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HomeMy WebLinkAboutWQ0003035_Residual Annual Report 2014_20150302CITY OF EDEN, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0003035 2014 ANNUAL REPORT City of Eden, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analyses 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00003035 County Rockingham Year 2014 Facility Name (as shown on permit) Mebane Bridge WWTP NPDES No. NCO025071 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 102 Total number of fields utilized for land application during the year: 19 Total amount of dry tons applied during the year for all application sites: 591.47 Total number of acres utilized for land application during the year: 237.1 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 143 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Melinda Ward, WWTP Superintendent Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) a e itte ®Iti� �lo1C Signature of LaNd Applier Date (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION EDEN, NC EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE MONTHNEAR AMOUNT UNIT DRY TONS UNIT January 2014 84.00 W 14.19 D February 2014 468.00 W 79.04 D March 2014 180.00 W 30.40 D April 2014 528.00 W 89.60 D May 2014 360.00 W 61.10 D June 2014 348.00 W 59.05 D July 2014 216.00 W 27.84 D August 2014 672.00 W 86.62 D September 2014 228.00 W 29.39 D October 2014 228.00 W 29.39 D November 2014 180.00 W 34.40 D December 2014 264.00 W 50.45 D YEARLY TOTAL 3,756.00 W 591.47 D DRY METRIC TONS 12.86 71.69 27.57 81.27 55.41 53.58 25.25 78.55 26.66 26.65 31.20 45.76 536.45 1/30/2015 2014 ANNUAL REPORT PROJECT: City of Eden NC FACILITY: Mebane Bridge WWTP 204 Mebane Bridge Road Eden, North Carolina 27278 NPDES Permit Number: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: NCO025071 Melinda Ward, WWTP Superintendent City of Eden P.O. Box 70 Eden, North Carolina 27289-0070 (336) 627-1009, ext. 130 Joel Freeman, Chief Operator City of Eden 204 Mebane Bridge Road Eden, North Carolina 27289-0070 (336) 627-1009, ext. 103 Synagro Central, LLC Contact: Marshall Puryear (434) 738-8002 �% ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0003035 Laboratory Facility Name: EDEN, NC A&L Eastern Laboratories Inc. NPDES# : NCO025071 or WQ# (residual only) WWTP Name: MEBANE BRIDGE WWTP Residuals Analysis Data Product Type AEDCAK AEDCAK AEDCAK AEDCAK Date Sampled (grab) or 01/03/14 03/24/14 07/02/14 10/07/14 Date Composited Percent Solids 16.89 16.97 12.89 19.11 PARAMETERS (mg/kg dry weight) Arsenic 8 8 7 9 Cadmium 5 4 4 5 Mercury 0.9 1 0.6 1.7 Chromium 60 61 58 65 Copper 2070 1780 2060 2390 Lead 68 61 50 54 Molybdenum 11 9 6 9 Nickel 29 28 31 27 Selenium 5 5 5 6 Zinc 1410 1210 1260 1390 Total Phosphorus 24100 22000 21600 23900 TKN 39900 43500 42800 39200 Ammonia -Nitrogen 6510 6720 5740 6330 Nitrate and Nitrite 7.1 10 24 785 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X Date ( S NA 'ARER) DENR FORM RSSF (5/2003) Printed: Friday - January 30, 2015 at 17:37:28 for: 2013 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0003035 Laboratory Facility Name: EDEN, NC A&L Eastern Laboratories Inc. NPDES# : ' NCO025071 or WQ# (residual only) WWTP Name: MEBANE BRIDGE WWTP Residuals Analysis Data Product Type AEDCAK AEDCAK AEDCAK AEDCAK Date Sampled (grab) or 01/03/14 03/24/14 07/02/14 10/07/14 Date Composited Percent Solids 16.89 16.97 12.89 19.11 PARAMETERS (mg/kg dry weight) Aluminum 44800 50600 58200 56800 Calcium 7550 7110 10900 7510 Magnesium 2580 2440 3440 2190 pH 6.51 6.49 7.56 6.02 Potassium 2460 2660 2480 2180 Sodium 552 648 801 679 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including, the possibility of fines and imprisonment for knowing violations." V14 NR - Data Not Reported or Data Not Required Date c2 V —° DENR FORM RSSF-B (712002) Printed: Friday - January 30, 2015 at 17:37:48 for: 2013 01 Page: 1 of 2 Report Number: 147010-0204 Account Number: 46452 Submitted By: JAMES BLACKWELL Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 97423 Sample Id : EDEN WWTP A&L Eastern Laboratories, Inc. AFL 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 wwmaleastern.prn Project: EDEN WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/3/2014 13:40:00 Date Received: 01/10/2014 00:00 Date Reported: 01/15/2014 Total Solids" 16.89 168900 100.0 JM 01/10/2014 14:19 SM-254OG Moisture * 83.11 100.0 JM 01/10/2014 14:19 SM-2540G Total Kjeldahl Nitrogen 3.99 39900 10.0 JM 01/13/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 2.41 24100 100 KM 01/13/2014 11:35 SW 6010C Total Potassium 0.25 2460 100 KM 01/13/2014 11:35 SW 6010C Total Sulfur 0.66 6630 100 KM 01/13/2014 11:35 SW 6010C Total Calcium 0.76 7550 100 KM 01/13/2014 11:35 SW 6010C Total Magnesium 0.26 2580 100 KM 01/13/2014 11:35 SW 6010C Total Sodium 0.06 552 100 KM 01/13/2014 11:35 SW 6010C Total Iron 29000 100 KM 01/13/2014 11:35 SW 6010C Total Aluminum 44800 100 KM 01/13/2014 11:35 SW 6010C Total Manganese 1580 5 KM 01/13/2014 11:35 SW 6010C Total Copper 2070 5 KM 01/13/2014 11:35 SW 6010C Total Zinc 1410 5 KM 01/13/2014 11:35 SW 6010C Ammonia Nitrogen 0.65 6510 10.0 JM 01/13/2014 08:30 SM-4500-NH3C Organic N 3.34 33390 10.0 01/13/2014 08:30 CALCULATION Nitrate+Nitrite-N 7.10 2.00 JM 01/13/2014 08:30 SM450ONO3F Total Cadmium 5.0 2.0 KM 01/13/2014 11:35 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , (` to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-010-0204 A&L Eastern Laboratories, Inc.. Account Number: 46452 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271,W, 6 Submitted By: JAMES BLACKWELL wwmaleastern.com Send To: SYNAGRO CENTRAL LLC/EDEN Project: EDEN WWTP Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 1/3/2014 13:40:00 Lab Number: 97423 Date Received: 01/10/2014 00:00 Sample Id : EDEN WWTP Date Reported: 01/15/2014 PARAMETER RESULT RESULT QUANTITATION LIMIT ANALYST ANALYSIS •1 Total Chromium 60 5 KM 01/13/2014 11:35 SW 6010C Total Nickel 29 5 KM 01/13/2014 11:35 SW 6010C Total Lead 68 5 KM 01/13/2014 11:35 SW 6010C Total Arsenic 8.0 3.0 KM 01/13/2014 11:35 SW 6010C Total Mercury 0.9 0.4 KM 01/13/2014 09:00 SW-7471 B Total Selenium 5.0 5.0 KM 01/13/2014 11:35 SW 6010C pH (Standard Units) * 6.51 2.00 JM 01/13/2014 08:30 SW-9045D Total Volatile Solids 60.00 600000 100.0 JM 01/10/2014 14:19 SM-2540G Total Molybdenum 11 5 KM 01/13/2014 11:35 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt C r-M-1 1 L I N 6 LOG S, 77 M6�"'A4A00k. Phone:.A" 'A'&]Ll CUSTQffEhS;AMRLiIfi1G; ':SAI ;SA A P L tl P. r —A "All 46452 SYNA , dk&CENTRALLMEDEN' RECORD RD PEN WWTP 13:02':00 P -p TOP& Agd, i�'i7qt tin, gproceddr-es were quea uuf, �ng,--e -'c -qI1-6didn these sam, p es. -21 U-"' h&d"•;S:,a-m-rble-r bate -,-,rirri Win qdshebv7_,: V 171 j r(Tiri 501Wquis66'&& r SPECIALINSTRU. iJCNS-,' 'mo Ltoftngw-P !'- I - Am -SAMR LNG �- ... :PQNT TAME R,&ci ved: Rkibv661by.- v m P�r--H D,' METH.Ob- PRES,E-RVffD- tHIPPED AL'ftISREQUE$T,,�' AN E �SLI L,.2� �A- iV LWIP�:N ogapic CcjI c 6 ell -- fm jvq�' N qu -'solidi -V 'Of X, 10 Z. 1 1A, 17 V, SLi 4,1 -Kjelda}ni ---,'N1&,_-.p.- "jF -eh�.Ph9spho,. dnd�Pdtassi u-mI'�-'- SL2:,:Basf6TestsLI'-I S,suU-IG !nps _odum,IronAlumfnum,4a ngpne��,Co P---p-1-er.1 t.7a1 -n d-"Z- 'na.I MANAGEji%cCop y Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AEROB. 1/3/2014 111/2014-3/31/2014 0.5731 DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) = 100 = (552 x 16.8900) = 100 = 93.2328 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (7550 x 16.8900) = 100 = 1275.19 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2580 x 16.8900) = 100 = 435.762 Na meq = Na mg/I = Molec.Wgt.Na = 93.2328 = 23 = 4.0536 Ca meq = Ca mg/I = Molec.Wgt.Ca = 1275.19 = 20 = 63.7597 Mg meq = Mg mg/I = Molec.Wgt.Mg = 435.762 = 12 = 36.3135 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4:0536 = SgrRoot[0.5(63.7597+36.3135)] = 0.573056 Printed: 1 /30/2015 Page 1 17:38 Page: 1 of 2 Report Number: 14-087-0202 A&L Eastern Laboratories, Ind.. Account Number: 46452 �!L 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9.401 Fax (804) 271.6446 Submitted By: JAMES BLACKWELL wwwaieastern.com Send To: SYNAGRO CENTRAL LLC/EDEN Project: EDEN WWTP Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 3/24/2014 11:35:00 Lab Number: 98637 Date Received: 03/28/2014 00:00 Sample Id : EDEN WWTP Date Reported: 04/03/2014 Total Solids * 16.97 169700 100.0 im U:3/Zd/ZU"14 'I J:OU 51V1-G-04UU Moisture * 83.03 100.0 JM 03/28/2014 13:59 SM-254OG Total Kjeldahl Nitrogen 4.35 43500 10.0 JM 03/31/2014 09:00 SM-4500-NH3C-TKN Total Phosphorus 2.20 22000 100 KM 03/31/2014 13:30 SW 6010C Total Potassium 0.27 2660 100 KM 03/31/2014 13:30 SW 6010C Total Sulfur 0.69 6890 100 KM 03/31/2014 13:30 SW 6010C Total Calcium 0.71 7110 100 KM 03/31/2014 13:30 SW 6010C Total Magnesium 0.24 2440 100 KM 03/31/2014 13:30 SW 6010C Total Sodium 0.06 648 100 KM 03/31/2014 13:30 SW 6010C Total Iron 30100 100 KM 03/31/2014 13:30 SW 6010C Total Aluminum 50600 100 KM 03/31/2014 13:30 SW 6010C Total Manganese 1440 5 KM 03/31/2014 13:30 SW 6010C Total Copper 1780 5 KM 03/31/2014 13:30 SW 6010C Total Zinc 1210 5 KM 03/31/2014 13:30 SW 6010C Ammonia Nitrogen 0.67 6720 10.0 JM 03/31/2014 09:00 SM-4500-NI3C Organic N 3.68 36780 10.0 03/31/2014 09:00 CALCULATION Nitrate+Nitrite-N 10.0 2.00 JM 03/31/2014 09:00 SM-4500NO3F Total Cadmium 4.0 2.0 KM 03/31/2014 13:30 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-087-0202 Account Number: 46452 Submitted By: JAMES BLACKWELL Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 98637 Sample Id : EDEN WWTP py� A&L .Eastern Laboratories, Inc. 7621 Whltep(ne Road Richmond, Virginia 23237 (604) 7435401 Fax (604) 271-6446 wwwaleastern.com Project: EDEN WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 3/24/2014 11:35:00 Date Received: 03/28/2014 00:00 Date Reported: 04/03/2014 Total Chromium 61 5 KM 03/31/2014 13:30 SW 6010C Total Nickel 28 5 KM 03/31/2014 13:30 SW 6010C Total Lead 61 5 KM 03/31/2014 13:30 SW 6010C Total Arsenic 8.0 3.0 KM 03/31/2014 13:30 SW 6010C Total Mercury 1.0 0.4 KM 03/31/2014 09:00 SW-7471 B Total Selenium 5.0 5.0 KM 03/31/2014 13:30 SW 6010C pH (Standard Units) 6.49 2.00 JM 03/31/2014 09:00 SW-9045D Total Volatile Solids 61.69 616900 100.0 JM 03/28/2014 13:59 SM-2540G Total Molybdenum 9 5 KM 03/31/2014 13:30 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt I Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AEROB. 3/24/2014 4/l/2014-6/30/2014 0.6943 DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) = 100 = (648 x 16.9700) _ 100 = 109.966 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (7110 x 16.9700) _ 100 = 1206.57 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2440 x 16.9700) _ 100 = 414.068 Na meq = Na mg/I + Molec.Wgt.Na = 109.966 = 23 = 4.78111 Ca meq = Ca mg/I = Molec.Wgt.Ca = 1206.57 = 20 = 60.3284 Mg meq = Mg mg/I + Molec.Wgt.Mg = 414.068 _ 12 = 34.5057 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.78111 _ SgrRoot[0.5(60.3284+34.5057)]='0.694324 Printed: 1 /30/2015 Page 1 17:38 Page: 1 of 2 Report Number: 14-189-0213 Account Number: 46452 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 56323 Sample Id : EDEN WWTP �LA&L Eastern- Laboratories, Inc:. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401, Fax (804(271.6446 wwwaleastemcom Project: EDEN WWTP NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 7/2/2014 08:45:00 Date Received: 07/08/2014 00:00 Date Reported: 07/11/2014 Total Solids 12.89 128900 100.0 JM 07/08/2014 14:24 SM-254OG Moisture * 87.11 100.0 JM 07/08/2014 14:24 SM-2540G Total Kjeldahl Nitrogen 4.28 42800 10.0 JM 07/10/2014 08:50 SM-4500-NH3C-TKN Total Phosphorus 2.16 21600 100 KM 07/09/2014 13:05 SW 6010C Total Potassium 0.25 2480 100 KM 07/09/2014 13:05 SW 6010C Total Sulfur 0.73 7320 100 KM 07/09/2014 13:05 SW 6010C Total Calcium 1.09 10900 100 KM 07/09/2014 13:05 SW 6010C Total Magnesium 0.34 3440 100 KM 07/09/2014 13:05 SW 6010C Total Sodium 0.08 801 100 KM 07/09/2014 13:05 SW 6010C Total Iron 31700 100 KM 07/09/2014 13:05 SW 6010C Total Aluminum 58200 100 KM 07/09/2014 13:05 SW 6010C Total Manganese 1370 5 KM 07/09/2014 13:05 SW 6010C Total Copper 2060 5 KM 07/09/2014 13:05 SW 6010C Total Zinc 1260 5 KM 07/09/2014 13:05 SW 6010C Ammonia Nitrogen 0.57 5740 10.0 JM 07/09/2014 07:59 SM-4500-NI3C Organic N 3.71 37060 10.0 07/09/2014 07:59 CALCULATION Nitrate+Nitrite-N 24.0 2.00 JM 07/09/201410:00 SM-450ONO3F Total Cadmium 4.0 2.0 KM 07/09/2014 13:05 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: - 14-189-0213 Account Number: 46452 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 A&L Eastern- Laboratories Inc. 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271-696 www aleastern.com Project; EDEN WWTP NC CERT # 257 REPORT OF ANALYSIS Date Sampled: 7/2/2014 08:45:00 Lab Number: 56323 Date Received: 07/08/2014 00:00 Sample Id : EDEN WWTP Date Reported: 07/11/2014 Total Chromium 58 5 KM 07/09/2014 13:05 SW 6010C Total Nickel 31 5 KM 07/09/2014 13:05 SW 6010C Total Lead 50 5 KM 07/09/2014 13:05 SW 6010C Total Arsenic 7.0 3.0 KM 07/09/2014 13:05 SW 6010C Total Mercury 0.6 0.4 KM 07/09/2014 09:00 SW-7471 B Total Selenium 5.0 5.0 KM 07/09/2014 13:05 SW 6010C pH (Standard Units) * 7.56 2.00 JM 07/09/2014 07:59 SW-9045D Total Molybdenum 6 5 KM 07/09/2014 13:05 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca" AND "Cr," ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date ReportRange Ratio 2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AEROB. 7/2/2014 71112014-10/1512014 0.6132 DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) + 100 = (801 x 12.8900) = 100 = 103.249 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10900 x 12.8900) _ 100 = 1405.01 Mg mg/1 = (mg mg/kg x % Solids) _ 100 = (3440 x 12.8900) = 100 = 443.416 Na meq = Na mg/1= Molec.Wgt.Na = 103.249 = 23 = 4.48908 Ca meq = Ca mg/I = Molec.Wgt.Ca = 1405.01 _ 20 = 70.2505 Mg meq = Mg mg/1-= Molec.Wgt.Mg = 443.416 _ 12 = 36.9513 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.48908 = SgrRoot[0.5(70.2505+36.9513)] = 0.613157 Printed: 1/30/2015 Page 1 17:38 Page: 1 of 2 Report Number: 14-283-0210 � � A&L Eastern Laboratories,, Inc.. Account Number: 46452 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-W6 Submitted By: MARSHALL PURYEAR wwwaldastem.com Send To: SYNAGRO CENTRAL LLC/EDEN Project: EDEN WWTP Mary Brewer NC CERT#257 284 BOGER RD MOCKSVILLE , NC 27028 REPORT OF ANALYSIS Date Sampled: 10/7/2014 10:00:00 Lab Number: 58054 Date Received: 10/10/2014 00:00 Sample Id: EDEN WWTP Date Reported: 10/21/2014 Total Solids * 19.11 191100 100.0 MW 10/13/2014 07:39 SM-2540G Moisture * 80.89 100.0 MW 10/13/2014 07:39 SM-2540G Total Kjeldahl Nitrogen 3.92 39200 10.0 JM 10/13/2014 07:54 SM-4500-NH3C-TKN Total Phosphorus 2.39 23900 100 KM 10/17/2014 11:35 SW 6010C Total Potassium 0.22 2180 100 KM 10/17/2014 11:35 SW 6010C Total Sulfur 0.57 5680 100 KM 10/17/2014 11:35 SW 6010C Total Calcium 0.75 7510 100 KM 10/17/2014 11:35 SW 6010C Total Magnesium 0.22 2190 100 KM 10/17/2014 11:35 SW 6010C Total Sodium 0.07 679 100 KM 10/17/2014 11:35 SW 6010C Total Iron • 37800 100 KM 10/17/2014 11:35 SW 6010C Total Aluminum 56800 100 KM 10/17/2014 11:35 SW 6010C Total Manganese 1360 5 KM 10/17/2014 11:35 SW 6010C Total Copper 2390 5 KM 10/17/2014 11:35 SW 6010C Total Zinc 1390 5 KM 10/17/2014 11:35 SW 6010C Ammonia Nitrogen 0.63 6330 10.0 JM 10/13/2014 07:54 SM-4500-NH3C Organic N 3.29 32870 10.0 10/13/2014 07:54 CALCULATION Nitrate+Nitrite-N 785 2.00 JM 10/13/2014 07:55 SM-450ONO3F Total Cadmium 5.0 2.0 KM 10/17/2014 11:35 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , (` to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-283-0210 Account Number: 46452 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab, Number : 58054 Sample Id : EDEN WWTP fLA&L E .astern Laboratories, Inc 7621 Whitepine Road Richmond, Virginia 23237 (604)'743 9901 Fax (604) 271 6446 wwwalea,stern.com Project: EDEN WWTP NC CERT#257 REPORT OF ANALYSIS Date sampled: 10/7/2014 10:00:00 Date Received: 10/10/2014 00:00 Date Reported: 10/21/2014 Total Chromium 65 5 KM 10/17/2014 11:35 SW 6010C Total Nickel 27 5 KM 10/17/2014 11:35 SW 6010C Total Lead 54 5 KM 10/17/2014 11:35 SW 6010C Total Arsenic 9.0 3.0 KM 10/17/2014 11:35 SW 6010C Total Mercury 1.7 0.4 KM 10/13/2014 09:00 SW-7471 B Total Selenium 6.0 5.0 KM 10/17/2014 11:35 SW 6010C pH (Standard Units) * 6.02 2.00 JM 10/13/2014 07:54 SW-9045D Total Molybdenum 9 5 KM 10/17/2014 11:35 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Cr", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2013-01-AEDCAK-NC EDEN, NC MEBANE BRIDGE WWTP AEROB. 10/7/2014 10/16/2014-12/3112014 0.7726 DIGESTED CAKE Na mg/I = (Na mg/kg x % Solids) = 100 = (679 x 19.1100) + 100 = 129.757 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (7510 x 19.1100) _ 100 = 1435.16 Mg mg/I = (mg mg/kg x % Solids) _ 100 = (2190 x 19.1100) _ 100 = 418.509 Na meq = Na mg/I _ Molec.Wgt.Na = 129.757 = 23 = 5.6416 Ca meq = Ca mg/I _ Molec.Wgt.Ca = 1435.16 _ 20 = 71.758 Mg meq = Mg mg/I z- Molec.Wgt.Mg = 418.509 _ 12 = 34.8758 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.6416 _ SgrRoot[0.5(71.758+34.8758)] = 0.772628 Printed: 1 /30/2015 Page 1 17:38 FACILITY NAME: EDEN, NC OWNER: JAMES BLACKWELL SITE #: NC CS 00007 FIELD# : CS 00007 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLIFFORD PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 97.29 OPERATOR: JAMES R BLACKWELL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.80 ACRES PERMITTED: 20.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 2/6/14 72.00 (W) 3.462 16.89 0.585 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE 2/7/14 72.00 (W) 3.462 16.89 0.585 EDMBAEL MOIST 0-<I/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE 2/8/14 72.00 (W) 3.462 16.89 0.585 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE 2/11/14 60.00 (W) 2.885 16.89 0.487 EDMBAEF MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE 2/12/14 48.00 (W) 2.308 16.89 0.390 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE 2/21/14 12.00 (W) 0.577 16.89 . 0.097 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE 2/26/14 72.00 (W) 3.462 16.89 0.585 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE 2/27/14 60.00 (W) 2.885 16.89 0.487 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE Feb-14 468.00 (W) 22.503 3/14/14 48.00 (W) 2.308 16.89 0.390 EDMBAEE MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 I FESCUE PASTURE 3/27/14 60.00 (W) 2.885 16.89 0.487 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE Mar-14 108.00 (W) 5.193 FACILITY NAME: EDEN, NC OWNER: JAMES BLACKWELL SITE #: NC CS 00007 FIELD# : CS 00007 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLIFFORD PERMIT #: WQ0003035 ANNUAL DRY TONS APPLIED: 97.29 OPERATOR: JAMES R BLACKWELL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 20.80 ACRES PERMITTED: 20.80 Page: 2 Lune Applied *** Date Lbs/Ac. allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids Total Wet Tons/Ac: 27.69 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.075 0.047 0.561 19.364 0.636 0.008 0.103 0.271 0.047 13.190 225.44 124 Cumulative lbs/acre 0.425 0.150 4.208 95.334 3.080 0.050 0.478 1.991 0.169 'x * 156 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop s ., F 47 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 �k EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/,kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: JAMES BLACKWELL SITE #: NC CS 00007 FIELD# : CS 00007 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: FAIRVIEW PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 16.23 OPERATOR: JAMES R BLACKWELL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 33.60 ACRES PERMITTED: 33.60 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) off" Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 3/27/14 12.00 (W) 0.357 16.89 0.060 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p F13279 I FESCUE HAY 3/31/14 60.00 (W) 1.786 16.89 0.302 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13271 FESCUE HAY Mar-14 72.00 (W) 2.143 4/1/14 24.00 (W) 0.7141 16.97 0.121 MOIST 1 0-<1/2" SUR 0.5 1 0.30 1 43,500. p 6,720.00 p 10.00 p 1 14404 FESCUE HAY Apr-14 24.00 (W) 0.714 JEDMBAET- Total Wet Tons/Ac: 2.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.008 0.005 0.058 1.930 0.064 <.001 0.010 0.028 0.005 1.314 22.78 13 . ,7 Cumulative lbs/acre 0.471 0.132 4.239 100.179 3.043 0.053 0.440 1.934 0.156 59.024::.-_ 182 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop t , , . FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 _& 1339.0 267.9 15.0 375.0 89.0 2500.0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify,, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: JAMES BLACKWELL SITE #: NC CS 00008 FIELD# : CS 00008 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: RHODHISS PERMIT#: W00003035 ANNUAL DRY TONS APPLIED: 14.19 OPERATOR: JAMES Y BLACKWELL CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 25.90 ACRES PERMITTED: 25.90 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1/2/14 36.00 (W) 1.390 16.89 0.235 EDMBAEI: MOIST 0-<1/2" SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p F 13279 FESCUE PASTURE 1/9/14 48.00 (W) 1.853 16.89 0.313 EDMBAEL MOIST 0-<1/211. SUR 0.5 0.30 39,900. p 6,510.00 p 7.10 p 13279 FESCUE PASTURE Jan-14 84.00 (W) 3.243 Total Wet Tons/Ac: 3.24 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.009 0.005 0.066 2.268 0.075 <.001 0.012 0.032 0.005 1.545 26.40 15 Cumulative lbs/acre 0.311 0.134 2.521 59.495 1.844 0.028 0.270 1.139 0.147 33.080 J° = " 125 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ., ,.. FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 c 375.0 89.0 2500.0 ' EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE x dzb) (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the infornation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: EDEN, NC PREDOMINANT SOIL SERIES: CLOVER OWNER: GRAY TUTTLE PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 23.20 SITE #: NC RC 00011 FIELD# : RC 000 110001 OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 8.70 ACRES PERMITTED: 8.70 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 8/8/14 12.00 (W) 1.379 12.89 0.178 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 I FESCUE 8/25/14 84.00 (W) 9.655 12.89 1.245 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 I FESCUE 8/29/14 36.00 (W) 4.138 12.89 0.533 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE Aug-14 132.00 (W) 15.172 9/2/14 48.00 (W) 5.5171 12.89 0.711 DRY 0-<1/2" SUR 1 0.5 0.30 42,800. p 1 5,740.00 p 24.00 p 14012 FESCUE Sep-14 48.00 (W) 5.517 JEDMBAEF I Total Wet Tons/Ac: 20.69 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 75 Annuallbs/acre 0.037 0.021 0.309 10.988 0.267 0.003 0.032 0.165 0.027 6.721 115.21 Cumulative lbs/acre 0.300 0.072 4.195 102.438 3.711 0.044 0.597 3.527 0.126 28.563 a• r . Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop '''; ,'. ..... .C" h Y ..f. ,yn'4,'' .0.,, ,. _ i'.,, a." 4.: .+ „ ...1 "„"+'�" ale b .0 ^. :wY. # ga� 14 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 'tea f 15.0 .:" 375.0 89.0 R'a 4 d,s. e"^7 2500.0 t.j.^e F,. ' EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X �l (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 o r F ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: EDEN, NC PREDOMINANT SOIL SERIES: CLOVER OWNER: GRAY TUTTLE PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 60.33 SITE #: ' NC RC 00011 FIELD# : RC 00011 0002 OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report . ACRES UTILIZED: 17.80 ACRES PERMITTED: 17.80 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 8/6/14 84.00 (W) 4.719 12.89 0.608 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p F 14012 FESCUE 8/7/14 36.00 (W) 2.022 12.89 0.261 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE 8/8/14 60.00 (W) 3.371 12.89 0.434 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE 8/25/14 12.00 (W) 0.674 12.89 0.087 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE 8/26/14 108.00 (W) 6.067 12.89 0.782 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE 8/27/14 96.00 (W) 5.393 12.89 0.695 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE 8/28/14 24.00 (W) 1.348 12.89 0.174 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE 8/29/14 48.00 (W) 2.697 12.89 0.348 EDMBAEL DRY 0-<1/2" SUR 0.5 . 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE Aug-14 468.00 (W) 26.291 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: EDEN, NC PREDOMINANT SOIL SERIES: CLOVER OWNER: GRAY TUTTLE PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 60.33 SITE #: NC RC 00011 FIELD# : RC 000 110002 OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 17.80 ACRES PERMITTED: 17.80 Page : 2 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) "�o Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total 7;Acre Solids Total Wet Tons/Ac: 26.29 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 95 Annual Ibs/acre 0.047 0.027 0.393 13.963 0.339 0.004 0.041 0.210 0.034 8.540 146.41 Cumulative Ibs/acre 0.449 0.117 6.662 171.916 5.225 0.068 0.871 6.676 0.205 38.975 r.. ..$ r,V` ' "g 146 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ,' % FD Cumulative Pollutant Loading Rate Limit Ibs/acre g ( ) 36.6 34.8 r"a 1339.0 267.9 15.0 375.0 89.0 2500.0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE i Xzqk (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: GRAY TUTTLE SITE #: NC RC 00011 FIELD# : RC 000 110006 RESIDUAL SOURCE(S)•* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLOVER PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 37.12 OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 13.60 ACRES PERMITTED: 13.60 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 7/9/14 84.00 (W) 6.176 12.89 0.796 EDMBAEr DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 I FESCUE 7/10/14 72.00 (W) 5.294 12.89 0.682 EDMBAEr DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 I FESCUE 7/11/14 60.00 (W) 4.412 12.89 0.569 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE Jul-14 216.00 (W) 15.882 8/21/14 12.00 (W) 0.882 12.89 0.114 EDMBAEr DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 I FESCUE 8/22/14 60.00 (W) 4.412 12.89 0.569 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 FESCUE Aug-14 72.00 (W) 5.294 Total Wet Tons/Ac: 21.18 As Cd Cr Cu Ph Hg Mo Ni Se Zn P PAN TOTALS: 76 Annual lbs/acre 0.038 0.022 0.317 11.246 0.273 0.003 0.031 0.169 0.027 6.879 117.92 Cumulative lbs/acre 0.149 1 0.056 1.132 36.740 1 0.990 0.016 0.143 0.659 0.072 17.905 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop �- xTi A. 146 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6. 34.8 ";, . " 1339.0 267.9 15.0 375.0 89.0 2500.0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X a/ 0 2,47 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: GRAY TUTTLE SITE #: NC RC 00011 FIELD# : RC 00011 0007 RESIDUAL SOURCE(S):* See list at bottom of report allons (G) or Cubic Yards (CY) Dry or Wet Tons (WT) (specify) % Tons DATE or MONTH Total Per Acre Solids Per 12/1/14 72.00 (W) 18.000 19.11 3.440 Dec-14 72.00 (W) 18.0001 Total Wet Tons/Ac: 18.00 TOTALS: Annual lbs/acre Cumulative lbs/acre ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLOVER PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 13.76 OPERATOR: GRAY TUTTLE CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 4.00 ACRES PERMITTED: 4.00 Site Inches Appli- Vola- Miner- Cond. Precip. cation tili- ali- Ammonia Nitrate PAN Residual Dry, Wet, Past 24 Method nation zation TKN Nitrogen and (pprn) Crop MOIST 1 0-<1/2" 1 SUR 1 0.5 1 0.30 1 39,200.p 1 6,330.00 p 1 785.00 p 1 13811 1 FESCUE Page : 1 Lune Applied *** Date Lbs/Ac As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 95 0.062 0.034 0.447 16.442 0.372 0.012 0.062 0.186 0.041 9.563 164.42 0.137 0.062 1.208 32.705 0.951 0.020 0.168 0.628 0.083 13.517 109 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop.` """ FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 "' 1339.0 267.9 15.0 375.0 89.0 2500.0 r EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X W1140�, 041"111-4- - (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: CLAUDE FRENCH SITE #: NC RC 00026 FIELD# : RC 00026 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: FAIRVIEW PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 50.91 OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 18.00 ACRES PERMITTED: 18.00 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 4/10/14 72.00 (W) 4.000 16.97 0.679 EDMBAEE DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE 4/11/14 96.00 (W) 5.333 16.97 0.905 EDMBAEE DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE 4/12/14 96.00 (W) 5.333 16.97 0.905 EDMBAEE DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE 4/21/14 36.00 (W) 2.000 16.97 0.339 EDMBAEE DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE Apr-14 300.00 (W) 16.666 Total Wet Tons/Ac: 16.67 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 81 Annuallbs/acre 0.045 0.023 0.345 10.069 0.345 0.006 0.051 0.158 0.028 6.845 124.45 "' Cumulative lbs/acre 0.712 0.216 7.561 182.297 6.011 0.066 0.970 5.430 0.311 54.766 14 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop as ' ` ' FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X Z(y (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent' p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: EDEN, NC PREDOMINANT SOIL SERIES: CLIFFORD OWNER: CLAUDE FRENCH PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 11.47 SITE #: NC RC 00026 FIELD# : RC 00026 0002 A OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5.70 ACRES PERMITTED: 5.70 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) ova Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 12/3/14 48.00 (W) 8.421 19.11 1.609 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,200. p 6,330.00 p 785.00 p 13811 F11811 I FESCUE 12/5/14 12.00 (W) 2.105 19.11 0.402 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,200. p 6,330.00 p 1 785.00 p FESCUE Dec-14 60.00 (W) 10.526 Total Wet Tons/Ac: 10.53 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 56 Annuallbs/acre 0.036 0.020 0.262 9.615 0.217 0.007 0.036 0.109 0.024 5.592 96.15 Cumulative lbs/acre 0.341 0.144 3.014 74.126 2.456 0.030 0.391 1.606 0.159 35.278 115 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6A... 34.8 1339.0 267.9 15.0 » " " 375.0 89.0 2500.0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X dzlo . (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: CLAUDE FRENCH SITE #: NC RC 00026 FIELD# : RC 00026 0002 B RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLIFFORD PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 24.44 OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 12.00 ACRES PERMITTED: 12.00 Page: 1 Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 5/28/14 48.00 (W) 4.000 16.97 0.679 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p F 14404 I SOYBEANS 5/29/14 96.00 (W) 8.000 16.97 1.358 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 SOYBEANS May-14 144.00 (W) 12.000 Total Wet Tons/Ac: 12.00 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 59 F4.928 Annuallbs/acre 0.033 0.016 0.248 7.250 0.248 0.004 0.037 0.114 0.020 89.60 Cumulative lbs/acre 0.406 0.161 3.471 85.665 2.765 0.035 0.447 1.737 0.188 43.766 F A. 1 191 Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop s FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 . 1339.0 267.9 15.0 375.0 89.0 2500.0 r w_ EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE XW4a (SIGNAT RE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: CLAUDE FRENCH SITE #: NC RC 00026 FIELD# : RC 00026 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLIFFORD PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 25.23 OPERATOR: CLAUDE FRENCH CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 10.80 ACRES PERMITTED: 10.80 Page Lane Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or. Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 12/3/14 24.00 (W) 2.222 19.11 0.425 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,200. p 6,330.00 p 785.00 p 13811 I WHEAT 12/4/14 108.00 (W) 10.000 19.11 1.911 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,200. p, 6,330.00 p 785.00 p 13811 WHEAT Dec-14 132.00 (W) 12.222 Total Wet Tons/Ac: 12.22 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 65 Annuallbs/acre 0.042 0.023 0.304 11.164 0.252 0.008 0.042 0.126 0.028 6.493 111.64 Cumulative Ibs/acre 0.369 0.156 3.529 82.931 1 2.683 0.035 0.513 1 1.673 0.173 39.241" �_` 118 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop t FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 - s 375.0 89.0 2500.0 �- EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME; EDEN, NC OWNER: CLAUDE FRENCH SITE #: NC RC 00026 FIELD# : RC 00026 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: FAIRVIEW PERMIT #: W00003035 OPERATOR: CLAUDE FRENCH ANNUAL DRY TONS APPLIED: 14.26 CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 5.80 ACRES PERMITTED: 5.80 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 1 4/22/14 84.00 (W) 14.483 16.97 2.458 EDMBAEE DRY 0- 1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 1 10.00 p f-14404 FESCUE Apr-14 84.00 (W) 14.483 Total Wet Tons/Ac: 14.48 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 71 Annuallbs/acre 0.039 0.020 0.300 8.750 0.300 0.005 0.044 0.138 0.025 5.948 108.14 °.Xt., ��'�'` Cumulative Ibs/acre 0.418 0.165 3.727 89.391 3.103 0.037 0.475 1.842 0.217 43.790 w " 115 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36,6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 . e, EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: EDEN, NC PREDOMINANT SOIL SERIES: CLIFFORD OWNER: AUMAN FRENCH PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 38.69 SITE #: NC RC 00027 FIELD# : RC 00027 0002 OPERATOR: AUMAN FRENCH CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry' Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) "' Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or % Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/22/14 12.00 (W) 1.875 16.97 0.318 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p F 14404 I FESCUE 4/23/14 108.00 (W) 16.875 16.97 2.864 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE Apr-14 120.00 (W) 18.750 5/23/14 108.00 (W) 16.875 16.97 2.864 DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE May-14 108.00 (W) 16.875 1 JEDMBAEE Total Wet Tons/Ac: 35.63 TOTALS: Annual lbs/acre Cumulative lbs/acre As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 174 0.097 0.048 0.738 21.522 0.738 0.012 0.109 0.339 0.060 14.630 266.00 0.185 0.096 2.024 45.712 1.820 0.018 0.331 1 0.984 0.100 21.286 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop „fix FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 .s EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate : Surface 0.5, hijection/Incorporation 1.0 k Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: S. HERBERT YOUNG, JR. SITE #: NC RC 00042 FIELD# : RC 00042 0002 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLOVER PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 42.76 OPERATOR: S. HERBERT YOUNG, JR. CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 10.70 ACRES PERMITTED: 10.70 Page Lime Applied *** Date LWAc DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (pprn) Crop MONTH Total Per Acre Solids 6/6/14 96.00 (W) 8.972 16.97 1.523 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 4404 I P14404 FESCUE 6/16/14 96.00 (W) 8.972 16.97 1.523 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p I FESCUE 6/17/14 60.00 (W) 5.607 16.97 0.952 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE Jun-14 252.00 (W) 23.551 Total Wet Tons/Ac: 23.55 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 115 Annuallbs/acre 0.064 0.032 0.488 14.228 0.488 0.008 0.072 0.224 0.040 9.672 175.85 Cumulative lbs/acre 0.144 0.053 1.163 32.219 0.975 0.013 0.144 0.660 0.060 15.492 1 1 1 4 ». Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop a - 146 �� FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 v 375.0 89.0 2500.0777k V* s u , EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hrcorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: S. HERBERT YOUNG, JR. SITE #: NC RC 00042 FIELD# : RC 00042 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLOVER PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 34.62 OPERATOR: S. HERBERT YOUNG, JR. CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.50 ACRES PERMITTED: 8.50 Page: 1 Lime Applied *** Date LW/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) _ oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/30/14 108.00 (W) 12.706 16.97 2.156 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE May-14 1 108.00 (W) 12.706 6/3/14 96.00 (W) 11.2941 16.97 1.917 EDMBAEL DRY 1 0-<1/2" 1 SUR 1 0.5 1 0.30 43,500. p 6,720.00 p 10.00 p 14404 FESCUE Jun-14 96.00 (W) 11.294 1 Total Wet Tons/Ac: 24.00 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 117 Annuallbs/acre 0.065 0.033 0.497 14.499 0.497 0.008 0.073 0.228 0.041 9.856 179.20 Cumulative Ibs/acre 0.272 0.079 .174 2.074 56 1.581 0.026 0.243 1.037 0.107 29.569 ' 123 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop x + " �zr FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 " " 1339.0 267.9 15.0 375.0 89.0 2500 0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE x (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: EDEN, NC PREDOMINANT SOIL SERIES: PINKSTON OWNER: BARRY KNIGHT PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 23.20 SITE #: NC RC 00105 FIELD# : RC 00105 0002 OPERATOR: BARRY KNIGHT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 14.10 ACRES PERMITTED: 14.10 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or % Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/16/14 72.00 (W) 5.106 12.89 0.658 EDMBAEL DRY 0-<I/2" SUR 0.5 0,30 42,800. p 5,740.00 p 24.00 p 14012 F14012 I FESCUE 9/17/14 108.00 (W) 7.660 12.89 0.987 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p I FESCUE Sep-14 180.00 (W) 12.766 Total Wet Tons/Ac: 12.77 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 46 Annuallbs/acre 0.023 0.013 0.191 6.780 0.165 0.002 0.020 0.102 0.016 4.147 71.09 Cumulative lbs/acre 0.207 0.121 1.993 50.361 2.587 0.070 0.452 2.106 0.178 27.043 , 123 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop " FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8° 1339.0 267.9 15.0 375.0 89.0 2500.0 t' EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE x OZ/D ���� (SIGNAT RE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: BARRY KNIGHT SITE #: NC RC 00105 FIELD# : RC 00105 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLOVER PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 34.40 OPERATOR: BARRY KNIGHT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 13.00 ACRES PERMITTED: 13.00 Page : 1 Lune Applied *** Date LWAc allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppni) Crop MONTH Total Per Acre Solids 11/20/14 48.00 (W) 3.692 19.11 0.706 EDM13AEI: MOIST 0-<1/2" SUR 0.5 0.30 39,200. p 6,330.00 p 785.00 p 13811 I FESCUE 11/21/14 96.00 (W) 7.385 19.11 1.411 EDMBAEL MOIST 0-<1/2" SUR 0.5 0.30 39,200. p 6,330.00 p 785.00 p 13811 I FESCUE 11/22/14 36.00 (W) 2.769 19.11 0.529 EDMBAEL MOIST 0-<I/2" SUR 0.5 0.30 39,200.p 6,330.00 p 785.00 p 13811 FESCUE Nov-14 180.00 (W) 13.846 Total Wet Tons/Ac: 13.85 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 73 Annuallbs/acre 0.048 0.026 0.344 12.648 0.286 0.009 0.048 0.143 0.032 7.356 126.48 Cumulative ibs/acre 0.492 0.239 4.717 105.880 4.956 0.123 0.873 3.649 0.397 62.555 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 , EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X v - Q y/ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: EDEN, NC OWNER: BARRY KNIGHT SITE #: NC RC 00105 FIELD# : RC 00105 0005 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CLOVER PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 9.28 OPERATOR: BARRY KNIGHT CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 3.50 ACRES PERMITTED: 3.50 Page: I Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 10/10/14 72.00 (W) 20.571 12.89 2.652 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 1. 24.00 p 14012 FESCUE Oct-14 72.00 (W) 20.571 Total Wet Tons/Ac: 20.57 As Cd Cr Cu Pb Hg Mo Ni Sc Zn P PAN TOTALS: 74 Annual lbs/acre 0.037 0.021 0308 10.925 0.265 0.003 0.032 0.164 0.027 6.682 114.55 Cumulative lbs/acre 0.359 1 0.160 1 3.767 1 81.845 3.373 0.061 0.554 1 2.376 0.266 46.725 Permit PAN Limit (ibs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppin or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: EDEN, NC PREDOMINANT SOIL SERIES: CLOVER OWNER: BARRY KNIGHT PERMIT #: W00003035 ANNUAL DRY TONS APPLIED: 20.11 SITE #: NC RC 00105 FIELD# : RC 00105 0006 OPERATOR: BARRY KNIGHT CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 4.20 ACRES PERMITTED: 4.20 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, hiches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppnl) Crop MONTH Total Per Acre Solids 10/8/14 48.00 (W) 11.429 12.89 1.473 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 I FESCUE 10/9/14 96.00 (W) 22.857 12.89 2.946 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30 42,800. p 5,740.00 p 24.00 p 14012 I FESCUE 10/10/14 12.00 (W) 2.857 12.89 0.368 EDMBAEL DRY 0-<1/2" SUR 0.5 0.30' 42,800.p 5,740.00 p 24.00 p 14012 FESCUE Oct-14 156.00 (W) 37.143 Total Wet Tons/Ac: 37.14 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.067 0.038 0.555 19.725 0.479 0.006 0.057 0.297 0.048 12.065 206.83 134 Cumulative lbs/acre 0.294 0.099 2.365 66.764 2.071 0.026 0.242 1.155 0.174 36.541 a"x Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 `. ? 375.0 89.0 2500.0 EDMBAEDC = EDEN, NC MEBANE BRIDGE WWTP AEROB. DIGESTED CAKE X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % =.percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 F4 l�IR t�iaicN`Ya1.LT 1 � Ol mGlES; INC 4niPlyiicsl Lac`i4t�1�?a•d - January 16, 2014 James Blackwell Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Eden WWTP Dear James Blackwell: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hQ.-Ilivtviv.settek.com Order No.: 14010512 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/10/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, /1-11-� Dr. Mo Osman V� Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-011-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-I1-5, Region 8 8TMS- L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 7 Summit Environmental Technologies, Inc. ARM01.113310 Win St. Ti�.L�$t3tZLtGIaS 9 a Cuyahoga Falls, Ohio 44223 Workorder Sample Summary AirHtV i+:aS TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 14010512 Website: httn://www.settek.com 17-Jan-14 CLIENT: Synagro Project: Eden WWTP Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 14010512-001 Eden WWTP 1/3/2014 11:40:00 AM 1/10/2014 9:52:00 AM Sludge Page 2 of 7 f - Summit Environmental Technologies, Inc. Case Narrative 3310 Win St. ENVIRo S;. wr'. Cuyahoga Falls, Ohio 44223 WO#: 14010512 xrra;ftical i- TEL: (330) 253-8211 FAX. • (330) 253-4489 Wehsite: hUy.-11www.se1tek.con: Date: 1/16/2014 CLIENT: Synagro Project: Eden WWTP This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as estimated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. Revision v1 Page 3 of 7 Summit Environmental Technologies, Inc. 3310 Win St. t tStrlRC+tdh9�A1'rikL t t$td LO` �5 ANC. 00whoga Falls, Ohio 44223 Id'reF}rtic/tFaprriPot€ TEL: (330) 253-8211 FAX.- (330) 253-4489 Websile: htto://www.settek.conz WO#: 14010512 Date Reported: 1/16/2014 Company: Synagro Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: Eden WWTP TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Eden WWTP 001 1/3/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/14/2014 WK Eden WWTP 001 1/3/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 1/14/2014 WK Eden WWTP 001 1/3/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 1/14/2014. WK Eden WWTP 001 1/3/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 1/14/2014 WK Eden WWTP 001 1/3/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/14/2014 WK Eden WWTP 001 1/3/2014 'TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 1/14/2014 WK Eden WWTP 001 1/3/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/14/2014 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Eden WWTP 001 1/3/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 1/14/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Eden WWTP 001 1/3/2014 Chlordane, total 0.010 ND mg/L Sludge EPA 8081 B 1 0.030 1/15/2014 JBN Eden WWTP 001 1/3/2014 Toxaphene 0.10 ND mg/L Sludge EPA 8081 B 1 0.50 1/15/2014 JBN Eden WWTP. 001 1/3/2014 Endrin 0.0020 ND mg/L Sludge EPA 8081 B 1 0.020 1/15/2014 JBN Eden WWTP 001 1/3/2014 gamma-BHC 0.0020 ND mg/L Sludge EPA 8081 B 1 0.40 1/15/2014 JBN Eden WWTP 001 1/3/2014 Heptachlor 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 1/15/2014 JBN Eden WWTP 001 1/3/2014 Heptachlor epoxide 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 1/15/2014 JBN Eden WWTP 001 1/3/2014 Methoxychlor 0.0020 ND mg/L Sludge EPA 8081 B 1 10 1/15/2014 JBN VOC by GCIMS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Eden WWTP 001 1/3/2014 1,1-Dichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 1/15/2014 MES Eden WWTP 001 1/3/2014 1,2-Dichloroethane 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/15/2014 MES Eden WWTP 001 1/3/2014 Benzene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/15/2014 MES Eden WWTP 001 1/3/2014 Carbon tetrachloride 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/15/2014 MES Eden WWTP 001 1/3/2014 Chlorobenzene 0.10 ND mg/L Sludge EPA 8260 B 1 100 1/15/2014 MES Eden WWTP 001 1/3/2014 Chloroform 0.10 ND mg/L Sludge EPA 8260 B 1 6.0 1/15/2014 MES Eden WWTP 001 1/3/2014 Tetrachloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 1/15/2014 MES Eden WWTP 001 1/3/2014 Trichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/15/2014 MES Eden WWTP 001 1/3/2014 Vinyl chloride 0.20 ND mg/L Sludge EPA 8260 B 1 0.20 1/15/2014 MES Eden WWTP 001 1/3/2014 MEK 2.0 ND mg/L Sludge EPA 8260 B 1 200 1/15/2014 MES Page 4 of 7 r Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14010512 f3IVIR;0'11AE3Y!AL`E`f� 0,309w:gA's,I Cu�ahogaFalls, Ohio94223 Date Reported: 1/16/2014 Arrar;t1d.-I TEL: (330) 253-8211 FAX. • (330) 253-4489 Company: Synagro Website: hay. -Ili msettek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: Eden WWTP SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Eden WWTP 001 1/3/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 1/14/2014 AKE Eden WWTP 001 1/3/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 400 1/14/2014 AKE Eden WWTP 001 1/3/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 1/14/2014 AKE Eden WWTP 001 1/3/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/14/2014 AKE Eden WWTP 001 1/3/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 1/14/2014 AKE Eden WWTP 001 1/3/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 1/14/2014 AKE butadiene Eden WWTP 001 1/3/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/14/2014 AKE Eden WWTP 001 1/3/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 1/14/2014 AKE Eden WWTP 001 1/3/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 1/14/2014 AKE Eden WWTP 001 1/3/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 1/14/2014 AKE Eden WWTP 001 1/3/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 1/14/2014 AKE SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Eden WWTP 001 1/3/2014 2,4-D 5.0 ND mg/L Sludge EPA 8321 A 1 10 1/14/2014 AMZ Eden WWTP 001 1/3/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 1/14/2014 AMZ Page 5 of 7 A m :,-t� L A, 9111ummit SEnvironmental Technologies, Inc. 3310 Win St. WO#: 14010512 , MVIROMMENTAL TECH QW'GIFS_ �WC Cuyahoga Falls, Ohio 44223 Date Reported: 1/16/2014 rnaFr�rticsl L:taara7et TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: hitn://www.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: Eden WWTP Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Eden WWTP 001 1/3/2014 Flashpoint (140°F) >140 °F Sludge EPA 1010 1 1/13/2014 TAH Eden WWTP 001 1/3/2014 Cyanide, Reactive ND ppm Sludge EPA 9014 1 0.50 1/13/2014 TIR Eden WWTP 001 1/3/2014 pH 6.3 sm. Sludge EPA 9045 D 1 1/13/2014 AYS Eden WWTP 001 1/3/2014 Sulfide, Reactive ND ppm Sludge EPA 9034 1 25 1/13/2014 TIR Page 6 of 7 'Summit Environmental TWM1006s. 111c- Analysis Request/Chain bf Custody' 3310 VMin.Street Fax- I'v3O.'253.4489. For Sumn4iL Envii6limental Techifololl.1 ie.s. Inc. Use 0311y cuyah6,6,,vFh11s; Ohio 44223 Tef: 330.2i3.82 C.C1111011YIN.Ilyke (Please Print) AnalyticalTarame-ters aiidMethods 'j, Z Report to Client Phone'No. Client Rx No. r1cAqe vaN Result Po" -7 5, k. cj. ;I }Tease NO. I VA Chet], if.01floNIAl'samples 4 Q Date c 3 P A Sample Identification Collected .3- Collected 2L P,;,. Clv& AMJI 1p A 1 LVA —1 #01 Date III Il Date Time M trst be approved Receive Rush-Requestcd By:.— h,v iab Dalc _- piztnager _j Vhilo:}q� yellow Pages iliel,l,,il,)tirii(o,ry.'Fti,2,=clint M.aiasthe p''iniz Page._ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035 WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071 Monitoring Period: From 01/01/14 To 03/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If annlirahlr fn alternative nerfnrmed (('lase A nr f lase Rl rmmnletr thr fnllnwinu mnnitnrinu data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 0 MPN MPN/g Coliform power per gram of total solids CFU 55 4499 153333 CFU/g 0 4/yr Grab 9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Melinda Ward, WWTP Superintendent P sparer Name an Titl ( type or print) V. a Signat6re of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: James Blackwell Client: Synagro 284 Boger Road Page 1 Report Date 1/23/2014 Mocksville, NC 27028 Date Sample Rcvd: 1/15/2014 Meritech Work Order # 01151464 Sample: Eden WWTP Grab 1/15/14 Parameters Results Analysis Date Reporting Limit Metho Qualifier % Total Solids 15.7 % 1/20/14 0-100 % SM 2540B Fecal Coliform (Sludge) 1,477 col/g dry wt 1/16/14 130 col/g dry wt SM 9222D Meritech Work Order # 01151465 Sample: Eden WWTP Grab 12/2/13 Parameters Results Analysis Date Reporting Limit Method Qualifler % Total Solids 16.7 % 1/20/14 0-100 % SM 2540B Fecal Coliform (Sludge) 3,614 col/g dry wt 1/16/14 130 col/g dry wt SM 9222D 134 Meritech Work Order # 01151466 Sample: Eden WWTP Grab 1/15/14 Parameters Results Analysis Date, Reporting Limit Method QuaIifler % Total Solids 16.4 % -1/20/14 0-100 % SM 2540B Fecal Coliform (Sludge) 55 col/g dry wt 1/16/14 130 col/g dry wt SM 9222D Meritech Work Order # 01151467 Sample: Eden WWTP Grab 1/15/14 Parameters Results Analysis Date Reporting Limi Method Qualifier % Total Solids 15.5 % 1/20/14 0-100 % SM-2540B Fecal Coliform (Sludge) 22,581 col/g dry'wt 1/16/14 130 col/g dry wt SM 9222D Meritech Work Order # 01151468 Sample: Eden WWTP Grab 1/15/14 parameters Results Analysis Date Reporting Limit Method ualifier % Total Solids 15.0 % 1/20/14' 0-100 % SM 2540B Fecal Coliform (Sludge) 153,333 col/g dry wt 1/16/14 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: James Blackwell Client: Synagro 284 Boger Road Page 2 Report Date 1/23/2014 . Mocksville, NC 27028 Date Sample Rcvd: 1/15/14 Meritech Work Order # 01151469 Sample: Eden WWTP Grab 1/15/14 Parameters Results Analy-is Date Reporting Limit Me Quglifler % Total Solids 15.0 % 1/20/14 0-100 % SM 2540B Fecal Coliform (Sludge) 3,000 col/g dry wt -1/16/14 130 col/g dry wt SM 9222D Meritech Work Order # 01151470 Sample: Eden WWTP Grab 1/15/14 Parameters Results Analysis Date Reporting Limit Method ualifier % Total Solids 15.6 % 1/20/14 0-100 % SM 2540B Fecal Coliform (Sludge) 12,238 col/g dry wt 1/16/14 130 col/g dry wt SM 9222D B1 B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 ml. B4 Filters have counts of both >60 or 80 and a20. Reported value is a total of the counts from all countable filters reported per 100 ml. rzi?ereby certify that I have reviewed and approve these data. �L Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-7.522 Chain of Custody Record (COC) Client: 1Anf Address: a%4 7*1)bU%r j, _ o �� �— ,2 _ Attention: V ` L6G,lsl° NPDES# Phone: Fax: %� 1 Y■ ERITECH INC. � w ` ENVIRONMENTAL LABORATORIES r A DYW'sion of Water Teohnologyand Controls, lnc. Phone: 1-336-342-4748QC-- 642 Tamco Rd. Fax: 1-336-342-1522 Reidsville, NC 27320 Email: srmrtech@bellsouth.net Web Site: www.meritech-labs.com Email: Project# p q # Turn Around Time* *RUSH work must have prior approval. Std (10 days) 3 - 5 Day 0 24 - 48 Hr 0 Sample Location/ID # Sampling Dates &Times Person king Sam le 5i nature : Method L Only e START END Comp? #ot Conts. Tests Required 200.8i 200.E c 2oK? Date Time Date Time ppGrab? j S I to Compositor # dug# ***Dechlorina#ion (<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation.*** Comments: �( ` &AJ— 1:—� Dvlti Method of Shipment: ❑ Ups ❑ Fed Ex Hand Delivery ❑ Other F Are these results for regulatory purposes? YES NO ❑ Report results in mg/L ❑ mg/Kg ID pg/L ❑ On Ice? 1 Temperature On Receipt g a nquisj�e� bye, Date Time Received by Date Time Reli u!shed by Date Time Received by Date Time Relinquished by Date Ti ceived lab t Tim Contact: James Blackwell Client: Synagro 284 Boger Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 2/21/2014 Date Sample Rcvd: 1/15/2014 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order# 01151471 Sample: Eden WWTP 1/15/14 �gtal Solids Volatile Solids % Volatile Solids Week 1 1/16/14 1.780 1.100 0.620 Week 2 1/23/14 1.850 1.120 0.608 Week 3 1/30/14 1.980 1.190 0.603 Week 4 2/7/14 1.510 0.890 0.588 Week 5 2/15/14 1.640 0.960 0.583 1 hereby certify that I have reviewed and approve these data. u � A24; Laboratory Represent ive 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record (C®C) Client:0 NPDESN Phone: MERITECH+, 9 ENVIRONMENTAL LABORATORIES j,4 t A DIvIslon of Water Technolo and Controls, /nc. •��s::':� Phone: 1-336-342-4748 642 Tamoo Rd. Fax: 1-336-342-1522 Reidsville, NO 2732o Email: srmrtech@belisouth.net Web Site: www.maritech-labs.com ��a� Address: _ Jt)!t P. V _ �� _ 0 �y t t tL t?5 t l Attention: Email: Project# P.O. # Turn Around Time* 'RUSH work must have prior approval. Std (to days) 3 - b flay 24 - 48 Hr Sample Location/ID # Sampling Dates & Times p 9 Person Taltin Sam le St nature iaethod Use �' only START END Comp? Grab? Contonts. Tests Required zoo.a/2oo.� HO z K? Data Time Date 7lme W l� t �,, �i�a _ a.3Q n (�rA� 44 ti reca C.-A arm^ G L( Cr lam` 3 Ct r�� I r N-7 GGG t 1 I Compositor ***Dech lori nation (<0.5 ppm) of Ammonia, Cyanide, Phenol or TKN samples must be done in the field prior to preservation.*** # Jug# Comments: �lkJ �t1 nP111`j 1 C!;�C� � o c4 �b� `- s Method of Shipment: UPS Fed EX Are these results for regulatory purposes? YES I NO ❑ Report results in mg/L (� mg/Kg [ µg/L On Ice? r'- Temperature On Receipt Fie(inquis e� by Date Time V Received by Date Time > Hand Delivery Other Reli wished by Date lime Recelvedby Date Time _ Retinqulshed by Date Time -Rd sewed a lab bye toj T �.e C, ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Eden WWTP WQ Permit Number: WWTP Name: Mebane Bridge WWTP NPDES Number: Monitoring Period: From 4/01/14 To 06/30/14 WQ 0003035 NC 0025071 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlirahle to niternntive nerfnrmed !Glace A nr Cincc R) rmmnlete the fhUnwinu mnnitnrinu dntn- Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2x10 to the 6` MPN CFU/g Coliform power per gram of total solids CFU 659 1760 4723 CFU/g 0 4/yr Grab 9222 D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Melinda Ward, WWTP Superintendent Preparer Name d Title (ty e or pn ) Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) E�t Contact: James Blackwell Client: Synagro 284 Boger Road Mocksville, NC 27028 Meritech, Inc® Environmental Laboratory Laboratory Certification No.165 Page 1 Report Date 4/7/2014 Date Sample Rcvd: 3/24/2014 Meritech Work Order # 03241405 Sample: Eden WWTP Grab 3/24/14 Parameters Results Analysis Date Reporting Limit ifie Method Qualifier % Total Solids 16.4 % 3/25/14 0-100 % SM 2540B Fecal Coliform (Sludge) 659 col/g dry wt 3/25/14 130 col/g dry wt SM 9222D B1 Meritech Work Order # 03241406 Sample: Eden WWTP Grab 3/24/14 Parameters Results Analysis Date Reporting Limit Metho Qualifler % Total Solids 15.5 % 3/25/14 0-100 % SM 2540B Fecal Coliform (Sludge) 1,355 col/g dry wt 3/25/14 130 col/g dry wt SM 9222D Meritech Work Order # 03241407 Sample: Eden WWTP Grab 3/24/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 14.8 % 3/25/14 0-100 % SM 2540B Fecal Coliform (Sludge) 1,622 col/g dry wt 3/25/14 130 col/g drywt SM 9222D Meritech Work Order # 03241408 Sample: Eden WWTP Grab 3/24/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 14.7 % 3/25/14 0-100 % SM 2540B Fecal Coliform (Sludge) 1,769 col/g dry wt 3/25/14 130 col/g dry wt SM 9222D Meritech Work Order # 03241409 Sample: Eden WWTP Grab 3/24/14 Parameters Results Analysis Date Reporting Limit Method Qualifle,r % Total Solids 14.2 % 3/25/14 0-100 % SM 2540B Fecal Coliform (Sludge) 1,270 col/g dry wt 3/25/14 130 col/g dry wt SM 9222D B1 B2 Countable inembranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 nil. 642-Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Contact: James Blackwell Client: Synagro 284 Boger Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 2 Report Date 4/7/2014 Date Sample Rcvd: 3/24/14 Meritech Work Order # 03241410 Sample: Eden WWTP Grab 3/24/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 15.0 % 3/25/14 0-100 % SM 2540B Fecal Coliform (Sludge) 3,400 col/g dry wt 3/25/14 130 col/g dry wt SM 9222D Meritech Work Order # 03241411 Sample: Eden WWTP Grab 3/24/14 Parameters Results Analysis Date Reporting Limit Method Qualifier % Total Solids 15.4 % 3/25/14 0-100 % SM 2540B Fecal Coliform (Sludge) 4,723 col/g dry wt 3/25/14 130 col/g dry wt SM 9222D B1 B1 Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters reported per 100 nil. i" I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3-20-2013 Chain of Custody Record (COC) NPDES#: Client: 51 _tiil4.�r" Phorre: Address: Fax: c '� �`, Email: L ` t^' �o : Svc c ►5c— o�1�� Project: P.O.#: Attention: 7A`s �� 'a�k�"' Turn Around lime* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply: Email referred), Fax, Mail Std 10days) 3->; Days za.aaHrs 1 INC, ENVIRONMENTAL LABORATORIES " 642 TamcoRd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritech=labs.com www.meritech-labs.com Sample Location acid/or ID # Sampling ®aces Times�y' Person Taki Sa !e (' r t): I.ab Use:®n1y Start End comp? Grab? #of Cont. ,pp Test(s) p p Required :on Ice?. Yes No ;.pH OTC?' ` CIOK?: Date Time Date Time Oil 1 L • Temperature,Upon; Receipt: Method O Shipment: *** Dechlorination (<O.S ppm) of Ammonia, Cyanide, Phenol and TO samples must be done in the field prior to preservation. Comments: �. L ,o a � l.as` 1'� a . Compositor Jug #. []: UPS Fed Ex Are these results for regulatory purposes? Yes ..:., No Report results in: mg/L mg/kg a: ug/L �� �'�++�land Delivery Relin ish by Dat Time: "3-- �A '�t ,ti.. Received by: Date: Time: ' Chi Other Relinq ' hed by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Received jay Lab: Date: Time: y L 1 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Marshall Puryear Client: Synagro 284 Boger Road Report Date: 4/25/2014 MocksvilIe; NC 27028 Date Sample Rcvd: 3/24/2014 Vector Attraction Reduction / Aerobically Digested Sludge 30 Day Test) Meritech Work Order # 03241412 Sample: Eden WWTP 3/24/14 Total Solids Volatile Solids % Volatile Solids Week 1 3/25/14 1.380 0.840 0.606 Week 2 4/1/14 1.450 0.750 0.514 Week 3 4/8/14 1.520 0.890 0.587 Week 4 4/15/14 1.630 0.950 0.582 Week 5 4/23/14 1.860 1.070 0.574 I hereby certify that have reviewed and approve these data. ll.�tG Laboratory Representative 642 Tainco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3-20.2013 Chain of Custody Record (COC) NPDES#: Client: ~05 Phone: MERRIT E INC, 9 Address: Fax: ^ ENVIRONMENTAL LABORATORIES Email: 642TamcoRd. Phone: 336-342-4748 ° Ao LLs,,,, Utz'. 01� � _ Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@meritech-labs.com @ J �i*r•Cr5 c Turn Around Time* Attention: �� �'" How would you like your report sent? *RUSH work needs prior approval. ��pp www.meritech-labs.com l r�1 1 Std 10 days) 3 - 5 Da s 24 - 48 Firs Circle all that apply:�Ematlreferred), Fax, Mail ` �F .Sampling Dates & Times Person Taki�rrtylett�.00 ACC Lab Use Only Sample Location and/or ID # Start End ? Comp. #of Test(s) Required On Ice?. Yez..No :.pH :OP •:CIOK? Date Time Date Time Grab? Cont. r ( ( Gr. ;..:; ...... ::. o < ... 4 l i 'Temperature,Upon Receipt. • .. 3' •' ' Method of "** Dechlorination (<Q•S ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. "** Comments: t �i �� � -S0 Q� , vs�i�c� -7 Compositor:#" Jug# Shipment: UPS Fed Ex Are these results for regulatory purposes? Yes No Report results in: mg/I_ mg/kg ug/L nd. Delivery RetingWish d y Dat Time. Received by: Date: Time: Other Relinqu` hed by: Date: Time: Date: Time Received by: • n Relinquished by Date: Time: Received b Lab: 1 Date: / Time: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Eden WWTP WQ Permit Number: WQ 0003035 WWTP Name: Mebane Bridge WWTP NPDES Number: NC 0025071 Monitoring Period: From 07/01/14 To 09/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If anni-ahla 4n alffnrnafiwA narfnrmad Wince A nr (lace R) emmnlete the fnllnwinv mnnitnrina flatae Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2x10 to the 61 MPN MPN/g Coliform power per gram of total solids 1506 2186 2774 CFU/g 0 4/yr Grab 9222 D CFU 1000 MPN per gram of total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt.5 Option/Alt.6 9ption/Alt.7 - Option/Alt.8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/I5A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment." Melinda Ward, WWTP Superintendent Preparer name And Title (print or type) --)1 �J �s Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Y L . Page 1 Contact: Marshall Puryear Report Date 7/14/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 7/2/2014 Meritech Work Order # 07021421 Sample: Eden WWTP 1 Grab 7/2/14 Parameters Results Analysis Date Reporting Limit M t od % Total Solids 16.6 % 7/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 2,108 col/g dry wt 7/2/14 130 col/g dry wt SM 9222D Meritech Work Order # 07021422 Sample: Eden WWTP 2 Grab 7/2/14 Parameters Re ui Analygi$ Date Reporting limit Method % Total Solids 16.6 % 7/3/14 0-100 % SM 2540E Fecal Coliform (Sludge) 1,506 col/g dry wt 7/2/14 130 col/g dry wt SM 9222D Meritech Work Order # 07021423 Sample: Eden WWTP 3 Grab 7/2/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 16.7 % 7/3/14 0-100 % SM 2540E Fecal Coliform (Sludge) 2,335 col/g dry wt 7/2/14 130 col/g dry wt SM 9222D Meritech Work Order # 07021424 Sample: Eden WWTP 4 Grab 7/2/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 13.1 o/Q 7/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 2,366 col/g dry wt 7/2/14. 130 col/g dry wt SM 9222D Meritech Work Order # 07021425 Sample: Eden WWTP 5 Grab 7/2/14 Parameters Results AnalyEis Date Reporting Limit Method % TotaI Solids 13.7 % 7/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 2,774 col/g dry wt 7/2/14 130 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 2 Contact: Marshall Puryear Report Date 7/14/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 7/2/2014 Meritech Work Order # 07021426 Sample: Eden WWTP 6 Grab 7/2/14 Parameters Results Analysis Date ReRortin ,Limit M to hod %Total Solids 16.7 % 7/3/14 0-100 % SM 2540B Fecal CoIiform (Sludge) 2,335 col/g dry wt 7/2/14 130 col/g dry wt SM 9222D Meritech Work Order # 07021427 Sample: Eden WWTP 7 Grab 7/2/14 Parameters Results AnalMis Date Reporting Limit Method % Total Solids 15.7 % 7/3/14 0-100 % SM 2540B Fecal Coliform (Sludge) 2,102 col/g dry wt 7/2/14 130 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3:20-2013 Chain of Custody Record (COC) NPDES#: Client:��� �� Phone: Address: ;;?45 F 6�"- W Fax: M604, / li c ,,cif Email: Project: P.O.#: Attention: h(C,,sf~a(( Turn Around Time* How Would youlike our report sent? *RUSH work needs prior approval. :Email (preferred), ax, Mail std i�s 3 s Dais Z�s Circle allthatappiK— � o �� � � � � � � � MC. , ENVIRONMENTAL LABORATORIES 642 Tameo.Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: inf6@meritech-18bs.com VV VV �V Ameritech—labs.co I I Sample Location and/or ID # .Sampling Dates & Tildes Person Taking sample (Sign/Print): Lamb Use Only Start End ? Comp. Grab? #oF Cont. Test(s) �,JI ` Required I I red On Ice? Yes / No =pH OK? ClCI OK. Date Time Date Time h'� {•-� �� 1%ate �•� Icu �-�. - Ll `� D iJ�?jct,.+.. �•'�'3�t+^ 1 sue' `j lay �S�h �•4J �� I Temperature Upon �Reapipt: <33 Method of Shipment: *** Dechlorination <0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done,in the field prior -to preservation. *** Comments: 1JUg Compositor # it ❑; UPS Fed Ex Are th se results for regulatory purposes? Yes 0° No E_- Report results in: mg/L E1- mg/kg Q ug/L Q, 0= =- Hand Delivery Relinquished by at L` /M 7 Time: Received by: Date: Time: EOther Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: rve ab• -Date: Li I: Meritech, Inc. _ Environmental Laboratory Laboratory Certification No.165 Contact: Marshall Puryear Report Date: 8/4/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 7/2/2014 Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test Meritech Work Order # 07021428 Sample: Eden WWTP 7/2/14 Total Solids Volatile Solids % Volatile Solids Week 1 1.500 0.780 0.521 Week 2 1.550 0.B00 0.519 Week 3 1.520 0.760 0.499 Week 1.400 0.700 0.501 Week 5 1.500 0.740 0.491 • i that I have reviewed and approve these data. A I hereby certify tl a t pp Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 30 ®ay Bench Worksheet 070223 Eden Week 1 7/3/2014 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.48 0.79 0,534 2 1.52 0.82 0.539 3 1.51 0.74 0.490 Average 1.501 0.781 0.521 Week 2 7/1012014 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.55 0.80 0'.516 2 1.55 0.81 0.523 3 1.54 0.801 0.519 Average 1.661 0.80 0.519 Week 3 7/17/2014 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.53 0.77 0.503 2 1.51 0.77 0.510 3 1.53 0.741 0.484 Average 1.521 0.761 0.499 Week 4 7/24/2014 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.39 0.7 0,504 2 IA 0.70 0.500 3 1.41 0.701 0.500 Average 1.401 0.70 0.501 Week 5 7/31 /2014 Samples Total Solids Volatile Solids % Volatile Fraction 1 1.49 0.75 0.603 2 1.51 0.72 0.477 3 1.50 0.741 0,493 Average 1,501 0.741 0.491 Van Kleeck Reduction (%): 11.29 ale Chain of Custody Record (COQ NPDES#: Client: J�✓��fi t�-7 Phone: a � Address: ae64 9 Q� �_ Fax: u ENVIRONMENTALLABORATOJiIES Email: µ # 642 TamcoRd. Phone: 336-342-4748 Project: Reidsville NC 27320 Fax: 336-342-1522 P.O.#: Email: info@meritech-labs.com u��'"'r Attention: 6' i� &:sf Q Turn Around Time* *RL65H work needs prior approval. How would you like your report sent? A �� !®� vv Vie edtA e eritech—labs.com St Soda 3-5 Da s za.aaHrs Circle all that apply: ail{preferred max, Mail .Sampling Dates & Times Person Taking Sample(Sign/Print): Lab Use ®n1' Sample Location and/or ID # Start End Comp? #of Test(s) Required On -Ice?. Yes / No pH OK? Date Time Date Time Grab? Cont. .:CIOK? O^r VL1M1� f Y.�N 7T O"M� Temperature Upon *** -Receipt: D Method o **` Dechlorination {a0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. . 9 Compositor# Comments: Shipment: UPS Jug # se results for regulatory purposes. Yes Fed Ex Are Q#. p Q> . No art results i n: mg/L mg/kg Qi ug/L �.�.` Re Relinquished b : a Time: Received by: Hand Delivery Zti`F !�-'� Date: Time: Relinquished hy: Date: Time: Received by: Q Other Date: Time: Relinquished by: Date: Time: Rea b r Rate: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Eden WWTP WQ Permit Number: WWTP Name: Mebane Bridge WWTP NPDES Number: Monitoring Period: From 10/01/14 To 12/31/14 WQ 0003035 NC 0025071 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion re.. ..a.., 1,1. — ..1�........4:..,. .. F..........1 /01— A — 9-1— M nn .Jofo +h. fnlln .4.Ana dw*a• Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61 MPN MPN/g Coliform power per gram of total solids 37 69 503 CFU/g 0 4/yr Grab 9222D CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Mt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107"have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Melinda Ward, WWTP Superintendent Preparer Name d Tit e Signature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Meritech, IncA .: Environmental Laboratory -' Laboratory Certification No.165 Page 1 Contact: Marshall Puryear Report Date 10/13/2014 Client: Synagro 284 Boger Road Mocksville, NC 27028 Date Sample Rcvd: 10/7/2014 Meritech Work Order # 10071403 Sample: Eden WWTP 1 Grab 10/7/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 25.3 % 10/8/14 0-100 % SM 2540B Fecal Coliform (Sludge) 107 col/g dry wt 10/7/14 30 col/g dry wt SM 9222D Meritech Work Order # 10071404 Sample: Eden WWTP 2 Grab 10/7/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 20.4 % 10/8/14 0-100 % SM 2540E Fecal Coliform (Sludge) 44 col/g dry wt 10/7/14 30 col/g dry wt SM 9222D Meritech Work Order # 10071405 Sample: Eden WWTP 3 Grab 10/7/14 Parameters..Results Analysis Date Reporting Liiuit Method % Total Solids 17.9 % 10/8/14. 0-100 % SM 2540B Fecal Coliform (Sludge) . , - 503 col/g dry wt 10/7/14 — 30 col/g day wt :.... SM 9222D Meritech Work Order # 10071406 Sample: Eden WWTP 4 Grab 10/7/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 24.3 % 10/8/14 0-100 % SM 2540B Fecal Coliform (Sludge) 37 col/g dry wt 10/7/14- 30- col/g dry wt SM 9222D Meritech Work Order # 10071407 Sample: Eden WWTP 5 Grab 10/7/14 Parameters Results Analysis Date Reporting Limit Method %Total Solids 25.2 % 10/8/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 40 col/g dry wt 10/7/14 40 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Page 2 Contact: Marshall Puryear 1zeport Date 10/13/2014 Client: Synagro 2B4 Boger Road Mocksvilie, NC 27028 Date Sample Rcvd: 10/7/2014 Meritech Work Order # 10071408 Sample: Eden WWTP 6 Grab 10/7/14 Parameters Results Analysis Date ReportingLimit imit Method 0/6 Total Solids 21.3 % 10/8/14 0-100 % SM 2540B Fecal Coliform (Sludge) < 47 col/g dry wt 10/7/14 47 col/g dry wt SM 9222D Meritech Work Order # 10071409 Sample: Eden WWTP 7 Grab 10/7/14 Parameters Results Analysis Date Reporting Limit Method % Total Solids 20.0 % 10/8/14 0-100 % SM 2540B Fecal Coliform (Sludge) 45 col/g dry wt 10/7/14 30 col/g dry wt SM 9222D I hereby certify i that I have reviewed and approve these data. �{.• �y `� Laboratoty Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 3.10•2on Chain of Custody Record (COC) : ' NPDES#: Client: l z t,y Phone: Address: Fax: Email: Project: P.O.#: Attention: TurnAraundTime* How -would you like your report sent? *RUSH work needs prior approval. Circle all that apply:. Email. (preferred), Fax, Mail Std 10days) 3_ 5 Da vs zap-a_8Firs ENVIRONMENTAL LABORATORIES 642 TamcoRd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritech-labs.com ®°���� �^� w. �r+� � eritec� l—labs.co Sample Location and/or ID # .Sampling, Dates & Times Person Taking Sample (sign/Print): Lab Use Only' Start End Comp? Grab? #of Cont. e'st(5) :Req red 0 Ice? ` :Y / No pH OK?, ' Cl OK? Date Time Da Time ism CP i f Temperature; Upon R�ppzt 31Ie��• " Method of Shipment: "** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Comments: I Compositor # JUg# [� UPS Q?. Fed Ex Are these results for regulatory purposes? Yes No Report results in: mg/L [ mg/kg (—..� ug/L' �J`r. ilHand Delivery Relinquished by. Date: Time: , Z / 7 p _ /t r Received by: Date: Time: Q Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: 1me: ceived byr b:i r� D�t : Time: / l ., i - eritech, Inc. Environmental Laboratory . ; Laboratory Certification No 165 . R....., ... •. i .. .... ..... .. ................ ... ..... ... ... ........ .. ... .................................................... .............................. .. Contact: Marshall Puryear Client: Synagro 284 Boger Road Mocksville, NC 27028 Report Date: 11/13/2014 Date Sample Rcvd: 10/7/2014 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 10071410 Sample: Eden W WTP 10/7/14 Total Solids Volatile Solids % Volatile Solids Week 1 1.600 0.847 0.530 Weelc 2 0.557 1.590 0.880 Week 3 0.533 1.690 0.900 I hereby certify that I have reviewed and approve these data. - Laboratory Repl esen ative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Chain of Custody Record (COC) NPDES#: Client: {'�'`'.�' Phone: Address: Fax: Email Project: P.O.#: Attention: Turn Around Time* Now would you like your report sent? *RUSH work needs prior approval. ' Std 1Qda s) 3-5 Da s 24-aSNrs Circle ail that'app]y: mail (preferred) , Fax, Mail ® ENVIRONMENTAL LABORATORIES I 542 TamcoRd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritech-labs.com ® CIO �S'a.mer itech—labs,co Sample Location and/or 10 # Sampling Dates & Times Person Taking Sample (Sign/Print): Lab Use,.Only Start End Comp? Grab? #of Cont. Test(s) e u i red �ce? No: ClPH'OK? ? Date Time Date Time t Temperature Upon R_eceip a Method oy Shipment: I *** Dechlorination (<O.S-ppm) of Ammonia, Cyanide, Phenol and T KN samples must be done in the field priorto preservation. Comrnents: 1 Compositor Jug # D UPS Fed Ex Are these results for regulatory purposes? Yes Q` No r,1 Report results in: mg/L mg/kg ug/L Q'Nand"Delivery Re inciuished by: �. �� Date: Time: ,s I Received by: Date- Time: Other Qeiinquished by: Date: Time: Received by: Date: Time: :Re nquished by: Date: Time: c wed b tg: g e: Agricultural Lime Application Log Year: 2014 Project: EDEN Field (state -county -site -field) NC-CS-07-01 James R Blackwell Soil Lime Requirement pH 11 (from soil analysis) 6.4 O.OT/Ac Tons/Acre Applied Date Applied NC-CS-07-02 James R Blackwell 6.7 O.OT/Ac NC-CS-08-02 James R Blackwell 6.3 O.OT/Ac NC-RC-11-01 Gray Tuttle 5.7 OAT/Ac NC-RC-11-02 Gray Tuttle 5.8 0.5T/Ac NC-RC-11-06 Gray Tuttle 6.0 O.OT/Ac NC'RC-11-07 Gray Tuttle 5.7 1.3T/Ac. NC-RC-26-01 Claude French 6.4 O.OT/Ac NC-RC-26-2A Claude French 5.4 1.3T/Ac NC-RC-26-213 Claude French 5.3 0.8T/Ac NC-RC-26-03 Claude French 5.6 0.8T/Ac NC-RC-26-04 Claude French 5.6 0.6T/Ac NC-RC-27-02 Auman French 6.0 O.OT/Ac NC-RC-42-02 Herbert Young 6.3 O.OT/Ac NC-RC-42-04 Herbert Young 6.1 O.OT/Ac NC-RC-405-02 Barry Knight 6.2 O.OT/Ac NC-RC-105-03 Barry Knight 6.0 O.OT/Ac NC-RC-105-05 Barry Knight 6.0 O.OT/Ac NC-RC-105-06 Barry Knight 6.6 O.OT/Ac Remaining lime will be spread as field conditions allow. NCDA&CS „9iv'aomic Division Phone: (919) 733-2655 Website: www.r?__.-'gov/agronomi/ Report No. FYI- __J16374 Client: James Blackwell Advisor: Nate Roth Predictive 7089 US Highway 158 West Synagro Yanceyville, NC 27389 284 Boger Rd Mocksville, NC 27028 �"-�' '�``Soil Report rt Mehlich-3 Extraction •' .� �. N Sampled County :Caswell -�� sampled: Received: 11/14/2014 Completed: 12/10/2014 Farm: NC-CS-7 Links to Helpful Information Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test index levels of 2000 or more; for peanuts with zinc, the level is 300. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu &amp; Zn has been set at 3000 index; for peanuts with zinc, the level is 500. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to erevent levels from accumulating to the point where they become toxic to crops grown on a field. Sample ID: 07-01 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/cm3; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 1.05 7.5 90 0.7 6.4 70 67 62 24 33 1180 719 340 340 890 0.1 1 Sample ID: 07-02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, 1 0.0 120-200 0 50 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units -W/V in g/cd; CEC and Na in meg1100 cO; NO3-N in mgldd]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.46 0.86 15.3 96 0.6 6.7 130 43 70 25 50 203 128 673 673 2005 0.2 1 orlh Carolina v Tobacco Trust Fund Commbsion Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality., - Steve Troxler, Commissioner of Agriculture NCDA&CS Ngndr omic Division Phone: (919) 733-2665 Website: www.n,;.u..gov/agronomi/ Report No. FY1 �LJ16374 James Blackwell Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index Ib%acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncaar..gov/aaronomi/obpart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P206 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-Al1, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.gov/apronomi/uvrst.htm for more information. NCDA&CS Agronomic Division Phone: (919) 733-2665 Predictive ,t F Soil Report !t7u515F'''. Client: James Blackwell 7089 US Highway 158 West Yanceyville, NC 27389 Mehlich-3 Extraction Sampled County: Caswell Report No. FY1:; ..:016365 Advisor: Nate Roth Synagro 284 Boger Rd Mocksville, NC 27028 Sampled: Received: 11/14/2014 Completed: 1'2/09/2014 Farm: NC-CS-08 Links to Helpful Information Sample ID: 08-02 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 50 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cd; CEC and Na in meg1100 cd; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 1.02 7.7 91 0.7 6.3 201 46 67 21 56 163 110 393 393 1080 0.1 1 Norlh`Carolina- E. €t"oi+acac►;?'rzis, Fw6�1,Coanizimssiole- Reprogramming of the laboratory -information -management system that makes this report possible is being funded . through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.n . gov/agronomi/ Report No. FY1'=QLJ16365 James Blackwell Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncapr.gov/aaronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-1, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS-1, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.crov/apronomi/uvrst.htm for more information. Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-AI1 Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P206 phosphate S-1 sulfur index SS-1 soluble salt index' WN weight per volume Zn-AI zinc availability index Zn-I zinc index NCDA&CS Agronomic Division Phone: (919) 733-2665 -'- ,�,• Predictive } Soil Report �'i13'111:1�5°' Website: www.r...u..gov/agronomi/ Client: Gray Tuttle 286 Whetstone Creek Rd. Stoneville, NC 27048 Mehlich-3 Extraction Sampled County: Rockingham Report No. FY1' ,_016364 Advisor: Nate Roth Synagro 284 Boger Rd Mocksville, NC 27028 Sampled: Received: 11/14/2014 Completed: 12/09/2014 Farm: NC-RC-11 Links to Helpful Information Sample ID: 11-01 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P2Os K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.4 120-200 0 90, 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cd; CEC and Na in meq/1'00 cmP; NO3-N in mg/drrt3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.60 1.08 5.2 79 1.1 . 5.7 152 24 51 25 46 265 176 270 270 842 0.1 2 :North "Carol ina, �St±aea:o:%s��t.I�ws�l C�,rt^�isi65sfo�a_ Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant.from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Troxler, Commissioner of Agriculture NCDA&CS ,;uruaomic Division Phone: (919) 733-2665 Website: www.r.__,i.`gQv1agronoMi/ " Report No. FY1'; _..J16364 Gray Tuttle Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be'given in units of either B ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at Ca% one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I ESP Fertilizer HM% Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn only on reports for greenhouse soil or problem samples. Mn-AI1 Mn-AI2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z MM-0 notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na ncagr.gov/agronomi/pubs.htm. NO3-N ORG Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH find the exact fertilizer grade recommended on the report, visit www.ncaar.aov/aaronomi/oboart4.htm#fs to find P-1 information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P206 S-1 Test Results SS-1 W/V The first seven values [soil class, HM%, WN, CEC, BS%j Ac and pH] describe the soil and its degree of acidity. The Zn-AI remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not Zn-1 routinely available)] indicate levels of plant nutrients or other fertility measurement.. Visit www.ncagr.pov/aaronomi/uvrst.htm for more information. exchangeable acidity boron % CEC occupied by basic cations % CEC occupied by calcium cation exchange capacity copper index exchangeable sodium percent percent humic matter potassium index potash % CEC occupied by magnesium mineral soil class manganese Mn-availability index for crop 1 Mn-availability index for crop 2 manganese index mineral -organic soil class. nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index NCDA&CS ,',. .iomic Division Phone: (919) 733-2656 Website: www.r - gov/agronomi/ Report No. FYT' ,_ .j )01827 Client: Gray Tuttle Advisor: Creighton Brown .� Predictive 286 Whetstone Creek Rd. Synagro Central Stoneville, NC 27048 284 Boger Rd Soil Report Mehlich-3 Extraction Mocksville, NC 27028 =-X N Sampled County: Rockingham Sampled: 07/01/2014 Received: 07/30/2014 completed: 08/07/2014 Farm: Eden Links to Helpful Information Sample ID: RC112 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.5 120-200 0 0 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - W/V in glcd; CEC and Na in meq/100 crrP; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.01 8.6 79 1.8 5.8 153 107 45 28 32 318 208 178' 178 859 0.0 Sample ID: RC116 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre), N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 30 10 0 0 0 0 0 0 Note: 12 2 - $pH Test Results [units - WN in g/cO; CEC and Na in meq/100 crrr3; NO3-N in mg/do]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1- K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.05 9.2 84 1.4 6.0 47 75 49 32 32 312 204 160 160 573 0.0 _-:Northtarolina ,�.r. .�� •:i r•b k� 4 ''r7%uccr�.i'r�se�l°mil. Cr:arntlbis'tot6. Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone:,.(919) 733-2.656 Website: www.ncagr.gov/agronomi/ Report No. FYI s= �001827' Gray Tuttle Page 2 of 2 I Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8.inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ' I ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncacir.gov/aaronomi/uvrsthtm for more information. Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-0 mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index WN weight per volume Zn-AI zinc availability index Zn-I zinc index Pagel of 2 Report Number: 15-007-0674 AL Account Number: 46452 -WWW.aleastemcom Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/07/2015 Date Of Analysis: 01/08/2015 A&L Eastern _Laboratories_ 7621 Whitepitie Road Richmond, Virginia 23237 (804) 743.9401' Fax (864) 27176446 Grower: Submitted By: NATE ROTH GRAY TUTTLE Farm ID: RC-11 EDEN PROJECT SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 01/09/2015 ` Organic Matter Phosphorus -,Potassium Magnesium Calcium - Sodium,- pH' Acidity C.E.0 Sample ID Field ID Lab Number ENR % 'Rate Mehlich 3 Reserve K Mg Ca _ Na Soil Buffer H Ibs/A ppm Rate ppm Rate ppm Rate ppm - Rate- ppm - Rate' . ppm Rate p H Index meq/100g meq/100g, 11-07 59 H 89 L 225 H 1054 M 27 VL 01132 7.3 VH 150 5.7 6.73 2.0 9.5 NC=49 NC=46 PercentBaseSaturation Nitrate Sulfur Zinc Manganese �'w Iron--, ; Copper Boron_ --;,soluble salts 'Chloride Aluminum,, Sample ID_:Field K Mg Ca., ':-'Na' H NOaN � S ., 2n Mn �_ Fe — ° �° Cu B SS - Cl: Al ID. % % % "�° ppm a Rate ppm Rate ppm Rate ppm' Rate ppm Rate _° ppm Rate ppm Rate ms/cm. Rate° ppm :Rate ppm 11-07 17 M 5.4 H 48 H 160 VH 16.0 VH 0.8 M 0.07 VL 2.4 19.7 55.5 1.2 21.1 NC=35 NC=135.0 NC=300 1 NC=800.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pawl. Inc G H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. v C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 15-007-0674 Account Number:46452 Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/07/2015 Date Of Report: 01/09/2015 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 A : wwwaleastem.com Grower: Submitted By: NATE ROTH GRAY TUTTLE Farm ID: RC-11 EDEN PROJECT SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 11-07 Fescue Hay 4 1.3 50 30 250 0 11 0 0 0 0 0 Comments "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Q M Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary NCDA&CS Agronomic Division Phone: (919) 733-2656 Website: www.nca6r.goV/agronomi/ Report No. FY14=5L034332 Client: French, Claude/Auman Advisor: Creighton Brown Predictive 167 French Rd Synagro Central 4r Reidsville, NC 27320 284 Boger Rd S oil I Re o rt Mehlich-3 Extraction Mocksville, NC 27028 p Sampled County: Rockingham Sampled: 04/01/2014 Received: 04/28/2014 Completed: 05/07/2014 Farm:., Eden Links to Helpful Information Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C.and Z symbols are printed on your report for soil test index levels of 2000 or more; for peanuts with zinc, the level is 300. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu &amp; Zn has been set at 3000 index; for peanuts with zinc, the level is 500. These levels are used by DENR as a benchmark to determine when application of waste products should be'stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on a field. Sample ID: RC261 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn _ Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 30 0 0 0 0 0 0 Note: 12 2-Fescue/OGrass/Tim, 0.0 120-200 0 30 0 0 0 0 0 0 Note: 12 Test Results [units -WIV in g/crrP; CEC and Na in meq/100 cnr ; NO3-N in mg/dnt3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 1.31 1.00 10.6 87 1.4 6.4 343 59 60 24 39 149 101 101 650 650 2050 0.1 1 =North, Carolina yl ccs�7u%tkwtd,cbinluisskrn_ Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.n6agr.gov/agronomi/ Report No. Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations I Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a. time recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations -for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations 'given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-AI1 Mn-AI2 Mn-availability index for crop 1 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr.pov/aaronomi/obpart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P206 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS-1, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagrgov/apronomi/uvrsthtm for more information. NCDA&CS ...:iomic Division Phone: (919) 733-2655 Website: www.y _-..gov/agrononii/' Report No. FY1tiD 16362 V4. Predictive Client: Anman French 1612 Crutchfield Rd Advisor: Nate Roth Synagro Reidsville, NC 27320 284 Boger Rd 1q, Mehlich-3 Extraction Soil Report Mocksville, NC 27028 Sampled County: Rockingham kvias". Sampled: Received: 11/14/2014 Completed: 12/09/2014 Farm: NC-RC-26 Links to Helpful Information Sample ID: 26-04 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.6 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/cd; CEC and Na in meq/100 cO; NO3-N in mg/dO]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.60 0.90 6.8 78 1.5 5.6 127 68 49 24 61 223 151 248 248 799 0.1 1 Sample ID: 26-2bRecommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg 8 Mn Zn Cu B Information Lime History: 1-Soybean 0.8 0 0 60 0 0 0 0 0 0 Note: 3 2- Test Results [units - WIV in g1cO; CEC and Na in meq/100 crr?; NO3-N in mg/do]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.86 0.98 4.1 64 1.5 5.3 120 37 38 21 86 137 92 200 200 823 0.1 2 "North t rolina,� Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/a-gronomi/ Report No. FY15-Z L016362 Anman French Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncapr.pov/apronomi/obpart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P206 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-1 zinc index routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/aclronomi/uyrst.htm for more information. Page 1 of 2 Report Number: 15-007-0675 Account Number: 46452 0 vmwaleasteM.'CoM Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 n F o. :..e.�• n�ln7/7r14� nnf. (V Anniucia. nimpt/7f11si A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804),7439401 Fax (804)'271.6446 Grower: AUMAN FRENCH EDEN PROJECT SOIL ANALYSIS REPORT natp Of Rpnnrt: 01/09/2015 Submitted By: NATE ROTH Farm ID: RC-26 Analytical Method(s): Mehlich 3 Organic Matter . Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.C: Sample ID Lab ENR 'Rate, Mehlich 3 Reserve ' K Mg Ca Na Soil Buffer; H. Field'ID, Number % IbslA' ppm a. Rate ppm Rate ppm Rate ppm Rate ppm Rate 'ppm - Rate- pH In meq/100g meq/1009" 26-2A 01133 5.6 H 150 138 VH 110 M 173 H 591 L 28 VL 5.4 6.74 1.9 6.7 INC =115 NC=56 RC263 01134 5.1 H 145 109 VH 108 H 126 H 1 453 L 118 VL 5.6 6.82 1.1 4.8 NC=91 NC=55 Percent Base Saturation Nitrate . , Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride", Aluminum' Sample ID K Mg Ca Na H NO3N S! � Zn Mn Fe Cu B S$ CI . AI Field ID % % % % %. , ppm 'Rate ppm Rate ppm Rate ppm. Rate ppm- Rate ppm Rate ppm Rate ms/cm Rate ppm _ Rate ppm 26-2A 36 VH 12.0 VH 24 H 175 VH 23.6 VH 0.6 M 0.1 VL 4.2 21.5 44.1 1.8 28.3 NC = 75 NC = 300.0 NC = 150 1 1 NC = 1180.0 RC263 M H H VH 10.5 VH L VL 5.8 21.9 47.2 1.6 23.2 123 NC=48 15.3 NC=132.5 142 NC=263 1199 NC=525.0 10.4 10.08 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pwz. me Gawr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640, = ppm. Pauric McGroary Page 2 of 2 Report Number: 15-007-0675 Account Number:46452 Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/07/2015 Date Of Report: 01/09/2015 99. A&L Eastern _Laboratories 7621. Whitepine Road Richmond, Virginia 23237 (804),743-9401 Fax (804) 271-8446 www.aleastern.com Grower: Submitted By: NATE ROTH AUMAN FRENCH Farm ID: RC-26 EDEN PROJECT SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 26-2A Fescue Hay 4 1.3 50 0 250 0 0 0 0 0 0 0 RC263 Wheat 65 0.8 72 25 30 0 5 1.4 0 0 0 0.5 Comments: Sample(s) : RC263 Crop: Wheat Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate. Boron recommendations are on a broadcast basis. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Division Phone: (919) 733-2655 Predictive rs. Report Soil Re fi p Website: vvww.i,L;�dyi.gov/agronomi/ 'Report No. FY V,(01'6363 Client: Anman French Advisor: Nate Roth 1612 Crutchfield Rd Synagro. Reidsville, NC 27320 284 Boger Rd Mehlich-3 Extraction Mocksville, NC 27028 Sampled County :Rockingham i Sampled: Received: 11/14/2014 Completed: 12/09/2014 Farm: NC-RC-27 Links to Helpful Information Sample ID: 27-02 Recommendations: Lime Nutrients (Ib/acre) More Crop (tons/acre) N P2Oe K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 50 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in glcrif; CEC and Na in meq/100 crtr3; NO3-N in mg/da]: Soil Class: Mineral HM% WN CEC BS%a Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0'.51 0.88 9.1 88 1.1 6.0 143 46 56 30 61 158 ill 331 331 931 0.2 2 --North. Carol na, apt . A ;1's�itiacc� 3"ru,t fu��il:'Ciiaruttrssicsn. Reprogramming of the laboratory" -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.rit;agr.gov/agronomi/ Report No. FY'I3-JL016363 Anman French Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 M manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-0 mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/oboart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P205 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/V weight per volume The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The 'Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-Al, Cu-I, S4, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.aov/apronomi/uvrst.htm for more information. NCDA&CS Agr6riomic Division Phone: (919) 733-2655 Website: www.n•--,..gov/agronomi/ Report No. FYt� -, _037102 Predictive . _ } ' Mehlich-3 Extraction Report a.tviir57.1t'� Client: Herbert/Samuel Young 544 Youngs Rd Stoneville, NC 27048 Sampled County: Rockingham Advisor: Creighton Brown Synagro Central 284 Boger Rd Mocksville, NC 27028 Sampled: 05/27/2014 Received: 06/04/2014 Completed: 06/12/2014 Farm: Eden Links to Helpful Information .Sample ID: RC422 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information - Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 50 30 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, 0.0 120-200 50 30 0 0 0 0 0 0 Note: 12 Test Results [units -WIV in glcrrf; CEC and Na in meq/100 crrr3; NO3-N in mgldm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.36 1.11 8.2 87 1.0 6.3 37 55 77 6 101 318 202 202 85 85 165 0.1 1 Sample_ ID: RC424 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 2- Fescue/OGrass/Tim, 0.0 120-200 70 120-200 70 100 100 0 0 0 0 0 0 0 0 0 0 0 0 Note: 12 Note: 12 Test Results [units - WN in g/crrP; CEC and Na in meq/100 cd; NO3-N in mgldm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%a S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.10 7.3 84 1.2 6.1 28 19 72 11 34 128 93 93 192 192 349 0.1 1 Orth "Caroflna: ���tia[i[l�7tU36 �'uir�l,�c��ivs[rssfcsa Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2656 _ Website: www.n..u..gov/agronomi/ : Report No. FY1_-_. .fil37102 Herbert/Samuel Young Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For; best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended.and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash . for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-n- I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z mineral -organic soil class notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agtonomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncapr.pov/apronomi/obpart4.htm#fs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P206 phosphate S-1 sulfur index Test Results SS-1 soluble salt index W/v weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI n-I zinc availability index zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncaarpov/acironomi/umst.htm for more information. Page 1 of 2 Report Number: 15-007-0673 Account Number:46452 Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/07/2015 _ A &L Eastern .Laboralt_bri_e_s N! L!L 7621,Whitepine Road Richmond, Virginia 23237(8C44) 743.9401 _Fax (804) 271-644fi www.aleastern.com . Grower: Submitted By: NATE ROTH BARRY KNIGHT Farm ID: RC-105 EDEN PROJECT SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Analvsis: 01/08/2015 Date Of Report: 01/09/2015 - Organic Matter Phosphorus Potassium Magnesium_ Calcium Sodium _ pH Acidity C.E.0 Sample ID Lab ENR' MehlicFi s ` Reserve K Mg Ca Na Soil Buffer H Field ID Number ° /° Rate IbslA ppm . Rate ppm Rate; ppm Rate ppm Rate- ppm Rate ppm Rate - p. H : Index meq/100g meq/100g 105-2 01127 9.7 VH 150 317 VH 167 H 348 H 1467 M 33 VL 6.2 1.5 12.3 NC=264 NC=85 105-3 01128 7.7 VH 150 294 VH 95 M 275 H 1 1138 M 130 VL 1 6.0 6.78 1.5 9.9 NC=245 NC=49 105-5 01129 4.0 M 117 130 VH 66 L 212 H 1128 M 136 VL 6.0 6.79 1.4 9.1 NC=108 NC=34 105-6 01130 3.2 M 105 H 161 54 VL 245 VH 756 M 120 VL 6.6 0.4 - 6.4 NC=51 NC=28 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper - Boron Soluble Salts , Chloride Aluminum Sample ID K Mg pa',' - Na. H NO3N - S Zn Mn Fe Cu B SS CI AI - Field ID % o -%• % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate 'ppm Rate ,ppm Rate ms/cm Rate ppm Rate ppm 105-2 25 M 22.1 VH 45 H 253 VH 27.5 VH 0.9 M 0.15 VL 3.5 23.6 59.6 1.2 12.1 NC=52 NC=552.5 NC=281 NC=1375.0 105-3 H VH 164 VH VH .0 VH M VL 2.5 23.1 57.5 1.3 15.4 134 126.0 1247 141 10.8 10.1 NC = 71 NC = 650.0 NC = 1025 NC = 2050.0 105-5 L VH 135 VH VH 18.5 VH 0.6 M VL 1.9 19.4 62.0 1.4 15.4 112 110.7 1164 1 10.09 NC=25 NC=267.5 NC=844 NC=925.0 - L H 167 VH VH 11.7 VH L VL !�7 2.2 31.9 59.1 1.4 1 6.0 115 15.9 1127 10.4 10.08 NC=31 NC=147.5 NC=1044 NC=585.0 Values on this report represent the plant available nutrients in the Explanation of symbols: %(percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pew;. IV 607-.- H (High), VH (Very High). ENR - Estimated.Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 v- Report Number: 15-007-0673 Account Number: 46452 Send To: SYNAGRO CENTRAL LLC/EDEN Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/07/2015 Date Of Report: 01/09/2015 A&L Eastern .Laboratories ('AIL 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 v aleastern.com Grower: Submitted By: NATE ROTH BARRY KNIGHT Farm ID: RC-105 EDEN PROJECT SOIL FERTILITY RECOMMENDATIONS Nitrogen., Phosphate Potash Magnesium Sulfur. Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P O s K O- 2 M 9 S Zn Mn Fe Cu B' Field ID Tons Tons/A Ib/A Ib/A lb/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A 105-2 Fescue Hay 4 0.0 50 0 143 0 0 0 0 0 0 0 105-3 Fescue Hay 4 0.8 50 0 250 0 0 0 0 0 0 0 105-5 Fescue Hay 4 0.8 50 0 250 0 17 0 0 0 0 0 105-6 Fescue Hay 4 0.0 50 30 250 0 14 0 0 0 0 0 Comments: Sample(s) : 105-3 Crop: Fescue Hay If this soil is organic sand, no lime is needed for soil with pH 5.2 or above. If the soil pH is lower than 5.2 then apply 1.0 ton per acre. Sample(s) : 105-3,105-5,105-6 Crop: Fescue Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. The recommended potash is the total pounds/acre needed to achieve the specified yield goal. Apply 1/2 or 1/3 (100-150 pounds) of the total at the first application in spring or fall. Application of the remaining should be determined by the yield achieved after the first cutting and the moisture condition. If in drought condition and yield is low the following applications should be reduced or eliminated. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary