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HomeMy WebLinkAboutWQ0003351_2014 Residual Annual Report_20150219�EMA ^s �fl ,Resources, Inc. February 13, 2015 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2014 Annual Report - Mocksville Treatment and Land Application of Residuals Permit No. WQ0003351 Dear Sir or Madam: Enclosed are three copies of the 2014 Annual Report for the above referenced land application permit. During 2014 EMA Resources, Inc. land applied 43.92 dry tons of wastewater residuals to 20.3 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sinc y, Brent Collins Director of Technical Services brent. collins&emaresourcesinc. com FEg i 9 zm5 Phone 336.751.1441 — Fax 336.751.1442 755 Yadkinville Road — Mocksville, NC 27028 l 0--l>6 �--� -� l s, Inc. Town of Mocksville 2014 Annual Report Residuals Land Application Permit No. WQ0003351 Prepared By: EMA Resources, Inc. Phone 336.751.1441 — Fax 336*751.1442 755 Yadkinville Rd — Mocksville, NC 27028 MCEVEDIDEM041% FEB 19 xK jP9 C9On WQ Permit#: ANNUAL LAND APPLICATION CERTIFICATION FORM WQ0003`351 County: Davie Year: 2014 iJ Facility Name (as shown on permit): Land Application-Operator: EMU Resources Inc. Town of Mocksville Phone: 336-751-1441 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes [3No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not -land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepen-nit: 4 Total number of fields utilized for land application during the year: 2 Total amount of dry tons applied during the year for all application sites: 43.92 Total number of acres utilizes for land application during the year: = 20.3 Part B -Annual Compiance Statement: I, Facility was compliant during calendar year 2014 with all conditions of the land application permit IJ (including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes ElNo If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or J the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies { of laboratory results are attached. �— 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. J 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T. 1 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 1 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. j 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Christine Bralle, Town Manager �I Permittee eWTit e(type or print) :_k� Signature of Permittee Date 517.015 ;e5�e 1/23/2015 Signature of Prep r* Date Signature of Land Applier Date (if different from Pe ' e) (if different from Permittee and Preparer) -` * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - I WQ Permit Number: WQ0003351 Laboratory: 1) Facility Name: Town of Mocksville 2) Residual Source WQ # or 3) NPDES #: NCO021491 4) WWTP Name: Dutchman's Creek WWTP 5) Residual Analvsis Data A&L Eastern Laboratories, Inc. Parameter (mg/kg) Conc. Limit (mg/kg a Sample or Composite Date 7/21/14 Percent Solids (%) NA 3.5 Arsenic 75 6 Cadmium 85 3 Copper 4,300 475 Chromium NA 62 Lead 840 56 Mercury 57 3.2 Molybdenum 75 5 Nickel 420 33 Selenium. 100 6 Zinc 7,500 1610 Total Phosphorus NA 18400 TKN NA 39400 Ammonia -Nitrogen NA 8570 Nitrate and Nitrite NA 22.9 " For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for sub Wing false information, including the possibility of fines and imprisonment for knowing violations." Z 15 11015 Signature of Pre re Date *Preparer is defined in CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ0003351 Laboratory: 1) A&L Eastern Laboratories, Inc. Facility Name: Town of Mocksville 2) Residual Source 3) NPDES # or WQ#: NC0021491 4) WWTP Name: Dutchman's Creek WWTP 5) Residual Analvdv. Data Parameter Potassium "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer bate *Preparer is defined in 40 R Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* ! Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Mocksville Total Dry Tons Applied (Annual):-3,984d =r ermit #: WQ0003351 Cation Exchange Capacity (non 503 only): -Operator: John Garwood Owner: John Garwood Predominant Soil Series: GnB2 - Gaston Lcres Used: 15.6 Acres Permitted: 15.6 Site #: NC-MK03 Field #: 1 1 _ tesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 11 1213 4J L5J L6J7 8 9 10 11 12 Com- 7/21/14 la ite te `io Solids 3.5 Arsenic 6 Lead 3 475 62 56 3.2 IMolyb- 5 ,demur Nickel 33 selenium 6 Zinc 1610 Total -' Phos- 18400 horus 'nnual Heavy Metal Field Ill2 3 ITotal _ nT/Ac./ App. 'Event 2.55 Arsenic , admium %opper ,21_2,42'.6''s -hromiurn,0, 3u 7 0 0'Q,0 _0 Lead Nickel e ,lenium Zinc Total Phos- in lbs/acre --1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am vare that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/23/2015 .%gnature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 1 Acres Utilized: Land Owner: John Garwood Annual D Tons Applied: .° 39$4M=' ° 1 Dry Pp �,�„-0Site #: NC-MK03 Acres Permitted: Operator: John Garwood Predominant Soil Series: GnB2 - Gaston Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN: 15.6 15.6 Volume applied Volume Residual Sources Soil Precip. Y o Z a Nitrate Name of Cro Type p yp ° (enter one) Solids/ % Applied per (NPDES #, WQ#, Cond. Past 24 b w �; 7y T'KN cx o and PAN Applied Receiving Residual Y o A Liquid Solids Acre Fert., Animal D (rye Hrs. a w w a Nitrite Ibs/acre ) Application Cu. Yds Gallons D Tons/Ac (Dry ) Waste, etc) Wet, Moist) inches * * * c mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 8/6/14 94500 3.5 xv{r 'Q``$l°4;`-w z__,.•- Dutchman's Creek Dry D <.5" S 0.5 0.3 39400 8570 22.9 ;23i97�2�,NA�1 1`-=' Fescue 8/7/14 80500 3.5 Qx753 §` Dutchman's Creek Dry <.5" S 0.5 0.3 39400 8570 22.9 Fescue 12/14/14 14000 3.5�f bTT �, �; Dutchman's Creek Dry <.5" S 0.5 0.3 39400 8570 22.9 Fescue 12/15/14 84000 3.5 „0786a Dutchman's Creek Dry <.5" S 0.5 0.3 39400 8570 22.9 213r0,8 MNA, Fescue 1 w 40 000M t'*` 000 �` 0 ,0`000 � c t 6000, },,IO OUO OOOO� r. m r 'H O:000 v:3S�,IF:."a,1;;'k1."� „E,... A.fi ^ ^�7iuv,av .:;i 1``� :t �y�,y�"A'kx $..,,:• =•T'%`.YF.'>;7;75�ti%r,$•� 4;e1+�,=. f..,� v<.i^u v'.,f is Applications totals on FORM FSF su attach FORM FSF su to this form 's,. ;xa .t,::1'r: ;:Tk..'.T�v'x'4:ur .a"i'P�. „:.., r.. ,,,.._ .. , ;,,r,7, �5, TOTALS:;a" ....... As Cd Cu Cr Pb H Mo Ni Se Zn P 69y252�;. n; _ ' ; �o,0otl,,� Lime Aplied Annuallbs/acre ," : t �, t hr. ��0.03<iu.. .1.�„y �,,.. .:„ - w 'a 1= ... r 1 1.' 8 .7 :�� 0.0�6.�r�� � 3K' ���„��'. ,.. 4 �a22'" • 0.104 0.061~ -,M r r..F./ T6:;,. ,�r=4„ 6.032 u4• _ . � 0.568 . 1.071 - ,U�� ,6':� ;� 0.017 =+gam. -• . �,��,.,. 0.205 - `�. .,0:.1",6 A�:, �.,r��4 0.58 - 0 =,0:=0`3 �.. 0.108.^ ��- 8 �� 19.741 279- =''S-,:•. ,9� : x3;>9$7ss ::R Date lbs/ac Prior Years Cumulative lbs/ac Cumulative lbs ac 36 34 �.. 1338 1 �i��.., �r�^Y,:•1•�3"57..0:033:�- 1 267 1 .Current 15 1 .•0:�3.1%" 25 374 89 2498 Permitted C. P. L. R.**** PAN Limit lst/2nd Crop Y9 2 iPermit ,.. - v'h "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Z—e *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/23/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* L Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Mocksville Total Dry Ton Applied (Annual): ` s A i Annual ermit #: WQ0003351 Cation Exchange Capacity (non 503 only): Operator: Jeff Smith Owner: Town of Mocksville Predominant Soil Series: CeB2 - Cecil A cres Used: 4.7 Acres Permitted: 4.7 Site #: NC-MK05 Field #: 1 _'tesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 1L2-1 L3J L4JL5J 161L7J L8J9 10 11 12 Com- 7/21/14 posite Date /o Solids 3.5 —Arsenic 6 Cadmium 3 Copper 475 ic.hromium 62 Lead 56 vlercury 3.2 IMolyb- 5 denum Nickel 33 selenium 6 Zinc 1610 (Total Phos- 18400 �.nnuai L-'Total -nT/Ac./ App. Event Arsenic �admium .Lead Mercury 0.87 Calculated in lbs/acre Nickel 0D ObO 0 OUQ 0 QOQw 0 000 OT000 OK000 ` 0 000 0 000 PISO'OOQ_, ` ?,- 000 0 Or57. r ... `-,r,.�, -;•� �.y^yi , � fit, � �:•. _ .q:.. <:�... « £, ��lexuum 0 01Q= 0 000 0 000 w 0 OOQ 0 000 ' Ot000 0 000F1 , Oti000 v 0 000 i_0 000, 0 OOU M 0 000 : -0 O10' Zinc > 2 798 OY000`= AMR MW 0 UUO _;#,­0WANE, ar.z0 000 „ 0 000 � 0:0300 0 000,.tP0 000' U 000 �� 79$ Totalnu Phos- n31 979 rt 0 000 3 0 000 { 0 Q00 0 OOC) 0 000# m0 000 0 OOD' fi 0 000 0 000 0 000 0 000 31 975, )horUS s:, >. .... :. -...., y _-..,.. ,. ..r . ':-_.,, ,a '.. .. "i certify, under penalty of law, that this document was prepared under my direction or supervision in accordance wit ,-system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am t_ `vare that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". I' 1/23/2015 C�gnature of Land Applier 1 L, Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Mocksville WQ Permit #: W 0003351 Field #• Q 1 Acres Utilized: Land Owner: Town of Mocksville Annual D ''`'`'`r°i''N 'a'@``-' ':4' - ry Tons Applied: � ;�r- �,,,,Y.,�" 4:,0,8,<�4�n'��;� >�.` ` ,, Site #: NC-MKOS Acres Permitted: P t ed: Operator: Jeff Smith Predominant Soil Series: CeB2 - Cecil Cation Exchange Capacity (non 503): Crop 1 Name: Rye Grass Crop 1 Max. PAN: 115 Crop 2 Name: Rye Grass Cron 2 Max. PAN: 4.7 4.7 50 N � Volume applied PP Volume Residual Sources Soil Precip. � C o E Z � Nitrate Name of Crop Type o(enter >~ one) Solids/ % Applied per P (NPDES #, W # Q , Cond. Past 24 c� .. � a� m ., TKN c and PAN Applied Receiving Residual Liquid Solids Acre Fert., Animal (Dry, Hrs. o� * N � w. Nitrite lbs/acre ( ) Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, Moist) inches c 0 * 0 mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 12/13/14 14000 3.5. r;s.,'r'043,5 ,$,>s Dutchman's Creek Dry <,5" S 0.5 0.3 39400 8570 22.9 ; �i1+:7;88 x , N'Ar Fescue 12/14/14 14000 3.5 Dutchman's Creek Dry <.5" S 0.5 0.3 39400 8570 22.9 10NAm Fescue r Q, 000, 0 Q00 " `0r000 u G Q 000 0 66Oz$ 0 0�0 0/OOyO" `) �O��OOOF '"�i' 5,�0AQdU h<3'�Or000?3-' is '��0,"0(i0 `` 1 'IUv0f00}'k�g�5.000O�r{ k,�AO000'� ;x0 000�� tTOTALS: d,'Mk, xs .:a r?1 l�747j9 ,, �.FY 4 £ 9..... kE , , ,; .'t4 Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form) .. u,;i,¢0 , `;„°28�000 �� As Cd Cu Cr Pb H Mo Ni Se Zn P ..y; ;=23 t575 w,,> b�t000 �' Lime A lied Annual lbs/acrea„ r, WM r,>t.r . � 0`b� �.sx�. 10. .. ,, w, , � ���. 0.0�5,. �_♦ ,� A'... '„'a,d , ,,,0="108�� ;�,. � � b9;7 s :,,. 7!: , � � � 0 b0.6.. E.b -.w. Ff- 0�009,., w h,- $�� �"�} ��;w � , '�-.� �,. .N�. :, 0.065 ..a a.n.,..-..4.?:Ov:b7„c'.5•s.s,:.u... 0.028 .�0�826�<, 4.589 fx�,h . y. 0.424 , , � 0.681 ..��,. 0.032 �,n.h. . �,: 0.151 xCurrent �.0:05:7F� �; ,, 0.518 ':.0,0':0�= ��t,,..1 ,�;�..�_ 0.057 >,�. �'�9'8>i 12.796 ,3);979s . _ Date lbs/ac Prior Years Cumulative lbs/ac Cumulative033, 1 s/ac 36 34 <X.A..�a°g4 1338 .. 267 15 _ a: n-.}.....;:` 374 89 ' - SAS 2498 ............ . Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop P 5 .::: ;. tr.. w. 1 certay, under penaity oI iaw, that this aocument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/23/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Page: 1 of 2 Report Number: 14-203-0204 Account Number: 46245 Submitted By: ROY WHITAKER Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 www.oleastem.com A&L Eastern Laboratories, Inc. 7621 White -pine Road Richmond; Wginia23237 (804) 743-9401 Fax (804) 271-6446 Project: MOCKSVILLE NC NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/21/201410:30:00 Lab Number: 56605 Date Received: 07/22/2014 00:00 Sample Id : DUTCHMAN CREEK WWTP Date Reported: 07/25/2014 i oiai aouas 3.50 35000 100.0 JM Moisture * 96.50 100.0 JM Total Kjeldahl Nitrogen 3.94 39400 10.0 JM Total Phosphorus 1.84 18400 100 KM Total Potassium 0.22 2230 100 KM Total Sulfur 0.72 7240 100 KM Total Calcium 1.27 12700 100 KM Total Magnesium 0.29 2900 100 KM Total Sodium 0.20 2000 100 KM Total Iron 53300 100 KM Total Aluminum 39100 100 KM Total Manganese 1880 5 KM Total Copper 475 5 KM Total Zinc 1610 5 KM Ammonia Nitrogen 0.86 8570 10.0 JM Organic N 3.08 30830 10.0 Nitrate+Nitrite-N 22.9 2.00 JM Total Cadmium 3.0 2.0 KM All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis 07/22/2014 14:05 07/22/2014 14:05 07/23/2014 08:10 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 14:00 07/23/2014 08:10 07/23/2014 08:10 07/23/2014 08:10 07/23/2014 14:00 Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SM-2540G SM-2540G SM-4500-NH3C-TKN SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SW 6010C SM-4500-NI3C CALCULATION SM-450ONO3F SW 6010C --- -- _;- Page: 2 of 2 Report Number: 14-203-0204 Account Number: 46245 Submitted By: ROY WHITAKER wwwaleastern.com Send To: EMA RESOURCES INC 755 YADKINVILLE RD MOCKSVILLE , NC 27028 Lab Number: 56605 Sample Id: DUTCHMAN CREEK WWTP A&L Eastern Laboratories; Inc. 1624 Whitepine Road Richmond, Virginia 23237 (804) 7.43-9401 Fm (804) 271-6446 Project: MOCKSVILLE NC NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/21/2014 10:30:00 Date Received: 07/22/2014 00:00 Date Reported: 07/25/2014 Total Chromium 62 5 KM 07/23/2014 14:00 SW 6010C Total Nickel 33 5 KM 07/23/2014 14:00 SW 6010C Total Lead 56 5 KM 07/23/2014 14:00 SW 6010C Total Arsenic 6.0 3.0 KM 07/23/2014 14:00 SW 6010C Total Mercury 3.2 0.4 KM 07/23/2014 09:00 SW-7471 B Total Selenium 6.0 5.0 KM 07/23/2014 14:00 SW 6010C pH (Standard Units) * 7.16 2.00 JM 07/23/2014 08:10 SW-9045D Total Volatile Solids 51.28 512800 100.0 JM 07/22/2014 14:05 SM-2540G Total Molybdenum 5 5 KM 07/23/2014 14:00 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LCS WAS OUT OF LIMITS FOR "Se", THE MS WAS OUT OF LIMITS FOR "Al", "Cr", "Fe", "Pb", "P", AND "S", ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt ._------ -! eitiFllICl?�4✓�iRf�9E�'S�.I''ItIIL3ffff�r.NCiE��►.S.� �'�I�t1�C lf�l�u��---��_lll��li �_�►�.�s r4Z I 0 ,E�, BIOSMI;. `-__,DS'SANO mi 14 -- - -- - ix- S" AAL EOLStIt 74ZIWIO*o Rood PLiohtii6tvd,,,V:A 13237: T.,oP. Submitt.w By Elf--l'Tilly Copy Td, ETA. Ri*oxrocs hit EW IA RrRe-49urces ln*c '1 7:55'Y� 11 Ok 7,55- YA.d ffnvjllcRd' _k Mocksvillej NC -270:10 XQo�M]16, INC 270a, 6 bomple.lo L (�ab Usw Irter.-Infomiallon _0jjjjjj�d;- oewma irod-Tests `type j: DeAw Th* of otites Type vcgwm 503 Metals: ;Nft­gan wes 0141 am Cl VOW* Sal i offifits. 'Ptimpoi 2ass A Grib Catriposite Plastic -plot Grub lj�ss' 061npwte Grob Glass COMP05ft ----pint: ,,I;. Tota1 Sdilda Ritr000r, pjlosphom.aftdpiiiissium ,2., B41c'Toof. SLI, plus, surrur, Calbl'um, Magna lklmiSodim" tToow, Ajwmlnirm'. Manganese, . Copper.And Zinc COWTurn':0h TOWnph 'L. emW Molyttlenurrf, Lead, Nickel, SsIOMM, tGapper& Jn6tidoWin SU), Nitrate & Organi.cMirogely. r i < _J OESC I Mr. Brent Collins EMA Resources 755 Yadkinville Road Mocksville, NC 27028 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: Terrie Fudge/, ESC presentative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 3 WYOURB Q:F' 0111.. 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Brent Collins July 29,2014 EMA Resources 755 Yadkinville Road Mocksville, NC 27028 I Date Received July 22, 2014 ESC Sample # L711390-01 Description Mocksville NC Site ID Sample ID DUTCHMAN CRK WWTP I Collected By Roy Whitaker Project MOCKSVILLE NC Collection Date 07/21/14 10:30 Parameter Result Det. Limit Units Limit Method Date/Time By Dil Corrosivit Y Non-Corrosiv 9045D 07/29/14 0957 KBC 1 Ignitability See Footnote Deg. F D93/101 07/29/14 1438 DR 1 Reactive CN (SW846 7.3.3.2) BDL 0.125 mg/kg 9012B 07/24/14 1826 MCG 1 j Reactive Sulf.(SW846 7.3.4.1) BDL 25. mg/kg 9034/90 07/24/14 1646 DJD 1 TCLP Extraction } - 1311 07/24/14 0827 LJN 1 Mercury BDL 0.010 mg/1 0.20 7470A 07/24/14 1721 CCE 1 Arsenic Barium BDL 0.45 mg/1 5.0 6010C 07/25/14 0208 CAP 1 Camium BDL 1.4 mg/1 100 6010C 07/25/14 0208 CAP 1 Chaomium BDL 0.45 mg/l 1.0 6010C 07/25/14 0208 CAP 1 Lead BDL 0.45 mg/1 5.0 6010C 07/25/14 0208 CAP 1 Selenium BDL 0.45 mg/1 5.0 6010C 07/25/14 0208 CAP 1 Silver BDL 0.45 mg/l 1.0 6010C 07/25/14 0208 CAP 1 BDL 0.45 mg/1 5.0 6010C 07/25/14 0208 CAP 1 TCLP ZHE Extraction - 1311 07/25/14 0740 CCS 1 TCLP Volatiles Benzene BDL 0.050 mg/l 0.50 8260B 07/25/14 1636 JC 1 - Carbon tetrachloride BDL 0.050 mg/1 0.50 8260B 07/25/14 1636 JC 1 Chlorobenzene BDL 0.050 mg/l 100 8260B 07/25/14 1636 JC 1 Chloroform BDL 0.25 mg/1 6.0 8260B 07/25/14 1636 JC 1 1,2-Dichloroethane BDL 0.050 mg/1 0.50 626013 07/25/14 1636 JC 1 1,1-Dichloroethene BDL 0.050 mg/l 0.70 8260B 07/25/14 1636 JC 1 2-Butanone (MEK) BDL 0.50 mg/1 200 8260B 07/25/14 1636 JC 1 Tetrachloroethene BDL 0.050 mg/1 0.70 8260B 07/25/14 1636 JC 1 Trichloroethene BDL 0.050 mg/1 0.50 826013 07/25/14 1636 JC 1 Vinyl chloride BDL 0.050 mg/1 0.20 8260B 07/25/14 1636 JC 1 Surrogate Recovery - Toluene-d8 103. °s Rec. 114. 826013 07/25/14 1636 JC 1 Dibromofluoromethane 107. o Rec. 125. 8260E 07/25/14 1636 JC 1 a,a,a-Trifluorotoluene 96.2 o Rec. 114. 8260B 07/25/14 1636 JC 1 4-Bromofluorobenzene 96.8 o Rec. 128. 8260B 07/25/14 1636 JC 1 TCLP Pesticides I Chlordane Endrin BDL 0.0050 mg/1 0.030 8081 07/25/14 1250 CBB 1 Heptachlor BDL 0.0050 mg/l 0.020 8081 07/25/14 1250 CBB 1 BDL 0.0050 mg/l 0.0080 8081 07/25/14 1250 CBB 1 { L711390-01 (IGNITABILITY) - Did Not Ignite Q 170 F f Page 2 of 3 i 4 REPORT OF ANALYSIS Mr. Brent Collins EMA Resources 755 Yadkinville Road Mocksville, NC 27028 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 July 29,2014 ESC Sample # L711390-01 Date Received July 22, 2014 Description Mocksville NC Site ID Sample ID DUTCHMAN CRK WWTP Project MOCKSVILLE NC Collected By Roy Whitaker Collection Date 07/21/14 10:30 Parameter Result Det. Limit Units Limit Method Date/Time By Dil Lindane BDL 0.0050 mg/1 0.40 8081 07/25/14 1250 CBB 1 Methoxychlor BDL 0.0050 mg/l 10. 8081 07/25/14 1250 CBB 1 Toxaphene BDL 0.010 mg/l 0.50 8081 07/25/14 1250 CBB 1 Surrogate Recovery Decachlorobiphenyl 126. % Rec. 123. 8081 07/25/14 1250 CBS 1 Tetrachloro-m-xylene 85.7 % Rec. 114. 8081 07/25/14 1250 CBB 1 TCLP Herbicides 2,4,5-TP (Silvex) BDL 0.0020 mg/l 1.0 8151A 07/28/14 2120 KLM 1 2,4-D BDL 0.0020 mg/l 10. 8151A 07/28/14 2120 KLM 1 Surrogate Recovery 2,4-Dichlorophenyl Acetic Acid 74.2 % Rec. 8151A 07/28/14 2120 KLM 1 TCLP Semi-Volatiles 1,4-Dichlorobenzene BDL 0.10 mg/l 7.5 8270D 07/27/14 2100 ADF 1 2,4-Dinitrotoluene BDL 0.10 mg/l 0.13 8270D 07/27/14 2100 ADF 1 Hexachlorobenzene BDL 0.10 mg/l 0.13 8270D 07/27/14 2100 ADF 1 Hexachloro-1,3-butadiene BDL 0.10 mg/l 0.50 8270D 07/27/14 2100 ADF 1 Hexachloroethane BDL 0.10 mg/l 3.0 8270D 07/27/14 2100 ADF 1 Nitrobenzene BDL 0.10 mg/l 2.0 8270D 07/27/14 2100 ADF 1 Pyridine BDL 0.10 mg/l 5.0 8270D 07/27/14 2100 ADF 1 3&4-Methyl Phenol BDL 0.10 mg/l 400 8270D 07/27/14 2100 ADF 1 2-Methylphenol BDL 0.10 mg/1 200 8270D 07/27/14 2100 ADF 1 Pentachlorophenol BDL 0.10 mg/l 100 8270D 07/27/14 2100 ADF 1 2,4,5-Trichlorophenol BDL 0.10 mg/l 400 8270D 07/27/14 2100 ADF 1 2,4,6-Trichlorophenol BDL 0.10 mg/1 2.0 8270D 07/27/14 2100 ADF 1 Surrogate Recovery 2-Fluorophenol 42.9 % Rec. 87.0 8270D 07/27/14 2100 ADF 1 Phenol-d5 30.7 Rec. 67.0 8270D 07/27/14 2100 ADF 1 Nitrobenzene-d5 54.0 % Rec. 120. 8270D 07/27/14 2100 ADF 1 2-Fluorobiphenyl 73.2 % Rec. 122. 8270D 07/27/14 2100 ADF 1 2,4,6-Tribromophenol 77.8 % Rec. 148. 8270D 07/27/14 2100 ADF 1 p-Terphenyl-d14 68.7 - Rec. 149. 8270D 07/27/14 2100 ADF 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Limit - Maximum'Contaminant Level as established by the US EPA Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. 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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Mocksville WQ Permit Number: WQ0003351 WWTP Name: Dutchman's Creek WWTP PWS Number: NCO021491 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathouen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ElAlt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray. ❑Gamma Ra ❑ Y Pasteurization Class B: Alt. (1) Fecal Density 211 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ 1 Composting ❑ jAerobic Digestion ❑ Anaerobic b1c Digestion ........................................................................................................................................ . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number of Excee- Frequency of Analysis y Sample Type Analytical Tech-ni ue q Minim Geo. Mean axim Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 183 229 287 MPN/g 0 Annual G SM92210E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) vector Attraction Keauction W)A INUAU U2T .11U71 - Ylease indicate alternative performed: Alt.1 (VS reduction) ❑ 1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-daybench) El Alt. 4 (Spec. Oz uptake) ElAlt. 5 (14-Day Aerobic) [3Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ jAlt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Bryan - WWTP ORC Preparer Name and Mle (type or print) Signature of Brent Collins - Director of Technical Services Land Applier Nameefe and (if applicable)(t3'pe or print) Z 1/23/2015 a e. Signature of Land Applier (if applicable) Date v *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Analytical;•Results` -755 �Yadkinville Rd: A6'CksvWe NO. 2702B �. nfered. 7/21'l201.4 ` w .worted: 9/3/2014 or:. Dutchman Creek WTP Dat6- Sample ID Parameter Cust ID . Result Units ;:. Metho Ana{yzed Analyst 140721=13.1 %Solids . Y : 1. 8 90' ° % SM2540B-1997 7/21/14. HM: '14Q721-13-A Fecal;Coliforih,MT'F' I. < 25`. ` MP 1/g:'. SM9 2'fCE=20C6 7/21/14, HM f4072.1�13:1 Ceorpetnc Mean 1 <22g MPNIg.: dry wk, basis 7/29114�. CC 140721.-13:2, /o .Solidi' : 2 ' . 9;01 SM25dQB-1997 7/21114: - - HM . r40721-13.2 FectiMblifomn MTF 2 . ,. <2 MPNIg SM92210E4006:. ' . 7/21/14 HM =.�._. 1,40721, -113, %°Solids. 3 $:39,. - %SM2a40s=1ss7 . 7121/14 HM'. f40121-13.3: FecafColifoim MTF' 3, <238. MPN/g SM92210E-2006 7/21/14 HM 140721-13'* % Solids 4. 16.9 % .. SM25408-1997, 7/21/14 HM 40721 13 4 Fecal Col>form MTF 4 <1$3 MPNIg, SM9221 6E-2006 7/21I14 HM: :4075 a . 497 =7i21/14 `HMM25D19 = 140721-13:5 Fecal Coliiform MTF 5 <2$7 . MP_.N/g SM9221.CE-2006 7/21/14 HM '4072.1-13'.6 % Solids' - :.: ,..: ..,, 6 '. $22; , : ':;'°:=`::.=..,/4°:; .: SM2540&1997 .. 7121/14 HM 140721 13.6' Fecal;Caldorin MTF 6 <243` MPNIg .; ;: 'SM92210E 2006 -7/21/l4 HM 40121-13 7 ; . % Solids 7 915' % SM2540B-1997 7/21114' HM :1'4072'I 13:7.: ': Fecal Cbliform MTF 7 .. <219' } MFN/g: SM9221,CE-2006 . 71211 l4 HIVI 40721=13,8 Bencti'30_Day::. 30 beirch . ,. °, -.7.47 0%; ; EPA625R=92/0 7/21/14% CL i P.O Bow 228, �. Statesville; North:Caroliria'28687 o 704;�872/4697 EMA:Resources, inc:. EMA Resourcesi Inc, 755-Yad.kinville Rd. Mocksville,Nt 27028 Entered: 7/21/2014 Reported: 8/28/20i4 S6MplqJD!'14072-!-13.8; Analytical Results, For: Dutchman PARAMETER: 1hector Attraction. Reduction/Aerobically Digested Sludke, (30day) Total Solids. Volatile. Solids %'Volaille Solids Week.- 1 1.70, 0.87 OS128 Week 1 1.61. —0.86- OA986 Week A. 1.59 0.79 0.49 Week 4: 1.57 OJ7 0.4936 -Week, 9 1.50 0.74 0A934. Volatile $a►6ds Reduction; 00-5128- - OA934X100_.=7A7% 0.5128 - -(0.-5128 X-0.49-34) Respectfully submitted,. Dena Myers Statesville Analytical,. Inc: NC WW. Cert* 44:014C DW Cert.. #37755 PO. Box 228 - Statesville, North Carolina 28687 - 704/872/4697 Client ry ���---� � 7 (f C T mkt" :4li STA7 EW LLE ANALY7TM Court Street �.' P.O.'Boz 228 Statesville, NC 28687 (704) 872-.4697 Chain': og Custody Record. Address: .,, �,, • t , ,+ r;r t'l" c� �r /� • ((., Contact Persan: Phone FAX# 'PO # f' r +} Re uisitioned by:.. (® Date) . A T 6 ( ''. a., .... . . Customer Sample fl]# l.ab•ID # Tlate Sampled (Grab Onhj} Date Sampled ', (Grab Only) Matruh - Parameters re nested for.anal sis, 4 slut w yyv Ak ` iP t"'t f b s1 ti tt va+ i 1, '� <� 1_Al AU w 0 0 c?l t O,` o A 7 ,& 1-2 V Relinquished by: Theo 1."0 a, pm Date/ /� Sampled by: Received by: fr, Time Lit ( mm Dated `' Transported by: r r Relinquished by; Time am, pm Date Holding, times met Received by; Time am, pm Date Compliance work: Composite Sampling #1: Time begin am, pm ,Date-__� _ Nan -compliance work: Time end am, pm Date / / Lab Comments: Composite Sampling #2: Time .begin am, pm Date .Time end am;..pm Date ��_ Report Number: 14-010-0507 At Laib_oratories A L Eastern Account Number:46245 7621 Whitepine.Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.MG aleastern�com Send To: EMA RESOURCES INC wwwGrower: 755 YADKINVILLE RD TOWN OF MOCKSVILLE Farm ID: MOCKSVILLE NC 27028 NC-MK-05 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Received: 01/10/2014 Date Of Analysis: 01/13/2014 Date Of Report: 01/13/2014 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: ?M j. OF G C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary