass
The NPDES permit for the wastewater treatment facility prohibits
bypassing any portion of the wastewater treatment facility which will
result in effluent limitation being exceeded unless:
1. Proper notice has been provided to the regulators (ten days for an
anticipated bypass, 24 hours notice for an unanticipated bypass).
2. The bypass was unavoidable to prevent loss of life, personal injury,
or severe property damage.
3. There was no feasible alternative to the bypass.
If the bypass will not cause effluent limitations to be exceeded, the bypass
is allowable, but ONLY if it is for essential maintenance to assure efficient
operation. For example, if maintenance of the Equalization Basin or the
Aeration Basin is required these tanks may be bypassed, but only if the
bypass will not result in effluent limitation violations.
Please note that NCDENR requires Duvaltex US Inc. to report
any noncompliance which may endanger health or the
environment. Any information shall be provided orally within
24 hours form the time the permittee becomes aware of the
circumstances or the next working day. Furthermore, a written
submission shall also be submitted to NCDENR within five (5)
days of the time the permittee becomes aware of the
circumstances.
39

12. SAFETY
12.1 LOCKOUT / TAGOUT
Duvaltex US Inc. has a strict policy regarding energy isolation procedures.
This policy established the minimum requirements for the lockout of
energy isolating devices whenever maintenance or servicing is done on
machines or equipment. It shall be used to ensure that the machine or
equipment is stopped, isolated from all potentially hazardous energy
sources and locked out before employees perform any servicing or
maintenance where the unexpected tenderization of startup of the machine
or equipment or release of stored energy could cause injury.
12.2 CONFINED SPACE ENTRY PROGRAM
A confined space is defined as a space, which by design has limited
openings for entry and exit unfavorable natural ventilation which could
contain or product dangerous air contaminants, and which is not intended
for continuous occupancy. Confined spaces include, but are not limited
to: storage tanks, compartments of ships, process vessels, pits, vats,
degreasers, reaction vessels, boilers, ventilation and exhaust ducts, sewers,
tunnels, underground utility vaults, and pipelines.
Conditions that are immediately dangerous to life or health (IDLH) are of
utmost concern to Duvaltex US Inc. Confined space entry is one such
operation that if not approached in a safe manner poses a serous threat to
the health and well being of employees and may even cause death.
Confined spaces at the wastewater treatment plant include, but are not
limited, to the following:
• Influent Lift Station Wet well
• Clarifiers
• Clarifier Scum Sumps
• Digester
• Intermediate Lift Station
• > Q valve vault
• Manholes
• Flow Splitter Box
12.3 HAZARD COMMUNICATION PROGRAM
Duvaltex US Inc. provides information to all employees about the
hazardous chemicals to which they are exposed by means of a Ilazard
Communication Program, levels and other forms of warning, Material
Safety Data Sheets, and information and training.
40

12.4 PPE PROGRAM
The proper use of Personal Protective Equipment (PPE) is an integral part
of the company's comprehensive Safety and Health Management
program. Personal protective equipment is available for a variety of uses,
including eye and face protection, foot protection, hearing protection,
respiratory protection, head protection, and hand protection.
Locations containing chemicals in which the Material Safety Data Sheets
(MSDS) should be consulted include, but are not limited to:
• Chemical Feed Pumps
Chemical Storage Areas
The following is a list of areas in the wastewater treatment facility
requiring PPE and the PPE required for each of these areas. These areas
include, but are not limited to:
Entire Treatment Facility
Entire Treatment Facility
Chemical Storage/Feed Areas
Laboratory (performing tests)
Foot Protection
Hand Protection
Chemical Resistant Hand
Protection and
Eye/Face Protection
Respiratory Protection (check
MSDS)
Protection Apron
Long pants/long sleeve shirt
Foot protection (rubber boots
may be required)
Eye/Face Protection
Hand Protection
Note that loose fitting clothing, jewelry, and long hair must all be kept
clear of rotating or reciprocating equipment. At a minimum, head
protection must be worn when working below other workers, working
under conveyer belts, working below machinery, and working in crane
areas.
12.5 WELDING, CUTTING, and BRAZING POLICY
The Duvaltex US Inc. policy on Welding, Cutting, and Brazing Safety has
been developed to prevent injuries and illnesses derived from fire fro n
sparks and splatter, explosions and fires from reactions with welding
gases, asphyxiation, electric shock, inhaling toxic fumes, and eye injuries
from heat rays.
12.6 HEARING CONSERVATION PROGRAM
In order to protect the hearing of all employees and to remain in
compliance with OSHA Standards on Occupational Noise Exposure 29
CFR1910.95, all employees will be subject to the company hearing
conservation program.
41

APPENDIX A
WWTP PERMITS:
Section 1:
Duvaltex US, Inc. WWTP
Permit No. NC0005312
Section 2:
Duvaltex US, Inc. Land Application Permit
Permit No. WQ0013982

Permit NC0005312
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER RESOURCES
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
(NPDES)
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and
the Federal Water Pollution Control Act, as amended,
True Elkin, Inc.
is hereby authorized to discharge wastewater from a facility located at the
True Elkin, Inc.
304 East Main Street, Elkin
Surry County
to receiving waters designated as the Yadkin River located within the Yadkin Pee -Dee River Basin in
accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, 11,
and 111 hereof.
This permit shall become effective January I, 2014.
This permit and authorization to discharge shall expire at midnight on December 31, 2018.
Signed this day December 5, 2013.
ORIGINAL SIGNED BY TOM BELNICK
Thomas A. Reeder, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Page I of 6

Permit NC0005312
SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDE,S Permits issued to this facility, whether for operation or discharge are hereby
revoked, and as of this issuance, any previously issued permit bearing this number is no longer
effective. Therefore, the exclusive authority to operate and discharge from this facility arises under
the permit conditions, requirements, terms, and provisions described herein.
True Elkin, Inc.
is hereby authorized to:
1. continue to operate an existing 4.0 MGD extended aeration system treating combined industrial
wastewater and contaminated groundwater, consisting of
• a manual bar screen, fine screening, pH adjustment using lime
• equalization basin,
• aeration basin
• dual clarifiers
• suspension of dissolved calcium hypochlorite
• post -chlorination aeration tank,
• aerobic digester, and sludge drying beds
located at True Elkin, Inc., 304 East Main Street, Elkin, Sung County, and
2. discharge from said treatment works at the location specified on the attached map into the
Yadkin River classified Class C waters in the Yadkin -Pee Dee River Basin.
Page 2 of 6

Permit NC0005312
PART
A (1). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
During the period beginning on the effective date of the permit and lasting until
expiration, the Permittee is authorized to discharge from Outfall 001. Such discharges
shall be limited and monitored by the Permittee as specified below:
EFFLUENT
CHARACTERISTICS
EFFLUENT LIMITS
MONITORING REQUIREMENTS
Monthly
Average
Weekly
Average
Daily
Maximum
Sample
Type
Sample
Locationl
Flow
4.0 MGD
Recording
I or E
BOD, 5 da , 20°C
101.6 Ibs/da
203.2 Ibs/daCom
NContinuous
osite
E
COD
1,526.5lbs/day
3,052.9lbs/dayComposite
E
Total Sus ended Solids
272.3 Ibs/da
5449 Ibs/daCom
osite
E
Sulfides
3.0 Ibs/da
6.1 Ibs/da
Grab
E
Phenols
1.5 lbs/day
3.0 Ibs/da
2 / Month
Grab
E
Chromium
1.5 lbs/day
3.0 Ibs/da
2 / Month
Composite
E
Fecal i
(geometric mean)
200 / 100 ml,
400 / 100 mL
2 / Month
Grab
E
Total Residual Chlorine
28 ie/L
Daily
Grab
E
H
> 6 and <9 SU
Daily
Grab
E
Temperature
Daily
Grab
E
Total Nitrogen (NOS +
No, +TKN)
Monthly
Composite
E
Total Phosphorus
Monthly
Composite
E
Chronic Toxicity
Quarterly
Composite
E
Footnotes:
1. Sample locations: I = Influent; E = Effluent
2. The facility shall report all efiluent'PRC values reported by a NC certified laboratory including field
certified. However, effluent values below 50 ug/I will be treated as zero for compliance purposes. The permittee
shall monitor for chlorine only if chlorine is used at the facility.
3. Chronic Toxicity (Ceriodaphnia) P/F at 1.9%; February, May, August, November; See Special Condition A.(2).
Discharge shall contain no floating solids or foam visible in other than trace amounts.
Page 3 of 6

Permit NC0005312
A. (2.) CHRONIC TOXICITY PEI2MIT LIMIT (QUARTERLY)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality
to Ceriodaphnia duhia at an effluent concentration of 1.9%.
The permit holder shall perform at a minimum, quarterly monitoring using test procedures outlined in the
North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised December 2010. or
subsequent versions or "North Carolina Phase 11 Chronic Whole Effluent Toxicity Test Procedure'
(Revised- December 2010) or subsequent versions. The tests will be performed February, May, August,
and November. These months signify the first month of each three month toxicity testing quarter
assigned to the facility. Effluent sampling for this testing must be obtained during representative effluent
discharge and shall be performed at the NPDES permitted final effluent discharge below all treatment
processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below
the permit limit, then multiple -concentration testing shall be performed at a minimum, in each of the
two following months as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test
Procedure" (Revised -December 2010) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP313
for the pass/fail results and THP3113 for the Chronic Value. Additionally, DWR Form AT-3 (original) is to
be sent to the following address:
Attention: North Carolina Division of Water Resources
Environmental Sciences Section
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later
than 30 days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate
signature. Total residual chlorine of the effluent toxicity sample must be measured and repotted if chlorine
is employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is
required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test
form indicating the facility name, permit number, pipe number, county, and the month/year of the report
with the notation of"No Flow" in the comment area of the form. The report shall be submitted to the
Environmental Sciences Section at the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring
will be required during the following month. Assessment of toxicity compliance is based on the toxicity
testing quarter, which is the three month time interval that begins on the first day of the month in which
toxicity testing is required by this permit and continues until the final day of the third month.
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Permit NC0005312
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of
Water Resources indicate potential impacts to the receiving stream, this permit may be re -opened and
modified to include alternate monitoring requirements or limits.
If the Permittee monitors any pollutant more frequently than required by this permit, the results of such
monitoring shall be included in the calculation & reporting of the data submitted on the DMR & all AT
Form submitted.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control
organism survival, minimum control organism reproduction, and appropriate environmental controls, shall
constitute an invalid test and will require immediate follow-up testing to be completed no later than the last
day of the month following the month of the initial monitoring.
A. (3.) ELECTRONIC REPORTING OF DISCHARGE MONITORING REPORTS
Proposed federal regulations require electronic submittal of all discharge monitoring reports (DMRs) and
specify that, if a state does not establish a system to receive such submittals, then permittees must submit
DMRs electronically to the Environmental Protection Agency (EPA). The Division anticipates that these
regulations will be adopted and is beginning implementation in late 2013.
NOTE: This special condition supplements or supersedes the following sections within Part 11 of this
permit (Standard Conditions for NPDES Permits):
• Section B. (11.) Signatory Requirements
• Section D. (2.)
• Section D. (6.)
• Section E. (5.)
Reporting
Records Retention
Monitoring Reports
1. Reportina [Supersedes Section D. (2.) and Section E. (5.)(a)]
Beginning no later than 90 days from the effective date of this permit, the permittee shall begin
reporting discharge monitoring data electronically using the NC DWR's Electronic Discharge
Monitoring Report (eDMR) internet application.
Monitoring results obtained during the previous month(s) shall be summarized for each month and
submitted electronically using eDMR. The eDMR system allows permitted facilities to enter
monitoring data and submit DMRs electronically using the internet. Until such time that the state's
eDMR application is compliant with EPA's Cross -Media Electronic Reporting Regulation
(CROMERR), permittees will be required to submit all discharge monitoring data to the state
electronically using eDMR and will be required to complete the eDMR submission by printing, signing,
and submitting one signed original and a copy of the computer printed eDMR to the following address:
NC DENR / DWR / Information Processing Unit
ATTENTION: Central Files / eDMR
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
If a permittee is unable to use the eDMR system due to a demonstrated hardship or due to the facility
being physically located in an area where less than 10 percent of the households have broadband access,
then a temporary waiver from the NPDES electronic reporting requirements may be granted and
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Permit NC0005312
discharge monitoring data may be submitted on paper DMR forms (MR I, 1.1, 2, 3) or alternative
forms approved by the Director. Duplicate signed copies shall be submitted to the mailing address
above.
Requests for temporary waivers from the NPDES electronic reporting requirements must be submitted
in writing to the Division for written approval at least sixty (60) days prior to the date the facility would
be required under this permit to begin using eDMR. Temporary waivers shall be valid for twelve (12)
months and shall thereupon expire. At such time, DMRs shall be submitted electronically to the
Division unless the permittee re -applies for and is granted a new temporary waiver by the Division.
Information on eDMR and application for a temporary waiver from the NPDES electronic reporting
requirements is found on the following web page:
http://poual. ncd_enr. oi:6/web/wq/adm_ i n/bog/i_pu/ednfr
Regardless of the submission method, the first DMR is due on the last day of the month following the
issuance of the permit or in the case of a new facility, on the last day of the month following the
commencement of discharge.
2. Signatory Requirements (Supplements Section B. (11.) (b) and supersedes Section B. (11.) (d)l
All eDMRs submitted to the permit issuing authority shall be signed by a person described in Part 11,
Section B. (1 1.)(a) or by a duly authorized representative of that person as described in Part 11, Section
B. (1 1.)(b). A person, and not a position, must be delegated signatory authority for eDMR reporting
purposes.
For eDMR submissions, the person signing and submitting the DMR must obtain an eDMR user
account and login credentials to access the eDMR system. For more information on North Carolina's
eDMR system, registering for eDMR and obtaining an eDMR user account, please visit the following
web page:
http://porta I. nedcnr.org/web/wq/ad m i n/bog/ipu/edm r
Certification. Any person submitting an electronic DMR using the state's eDMR system shall make the
following certification [40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL
BE ACCEPTED:
V certi� under penalty of law, that this docwnent and all attachments were prepared ender nny
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted Based on my inquhy ofthe person or persons
who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best ofrny knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations. "
3. Records Retention [Supplements Section D. (6.)]
The permittee shall retain records of all Discharge Monitoring Reports, including eDMR submissions. These
records or copies shall be maintained for a period of at least 3 years from the date of the report. This period
may be extended by request of the Director at any time [40 CFR 122.41 ].
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PART 11
STANDARD CONDITIONS FOR NPDES PERMITS
Section A. Definitions
2/Month
Samples are collected twice per month with at least ten calendar days between sampling events. These samples shall be
representative of the wastewater discharged during the sample period.
3/Week
Samples are collected three times per week on three separate calendar days. These samples shall be representative of
the wastewater discharged during the sample period.
Act or "the Act"
The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33 USC 1251, et.
seq.
Annual Average
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar year. In the case of fecal
coliform, the geometric mean of such discharges.
Arithmetic Mean
The summation of the individual values divided by the number of individual values.
Bypass
The known diversion of waste streams from any portion of treatment facility including the collection system, which is
not a designed or established or operating mode for the facility.
Calendar Day
The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any
consecutive 24-hour period that reasonably represents the calendar day may be used for sampling.
Calendar Week
The period from Sunday flrough the following Saturday.
Calendar Ouarler
Oneofthe following distinct periods: January through March, April through little, July through September, and
October through December.
Composite Sample
A sample collected over a 24-1101,11- period by continuous sampling or combining grab samples of at least 100 mL in
such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The
Director may designate the most appropriate method (specific number and size of aliquots necessary, the time interval
between grab samples, etc.) on a case -by -case basis. Samples may be collected manually or automatically. Composite
samples may be obtained by the following methods:
(1) Continuous: a single, continuous sample collected over a 24-hour period proportional to the rate of flow.
(2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24 hour period
of discharge and combined proportionate to the rate of flow measured at the tine of individual sample
collection, or
(3) Variable time/constant volume: a series ofgrab samples of equal volume collected over a 24 hour period with
the time intervals between samples determined by a preset number of gallons passing the sampling point. Flow
measurement between sample intervals shall be determined by use of a flow recorder and totalizer, and the
preset gallon interval between sample collection fixed at no greater than 1/24 of the expected total daily flow at
the treatment system, or
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(4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at a
constant time interval. Use of this method requires prior approval by the Director. This method may only be
used in situations where effluent flow rates vary less than 15 percent. The following restrictions also apply:
Influent and effluent grab samples shall be of equal size and of no less than 100 milliliters
Influent samples shall not be collected more than once per hour.
Pet mittees with wastewater treatment systems whose detention time < 24 horns shall collect effluent grab
samples at intervals of no greater than 20 minutes apart during any 24-hour period.
> Permittees with wastewater ueahnent systems whose detention time exceeds 24 hours shall collect effluent
grab samples at least every six hours; there must be a minimum of four samples during a 24-hour sampling
period.
Continuous flow measurement
Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be
monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance
activities on the Flow device.
Daily Discharge
The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the
calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is calculated as
the total mass of the pollutant discharged over the day. For pollutants expressed in other units of measurement, the
"daily discharge" is calculated as the average measurement of the pollutant over the day. (40 CFR 122.2; see also
"Composite Sample," above.)
Daily Maximum
The highest "daily discharge" during [lie calendar month.
Daily Sampling
Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the
permit. Sampling shall be conducted on weekdays except where holidays or other disruptions of normal operations
prevent weekday sampling. If sampling is required for all seven days of the week for any permit parameter(s), that
requirement will be so noted on the Effluent Limitations and Monitoring Page(s).
DWQ or "the Division'
The Division of Water Quality, Department of Environment and Natural Resources.
Effluent
Wastewater discharged following all treatment processes from a water pollution control facility or other point source
whether heated or untreated.
EMC
The North Carolina Environmental Management Commission
EPA
The United States Environmental Protection Agency
Facility Closure
Cessation of all activities that require coverage under this NPDES permit. Completion of facility closure will allow this
permit to be rescinded.
Geometric Mean
The Nth root of the product of the individual values where N = the number of individual values. For purposes of
calculating the geometric mean, values of "0" (or "< [detection level]") shall be considered = 1.
Grab Sample
Individual samples of at least 100 iuL collected over a period of time not exceeding 15 minutes. Grab samples can be
collected manually. Grab samples must be representative of the dischare (or the receiving stream, for instream
samples).
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Hazardous Substance
Any substance designated under 40 CPR Part 1 16 pursuant to Section 311 ofthe CWA.
Instantaneous flow measurement
The flow measured daring the minimum time required for the flow measuring device or method to produce a result in
that instance. To the extent practical, instantaneous flow measurements coincide with the collection of any grab
samples required for the same sampling period so that together the samples and flow are representative of the discharge
during that sampling period.
Monthly Average (concentration [unit)
The at mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of fecal
coliform or other bacteria( parameters or indicators, the geometric mean of such discharges.
Permit Issuing Authority
The Director ofthe Division of Water Quality.
Quarterly Average (concentration limit)
The arithmetic mean of all samples taken over a calendar quarter.
Severe property darnme
Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable, or
substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a
bypass. Severe property damage excludes economic toss caused by delays in production.
Toxic Pollutant:
Any pollutant listed as toxic under Section 307(a)(I I ofthe CWA.
Uuset
An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with
permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by
operational error, improperly designed treatment facilities, inadequate treatment facilities, lack of preventive
maintenance, or careless or improper operation.
Weekly Average (concentration limit)
The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar Nveek. In the case offecal
coliform or other bacterial parameters or indicators, the geometric mean of such discharges.
Section B. General Conditions
1. Duty to Como)y
The Permittee must comply with all conditions of this permit. Any permit noncompliance constinnes a violation of
the CWA and is grounds for enforcement action; for permit termination, revocation and reissuance, or
modification; or denial of a permit renewal application [40 CPR 122.41].
a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
CWA for toxic pollutants and with standards for sewage sludge use or disposal established under section
405(d) of the CWA within the time provided in the regulations that establish these standards or prohibitions or
standards for sewage sludge use or disposal, even if the permit has not yet been modified to incorporate the
requirement.
b. The CWA provides that any person who violates section[s] 301, 302, 306, 307, 308, 318 or 405 of the Act, of
any permit condition or limitation implementing any such sections`in a permit issued under section 402, or any
requirement imposed in a pretreaument program approved under sections 402(a)(3) or 402(b)(8) of the Act, is
subject to a civil penalty not to exceed DT500 per day for each violation. [33 USC 1319(d) and 40 CPR
122.41(a)(2)]
c. The CWA provides that any person who negligently violates sections 301, 302, 306, 30T 308, 318, or 405 of
the Act, or any condition or limitation implementing any of such sections in a permit issued under section 402
of the Act, or any requirement imposed in a pretreatment program approved under section 402(a)(3) or
402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
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imprisonment of not more than I year, or both. In the case of a second or subsequent conviction for a negligent
violation, a person shall be subject to criminal penalties of not more than $5 AO per day of violation, or by
imprisonment of not more than 2 years, or both. 133 USC to 19(c)(1) and 40 CFR 122.41(a)(2)]
d. Any person who knowingly violates such sections, or such conditions or limitations is subject to criminal
penalties of $5,000 to $50.000 per day of violation, or imprisonment for not more than 3 years, or both. fit the
case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal
penalties of not more than S 100,000 per day of violation, or imprisonment of not more than 6 years, or both.
[33 USC 1319(c)(2) and 40 CPR 122.41(a)(2)]
e. Any person who know ingh- violates section 301, 301303, 306, 307, 308, 318 or 405 of the Act, or any permit
condition or limitation implementing any of such sections in a permit issued under section 402 of the Act, and
who knows at that time that he thereby places another person in imminent danger of death or serious bodily
injury, shall, upon conviction, be subject to a fine of not more than $250,000 or imprisonment of not more than
15 ),eats, m both. In (lie case of a second or subsequent conviction for a knowing endangerment violation, a
person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than 30 years, or
both. An organization, as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon conviction of violating
the imminent danger provision, be subject to a fine of not more than $1,000,000 and can be fined up to
$2,000,000 for second or subsequent convictions. [40 CFR 122.4l (a)(2)]
f. Under state law, a civil penalty of not more than 525,000 per violation may be assessed against any person
who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North
Carolina General Statutes § 143-215.6A]
g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302,
306, 307, 308, 318 or 405 of this Act, or any pennit condition or limitation implementing any of such sections
in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are not to
exceed S 16,000 per violation, with the maximum amount of any Class I penalty assessed not to exceed
537,500. Penalties for Class 11 violations are not to exceed $16,000 per day for each day during which the
violation continues, with the maximum amount of any Class II penalty not to exceed $177,500, 133 USC
1319(g)(2) and 40 CPR 122.41(a)(3)]
2. Duty to Miti =ate
The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permit with a reasonable likelihood of adversely affecting human health or the environment [40
CFR 122.41(d)].
3. Civil and Criminal Liability
Except as provided in permit conditions on 'Bypassing" (Part ILCA), "Upsets" (Part ILC.5) and "Power Failures"
(Part ILC.7), nothing in this permit shall be construed to relieve the Permittee from any responsibilities, liabilities,
or penalties for noncompliance pursuant to NCGS 143-215.3. 143-215.6 or Section 309 of the Federal Act, 33 USC
1319. Furthermore, the Permittee is responsible for consequential damages, such as fish kills, even though the
responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Substance Liability
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee
from any responsibilities, liabilities, or penalties to which the Pcrmittee is or may be subject to under NCGS 143-
215.75 et seq. or Section 31 1 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Property Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any exclusive
privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor any
infringement of Federal, State or local laws or regulations [40 CFR 122.41(g)].
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical Stuctures or
facilities or the undertaking of any work in any navigable waters.
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7. Severability
The provisions of this permit are severable. If any provision of this permit, or the application of any provision of
this permit to any circumstances, is held invalid, the application of such provision to other circumstances and the
remainder of this permit, shall not be affected thereby [NCGS 150Q-23].
8. Duty to Provide Information
The Pennittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which the
Permit Issuing Authority may request to determine whether cause exists for modifying, revoking and reissuing, or
terminating this permit or to determine compliance with this permit. The Pennittee shall also furnish to the Permit
Issuing Authority upon request, copies of records required by this permit [40 CFR 122.41(h)].
9. Duty to Reapply
If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit, the
Permittee must apply for and obtain a new permit [40 CPR 122.41(b)],
10. Expiration of Permit
Fhe Permittee is not authorized to discharge after the expiration date. In ordet to receive automatic authorization to
discharge beyond the expiration date, the Permittee shall submit such information, forms and fees as are required
by the agency authorized to issue permits no later than 180 days prior to the expiration date unless permission for a
later date has been granted by the Director. (The Director shall not grant permission for applications to be
submitted later than the expiration date of the existing permit.) [40 CFR 122.21(d)] Any Permittee that has not
requested renewal at least 180 days prior to expiration, or any Permittee that does not have a permit after the
expiration and has not requested renewal at least 180 days prior to expiration, will subject the Permittee to
enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
1 1. S�gnsitory 12equirements
All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified [40
CPR 122A1(k)].
a. All permit applications shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in charge
of a principal business function, or any other person who performs similar policy or decision making
functions for the corporation, or (b) the manager of one or more manufacturing, production, or operating
facilities, provided, the manager is authorized to make management decisions which govern the operation
of the regulated facility including having the explicit or implicit duty of making major capital investment
reconnnendations, and initiating and directing other comprehensive measures to assure long term
environmental compliance with environmental laws and regulations; the manager can ensure that the
necessary systems are established or actions taken to gather complete and accurate information for permit
application requirements; and where authority to sign documents has been assigned or delegated to the
managerin accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or
ranking elected official [40 CFR 122.22].
b. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described in paragraph a. above or by a duly authorized representative of that person. A
person is a duly authorized representative only if.
(1) The authorization is made in writing by it person described above;
(2) The authorization specified either an individual or a position having responsibility for the overall operation
of the regulated facility or activity, such as the position of plant manager, operator of a well of well field,
superintendent, a position of equivalent responsibility, or an individual or position having overall
responsibility for environmental matters for the company. (A duly authorized representative may thus be
either a named individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Permit Issuing Authority [40 CPR 122.221
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c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate because
a different individual or position has responsibility for the overall operation of the facility, a new authorization
satisfying the requirements of paragraph (b) of this section must be submitted to the Director prior too]
together with any reports, information, or applications to be signed by an authorized representative 140 CPR
122.22]
d. Certification. Any person signing a document uncle[ paragraphs a. or b. of this section shall make the following
certification 140 CPR 122,221. NO OTHER STATEMENTS OF CERTIFICATION WILL BE ACCEPTED:
V cert f,, under penulty of law, that this document and ull attachments were prepared under my direction or
supervision in accordance Ivith a system designed to assure that qualified personnel properly gather and
evaluate the informatiaa submitted. Ru,sed on m3+ inquif y of the person or persons who manage the system, or
those persons directly responsible far gathering the information, the information submitted is, to the hest ofnry
knowledge and belie( true, accurate, and complete. I ane aware that there are significant penaltiesJor
submitting false information, including the possibililY offiiees and imprisonment for knowing violations."
12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned changes
or anticipated noncompliance does not stay any permit condition 140 CPR 122.41(0].
13. Permit Modification. Revocation and Reissuance, or Termination
The issuance of this permit does not prohibit the permit issuing authority fiom reopening and modifying the permit,
revolving and reissuing the permit, or terminating the permit as allowed by the laws, rules, and regulations
contained in Title 40, Code of Federal Regulations, Parts 122 and 123: Title 15A of the North Carolina
Administrative Code, Subchapter 02H .0100: and North Carolina General Statute 143.215.1 et. al.
14. Annual Administering and Compliance Monitoring Pee Requirements
The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being
billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 02H .0105(b)(2)
may cause this Division to initiate action to revoke the permit.
Section C. Operation and Maintenance of Pollution Controls
I. Certified Operator
Owners of classified water pollution control systems must designate operators, certified by the Water Pollution
Control System Operators Certification Commission (WPCSOCC), of the appropriate type and grade for the
system, and, for each classification must IT15A NCAC 08G 0201 ]:
a, designate one Operator In Responsible Charge (ORC) who possesses a valid certificate of the type and grade at
least equivalent to the type and grade of the system;
b. designate one or more Back-up Operator(s) in Responsible Charge (Back -tip ORCs) who possesses a valid
certificate of the type of the system and no more than one grade less than the grade of the system, with the
exception of no backup operator in responsible charge is required for systems whose minimum visitation
requirements are twice per year; and
C. submit a signed completed "Water Pollution Control System Operator Designation Form" to the Commission
(or to the local health department for owners of subsurface systems) countersigned by the designated certified
operators, designating the Operator in Responsible Charge (ORC) and the Back-up Operator in Responsible
Charge (Back-up ORC):
(1) 60 calendar days prior to wastewater or residuals being introduced into a new system; or
(2) within 120 calendar days following:
receiving notification of a change in the classification of the system requiring the designation of a new
Operator in Responsible Charge (ORC) and Back-up Operator in Responsible Charge (Back-up ORC)
of the proper type and grade; or
a vacancy in the position of Operator in Responsible Charge (ORC) or Back-up Operator in
Responsible Charge (Back-up ORC).
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(3) within seven calendar days of vacancies in both ORC and Back-up ORC positions replacing or designating
at least one of the responsibilities.
The ORC of each Class t facility for the Back -tip ORC, when acting as surrogate For the ORC) must:
Y Visit the facility as often as is necessary to insure proper operation of the treatment system; the ueatment
facility must be visited at least weekly
> Comply with all other conditions of I5A NCAC 08G .0204.
The ORC of each Class 11, ill and IV facility for the Back-up ORC, when acting as surrogate for the ORC) must:
Visit the facility as often as is necessary to insure proper operation of the treatment system; the treatment
facility must be visited at least Five days per week, excluding holidays
Y Properly manage and document daily operation and maintenance of dnc facility
➢ Comply with all other conditions of 15A NCAC 08G .0204.
2. Piooer Operation and Maintenance
The Permittee shall at all times properly operate and maintain all facilities and systems of ueaunent and control
(and related appurtenances) which are installed or used by the Permittee to achieve compliance with the conditions
of this permit Proper operation and maintenance also includes adequate laboratory controls and appropriate quality
assurance procedures. This provision requires the Permittee to install and operate backup or auxiliary facilities only
when necessary to achieve compliance with the conditions of the permit [40 CPR 122.41(e)].
NOTE: Properly and officially designated operators ate fully responsible for all proper operation and maintenance
of the facility, and all documentation required thereof, whether acting as a contract operator [subcontractor] of a
member of the Permittee's staff.
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a Pennittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of -this permit [40 CPR 122.41(c)].
4. �passin of Treatment facilities
a. Bypass not exceeding limitations [40 CPR 122.41(m)(2)]
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but
only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the
provisions of Paragraphs b. and c. of this section.
b. Notice [40 CFR 122.41(m)(3)]
(1) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior notice,
if possible at least ten days before the date of the bypass; including an evaluation of the anticipated quality
and effect of the bypass.
(2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in Part
ILEA (24-hour notice).
c. Prohibition of Bypass
(I) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for bypass, unless:
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities,
retention of untreated wastes or maintenance dining normal periods of equipment downtime. This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance; and
(C) The Permittee submitted notices as required under Paragraph b. of this section.
(2) Bypass fronn the collection system is prohibited and the Permit Issuing Authority may take enforcement
action against a Permittee for a bypass as provided in any current or future system -wide collection system
permit associated with the treatment facility.
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(3) "fhe Permit Issuing Authority may approve an anticipated bypass, after considering its adverse effects, if
the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph C.
( I ) of this section.
5. Upsets
a. Effect of an upset [40 CFR 122.4 1 (n)(2)]: An upset constitutes an affirmative defense to an action brought for
noncompliance with such technology based permit effluent limitations if the requirements of paragraph b. of
this condition are met No determination made during administrative review ofelaims that noncompliance was
caused by upset, and before an action for noncompliance, is final administrative action subject tojudicial
review.
b. Conditions necessary for a demonstration of upset: Any Permittee who wishes to establish the affirmative
defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or other relevant
evidence that:
(I ) An upset occurred and that the Permittee can identify the cause(s) of the upset;
(2) The Permiaec facility was at the time being properly operated; and
(3) The Permittee submitted notice of the upset as required in Part II.E.6.(b) of [his permit.
(4) The Permittee complied with any remedial measures required under Part II.t3.2. of this permit.
c. Burden of proof [40 CPR 122.4 1 (n)(4)]: The Permittee seeking to establish the occurrence of an upset has
the burden of proof in any enforcement proceeding.
6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials fi'om entering waters of the State or navigable waters of the United States except as permitted
by the Commission. The Permittee shall comply with all applicable state and Federal regulations governing the
disposal of sewage sludge, including 40 CFR 503, Standards for the Usc and Disposal of Sewage Sludge; 40 CFR
Part 258, Criteria For Municipal Solid Waste Landfills; and I SA NCAC Subchapter 2T, Waste Not Discharged To
Surface Waters. The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use
or disposal practices.
7. Power Failures
The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 02H .0124) to
prevent the discharge of untreated or inadequately treated wastes during electrical power failures either by means
of alternate power sources, standby generators or retention of inadequately heated effluent.
Section D. Monitoring and Records
I. Representative Sampling
Samples collected and measurements taken, as required herein, shall be representative of the permitted discharge.
Samples collected at a frequency less than daily shall be taken on a day and time that is representative of the
discharge for the period the sample represents. All samples shall be taken at the monitoring points specified in this
permit and, unless otherwise specified, before the effluentjoins or is diluted by any other wastestream, body of
water, or substance. Monitoring points shall not be changed without notification to and the approval of the Permit
Issuing Authority [40 CFR 122.41(j)].
2. Reporting
Monitoring results obtained during the previous month(s) shall be summarized for each month and reported on a
monthly Discharge Monitoring Report (DMR) Form (MR 1, 1,1, 1 3) or alternative forms approved by the
Director, postmarked no later than the last calendar day of the month following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of these,
and all other reports required herein, shall be submitted to the following address:
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NC DENR / Division of Water Quality / Surface Water Protection Section
ATTENTION: TENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
3. Flow Measurements
Appropriate flow ineasurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The
devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements is consistent
with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10% front the true discharge rates throughout the range of expected discharge
volumes. Plow measurement devices shall be accurately calibrated at a minimum o'once per year and maintained
to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device.
The Director shall approve the flow measurement device and monitoring location prior to installation.
Once -through condenser cooling water flow monitored by pump logs, or pump hour meters as specified in Part I of
this permit and based on the manufacturer's pump curves shall not be subject to this requirement.
4. Test Procedures
Laboratories used for sample analysis must be certified by the Division. Permittees should contact Pile Division's
Laboratory Certification Section (919 733-3908 or http://portal.ncdenr.oig/web/wq/lab/cent) for information
regarding laboratory certifications.
Facilities whose personnel are conducting testing of field -certified parameters only nmst hold the appropriate field
parameter laboratory certifications.
Test procedures for the analysis ofpollutauts shall conform to the EMC regulations (published pursuant to NCGS
143-215.63 et. sect.), the Water and Air Quality Reporting Acts, and to regulations published pursuant to Section
304(g), 33 USC 1314, of the CWA (as amended), and 40 CPR 136; or in the case of sludge use or disposal,
approved Under 40 CPR 136, unless otherwise specified in 40 CFR 503, unless other test procedures have been
specified in this permit [40 CPR 122.41].
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum detection
and reporting levels that are below the permit discharge requirements and all data generated must be reported down
to the minimum detection or lower reporting level of the procedure. If no approved methods are determined
capable of achieving minimum detection and reporting levels below permit discharge requirements, then the most
sensitive (method with the lowest possible detection and reporting level) approved method must be used.
5. Penalties for Tanmerin<u
The CWA provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any motntorltlg
device or method required to be maintained under this permit shall, upon conviction, be punished by a fine of not
more than $10,000 per violation, or by imprisonment for not more than two years per violation, or by both. If a
conviction of a person is for a violation committed after a first conviction of such person under this paragraph,
pwlishnleut is a fine of not more than $20,000 per day of violation, or by imprisonment of not more than 4 years,
or both [40 CFR 122.41 ].
6. Records Retention
Except for records of monitoring information required by this pennit related to the Permittee's sewage sludge use
and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40 CFR
503), the Pernlittee shall retain records of all monitoring information, including:
➢ all calibration and maintenance records
i all original ship chart recordings for continuous monitoring instrumentation
copies of all reports required by this permit
copies of all data used to complete the application forthis permit
These records or copies shall be maintained for a period of at least 3 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time [40 CFR
122.411.
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7. Recordin, Results
For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shall record the
following information 140 CFR 122.4 1]:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses:
e. The analytical techniques or methods used: and
f. The results of such analyses.
8. Inspection and Envy
'Pile Permittee shall allow the Director, or an authorized representative (including an authorized contractor acting as
a representative of the Director), upon the presentation of credentials and other documents as may be required by
law, to;
a. Enter, at reasonable times, upon the Permittee's premises where a regulated facility or activity is located or
conducted, or where records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices,
or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the CWA, any substances or parameters at any location [40 CFR I22.41(i)].
Section E Reportintr Requirements
I. Chaneein Discharge
All discharges authorized herein shall be consistent with the terms and conditions of this permit. The discharge of
any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall constitute
a violation of the permit.
2. Planned Chanizes
The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or additions
to the permitted facility 140 CFR 122.41(1)]. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CPR
122.29(b); or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants subject neither to effluent limitations in the permit, nor to
notification requirements under 40 CFR 122.42(a)(I ); or
c. The alteration or addition results in a significant change in the Penuittee's sludge use or disposal practices, and
such alteration, addition or change may justify the application of permit conditions that are different from or
absent in the existing permit, including notification of additional use or disposal sites not reported during the
Permit application process or not reported pursuant to an approved land application plan.
3. Anticipated Noncompliance
The Pei mittee shall give advance notice to the Director of any planned changes to the permitted facility or other
activities that might result in noncompliance with the permit [40 CFR 122.4l (I)(2)].
4. Transfers
This permit is not transferable to any person without prior written notice to and approval from the Director in
accordance with 40 CFR 122.61. The Director may condition approval in accordance with NCGS 143-215.1, in
Particular NCGS 143-215.1(b)(4)b2., and may require modification or revocation and reissuance of tile permit, or
a minor modification, to identify the new permittee and incorporate sucl6 other requirements as may be necessary
under the CWA [40 CFR 122.41(])(3), 122.6 1] or state statute.
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5. Monitoring Reports
Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.41(I)(4)].
a. Monitoring results nmst be reported on a Discharge Monitoring Report (DMR) (See Part It.D.2) or forms
provided by the Director for reporting results of monitoring of sludge use or disposal practices.
b. If the Permittee monitors any pollutant more frequently than required by this permit using test procedures
approved under 40 CFR Part 136 and at a sampling location specified in this permit or other appropriate
instrument governing the discharge, the results of such monitoring shall be included in the calculation and
reporting of the data submitted on the DMR.
6. Twenty-four Hour Reporting
a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that
potentially threatens public health or the environment. Any information shall be provided orally within 24
hours from the time the Permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time (he Permittee becomes aware of the circumstances. The written submission
shall contain a description ofthe noncompliance, and its cause; the period of noncompliance, including exact
dates and times, and if the noncompliance has not been corrected, the anticipated time it is expected to
continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the noncompliance 140
CFR 122.41(1)(6)].
b. The Director may waive the written report on a case -by -case basis for reports under this section if the oral
report has been received within 24 hours.
c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response
personnel at [phone], [phone] or [phone].
7. Other Noncompliance
The Permittee shall report all instances of noncompliance not reported under Part II.E.5 and 6. of this permit at the
time monitoring reports are submitted. The reports shall contain the information listed in Part II.E.6. of this permit
[40CFR 122.41(1)(7)1,
8. Other Information
Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or submitted
incorrect information in a pennit application or in any report to the Director, it shall promptly submit such facts or
information [40 CPR 122.4 1 (1)(8)].
9. Noncompliance Notification
The Permittee shall report by telephone to either the central office or the appropriate regional office of the Division
as soon as possible, but in no case more than 24 hours o' on the next working day following the occurrence or fast
knowledge of the occurrence of any of the following:
a. Any occurrence at the water pollution control facility which results in the discharge ofsignificant amounts of
wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge
digester; the known passage of a slug of hazardous substance through the facility; o any other unusual
ci[cumstances.
b. Any process unit failure, due to known o unknown reasons, that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps, aerators, compressors, etc.
c. Any failure of a pumping station, sewer line, or Treatment facility resulting in a by-pass without treatment of all
or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report within 5 days following first
knowledge Of the occurrence. Also see reporting requirements for municipalities in ]'art IV.C.2.c. of this permit.
10. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33
USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division. As required by the Act, effluent data shall not be considered confidential. Knowingly making any
false statement on any such report may result in the imposition of criminal penalties as provided for in NCGS 143-
215.1(b)(2) or in Section 309 of the Federal Act.
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11, Penalties for Falsification of Reports
The CWA provides that any person who knowingly makes any false statement, representation, or certification in
any record or other document submitted or required to be maintained under this permit, including monitoring
reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of not more than
$25,000 per violation, or by imprisonnnent for not more than two years per violation, or by both [40 CFR 122.41 ].
12. Annual Performance Reports
Pet mittees who own or operate facilities that collect or it municipal or domestic waste shall provide an annual
report to the Permit Issuing Authority and to the users/customers served by the Permittee (NC:GS 143-215.1C). The
report shall summarize the performance of the collection or treatment system, as well as the extent to which the
facility was compliant with applicable Federal or State laws, regulations and rules pertaining to water quality. The
report shall be provided no later than sixty days after the end of the calendar or fiscal year, depending upon which
anmral period is used for evaluation.
The report shall be sent to:
NC DENR / Division of Water Quality / Surface Water Protection Section
ATTEN"PION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
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PART III
OTHER REQUIREMENTS
Section A. Construction
a. The Permittee shall not commence construction of wastewater treatment facilities, nor add to the plant's treatment
capacity, nor change the treatment process(es) utilized at the treatment plant unless (1) the Division has issued an
Authorization to Construct (AtC) permit or (2) the Permittee is exempted from such AtC permit requirements
under Item b. of this Section.
b. In accordance with NCGS 143-215.1(a5) [SL 201 1-394], no permit shall be required to enter into a contract for the
constuction, installation, or alteration of any treatment work or disposal system or to construct, install, or alter any
treatment works or disposal system within the State when the system's or work's principle function is to conduct,
treat, equalize, neutralize, stabilize, recycle, or dispose of industrial waste or sewage from an industrial facility and
the discharge of the industrial waste or sewage is authorized under a permit issued for the discharge of the
ndustrial waste or sewage into the waters of the State. Notwithstanding the above, the permit issued for the
discharge may be modified if required by federal regulation.
C. Issuance of an AtC will not occur until Final Plans and Specifications for the proposed construction have been
submitted by the Permittee and approved by the Division.
Section B. Groundwater Monitoring
The Permittee shall, upon written notice from lie Director, conduct groundwater monitoring as may be required to
determine the compliance of this NPDFS pennitted facility with the current groundwater standards.
Section C. Changes in Discharges of Toxic Substances
The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CPR 122.42):
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent basis, of
any toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the following
"notification levels";
(I ) One hundred micrograms per liter (100 µg/L);
(2) Two hundred micrograms per liter (200 µg/L) for acrolein and acrylonitrile; five hundred micrograms per liter
(500 µg/L) for 2,4-dinitrophenol and fort-methyl-4,6-dinitrophenol; and one milligram per liter (I mg/L.) for
antimony;
(3) Five times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine or infrequent
basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the
following "notification levels",
(1) Five hundred micrograms per liter(500
(2) One milligram per liter (I mg/L) for antimony;
(3) Ten times the maximum concentration value reported for that pollutant in the permit application.
Section D. Facility Closure Requirements
The Permittee must notify the Division at least 90 days prior to the closure of at)) wastewater treatment system covered
by this permit. The Division may require specific measures during deactivation of the system to prevent adverse
impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit continue at the
pennitted facility.
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PART IV
SPECIAL CONDITIONS FOR MUNICIPAL FACILITIES
Section A. Definitions
In addition to the definitions in Part 11 of this permit, the following definitions apply to municipal facilities:
Indirect Discharge or Industrial User
Any non -domestic source that discharges wastewater containing pollutants into a POTW regulated under section
307(b), (c) or (d) of the CWA. [40 CFR 403.3 (i) and (j) and 15A NCAC 0214 .0903(1b)(1 1)]
Interference
Inhibition or disruption of the POTW treatment processes; operations; or its sludge process, use, or disposal which
causes or contributes to a violation of any requirement of the Permittee's (or any satellite POTW's if different from the
Permittee) NPDFS, collection system, or non -discharge permit or prevents sewage sludge use or disposal in
compliance with specified' applicable State and Federal statutes, regulations, or permits. [ I5A NCAC 0211
.0903 (b)(14)]
Pass Through
A discharge which exits the POTW into waters of the State in quantities or concentrations which, alone or with
discharges from other sources, causes a violation, including an increase in the magnitude or duration of a violation, of
the Permittee's (or any satellite POTW's, if different from the Permittee) NPDFS, collection system, or non -discharge
permit. [I5A NCAC 02I1 .0903(b)(23)]
Publicly Owned Treatment Works (POTW)
A treatment works as defined by Section 212 of the CWA, which is owned by a State or local government organization.
This definition includes any devices and systems used in the storage, treatment, recycling and reclamation of municipal
sewage or industrial wastes of a liquid nature. It also includes the collection system, as defined in 15A NCAC 2T
0402, only if it conveys wastewater to a POTW treatment plant. The term also means the local government
organization, or municipality, as defined in section 502(4) of the CWA, which hasjurisdiction over indirect discharges
to and the discharges fi om such a treatment works. In this context, the organization may be the owner of the POTW
treatment plant or the owner of the collection system into which all indirect discharger discharges. This second type of
POTW may be referred to as a "satellite PO'I'W organization." [15A NCAC 0211 .0903(b)(26)]
"Significant Industrial User" or "SIU"
An Industrial User that discharges wastewater into a publicly owned treatment works and that [I5A NCAC 0211
0903 (b)(33 )] :
I . Discharges an average of 25,000 gallons per day or more of process wastewater to the POTW (excluding sanitary,
❑oncontact cooling and hoiler blowdown wastewaters); or
2. Contributes process wastewater which makes up five percent or more of the NPDES or non -discharge permitted
flow limit or organic capacity of the POTW treatment plant. In this context, organic capacity refers to BOD. TSS
and ammonia; or
3. Is subject to categorical standards under 40 CFR Part 403.6 and 40 CFR Parts 405-471: or
4. Is designated as such by the Permittee on the basis that the Industrial User has a reasonable potential for adversely
affecting the PO"I'W's operation or for violating any pretreatment standard or requirement, or the POTW's effluent
limitations and conditions in its NPDES or non -discharge permit, or to linnit the POTW's sludge disposal options;
5. Subject to approval under I5A NCAC 0211 .0907(b), the Permittee may determine that an Industrial User meeting
the criteria in paragraphs I or 2 of this definition above has no reasonable potential for adversely affecting the
POTW's operation or for violating any pretreatment standard or requirenent, the PO'FW's effluent limitations and
conditions in its NPDES or non -discharge permit, or to limit the POTW's sludge disposal options, and thus is not a
Significant Industrial User (SIU); or
6. Subject to approval under I5A NCAC 02H .0907(b), the Permittee may determine that an Industrial User meeting
the criteria in paragraph 3 of this definition above meets the requirements of 40 CFR Part 403.3(v)(2) and thus is a
non -significant categorical Industrial User.
Section B. Publicly Owned Treatment Works (POTWs)
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All POTWs must provide adequate notice to the Director of the following [40 CPR 122.42(b)]:
I. Any new introduction of pollutants into the POTW from all indirect discharger, regardless of the means of
transport, which would be subject to section 301 or 306 of CWA if it were directly discharging those pollutants;
and
2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger as
influent to that POTW at the time of issuance of the permit
3. For purposes of this paragraph, adequate notice shall include information on (1) the quality and quantity of effluent
introduced into the POTW, and (2) any anticipated impact that may result fi-om the change of the quantity or
quality of effluent to be discharged from the POTW.
Section C. Municipal Control of Pollutants from Industrial Users.
1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs fiont Industrial Users
discharging to the POTW may be present in the Permittee's discharge. At such time as sufficient information
becomes available to establish limitations for such pollutants, this permit may be revised to specify effluent
limitations for any or all of such other pollutants in accordance with best practicable technology or water quality
standards.
2. Prohibited Discharges
a. The Pei
mittee shall develop and enforce their Pretreatment Program to implement the prohibition against the
introduction of pollutants or discharges into the waste treatment system or waste collection system which
cause or contribute to Pass Through or Interference as defined in 15A NCAC 02H .0900 and 40 CPR 403. [40
CFR 403.5(a)(I)]
b. The Pennittee shall develop and enforce their Pretreatment Program to implement the prohibitions against the
introduction of the following wastes in the waste treatment or waste collection system [40 CFR 403.5(b)]:
(1) Pollutants which create a fire or explosion hazard in the POTW, including, but not limited to,
wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees Centigrade
using the test methods specified in 40 CFR 261.21;
(2) Pollutants which cause corrosive structural damage to the POTW, but in no case discharges with pH lower
than 5.0, unless the works is specifically designed to accommodate such discharges;
(3) Solid or viscous pollutants in amounts which cause obstruction to the flow in the POTW resulting in
Interference;
(4) Any pollutant, including oxygen demanding pollutants (BOD, etc.) released in a Discharge at a flow rate
and/or pollutant concentration which will cause Interference with the POTW;
(5) Heat in amounts which will inhibit biological activity in the POTW resulting in Interference, but in no
case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C (104°F)
unless the Division, upon request of the PO"rW, approves alternate temperature limits;
(6) Petroleum oil, non -biodegradable cutting oil, or products of mineral oil origin in amounts that will cause
Interference or Pass Through;
(7) Pollutants which result in the presence of toxic gases, vapors, or fines within the POTW in a quantity that
may cause acute worker health and safety problems; or
(8) Any trucked or battled pollutants, except at discharge points designated by the POTW.
e. The Permittee shall investigate the source of all discharges into the POTW, including slug loads and other
unusual discharges, which leave the potential to adversely impact the Pennittee's Pretreatment Program and/or
the operation of the POTW.
The Permittee shall report such discharges into the POTW to the Director or the appropriate Regional Office.
Any information shall be provided orally within 24 hours from the tittle the Pennittee became aware of the
circumstances. A written submission shall also be provided within 5 days of the time the Pennittee becomes
aware of the circumstances. The written submission shall contain a description of the discharge; the
investigation into possible sources; the period of the discharge, including exact dates and times; if the
discharge has not ceased, the anticipated tone it is expected to continue; and steps taken or planned to reduce,
eliminate, and prevent reoccurrence of the noncompliance,
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3. With regard to the effluent requirements listed in Pail I of this permit, it may be necessary for the Permittee to
supplement the requirements of the Federal Pretreatment Standards (40 CPR, Part 403) to ensure compliance by
the Permittee with all applicable effluent limitations. Such actions by the Permittee may be necessary regarding -
scale or all of the industries discharging to the municipal system.
4. The Permittee shall require any Industrial User (IU) discharging to the POTW to meet Federal Pretreatment
Standards developed under Section 307(b) of the Act as amended (which includes categorical standards and
specific local limits, best management practices and narrative requirements). Prior to accepting wastewater from
any Significant Industrial User (S1U), the Permittee shall either develop and submit to the Division a new
Pretreatment Program or, as necessary, a modification of an existing Pretreatment Program, for approval as
required Under section D below as well as I5A NCAC 02H .0907(a) and (b). [40 CFR 122.440)(2)]
5. This permit shall be modified, or alternatively, revolved and reissued, to incorporate or modify an approved POTW
Pretreatment Program or to include a compliance schedule for the development of a POTW Pretreatment Program
as required under Section 402 (b)(8) of the CWA and implementing regulations or by tine requirements of the
approved State pretreatment program, as appropriate.
Section D. Pretreatment Programs
Under authority of sections 307 (b) and (c) and 402(b)(8) of the CWA and implementing regulations 40 CFR 403,
North Carolina General Statute 143-215.3(14) and implementing regulations 15A NCAC 02H .0900, and in accordance
with the approved pretreatment program, all provisions and regulations contained and referenced in the pretreatment
program submittal are an enforceable par[ of this permit. [40 CFR 122.440)(2)]
The Pernittee shall operate its approved pretreatment program in accordance with Section 402(b)(8) of the CWA, 40
CFR 403, 15A NCAC 0211 .0900, and the legal authorities, policies, procedures, and financial provisions contained in
its pretreatment program submission and Division approved modifications thereof. Such operation shall include but is
not limited to the implementation of the following conditions and requirements. Terms not defined in Part 11 or Part IV
of this permit are as defined in 15A NCAC 0211 .0903 and 40 CFR 4033.
I . Sewer Use Ordinance (SUO)
The Permittee shall maintain adequate legal authority to implement its approved pretreatment program. [ 15A
NCAC 0211 .0903(b)(32), .0905 and .0906(b)(1); 40 CPR 403.8(0(1) and 403.9(b)(I ) and (2)]
2. Indus0ialWaste Sol ve (IWS)
The Permittee shall implement an IWS consisting of the survey of users of the POTW collection system or
treatment plant, as required by 40 CFR 403.8(0(2)(i-iii) and 15A NCAC 0211 .0905 [also 40 CFR 122.440)(1)],
including identification of all Industrial Users that may have an impact on the POTW and the character and announl
of pollutants contributed to the POTW by these Industrial Users and identification of those Industrial Users
meeting the definition of SIU. Where the Permittee accepts wastewater from one or more satellite POTWs, tine
IWS for the Permittee shall address all satellite POTW services areas, unless the pretreatnnent program in those
satellite service areas is administered by a separate Permittee with an approved Pretreatment Program. The
Permittee shall submit a summlary of its IWS activities to the Division at least once every five years, and as
required by the Division. ']'be IWS submission shall include a summary of any investigations conducted under
paragraph C.2.c. of this Part. [ 15A NCAC 0211 .0903(b)(13), .0905 and .0906(b)(2); 40 CFR 403.8(f)(2) and 403.9]
3. Monitoring Plan
The Permittee shall implement a Division -approved Monitoring Plan for the collection of facility specific data to
be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of specific preteatnent
local limits. Effluent data from the Plan shall be reported on the DMRs (as required by Parts ILD and II.E.S.). [15A
NCAC 02H .0903(b)(16), .0906(b)(3) and .0905]
4. Headworks Analysis (HWA) and Local Limits
The Permittee shall obtain Division approval of a HWA at least once every five years, and as required by the
Division. Within 180 days of the effective date of this permit (or any subsequent permit modification) the
Permittee shall submit to the Division a written technical evaluation of the need to revise local limits (i.e., an
updated HWA or documentation of why one is not needed) [40 CFR 122,44]. The Permittee shall develop, in
accordance with 40 CFR 403.5(c) and 15A NCAC 0211 .0909, specific Local Limits to implement the prohibitions
listed in 40 CPR 403.5(1) and (b) and 15A NCAC 02H .0909. Pursuant to 40 CFR 403.5, local limits are
Version 1110912011

NPDES Permit Standard Conditions
Page 17 of 18
enforceable Pretreatment Standards as defined by 40 CFR 403.3(1). 115A NCAC 02H .0903(b)(10), .0905, and
.0906(b)(4)]
S. Industrial User Pretreatment Permits IU( P) & Allocation Tables
In accordance with NCGS 143-215.1, the Permittee shall issue to all Significant Industrial Users, permits for
operation of pretreatment equipment and discharge to the Permittee's collection system or treatment works. These
permits shall contain limitations, sampling protocols, reporting requirements, appropriate standard and special
conditions, and compliance schedules as necessary for the installation of treatment and control technologies to
assure that their wastewater discharge will meet all applicable pretreatment standards and requirements. The
Permittee shall maintain a current Allocation Table (AT) which summarizes the results of the HWA and the limits
from all IUPs. Permitted JUP loadings for each parameter cannot exceed the treatment capacity of the POTW as
determined by the HWA. [ I5A NCAC 0211 .0906(b)(6), .0909, .0916, and .0917; 40 CFR 403.5, 403.8(f)(I )(iii);
NCGS 143-215.67(a)]
6. Authorization to Construct (AtC)
The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable Industrial
Users for the construction or modification of any prctreatuent facility. Prior to the issuance of an AtC, the
proposed pretreatment facility and treatment process nmst be evaluated for its capacity to comply with all
Industrial User Pretreatment Pennit (IUP) limitations. [ 15A NCAC 021-1 .0906(b)(7) and .0905; NCGS 143-
215.1(a)(8)]
7. POTW Inspection & Monitorint" of their 1LJs
The Permittee shall conduct inspection, surveillance, and monitoring activities as described in its Division
approved pretreatment program in order to determine, independent of information supplied by Industrial Users.
compliance with applicable pretreatment standards. [I 5A NCAC 0211 .0908(e); 40 CPR 403.8(f)(2)(v)] The
Permittee must:
a. inspect all Significant Indust ial Users (SIUs) at least once per calendar year;
b. Sample all Significant Industrial Users (SIUs) at least once per calendar year for all SIU permit -limited
parameters including flow except as allowed under 15A NCAC .0908(e); and
c. At least once per year, document an evaluation of any non -significant categorical Industrial User for
compliance with the requirements in 40 CPR 403.3(v)(2), and either continue or revoke the designation as non-
significant.
8. IU Self Monitoring, and Reporting
The Permittee shall require all Industrial Users to comply with the applicable monitoring and reporting
requirements outlined in the Division -approved pretreatment program, the industry's pretreatment permit, or in 15A
NCAC 021-1 .0908. [15A NCAC 02H .0906(b)(5) and .0905; 40 CFR 403.8(f)(1)(v) and (2)(iii); 40 CPR
122.440)(2) and 40 CFR 403.12]
9. Enforcement Response Plan (ERP)
The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards
pronuilgated pursuant to section 307(b) and (c) of the CWA (40 CFR 405 et. seq.), prohibitive discharge standards
as set forth in 40 CFR 403.5 and 15A NCAC 0211 .0909, specific local limitations, and other pretreatment
requirements. All remedies, enforcement actions and other, shall be consistent with the Enforcement Response
Plan (ERP) approved by the Division. [I5A NCAC 02H .0903(b)(7), .0906(b)(8) and .0905; 40 CFR 403.8(f)(5)]
10. Pi eu eatment Annual Reports (PAR)
The Permittee shall report to the Division in accordance with 15A NCAC 02H .0908. In lieu of submitting annual
reports, Modified Pretreatment Programs developed under I5A NCAC 02H .0904 (b) may be required to submit a
partial annual report or to meet with Division personnel periodically to discuss enforcement of pretreatment
requirements and other pretreatment implementation issues.
For all other active pretreatment programs, the Permittee shall submit two copies of a Pretreatment Annual Report
(PAR) describing its pretreatment activities over the previous calendar year to the Division at the following
address:
Version 1110912011

NPDES Permit Standard Conditions
Page 18 of 18
NC DENR / Division of Water Quality / Surface Water Protection Section
Pretreatment, Emergency Response, and Collection Systems (PERCS) Unit
1617 Mail Sei vice Center
Raleigh, North Carolina 27699-1617
These reports shall be submitted by March I of each year and shall contain the following:
a. Narrative
A narrative suns nary detailing actions taken, or proposed, by the Permittee to correct significant non-
compliance and to ensure compliance with pretreatment requirements;
b. Pretreatment Program Sununary (PPS)
A pretreatment program summary (PPS) on forms or in a format provided by the Division;
C. Si¢❑ificantNon-Compliance Report (SNCR)
A list of Indusrial Users (lUs) in significant noncompliance (SNC) with pretreatment requirements, and the
nature of the violations on forms or in a format provided by the Division;
d. Industrial Data _Summary Forms IDSF
Monitoring data from samples collected by both the POTW and the Significant Industrial Users (SIUs). "these
analytical results must be reported on Industrial Data Summary Forms (IDSF) or on other forms or in a format
provided by the Division;
e. Other Information
Copies of the POTW's allocation table, new or modified enforcement compliance schedules, public notice of
IUs in SNC, a summary of data or other information related to significant noncompliance determinations for
lUs that are not considered SIUs, and an), other information, upon request, which in the opinion of the Director
is needed to determine compliance with the pretreatment implementation requirements of this permit;
1 1. Public Notice
The Permittee shall publish annually a list of Industrial Users (lUs) that were in significant noncompliance (SNC)
as defined in the Permittee's Division -approved Sewer Use Ordinance with applicable pretreatment requirements
and standards during the previous twelve month period. This list shall be published within four months of the
applicable twelve-month period. [ 15A NCAC 02H .0903(b)(34), .0908(b)(5) and .0905 and 40 CFR
403.8(f)(2)(vi i i )]
12. Record Keeping,
The Permittee shall retain for a minimum of three years records of monitoring activities and results, along with
support information including general records, water quality records, and records of indusu ial impact on the
POTW and shall retain all other Pretreatment Program records as required by 15A NCAC 0211 .0908(f). [ 15A
NCAC 02H .0908(f); 40 CPR 403.12(o)]
13. Pretreatment Program Resources
'File Permittee shall maintain adequate funding and qualified personnel to accomplish the objectives of its approved
pretreatment program. and retain a written description of those current levels of inspection. [ 15A NCAC 0211
.0906(b)(9) and (10) and .0905; 40 CPR 403.8(f)(3), 403.9(b)(3)]
14. Modification to Pretreatment Programs
Modifications to the approved preueannent program including but not limited to local limits modifications, POTW
monitoring of their Significant Indusuial Users (SIUs), and Monitoring Plan modifications, shall be considered a
permit modification and slhall be governed by 40 CFR 403.18, 15 NCAC 021-1 .0114 and 15A NCAC 02H .0907.
Version 1110912011

APPENDIX B
LABORATORY ANALYSES:
Section 1: TEMPERATURE
Section 2:
pH ANALSIS
Section 3:
DO ANALYSIS
Section 4:
LOW LEVEL CHLORINE
Section 5:
MLSS
Section 6:
LABORATORY ANALYSIS BY
OUTSIDE CONTRACTOR

SECTION 1: TEMPERATURE
Reference: SM 4500 6-2000 (Aqueous)
Sample Type: Grab
Container:
Glass or Plastic (Polyethylene or equivalent)
Preservative:
None -Analyze immediately (within 15 minutes of
Sampling)
Equipment:
Normally, temperature measurements may be made with
any good mercury -filled Celsius thermometer. As a
minimum, the thermometer should have a scale marked for
every 0.1 °C. The thermometer should have a minimal
thermal capacity to permit rapid equilibrium. All lab
equipment associated with NPDES reporting is calibrated
yearly. Check the thermometer against a precision
thermometer certified by the National Institute of Standards
and'fechnology (MIST) on an annual basis.
Procedure:
When obtaining temperature measurements, the
thermometer should be immersed up to the immersion line
on a partial immersion thermometer or totally immersed in
the sample when using a total innnersion thermometer.
Check for those markings on the thermometer prior to use.

SECTION 2: pH ANALYSIS
Reference: SM4500IJ4B-2000
Sample Type:
Grab
Container:
Glass or Plastic (Polyethylene or equivalent)
Preservative:
None -analyze immediately (within 15 minutes of sampling)
Interference:
The glass electrode is relatively free form interference from
color, turbidity, colloidal matter, oxidants, reductants, or
high salinity, except for a sodium error at pH>10. This
error can be reduced by using "low sodium error"
electrodes. Furthermore, temperature affects pH
measurements: chemical equilibrium changes with
temperature, affecting pH. Therefore, one should always
report the temperature at which the pH is measured.
Equipment:
For liquid NPDES compliance samples, the pH meter
should consist of a potentiometer, a refillable electrode, a
reference electrode and a temperature compensating device.
Also, the meter should be capable of reading to 0.01
standard units and successive readings should be accurate
and reproducible to 0.10 standard units and have a range of
0 to 14.
Rea(c� nts:
Utilize either commercially available standardized pH
buffers or to prepare buffers fresh. Current use is Fisher
Scientific pH 10.00, pH 7.00, and pH 4.00 buffers. After
completing the three-point calibration, the 7.00 buffer is
checked for accuracy.
Procedure:
In each case follow manufacturer's instruction for pH meter
and for storage and preparation of electrodes for use.
Precision and Accuracy: When the pH meter and electrodes are in good
working condition and proper procedures are consistently
utilized, a precision of 0.02 pH units and an accuracy of+/-
0.05 pH units can be achieved. However, under normal
conditions, the limit of accuracy is expected to be +/- .01
pH units. `fhis is especially true when water samples or
poorly buffered solutions are analyzed for pH.

Instrument Calibration for pH meter
1. Activate Oakton 6+ Meter, Press I/O EXIT.
2. Press CAL, The display will prompt for standard 1.
3. Remove pH probe from storage solution and rinse with distilled water.
4. Place probe in designated pH Buffer 7.00 Solution Beaker to begin
calibration.
5. Activate Magnetic Stir plate using caution not to immerse pH probe too
deep into the standard.
6. Press READ/ENTER. Wait until electrode stabilizes. Record pH value
and temperature reading when stabilized indicated by three beeps.
7. The display will prompt for standard 2, Rinse electrode with distilled
water.
8. Place the electrode in the second buffer pH Buffer 10.00 Solution beaker
and activate Magnetic Stir plate. Press READ/ENTER. Wait until
electrode stabilizes. Record pH value and temperature reading when
stabilized indicated by three beeps.
9. The display will prompt for standard 3, Rinse electrode with distilled
water.
10. Place electrode in the third buffer pH Buffer Solution 4.00 Solution beaker
and activate Magnetic Stir plate. Press READ/ENTER. Wait until
electrode stabilizes. Record pH Value and temperature reading when
stabilized indicated by three beeps.
11. When the reading is stable, the SLOPE and STORE FUNCTION will
appear.
12. Record electrode SLOPE reading. Acceptable operating range is — 58 + 3
3nV/decade. All Buffers must be within .1 so to be acceptable
13. To save this calibration, press ENTER. To exit without saving the
calibration press EXIT.
Reviewing the Calibration
A. From the pH Reading mode, press the REVIEW key.
B. The display will show the standard number, standard pH,
and temperature (view mV value by pressing pH/mV).
Press the up arrow once.
C. The meter will continue to scroll through the standard
information with each press of the up arrow key. When all
the standards have been displayed, press the up arrow key
again.
1). The meter will display the slope and offset of the
calibration curve.
E. To exit Cal review mode, press EXIT. To review any
standard or slope information again, press the arrow key.

Performing Analytical Procedures
The Oakton 6+pH meter has been properly calibrated and is ready to
perform Standard pl-I Analytical Procedures as follows:
I . Immerse the rinsed pH probe into the selected sample to be
analyzed.
2. Activate magnetic stir plate; press READ/ENTER, stabilizing
will appear along with the sample temperature and the pH
reading. These values may fluctuate until the system is
stable.
3. When the reading is stable, `STABILIZING' will disappear.
If the display lock is off, the display will show the current
reading and temperature, but the values may fluctuate.
4. Record the pH or mV reading and temperature.
5. Remove the pH probe from the sample; rinse with deionized
water and place probe in the duplicate sample to be analyzed.
6. Activate the magnetic stir plate; press READ/ENTER;
`Stabilizing' will appear along with the sample temperature
and the pH reading. These values may fluctuate until the
system is stable.
7. Once sample is stabilized, record the pH reading and
temperature.
8. Perform a final check on the 7.0 standard buffer and record
the pH value and temperatures when stabilized; the
difference should be between 6.9 and 7.1 for the buffer.

SECTION 3: DO ANALYSIS
(Effluent 7enrperature is Compliance Reporting)
Reference: SM 4500 O G-2001 (Aqueous)
General Discussion: Membrane electrodes provide an excellent method
for DO analysis in polluted waters, highly colored waters and strong waste
effluents. They are recommended for use especially under conditions that
are unfavorable for use of the iodometric method, or when that test and its
modifications are subject to serious errors caused by interferences.
Principle: Oxygen -sensitive membrane electrodes of the galvanic type are
composed of two solid metal electrodes in contact with supporting
electrolyte; an external source of applied voltage is needed to polarize the
indicator electrode. Membrane electrodes are commercially available in
some variety. In all these instruments, the "diffusion current' is linearly
proportional to the electrical potential of the membranes permeability.
Interference: Plastic films used with membrane electrode systems are
permeable to a variety of gases besides oxygen, although none are
depolarized easily at the indicator electrode. Prolonged use of membrane
electrodes in waters containing such gases as hydrogen sulfide (II2S) tends
to lower cell sensitivity. Eliminate this interference by frequently
changing and calibrating the membrane electrode.
Sampling: Because membrane electrodes offer the advantage of analysis
in situ, they eliminate errors caused by sample handling and storage
Apparatus: Oxygen -sensitive membrane electrode with appropriate meter
(YSI 55 meter).
Calibration: Follow the procedure below exactly to obtain guaranteed
precision and accuracy.
A. Switch instrument to OFF and adjust meter mechanical zero.
B. Switch to ZERO and adjust to "O" on mg/L scale.
C. Switch to FULL SCALE and adjust to "45" on C scale.
D. Prepare probe for operation, plug into instrument, wait 10 to 15
minutes for probe to polarize. Probe can be in calibration
chamber or ambient air.
E. Switch to CALIB.02 and adjust CALM control until meter
indicates local altitude on short scale in upper right corner of
meter.
DO Measurement:

A. Place probe in sample and stir.
B. Allow sufficient time for probe to stabilize to sample temperature
and DO.
C. Switch to READ TEMP AND SET DIAL. Set Oz
SOLUBILITY FACTOR dial to sample temperature.
D. Switch to READ Oz and read mg/L DO while stirring.
E. It is recommended that the instrument be left `on' between
measurements to avoid necessity to polarize the probe and re -
calibrate.
General Care
A. Replace batteries after 1000 hours of operating or if full scale
adjustment cannot be made. [Use Eveready #935 "C" size or equal.]
B. Replace membrane every 3-4 weeks. Probe should be stored in humid
environment to prevent drying out.
Validation of Temperature: Check frequently one or two points to verify
temperature correction data against a NIST certified thermometer.

SECTION 4: LOW LEVEL CHLORINE ANALYSIS
Reference: SM 4500 CI G-2000 (Aqueous) Hach 8167 HR (Aqueous)
Note: Under direction of the Plant Manager, laboratory analysis will be required
to prepare a Chorine Standard Curve prior to conducting Chlorine analysis at
the Wastewater Treatment Plant. A five point Standard Curve must be performed
yearly.
Chlorine Standard Curve Preparation Procedures:
Materials Required:
• Hach DR/2800 Colorimeter with pour through sample cell.
• 6 - 100 ml. Pyrex Class "A" Volumetric Flasks with stoppers.
• 5 - 100 ml. Tri-Cornered Polypropylene Beakers
• 1 - 0.5 ml. Class A Volumetric Pipette
• 1 - 1 nil. Class A Volumetric Pipette
• 1 - 10 nil. Class A Volumetric Pipette
• 1 - 25 ml. Class A Volumetric Pipette
Reagents:
• Potassium Permanganate Stock Solution = 891 mg KMNO4 diluted to 1000
nil.
• Potassium Permanganate Working Solution = 5 nil KMNO4 Stock Solution
diluted to 100ml.
• Hack DPD Total Chlorine Reagent for 25 ml. samples.
Procedure:
1. Operate and edit the I-Iack DR/2800 as directed for Hach Standard Method *
8370 Chlorine, Total ULR (2 to 500 ug/1 as e12) set to program 4 86 prior to
preparing a Potassium Permanganate Working Solution
2. Prepare a Potassium Permanganate Working Solution by diluting 5 ml Of
KMNO4 Stock Solution to 100 ml of distilled water.
3. Prepare a series of Calibration Standards in the following manner.
SAMPLE IDENTIFICATION COMPOSITION
500 PPB Standard ]nil KMNO4 Working Solution / 100 ml distilled
water
250 PPB Standard .5 KMNO4 Working Solution / 100 nil distilled
water
125 PPB Standard 25m1(500 PPM Standard) / 100 nil distilled water

50 PPB Standard 10 nil (500 PPM Standard) / 100 nil distilled water
25 PPB Standard 10 nil (250 PPM Standard) / 100 nil distilled water
0 PPB Standard 25 nil distilled water
4. Beginning with the Zero PPM Standard, measure and dispense 25 mis of the
prepared Calibration Standards into Polypropylene Beakers weakest
concentration to the greatest.
5. Add the contents of one Hach DPD Total Chlorine Reagent package to each
measured sample.
6. Set the Hach DR/2800 Colorimeter timer for 3:00 minutes..
When the 3-minute period is complete, dispense samples into Pour Through
cell.
Beginning with the Zero 1111M Standard, pour into Hach DR/2800
Colorimeter. Be sure to rinse the Pour Through cell between each Calibration
Standard to be analyzed and zero flach DR/2800 Colorimeter with remainder
of sample standard to be analyzed.
9. Record Concentration Observed relative to Sample Identification.
10. Proceed to determine Slope, Intercept, and Correlation values for Texas
Instruments TI- 36X Scientific Calculator.
TI —36 X CALCULATOR OPERATION
I. To clear — ON/AC, to clear statistical data — 3"'/ Stat 2 then, 2i" / Statt
2. For true calculations:
3. Sample Identification, then Stat 1, Concentration Observed, then Stat 2;
until all data points are entered.
4. Determine Slope = 2i1 function — SLP(5)
5. Determine Intercept = 2"1 function — ITC (4)
6. Determine Correlation Coefficient = 3" function - ITC (4)
7. Observed Concentration values, then 211d function (y) = True Value
Calculation
RPD = (Difference of Observed Concentrations) x 200
(Sum of Observed Concentrations)
°/o RE = (Observed Concentration x 100
(Sample Identification)
REC is calculated on standards only

SECTION 5: MLSS (Mixed Liquor Suspended Solids) (Process Control Test)
Sample Type: Grab
Procedure: Mix sample thoroughly. Weigh dry filter. Pour sample
through a vacuum filter. Place in drying oven (103 - 105°C) for at
least one hour. Place filter in desiccator for one hour. Remove and
weigh filter.
Interferences: Filtration apparatus, filter material, pre -washing, and
drying temperature are specified because these variables have been
shown to affect the results. Samples high in filterable residue
(dissolved solids), such as slime waters, brines and some wastes, may
be subject to a positive interference.
Equipment:
Analytical Balance: Capable of weighing to 0.1 mg
Desiccator: Preferably containing a desiccant that utilizes a color
for moisture content.
Drying Oven: Capable of maintaining a constant temperature
between 103-105' degrees Celsius.
Glass Fiber Filter Disks: These filters should not contain organic
binder.
Filtration Apparatus: either a membrane filter funnel, Gooch
crucible (25-40ml capacity) or filter apparatus that contains a
reservoir and a coarse 40 to 60 um) fritted disk as a filter support.
Filtration Setup: suction flask consisting of the filtration
apparatus, side arm flask and vacuum source.
Reagents: None
Temperature Monitoring: The temperature of the drying oven
should be monitored whenever compliance monitoring samples are
being dried in the oven.
Calculation: MLSS (mg/L) = (A-B)* 1,000,000
Sample volume (mLs)
A= weight of filter + dried residue in mg.
B= weight of filter in mg

SECTION 6: LABORATORY ANALYSIS BY OUTSIDE CONTRACTOR
Pace Analytical Services Inc, our certified contract laboratory,
conducts the following permit required tests to include the
following:
Daily: Total Suspended Solids (TSS), BOD
Bi-monthly: Sulfides, Phenols, Chromium, I ecal
Coliform
Quarterly: Chronic Toxicity, Lead, Arsenic,
Chloroform
Weekly: COD, Total Nitrogen, Phosphorus
Semi -Annually: Benzene, Ethylbenzene
Please refer to the permit for the required analyses that need to
be completed (See Appendix A for a copy of the WWTP permit).
Since our laboratory at the WWTP is only certified as a Field
Laboratory, the only analyses required by the permit that are
ran in-house include the following: Total Residual Chlorine,
PH, Temperature, and Continuous Flow.

APPENDIX C
PREVENTIVE MAINTENANCE PLAN

APPENDIX D
WWTP DRAWINGS

DUVALTEX WWTP
RSC FORM
VICINITY MAP
PROCESS FLOW DIAGRAM / NARRATIVE
QUANTITATIVE JUSTIFICATION
SAMPLING PLAN
LABORATORY ANALYTICAL

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permtfth g BM
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T.1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC I 1-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Man Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensue that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page I of I

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State of North Carolina
A � � Department of Environmental Quality
LOU s Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
1. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
I. Facility Name: Duvaltex WWTP
2. Facility permit holder is: ❑ Federal, ® State, ❑ Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Ilealth,
or ❑ Other (explain _).
3. Facility contact person and title: Mr. Glen Gary. ORC
Complete mailing address: 304 East Main Street
City: Elkin State: NC Zip: 28621-
Telephone number: Q36) 526-941 1 E-mail address: glen gary/a duvaltex.cont
4. Facility physical address: 175 Fabric Lane
City: Elkin State: NC Zip: 28621-
Coordinates: Latitude: 36' 14' 41 51" Longitude: 8W 50' 29.49"
Datum: NAD83 Level of accuracy: Hundreths_of second
Method of measurement: MAP
5. Purpose of the facility:
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
® treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: 95 % industrial and 5 % domestic)
❑ other (explain: ' ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 4.0 MGD and facility average daily flow: 0,1 MGD
8. Average amount of residuals being generated at this facility 520 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: aerobic (See Attached O&M Manual),
Type and volume of residuals storage (i.e., outside of residuals treatment units): 6 sand drvin&beds each approx. 35'x82')
11. RESIDUALS QUALITY INFORMATION (See Instruction C.):
I. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Pair 257.
Note: Only residuals that are generated during domestichnunicipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1 102(6) as:
® Biological ❑ Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page I of

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no.
If yes, list the number(s). _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical and Date of analysis: 3=14_19
Passed corrosivity test: ® yes E] no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes Q no. Flashpoint: >170 OF (> 140°F)
Passed reactivity test: Eyes Qno. HCN: <1.2 mg/kg (<250) & 112S: <12.5 mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(177g/1)
Result
(nvg/1)
Arsenic
5.0
<0.050
1-1 exach I oroben zen e
0.13
<0.05
Barium
100.0
<0.25
Ilexachloro-1,3-Butadiene
0.5
<0.05
Benzene
0.5
<0.01
Hexachloroethane
3.0
<0.05
Cadmium
1.0
<0.0050
Lead
5.0
<0.025
Carbon Tetrachloride
0.5
<0.01
Lindane
0.4
<0.005
Chlordane
0.03
<0.03
Mercury
0.2
<0.00020
Chlorobenzene
100.0
<0.01
Methoxychlor
10.0
<10
Chloroform
6.0
<0.01
Methyl Ethyl Ketone
200.0
<0.02
Chromium
5.0
<0.050
Nitrobenzene
2.0
<0.05
m-Cresol
200.0
<0.05
Pentachlorophenol
100.0
<0.01
0-Cresol
200.0
<0.05
Pyridine
5.0
<0.05
p-Cresol
200.0
<0.05
Selenium
1.0
<0.10
Cresol
200.0
<0.05
Silver
5.0
<0.025
2,4-D
10.0
0.0050
Tetrachloroethylene
0.7
<0.01
1,4-Dichlorobenzene
7.5
<0.01
Toxaphene
0.5
<0.03
1,2-Dichloroethane
0.5
<0.01
Trichloroethylene
0.5
<0.01
1, 1 -Dichloroethylene
0.7
<0.01
2,4,5-Trichlorophenol
400.0
<0.05
2,4-Dinitrotoluene
0.13
<0.05
2,4,6-Trichlorophenol
2.0
<0.05
Endrin
0.02
<0.005
2,4,5-TP (Silvex)
1.0
0.010
Heptachlor and its Hydroxide 1
0,008
1 <0.005
Vinyl Chloride
0.2
<0.01
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical and Date of analysis: 3-14-19
Parameter
Ceiling
Concentration Limits
(ClassA & Class6)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(rng/kg)
Result
(mg/kg)
Arsenic
75
41
0.77
Cadmium
85
39
0.67
Copper
4,300
1,500
Ill
Lead
840
300
17.4
Mercury
57
17
0.096
Molybdenum
75
n/a
0.96
Nickel
420
420
7.8
Selenium
100
100
1.3
Zinc
7,500
2,800
330
b. For Surface Disposal Unit (lrrnrltill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(nigAg)
chromium
(mg/kg)
Nickel
(mg/kg)
El > 0 but < 25
30
200
210
> 25 but < 50
34
220
240
> 50 but < 75
39
260
270
F-I> 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (ntg4g)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 79.7 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analvtical and Date of analysis: 3-14-19
Parameter
Result
(mg/kg)
Aluminum
13,500
Ammonia -Nitrogen
11.8
Calcium
6,130
Magnesium
1,490
Nitrate -Nitrite Nitrogen
5
pH (Standard Unit)
6.2
Phosphorus
3,700
Potassium
568
---
Sodium —--
_-- —---- 383 ---
Total Kjeldahl Nitrogen
7,980
c. Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 1.013
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): ® default value, or E] actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: N/A
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (I") Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
2,401
3,956
Injection/Incorporation
2,407
3,962
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: N/A
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T 1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Lmrrl Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative I [ I5A NCAC 02T.1 106(b)(3)(A)] - Time/Temperature Compliance.
Alternative 2 [I5A NCAC 02T.1 106(b)(3)(B)] - Alkaline Treatment.
Alternative 3 [15A NCAC 02T.1106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Hehninth Ova.
Alternative 4 [15A NCAC 02T.1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [ 15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
thermophilic aerobic digestion, ❑ beta ray irradiation,
El gannna ray irradiation, or ❑ pasteurization.
b. for Laarl AUUlieatiar of Class B:
® Alternative 1 [15ANCAC 02T.1 106(c)(1)] -Fecal Coliform Density Demonstration.
® Alternative 2 [15A NCAC 02T.1106(c)(2)] - Process to Significantly Reduce Pathogens (PS11P).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
El composting, or Ellime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item It. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
❑ Exempt - If Daily Cover Alternative is chosen in Item 11.8. below [I5A NCAC 02T.I 106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per I5A NCAC 02T 1107, specify how residuals will meet the VAR requirements:
❑ Alternative I [I5A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T. 1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 021'. 1 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
® Alternative 7 [15A NCAC 02T.1 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [ I5A NCAC 02T.1 107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection.
❑ Alternative 10 [I5A NCAC 021'.1107(a)(l0)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

VICINITY MAP

PROCESS FLOW DIAGRAM / NARRATIVE
(SEE O&M PLAN)

QUANTITATIVE JUSTIFICATION

DUVALTEX
FIELD
LOADINGS
DATE SPD:
FARM:
ACRES:
1.00
SITE:
WETTONS
652.00
FIELD:
W T/ACRE:
652.00
CROP:
Fescue
% SOLIDS:
79.70
Site Cond
DRY
G/D
TONS:
DT/ACRE:
519.64
51964
`Ltg41$ IIVI-
TOTAL
>g,,ae.CI
15b
Soil Prod/Series Ree. N
Soil PH Ree. P
Ree. K
County
Parameter
#'s/DT
#'s/Acre
PAN (incorporated)
8.126
4222.59
PAN surface
8.114
4216.36
Phos horns
7.400
3845.34
Potassium
1.136
590.31
Ma nesium
2.980
Aluminum
27.000
14030.28
Arsenic
0.002
1.039
Cadmium
0.001
0.520
Chromium
---
#VALUE!
Copperr
0.224
116.399
Lead
0.035
18.187
Mercury
0.000
0.000
Mol -bdcnum
0.002
1.039
Nickel
0.016
8.314
Selenium
0.003
1.559
Zinc
0.660
342,962
TKN
27.000
14030.280
NI13
0.024
12.471
N2-N3
0.010
5.196
Report: 92421239

SAMPLING PLAN
(SEE, O&M PLAN)

LABORATORY ANALYTICAL

DUVALTEX
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date Sampled: March 14, 2019
Permit No. WO0013982
DUVALTEX 79.70 %Solids
Stockoile Residuals 6.2 DH
Parameter
%
Mg/Kg Dry Weight
(% x 10,000)
Pounds/Dry Ton!
(M /K x 0.002) s
Nitrogen (PKN)
1.3500
11500.000
27.000
Phosphorus
0.3700
3,700.000
7.400
Potassium
0,0568
568.000
1.136
PAN (injected)*
0.4063
4,063.000
8.126
PAN surface *
0.4057
4,057.000
8.114
Ammonia Nitrogen
0.00118
11.800
0.024
Calcium
0.6130
6,130,000
12.260
Calcium Carbonate E .
---
---
---
Magnesium
0.1490
1.490.000
2.980
Sodium
0.0383
383.000
0.766
Sulfate
---
---
---
Nitrate N / Nitrite N
5.000
0.010
]ron
---
---
---
Aluminum
13.500.000
27.000
Arsenic
0.770
0,002
Cadmium
---
0.670
0,001
Chromium
---
---
---
Copper
---
112.000
0.224
Lead
---
17.400
0.035
Mercer
0.096
0.000
Molybdenum
---
0.960
0,002
Nickel
7.800
0.016
Selenium
1.300
0.003
Zinc
--
330.000
0.660
Pace Analytical 4 92421239
*Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate)(1RN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
Surface Application:
(Min for calculation purposes.
Note. Constituents N.D. (Not Detected) or < detection limits are listed as detection limits

/ /PaceAnalXical e
vnwepacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HUntersville, NC 28078
[phone]
March 28, 2019
Mr. Glen Gary
TRUE, Inc.
304 E. Main St,
Elkin, INC 28621
RE: Project: Land Application
Pace Project No.: 92421239
Dear Mr. Gary:
Enclosed are the analytical results for sample(s) received by the laboratory on March 14, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Scott Taylor, True Textiles
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 48

17aceAnalytical
/ - rwiw.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Land Application
Pace Project No.: 92421239
Atlanta Certification IDs
110 Technology Parkway Peachtree Corners, GA 30092
North Carolina Certification #: 381
Florida DOH Certification M E87315
South Carolina Certification M 98011001
Georgia DW Inorganics Certification #: 812
Virginia Certification #: 460204
Georgia DW Microbiology Certification #: 812
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
Missouri Certification M 235
ANAB DOD-ELAP Rad Accreditation #: L2417
Montana Certification #: Cert0082
Alabama Certification #: 41590
Nebraska Certification #: NE-OS-29-14
Arizona Certification #: AZ0734
Nevada Certification #: PAO14572018-1
Arkansas Certification
New Hampshire/TNI Certification* 297617
California Certification #: 04222CA
New JerseyrTNI Certification #: PA051
Colorado Certification #: PA01547
New Mexico Certification #: PA01457
Connecticut Certification #: PH-0694
New YorkfTNI Certification #: 10888
Delaware Certification
North Carolina Certification #: 42706
EPA Region 4 DW Rad
North Dakota Certification #: R-190
Florida/TNI Certification #: E87683
Ohio EPA Rad Approval: #41249
Georgia Certification #: C040
Oregon/iNI Certification #: PA200002-010
Guam Certification
Pennsylvania/TNI Certification #: 65-00282
Hawaii Certification
Puerto Rico Certification #: PA01457
Idaho Certification
Rhode Island Certification #: 65-00282
Illinois Certification
South Dakota Certification
Indiana Certification
Tennessee Certification #: 02867
Iowa Certification #: 391
TexasfTNI Certification #: T104704188-17-3
Kansas/TNI Certification #: E-10358
Utah/TNI Certification #: PA014572017-9
Kentucky Certification #: KY90133
USDA Soil Permit #: P330-17-00091
KY WW Permit#: KY0098221
Vermont Dept. of Health: ID# VT-0282
KY WW Permit #: KY0000221
Virgin Island/PADEP Certification
Louisiana DHHfTNI Certification M LA180012
VirginiaNELAP Certification #: 9526
Louisiana DEQ/TNI Certification M 4086
Washington Certification #: C868
Maine Certification M 2017020
West Virginia DEP Certification #: 143
Maryland Certification #: 308
West Virginia DHHR Certification #: 9964C
Massachusetts Certification #: M-PA1457
Wisconsin Approve List for Rad
Michigan/PADEP Certification #: 9991
Wyoming Certification #: 8TMS-L
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification M 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NCO30
Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 2 of 48

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Land Application
92421239
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92421239001
Stock Pile Residual Solids
EPA 8081E
SEM
9
PASI-C
EPA8151A
MZP
3
PASI-GA
EPA6010D
DS, KQ
13
PASI-A
EPA6010D
DS
7
PASI-A
EPA 7470A
RUT
1
PASI-A
EPA 7471B
RDT
1
PASI-A
EPA8270E
PKS
18
PASI-C
EPA8260D
SAS
14
PASI-C
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA9045D
ECH
1
PASI-A
SM 271OB-2011
DMN
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod,
NAL
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
EPA 9014
PAS
1
PASI-PA
SM 4500S2F-00
PAS
1
PASI-PA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 48

�PalceAnalytical'
vni w,paxfabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Land Application
Pace Project No.: 92421239
Sample: Stock Pile Residual Solids Lab ID: 92421239001 Collected: 03/14/19 07:30 Received: 03/14/19 08:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
8081 TCLP Pesticides RVE
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl(S)
Tetrachloro-m-xylene (S)
8151A Cl Acid Herbicides TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
Analytical Method: EPA 8081E Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 03/19/19 18:30 Initial pH: 6,39; Final pH: 4
ND
ug/L
5.0
10
03122/1915:32
03127/1917:11
58-89-9 L1
ND
ug/L
30.0
10
03/22/1915:32
03127/1917:11
57-74-9
ND
ug/L
5.0
10
03122/1915:32
0312711917:11
72-20-8
ND
ug/L
5.0
10
03/22/1915:32
03/27/1917:11
76-44-8
ND
ug/L
5.0
10
03122/1915:32
03/27/1917:11
1024-57-3
ND
ug/L
10000
10
03/22/1915:32
03/27/1917:11
72-43-5
ND
ug/L
30.0
10
03/2211915:32
03127/1917:11
8001-35-2
0
%
10-138
10
03/2211915:32
03/27/1917:11
2051-24-3 S4
0
%
10-110
10
03/22/1915:32
03/27/1917:11
877-09-8 D3,34
Analytical Method: EPA 8151A Preparation Method: EPA 8151A
Leachate Method/Date: EPA 1311; 03/21/19 12:00 Initial pH: 8.54; Final pH: 4.49
ND mg/L 0.0050 1 03/25/19 09:30 03/26/19 02:34 94-75-7
ND mg/L 0.010 1 03/25/19 09:30 03/26/19 02:34 93-72-1
105 A. 10-155 1 03/25/19 09:30 03/26/19 02:34 19719-28-9
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Aluminum
13500
mglkg
76.5
10
03/23/19 10:10
03/25/19 21:39
7429-90-5
Arsenic
ND
mg/kg
0.77
1
03/23/19 10:10
03/24/19 21:51
7440-38-2
Cadmium
0.67
mg/kg
0.077
1
03/23/19 10:10
03/24/19 21:51
7440-43-9
Calcium
6130
mglkg
7.7
1
03/23/19 10:10
03/24/19 21:51
7440-70-2
Copper
112
mg/kg
0.38
1
03/23/19 10:10
03/24/19 21:51
7440-50-8
Lead
17.4
mg/kg
0.38
1
03/23/19 10:10
03/24/19 21:51
7439-92-1
Magnesium
1490
mg/kg
7.7
1
03/23/19 10:10
03/24/19 21:51
7439-95-4
Molybdenum
0.96
mg/kg
0.38
1
03/23/19 10:10
03/24/19 21:51
7439-98-7
Nickel
7.8
mg/kg
0.38
1
03/23/19 10:10
03/24/19 21:51
7440-02-0
Potassium
568
mg/kg
383
1
03/23/19 10:10
03/24/19 21:51
7440-09-7
Selenium
1.3
mg/kg
0.77
1
03/2311910:10
03/24/19 21:51
7782-49-2
Sodium
ND
mg/kg
383
1
03/23/19 10:10
03/24/19 21:51
7440-23-5
Zinc
330
mg/kg
0.77
1
03/23/19 10:10
03/24/19 21:51
7440-66-6
6010 MET ICP, TCLP
Analytical Method:
EPA 601 OD Preparation Method: EPA 3010A
Leachate Method/Date:
EPA 1311;
03/21/19 22:24
Initial
pH: 8.11; Final
pH: 4.5
Arsenic
ND
mg/L
0.050
1
03/23/19 09:04
0312411917:54
7440-38-2
Barium
ND
mg/L
0.25
1
03/23/19 09:04
03/24/19 17:54
7440-39-3
Cadmium
ND
mg/L
0.0050
1
03/23/19 09:04
03/24/19 17:54
7440-43-9
Chromium
ND
mg/L
0,050
1
03/23/19 09:04
03/24/19 17:54
7440-47-3
Lead
ND
mg/1-
0.025
1
03/2311909:04
03/24/19 17:54
7439-92-1
Selenium
ND
mg/L
0.10
1
03/23/19 09:04
03/24/19 17:54
7782-49-2
Silver
ND
mg/L
0,025
1
03/23/19 09:04
03/24/19 17:54
7440-22-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 48

�AaceAnalytical
i-Ampacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Land Application
Pace Project No.: 92421239
Sample: Stock Pile Residual Solids Lab ID: 92421239001 Collected: 03/14/19 07:30 Received: 03/14/19 08:10 Matrix: Solid
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 03/21/19 22:24 Initial pH: 8,11; Final pH: 4.5
Mercury ND mg/L 0.00020 1 03/2311912:08 03/2511913:44 7439-97-6
7471 Mercury
Mercury
8270E TCLP RVE
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methy Iphe nol(o-C resop
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2, 4,5-Tri ch to rophe n o I
2,4, 6-Trich loro p he n of
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl(S)
Terphenyl-cI14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol(S)
8260D MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Analytical Method: EPA 7471B Preparation Method: EPA 7471 B
0.096 mg/kg 0,0053 1 03/21/1919:08 03/22/1915:39 7439-97-6
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
ND
ug/L
60.0
1
03/25/1911:16
03/26/1910:46
106-46-7
ND
ug/L
50.0
1
03/25/1911:16
03/26/1910:46
121-14-2
ND
ug/L
%0
1
03/25/1911:16
03/2611910:46
87-68-3
ND
ug/L
50.0
1
03/25/1911:16
03/26/1910:46
118-74-1
ND
ug/L
50.0
1
03/25/1911:16
03/26/1910:46
67-72-1
ND
ug/L
50.0
1
03/25/1911:16
03/26/1910:46
95-48-7
ND
ug/L
50.0
1
03/2511911:16
03/26/1910:46
15831-10-4
ND
ug/L
50.0
1
03/25/1911:16
03/26/1910:46
98-95-3
ND
ug/L
100
1
03/25/1911:16
03/26/1910:46
87-86-5
ND
ug/L
50.0
1
03/25/1911:16
03/2611910:46
110-86-1
ND
ug/L
50.0
1
03/25/1911:16
03/26/1910:46
95-95-4 L2
ND
ug/L
50.0
1
03/25/1911:16
03126/1910:46
88-06-2
71
%
12-102
1
03/25/1911:16
03/26/1910:46
4165-60-0
64
%
13-107
1
03/25/1911:16
03/26/1910:46
321-60-8
75
%
21-132
1
03/2511911:16
03/26/1910:46
1718-51-0
31
%
10-110
1
03/2511911:16
03/26/1910:46
13127-88-3
48
%
10-110
1
03/25/19 11:16
03/26/19 10:46
367-12-4
70
%
27-108
1
03/25/1911:16
03/26/1910:46
118-79-6
Analytical Method: EPA 8260D
ND
ug/L
100
20
03/2311917:28
71-43-2
ND
ug/L
200
20
03/23/1917:28
78-93-3
ND
ug/L
100
20
03/23/1917:28
56-23-5
ND
ug/L
100
20
03/23/1917:28
108-90-7
ND
ug/L
100
20
03/23/1917:28
67-66-3
ND
ug/L
100
20
03/23/1917:28
106-46-7
ND
ug/L
100
20
03/23/1917:28
107-06-2
ND
ug/L
100
20
03/23/1917:28
75-35-4
ND
ug/L
100
20
03/23/1917:28
127-18-4
ND
ug/L
100
20
03/23/1917:28
79-01-6
ND
ug/L
100
20
03/23/1917:28
75-01-4
95
%
70-130
20
03/23/1917:28
17060-07-0
101
%
67-135
20
03/23/1917:28
2037-26-5
97
%
70-130
20
03/23/1917:28
460-00-4
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, L-C. Page 5 of 48

OaceAnapical e
vrvnv.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
tiunlersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Land Application
Pace Project No.: 92421239
Sample: Stock Pile Residual Solids Laidig: 92421239001 Collected: 03/14/19 07:30 Received: 03/14/19 08:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
733C S Reactive Cyanide
Cyanide, Reactive
734S Reactive Sulfide
Sulfide, Reactive
Date: 03/28/2019 06:56 PM
Analytical Method: SM 2540G-2011
79.7 % 0.10 1
03/1511916:06
Analytical Method: ASTM D2974-87
20.3 % CA0 1
03/15/1916:00
Analytical Method: EPA 9045D
6.2 Std. Units 0.10 1
03/15/19 15:58 H7
Analytical Method: SM 271OB-2011
2390 mg/kg 0.12 1 03/28/1911:53 N2
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod, Preparation Method: EPA 350A Rev 2.0 1993 Mod.
ND mg/kg 11.8 1 03/18/1915:02 03/19/1915:11 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
7980 mg/kg 299 5 03/20/19 14:00 03/21/19 01:10 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
ND mg/kg 5.0 1 03/15/19 00:43 03/15/19 02:58
ND mg/kg 5.0 1 03/15/19 00:43 03/15/19 02:58 14797-55-8
ND mg/kg 5.0 1 03/15/19 00:43 03/15/19 02:58 14797-65-0
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
3700 mg/kg 62.7 50 03/20/19 21:14 03/20/19 23:35 7723-14-0
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
ND mg/kg 1.2 1 03/1911917:08 03/19/1918:20
Analytical Method: SM 4500S2F-00 Preparation Method: SW-846 7.3.4.2
ND mg/kg 12.5 1 03/19/1917:08 03/19/1917:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 48

aceAnalyticalx
wvmpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Nuntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.'. 92421239
QC Batch: 465000
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92421239001
METHOD BLANK: 2527185
Matrix: Water
Associated Lab Samples: 92421239001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
mg/L
ND 0.00020
03/25/1913:09
METHOD BLANK: 2627581
Matrix: Water
Associated Lab Samples: 92421239001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
mg/L
NO 0,00020
03/2511913:14
LABORATORY CONTROL SAMPLE: 2528972
Spike LCS
LCS % Roo
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Mercury
mg/L
0.0025 0.0029
118 80-120
LABORATORY CONTROL SAMPLE: 2528973
Spike LCS
LCS %Rec
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Mercury
mg/L
0.0025 0.0028
112 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2528974 2528975
MS MSD
92421567001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units
Result
Conc. Conc. Result
Result % Roo % Rao Limits RPD Qual
Mercury mg/L
ND
0.0025 0.0025 0.0031
0,0030 124 119 75-125 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 48

P ceAnalytical
pacelabs.con,
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
liuntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 464634
Analysis Method: EPA 7471E
QC Batch Method: EPA 7471B
Analysis Description: 7471 Mercury
Associated Lab Samples: 92421239001
METHOD BLANK: 2526699
Matrix: Solid
Associated Lab Samples: 92421239001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0060
03/22/1915:18
LABORATORY CONTROL SAMPLE: 2526700
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/kg
0.083 0.080
96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2526701 2526702
MS MSD
92420834001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result %Rec %Rec Limits RED Qual
Mercury mg/kg NO
0.34 0.31 0.32
0.30 92 96 75-125 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 48

/ P ceAnalytical
/ www.pacelabs.rom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 465018
Analysis Method:
EPA 6010D
QC Batch Method: EPA 3050E
Analysis Description:
6010
MET
Associated Lab Samples: 92421239001
METHOD BLANK: 2529035
Matrix: Solid
Associated Lab Samples: 92421239001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Aluminum
mg/kg
ND
10.0
03/24/1921:23
Arsenic
mg/kg
ND
1.0
0312411921:23
Cadmium
mg/kg
ND
0,10
03/24/1921:23
Calcium
mg/kg
ND
10.0
03/24/1921:23
Copper
mg/kg
ND
0.50
03/24/19 21:23
Lead
mg/kg
ND
0.50
03/24/19 21:23
Magnesium
mg/kg
ND
10.0
03/24/19 21:23
Molybdenum
mg/kg
ND
0.50
03/24/19 21:23
Nickel
mg/kg
ND
0.50
03/24/1921:23
Potassium
mg/kg
ND
500
03/24/1921:23
Selenium
mg/kg
ND
1.0
03/2411921:23
Sodium
mg/kg
ND
500
03/24/1921:23
Zinc
mg/kg
ND
1.0
03/24/19 21:23
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2529036
Units
Spike
Conc.
LCS
Result
LCS
%Rec
% Rec
Limits
Aluminum
mg/kg
500
488
98
80-120
Arsenic
mg/kg
50
47.0
94
80-120
Cadmium
mg/kg
50
48.2
96
80-120
Calcium
mg/kg
500
470
94
80-120
Copper
mg/kg
50
50.4
101
80-120
Lead
mg/kg
50
48.1
96
80-120
Magnesium
mg/kg
500
467
93
80-120
Molybdenum
mg/kg
50
47.9
96
80-120
Nickel
mg/kg
50
48.8
98
80-120
Potassium
mg/kg
500
ND
95
80-120
Selenium
mg/kg
50
45.8
92
80-120
Sodium
mg/kg
500
479J
96
80-120
Zinc
mg/kg
50
48.5
97
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2529037
MS
92421002001
Spike
Parameter Units
Result
Conc.
Aluminum mg/kg
1530
332
Arsenic mg/kg
24.5
33.2
Cadmium mg/kg
0.22
33.2
Qualifiers
2529038
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result %Rec %Rec Limits RPD Qual
382 2330 2460 242 243 75-125 5 M1
38.2 30.0 29.5 17 13 75-125 2 M1
38.2 30.6 35.9 92 93 75-125 16
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC,
Page 9 of 48

,�F�aceAnalytical
eompacelabs.conl
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Land Application
92421239
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2529037
2529038
MS
MSD
92421002001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Dual
Calcium
mg/kg
2340
332
382
3080
3200
222
224
75-125
4 M1
Copper
mg/kg
4.3
33.2
38.2
36.3
42.5
97
100
75-125
16
Lead
mg/kg
11.7
33.2
38.2
41.7
47.4
90
93
75-125
13
Magnesium
mg/kg
208
332
382
588
656
115
117
75-125
11
Molybdenum
mg/kg
8.7
33.2
38.2
28.3
21.4
59
33
75-125
28 M1,R1
Nickel
mg/kg
3.6
33.2
38.2
33.4
39.0
90
93
75-125
15
Potassium
mg/kg
ND
332
382
445
506
97
101
75-125
13
Selenium
mg/kg
ND
33.2
38.2
7.5
8.9
23
23
75-125
16 M1
Sodium
mg/kg
560
332
382
855
913
89
92
75-125
7
Zinc
mg/kg
2.7
33.2
38.2
33.6
38.9
93
95
75-125
15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 48

— aceAnalytical e
mrwpacelabs.com
Pace Analytical Services, LLC
9800 Kineey Ave. Suite 100
Hunlersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Land Application
Pace Project No.:
92421239
QC Batch:
464999 Analysis Method: EPA 601 OD
QC Batch Method:
EPA 3010A Analysis Description: 6010 MET TCLP
Associated Lab Samples:
92421239001
METHOD BLANK: 2527185
Matrix:
Water
Associated Lab Samples: 92421239001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
ND
0,050
03/24/1917:14
Barium
mg/L
ND
0.25
03/2411917:14
Cadmium
mg/L
ND
0.0050
03/24/1917:14
Chromium
mg/L
ND
0.050
03/24/1917:14
Lead
mg/L
ND
0.025
03/2411917:14
Selenium
mg/L
ND
0.10
03/24/1917:14
Silver
mg/L
ND
0.025
03124/1917:14
METHOD BLANK: 2527581
Matrix:
Water
Associated Lab Samples: 92421239001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Arsenic
mg/L
ND
0,060
03/24/1917:20
Barium
mg/L
ND
0,25
03/24/1917:20
Cadmium
mg/1-
ND
0,0050
03/24/1917:20
Chromium
mg/L
ND
0.050
03/24/1917:20
Lead
mg/L
ND
0.025
03/24/1917:20
Selenium
mg/L
ND
0,10
03/24/1917:20
Silver
mg/L
ND
0.025
03/24/1917:20
LABORATORY CONTROL SAMPLE:
2528968
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Qualifiers
Qualifiers
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
2.5
2.4
96
80-120
2.5
2.4
95
80-120
2.5
2.4
98
80-120
2.5
2.5
98
80-120
2.5
2.3
94
80-120
2.5
2.5
99
80-120
1.2
1.2
98
80-120
Qualifiers
LABORATORY CONTROL SAMPLE:
2528969
Spike
LCS LCS % Rec
Parameter
Units
Cone.
Result % Rec Limits Qualifiers
Arsenic
mg/L
2.5
2.3 94 80-120
Barium
mg/L
2.5
2.4 97 80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, L-C.
Page 11 of 48

�?aceAnalytical
mm.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
1704)875-9092
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
LABORATORY CONTROL SAMPLE:
2528969
Spike
LCS
LCS
% Rae
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
mg/L
2.5
2.5
98
80-120
Chromium
mg/L
2.5
2.5
99
80-120
Lead
mg/L
2.5
2.4
96
80-120
Selenium
mg/L
2.5
2.5
99
80-120
Silver
mg/L
1.2
1.2
97
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2528970
2528971
MS
MSD
92421077001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Arsenic
mg/L
NO
2.5
2.5
2.5
2.4
99
98
75-125
1
Barium
mg/L
ND
2.5
2.5
2.5
2.5
98
97
75-125
1
Cadmium
mg/L
ND
2.5
2.5
2.5
2.5
100
99
75-125
1
Chromium
mg/L
ND
2.5
2.5
2.5
2.5
100
99
75-125
1
Lead
mg/L
ND
2.5
2.5
2.4
2.4
96
95
75-125
1
Selenium
mg/L
ND
2.5
2.5
2.5
2.5
101
99
75-125
2
Silver
mg/L
NO
1.2
1.2
1.2
1.2
99
99
75-125
0
Results presented an this page are in the units indicated by the "units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 48

/ AaceAnalytical
w ..pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 465037
Analysis Method:
EPA 8260D
QC Batch Method: EPA 8260D
Analysis Description:
8260D MSV TCLP
Associated Lab Samples: 92421239001
METHOD BLANK: 2529093
Matrix:
Water
Associated Lab Samples: 92421239001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
1,1-Dichloroethene
ug/L
ND
5.0
03/23/19 17:12
1,2-Dichloroethane
ug/L
ND
5.0
03/2311917:12
1,4-Dichlorobenzene
ug/L
ND
5.0
03/23/19 17:12
2-Butanone (MEK)
ug/L
NO
10.0
03/23/19 17:12
Benzene
ug/L
NO
5.0
03/23/19 17:12
Carbon tetrachloride
ug/L
NO
5.0
03/23/19 17:12
Chlorobenzene
ug/L
NO
5.0
03123/1917:12
Chloroform
ug/L
ND
5.0
03/23/19 17:12
Tetrachloroethene
ug/L
NO
5.0
03/23/19 17:12
Trichloroethene
ug/L
ND
5.0
03/23/19 17:12
Vinyl chloride
ug/L
ND
5.0
03/23/19 17:12
1,2-Dichloroethane-d4 (S)
%
96
70-130
03/23/19 17:12
4-Bromofluorobenzene (S)
%
99
70-130
03/23/19 17:12
Toluene-d8 (S)
%
101
67-135
03/23/19 17:12
LABORATORY CONTROL SAMPLE: 2529092
Spike
LCS
1-CS %
Rec
Parameter
Units
Conc.
Result
%Rec Limits Qualifiers
1,1-Dichloroethene
ug/L
50
45.1
90
70-130
1,2-Dichloroethane
ug/L
50
42.7
85
70-130
1,4-Dichlorobenzene
ug/L
50
46.6
93
70-130
2-Butanone (MEK)
ug/L
100
87.9
88
64-135
Benzene
ug/L
50
45.5
91
70-130
Carbon tetrachloride
ug/L
50
45.5
91
70-130
Chlorobenzene
ug/L
50
45.6
91
70-130
Chloroform
ug/L
50
42.7
85
70-130
Tetrachloroethene
ug/L
50
47.1
94
69-130
Trichloroethene
ug/L
50
46.2
92
70-130
Vinyl chloride
ug/L
50
45.5
91
70-131
1,2-Dichloroethane-d4 (S)
%
92
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8(S)
%
97
67-135
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2529094
2529095
MS
MSD
92421239001
Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units
Result
Conc
Conc.
Result
Result %Rec %Rec Limits RPD Qual
1,1-Dichloroethene ug/L
NO
400
400
431
433 108
108 70-154 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, U.C. Page 13 of 48

1 7PaceAnalytical
twnypacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2529094 2529095
Parameter
1,2-Dichloroethane
1,4-Dichlorobenzene
2-Butanone (MEK)
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Tetrachloroethene
Trichloroethene
Vinyl chloride
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
92421239001
Units Result
MS
Spike
Conic.
MSD
Spike
Conic.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
%Rec
Limits
RPD
ug/L
ND
400
400
370
372
93
93
70-137
0
ug/L
ND
400
400
373
397
93
99
70-133
6
ug/L
ND
800
800
747
745
93
93
60-139
0
u9/L
ND
400
400
392
431
98
108
70-151
10
ug/L
ND
400
400
410
432
102
108
70-143
5
ug/L
ND
400
400
399
408
100
102
70-138
2
ug/L
ND
400
400
395
419
92
99
70-139
6
ug/L
ND
400
400
420
411
105
103
59-143
2
ug/L
ND
400
400
414
426
103
106
70-147
3
ug/L
ND
400
400
411
425
103
106
70-156
3
%
97
97
70-130
%
101
99
70-130
%
96
101
67-135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, L-C.
Qual
Page 14 of 48

�-PaceAnalytical
nvA¢pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 464933 Analysis Method: EPA 8081E
QC Batch Method: EPA 351 OC Analysis Description: 8081 TCLP Pesticides RV
Associated Lab Samples: 92421239001
METHOD BLANK: 2524228
Matrix:
Water
Associated Lab Samples: 92421239001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chlordane (Technical)
ug/L
ND
3.0
03/25/19 10:27
Endrin
ug/L
NO
0,50
03/25/19 10:27
gamma-BHC (Lindane)
ug/L
NO
0.50
03/25/19 10:27
Heptachlor
ug/L
ND
0.50
03/25/19 10:27
Heptachlor epoxide
ug/L
ND
0.50
03/25/19 10:27
Methoxychlor
ug/L
ND
1000
03/25/19 10:27
Toxaphene
ug/L
NO
3.0
03/25/19 10:27
Decachlorobiphenyl (S)
%
122
10-138
03/25/19 10:27
Tetrachloro-m-xylene (S)
%
106
10-110
03/25/19 10:27
LABORATORY CONTROL SAMPLE:
Parameter
2528359
Units
Spike
Conc.
LCS
Result
LCS
%Rec
% Rec
Limits Qualifiers
Endrin
ug/L
1.2
1.5
120
20-134
gamma-BHC (Lindane)
ug/L
1.2
1.5
122
20-118 L1
Heptachlor
ug/L
1.2
1.4
114
20-142
Heptachlor epoxide
ug/L
1,2
1.5
121
22-133
Methoxychlor
ug/L
3.8
4.7J
124
44-150
Decachlorobiphenyl (S)
%
136
10-138
Tetrachloro-m-xylene (S)
%
118
10-110 SO
MATRIX SPIKE SAMPLE:
Parameter
2528361
Units
92421718001
Result
Spike
Conc.
MS
Result
MS
%Rec
% Rec
Limits Qualifiers
Endrin
ug/L
ND
1.2
1.5
120
21-133
gamma-BHC (Lindane)
ug/L
NO
1.2
1.5
121
24-119 MO
Heptachlor
ug/L
ND
1.2
1.3
105
16-128
Heptachlor epoxide
ug/L
NO
1.2
1.4
115
50-150
Methoxychlor
ug/L
NO
3.8
4.8J
127
50-150
Decachlorobiphenyl (S)
%
177
10-138 SO
Tetrachloro-m-xylene (S)
%
106
10-110
SAMPLE DUPLICATE: 2528360
92421396002
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Chlordane (Technical)
ug/L
NO
NO
Endrin
ug/L
NO
NO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC. Page 15 Of 48

No
aceAnalytical
� wvnvpacelebs.cem
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
SAMPLE DUPLICATE: 2528360
Parameter
Units
92421396002
Result
Dup
Result RPD Qualifiers
gamma-BHC (Lindane)
ug/L
ND
ND
Heptachlor
ug/L
ND
ND
Heptachlor epoxide
ug/L
ND
ND
Methoxychlor
ug/L
ND
ND
Toxaphene
ug/L
ND
ND
Decachlorobiphenyl(S)
%
111
99 12
Tetrachloro-m-xylene (S)
%
108
94 14
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, L-C. Page 16 of 48

PaceAnalytical
mmpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 25022
Analysis Method: EPA 8151A
QC Batch Method: EPA S151A
Analysis Description: 8151
GCS TCLP Herbicides
Associated Lab Samples: 92421239001
METHOD BLANK: 110905
Matrix: Water
Associated Lab Samples: 92421239001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
2,4,5-TP (Silvex)
mg/L
NO 0,010
03/25/19 19:41
2,4-D
mg/L
NO 0.0050
03125/1919:41
2,4-DCAA (S)
%.
89 10-155
03/25/19 19:41
METHOD BLANK: 111550
Matrix: Water
Associated Lab Samples: 92421239001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
2,4,5-TP (Silvex)
mg/L
NO 0,010
03/25/19 20:02
2,4-D
mg/L
NO 0,0050
03/25/19 20:02
2,4-DCAA (S)
%.
80 10-155
03/25/19 20:02
METHOD BLANK: 112131
Matrix: Water
Associated Lab Samples: 92421239001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
2,4,5-TP (Silvex)
mg/L
NO 0.010
03/25/19 20:24
2,4-D
mg/L
ND 0.0050
03/25/19 20:24
2,4-DCAA (S)
%.
66 10-155
03/25/19 20:24
LABORATORY CONTROL SAMPLE: 112852
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
2,4,5-TP (Silvex)
mg/L
2 1.6
80 39-138
2,4-D
mg/L
2 1.4
70 29-145
2,4-DCAA (S)
%.
88 10-155
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 112853
112854
MS MSD
92420545014
Spike Spike MS
MSD MS MSD
%Rec
Parameter Units
Result
Conc. Conc. Result
Result %Rec %Rec
Limits RPD Qual
2,4,5-TP (Silvex) mg/L
NO
2 2 1.6
1.6 80 82
10-156 2
2,4-D mg/L
ND
2 2 1.4
1.5 72 74
10-156 3
2,4-DCAA(S) %.
84 86
10-155
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, L-C.
Page 17 of 48

aceAnalytical
vnrvipacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite t 00
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 465141 Analysis Method: EPA 8270E
QC Batch Method: EPA 3510C Analysis Description: 8270E TCLP MSSV
Associated Lab Samples: 92421239001
METHOD BLANK: 2524228
Associated Lab Samples: 92421239001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,4-Dichlorobenzene
ug/L
NO
50.0
03/25/19 13:16
2,4,5-Trichlorophenol
ug/L
ND
50.0
03/2511913:16
2,4,6-Trichlorophenol
ug/L
NO
50.0
03/25/19 13:16
2,4-Dinitrotoluene
ug/L
NO
50.0
03/2511913:16
2-Methylphenol(o-Cresol)
ug/L
NO
50.0
03/2511913:16
3&4-Methylphenol(m&p Cresol)
ug/L
ND
50.0
03/25/19 13:16
Hexachloro-1,3-butadiene
ug/L
ND
50.0
03/2511913:16
Hexachlorobenzene
ug/L
ND
50.0
03/25/19 13:16
Hexachloroethane
ug/L
ND
50.0
03/25/19 13:16
Nitrobenzene
ug/L
ND
50.0
03/25/19 13:16
Pentachlorophenol
ug/L
ND
100
03/25/19 13:16
Pyridine
ug/L
ND
50.0
03/25/19 13:16
2,4,6-Tribromophenol (S)
%
57
27-108
03/25/19 13:16
2-Fluorobiphenyl (S)
%
46
13-107
03/25/19 13:16
2-Fluorophenol (S)
%
39
10-110
03/25/19 13:16
Nitrobenzene-d5 (S)
%
52
12-102
03/25/19 13:16
Phenol-d6 (S)
e/
28
10-110
03/25/19 13:16
Terphenyl-d14 (S)
%
90
21-132
03/25/19 13:16
LABORATORY CONTROL SAMPLE:
Parameter
2529353
Units
Spike
Conic.
LCS
Result
LCS
%Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
500
178
36
30-130
2,4,5-Trichlorophenol
ug/L
500
191
38
40-130 L2
2,4,6-Trichlorophenol
ug/L
500
198
40
40-130
2,4-Dinitrotoluene
ug/L
500
313
63
49-130
2-Methylphenol(o-Cresol)
ug/L
500
186
37
30-130
3&4-Methylphenol(m&p Cresol)
ug/L
500
171
34
20-130
Hexachloro-1,3-butadiene
ug/L
500
152
30
10-130
Hexachlorobenzene
ug/L
500
263
53
30-130
Hexachloroethane
ug/L
500
148
30
10-130
Nitrobenzene
ug/L
500
181
36
20-130
Pentachlorophenol
ug/L
1000
420
42
10-140
Pyridine
ug/L
500
78.9
16
10-130
2,4,6-Tribromophenol (S)
%
65
27-108
2-Fluorobiphenyl(S)
%
38
13-107
2-Fluorophenol(S)
%
32
10-110
Nitrobenzene-d5 (S)
%
42
12-102
Phenol-d6 (S)
%
23
10-110
Terphenyl-d14 (S)
%
87
21-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Anaytical Services, LLC. Page 18 of 48

. �aceAnalXical o
wwwpacelabs.com
Pace Analytical Services, LLC
9800 Kmcey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 463640 Analysis Method. ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92421239001
SAMPLE DUPLICATE: 2522273
92421203011 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 69.7 67.3 3
SAMPLE DUPLICATE: 2522274
92421239001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 20.3 19.4 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC, Page 19 of 48

�I^
/ �aceAnalytical
Vnvw.pacelahs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 463530 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92421239001
SAMPLE DUPLICATE: 2521716
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2521717
Parameter
pH at 25 Degrees C
92420457002 Dup
Units Result Result RPD Qualifiers
Std. Units 4.3 4.3 0 H1
92421108002 Dup
Units Result Result RPD Qualifiers
Std. Units 12.1 12.1 0 E,H1
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LILC. Page 20 of 48

aceAnalytical0
vnvw.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 463836
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92421239001
METHOD BLANK: 2522994
Matrix: Solid
Associated Lab Samples: 92421239001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/kg
ND 8.8
03/19/1914:54
LABORATORY CONTROL SAMPLE: 2522995
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
%Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg
446 450
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2522996 2522997
MS MSD
7081680001
Spike Spike MS
MSD MS MSD %Rec
Parameter Units Result
Conc. Conc Result
Result %Rec %Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 2840
1920 1720 3500
3710 34 50 90-110 6 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 48

-PaceAnalytical o
/ wvnvpacelabscom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 464291 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Associated Lab Samples: 92421239001
METHOD BLANK: 2524971
Associated Lab Samples: 92421239001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
LABORATORY CONTROL SAMPLE: 2524972
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
NO 38.5 03/21/1900:43
Spike LCS LCS %Rec
Conic. Result % Rec Limits Qualifiers
690 684 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2524973
2524974
MS
MSD
92420605002 Spike
Spike
MS MSD MS
MSD % Rec
Parameter Units Result Cone.
Cone.
Result Result % Rec
% Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 36400 12800
9990
53600 38300 134
19 90-110 33 M1,R1
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, -LC.
Page 22 of 48

ff
PaceAnalytical
"mpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 463486 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92421239001
METHOD BLANK: 2521522
Matrix:
Solid
Associated Lab Samples: 92421239001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND
4.0
03/15/1902:51
Nitrogen, Nitrite
mg/kg
ND
4.0
03/15/1902:51
Nitrogen, NO2 plus NO3
mg/kg
ND
4.0
03/15/19 02:51
LABORATORY CONTROL SAMPLE:
2521523
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
15
14.9
99 90-110
Nitrogen, Nitrite
mg/kg
10
10.2
102 90-110
Nitrogen, NO2 plus NO3
mg/kg
25
25A
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2521524
2521525
MS
MSD
92421077001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
NO
25.7
25.5
25A
27.4
98
107
90-110
9
Nitrogen, Nitrite
mg/kg
NO
17.1
17A
18.4
16.0
103
90
90-110
14 R1
Nitrogen, NO2 plus NO3
mg/kg
NO
43
42.7
43.5
43.4
101
101
90-110
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 48

1117-PaceAnalytical
wviw.pacelabs.crom
Pace Analytical Services, LLC
98001,incey Ave. Suite100
Huntersville, NC 28078
(704)87e-9092
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 464438
Analysis Method: EPA
365.1 Rev 2.0 1993
QC Batch Method: EPA 366.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92421239001
METHOD BLANK: 2525762
Matrix: Solid
Associated Lab Samples: 92421239001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phosphorus mg/kg
ND 1.0
03/20/1923:31
LABORATORY CONTROL SAMPLE: 2525763
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Phosphorus mg/kg
50 52.0
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2525764 2525765
MS MSD
92421077001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Cone. Cone. Result
Result %Rec %Rec Limits RPD Qual
Phosphorus mglkg 2000
70.5 81 2720
1880 1020 -143 90-110 36 M6,R1
Results presented on this page are in the units indicated by rho "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 48

f�aceAnalytical
/ vrvi✓eAacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Humersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 334279 Analysis Method: EPA 9014
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 92421239001
METHOD BLANK: 1626779
Associated Lab Samples: 92421239001
Parameter Units
Cyanide, Reactive mg/kg
LABORATORY CONTROL SAMPLE: 1626780
Parameter Units
Cyanide, Reactive mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.99 03/19/1918:07
Spike LCS LCS %Rec
Conic. Result % Rao Limits Qualifiers
99.9 NO 0 0-8
SAMPLE DUPLICATE: 1626781
30284245001 Dup
Parameter Units Result Result
Cyanide, Reactive mg/kg ND ND
RED Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 48

aceAnalytical
aww.pecelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Land Application
Pace Project No.: 92421239
QC Batch: 334278 Analysis Method: SM 450oS2F-00
QC Batch Method: SW-846 7.3.4.2 Analysis Description: 734S Reactive Sulfide
Associated Lab Samples: 92421239001
METHOD BLANK: 1626776
Associated Lab Samples: 92421239001
Parameter Units
Sulfide, Reactive mg/kg
LABORATORY CONTROL SAMPLE: 1626777
Parameter Units
Sulfide, Reactive mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 9.9 03/19/1917:12
Spike LCS LCS % Rec
Conic. Result % Rec Limits Qualifiers
200 44.0 22 0-52
SAMPLE DUPLICATE: 1626778
30284245001 Cup
Parameter Units Result Result
Sulfide, Reactive mg/kg ND ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 48

f aceAnalytical
� �rw,vpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Land Application
Pace Project No.: 92421239
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical Services - Asheville
PASI-C
Pace Analytical Services - Charlotte
PAST -GA
Pace Analytical Services -Atlanta, GA
PASI-PA
Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
H1 Analysis conducted outside the EPA method holding time.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M7 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifcations is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent or Pace Analytical Services, LLC, Page 27 of 48

PaceAnalytical
r�vxpacela6s.corn
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Land Application
Pace Project No.: 92421239
ANALYTE QUALIFIERS
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/28/2019 06:56 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 48

/ ,Pal ceAnalytical
rrvnvpacelebs.com
Pace Analytical Services, LLC
9800 kincey Ave. Suite 100
I luntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Land Application
92421239
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92421239001
Stock Pile
Residual Solids
EPA 3510C
464933
EPA 8081 B
465120
92421239001
Stock Pile
Residual Solids
EPA8151A
25022
EPA 8151A
25081
92421239001
Stock Pile
Residual Solids
EPA 3050B
465018
EPA 6010D
465056
92421239001
Stock Pile
Residual Solids
EPA 3010A
464999
EPA 6010D
465053
92421239001
Stock Pile
Residual Solids
EPA 7470A
465000
EPA 7470A
465052
92421239001
Stock Pile
Residual Solids
EPA 7471B
464634
EPA 7471B
464739
92421239001
Stock Pile
Residual Solids
EPA 3510C
465141
EPA 8270E
465204
92421239001
Stock Pile
Residual Solids
EPA 8260D
465037
92421239001
Stock Pile
Residual Solids
SM 2540G-2011
463841
92421239001
Stock Pile
Residual Solids
ASTM D2974-87
463640
92421239001
Stock Pile
Residual Solids
EPA 9045D
463530
92421239001
Stock Pile
Residual Solids
SM 2710B-2011
465999
92421239001
Stock Pile
Residual Solids
EPA 350.1 Rev 2.0 1993
463836
EPA 350.1 Rev 2.0 1993
463919
Mod.
Mod.
92421239001
Stock Pile
Residual Solids
EPA 351.2 Rev 2.0 1993
464291
EPA 351.2 Rev 2.0 1993
464477
92421239001
Stock Pile
Residual Solids
EPA 353.2 Rev 2.0 1993
463486
EPA 353.2 Rev 2.0 1993
463489
92421239001
Stock Pile
Residual Solids
EPA 365.1 Rev 2.0 1993
464438
EPA 365.1 Rev 2.0 1993
464473
92421239001
Stock Pile
Residual Solids
SW-846 7.3.3.2
334279
EPA 9014
334475
92421239001
Stock Pile
Residual Solids
SW-846 7.3.4.2
334278
SM 4500S2F-00
334467
Date: 03/28/2019 06:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent or Pace Analytical Services, LLC.
Page 29 of 48

Document Name: Document Revised: February 7, 2018
sample Condition U on RecelpCU tR) Page 1 of 2
aceARapicalP Document No.: Issuing Authority:
F•CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
........... .
Client Name:
Project
Courier: ❑F Ex ❑UPS ❑USPS []Client
❑ Commercial ace ❑Other: ___
Custody Seal Present? ❑Yes No Seals Intact? ❑Yes ❑ No
Packing Material: ❑Bubble Wrap 36,bbl, Bags ❑None Other
Thermometer• 92T048 rypaosice: wet ❑slue
R Gun ID:
Cooler Temp (°C): S5: ) Correction Factor: Add/Subtract (°C) 0.0
Cooler Temp Corrected ('C)°C));
USDA Regulated Soil ( VJA, water sample)
Did samples o�inta in a quarantine zone within the United States: CA, NY, or SC (check maps)?
W®#:92421239
92421239
Date/Initials Parson Examining Contents: �+^' ✓ /���
Biological Tissue rr n?
❑Yes []No/A
❑None
Temp should be above freezing to 6"C
❑Samples out oftemp critarla. Samples an ice, cooling process
has begun
Did samples originate from a foreign source (intnaliy,
i..A..dinn W.— i and Puerto Riml? f IYCS MNO
Comments/Discrepant :
Chain of CustbdV Present?
Yes
[]NO
N/A
1.
Samples Arrived within Hold Time? .
es
No
❑N/A
2.
Short Hold Time Analysis <72 hr.)?
❑Yes
060
❑N/A-
3.
Rush Turn Around Time Requested?
QYes
rtd<
❑N/A
4.
Sufficient Volume?
2<1
❑Na
NA
S.
Correct Containers Used?
-Pace Containers Used?
de
es
[IN.
MNO
❑N/A
❑N A
6.
Containers Intact?
C3 es
No
❑N
7.
Dissolved analysis: Samples Field Filtered?
❑ye
[]No
N/A
8. —_
Sample Labels Match COC7
-Includes Date/Time/ID/Analysis Matrix:-
es
L
El No
❑N/A
9.
Headspace In VOA Vials (>5-6mm)7
❑Ye
No
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
HT:❑No
OYes
No
//A/
061A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ONO
Person contacted:
Date/Time:
Project Manager SCURF Review:. - Dale:
Project Manager SRF Review: Date:e
Page 30 of 48

e
dC2A17fIjICB%
Document Name: J
Sample Condition Upon Receipt{SOUR)
Document Revised: February 7, 201a
Page 1 Of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Autfiarity:
Pace Carolinas Quality OfRce
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Gil and Grease, DRO/8015 {water) DOC, LLH8
**Bottom half of box is to list number of bottle
Project I WO# : 92421239
PM: MWB Due Date: 03/28/19
CLIENT: 92—Interface
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12
PH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Timepreservation
adjusted
Amount of Preservative
added
Lot
Note: Whenevesthereis a discrepancy affecting North Carolina compliance samples, a copyofthis formwlll hesentio the North Carolina DF.HNR Cenihcation Office (i.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 31 of 48

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aceAnalyticalANALYTICAL R E P O R T
nc..=icnmc o rtrp 3In,mx"" March 28, 2019
Pace Analytical - Huntersville, NC
Sample Delivery Group:
L1082700
Samples Received:
03/27/2019
Project Number:
92421239
Description:
Land Application
Site:
001
Report To: Matthew Brainard
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By
'`A� L9"�V'—
Nancy McLain
Project Manager
R1,SUl'5 relate only to the bn1S tested of calart ated and die reported as rounded values. f is lest report shall no; be
reproduced. except in full, without mitten approval of the laboratory. Where applicable, sampling conducted by Par( National
is pe:r0mmatl Pei gwdonce provided in laboram:y standard opeia6ng pmcedaes 060302, 060303, and 060304
s:

I ABLE C)I CON I L-N I S
Tc'iablc of Contents 2 .........
Ss: Sample Summary 3 e
Cn: Case Narrative 4
Sr: Sample Results 5 iSS
STOCK PILE RESIDUAL SOLIDS L1082700-01 5 a
Oc: Quality Control Summary 6
Total Solids by Method 2540 G-2011 G
Wet Chemistry by Method D93/1010A 7
GI: Glossary of Terms 8 C <
AI: A.ccr: c; itr.ti::ns A L1Jc MTQ11`i 9
'GI
SC: Sample Chain of Custody 10
Page 35 of 48
ACCOUNT: PROJECT'. SDG: DATEMME: PAGE:

SAMPLE SUMMARY
Colloctod by
ON[ I.."R NP. I:OiV:4DI, 47,
STOCK PILE RESIDUAL SOLIDS 11082700-01 .Solid
Method Batch Diludon Preparation
Total Solids by Method 2540 G-2011
Wet Chemistry by Method D93/1010A
date/1Inu9
WG1256276 1 03/27/1912:56
W G1256278 1 03/28/1914:40
Colhvmd d,it, tw!r Row,'md ddAUmt
03114i19 07:30 Q �2:%%i90G4E.
Analysis
Analyst
Location
date/time
03/27/1913:16
JD
Mt. Juliet, TN
0312811914:40
JD
Mt. Juliet, TN
h
L c
ACCOUNT: PROJECT: GOO.
Page 36 of 48
DATE/TIME: PAGE:

CASE NARRA I IVl_
'JNE V-nO ll' c
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding tirnes, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor Used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results, By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
I,
Nancy McLain
Project Manager
E
E
I
Sr
C<
GI
1. -
C
ACCOUNT: PROJECT: SDG:
DATErrIME:
Page 37 of 48
PAGE:

JIU(.K PILE HtJIUUAI- JULIUJ
Collected datelllnie: 03/14H9 07:30
Total Solids by Method 2510 G-.7_011
SAMPLE HI=SUL
L1082700
IS - 01
ONES<vJ.�inrioi,r,Nloe
Result Qualifier
Dilution Analysis
Batch
Analyte %
date I tnne
Totol Solids 80.0
1 03127/2019 13 16
ul)jQ7E
Wet Chemistry by Method D93/101OA
3Ss
Result Qualifier
Dilution Analysis
Batch
Analyte Deg. F
date I time
"
Ignitabillty DNI at 170
i 03/28/201914.40
t-l6125 6278
QC
GI
:Sc
F�
Page 38 of 48
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:

[f] W. 11 -�
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GLUSSAHY UI- 1 LRMS
Guide to Reading and Understanding Your Laboratory Re):)oit
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have add ltlonal questions please contact your project representative.
Abbreviations and Definitions
-
MDL
Method Detection Limit
RDL
Reported Detection Limit.
�SS
Pee.
Recovery.
RPD
Relative Percent Difference.
n
SDG
Sample Delivery Group.
Cr
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analyses
reported.
BSI
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analyses in the sample are higher than the highest Irmit of concentration that the
-
laboratory can accurately report, the sample may be diluted for analysis- If a value different than 1 is used in this field, the
_
-result reported has already been corrected for this factor_
C
These are the target % recovery ranges or W. difference value that the laboratory has historically determined as normal
—
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Ongupal Sample
the prep bateh used to determineRelative Percent Difference (RPD) from a quality control
then
sample. The trial Sale mple. included the e
p 9 P Y p SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
>•,I
Qualifier
reported. If a Qualifier is presenC a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
Ie
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (on)
observed either at sample receipt bythe laboratory from the field or during the analytical process. If present there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were Initially collected. This is used to venfy the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your sarnples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis-
Quahfi(-i
Description
The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG.
ACCOUN"C PROJECT: SDG.
Page 41 of 48
DATE/TIME: PAGE:

ACCKFUI I A I TUNS & LUCA I TUNS
Pace National is the only enwromnenlal laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the counlly Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories In out industry, The most s19nt6cant benefit to our one location design is the design of out laboratory (outputs. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample magrite Our focus on premium quality and prompt service allows us to be Y0UR IAB OF CHOICE.
'Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation 1s only applicable to the test methods specified on each scope of accreditation held by Pace National
Alabama
40660
Nebraska
NE-OS-15�05
Alaska
17-026
Nevada
TN 03-2002.-34
Arizona
A20612.
New Hampshire
2975
Arkansas
88-0469
New Jersey-NELAP
TN002
California
2932
New Mexico
me
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
Noun Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
kniume
C TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68 02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky "
90010
South Carolina
84004
Kentucky °
16
South Dakota
the
Louisiana
A130792
Tennessee 'a
2006
Louisiana'
LA180010
Texas
T104704245-18 IS
Maine
TN0002
Texas s
LAB0152
Maryland
324
Utah
TN00003
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CER10086
Wyoming
A2LA
"A2LA— ISO 17025
1461.01
All IA-L AP,U.0 EM LAP
100789
A2LA— ISO 17025 `-
1461,02
DOD
1461,01
Canada
146101
USDA
P330-15-00234
EPA—Crypto
TN00003
`Drinking Water ° Underground
Storage lanks ' Aquatic Toxicity
4ChemicaUlaicrobiological sMold "Wastewater n/a Accreditation not applicable
Pace National has sixty four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing adopt central laboratory.
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Page 42 of 48
PAGE:
ACCOUNT: PROJECT: SDG'.
DATE/TIME:

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Analytical Results
Pace Analytical
9800 Kincey Suite
100
Huntersville, NC 28078
Receive Date:
03/14/2019
Reported:
03/18/2019
For:
Stock Pile
Residual
Comments:
Geometric
Mean
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
190314-14-01
Fecal Coliforms
1
<24
MPN/g
SM92210E-2006
03/14/2019
WC
190314-14-01
Percent Solids
1
83.1
ova
SWWB-2011
03/14/2019
WC
190314-14-02
Fecal Coliforms
2
<26
MPN/g
SM92210E-2006
03/14/2019
WC
190314-14-02
Percent Solids
2
77.3
%
SM2540B-2011
03/14/2019
WC
190314-14-03
Fecal Coliforms
3
<26
MPN/g
SM92210E-2006
03/14/2019
WC
190314-14-03
Percent Solids
3
80.3
%
SM2540B-2011
03/14/2019
WC
190314-14-04
Fecal Coliforms
4
<25
MPN/g
SM92210E-2006
03/14/2019
WC
190314-14-04
Percent Solids
4
79
%
SM2540B-2011
03/14/2019
WC
190314-14-05
Fecal Coliforms
5
<25
MPN/g
SM92210E-2006
03/14/2019
WC
190314-14-05
Percent Solids
5
79
%
SM2540B-2011
03/14/2019
WC
190314-14-06
Fecal Coliforms
6
<24
MPN/g
SM92210E-20M
03/14/2019
WC
190314-14-06
Percent Solids
6
84
ova
SM254OB-2011
03/14/2019
WC
190314-14-07
Fecal Coliforms
7
<24
MPN/g
SM92210E-200e
03/14/2019
WC
190314-14-07
Percent Solids
7
82
%
SM25408-2011
03/14/2019
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cent #37755,
EPA #NC00909
PO Box 228 e Statesville, NC 28687--704/872/4697
Page 1 Rage 45 of 48

Condition of Receipt
Sample Number 190314-14-01 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190314-14-02 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190314-14-03 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190314-14-04 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190314-14-05 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190314-14-06 Temp on Arrival: 3.3
PO Box 228 a Statesville, NC 28687 ^ 704/872/4697
Page 2 wage 46 of 48

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 190314-14-07 Temp on Arrival: 3.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 0 704/872/4697
Page 3 gage 47 of 48

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Page 4 Pfa'ge 48 of 48

Willcox & Mahe Soil Solutions, PLLC
Summerfield, North Carolina
RESIDUAL PAN CALCULATION
Duvaltex (US), Inc.
TKN= 7,980 mg/kg
NH3= 12 mg/kg
NO3-NO2-N= 5 mg/kg
Min Rate= 0.30
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO21
0.30 7,968 6
PAN= 2401.36 mg/kg
5.00
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N]
0.15 7,968 2,390
PAN= 836.66 mg/kg remaining from I st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N]
0.08 5,578 837
PAN= 379.29 mg/kg remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N]
0.05 4,741 379
PAN= 218.09 mg/kg remaining from 1st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N]
0.03 4,362 218
PAN= 120.46 mg/kg remaining from I st year application
Residual PAN from years 2 thru 5 after the initial application = 1554.49 mg/kg
Application
Method
First Year PAN
m /k
Five Year Maximum
Adjusted PAN
Surface
2,401
3,956

SAR
SAR Calculation
Na mg/I
Ca mg/I
Mg mg/I
305.251
4885.61
1187.53
Na Ca Mg SAR
13.272 244.281 98.961 r-71-01-3--j
Na mil eq
Ca mil eq
Mg mil eq
13.272
244.281
98.961
Enter
Enter .% TS
79.7
Data
Na mg/kg
383
Ca mg/kg
6130
Mg mg/kg
1490
Job Name: 'Duvaltex WWTP
Page 2

LASC FORM

§� State of North Carolina
a ,' Department of Environmental Quality
Division of Water Resources
Division of Water Resources LAND APPLICATION SITE CERTIFICATION
INSTRUCTIONS FOR FORM: LASC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non Discharge Permitting Unit
General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include
water treatment plant of other type residuals) in accordance with 15A NCAC 02T_ 1100. Do not submit this certification for review
without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Application Site Certification (FORM: LASC 06-16):
® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please
do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments
to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
® For new or renewed permits, submit the requested information for all land application sites.
❑ For modified permits, submit the requested information fat o� those sites that are new, transferred or affected by the
proposed modification.
B. Land Application Site Information:
® The status of the land application site with respect to this residuals land application program must be provided in table I. The
status categories and their corresponding codes are as follows:
♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D)
❑ Attach the following in accordance with each status code:
Status Code
Required Item
N
R
T
M
�41
County Board
Notification. doc
Land Owner
Agreement
(if applicable)
Setback Waiver
Agreement
An updated vicinity/setback map in accordance with the Map Guidance
✓
�
lot RestickHls Land Application Permits"
✓
✓
A soils and agronomic evaluation in accordance with the "Soil Scientist
✓
Fvaluation PollOr"
INSTRUCTIONS FOR FORM: LASC 06-16 Page I of 3

An updated accounting of the land application sites cumulative
ollutant loading rates (CPL,Rs) _ _---- _
Status Code
Required Item
—""�-���
N
�"��—"
R
T
M _
For previously permitted sites without a soil series name indicated in the
Attachment B, submit County Soil Survey Map (or equivalent) clearly
indicate the location of the land application site and in accordance with
the soil map requirements in the "Soil Scientist Evaluation Policy"
Acknowledgement of field transfer from Land Owner (Fields may not
be permitted to multiple Permittees over the same time period)
This item may be required for land application site with a status code "M", please contact the Division if you need assistant in
determining attachment requirements.
® Crop Type should include the most likely crop types for the life of the permit (five years).
® Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or
name of the soil series as provided by the licensed soil scientist.
® Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each
site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please
note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct
mapping unit. If a representative slope is provided, it must be determined accordingly:
® For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides
information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope
by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8%
would have a representative slope of 6%.
❑ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist.
® Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as
follows:
• Address Matching (ADD)
• Aerial Photography with Ground Control (AER)
• Cadasual Survey (SUR)
• Conversion from Coordinate Plane (CP)
• Conversion from Township -Section -Range (TSR)
• Conversion from Universal Trans Mere (UTM)
• Map Interpretation by Digital or Manual Extraction (MAP)
C. Waterbody and Classifications Information: (new sites only)
• Digital or Raw Photo Extraction (EXT)
• Geodetic Quality GPS Survey (CEO)
• LORAN-C Navigation Device (LOR)
• Navigation Quality GPS (GPS)
• Remote Sensing (RS)
• Zip Code Centroid (ZIP)
❑ Use an 8.5 by I I -inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the
residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each
map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality.
❑ Surface water body classifications information may be found at: littl):,/(Ieq,iic.gov/,,ibotit/divisjoiis,watei-
i esources/planning/class ification slandai ds/c lassi ficati oils
❑ Any questions concerning the waterbody and its classification, please contact the Division's regional offices.
❑ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at:
littl)://dcq nc gov/contacthrogional-offices
❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned
subbasins, location descriptions, stream index numbers and established classifications.
I. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area
should be submitted with the permit application regardless of whether a Stream classification was completed).
2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see
Table I: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as
"UT to slreanv name" as the waterbody name.
3. Open the link http;//deq.ne gov_/about/divisions/water-reso(irces/plannmg/classiticatioiistandards/classificatioi)s.
❑ Stream Classification Process: One of the options below may be used depending on the known initial project information.
❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED
1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide
the proper location descriptions if multiple runs.
INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3

2. Locate the name of the identified waterbody (from General Directions) on the list.
3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term
"source" in the description means the beginning of the waterbody segment (most upstream point).
4. Record all Basins, Stream Index Numbers and Classifications applicable to the project.
❑ KNOWN COUNTY WHERE; CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED
1. Select the proper county from the List all Waterbodies in county, hydrologically report.
2. Locate the name of the identified waterbody (from General Directions) on the list.
3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term
"source" in the description means the beginning of the waterbody segment (most upstream point).
4. Record all Basins, Stream Index Numbers and Classifications applicable to the project.
❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED
1. Use the Clickable basin map to hydrologically sorted list report.
2. Click on the approximate project location to bring up the hydrologically sorted list.
3. Locate the name of the identified waterbody (from General Directions) on the list.
4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term
"source" in the description means the beginning of the waterbody segment (most upstream point).
5. Record all Basins, Stream Index Numbers and Classifications applicable to the project.
❑ Notes on index number and unnamed streams:
Unnamed Streams 15A_NCAC 02B 0301(i).
❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned
to the stream segment to which it is tributary (at the point of entry) except:
(A) unnamed streams specifically described in the schedule of classifications;
(B) unnamed freshwaters tributary to tidal saltwaters will be classified "C'; or
(C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by
approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted.
❑ The following river basins have different policies for unnamed streams entering other states m for specific areas of the
basin:
Unnamed Tributaries Entering Other States or for Specific Basin Areas
Hiwassee River Basin
Streams entering Georgia m Tennessee shall be classified "C Ti."
Little Tennesse River
Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah
Basin And Savannah
River drainage area entering South Carolina shall be classified "B Tr."
River Drainage Area
French Broad River
Basin
__
Streams entering Tennessee will be classified "B."
Watauga River Basin
Streams entering the State of Tennessee are classified "C." _ —
Broad River Basin
Streams enteri�LSouth Carolina are classified "C. _
New River Basin
Streams entering the State of Tennessee are classified "C." —
--
Catawba River Basin
---- — ---
Streams entering South Carolina are classified 'C."
Yadkin -Pee Dee River
Streams entering Virginia are classified "C," and such streams entering South Carolina are
Basin
classified "C."
Lumber River Basin
Streams entering South Carolina are classified "C Sw."
Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr
Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or
Roanoke River Basin
described shall carry the classification "B," and all backwaters of Lake Gaston and the North
Carolina portion of streams tributary thereto not otherwise named or described shall carry the
classification "C and B."
Chowan River Basin
Streams entering Virginia are classified "C." _
Tar -Pamlico River
All drainage canals not noted in the schedule are classified "C Sw." except the main drainage
Basin
canals to Pamlico Sound and its bays which shall be classified "SC "
Pas uotank River Basin
All drainage canals not noted in the schedule are classified "C."
INSTRUCTIONS FOR FORM: LASC 06-I6 Page 3 of 3

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UPDATED SITE MAPS
LANDOWNER AGREEMENT FORMS
SOIL SAMPLE RESULTS

Division of Water Resources
hate of worth t„arouna
Department of Environmental Quality
Division of Water Resources
1 SA NCAC 02T .1100 - LAND OWNER AGREEMENT
FORM: LOA 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one orieinai and two conies of the application and
supporting documentation
For more in1b)-mation, visit the Water Quality Permitting Section's Non-/Jiscli�n��a 1'ermittine C/nit
General This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of
Class B residuals (may include water treatment plant or other type residuals) in accordance with 1 SA Do not submit
this agreement for review without a corresponding application form (FORM: RLAP 06-16).
Unless othenvise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Owner Agreement (FORM: LOA 06-16):
Q� Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the
Applicant.
A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND
The undersigned landowner
or his representative hereby permits:
y �
Applicant's name: t_JA-e-" ��`�� ..S_wc_, - —
hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land
application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this
Agreement:
Site/Field ID
Lease
(yes/no)
Land Use or
Cropping Patterns
Intended Use of Crops
Residuals Source
(optional)
Special note
(no-till/over-seed.'
pasture)
V " 1 ` �
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/ "C- (-.iA %
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t�
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The landowner or his representative receives, in consideration, fall use of the nutrient value of the applied residuals while the
Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and
shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and
Stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement.
FORM: LOA 06-16 Page I of t

1. STIPULATIONS:
1. The landowner or his representative shall not enter into any additional rostduats application contracts ce agreements with another pennitted
entity for the sites) specified by this Agreement.
2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to it third party, the landowner shall
be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement.
3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 1p are met.
4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDFNR-DWR, Non -Discharge Permitting Unit, 1617 Mail
Service Center, Raleigh, NC 27699-1617,
S. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new
landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land
application site(s).
6. The Permittee has provided the landowner or his representative with information and data concerning the residuals lard application progrann,
including an analysis of constiluents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the
equipment used by the Permince.
7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land
application event and a copy of the results of each soil analysis.
8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve it final soil
PH of at least 6.0, unless air agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the
specified crop.
9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of
soil samples, and the permitted application limits.
10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis ofother sources of nutrients
(e.g., fertilizer, tavegulated animal waste, etc.) that have been applied to the land application sne(s).
11. The landowner or his representative will inform the Pennince of any revisions or modifications to the intended use and cropping patterns for
the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application
events at appropriate periods.
12. Specific residuals land application area boundaries shall be clea9y marked on the land application site(s) by the Permittee, the landowner, or
his representative prior to and during a residuals land application event.
13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and
inspect any property, premises, or place on or related to the land application sites) at any reasonable time for the purpose of determining
compliance with the permit; establish monitoring facilities on or near the land application sites) as required by the permit; copy any records
that must be kept under the terms and conditions of the permit; take necessary leachac, surface water, groundwater, or soil samples during the
term of, and 12 months after termination of, this Agreement.
11. RESTRICTIONS:
1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application
site(s) during active use and for the 12-nnontlr period following a residuals land application event. Such controls mury include the posting of
signs that indicate the activities being conducted at the land application site(s).
2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application
sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application
events.
3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event.
4. Food crops with harvested parrs that touch the residuals;soil mixture and are totally above the land surface shall not Inc harvested Cota 14-month
period following a residuals land application event.
5. Food crops with harvested parrs below the surface of the land shall not be harvested for a 20-month period following a residuals land application
event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil.
6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application
event when the residuals remain on the land surface for less than four months prior to incorporation into the soil.
T Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event.
IILALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one)
15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, i A N( 4C Q _}_ t. r 05(yn allows the compliance
boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided
the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following;
❑ A re -defined compliance boundary is needed for field(s) ID:
(Please include the rationale forthe requested re -location of the compliance boundary and attach a map showing the newly proposed compliance
boundary to the application package)
® A re -defined compliance boundary is not needed for this site.
IN'. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed)
❑ The land application field(s) ID: . is currently permitted under another
residuals land application progrun; Penult Number WQ: - The land owner hereby acknowledge that by signing this
agreement, he/she is requesting that the ftcld(sl be removed from the previously permitted residuals land application program and transferred
into the new program;
(Name of the new program)
FORM: LOA 06-16 Page 2 of

Landowner's Certification:
I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions
regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through
a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the
deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or
agreement with another municipality, contractor, or other pennitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of
field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified
herein.
Landown
Address:
City: cv �! I tr State: _ 1//C _ Zip: ,4-0-)o
Phonc: �.�=�,1 /tr..�r•�-is/a)l E-mail address: _
Signature: Date:
Date:
NORTHCAROLINA,., IkZ—�,_______..____ COUNTY
1, the undersigned Notary Public do hereby certify that _____ ki .AA,z
personally appeared before nre this day and acknowledged the due execution of the forgoing instrument.
WITNESS my hand and official seal this the _S-22'L_}y`__-,_
Signature and seal:
My commission expires: �-'D t fir'
Lessee's/Operator's Certification:
i
LA
When County, Ntxth
I certify that 1 have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Lessee -operator name
Address:
City:
Phone:
Signature:
Permittee's Certification:
State:
F-mail address:
Date:
Zip:
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Signing official name: _14"e.-jY-D� e
Signature: Z�iz6--.;�
Date:
FORM: LOA 06-16 )'age3 of

FIELD GH-3
FIELD GH-2
7
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'I FIELD GH-1
Y 1
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Ir�
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INV
f` • Well
Field Total Acres Buffered Acres Net Acres
A Structure
GH-1 18.0 5.4 12.6
GH-2 25.4 5.7 19.7 ■ Dwelling
GH-3 35.6 6.5 29.1 Gate
Access Road
REVIEW BOUNDARY shall be established around each land application site midway i
between the Compliance Boundary and the perimeter of the residuals land application area,
-- - Drain
COMPLIANCE BOUNDARY: The Compliance Boundary for each land applicaion site
is established at either 250 feet from the residuals land application area or 50 feet
within the property boundary, whichever is closest to the residual land application area. Pond
REFERENCE: Field Boundary
GIS DATA LAYERS WERE OBTAINED FROM YADKIN COUNTY GIS PLEASE NOTE THIS MAP IS FOR
INFORMATIONAL PURPOSES ONLY IT IS NOT MEANT FOR DESIGN, LEGAL, OR ANY OTHER USES. ® Buffer
THERE ARE NO GUARANTEES ABOUT ITS ACCURACY WMSS, PLLC ASSUMES NO RESPONSIBILITY S Iglt (c I ye �af '= r Property B011ndaf
FORANY DECISION MADE OR ANYACTIONS TAKEN BY THE USER BASED UPON THIS INFORMATION. P Y y '.
, a m t e
SCALE. 1 " = 600 ' FIGURE NO
GILBERT HEMRIC
DATE 06-12-19 BUFFER MAP 2
DRAWN BY' nnE.IvI wilicox&ma"e
PROJECT NO S O 1: 5 f] l U T 1 0 N S DUVALTEX
19-02 Ph:01 YADKIN COUNTY, NORTH CAROLINA
Haynes Road
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Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT
FORM: LOA 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Ajlplicant shall submit one orieinai and two conies of the application and
supportine documentation
For more ix formalion, visit Me Waier 01w1h), Permilun,,Section s Non Dis<hux r c Penuixtnt b'nit,_
General This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of
Class B residuals (may include water treatment plant or other type residuals) in accordance with I S t NC.At u'T. i 1 GCI. Do not submit
this agreement for review without a corresponding application form (FORM: RLAP 06-16).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Owner Agreement (FORM: LOA 06-16):
[� Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-I6) Conn. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attaelunents to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the
Applicant.
A copy of the completed and appropriately executed agreement nn.ist be provided to the landowner and the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND
The undersigned landowner or his representative hereby permits:
Applicant's name:
hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land
application she(s) (Le,, see attached setback maps) in accordance with fire stipulations and restrictions as given in this
Agreement:
Site/F'ictd ID
Lease
(yes/no)
Land Use or
Cropping Patterns
intended Use of Crops
Residuals Sowee
(optional)
Special note
Oxo-liluover-seed/
pasture)
--c
s
v
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the
Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and
shall be renewed each time this permit is renewed.
"fhe undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and
stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement.
FORM: LOA 06-16 Page I of 3

I, 'ITrc landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted
entity for the site(s) specified by this Agreement.
2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall
be responsible to ensure that the third party agrees and complies with the ternns and conditions of this Agreement.
3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 11) are met.
4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 A4ail
Service Center, Raleigh, NC 27699-1617.
5. The Permittee must request and obtain a permit modification from the Division prior to a transfe of the land application site(s) to a new
landowner. In addition, the current landowner shall give a notice to the new, landowner that gives fill details of the residuals applied at the land
application site(s).
6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program,
including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description ofthe
equipment used by the Permittee.
7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land
application even and a copy of the results of each soil analysis.
8. If the soil pit of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of little shall be applied to achieve a final soil
PH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the
specified crop.
9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of
soil samples, and the permitted application limits.
10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nut tents
(e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s).
11, The landowner or his representative will inform the Pemtince of any revisions or modifications to the intended use and cropping patterns for
the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application
events at appropriate periods.
12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or
his representative prior to and during a residuals land application event.
13, The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and
inspect any property, premises, m place or or related to the land application site(s) at any reasonable time for the purpose of determining
compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records
that must be kept under the terms and conditions of the permit take necessary Ieachate, surface water- groundwater, or soil samples during the
tern of, and 12 months after termination of, this Agreement.
11, RESTRICTIONS:
1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application
site(s) during active use and for the 12-month period followings residuals land application event. Such controls may include the posting of
signs that indicate the activities being conducted at the land application site(s).
2. Animals shall not be grazed on the land application site(s) for a 30-day period following it residuals land application event. Land application
sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application
events
3, Food crops, feed crops, and fibe crops shall not be harvested for a 30-day period following a residuals land application event.
4. Food crops with harvested parts that touch the residualssoil mixture and are totally above the land surface shall not be harvested for a 14-month
period following a residuals land application event,
5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application
event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil.
6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals and application
event when the residuals remain on the and surface for less than four months prior to incorporation into the soil.
7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event.
III.AL'1'CRNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one)
15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, I SA NC'AC 02T.0105lh) allows the compliance
boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided
the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following;
❑ A re -defined compliance boundary is needed for field(s) ID: ____
(Please include the rationale for the requested re -location of the compliance boundary and attach a nap showing the newly proposed compliance
boundary to the application package)
t�f A re -defined compliance boundary is not needed for this site.
W. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed)
❑ Tluc land application field(s) ID: v is currently permitted under another
residuals land application program; Permit Number WQ: ___. The land owner hereby acknowledge that by signing this
agreement, he she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred
into the new program; _._
(Name of the new program)
FORM: LOA 06-16 Page 2 of

Landowner's Certification:
I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions
regarding the use of the land application site(s) on behalf of other deeded landowners OR that 1 am otherwise authorized, through
a power of attorney or other legal delegation, to make decisions regarding the use of the land application sile(s) on behalf of the
deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or
agreement with another municipality, contractor, or other pennitted entity. Furthermore, 1 certify that 1 have read this Agreement,
understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of
field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified
herein.
Landowner name: " �•+-� iN. (_ut�av� lrv._/L�_ d2c,.
Address:
City:
Phone:
State:
E-mail
M
Signature: �_ ���-��a�.�`Z2—i>4.\- Date:
NORTH 7CA�R/OL[NA,�C_ COUNTY
1, the undersigned Notary Public do hereby certify that __k3a4_A. 25dy-ny ,
personally appeared before me this day and acknowledged the due execution of the forgoing instrument.
WITNESS my hand and official seal this the
day of
Signature and seal
My commission exp
Lessee's/Operator's Certification:
I certify that I have read this Agreement and do thereby agree to abide by the stipulations and restrictions as specified herein.
Lessee operator name: � , I
Address:
1y / n
City: _,/L/i+� Xp;i.�; i%r' .—.�._._ Stale: _ / / Zip:---v2—
Phone: E-mailaddress:�
Signature: GLG z1 _--,_q_Si�_ _— Date:
Permittee's Certification:
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Signing official name: 'ke:4-�L
Signature:
FORM: LOA 06-16 Page 3 of 3

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