HomeMy WebLinkAboutWQ0003351_2014 Residual Annual Report_20150219�EMA
^s
�fl ,Resources, Inc.
February 13, 2015
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2014 Annual Report - Mocksville
Treatment and Land Application of Residuals
Permit No. WQ0003351
Dear Sir or Madam:
Enclosed are three copies of the 2014 Annual Report for the above referenced land
application permit.
During 2014 EMA Resources, Inc. land applied 43.92 dry tons of wastewater residuals to
20.3 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sinc y,
Brent Collins
Director of Technical Services
brent. collins&emaresourcesinc. com
FEg i 9 zm5
Phone 336.751.1441 — Fax 336.751.1442
755 Yadkinville Road — Mocksville, NC 27028
l 0--l>6 �--� -� l
s, Inc.
Town of Mocksville
2014 Annual Report
Residuals Land Application
Permit No. WQ0003351
Prepared By:
EMA Resources, Inc.
Phone 336.751.1441 — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028
MCEVEDIDEM041%
FEB 19 xK
jP9 C9On
WQ Permit#:
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ0003`351 County: Davie Year:
2014
iJ
Facility Name (as shown on permit):
Land Application-Operator:
EMU Resources Inc.
Town of Mocksville
Phone: 336-751-1441
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes [3No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not -land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepen-nit:
4
Total number of fields utilized for land application during the year:
2
Total amount of dry tons applied during the year for all application sites:
43.92
Total number of acres utilizes for land application during the year:
= 20.3
Part B -Annual Compiance Statement:
I, Facility was compliant during calendar year 2014 with all conditions of the land application permit
IJ (including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes ElNo
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
J the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
{ of laboratory results are attached.
�— 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
J 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T. 1 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
1 503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
j 13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Christine Bralle,
Town Manager
�I Permittee eWTit
e(type or print)
:_k�
Signature of Permittee Date
517.015 ;e5�e 1/23/2015
Signature of Prep r* Date Signature of Land Applier Date
(if different from Pe ' e) (if different from Permittee and Preparer)
-` * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - I
WQ Permit Number:
WQ0003351
Laboratory: 1)
Facility Name:
Town of Mocksville
2)
Residual Source WQ # or
3)
NPDES #:
NCO021491
4)
WWTP Name:
Dutchman's Creek WWTP
5)
Residual Analvsis Data
A&L Eastern Laboratories, Inc.
Parameter
(mg/kg)
Conc.
Limit
(mg/kg a
Sample or Composite Date
7/21/14
Percent Solids (%)
NA
3.5
Arsenic
75
6
Cadmium
85
3
Copper
4,300
475
Chromium
NA
62
Lead
840
56
Mercury
57
3.2
Molybdenum
75
5
Nickel
420
33
Selenium.
100
6
Zinc
7,500
1610
Total Phosphorus
NA
18400
TKN
NA
39400
Ammonia -Nitrogen
NA
8570
Nitrate and Nitrite
NA
22.9
" For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for sub Wing false information, including the possibility of fines and imprisonment for knowing violations."
Z 15 11015
Signature of Pre re Date
*Preparer is defined in CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0003351 Laboratory: 1) A&L Eastern Laboratories, Inc.
Facility Name: Town of Mocksville 2)
Residual Source 3)
NPDES # or WQ#: NC0021491
4)
WWTP Name: Dutchman's Creek WWTP 5)
Residual Analvdv. Data
Parameter
Potassium
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer bate
*Preparer is defined in 40 R Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
! Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Tons Applied (Annual):-3,984d =r
ermit #: WQ0003351 Cation Exchange Capacity (non 503 only):
-Operator: John Garwood Owner: John Garwood Predominant Soil Series: GnB2 - Gaston
Lcres Used: 15.6 Acres Permitted: 15.6 Site #: NC-MK03 Field #: 1
1 _ tesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or 11 1213 4J L5J L6J7 8 9 10 11 12
Com- 7/21/14
la
ite
te
`io Solids 3.5
Arsenic 6
Lead
3
475
62
56
3.2
IMolyb-
5
,demur
Nickel
33
selenium
6
Zinc
1610
Total
-' Phos-
18400
horus
'nnual
Heavy
Metal Field
Ill2
3
ITotal
_ nT/Ac./
App.
