WQ0003487_Residual Annual Report 2014_20150318

March 1, 2015
NC Division of Water Quality
ATTN: Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Dear Sir;
novozymes. RD
Rethink Tomorrow
CSi V
MAR 18 2015
ORMATlgdq PROC6S§iNG UNff
Enclosed please find the 2014 Annual Residuals Application Report for Novozymes North America, Inc
(Permit #WQ0003487)
Please find attached 3 copies of the 2014 Land Application Report for the distribution and marketing of
Novozymes residuals under permit #WQ0003487.
The following information is attached:
1. Cover letter
2. Class A Distribution & Marketing/Surface Disposal Certification and Summary Forms: DMSDF
and DMSDF supplemental forms.
3. Annual Residual Summary Forms: RSSF and RSSF-B
4. Residual Analysis Lab Sheets
5. Annual Pathogen & Vestor Attraction Reduction Forms: PVRF
6. Pathogen & Vector Reduction Lab Sheets/Records i
This report reflects the .30 mineralization as stated in the permit.
Please contact me at your earliest convenience if you have any questions or require additional
information.
Sincerely,
911.1 '4 0*---
Randy Cutchin
Novozymes North America, Inc.
919/494-3393
[e-mail]
Enclosures

ANN-UAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: 3q Qj -1 Cou0ty: _ v�� i 1 lrl Year: ;;� p I y
Facility Name (as shower on permit): I J DV Z:i U S LJ O'Llix AM 2L'I <a' , Ir
Land Application Operator: NO"J p Phone: I Li - 300
Land application of residuals as allowed by the permit occurred during the past calendar year?
*yes ❑ No - If No, sldp Part A, and Part B and proceed to Part C. Also, If residuals were
generated but hot land applied, please attach an explanation on how the residuals were handled.
number of application fields in
Total number of fields utilized for land
Total amount of dry tons applied during the year for all
Total number of acres utilizes for land
the year:
ion sites:
the year:
Part B - Annual Com iance Statement;
Facilitty was compliant during calendar year (i with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action.
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration. Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Pez7mit were complied with (applicable to 40 CPR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on, the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
, C) I I'S
n ate
Permi ee Name and Title (type or pri t) Sign e of rmittee
Signature of Preparer'�
Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer'' ''fines' =- "".o PR Part 503.9 (r) and 15A NCAC 07 0 11�a a aano ��DENR FORM ACF (1212006)�
Z d HL0 N Il,H 9 19n o a Wd8[:L SIH 'U W

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: 3487 Novozymes North America, Inc.
PHONE: [phone] Franklin 41'ERATOR: Novozymes North America, Inc.
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A(Source(s) and "Residual In" Volume Only) and Part C)
p Distribution and Marketing ( complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes No (] ❑ If No skip parts A, B, C and certify form below
Part A` Part B*-.
Month
Sunrces(s) (include NPDES # if applicable)
Volume (dry tons}
Recipient Information
Amendment! Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended us*)
WAS
SBM
January
136
68
1110
1314
see attached DMSDF (Supp)
February
89
17
800
906
see attached DMSDF (Supp)
March •
138
73
1251
1462
see attached DMSDF (Supp)
April
104
40
926
970
see attached DMSDF (Supp)
May
86
78
643
807
see attached DMSDF (Supp)
June
107
29
808
944
see attached DMSDF (Supp)
July
112
65
1174
1351
see attached DMSDF (Supp)
August
242
8
849
1099
see attached DMSDF (Supp)
September
229
5
986
1220
see attached DMSDF (Supp)
October
247
3
2009
2258
see attached DMSDF (Supp)
November
132
17
837
986
see attached DMSDF (Supp)
December
177
94
1085
1356
see attached DMSDF (Supp)
Total from FORM DMSDF (sup)
0
.0
0-
0
0
Totals: Annual (dry tons): 1799
497
12377
14673 = =
14673
=
Amendment(s) used-1 Hydrated Lime
Bu lking A nts used: None
8 If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)17
Facility was compliant during the past calendar year with ail conditions of the land application permit (including 21 Yes
but not limited to items 1-3 below) issued by the Division of Water Quality: ONo if No, Explain in Narrative
1. All monitoring was done in accordance with the permit and reported for theyear as required and three (3) copies of certified laboratory results are attached.
2. Ail operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
t Gs 01 is
Sig e o tniltee Da
"Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Signature of Preparer**
(if different from Pemittee)
Date
z
0
0
E2
W
DENR FORM DMSDF (1212006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME:; ='= --
Nov6zymesNorth America;
PHONE: , ;(919),494,3390: COUNTY: Franklin•, OPERATOR: Novozyrnes `North America; Ini
,.
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
I Distribution and Marketinv (romnletP Parte A anti M
Part A*:
Part Bx:
Volume (dry tons)
Recipient Information
Month
Sources(s) (include NPDES # if
applicable)
pp )
Amendment/
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
Bulking Agent
January
Hunter Choplin
42
Agricultural
January
Herman Collier
301
Agricultural
January
RC Creech
11
Agricultural
January
Tim Duke
200
Agricultural
January
Andy Garrett
47
Agricultural
January
Clem & Jermey Mitchell
169
Agricultural
January
ED Moore
170
Agricultural
January
Novozymes
160
Agricultural
January
Thomas Perdue
214
Agricultural
February
David Clary
27
Agricultural
February
RC Creech
14
Agricultural
February
Craig Faulkner
13
Agricultural
February
Jimmy Harris
57
Agricultural
February
Paul Kearney
30
Agricultural
February
Ed Moore
64
Agricultural
February
HenryNelms
165
Agricultural
February
Al Privette
201
Agricultural
February
Lee Short
256
Agricultural
February
Mathew Whitley
79
Agricultural
Totals:
Annual (dry tons):
- : 0.: " '.
-0.
..........................................
0' 2 22
Amendment(s) used:
Bulking Agent(s) used:
(supp)): .' Total Number of Form DMSDF (Supp)l 7
k If more space is required, attach additional information sheets (FORM DMSDF
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL, DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL, CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME:Noyozymes North America;" Inc.
PHONE:.' (919) 4944390 COUNTY: Franklin -' OPERATOR: Novozyme9 North'Ain"e,ka 'Inc
FACILITY TYPE (please check one):
® Surface Disposal (complete Part A - "Month", "Sourcc(s)" and "Residual In" columns only)
21 Distribution and Marketing (complete Parts A, and B)
Part A*:
Part BX:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
March
Jason Aycock
165
Agricultural
March
Herman Collier
252
Agricultural
March
Nathaniel Davis
140
Agricultural
March
Doug May
156
Agricultural
March
Kevin Mitchell
228
Agricultural
March
Rex Murphy
47
Agricultural
March
Henry Nelms
187
Agricultural
March
Mike Norwood
22
Agricultural
March
Calton Robinson
24
Agricultural
March
Lee Short
178
Agricultural
March
Billy Wood
63
Agricultural
April
Herman Collier
198
Agricultural
April
James Davis
34
Agricultural
April
Nathaniel Davis
1 27
Agricultural
April
Phillip Fleming
14
Agricultural
April
Andy Garrett
34
Agricultural
April
Willie Loyd
168
Agricultural
April
Kevin Mitchell
101
Agricultural
April
Henry Nelms
55
Agricultural
April
Mike Norwood
38
Agricultural
April
Thomas Perdue
134
Agricultural
April
Lee Short
166
Agricultural
Totals:
Annual (dry tons):
'0
0"." ', `... ,::::''<::'::::'::::::'<::>::':<::::'::::::::::::::::::::::::::: 2431
............. I.......
Amendment(s) used: Bulking Agent(s) used:
r If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 7
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
W PERMIT #: 3487 FACILITY NAME: Novo mes orth=A"`­-­--- c`` ; nc -
Q 2y . N xna,7I
PHONE: � :: : �� � _. - - - . _ . .. - ... . _• - _ :, :.-, :..
_(91>9)`494:-3390' COUNTY: :Franklin OPERATOR:INovozymes North Am6kai;;lnb:
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
❑ Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
May
Jason Aycock
228
Agricultural
May
David Clary
47
Agricultural
May
James Davis
64
Agricultural
May
Nathaniel Davis
74
Agricultural
May
Phillip Fleming
124
Agricultural
May
Wilson Fleming
71
Agricultural
May
John Garrett
98
Agricultural
May
Paul Kearney
12
Agricultural
May
Kevin Mitchell
63
Agricultural
May
David Vick
26
Agricultural
June
Ann Bragg
28
Agricultural
June
Alpheus Jones
58
Agricultural
June
Bill Freeman
91
Agricultural
June
Bob Fowler
394
Agricultural
June
Craig Falkner
61
Agricultural
June
Paul Jessup
38
Agricultural
June
Richard Layton
20
Agricultural
June
William Peoples
30
Agricultural
June
Grace Perdue
35
Agricultural
June
Mark Perkinson
20
Agricultural
June
Mike Smith
108
Agricultural
June
Joe Tharrington
67
Agricultural
Totals:
Annual (dry tons):
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 7
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME:' Novo riles North America Inc:
zy.
PHONE: 919 49,4.-3390, COUNTY:,!'
( )Fran1{liii' - -
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A -"Month", "Source(s)" and "Residual In" columns only)
R1 Distribution and Marketing (comnlete Parts A. and R)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
July
David Clary
91
Agricultural
July
Herman Collier
30
Agricultural
July
Steve Collins
11
Agricultural
July
Tim Duke
126
Agricultural
July
Donald Edwards
103
Agricultural
July
Bob Fowler
15
Agricultural
July
E B Harris
43
Agricultural
July
Lee Inscoe
22
Agricultural
July
John Joyner
108
Agricultural
July
Ken Kreger
52
Agricultral
July
Spencer Marshall
14
Agricultural
July
Dave Moore
42
Agricultural
July
Mark Perkinson
30
Agricultural
July
J H Smith
40
Agricultural
July
Mike Smith
24
Agricultural
July
Joe Tharrington
52
Agricultural
July
Daryl Tharrington
76
Agricultural
July
Randy Thomas
120
Agricultural
July
Len Wester
353
Agricultural
August
Richard Breedlove
23
Agricultural
August
David Clary
16
Agricultural
August
Donald Edwards
46
Agricultural
August
Kenny Fuller
33
Agricultural
Totals:
Annual (dry tons
y )�
0
o..
-- ,g.
-1'4.70'
Amendments used:
O
Bulking Agent(s) used:
used:
(supp)): Total Number of Form DMSDF (Supp) 7
If more space is required, attach additional information sheets (FORM DMSDF
utNK rUKNi uMSur (6upp) (12iluub)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME: '. r= _ = ,Novozymes North America, Iric x
PHONE:3390: COUNTY:Frankhri OPERATOR:
>No�ozymes North"Amenca,Inc
•,
FACI'LITY TYPE (please check one): ® Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
91 Distribution and MarketinLy (complete Parts A. and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
August
Frank Gantt
25
Agricultual
August
Russell Gupton
37
Agricultual
August
EB Harris
347
Agricultual
August
Jimmy Harris
146
Agricultual
August
John Harris
96
Agricultual
August
Ken Kreger
15
Agricultual
August
Shane Mitchell
80
Agricultual
August
ED Moore
196
Agricultual
August
Ronald Murphy
23
Agricultual
August
Lee Short
49
Agricultual
August
Len Wester
31
Agricultual
September
Russell Gupton
49
Agricultual
September
EB Harris
392
Agricultual
September
Jimmy Harris
95
Agricultual
September
Greg Holtzmann
100
Agricultual
September
Martha Mobley
306
Agricultual
September
Len Wester
135
Agricultual
September
H W Windley
143
Agricultual
October
Spencer Dean
328
Agricultual
October
EB Harris
679
Agricultual
October
Jimmy Harris
13
Agricultual
Totals:
Annual (dry- tons
�.0'
0; .:..
Amendments used: Bulking Agent(s) used:
If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 7
DENR FORM DMSDF (Supp) (12/2006)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
PERMIT #•
W R 3487 FA •,, -
CILITY NAME. ,Nov
Q Ain ri I
,
PHONE•'',:` ' 919 494 339,0' COUNTY " Franklin
,). OPERATOR:Novozyrnes North;Amenca; Inc'.
_ .
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
El Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
October
Greg Holtzmann
340
Agricultual
October
Kevin Mitchell
218
Agricultual
October
Martha Mobley
303
Agricultual
October
Travis Pulley
20
Agricultual
October
Preston Williams
94
Agricultual
October
Len Wester
263
Agricultual
November
Tim Duke
147
Agricultual
November
EB Harris
94
Agricultual
November
Jim Huffman
28
Agricultual
November
Kevin Mitchell
16
Agricultual
November
Travis Pulley
246
Agricultual
November
Len Wester
263
Agricultual
November
Cecil Wilson
145
Agricultual
November
HW Windley
47
Agricultual
December
Gillis Alston
131
Agricultual
December
Greg Alston
7
Agricultual
December
Eddie Caudle
54
Agricultual
December
Glenn Coleman
24
Agricultual
December
Leon Dillard
51
Agricultual
December
Tim Duke
108
Agricultual
December
Robert Land
80
Agricultual
December
Doug May
73
Agricultual
December
Kevin Mitchell
142
Agricultual
9
Totals:
AnnuaIdrtons
Amendments used: Bulking Agent(s) used:
k If more space is required, attach additional information sheets (FORM RE415MRIPIP)ASDF (Supp) (12/2006) Total Number of Form DMSDF (Supp) 7

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
Supplemental Information
WQ PERMIT #: 3487 FACILITY NAME Novozymes'North A�merica,'Inc;
PHONE:?; (919)Y494 3390. COUNTY: ' x Franklin OPERATOR: Novorymes North America,°In,
t ., -.., _....... . . .. . .
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A -"Month", "Source(s)" and "Residual In" columns only)
Rl Distribution and Marketine (complete Parts A. and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
December
Mike Newton
12
Agricultual
December
Novozymes
379
Agricultual
December
Mike Preddy
10
Agricultual
December
Steve Preddy
10
Agricultural
December
Glenn Riggan
85
Agricultual
December
Len Wester
190
Agricultual
Totals.
Annual (dry tons):
Amendment(s) used: Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORMWSV0fi�ffDwbDF (Supp) (12/2006) Total Number of Form DMSDF (Supp) 7

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Dame:
Residual Source WQ # or
NPDES #:
WWT'P Name:
Residual Analvsis Data
3487
Novozymes North America, Inc.
Laboratory:
1)
2)
3)
4)
5)
ENCO
Parameter
(mg/kg)
Conc.
Limit
(m /k a
Sample or Composite Date
Jan
Feb
Mar
Apr
May
Jun
Jul
Aug
Sep
Oct
Nov
Dec
Percent Solids (%)
NA
4
3.8
6.2
5.4
3.4
4
4.2
4.3
4.7
5.7
4.3
3.9
Arsenic
75
<1.35
<1.42
<0.87
<1.00
<1.59
<1.35
<1.29
<2.51
<1.15
<0.95
<1.26
<1.36
Cadmium
85
<0.09
<0.09
<0.06
<0.07
<0.11
<0.09
<0.09
<0.17
<0.08
<0.06
<0.08
<0.09
Copper
4,300
7.77
13.21
6.79
8.52
5.88
11.2
10.29
8.26
11.13
15.19
16.67
9.87
Chromium
NA
Lead
840
<0.52
<0.55
<0.34
0.51
<0.62
<0.52
<0.50
<0.98
<0.45
<0.37
0.55
<0.54
Mercury
57
<0.09
<0.02
<0.01
<0.02
<0.02
<0.02
<0.08
<0.08
<0.07
<0.06
<0.08
<0.09
Molybdenum
75
1.01
1.35
0.83
1.09
1.50
1.52
1.12
2.05
1.03
1.17
1.54
1.44
Nickel
420
0.95
1.14
0.34
0.98
1.19
0.67
0.86
1.72
0.96
0.97
1.04
1.40
Selenium
100
<1.25
<1.32
<0.81
<0.93
<1.47
<1.25
<1.19
<2.33
<1.06
<1.75
<1.16
<1.26
Zinc
7,500
26.25
53.95
48.10
27.50
11.29
24.25
33.10
31.40
28.23
29.12
46.04
20.31
Total Phosphorus
NA
13,000
16,052
15,000
13,148
11,765
11,250
8,571
10,000
13,191
13,860
14,651
14,615
TKN
NA
45,000
52,631
43,548
40,741
38,235
47,500
33,333
39,534
36,170
38,596
46,512
51,282
Ammonia -Nitrogen
NA
2,125
3,157
2,258
2,037
1,647
3,000
2,262
2,163
2,978
1,929
3,256
3,846
Nitrate and Nitrite
NA
457
402
216
486
506
445
369
299
327
193
335
412
-- ror surtace disposal tacilitres the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Fume:
Raairinal Analvaic Data
3487
Novozymes North America, Inc.
Laboratory: 1)
2)
3)
4)
5)
ENCO
Parameter
(mg/kg)
Conc.
Limit
(m a
Sample or Composite Date
Jan
Feb
Mar
Apr
May
Jun
Jul
Aug
Sep
Oct
Nov
Dec
Percent Solids (%)
NA
4
3.8
6.2
5.4
3.4
4
4.2
4.3
4.7
5.7
4.3
3.9
Arsenic
75
<1.35
<1.42
<0.87
<1.00
<1.59
<1.35
<1.29
<2.51
<1.15
<0.95
<1.26
<1.36
Cadmium
85
<0.09
<0.09
<0.06
<0.07
<0.11
<0.09
<0.09
<0.17
<0.08
<0.06
<0.08
<0.09
Copper
4,300
7.77
13.21
6.79
8.52
5.88
11.2
10.29
8.26
11.13
15.19
16.67
9:87
Chromium
NA
Lead
940
<0.52
<0.55
<034
0.51
<0.62
<0.52
<0.50
<0.98
<0.45
<0.37
0.55
<0.54
Mercury
57
<0.09
<0.02
<0.01
<0.02
<0.02
<0.02
<0.08
<0.08
<0.07
<0.06
<0.08
<0.09
Molybdenum
75
1.01
1.35
0.93
1.09
1.50
1.52
1.12
2.05
1.03
1.17
1.54
1.44
Nickel
420
0.95
1.14
0.34
0.98
1.19
0.67
0.86
1.72
0.96
0.97
1.04
1.40
Selenium
100
<1.25
<1.32
<0.81
<0.93
<1.47
<1.25
<1.19
<2.33
<1.06
<1.75
<1.16
<1.26
Zinc
7,500
26.25
53.95
48.10
27.50
11.29
24.25
33.10
31.40
28.23
29.12
46.04
20.31
Total Phosphorus
NA
13,000
16,052
15,000
13,148
11,765
11,250
8,571
10,000
13,191
13,860
14,651
14,615
TKN
NA
45,000
52,631
43,548
40,741
38,235
47,500
33,333
393534
36,170
38,596
46,512
51,282
Ammonia -Nitrogen
NA
2,125
3,157
2,258
2,037
1,647
33000
2,262
2,163
1,929
3,256
3,846
Nitrate and Nitrite
NA
457
402
216
486
506
445
369
299
LSzj
193
335
412
a For surface disposal facilities the ceiling concentration limits listed in ties form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
PC nal ' s for submitting fals information, including the possibility of fines and imprisonment for knowing violations."
Signs a of P arer * D to
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DEN R FORM RSSF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional farms as needed.
WQ Permit Number: 3487 Laboratory: 1)
Facility Name: Novoyzmes North America, Inc. 2)
Residual Source 3)
NPDFS # or W Q#: 4)
WWTP Name: 5)
Residual Analvsis Data
ENCO
Parameter
(mg/kg)
Sample or Composite Date
Jan
Feb
Mar
Apr
May
Jun
Jul
Aug
Sep
Oct
Nov
Dec
Aluminum
Magnesium
Calcium
Potassium
Sodium
PAN
SAR
6,000
1,975
70,250
15,475
2,235
14,407
0.453
7,395
1,579
72,368
17,737
3,447
16,586
0.675
7,822
1,693
28,226
15,016
2,016
13,490
0.82
83389
1,294
60,000
12,148
2,907
1 13,189
0.745
5,558
485
35,882
32,941
2,838
12,476
0.751
5,150
1,225
56,250
18,275
3,625
15,145
0.826
5,571
1,571
74,524
14,048
3,428
10,749
0.696
4,000
2,084
-134,651
14,791
4,163
12,461
0.639
7,297
1,559
87,447
14,255
3,915
11,497
0.778
8,912
1,319
80,351
10,964
5,193
11,965
1.19
12,721
1,802
86,279
15,558
8,070
14,614
7,641
1,456
80,000
14,666
7,666
16,207
1.54
1.45
PH
12
11.8
12.3
12.1
12
12
11.8
11.98
11.7
12.4
12.4
12.3
--------------------------
" 1 certify, under penalty of law, that this document was prepared under -my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pe ties for submitting false information, including the possibility of fines and imprisonment for knowing violations.,,
�3 0l s
Sigma of parer ate
DENR FORM RSSF - B (1212006)

AKALINE STABILIZATION OF WASTEWATER BIOSOLIDS
Facility Novozymes North America Inc.
FFI 96 (SBM Initial)
FHG 409 SBM/WAS
Initial
FHG 407A (>2 our pH)
FLF 96 24 Hour pH
Date
1/20/2014
pH
12.24
Temp -c
Corr.
Factor
I Corr.
pH
Time
7:43
pH
12.30
Temp
Corr.
Factor
Corr.
pH
Time
8:00
pH
12.10
Temp *C
Corr.
Factor
Corr.
pH
Time
13:19
pH
Temp *
Corr.
Factor
Corr.
pH
Time
Operator
Initials
1/21/2014
12.00
13:10
RC
4/22/2014
12.48
7:331
12.30
8:15
12.40
11:50
4/23/2014
12.10
7:00
RC
7/30/2014
11.30
26.50
0.03
11.60
7:03
12.10
28.10
0.09
12.19
8:37
12.10
26.40
0.03
12.13
11:05
7/31/2014
11.80
27.00
0.06
11.88
9:00
RC
10/6/2014
12.03
25
01
12.03
8:131
12.47
28.9
0.12
12.59
8:02
12.03
27.1
0.06
12.09
10:46
10/7/2014
12.44
23.2
-0.06
12.38
10:00
RC
kA
Sig ture
FFI 96, FHG409, and FHG407 readings are from pH probes
FLF 96 pH is manually read from lab pH meter within 15 min. of taking sample
Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Novozymes North America, Inc. WQ Permit Number: 3487
WWTP Name: NPDES Number;
Monitoring Period: From 1/1/2014 To 12/31/2014
T)n4hnnd.. RaAtiti.•�:nr, r1 a TT! er min 11041-Pleslce indicate level achieved and alternative performed:
Class A:
Alt_ A time/temp) ❑
Alt B (A1k Treatment) ❑
Alt. C (Prior Testing) 21
A1t.D (No Prior Test)
Process to Further Reduce Pathoaengs ❑
Xf applicable to alternative performed (Class A only) indicate "process to Further Reduce Pathogens":
Compost 1a
Heat Drying ❑
Heat Treatment ❑
Thermo ®
Be Ray
GammaRay ❑
C7
Pasteurization
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Sicantly Reduce Pathogens":
Lime Stabilization El
Air Drying ❑
Com Ostia 2
Aerobic Digestion ❑
Anaerobic ies tion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number or
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
imu
Geo. Mean
axim
Units
Fecal Coliform
2 x 10 to the,N
6th power
per gram of
total solids
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 NON per 4 grams
total solid (dry
weight
C3.0
MPN/4g
0
QTLY
G
EPA 1682
\/nntn r• A1Tti-d M"nn te&.1" rinn ! 11%A IVI 'AI : 11L 1 . 1 111 / 1 - rle3RP_ 1LQ1C$LC Q11LCULL21161VC LJ% lUA 111GY.
Alt.1 (YS reduction) C)
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization Rl
Alt 7 (Drying - Stable) 111
Alt. 8 (Drying - Unstable) ❑
Alt. 9 Nectioa) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement]
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach aIt explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Angela Walsh Environmental Manager
Prepar,�.r Nam�3pa. dhTitle (type or print)
of
�3 0l 1
Da e
Land Appliez Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable)
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
1'1CAI0
cORIV o\ror r)2-r
9 d 1EVIN uo}l!N Rq ...1;[gno4 WdWL M6

RCU (Randy Cutchin)
From: Hardee, Ed <[e-mail]>
Sent: Tuesday, August 13, 2013 10:08 AM
To: RCU (Randy Cutchin)
Subject: Salmonela Testing
Randy,
As we discussed there is no NC certified lab for salmonella testing. The out of state labs are usually beyond the hold time due to distance. The Lab Certification Section i;
trying to work with any NC labs that desire to be certified for salmonella testing. Until there is a certified lab within the hold time distance you may use a out of state lat
for salmonella testing. If a lab in NC is certified I will forward you the contact information.
Ed Hardee
Aquifer Protection Section
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Phone [phone]
DISCLAIMER: Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be
disclosed to third parties unless the content is exempt by statute or other regulation.

www.encolabs.com
ANALYTICAL RESULTS
Description: SBM Lab Sample ID: C316719-01 Received: 01/07/14 13:15
Matrix: Sludge Sampled: 01/07/14 11:05 Work Order: C316719
Project: Monthly - Week One - SBM Sampled By: Kenneth Ball
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl Results Flaa it DF MDDL_ PO Batch Method Analyzed _By Notes
M [7439-97-6]^ 000340 U mg/L 1 0.00340 0.00400 4A10024 EPA 7470A 01/10/14 16:24 T1D
ercury
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results
Flaa
ni
DF
MDL
PO
Batch
Me
Analyzed
AM Notes
Aluminum [7429-90-5]^
240
mg/L
1
0.290
1.00
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Arsenic[7440-38-2]^
0.0540
U
mg/L
1
0.0540
0.100
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Boron [7440-42-8]^
0.216
J
mg/L
1
0.0500
0.500
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
1
0.00360
0.0100
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Calcium [7440-70-2]^
2810
mg/L
1
0.200
1.00
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Copper[7440-50-8]^
0.311
mg/L
1
0.0160
0.100
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Lead [7439-92-1]^
0.0210
U
mg/L
1
0.0210
0.100
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Magnesium [7439-95-4]^
79.0
mg/L
1
0.230
1.00
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Molybdenum [7439-98-7]^
0.0405
J
mg/L
1
0.0250
0.100
4A08015
EPA 6010C
01/09/14 11:08
JDH
Nickel [7440-02-0]^
0.0381
J
mg/L
1
0.0180
0.100
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Potassium [7440-09-7]1
619
mg/L
1
1.50
5.00
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Selenium [7782-49-2]^
0.0500
U
mg/L
1
0.0500
0.100
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Sodium [7440-23-5]^
89.4
mg/L
1
4.00
5.00
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Zinc[7440-66-6]^
1.05
mg/L
1
0.0380
0.100
4AO8015
EPA 6010C
01/09/14 11:08
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyte [NC 5911
Analyte rCAS Numberl
Results
Flaa
UnitsDF
MDL
PPOL_
Batch
method
An I
Notes
Ammonia as N [7664-41-7]^
85
D
mg/L
90
4.0
9.0
4AO8002
EPA 350.1
01/08/14 12:54
AIB
Biochemical Oxygen Demand
9500
mg/L
1
2.0
2.0
4AO8025
SM 521OB-2001
01/08/14 17:33
JOC
[ECL-0017]^
Chemical Oxygen Demand
25000
mg/L
1
400
400
4A10013
SM 5220D-1997
01/10/14 18:00
JOC
[ECL-0035]^
Chloride [16887-00-6]^
300
D
mg/L
5
11
25
4A08001
EPA 300.0
01/08/14 10:54
CV
Nitrate as N [14797-55-8]^
18
mg/L
1
0.025
0.10
4A14014
EPA 353.2
01/14/14 10:49
CV
Nitrite as N [14797-65-0]^
0.28
mg/L
1
0.017
0.10
4A07004
EPA 353.2
01/07/14 15:46
C1V
Phosphorus [7723-14-0]^
520
D
mg/L
200
5.0
20
4A17005
EPA 365.4
01/20/14 21:09
clv
Sodium Adsorption Ratio [ECL-0143]
0.453
[blank]
1
4A08015
CSU Method
01/09/14 13:50
JDH
Sulfate as SO4 [14808-79-8]^
120
D
mg/L
5
14
25
4AO8001
EPA 300.0
01/08/14 10:54
CV
Total Kjeldahl Nitrogen [ECL-0162]^
1800
D
mg/L
100
26
48
4A17004
EPA 351.2
01/20/14 10:52
clv
Total Solids [ECL-0168]^
4.0
% by Volume
1
0.0010
0.0010
4AO8020
SM 254OB-1997
01/08/14 15:05
MMR/J
Total Suspended Solids [ECL-0169]^
26000
mg/L
1
1.0
1.0
4AO8005
SM 254OD-1997
01/08/14 09:44
MMR
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 4 of 14

ANALYTICAL RESULTS
Desc"ription;SBM ; y : `"= Lab Sample ID:C400543-01
,*, atrix::,' U ge ..= :: Sampled:02/04/14 08:10
"Project:;•°Monthly, = Week One - SBM Sampled By:Joshua Darnell
Metals by>EPA":6000/7600"Series Methods
www.encolabs.com
Received: 02/04/14 13:05
Work Order: C400543
=4A w ENM,Cary certified analyte[NC 591]
Analyt-- f"c Numbed r „" _ Results" Flag Units DF MDL POL Bich Method Analyzed Notes
Me"rcury [7439 97 6]^. -." ;'- '" 0.000850 U mg/L 1 0.000850 0.00100 4610031 EPA 7470A 02/11/14 14:56 T1D
Metals, .total`.recoveilable) by EPA 6000/7000 Series Methods
c..
Lea
Results
Flaa
ni
DF
MDL
pQ,
MSh
Method
A110[1L" ".
lC N93S£
nu ri [Z429,=90
281
D
mg/L
2
0.290
1.00
4BO6015
EPA 6010C
02/17/1411:39
JDH "
c•[7,440-38-2]^- -
- 0.0540
UD
mg/L
2
0.0540
0.100
4B06015
EPA 6010C
02/17/14 11:39
-JDH
[7440-42-8]" ",,.." -
0.221
JD
mg/L
2
0.0500
0.500
4BO6015
EPA 6010C
02/17/14 11:39
JDH
^'
um{7440-43-9]^ `;
0.00360
UD
mg/L
2
0.00360
-0.0100
4BO6015
EPA 6010C
02/17/14:11:39
JDH
,.,,
rm [7440-70-2]^ .'-' :`_ ;
2750
D
mg/L
2
0.390
1.00
4B06015
EPA 6010C
02117/1411:39
JDH
0.502
D
mg/L
2
0.0160
0.100
4BO6015
EPA 6010C
02/17/14 11:39
JDH'
7439 92 1]^
0.0210
UD
mg/L
2
0.0210
0.100
4BO6015
EPA 6010C
02/17/14 11:39
JDH
eslum-[7439-95=4]^"',',' ; ;
60.0
D
mg/L
2
0.230
1.00
4BO6015
EPA 6010C
02/17/14 11:39
JDH'
)denum"[7439-9871A=; :'" _
0.0514
JD
mg/L
2
0.0250
0.100
4B06015,
EPA 6010C
02/17/14 11:39
JDH
ih[7440-02-0]^ ;'✓ ; °z `' -::.,,
0.0434
JD
mg/L
2
0.0180
0.100
4B06015
EPA 6010C
02/17/14 11:39
JDH
sium"[7440-09=7]^" '""
674
D
mg/L
2
1.50
5.00
4BO6015
EPA 6010C
02/17/14 11:39
JDH
_-
um'[7782-49=2]^": -;" .,
0.0500
UD
mg/L
2
0.0500
0. loor
4BO6015
EPA 6010C
02/17/14 11:39
JDH-
m�[Z440-23-Sj^
131
D
mg/L
2
4.00
5.00
4BO6015
EPA 6010C
02/17/14 11:39
JDH
7440=66=6]^.;"
2.65
D
mg/L
2
0.0380
0.100
4BO6015
EPA 6010C
02/17/14 11:39
JDH
Classical :Chemistry Parameters
-= ^�=.ENCO Gary,.'cerdhed ana/yte�(NC; 593J , °`
Results
Flan
rM
2F
MDL
POL
Batch
Method
Ammonia a�N-[7664-41,7]^�_-,''' ,
120
D
mg/L
90
4.0
9.0
4612004
EPA 350.1
Biochemical,Oxygen'Demand'-�.,.,
11000
mg/L
1
2.0
2.0
4BO5018
SM 521OB-2001
Chemical.Oxygeri Demand .-
28000
mg/L
1
800
800
4BO7022
SM 5220D-1997'
Chioride',-16887=00-6]'^
740
D
mg/L
10
22
50
4B10013
EPA 300.0
Nitrate as;N [1,097=55=8]^ _
15
mg/L
1
0.025
0.10
4B11027
EPA 353:2
Nitrite.'as N [14797=65=0]^: s- - .
0.29
mg/L
1
0.017
0,10
4605002
EPA 353.2
" " '
Phosphorus;[Z723-14=0]^.
610
D
mg/L
400
10
40
4B14003
EPA 365.4
Sodi.um;Adsorption'Ratio [ECL-0143]Z
0.675
[blank]
1
4BO6015
CSU Method
Sulfate'as SO4:[14808-79=8].^•"
150
D'
mg/L
10
29
50
4B10013
EPA 300.0
Totakjeldahl Nitrogen![ECL-0162]A
2000
D
mg/L
100
26
48
4B14002
EPA 351.2
Total•s6l1ds'[ECL-0168]^
3.8
% by Volume
1
0.0010
0.0010
4B10024
SM 254OB-1997
Total Suspended'Soiids,[ECL-0169]^
27000
mg/L
1
1.0
1.0
4806002
SM 254OD-1997
This report relates only to the
sample as, received by the laboratory, and may only be reproduced In full.
Analyzed •
ft Notes
02/12/14 10:43
Clv
02/05/14 15:50
JOC B-07
02/07/14 18:47 •
JOC
02/10/14 13:55
62/12/14 08:40
02/05/14 08:58
02/17/14 12:29
02/17/14 16:35
02/10/14 13:55
02/17/14 10:27
02/10/14 15:48
02/06/14 09:14
A]B
CV
Clv
C1v
JDH
AJB
C1v
MMR'
MMR
Page 4 of 13

=- • = www.encolabs.com
ANALYTICAL RESULTS
Descriptio"n":: SBM" Lab Sample ID:C401435-01 Received: 03/05/14 13:10
Mat�iz6.Sludge" "- Sampled: 03/05/14 08:30 Work Order:C401435
' Project: -Monthly - Week One - SBM Sampled By: Brooks Williams
Metals bj► EPA" 6000/7000 Series Methods
' ^ : ENCO Cary certlhed ana1xe [NC 5911
Analyfe=FCAS Numberl ,. Results Flag Units Df MDL POLL Batch Method np a tl zed BX ASSs
•Mercury [7439-97-6]^..` `,, ;-. 0.000850 U mg/L 1 0.000850 0.00100 4C12032 EPA 7470A 03/13/14 15:13 TiD
Metals,( 61 recoverable) 'by EPA 6000/7000 Series.Methods
^: ENCO Cary cerdfled analyte [NC -591J
AnalvtexfCAS Numberl
Aluminum [7429=90=5]^
Arsenic (7440 3i3-2]^:
Boron [7,"2-8]"
Cadmium"�[7440- 43-9]^,
Calciurim [7440-70-2]^,
Copper '[7440-50-8] ^;
Lead [7439-, 2-1]^
Magnesium [7438=95-4]^
Molybdenum [7439-98-7j^'`:
Nickel
Potassium [7440-09-7]^
Selenium [7782-49-2]^
Sodium [7440-23-5]^
Zinc[7440-66-6]^ "
Classical Chemistry,,Parameters
^ : ENCO Cary,cerUfied ana/yte [NC 591]
Results Flag Urfits DF MDL PPL Batch Method Analyzed BY Notes
485 mg/L 1 0.290 1.00 4D17010 EPA 6010C 04/18/14 11:41 JDH
0.0540 U mg/L 1, 0.0540 0.100 4CO6028 EPA 6010C 03/12/14 12:38 JDH
0.0500 U mg/L 1 0.0500 0.500 4CO6028 EPA 6010C 03/12/14 12:38 , JDH
0.00360 U mg/L 1 0.00360 0.0100 4CO6028 EPA 6010C 03/12/14 12:38 JDH
1750 mg/L 1 0.390 1.00 4CO6028 EPA 6010C 03/12/14 12:38 JDH
0.421 mg/L 1 0.0160 0.100 4CO6028 EPA 6010C 03/12/14 12:38 JDH
0.0210 U mg/L 1 0,0210 0.100 4CO6028 EPA 6010C 03/12/14 12:38 JDH
105 mg/L 1 0.230 1.00 41317010 EPA 6010C 04/18/14 11:41 JDH
0.0515 J mg/L 1 0.0250 0.100 4CO6028 EPA 6010C 03/12/14 12:38 JDH
0.0211 J mg/L 1 0.0180 0.100 4CO6028 EPA 6010C 03/12/14 12:38 JDH
931 mg/L 1 1.50 5.00 4CO6028 EPA 6010C . 03/12/14 12:38 JDH
0.0500 U mg/L 1 0.0500 0.100 4CO6028 EPA 6010C 03/12/14 12:38 JDH
125 mg/L 1 4.00 5.00 4CO6028 EPA 6010C 03/12/14 12:38 JDH
2.98 mg/L 1 0.0380 0.100 4D17010 EPA 6010C 04/18/14 11:41 JDH
AnalvtejCAS Number1,.-' Results Flag
Ammonia as N:[766441-7]^ 140 D
BiochemiQa ,oxygeribemand 16000
[ECL-0017]^.._,.
Chemical Oxygen -Demand ;
[ECL-0035]^-
Chloride [16887=00-6]^
Nitrate as.N [14797-55-8]^
Nitrite'as N [14797-65-0]^
Phosphorus [7772344-0]^ .
Sodium Adsorption Ratio [ECL-0143]
Sulfate as SO4 [14808-79-8]^ '
Total Kjeldahl Nitrogen [ECL=0162]^
Total Solids [ECL-0168]^:
Total Suspended solids [ECL-0169]^
Willits DF MDL Q Batch Method Analyzed AM Notes
mg/L 90 4.0 9.0 4C06004 EPA 350.1 03/06/14 13:39 C1V
mg/L 1 2.0 2.0 4CO6022 SM 521OB-2001 03/06/14 15:39 JOC
39000 mg/L 1 800 800 4C10022 SM 5220D-1997 03/10/14 16:47 30C
520 D mg/L 10 22 50 4C10021 EPA 300.0 03/10/14 19:02 CV
12 mg/L 1 0.025 0.10 4C10019 EPA 353.2 03/10/14 15:17 AJB
1.4 mg/L 1 0.017 0.10 4CO5030 EPA 353.2 '03/05/14 15:11 ciV
930 D mg/L 320 8.0 32 4C12002 EPA 365.4 03/13/14 12:08 ciV
0.820 [blank] 1 4CO6028 CSU Method 03/12/14 15:19 JDH
53 D mg/L 10 29 50 4C10021 EPA 300.0 03/10/14 19:02 CV
2700 D mg/L 200 52 96 4C12003 EPA 351.2 03/13/14 13:40 c1V
6.2 % by Volume 1 0.0010 0.0010 4CO7027 SM 254OB-1997 03/07/14 15:39 MMR
47000 mg/L 1 1.0 1.0 4CO6006 SM 2540D-1997 03/06/14 09:34 MMR
<FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 4 of 14,
AnalvtejCAS Number1,.-' Results Flag
Ammonia as N:[766441-7]^ 140 D
BiochemiQa ,oxygeribemand 16000
[ECL-0017]^.._,.
Chemical Oxygen -Demand ;
[ECL-0035]^-
Chloride [16887=00-6]^
Nitrate as.N [14797-55-8]^
Nitrite'as N [14797-65-0]^
Phosphorus [7772344-0]^ .
Sodium Adsorption Ratio [ECL-0143]
Sulfate as SO4 [14808-79-8]^ '
Total Kjeldahl Nitrogen [ECL=0162]^
Total Solids [ECL-0168]^:
Total Suspended solids [ECL-0169]^
Willits DF MDL Q Batch Method Analyzed AM Notes
mg/L 90 4.0 9.0 4C06004 EPA 350.1 03/06/14 13:39 C1V
mg/L 1 2.0 2.0 4CO6022 SM 521OB-2001 03/06/14 15:39 JOC
39000 mg/L 1 800 800 4C10022 SM 5220D-1997 03/10/14 16:47 30C
520 D mg/L 10 22 50 4C10021 EPA 300.0 03/10/14 19:02 CV
12 mg/L 1 0.025 0.10 4C10019 EPA 353.2 03/10/14 15:17 AJB
1.4 mg/L 1 0.017 0.10 4CO5030 EPA 353.2 '03/05/14 15:11 ciV
930 D mg/L 320 8.0 32 4C12002 EPA 365.4 03/13/14 12:08 ciV
0.820 [blank] 1 4CO6028 CSU Method 03/12/14 15:19 JDH
53 D mg/L 10 29 50 4C10021 EPA 300.0 03/10/14 19:02 CV
2700 D mg/L 200 52 96 4C12003 EPA 351.2 03/13/14 13:40 c1V
6.2 % by Volume 1 0.0010 0.0010 4CO7027 SM 254OB-1997 03/07/14 15:39 MMR
47000 mg/L 1 1.0 1.0 4CO6006 SM 2540D-1997 03/06/14 09:34 MMR
<FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 4 of 14,
<FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 4 of 14,

K RD
www.encolabs.com
ANALYTICAL RESULTS
Description: -"SBM Lab Sample ID:C403744-01 Received: 04/01/14 11:30
_=Mat�ixr.Sludge` Sampled: 04/01/14 07:40 Work Order: C403744
:,Project ,-Monthly - Week One - SBM Sampled By:Josh Darrell
Metal "I y.EPA 6000/7060 Series Methods
ENCO Cary certified a_ nape [NC 5911
Anal vte rCAS Numbed : ' - ' .'
Results
F]ag
UnitS
PIE
MpJ,
'EDL
.Batch
Mercury[7439-97-lA-_ :,
0.000850
U
mg/L
1
0.000850
0.00100
4DO7006
Metals (total -recoverable) -by EPA 6000/7000 Series Methods
---^-,ENCO'Cary-cerb'fiedanalyte.[N_C 5911
Analvte rCA§ Numbed
Results
Has
ynits
DE
MDL
EQL
Batch
Aluminum [7429=90-5]^ :, .
453
mg/L
1
0.290
1.00
4DO2021
Arsenic [7440-38-2]^_"'.''�,. - - I
0.0540
U
mg/L
1
0.0540
0.100
4DO2021
Boron[7440-42-8]^' ,°"_ . •
0:200
J
mg/L
1
0.0500
0.500
4DO2021
Cadmium, 7.440-43=9]^:: .
0.00360
U
mg/L
1
0.00360
0.0100
4DO2021
Calcium [7440770-2]^, ;.
3240
mg/L
1
0.390
1.00
4DO2021
Copper[7440.50=8]^.
0.460
mg/L
1
0.0160
0.100
4DO2021
Lead.[7439-9271]^ --,:
0.0274
J
mg/L,
1
0.0210
0.100
4DO2021
Magnesium [7439-95-4]^
69.9
mg/L
1
0.230
1.00
4DO2021
Molybdenum [7439-98-7]^
0.0588
J
mg/L
1
0.02S0
0.100
4DO2021
Nickel [7440-02-U]^_ .y
0.0530
J
mg/L
1
0.0180
0.100
4DO2021
Potassium [7440=09-7]^:
656
mg/L
1
1.50
5.00
4DO2021
Selenium [7782-49-2j^"': ,": -
0.0500
U
mg/L
1
0.0500
0.100
4DO2021
Sodium [7440-23-5]^
157
mg/L
1
4.00
5.00
4DO2021
Zinc[7440-66-6]^' '
1.49
mg/L
1
0.0380
0.100
4DO2021
Classical :Chemistry Parameters
:^ -,ENCO Cary certified analyze [NC' 591J
Method AnalII3.ed ly !Votes
EPA 7470A 04/07/14 16.59 T11)
Method
Analyzed
RAC !Votes
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
D4/03/14 10:56 ,
JDH
EPA 6010C
D4/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
7DH
EPA 6010C
04/03/14 10:56
JDH
EPA 6010C
04/03/14 10:56
JDH
Analvte,rCAS Numberl• .,
Results
Flag
Units
PE
MDL
ESL
Batch
Method
Analyzed
Ax N
Ammonia'as N"[7664=41-7]^
110
D
mg/L
90
4.0
9.0
4DO2015
EPA 350.1
04/02/14 13:37
c1v
Biochemical Oxygen Demand
18000
mg/L
1
2.0
2.0
4DO2007
SM 521OB-2001
04/02/14 13:57
30C
[ECL-0017]^
Chemical oxygen Demand-', -.
37000
mg/L
1
800
800
4DO3012
SM 5220D-1997
D4/03/14 18:25
30C
[ECL-0035]^
"__
Chloride116887-00=6]^ -
220
D
mg/L
10
22
50
4DO3007
EPA 300.0
04/03/14 22:34
AIB
Nitrate as N [14797-55-8]^ ,
26
mg/L
1
0.025
0.10
4D10012
EPA 353.2
04/10/14 09:38
CV
Nitrite as N [14797-65-0]^_`
0.25
mg/L
1
0.017
0.10
4DO1019
EPA 353.2
04/01/14 15:06
C1V
Phosphorus [7723-14-0]^,
710
D
mg/L
400
10
40
4DO4003
EPA 365.4
04/07/14 11:38 •
clv
Sodium Adsorption.Ratio [ECL-0143]
0.745
[blank]
1
.4DO2021
CSU Method
04/03/14 15:48
JDH
Sulfate.as�SO4 [14808-79-8]^
28
mg/L
1
2.9
5.0
4DO3007
EPA 300.0
04/03/14 22:01
AJB
Total Kjeldahl"Nitrogen [ECL-0162]^
2200
D
mg/L
100
26
48
4DO4004
EPA 351.2
04/07/14 09:51
Clv
Total Solid's [ECL=0168]^ "
5.4
% by Volume
1
0.0010
0.0010
4DO4018
SM 254OB-1997
04/04/14 11:30
MMR
Total Suspended Solids,[ECL-0169]^
35000
mg/L
1
1.0
1.0
4DO1016
SM 25QD-1997
D4/01/14 13:41
MMR
i
This report relates only to the
sample as received by the laboratory,
and may only be reproduced in full.
Page 4 of 14

-
www.encolabs.com
_ -
ANALYTICAL RESULTS
Description,SBM° ``'=: :'. .,
Lab Sample ID:C405229-01
Received: 05/06/1413:10
Matrixd;:Sludge .;_ "-` ,
Sampled:05/06/14 07,45
Work Order: C405229
Project: ;Monthly_- We&One - SBM
Sampled By: Brooks Williams
-.
Mefals byEPA, 6000' 7000 Series Methods
',=.•^ ENCOCary"cerGfedana/yfe[NC591J
Analvfe -fCAS Numberbz: Results Flaa
Units DF MDL POL Batch
Method Analyzed By Notes
Mercury,[7439,=97 6]^ lr..r = ": , 0.000850 U
mg%L 1 0,000850 0.00100 4EO7040
EPA 7470A 05/08/14 14:17 T1D
Metals-(tgta ,iecol erable).by EPA 6000/7000 Series Methods
^.= ENCO.Cary certified analyte [IC, 591]
Anaivte'rcAs Numberl ,:-
Results
Flag
Units
DF
MDL
POLL
Batch
Method
Analyzed
B1C
Aluminum [7429-90=5]^ ;'e' -
189
mg/L
1
0.290
1.00
4E20031
EPA 6010C-
05/22/14 12:57
JDH
0.0540
U
mg/L
1
0.0540
0.100
4E13020
EPA 6010C
05/14/14 16:22
JDH
Boron:[7440-42-8]" ° '. ::
0.119
J
mg/L
1
0.0500
0.500
4E13020
EPA 6010C
05/14/14 16:22
JDH
Cadhiium [7440 43-9]^"" ; .',, '-_;
0.00360
U
mg/L
1
0,00360
0.0100
4E13020
EPA 6010C
05/14/14.16:22
JDH
Calcium`[7440;'464j^,:=.°c ;- ' --.'F .. -
1226
mg/L
1
0.390
1.00
4E13020
EPA 6010C
05/14/14 16:22
JDH
Copper [744Q=50-8]^` A . ; " '= =
0.200
mg/L
1
0.0160
0.100
4E13020
EPA 6010C
65/14/14 16:22
JDH
Lead'[7434;92-1]^r.>-:: -_ -.""..
0.0210
U
mg/L
1
0.0210
0.100
4E13020
EPA 6010C
05/14/14 16:22
JDH
Magnei'Onl[7439-95-4]^ `,
16.5
mg/L
1
0.230
1.00
4E13020
EPA 6010C
05/14/14 16:22„
JDH
Molybdenum [7439.-98=7]^-
0.0511
J
mg/L
1
0.0250
0.100
4E13020
EPA 6010C
05/14/14 16:22
JDH
Nickel,[7440?02-0]^ -,
0.0405
J
mg/L
1
0.0180
0.100
4E13020
EPA 6010C
05/14/14 16:22
JDH
Potassium [7440-69-7]^ .:
1120
mg/L
1
1.50
5.00
4E13020
EPA 6010C
05/14/14 16:22
JDH
Selenium f[7782 49 2J^a ' .?" ;`
0.0500
U
mg/L
1
0.0500
0.100
4E13020
EPA 6010C
05/14/14 16:22
JDH
Sodi'4 7440=23=5]^ "-':
96.5
mg/L
1
4.00
5.00
4E13020
EPA 6010C
05/14/14 16:22
JDH
Zinc[7440.66-61^!:?
0:384
mg/L
1
0.0380
0.100
4E13020
EPA 6010C
05/14/14 16:22
JDH
Anal vte rCAS Numlierl`'.' ?:,• '
Ammonia as N,[7664=41-7]^
Biochemical"Oxygen Demand
Chemical'Oxygen Demand:.
Nitrate as.N, [147.97=55-8]^
Nitrite a`s N•[34797=65-0]^ ."
Phosphorus-[7723-14-'0]",
Sodium Adsorption Ratio [ECL-0143]
Sulfate -as 504,[148U8.79.8]^
Results
Maa
Units
DF
MDL
Q
Batch
Method
Analyzed
56
D
mg/L
90
4.0
9.0
4EO7005
EPA 350.1
05/07/14
11:00
5600
mg/L
1
2.0
2.0
4EO7003
SM 521OB-2001
05/07/14
12:41
19000
mg/L
1
400
400
4EO8019
SM 5220D-1997
05/09/14
11:50
330
D
mg/L
10
22
50
4E12004
EPA 300.0
05/12/14
12:22
17
mg/L
1
0.025
0,10
4EO9014
EPA 353.2
05/09/14
10:22
0.20
mg/L
1
0.017
0.10
4EO6028
EPA 353.2
05/06/14
15:51
400
D
mg/L
400
10
40
4E16009
EPA 365.4
05/19/14
12:55
0.751
[blank]
1
4E13020
CSU Method
05/15/14
10:53
97
D
mg/L
10
29
50
4E12004
EPA 300.0
05/12/14
12:22
Total I(jeldaFSl'Nitrogen [ECL-0162]^ 1300 D mg/L 100 26 48 4E16008 EPA 351.2 05/19/14 11:28
Total Solids [ECL-0168]^ - 3.4 % by Volume 1 0.0010 0.0010 4EO8035 SM 254OB-1997 05/08/14 12:53
Totel`$usuended Solids'rECL-0169]^ 21000 mg/L 1 1.0 1.0 4EO8010 SM 254OD-1997 05/08/14 08:54
ft
C1y
JOC
J0C
AIB
CV
Ciy
C1V
JDH
A76
Civ
MMR
MMR
Notes
QB-01
Page 4 of 14

ANALYTICAL RESULTS
Lab Sample ID: C406268-01
Sampled: 06/03/14 08:00
Sampled By:.Brooks Williams
CeNSI-RemO
www.encolabs.com
Received: 06/03/14 13:08
Work Order: C406268
-^ ENCO.'l�ry."certlfiedanalyle[NC 5911
nalyte-rCAS NWnberl - Results Flag ni DF MDL POLL Batch Method Analyzed
Sty£
lercury"[7439=97 6]^=> -' . 0.000850 U mg/L 1 0.000850 0.00100 4FO4023 EPA 7470A 06/06/14 13:45 T1D
M"0.(tot61;recoverable) by EPA r6000/7000 Series Methods
= ENCO Cary certified analyte [NC 59V
' Analvte'-rcAS Numbed.
Results ,
Flaa
Units
DF
IMDDL
PPOL,
Bich
Method
Aluminum,[7429-90=5]^ .
206
mg/L
1
0.290 -
1.00
4FO9021
EPA 6010C
Arsenlc[7440-38-2]^ ` " „
0.0540
U
mg/L
1
0.0540
0.100
4FO9021
EPA 6010C
Boron [7440-`42-8]^-
0.141
J
mg/L
1
0.0500
0.500
4FO9021
EPA 6010C
Cadmium,[7440-43-9]^,",..:
0.00360
U
mg/L
1
0.00360
0.0100
4FO9021
EPA 6010C
Calciulli-[7440 f70,-2]^ , ;
2250
mg/L
1
0.390
1.00
4FO9021
EPA 6010C
Copper[7440-50=8]^ :.
0.448
mg/L
1
0.0160
0.100
4FO9021
EPA 6010C
Lead [7439-92-1-]^--,,,.. '.,;_"-, ; -
0.0210
U
mg/L
1
0.0210
0.100
4FO9021
EPA 6010C
Magnesium [7439=95=4]^ :`: ° -
49.0
mg/L
1
0.230
1.00
4FO9021
EPA 6010C
Molybdenum [7439 9,8-7]^---: -
0.0606,
J
mg/L
1
0.0250
0.100
4FO9021
EPA 6010C
NickeL[7440=02-0]^,,_ =
6.0268
J
mg/L
1
0:0180
0.100
4FO9021
EPA 6010C
Potassium [7440-09=7]^-. ,
731
mg/L
1
1.50
5:00
4FO9021
EPA 6010C
14- ^
Seleniuro;[7782-49=2]. ,;-, ' "�
0.0500
U
mg/L
1
0.0500
0.100
4FO9021
EPA 6010C
Sodium,[7440-23 3]^-
14S
mg/L
1
4.00
5.00
4FO9021
EPA 6010C
Zinc,[7440-66'!'T - '. ,' -
0.970
mg/L
1
0.0380
0.100
4FO9021
EPA 6010C
ElassicaKhdmistly Parameters
-"-^,='ENCOCarycertlfiedana/yte[NC 591j
Analyzed AL Notes
06/13/14 13:35.. JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/1413:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
06/13/14 13:35 JDH
Analvte'fCAS Numbed '• .-
Results
Flag
Units
DF
MDL
PPL
Batch
Method
Analyzed
Ammonia as,N [7664-41-7]^ ' .
120
D
mg/L
90
4.0
9.0
4FO5003
EPA 350.1
06/05/14 11:03
Biochemical Oirygen Demand _
11000
mg/L
1
2.0
2.0
4FO4016
SM 521OB-2001
06/04/14 12:22.
[ECL=0017]^
Chemicai:6kygen,`Demand"", ., '
27000
mg/L
1
400
400
4FO5022
SM 5220D-1997
06/05/1418:52
[ECL-0035].. V
Chloride [16887-'00=6]^r, `' "
510
D
mg/L
10
22
50
4FO5028
EPA 300.0
06/05/14 18:18
Nitrate as N [14797=55-8]^: _ `
16
mg/L
1
0.025
0.10
4FO9027
EPA 353.2
06/09/14 11:03
Nitrite as,N [14Z97 65-0]^=;'
1.8
mg/L
1
0.017
0.10
4FO3025
EPA 353.2
06/03/14 15:02.
Phosphorus:[7723-14-0]^,° -=
450
D
mg/L
400
10
40
4FO6002
EPA 365.4
06/09/14 12:16
Sodium Adsorption_Ratio [ECL-0143]'.
0.826
[blank]
1
4FO9021
CSU Method
06/13/14 15:13
Sulfate,as SO4 [14808-79-8]^ • .
97
D
mg/L
2
5.8
10
4FO5028
EPA 300.0
06/05/14 19:26
Totallddidahl Nitrogen [ECL-0162]^
1900
D
mg/L
100
26
48
4FO6001
EPA 351.2
06/09/14 10:08
Total Solids [ECL-0168]^`;
4.0
% by Volume
1
0.0010
'0.0010
4F05032
SM 254OB-1997
06/05/14 14:55
Total Suspended Solids [ECL-0169]^
28000
mg/L
1
1,0
1.0
4FO9004
SM 254OD-1997
06/09/14 09:20
ft Notes
C1V
J0C
J0C
CV
CV
C1V
clv
JDH
CV
c1V
MMR
MMR
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 4 of 13

CeNk,011-00-)
www.encolabs.com
ANALYTICAL RESULTS
Description: SBM Lab Sample ID: C408210-01 Received: 07/01/14 13:30
Matrix: Sludge Sampled: 07/01/14 08:20 Work Order: C408210
Project: Monthly - Week One - SBM Sampled By: Brad Kearney
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 5911
AnalA2 rCAS Numberl
Results
11R4
Units
DF
MIDL
POL
Batch
Method
Analyzed
By Notes
Mercury[7439-97-6]^
0.00340
U
mg/L
1
0.00340
0.00400
4G14016
EPA 7470A
07/14/14 17:25
TiD
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591J
Analvte rCAS Numberl
Results
Flan
Units
DF
MDL
POL
Batch
Method
Analyzed
By Notes
Aluminum [7429-90-5]^
234
mg/L
1
0.290
1.00
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Arsenic[7440-38-2]^
0.0540
U
mg/L
1
0.0540
0.100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Boron [7440-42-8]^
2.67
mg/L
1
0.0500
0.500
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
1
0.00360
0.0100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Calcium [7440-70-2]^
3130
mg/L
1
0.390
1.00
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Copper[7440-50-8]^
0.432
mg/L
1
0.0160
0.100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Lead [7439-92-1]^
0.0210
U
mg/L
1
0.0210
0.100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Magnesium [7439-95-4]^
66.0
mg/L
1
0.230
1.00
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Molybdenum [7439-98-7]^
0.0469
J
mg/L
1
0.0250
0.100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Nickel [7440-02-0]^
0.0363
J
mg/L
1
0.0180
0.100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Potassium [7440-09-7]^
590
mg/L
1
1.50
5.00
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Selenium [7782-49-2]^
0.0500
U
mg/L
1
0.0500
0.100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Sodium [7440-23-5]^
144
mg/L
1
4.00
5.00
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Zinc[7440-66-G]^
1.39
mg/L
1
0.0380
0.100
4GO2020
EPA 6010C
07/07/14 11:06
JDH
Classical Chemistry Parameters
^ - ENCO Cary certified analyze [NC
Analvte rCAS Number]
Ammonia as N [7664-41-7]^
Biochemical Oxygen Demand
[ECL-0017]^
Chemical Oxygen Demand
[ECL-0035]^
Chloride [16887-00-6]^
Nitrate as N [14797-55-8]^
Nitrite as N [14797-65-0]^
Phosphorus[7723-14-0]^
Sodium Adsorption Ratio[ECL-0143]
Sulfate as SO4 [14808-79-B]^
Total Kjeldahl Nitrogen [ECL-0162]^
Total Solids [ECL-0168]^
Total Suspended Solids [ECL-0169]^
Results
Flao
Mnli&j
DF
MDL
POL
Batch
Method'
nA alvzed
ft Notes
95
D
mg/L
90
4.0
9,0
4GO3002
EPA 350.1
07/03/14 12:18
clv
9900
mg/L
1
2.0
2.0
4GO2012
SM 521OB-2001
07/02/14 13:31
30C
12000
mg/L
1
400
400
4GO3020
SM 522OD-1997
07/03/14 18:40
30C
380
D
mg/L
10
22
50
4GO3015
EPA 300.0
07/03/14 21:43
AJB GC-01
14
mg/L
1
0.025
0.10
4GO3025
EPA 353.2
07/03/14 15:30
CV
1.5
mg/L
1
0.017
0.10
4GO1025
EPA 353.2
07/01/14 15:30
clv
360
D
mg/L
400
10
40
4GO3006
EPA 365.4
07/07/14 12:12
c1v
0.696
[blank]
1
4GO2020
CSU Method
07/07/14 14:30
JDH
160
D
mg/L
10
29
50
4GO3015
EPA 300.0
07/03/14 21:43
AJB
1400
D
mg/L
100
26
48
4GO3005
EPA 351.2
07/07/14 10:33
civ
4.2
% by Volume
1
0.0010
0.0010
4GO3013
SM 254OB-1997
07/03/14 11:38
MMR
30000
mg/L
1
1.0
1.0
4GO3019
SM 254OD-1997
07/03/14 12:30
MMR
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 of 14

ANALYTICAL RESULTS
Description: SBM':_ Lab Sample ID:C409527-01
c. Matrix:,, SlWge • Sampled; 08/05/14 08:05
Project:-. Monthly -'Week One - SBM Sampled By: Brooks Williams
_IMetals.by`EPA 6000/7000 Series Methods
BEENS,00
Www.encolabs.com
Received: 08/05/14 11:55
Work Order: C409527
Analvte _69 Numberl Results Flaa Units DE MDL POL Batch_ Method od Analyzed Notes
Mercury.[7439-97-6]'-: 0.00340 U mg/L 1 0.00340 0.00400 4HO7011 EPA 7470A 08/07/14 17:06 TSD
Metals.(total'recoverable) by EPA 6000/7000 Series Methods
ENCO Cary certified analyte [NC 591]
Anallft;TCAS'Numberl.,
Results
Flaa
Units
DF
MDL
POL
Batch
Method
Analyzed
By
Notes
Aluminum ,[7429-90=5]^ •' "
172
D
mg/L
2
0.580
2.00
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Arsenlc+[7440 38-2]` :.
0.108
UD
mg/L
2
0.108
0.200
4H11018
EPA 6010C
08/12/14 14:14
JDH
R-01
Boron [7440-42-8]A
0.333
JD
mg/L
2
0.100
1.00
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Cadmium,[7440-43-9]^ : "
0.00720
UD
mg/L
2
0.00720
0.0200
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Calcium,[7440-70=2]A" -
5790
D
mg/L
2
0.780
2.00
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Coppe47440-50-8]A " --
0.355
D
mg/L
2
0.0320
0.200
4H11018
EPA 6010C
08/12/14 14:14
JDH
R-01
Lead [7439-92-1]^-
0.0420
UD
mg/L
2
0.0420
0.200
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Magnesium [7439-95-4]^
89.6
D
mg/L
2
0.460
2.00
4H11018
EPA 6010C
08/12/14 14:14
JDH
R-01
Molybdenum[7439-98-7]A
0.0881
JD
mg/L
2
0.0500
0.200
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
NickelE7440-62-0]^"
0.0739
JD
mg/L
2
0.0360
0.200
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Potassium [7440-09-7]^
` 636
D
mg/L
2
3.00
10.0
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Selenium [7782=49-2]^_�-- -
0.100
UD
mg/L
2
0.100
0.200
4H31018
EPA 6010C
08/12/14 14:14
JDH
R-01
Sodium [7440-23-S]A
179
D
mg/L
2
8.00
10.0
41113018
EPA 6010C
08/12/14 14:14
JDH
R-01
Zinc[7440-66-6]A-
1.35
D
mg/L
2
0.0760
0.200
41-111018
EPA 6010C
08/12/14 14:14
JDH
R-01
Classical --.Chemistry Parameters
^,- ENCO Cary certfied analyte [NC 59
AnaMe ICAS'Numberl
Ammonia
Biochemical -Oxygen :Demand'
[ECL-0017]^-r:.'-_
Chemical Oxygen Demand-
[ECL=0638]; _.. j
Chloride [16887-00-6]A
Nitrate as'N [14797-55-8]A
Nitrite as N [14797-65-0]A
Phosphorus[7723-14-0]A
Sodiu'm'Adsorption'Ratio [ECL-0143]
Sulfate''as SO4 [14808-79-8]A
Total ,ICjeldahl Nitrogen [ECL-0162]A
Total Solids [ECL=0168]^
Total Suspended Solids [ECL-0169]A
Results
Flaa
ni
DF
NMQL
P L
Batch
Method
nA alyzed
B� Notes
- 93
D
mg/L
90
4.0
9.0
4HO7002
EPA 350.1
08/07/14
10:37
c1V
7700
mg/L
1
2.0
2.0
4HO6008
SM 521OB-2001
08/06/14
11:44
MMR
10000
mg/L
1
400
400
4H08003
SM 522OD-1997
08/08/14
15:03
CV
530
D
mg/L
10
22
50
4H11013
EPA 300.0
08/11/14
15:58
CV
12
mg/L
1
0:025
0.10
4HO6030
EPA 353.2
08/06/14
13:24
CV
0.88
mg/L
1
0.017
0.10
4HO5015
EPA 353.2
08/05/14
14:01
clv
430
D
mg/L
400
10
40
4HO8009
EPA 365.4
08/11/14
12:43
civ
0.639
[blank]
1
4H11018
CSU Method
08/12/14
15:06
JDH R-01
.180
D
mg/L
10
29
50
41-111013
EPA 300.0
08/11/14
15:58
CV
1700
D
mg/L
100
26
48
4HO8008
EPA 351.2
08/11/14
11:06
clv
4.3
% by Volume
1
0.0010
0.0010
4H11008
SM 254OB-1997
08/11/14
11:45
MMR
29000
mg/L
1
1.0
1.0
4HO6025
SM 2540D-1997
08/06/14
14:30
AJB
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
Page 4 of 14

0JNC= I Gom
k, --- 9
www.encolabs.com
ANALYTICAL RESULTS
fiesicilpti6ii: SBM Lab Sample ID: C410397-01 Received: 09/02/14 13:30
MAtrb6 'Sludge Sampled -09/02/14 08:10 Work Order: C410397
,.
P i6ject: Monthly - Week One - SBM Sampled By: Brad Kearney
-:]Miitalis`by.&A
6000/700.0 Series Methods
5VC0 aiy certified analyte [NC 5911
Anaivie rcAS humbiri
Results
Flag
1jaM
aF
MDL
M
Batch
Method
Analyged
Notes
Mercuri. [7439-97-6]A,.
0.00340
U
mg/L
1
0.00340 0.00400
4104025
EPA 7470A
09/05/14 14:31
T1D
IMetals (total recoverable) by EPA 6000/7000 Series Methods
FJVC0 Cay, certified analyte [NC, 59.11
Results
Flaci
Units
PF
MDL
POL
Batch
Method
"n lyzed
Notes
'�
Alumi -[742il- -5]A
343
mg/L
1
0.290
1.00
4103023
EPA 6010C
09/04/14 16:05
JDH
Arsenic [74bm3tlm2]A',:'�
0.0540
U
mg/L
1
0.0540
0.100
4103023
EPA 6010C
09/04/14 16:05
JDH
Boron [7440-42-8]^
0.307
1
mg/L
1
0.0500
0.500
4103023
EPA 6010C
09/04/14 16:05
JDH
QB-01
Cadmi6m [744434]A.
0.00360
U
mg/L
1
0.00360
0:0100
4103023
EPA 6010C
09/04/14 16:05
JDH
-calcliufti [7440-70=Z]A
4110
mg/L
1
0,390
1.00
4103023
EPA 6010C
09/04/14 16:05
JDH
Copper ' �[7440-50-11!i
0.523
mg/L
1
0.0160
0.100
4I03023
EPA 6010C
09104/14 16:05
JDH
Lead [7439-92-1]A----`
0.0210
U
mg/L
1
0.0210
0.100
4103023
EPA 6010C
09/04/14 16:05
JDH
Maqheiilum.[7,,69-95-4]-
73.9
mg/L
1
0.230
1.00
4103023
EPA 6010C
09/04/14 16:05
JDH
Molybdenum [7439-98-7]A, -
.0.0483
1
mg/L
1
0.0250
0.100
4103023
EPA 6010C
09/04/14 16:05
JDH
Nickel' A
0.0452
3
mg/L
1
0.0180
0.100
4103023
EPA 6010C
09/04/14 16:05
JDH
670
mg/L
1
1.50
5.00
4103023
EPA 6010C
09/04/14 16:05
JDH
Selenium [778249-2]A-,--'
0.0500
U
mg/L
1
0.0500
0.100
4103023
EPA 6010C
09/04/14 16:05
JDH
Sodium 17440-23-5]A_
184
Mg/L
1
4.00
5.00
4103023
EPA 6010C
09/04/14 16:05
JDH
Zinc [7440-66-6]A
1.33
mg/L
1
0.0380
0.100
4103023
EPA 6010C
09/04/14 16:05
JDH
[Classical Chemistry Parameters.
SWO avy certified analyte [NC 5.911
Analyte'rCAS Numbed
Results
Flaci
Units
AF
MDL
POL
Batch
Method
Analyzed
BjC
Notes
Amnknia as N,[7664-41-7]-
140
D
mg/L
90
4.0
9.0
4105003
EPA 350.1
09/05/14 10:54
A)B
Bloch ' emical Oxygen*Demand
9100
mg/L
1
2.0
2.0
4103016
SM 521OB-2001
09/03/14 14:45
30C
CECIL.-
Chemical Oxygen , Demand
24000
mg/L
1
400
400
4108012
SM 522OD-1997
09/08/14 16:30
30C
EECL 0di93A-'--
Chloride [16887-00-6]A
450
D
mg/L
10
22
50
4104021
EPA 300.0
09/04/14 21:09
A313
Nilbrate'as'N [3'4797.55-8]^
14
mg/L
1
0.025
0.10
4104008
EPA 353.2
09/04/14 09:16
A)13
Nhrlt6as N [14797-65-0]^ ,
1.4
mg/L
1
0.017
0.10
41021004
EPA 353.2
09/03/14 10:07
AIB
Phosphbrus'[7723-,14-0]^
620
D
mg/L
266.7
6.7
27
4105002
EPA 365.4
09/08/14 1131
AIB
odi
Sodium
0.778
[blank]
1
4103023
CSU Method
09/05/14 09:17
JDH
-S61fate'a'tS64 [148018-79-8]A
65
D
mg/L
10
29
so
4104021
EPA 3010.0
09/04/14 21:09
AJB
Total- I Kjeldahl Nitrogen [ECL-0162]A
1700
D
mg/L
100
26
48
4105001
EPA 351.2
09/08/14 11:23
AIB
Total Solids [ECL-0168]A
4.7
% by Volume
1
0.0010
0.0010
4109013
SM 254OB-1997
09/09/14 11:45
MMR
TotaFSusoended Solids JECL-01691A
34000
mg/L
1
1.0
1.0
4108008
SM 254OD-1997
09/08/14 11:10
MMR
FINAL'
This report relates only to the
sample as received by the
laboratory, and may only be reproduced In full.
Page 4 of 14

www.encolabs.com
ANALYTICAL RESULTS
Description: SBM Lab Sample ID:C412648-01 Received: 10/07/14 14:05
Matrix: Sludge Sampled:10/07/14 08:00 Work Order: C412648
Project: Monthly - Week One - SBM Sampled By: Brooks Williams
Metals by.EPA 6000/7000 Series Methods
^ - ENCO Cary certified anaiyte [NC 5911
Analvte rCAS'Numberl
Results
Fig
MnM
DF
MDL
POLL
Batch
Method
Analyzed
41C Notes
Mercury[7439-97-6]^
0.00340
U
mg/L
1
0.00340 0.00400
4314015
EPA 7470A
10/15/14 13:44
T1D
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary cerGNed analyte [NC 5911
Analyte- rCAS Numberl
Results
Flaa
Units
DF
MDL
PQL
Batch
Method
Analyzed •
y Notes
Aluminum [7429-90-5]^
508
mg/L
1
0.290
1.00
4J15018
EPA 6010C
10/16/14 11:34
JDH
Arsenic-[7440-38-2]^
0.0540
u
mg/L
1
0.0540
0.100
4315018
EPA 6010C
10/16/14 11:34
JDH
Boron [7440-42-8]^
0.417
J
mg/L
1
0.0500
0.500
4J15018
EPA 6010C
10/16/14 11:34
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
1
0.00360
0.0100
4J15018
EPA 6010C
10/16/14 11:34
JDH
Calcium [7440770-2]^
4580
mg/L
1
0.390
1.00
4J15018
EPA 6010C
10/16/14 11:34
JDH
copper[7440-50-8]^
0.866
mg/L
1
0.0160
0.100
4J15018
EPA 6010C
10/16/14 11:34
JDH
Lead [7439-92-1]^
0.0210
U
mg/L
1
0.0210
0.100
4J15018
EPA 6010C
10/16/14 11:34
JDH
Magnesium [7439-95-4]1
75.2
mg/L
1
0.230
1.00
4J15018
EPA 6010C
10/16/14 11:34
JDH
Molybdenum [7439-98=7]^
0.0667
J
mg/L
1
0.0250
0.100
4315018
EPA 6010C
10/16/14 11:3.4
JDH
Nickel[7440-02-0]^
0.0554
J
mg/L
1
0.0180
0.100
4J15018
EPA 6010C
10/16/14 11:34
JDH
Potassium [7440-09-7]^
625
mg/L
1
1.50
5.00
4315018
EPA 6010C
10/16/14 11:34
JDH
Selenium [7782-49-2]^
0.100
UD
mg/L
2
0.100
0.200
4J15018
EPA 6010C
10/16/14 12:43
JDH R-01
'odium [7440-23-5]^
296
mg/L
1
4.00
5.00
4J15018
EPA 6010C
10/16/14 11:34
JDH
Zinc[7440-66-6]^
1.66
mg/L
1
0.0380
0.100
4J15018
EPA 6010C
10/16/14 11:34
JDH
Chemistry Parameters
^ - ENCO Cary cerb'Aed analy
Analvte rCAS Numberl
Ammonia as N.[7664-41-7]^
Biochemical Oxygen Demand
Chemical Oxygen Demand
Chloride [16887-00-6]^
Nitrate as N'[14797-55-B]^
Nitrite as N.[14797-65-O]^
Phosphorus[772344-0j^
Sodium Adsorption Ratio
Sulfate as SO4 [14808-79-8]^
Total Kjeldahl Nitrogen
Total Solids
Total Suspended Solids
Results
Flag
Units
RE
MDL
PPOL
Batch
Method
Analyzed
ft Notes
110
D
mg/L
90
4.0
9.0
4310006
EPA 350.1
10/10/14
11:48
clv
7600
mg/L
1
2.0
2.0
4JO8006
SM 521OB-2001
10/08/14
10:12
JOC
32000
mg/L
1
800
800
4J14017
SM 5220D-1997
10/14/14
14:39
30C
820
D
mg/L
10
22
50
4J09008
EPA 300.0
10/09/14
22:08
CV
8.4
mg/L
1
0.025
0.10
4116020
EPA 353.2
10/16/14
15:12
CV
2.6
D
mg/L
5
0.084
0.50
4JO8029
EPA 353.2
10/08/14
15:30
c1v
790
D
mg/L
400
10
40
4J10004
EPA 365.4
10/13/14
13:03
clv
1.19
[blank]
1
4315018
CSU Method
10/16/14
15:20
JDH
110
D
mg/L
10
29
50
4J09008
EPA 300.0
10/09/14
22:08
CV
2200
D
mg/L
100
26
48
4J10003
EPA 351.2
10/13/14
11:20
c1V
5.7
% by Volume
1
0.0010
0.0010
4309030
SM 254OB-1997
10/09/14
13:53
MMR
40000
mg/L
1
1.0
1.0
4309006
SM 254OD-1997
10/09/14
08:45
MMR
FINAL
This report relates only to the sample as received by the laboratory, and may only be reproduced In full.
Page 4 of 14

www.encolabs.com
ANALYTICAL RESULTS
DescripUon:,-SBM-
Lab Sample ID:C413507-01
Received: 11/04/14 13:00
.` Matrixd"Sludge:. ..
Sampled:11/04/14
07:30
Work Order: C413507
Project; Monthly-- Week One - SBM
Sampled By: Brad Kearney
Metals.by`EPA.6000/7000 Series Methods
ENCO'ary, cLWed ana/yte [NC 5911
Ana lvie-fCAS'Numberl.
Results
Fig
Units
o6
MDL
P L
Batch
Method
Analyzed
By Notes
Mercury [7439-97-6]^
0.00340
U
mg/L
1
0.00340
0.00400
4K32027
EPA 7470A
11/12/14 16:19
TiD
Metals (total; recoverable)' by EPA 6000/7000 Series Methods
,^ - aVCO Cary certl6ed anal a [NC 5911
Analvte=rCAS.Numbe'h
Results
Flag
Units
DF
MDI
L9J.
Batch
Method
Analyzed
Ry Notes
Alurhinum [7429-90-sj^
547
mg/L
1
0.290
1.00
41(10019
EPA 6010C
11/13/14 13:45 -
JDH
Arsenic [7440 38 2]^.,.
0.0540
U
mg/L
1
0.0540-
0,100
41<10019
EPA 6010C'
11/13/14 13:4.5
JDH
Boron [7440-42-8]^
0.921
mg/L
1
0.0500
0.500
41(10019
EPA 6010C
11/13/14 13:45
JDH
Cadmium;(7440-43-9]^
0.00360
U
mg/L
1
0.00360
0.0100
41(10019
EPA 6010C
11/13/14 13:45
JDH
Calcium;[7440-70-2]^
3710
mg/L
1
0.390
1.00
4K10019
EPA 6010C
11/13/14 13:45
JDH
topper,[7440-504]^
0.717
mg/L
1
0.0160
0,100
4K10019
EPA 6010C
11/13/14 13:45
JDH
Lead '[7439-92-1]^,
0.0237
J
mg/L
1
0.0210
0.100
41(10019
EPA 6010C
11/13/14 13:45
JDH
Magn64diii [7439-95-4]"
77.5
mg/L
1
0.230
1.00
41<10019
EPA 6010C
11/13/14 13:45
JDH
Molybdenum [7439=98-7j^
0.0664
J
mg/L
1
0.0250
0.100
4K10019
EPA 6010C
11/13/14 13:45
JDH
Nickeh[7440-02-0]^ -
0.0448
J
mg/L
1
0.0180
0.100
4K10019
EPA 6010C
11/13/14 13:45
JDH
Potassium [7440-09-7]^.. -
669
mg/L
1
1.50
5.00
4K10019
EPA 6010C
11/13/14 13:45
JDH QB-01
Seleniumy[7782-49-2]^,
0.0500
U
mg/L
1
0.0500
0.100
4K10019
EPA 6010C
11/13/14 13:45
JDH
Sodium [7440-23-5]^ ,
347
mg/L
1.
4.00
5.00
4K10019
EPA 6010C
11/13/14 13:45
JDH
Zinc•[7440-66-6]^ -
1.98
mg/L
1
0.0380
0.100
41<10019
EPA 6010C
11/13/14 13:45
JDH
Classical- Chemistry' Parameters
^'= ENCO..Cary certified ana/yte [NC -5911
Analvte`iCAS.Numberl '.
Results
Flag
ni
DF
MQL
PQ_L
Batch
Method
Analyzed
By L19SE
Ammonia as N:[7664-41-7]^
140
D
mg/L
90
4.0
9.0
4KO7018
EPA 350.1
11/07/14 13:40
SHA
Biochemical Oxygen,Demarid^
4300
mg/L
1
2.0
2:0
4KO5021
SM 521OB-2001
11/05/14 12:16
i0C B-07
Chemical Oxygen Demand^
26000
mg/L
1
800
800
41<14017
SM 522OD-1997
11/14/14 11:12
30C
Chloride [16887-00-6]^
590
D
mg/L
10
22
50
4KO6002
EPA 300.0
11/06/14 13:09
CV
Nitrate as N-[14797-55-8]^
14
mg/L
1
0.025
0.10
4K10025
EPA 353.2
11/10/14 13:59
AIB
Nitrite as N [14797-65-0]^
0.41
mg/L
1
0.017
0.10
4KO4033
EPA 353.2
11/04/14 17:54
SHA
Phosphorus [7723-14-0]^.
630
D
mg/L
400
10
40
4KO7015
EPA 365.4
11/10/14 13:13
SHA
Sodiun-im.orption,Ratio _
1.54
[blank]
1
4K10019
CSU Method
11/13/14 15:56
JDH
Sulfate as SO4 [34808-79-8]^
85
D
mg/L
10
29
50
4KO6002
EPA 300.0
11/06/14 13:09
CV
Total l(jeldahl Nitrogen^
2000,
D
mg/L
100
26
48
4KO7014
EPA 351.2
11/10/14 11:37
SHA
Total Solids^ "
4.3
% by Volume
1
0.0010
0.0010
41<10030
SM 254OB-1997
11/10/14 15:45
MMR
Total Suspended Solids^ ,
rs.
= r,
28000
mg/L
1
1.0
1.0
41(10002
SM 254OD-1997
11/10/14 09:43
MMR
FINAL -, '" „' ., " '" This report relates only to the
sample as received by the laboratory, and may only be reproduced In full.
Page 4 of 14

www.encolabs.com
ANALYTICAL RESULTS
Description: SBM Lab Sample ID: C415209-01 Received: 12/02/14 13:10
Matrix: Sludge Sampled; 12/02/14 07:45 Work Order: C415209
Project: Monthly - Week One - SBM Sampled By: Brad Kearney
(Metals by EPA 6000/7000 Series Methods i
^ - ENCO Cary cerGhed analyte [NC 597]
Analyte rCAS Numberl Results Flag Units PF MDDL POLL Batch Method Analyzed ft Notes
Mercury [7439-97-6]^ 0.00340 U mg/L 1 0.00340 0.00400 4LO8039 EPA 7470A 12/09/14 14:38 T1D
Metals (total recoverable) by EPA 6000/7000 Series Methods
•- - wvLv Lary cemneo anaryre 1 vL x5uj
Analyte rCAS Numbed
Results
FlactUnits
DF
MDL
FQL
Batch
Method
Analyzed
Ay Notes
Aluminum [7429-90-5]^
298
mg/L
1
0.290
1.00
41-10025
EPA 6010C
12/11/14 15:43
JDH
Arsenic[7440-38-2]^
0.0540
U
mg/L
1
0.0540
0.100
41-10025
EPA 6010C
12/11/14 15:43
JDH
Boron [744042-8]^
0.224
J
mg/L
1
0.0500
0.500
41-10025
EPA 6010C
12/11/14 15:43
JDH
Cadmium [7440-43-9]^
0.00360
U
mg/L
1
0.00360
0.0100
41-10025
EPA 6010C
12/11/14 15:43
JDH
Calcium [7440-70-2]^
3120
mg/L
1
0.390
1.00
41-10025
EPA 6010C
12/11/14 15:43
JDH
Copper [7440-50-8]^
0.385
mg/L
1
0.0160
0.100
4L10025
EPA 6010C
12/11/14 15:43
JDH
Lead [7439-92-1]^
0.0210
U
mg/L
1
0.0210
0.100
41-10025
EPA 6010C
12/11/14 15:43
JDH
Magnesium [7439-95-4]1
56.8
mg/L
1
0.230
1.00
41-10025
EPA 6010C
12/11/14 15:43
JDH
Molybdenum [7439-98-7]^
0.0560
J
mg/L
1
0.0250
0.100
4L10025
EPA 6010C
12/11/14 15:43
JDH
Nickel[7440-02-O]^
0.0546
J
mg/L
1
0.0180
0.100
41-10025
EPA 6010C
12/11/14 15:43
JDH
Potassium [7440-09-7]^
572
mg/L
1
1.50
5.00
4L10025
EPA 6010C
12/11/14 15:43
JDH
Selenium [7782-49-2]^
0.0500
U
mg/L
1
0.0500
0.100
41-10025
EPA 6010C
12/11/14 15:43
JDH
Sodium [7440-23-5]^
299
mg/L
1
4.00
5.00
4L10025
EPA 6010C
12/11/14 15:43
JDH
Zinc [7440-66-6]^
0.792
mg/L
1
0.0380
0.100
4L10025
EPA 6010C
12/11/14 15:43
JDH
Classical Chemistry Parameters
^ - ENCO Cary celVfied analyte [NC 5911
Analyte rCAS Numberl
Results
Flag
Units
DF
MOIL
POL
Batch
Method
Analyzed
Notes
Ammonia as N [7664-41-7]^
150
D
mg/L
90
4.0
9.0
4LO8031
EPA 350.1
12/09/14 13:31
SHA
Biochemical Oxygen Demand^
12000
mg/L
1
2.0
2.0
4LO3006
SM 521OB-2001
12/03/14 11:52
JOC
Chemical Oxygen Demand^
30000
mg/L
1
800
800
4LO8016
SM 5220D-1997
12/08/14 17:09
30C
Chloride [16887-00-6]^ '
670
D
mg/L
10
22
50
4LO5016
EPA 300.0
12/05/14 17:56
AIB
Nitrate as N [14797-55-8]^
16
mg/L
1
0.025
0.10
41-15010
EPA 353.2
12/15/14 10:00
AIB
Nitrite as N [14797-65-O]^
0.095
J
mg/L
1
0.017
0.10
4LO2039
EPA 353.2
12/02/14 17:08
SHA
Phosphorus [7723-14-O]^
570
D
mg/L
400
10
40
41-08004
EPA 365.4
12/10/14 11:29
SHA
Sodium Adsorption Ratio
1.45
[blank]
1
41-10025
CSU Method
12/12/14 09:07
JDH
Sulfate as SO4 [14808-79-8]^
20
mg/L
1
2.9
5.0
41-10010
EPA 300.0
12/10/14 12:33
A36
Total Kjeldahl Nitrogen
2000
D
mg/L
100
26
48
4L08003
EPA 351.2
12/10/14 09:33
SHA
Total Solids^
3.9
% by Volume
1
0.0010
0.0010
4LO3024
SM 254OB-1997
12/03/14 14:18
MMR
Total Suspended Solids^
24000
mg/L
1
1.0
1.0
4LO3003
SM 254OD-1997
12/03/14 08:59
MMR
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 14

HOOSIER MICROBIOLOGICAL
I4A
Ld
L A B O R A T O R Y
Sample: 280818
March 26, 2014
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
Testing • Research • Consulting
Multiple Analysis Report
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:09 AM,
01/22/2014, and collected at 1:00 PM, 01/21/2014:
TEST - METHOD
RESULT
MDL*
Date Complete
Salmonella -EPA 1682
<3 MPN/4 g dry
3 MPN/4 g dry
01/25/2014
Helminth Ova-EPA/625/R-92/013
<1 ovum/4g dry
1 ovum/4 g dry
03/24/2014
Solids, total-SM 2540G
1.81%
0.005%
01/31/2014
*Minimum Detection Level
This testing was completed by J.B. Please feel free to contact us if we can be of further service to you.
Sinc
4�70"
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone] page. 1
E-mail. 102255.152*ompuserve.cona Web Site: hh`p://www.hmLcom

H O OS I ER M I C R O B 10 LOG I C A L
I
L A B O R A T O R Y
Sample: 280817
March 26, 2014
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
Testing • Research* Consulting
Multiple Analysis Report
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:08 AM,
01/22/2014, and collected at 1:00 PM, 01/21/2014:
TEST - METHOD RESULT MDL* Date Complete
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 01/24/2014
Solids, total-SM 2540G
*Minimum Detection Level
4.91 % 0.005% 01 /31 /2014
This testing was completed by J.B. Please feel free to contact us if we can be of further service to you.
Sincerely,
Aamoa
al Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
L
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone] page: 1
E-mail. [e-mail] Web Site: http://www.hniLcom

HOOSIER M ICROBIOLOGICAL
L A B O R A T O R Y
Sample: 284128
June 5, 2014
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
Testing • Research • Consulting
Multiple Analysis Report
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 9:50 AM,
04/23/2014, and collected at 1:45 PM, 04/21/2014:
TEST - METHOD
RESULT
MDL*
Date Complete
Solids, total-SM 2540G
1.34%
0.005%
05/01/2014
Salmonella -EPA 1682
<3 MPN/4 g dry
3 MPN/4 g dry
05/01/2014
Helminth Ova-EPA/625/R-92/013
<1 ovum/4g dry
1 ovum/4 g dry
06/04/2014
*Minimum Detection Level
This testing was completed by J.B. and N.R. Please feel free to contact us if we can be of further service to you.
Sincerel ,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Faz: [phone] Page: 1
E-mail. [e-mail] Web Site: http://www.hmLcom

H OOS IER M IC ROB IOLOGI CA L
L A B O R A T O
Sample: 284129
June 5, 2014
R Y Testing • Research • Consulting
Multiple Analysis Report
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 9:50 AM,
04/23/2014, and collected at 1:55 PM, 04/21/2014:
TEST - METHOD RESULT MDL" Date Complete
Solids, total-SM 2540G 4.21% 0.005% 05/01/2014
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 04/25/2014
`Minimum Detection Level
This testing was completed by J.B. and N.R. Please feel free to contact us if we can be of further service to you.
Sincerely,
uonal A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone] Page: 1
E-mail: [e-mail] Web Site: http.11www.hmLcom

H OOSIER MICROBIOLOGICAL
I
L A B O R A T O R Y
Sample: 288125
December 5, 2014
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
Testing • Research • Consulting
Multiple Analysis Report
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 11:49 AM,
07/09/2014, and collected at 12:55 PM, 07/08/2014:
TEST - METHOD
RESULT
MDL*
Date Complete
Salmonella -EPA 1682
<3 MPN/4 g dry
3 MPN/4 g dry
07/24/2014
Helminth Ova-EPA/625/R-92/013
<1 ovum/4g dry
1 ovum/4 g dry
08/28/2014
Solids, total-SM 2540G
0.92%
0.005%
07/10/2014
*Minimum Detection Level
This testing was completed by J.B. and J.B. Please feel free to contact us if we can be of further service to you.
Sincerely,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone] page: 1
E-mail: [e-mail] Web Site: http://Www.hmLcom

H OOS I ER M I C ROB I OLOGICAL
1A I
L A B O R A T O R Y
Sample: 288124
December 5, 2014
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
Testing • Research • Consulting
Multiple Analysis Report
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 11:49 AM,
07/09/2014, and collected at 1:00 PM, 07/08/2014:
TEST - METHOD RESULT MDL* Date Complete
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 07/11/2014
Solids, total-SM 2540G 4.23% 0.005% 07/10/2014
*Minimum Detection Level
This testing was completed by J.B. and J.B. Please feel free to contact us if we can be of further service to you.
Sincerely,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone] page: 1
E-mail. [e-mail] Web Site: http://Www.hmLcom

H OOS I E R M I C ROB I O LOGICAL
JH
L A B O R A T O R Y
Sample: 293440
December 4, 2014
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
WAS
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
Testing • Research • Consulting
Multiple Analysis Report
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:20 AM,
10/09/2014, and collected at 1:00 PM, 10/08/2014:
TEST - METHOD
RESULT
MDL`
Date Complete
Salmonella -EPA 1682
<3 MPN/4 g dry
3 MPN/4 g dry
10/14/2014
Helminth Ova-EPA/625/R-92/013
<1 ovum/4g dry
1 ovum/4 g dry
11/19/2014
Solids, total-SM 2540G
2.8230%
0.005%
10/15/2014
"Minimum Detection Level
This testing was completed by J.B. and J.B. Please feel free to contact us if we can be of further service to you.
Sincerely,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone] page: 1
E-mail: [e-mail] Web Site: http://www.hmLcom

H O G S I E R M I C R O B I O LOG I CAL
jj
k A
L A B O R A T O R Y Testing • Research • Consulting
Multiple Analysis Report
Sample: 293441
December 4, 2014
Mr. Randy Cutchin
Novozymes N.A.
PO Box 576
Franklinton, NC 27525
RE: PWS ID#: Unavailable
Novozymes N.A.
SBM
77 Perry Chapel Church Rd.
Franklinton, NC 27525
Dear Mr. Cutchin:
The following are the result(s) of the test(s) performed on the sample(s) received at HML, Inc. at 10:20 AM,
10/09/2014, and collected at 1:00 PM, 10/08/2014:
TEST - METHOD RESULT MDL" Date Complete
Salmonella -EPA 1682 <3 MPN/4 g dry 3 MPN/4 g dry 10/14/2014
Solids, total-SM 2540G 5.35% 0.005% 10/15/2014
'Minimum Detection Level
This testing was completed by J.B. and J.B. Please feel free to contact us if we can be of further service to you.
Sincerely,
Donald A. Hendrickson, Ph.D.
President - Microbiologist
Chemistry Lab #C-18-01
Microbiological Lab #M-18-03
DAH/skp
912 West McGalliard, Muncie, IN 47303-1702 Phone: [phone] Fax: [phone] page: 1
E-mail: [e-mail] Web Site: http://www.hml.com