'Event
2.55
Arsenic
,
admium
%opper
,21_2,42'.6''s
-hromiurn,0,
3u 7
0 0'Q,0
_0
Lead
Nickel
e ,lenium
Zinc
Total
Phos-
in lbs/acre
--1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
vare that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
1/23/2015
.%gnature of Land Applier
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 1 Acres Utilized:
Land Owner: John Garwood Annual D Tons Applied: .° 39$4M=' ° 1
Dry Pp �,�„-0Site #: NC-MK03 Acres Permitted:
Operator: John Garwood Predominant Soil Series: GnB2 - Gaston Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
15.6
15.6
Volume applied
Volume
Residual Sources
Soil
Precip.
Y
o
Z a
Nitrate
Name of Cro Type
p yp
°
(enter one) Solids/
%
Applied per
(NPDES #, WQ#,
Cond.
Past 24
b
w �;
7y
T'KN
cx
o
and
PAN Applied
Receiving Residual
Y o
A
Liquid
Solids
Acre
Fert., Animal
D
(rye
Hrs.
a w
w
a
Nitrite
Ibs/acre )
Application
Cu. Yds Gallons
D Tons/Ac
(Dry )
Waste, etc)
Wet,
Moist)
inches
*
*
* c
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
8/6/14
94500
3.5
xv{r 'Q``$l°4;`-w
z__,.•-
Dutchman's Creek
Dry
D
<.5"
S
0.5
0.3
39400
8570
22.9
;23i97�2�,NA�1
1`-='
Fescue
8/7/14
80500
3.5
Qx753 §`
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
39400
8570
22.9
Fescue
12/14/14
14000
3.5�f
bTT �, �;
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
39400
8570
22.9
Fescue
12/15/14
84000
3.5
„0786a
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
39400
8570
22.9
213r0,8
MNA,
Fescue
1 w 40 000M t'*`
000
�`
0
,0`000
� c
t 6000, },,IO
OUO
OOOO� r.
m r
'H O:000
v:3S�,IF:."a,1;;'k1."�
„E,... A.fi ^
^�7iuv,av .:;i
1``� :t �y�,y�"A'kx
$..,,:•
=•T'%`.YF.'>;7;75�ti%r,$•�
4;e1+�,=. f..,� v<.i^u v'.,f
is Applications totals
on FORM FSF su attach
FORM
FSF su to this form
's,. ;xa
.t,::1'r:
;:Tk..'.T�v'x'4:ur .a"i'P�.
„:.., r..
,,,.._
.. , ;,,r,7,
�5,
TOTALS:;a"
.......
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
69y252�;.
n; _ '
; �o,0otl,,�
Lime Aplied
Annuallbs/acre
," :
t �, t hr.
��0.03<iu..
.1.�„y
�,,.. .:„
-
w
'a
1=
... r
1 1.'
8
.7
:�� 0.0�6.�r��
�
3K'
���„��'.
,..
4
�a22'"
•
0.104
0.061~
-,M r r..F./
T6:;,.
,�r=4„
6.032
u4•
_ . �
0.568
.
1.071
-
,U�� ,6':�
;�
0.017
=+gam. -•
.
�,��,.,.
0.205
-
`�.
.,0:.1",6
A�:, �.,r��4
0.58
-
0
=,0:=0`3
�..
0.108.^
��- 8 ��
19.741
279-
=''S-,:•.
,9�
: x3;>9$7ss
::R
Date
lbs/ac
Prior Years Cumulative lbs/ac
Cumulative lbs ac
36
34
�..
1338 1
�i��.., �r�^Y,:•1•�3"57..0:033:�-
1
267 1
.Current
15 1
.•0:�3.1%"
25
374
89
2498
Permitted C. P. L. R.****
PAN Limit lst/2nd Crop
Y9
2
iPermit ,..
- v'h
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Z—e *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/23/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM*
L Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Town of Mocksville Total Dry Ton Applied (Annual): `
s A i Annual
ermit #: WQ0003351 Cation Exchange Capacity (non 503 only):
Operator: Jeff Smith Owner: Town of Mocksville Predominant Soil Series: CeB2 - Cecil
A
cres Used: 4.7 Acres Permitted: 4.7 Site #: NC-MK05 Field #: 1
_'tesidual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or 1L2-1 L3J L4JL5J 161L7J L8J9 10 11 12
Com- 7/21/14
posite
Date
/o Solids 3.5
—Arsenic 6
Cadmium 3
Copper 475
ic.hromium 62
Lead 56
vlercury 3.2
IMolyb- 5
denum
Nickel 33
selenium 6
Zinc 1610
(Total
Phos- 18400
�.nnuai
L-'Total
-nT/Ac./
App.
Event
Arsenic
�admium
.Lead
Mercury
0.87
Calculated in lbs/acre
Nickel 0D ObO 0 OUQ 0 QOQw 0 000 OT000 OK000 ` 0 000 0 000 PISO'OOQ_, ` ?,- 000 0 Or57.
r ... `-,r,.�, -;•� �.y^yi , � fit, � �:•. _ .q:.. <:�... « £,
��lexuum 0 01Q= 0 000 0 000 w 0 OOQ 0 000 ' Ot000 0 000F1 , Oti000 v 0 000 i_0 000, 0 OOU M 0 000 : -0 O10'
Zinc > 2 798 OY000`= AMR MW 0 UUO _;#,0WANE, ar.z0 000 „ 0 000 � 0:0300 0 000,.tP0 000' U 000 �� 79$
Totalnu
Phos- n31 979 rt 0 000 3 0 000 { 0 Q00 0 OOC) 0 000# m0 000 0 OOD' fi 0 000 0 000 0 000 0 000 31 975,
)horUS s:, >. .... :. -...., y _-..,.. ,. ..r . ':-_.,, ,a '.. ..
"i certify, under penalty of law, that this document was prepared under my direction or supervision in accordance wit
,-system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
t_
`vare that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
I' 1/23/2015
C�gnature of Land Applier
1
L,
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: W 0003351 Field #•
Q 1 Acres Utilized:
Land Owner: Town of Mocksville Annual D ''`'`'`r°i''N 'a'@``-' ':4' -
ry Tons Applied: � ;�r- �,,,,Y.,�" 4:,0,8,<�4�n'��;� >�.` ` ,, Site #: NC-MKOS Acres Permitted:
P t ed:
Operator: Jeff Smith Predominant Soil Series: CeB2 - Cecil Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Grass Crop 1 Max. PAN: 115 Crop 2 Name: Rye Grass Cron 2 Max. PAN:
4.7
4.7
50
N �
Volume applied
PP
Volume
Residual Sources
Soil
Precip.
�
C
o
E
Z �
Nitrate
Name of Crop Type
o(enter
>~
one) Solids/
%
Applied per
P
(NPDES #, W #
Q ,
Cond.
Past 24
c�
..
� a�
m .,
TKN
c
and
PAN Applied
Receiving Residual
Liquid
Solids
Acre
Fert., Animal
(Dry,
Hrs.
o�
* N
� w.
Nitrite
lbs/acre
( )
Application
Q
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Wet,
Moist)
inches
c
0
*
0
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
12/13/14
14000
3.5.
r;s.,'r'043,5 ,$,>s
Dutchman's Creek
Dry
<,5"
S
0.5
0.3
39400
8570
22.9
; �i1+:7;88 x
, N'Ar
Fescue
12/14/14
14000
3.5
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
39400
8570
22.9
10NAm
Fescue
r Q, 000,
0 Q00
" `0r000 u
G Q 000
0 66Oz$
0 0�0
0/OOyO"
`)
�O��OOOF '"�i'
5,�0AQdU h<3'�Or000?3-'
is '��0,"0(i0 `` 1
'IUv0f00}'k�g�5.000O�r{
k,�AO000'�
;x0 000��
tTOTALS:
d,'Mk, xs
.:a r?1 l�747j9
,,
�.FY 4 £ 9.....
kE , , ,;
.'t4
Residuals Applications totals on FORM FSF supp (attach FORM
FSF supp to this form)
..
u,;i,¢0
,
`;„°28�000
��
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
..y;
;=23 t575
w,,> b�t000 �'
Lime A lied
Annual lbs/acrea„
r, WM
r,>t.r
. � 0`b� �.sx�.
10.
.. ,, w,
, � ���.
0.0�5,.
�_♦
,�
A'... '„'a,d
,
,,,0="108��
;�,. � �
b9;7
s :,,. 7!:
, � � �
0 b0.6..
E.b -.w.
Ff-
0�009,.,
w
h,-
$�� �"�}
��;w � ,
'�-.�
�,.
.N�.
:,
0.065
..a a.n.,..-..4.?:Ov:b7„c'.5•s.s,:.u...
0.028
.�0�826�<,
4.589
fx�,h . y.
0.424
, , �
0.681
..��,.
0.032
�,n.h.
. �,:
0.151
xCurrent
�.0:05:7F�
�; ,,
0.518
':.0,0':0�=
��t,,..1 ,�;�..�_
0.057
>,�. �'�9'8>i
12.796
,3);979s .
_
Date
lbs/ac
Prior Years Cumulative lbs/ac
Cumulative033,
1 s/ac
36
34
<X.A..�a°g4
1338
..
267
15
_
a: n-.}.....;:`
374
89 '
- SAS
2498
............
.
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
P
5
.::: ;.
tr..
w.
1 certay, under penaity oI iaw, that this aocument was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/23/2015 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
Page: 1 of 2
Report Number: 14-203-0204
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
www.oleastem.com
A&L Eastern Laboratories, Inc.
7621 White -pine Road Richmond; Wginia23237 (804) 743-9401 Fax (804) 271-6446
Project: MOCKSVILLE NC
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 7/21/201410:30:00
Lab Number: 56605 Date Received: 07/22/2014 00:00
Sample Id : DUTCHMAN CREEK WWTP Date Reported: 07/25/2014
i oiai aouas
3.50
35000
100.0
JM
Moisture *
96.50
100.0
JM
Total Kjeldahl Nitrogen
3.94
39400
10.0
JM
Total Phosphorus
1.84
18400
100
KM
Total Potassium
0.22
2230
100
KM
Total Sulfur
0.72
7240
100
KM
Total Calcium
1.27
12700
100
KM
Total Magnesium
0.29
2900
100
KM
Total Sodium
0.20
2000
100
KM
Total Iron
53300
100
KM
Total Aluminum
39100
100
KM
Total Manganese
1880
5
KM
Total Copper
475
5
KM
Total Zinc
1610
5
KM
Ammonia Nitrogen
0.86
8570
10.0
JM
Organic N
3.08
30830
10.0
Nitrate+Nitrite-N
22.9
2.00
JM
Total Cadmium
3.0
2.0
KM
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
07/22/2014 14:05
07/22/2014 14:05
07/23/2014 08:10
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07/23/2014 14:00
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07/23/2014 14:00
07/23/2014 14:00
07/23/2014 14:00
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07/23/2014 08:10
07/23/2014 08:10
07/23/2014 08:10
07/23/2014 14:00
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NI3C
CALCULATION
SM-450ONO3F
SW 6010C
--- -- _;-
Page: 2 of 2
Report Number: 14-203-0204
Account Number: 46245
Submitted By: ROY WHITAKER wwwaleastern.com
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 56605
Sample Id: DUTCHMAN CREEK WWTP
A&L Eastern Laboratories; Inc.
1624 Whitepine Road Richmond, Virginia 23237 (804) 7.43-9401 Fm (804) 271-6446
Project: MOCKSVILLE NC
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 7/21/2014 10:30:00
Date Received: 07/22/2014 00:00
Date Reported: 07/25/2014
Total Chromium
62
5
KM
07/23/2014 14:00
SW 6010C
Total Nickel
33
5
KM
07/23/2014 14:00
SW 6010C
Total Lead
56
5
KM
07/23/2014 14:00
SW 6010C
Total Arsenic
6.0
3.0
KM
07/23/2014 14:00
SW 6010C
Total Mercury
3.2
0.4
KM
07/23/2014 09:00
SW-7471 B
Total Selenium
6.0
5.0
KM
07/23/2014 14:00
SW 6010C
pH (Standard Units) *
7.16
2.00
JM
07/23/2014 08:10
SW-9045D
Total Volatile Solids
51.28 512800
100.0
JM
07/22/2014 14:05
SM-2540G
Total Molybdenum
5
5
KM
07/23/2014 14:00
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LCS WAS OUT OF LIMITS FOR "Se", THE MS WAS OUT OF LIMITS
FOR "Al", "Cr",
"Fe", "Pb", "P",
AND "S", ALL OTHER QC DATA IS
ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
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Submitt.w By
Elf--l'Tilly
Copy Td,
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EW IA RrRe-49urces ln*c
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Mocksvillej NC -270:10
XQo�M]16, INC 270a,
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Metals:
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offifits.
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-plot
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Glass
COMP05ft
----pint:
,,I;. Tota1 Sdilda Ritr000r, pjlosphom.aftdpiiiissium
,2., B41c'Toof. SLI, plus, surrur, Calbl'um, Magna lklmiSodim" tToow, Ajwmlnirm'. Manganese, . Copper.And Zinc
COWTurn':0h TOWnph 'L. emW Molyttlenurrf, Lead, Nickel, SsIOMM,
tGapper& Jn6tidoWin SU),
Nitrate & Organi.cMirogely.
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i
< _J
OESC
I
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Terrie Fudge/, ESC presentative
Laboratory Certification Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 3
WYOURB Q:F' 0111..
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT OF ANALYSIS
Mr. Brent Collins
July 29,2014
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
I Date Received July 22,
2014
ESC Sample
# L711390-01
Description Mocksville NC
Site
ID
Sample ID DUTCHMAN CRK WWTP
I Collected By Roy Whitaker
Project
MOCKSVILLE
NC
Collection Date 07/21/14 10:30
Parameter
Result Det. Limit
Units
Limit
Method
Date/Time
By
Dil
Corrosivit Y
Non-Corrosiv
9045D
07/29/14
0957
KBC
1
Ignitability
See Footnote
Deg. F
D93/101
07/29/14
1438
DR
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
07/24/14
1826
MCG
1
j Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
07/24/14
1646
DJD
1
TCLP Extraction
}
-
1311
07/24/14
0827
LJN
1
Mercury
BDL
0.010
mg/1
0.20
7470A
07/24/14
1721
CCE
1
Arsenic
Barium
BDL
0.45
mg/1
5.0
6010C
07/25/14
0208
CAP
1
Camium
BDL
1.4
mg/1
100
6010C
07/25/14
0208
CAP
1
Chaomium
BDL
0.45
mg/l
1.0
6010C
07/25/14
0208
CAP
1
Lead
BDL
0.45
mg/1
5.0
6010C
07/25/14
0208
CAP
1
Selenium
BDL
0.45
mg/1
5.0
6010C
07/25/14
0208
CAP
1
Silver
BDL
0.45
mg/l
1.0
6010C
07/25/14
0208
CAP
1
BDL
0.45
mg/1
5.0
6010C
07/25/14
0208
CAP
1
TCLP ZHE Extraction
-
1311
07/25/14
0740
CCS
1
TCLP Volatiles
Benzene
BDL
0.050
mg/l
0.50
8260B
07/25/14
1636
JC
1
- Carbon tetrachloride
BDL
0.050
mg/1
0.50
8260B
07/25/14
1636
JC
1
Chlorobenzene
BDL
0.050
mg/l
100
8260B
07/25/14
1636
JC
1
Chloroform
BDL
0.25
mg/1
6.0
8260B
07/25/14
1636
JC
1
1,2-Dichloroethane
BDL
0.050
mg/1
0.50
626013
07/25/14
1636
JC
1
1,1-Dichloroethene
BDL
0.050
mg/l
0.70
8260B
07/25/14
1636
JC
1
2-Butanone (MEK)
BDL
0.50
mg/1
200
8260B
07/25/14
1636
JC
1
Tetrachloroethene
BDL
0.050
mg/1
0.70
8260B
07/25/14
1636
JC
1
Trichloroethene
BDL
0.050
mg/1
0.50
826013
07/25/14
1636
JC
1
Vinyl chloride
BDL
0.050
mg/1
0.20
8260B
07/25/14
1636
JC
1
Surrogate Recovery
- Toluene-d8
103.
°s Rec.
114.
826013
07/25/14
1636
JC
1
Dibromofluoromethane
107.
o Rec.
125.
8260E
07/25/14
1636
JC
1
a,a,a-Trifluorotoluene
96.2
o Rec.
114.
8260B
07/25/14
1636
JC
1
4-Bromofluorobenzene
96.8
o Rec.
128.
8260B
07/25/14
1636
JC
1
TCLP Pesticides
I Chlordane
Endrin
BDL
0.0050
mg/1
0.030
8081
07/25/14
1250
CBB
1
Heptachlor
BDL
0.0050
mg/l
0.020
8081
07/25/14
1250
CBB
1
BDL
0.0050
mg/l
0.0080
8081
07/25/14
1250
CBB
1
{ L711390-01 (IGNITABILITY) - Did Not Ignite Q 170 F
f Page 2 of 3
i 4
REPORT OF ANALYSIS
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
July 29,2014
ESC Sample # L711390-01
Date Received July 22, 2014
Description Mocksville NC
Site
ID
Sample ID DUTCHMAN CRK WWTP
Project
MOCKSVILLE NC
Collected By Roy Whitaker
Collection Date 07/21/14 10:30
Parameter
Result
Det. Limit
Units
Limit
Method
Date/Time By
Dil
Lindane
BDL
0.0050
mg/1
0.40
8081
07/25/14
1250 CBB
1
Methoxychlor
BDL
0.0050
mg/l
10.
8081
07/25/14
1250 CBB
1
Toxaphene
BDL
0.010
mg/l
0.50
8081
07/25/14
1250 CBB
1
Surrogate Recovery
Decachlorobiphenyl
126.
% Rec.
123.
8081
07/25/14
1250 CBS
1
Tetrachloro-m-xylene
85.7
% Rec.
114.
8081
07/25/14
1250 CBB
1
TCLP Herbicides
2,4,5-TP (Silvex)
BDL
0.0020
mg/l
1.0
8151A
07/28/14
2120 KLM
1
2,4-D
BDL
0.0020
mg/l
10.
8151A
07/28/14
2120 KLM
1
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid
74.2
% Rec.
8151A
07/28/14
2120 KLM
1
TCLP Semi-Volatiles
1,4-Dichlorobenzene
BDL
0.10
mg/l
7.5
8270D
07/27/14
2100 ADF
1
2,4-Dinitrotoluene
BDL
0.10
mg/l
0.13
8270D
07/27/14
2100 ADF
1
Hexachlorobenzene
BDL
0.10
mg/l
0.13
8270D
07/27/14
2100 ADF
1
Hexachloro-1,3-butadiene
BDL
0.10
mg/l
0.50
8270D
07/27/14
2100 ADF
1
Hexachloroethane
BDL
0.10
mg/l
3.0
8270D
07/27/14
2100 ADF
1
Nitrobenzene
BDL
0.10
mg/l
2.0
8270D
07/27/14
2100 ADF
1
Pyridine
BDL
0.10
mg/l
5.0
8270D
07/27/14
2100 ADF
1
3&4-Methyl Phenol
BDL
0.10
mg/l
400
8270D
07/27/14
2100 ADF
1
2-Methylphenol
BDL
0.10
mg/1
200
8270D
07/27/14
2100 ADF
1
Pentachlorophenol
BDL
0.10
mg/l
100
8270D
07/27/14
2100 ADF
1
2,4,5-Trichlorophenol
BDL
0.10
mg/l
400
8270D
07/27/14
2100 ADF
1
2,4,6-Trichlorophenol
BDL
0.10
mg/1
2.0
8270D
07/27/14
2100 ADF
1
Surrogate Recovery
2-Fluorophenol
42.9
% Rec.
87.0
8270D
07/27/14
2100 ADF
1
Phenol-d5
30.7
Rec.
67.0
8270D
07/27/14
2100 ADF
1
Nitrobenzene-d5
54.0
% Rec.
120.
8270D
07/27/14
2100 ADF
1
2-Fluorobiphenyl
73.2
% Rec.
122.
8270D
07/27/14
2100 ADF
1
2,4,6-Tribromophenol
77.8
% Rec.
148.
8270D
07/27/14
2100 ADF
1
p-Terphenyl-d14
68.7
- Rec.
149.
8270D
07/27/14
2100 ADF
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum'Contaminant Level as established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 07/29/14 17:45 Printed: 07/29/14 17:46
L711390-01 (IGNITABILITY) - Did Not Ignite @ 170 F
Page 3 of 3
Summary of Remarks For Samples Printed
07/29/14 at 17:46:04
TSR Signing Reports; 064
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R5 - Desired TAT
Sample: L711390-01 Account: MARES Received: 07/22/14 09:00 Due Date: 07/29/14 00:00 RPT Date: 07/29/14 17:45
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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Mocksville WQ Permit Number: WQ0003351
WWTP Name: Dutchman's Creek WWTP PWS Number: NCO021491
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathouen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ElAlt
B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
Alt.D (No Prior Test) ❑
Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray. ❑Gamma
Ra ❑
Y
Pasteurization
Class B:
Alt. (1) Fecal Density 211
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
1 Composting ❑
jAerobic Digestion ❑
Anaerobic
b1c Digestion
........................................................................................................................................ .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
Frequency
of Analysis
y
Sample
Type
Analytical
Tech-ni ue
q
Minim
Geo. Mean
axim
Unitsences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
183
229
287
MPN/g
0
Annual
G
SM92210E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weight)
vector Attraction Keauction W)A INUAU U2T .11U71 - Ylease indicate alternative performed:
Alt.1 (VS reduction) ❑
1 Alt. 2 (40-day bench) ❑
Alt. 3 (30-daybench) El
Alt. 4 (Spec. Oz uptake) ElAlt.
5 (14-Day Aerobic) [3Alt.
6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
jAlt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Scott
Bryan - WWTP ORC
Preparer Name and Mle (type or print)
Signature of
Brent Collins - Director of Technical Services
Land Applier Nameefe and (if applicable)(t3'pe or print)
Z 1/23/2015
a e. Signature of Land Applier (if applicable) Date
v
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)
Analytical;•Results`
-755 �Yadkinville Rd:
A6'CksvWe
NO. 2702B
�.
nfered.
7/21'l201.4 `
w
.worted:
9/3/2014
or:. Dutchman Creek WTP
Dat6-
Sample ID
Parameter Cust ID .
Result
Units ;:.
Metho
Ana{yzed Analyst
140721=13.1
%Solids . Y :
1.
8 90' °
%
SM2540B-1997
7/21/14.
HM:
'14Q721-13-A
Fecal;Coliforih,MT'F'
I.
< 25`. `
MP 1/g:'.
SM9 2'fCE=20C6
7/21/14,
HM
f4072.1�13:1
Ceorpetnc Mean
1
<22g
MPNIg.:
dry wk, basis
7/29114�.
CC
140721.-13:2,
/o .Solidi' :
2 ' .
9;01
SM25dQB-1997
7/21114: - -
HM .
r40721-13.2
FectiMblifomn MTF
2 . ,.
<2
MPNIg
SM92210E4006:.
' . 7/21/14
HM
=.�._.
1,40721, -113,
%°Solids.
3
$:39,. -
%SM2a40s=1ss7
.
7121/14
HM'.
f40121-13.3:
FecafColifoim MTF'
3,
<238.
MPN/g
SM92210E-2006
7/21/14
HM
140721-13'*
% Solids
4.
16.9
% ..
SM25408-1997,
7/21/14
HM
40721 13 4
Fecal Col>form MTF
4
<1$3
MPNIg,
SM9221 6E-2006
7/21I14
HM:
:4075
a .
497
=7i21/14
`HMM25D19 =
140721-13:5
Fecal Coliiform MTF
5
<2$7 .
MP_.N/g
SM9221.CE-2006
7/21/14
HM
'4072.1-13'.6
% Solids' - :.: ,..:
..,,
6 '.
$22; , : ':;'°:=`::.=..,/4°:;
.:
SM2540&1997
.. 7121/14
HM
140721 13.6'
Fecal;Caldorin MTF
6
<243`
MPNIg .; ;:
'SM92210E 2006
-7/21/l4
HM
40121-13 7 ;
. % Solids
7
915'
%
SM2540B-1997
7/21114'
HM
:1'4072'I 13:7.:
': Fecal Cbliform MTF
7 ..
<219' }
MFN/g:
SM9221,CE-2006
. 71211 l4
HIVI
40721=13,8
Bencti'30_Day::.
30 beirch . ,. °,
-.7.47
0%; ;
EPA625R=92/0
7/21/14%
CL
i
P.O Bow 228, �. Statesville; North:Caroliria'28687 o 704;�872/4697
EMA:Resources, inc:.
EMA Resourcesi Inc,
755-Yad.kinville Rd.
Mocksville,Nt 27028
Entered: 7/21/2014
Reported: 8/28/20i4
S6MplqJD!'14072-!-13.8;
Analytical Results,
For: Dutchman
PARAMETER: 1hector Attraction. Reduction/Aerobically Digested Sludke, (30day)
Total Solids.
Volatile. Solids
%'Volaille Solids
Week.-
1
1.70,
0.87
OS128
Week
1
1.61.
—0.86-
OA986
Week
A.
1.59
0.79
0.49
Week
4:
1.57
OJ7
0.4936
-Week,
9
1.50
0.74
0A934.
Volatile $a►6ds Reduction; 00-5128- - OA934X100_.=7A7%
0.5128 - -(0.-5128 X-0.49-34)
Respectfully submitted,.
Dena Myers
Statesville Analytical,. Inc:
NC WW. Cert* 44:014C
DW Cert.. #37755
PO. Box 228 - Statesville, North Carolina 28687 - 704/872/4697
Client ry ���---�
� 7 (f C T mkt"
:4li
STA7 EW LLE ANALY7TM
Court Street �.' P.O.'Boz 228
Statesville, NC 28687
(704) 872-.4697
Chain': og
Custody Record.
Address: .,, �,, • t , ,+
r;r t'l" c� �r
/� • ((.,
Contact Persan: Phone FAX#
'PO # f' r +} Re uisitioned by:.. (® Date) .
A T 6 ( ''. a., .... . .
Customer
Sample fl]#
l.ab•ID #
Tlate Sampled
(Grab Onhj}
Date Sampled ',
(Grab Only)
Matruh
-
Parameters re nested for.anal sis,
4
slut
w
yyv
Ak
`
iP t"'t
f b s1
ti tt va+
i
1, '�
<� 1_Al
AU
w
0 0 c?l
t O,` o A 7 ,&
1-2
V
Relinquished by:
Theo 1."0
a, pm Date/ /�
Sampled by:
Received by: fr, Time Lit ( mm Dated
`'
Transported by: r r
Relinquished by;
Time
am, pm Date
Holding, times met
Received by;
Time
am, pm Date
Compliance work:
Composite Sampling #1:
Time begin am, pm ,Date-__� _
Nan -compliance work:
Time end am, pm Date / /
Lab Comments:
Composite Sampling #2:
Time .begin am, pm Date
.Time end am;..pm Date ��_
Report Number: 14-010-0507
At Laib_oratories
A L Eastern
Account Number:46245
7621 Whitepine.Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.MG
aleastern�com
Send To: EMA RESOURCES INC wwwGrower:
755 YADKINVILLE RD TOWN OF MOCKSVILLE Farm ID:
MOCKSVILLE NC 27028 NC-MK-05
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Received: 01/10/2014 Date Of Analysis: 01/13/2014 Date Of Report: 01/13/2014
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: ?M j. OF G
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary