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HomeMy WebLinkAboutWQ0001934_Residual Annual Report 2014_201503022014 ANNUAL REPORT TOWNOF CHADBOURN. RECEIV LAND APPLICATION PROGRAM PERMIT #WQ0001934 , . MAR 0 2.2015 .. . MR SECTION WFORMATION PROCESSING UNIT Prepared For: Town of Chadbourn. 602 North Brown Street Chadboum, North Carolina 28431 ' Prepared BY: Branch Residuals & Soils; LLC 8646 W. Market Street —Suite 111 Greensboro, North Carolina 27409 February 2015 BRANCH RESIDUALS & SOILS, LLC 8646 W. Market St. — Suite 111 • Greensboro, NC 17409 PHONE (336) 510-0340 • Fax (336) 510-0341 February 16, 2015 North Carolina Department of Environment and Natural Resources Division of Water Resources 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2014 LAND APPLICATION ANNUAL REPORT Town of Chadbourn Permit No. WQ0001934 Branch Residuals & Soils Project No. 2004-34 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of the Town of Chadbourn. This data includes: 1) Certification Forms, Facility Information, and Noncompliance Issues, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual Land Application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Annual Pathogen & Vector Attraction Forms, 8) Annual Pathogen and Vector. Attraction Reduction Documentation, 9) Soils Lab Data 10) '2014 Application Summary Table, and 11) 2014 Application Condition Summaries. A total of 390,000 gallons (27.65 dry tons or 25.13 dry metric tons) of Class B biosolids were land applied by Southern Solutions Environmental to 23.22 acres of permitted land in 2014 for the Town of Chadboum. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 510-0340. Sincerely; Robert T. Branch, L.S.S. Land Application/Residuals Operator #15676 RTB ' Enclosures TABLE OF CONTENTS SECTION NO. TITLE I Certification Forms and Facility Information II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary Forms V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Form VIII Pathogen and Vector Attraction Reduction Documentation IX Soil Analysis Reports X 2014 Application Summary Table XI 2014 Application Condition Summaries CERTIFICATION FORMS AND FACILITY INFORMATION ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001934 County: Facility Name (as shown on permit): Land Application Operator: Southern Solutions Environmental Phone: Land application of residuals as allowed by the permit occurred during the past calendar year? R1 Yes D No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Pav4 A - Racirinalc Annlicatinn Snmmarv- Columbus Year: 2014 Town of Chadbourn WWTP 336-753-1256 Total number of application fields in thepermit: 4 Total number of fields utilized for land application during the year: 3 Total amount of dry tons applied during the year for all application sites: 27.65 Total number of acres utilizes for land application during the year: 23.22 Part B - Annual Comoiance Statement: Facility was compliant during calendar year 2014 with all conditionsof the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes D No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Patricia Garrell, Interim Town Manager CQ U �d Permittee Name and Title (type or print) Date Signature of Permittee ate Z to - lam c �TS J -Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (12/2006) TOWN OF CHADBOURN WASTEWATER TREATMENT PLANT (WWTP) e Facility name, address, and telephone number: Town of Chadbourn 602 North Brown Street Chadbourn, North Carolina 28431 Phone: 910-654-3054 Facility NPDES permit number: NCO021865 e Name, address, and telephone number of the responsible official (permittee): Mr. Patricia Garrell, Interim Town Manager Town of Chadbourn 602 North Brown Street Chadbourn, North Carolina 28431 Phone: 910-654-4148 e Name, address, and telephone number of the facility operator: Mr. Daniel C. Ward, Wastewater Treatment Plant ORC Town of Chadbourn 602 North Brown Street Chadbourn, North Carolina 28431 Phone: 910-654-3054 e Name, address, and telephone number of land appliers: Southern Solutions Environmental 389 Main Church Road Mocksville, NC 27028 Phone: (336) 753-1256 e Dry metric tons of biosolids land applied: WWTP 27.65 Dry Tons or 25.13 Dry Metric Tons ANNUAL RESIDUAL SAMPLING SUMMARY FORM S ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - E WQ Permit Number: WQ0001934 Laboratory: 1) Enviroment 1, Inc Facility Name: Town of Chadbourn WWTP 2) Residual Source WQ # or NCO021865 3) NPDES #: 4) WWTP Name: Town of Chadbourn WWTP 5) 10—iA-1 A-1—.a Tn4n --------- ------ --- — Parameter (mg/kg) ----- Ceiling Conc. Limit Rample or Composite Date' 2/25/2014 5/14/2014 8/25/2014 Percent Solids (%) NA 2.06* 1.61 * 1.49* Arsenic 75 6.00 Cadmium 85 <0.5 Copper 4,300 106.00 Chromium NA 29.00 Lead 840 32.00 Mercury 57 0.13 Molybdenum 75 <5.00 Nickel 420 9.00 Selenium 100 <5.00 Zinc 7,500 317.00 Total Phosphorus NA 4,455 TKN NA 12,850 Ammonia -Nitrogen NA 336 Nitrate and Nitrite NA <3.65 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. * Average percent solids from samples collected each of three application events. G6I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submi formation, including the possibility of fines and imprisonment for knowing violations." /D- S— Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORMS ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Chadbourn Total Dry Tons Applied (Annual): 8.53 Permit #: WQ0001934 Cation Exchange Capacity (non 503 only): n/a Operator: Harry R Stickland Owner: Harry R Stickland Predominant Soil Series AuB Acres Used: 3.3 Acres Permitted: 3.3 Site #: 8 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft ST-To e Total Phos- pharusm-MEE'EMEME-000 • _■ TT_____. Ai 4.l u.-iA T in the/arrPl. � : e • . l Phos- MEN mmmm _phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Simature of Land A lier Date gn pP A, -4k— nn�ii n Uiorritt DFNR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Chadbourn Total Dry Tons Applied (Annual): 8.28 WQ0001934 Harry R Stickland Cation Exchange Capacity (non 503 only): n/a Owner: Harry R Stickland Predominant Soil Series AuB 4.5 Acres Permitted: 4.5 Site #: 8 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): moons .. • 1. 1 1 1. 11 7[ -Vmy Motal Tiialel T.nadinac (C alenlated in lhS/acre): 1 •1 ' 1 1 1 1 ---------- 1 1 . -• n Total h os- M • • . . "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibiili of fines and imprisonment for knowing violations" Date Signature of Land Applier A.,.h,,. nFNR FnRM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Chadbourn Total Dry Tons Applied (Annual): 10.84 WQ0001934 Cation Exchange Capacity (non 503 only): n/a Raymond Butler Owner: Raymond Butler Predominant Soil Series NoB 15.42 Acres Permitted: 15.42 Site #: 10 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Total h a. -r-USMENEENEENE00- A 11?i uA1 F al FiAd-1 vai inag(Calculated in lbs/acre)• NMI Total Phos- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includin the possib' ' of fines and imprisonment for knowing violations" Signature of Land Applier A„4,,— n—1 r, Uorriff Date nFNR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals lbs/ac) Nutrients (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. ANiN UAL LAiNli APrLiCATivrN FIELi, aUMivv-VnY F vJM1VI PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Chadbourn WQ Permit #: WQ0001934 Field #: 8 Acres Utilized: 3.30 Owner: Harry R Stickland Annual Dry Tons Applied: 8.53 Site #: 1 Acres Permitted: 3.30 Operator: Harry R Stickland Predominat Soil Series AuB Cation Exchange Capacity (non 503): NA Crop 1 Name: Coastal Bermudagrass Crop 1 Max PAN: 270.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A c d 0 o SpecifV Totals Per Acre o /e Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, Site Cond. (Dry' Wet, Moist Precip past 24 Hrs. Inches b `' t, w c w N 5 w w * # * o TKN m z > o B o w m Nitrate and Nitrite m PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 -Gal. Cu.Yd. . .<< Report Totals0) In Gal. Crop 1 Crop 2 Crop 1 Crop 2 May-14 90,000 27,273 1.61 1.83 wn of Chadbourn W S 0.50 0.30 12,850 336 4 14.38 X Aug-14 40,000 12,121 1.49 0.75 wn of Chadbourn WW S 0.50 0.30 12,850 336 4 5.91 X TOTALS: 39,394 >: >: Annuallbs/acre As 0.03 Cd 0.00 Cr 0.15 Cu 0.55 Pb 0.17 H 0.00 Mo 0.03 Ni 0.05 Se 0.03 Zn 1.64 P 23.02 PAN 1 20.29 PAN 2 0.00 Lime A lied Date lbs/ac lbs/ac Currre ent Cumulative C 0.19 0.04 NA 1 6.17 1.72 0.00 NA 0.3 4 0.20 17. 3 9 Prior Years Cumulative lbs/ acre 0.15 0.03 NA 5.62 1.56 0.00 NA 0.29 0.17 16.30 'tted C. P. L. R. *�*�: Perms 36 34 NA 13 38 267 15 N A 37 4 8 9 24 8 9 n d Crop PAN Limit 1st/2 2 0.00 7 "I certify, under penalty of law, that this document was prepares under my curecuon or supervisiun m nuum uaucc w. 11 a Ay at -a designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." e _ *Application Method: S - Surface, IN - Injection, INC - Incorporation Z f� ��� **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) - ANN UAL LANs) APYLICATiuN FIELD ntJNLviAxY Fumvi PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Chadbourn WQ Permit #: WQ0001934 Field #: 8 Acres Utilized: 4.50 Owner: Harry R Stickland Annual Dry Tons Applied: 8.28 Site #: 2 Acres Permitted: 4.50 Operator: Harry R Stickland Predominat Soil Series AuB Cation Exchange Capacity (non 503): NA Crop 1 Name: Coastal Bermudagrass Crop 1 Max PAN: 270.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A Specify o Volume Residual Sources Site Precip b o z > ct Nitrate PAN Applied Must Select GaI, 4 CJ o ?: Cu.Yd. Totals /o Solids Applied per (NPDES #, WQ#, Cond. Past 24 �. w _ TKN o c and (lbs/acre) Crop 1 or Crop 2 CD Sr o Report Per Acre As Decimal Acre Fert., Animal Waste, (Dry' Wet, Hrs. a w . �• * N * �:, # * w � W' Nitrite Totals etc.) Moist) �' Crop 1 Crop 2 Crop 1 Crop 2 ' in Gal. DT/Ac inches m m m May-14 40,000 8,889 1.61 0.60 wn of Chadbourn WW S 0.50 0.30 12,850 336 4 4.69 X Aug-14 90,000 20,000 1.49 1.24 wn of Chadbourn WW S 0.50 0.30 12,850 336 4 9.76 X TOTALS: 28,889 ;::_:<>:;>s< As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.02 0.00 0.11 0.39 0.12 0.00 0.02 0.03 0.02 1.17 16.39 14.44 0.00 Date lbs/ac u t Cacre Curren Cumulative lbs/ 0.21 0.04 NA 7.09 2.01 0.01 NA 0.58 0.3 2 2 27.52 s Cumulative lbacre Prior Years Cum / 0.19 0.04 NA 6. 0 7 1.89 0.01 N A 0.55 0.3 0 26.36 Permitted C .P.L.R. *:x** 3 6 34 N A 13 38 27 6 IS NA 37 4 89 48 2 9 t ,Permit PAN 12nd Crop a7o.o 0 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance wide a ,Nyaui designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /J *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANC UAL LA m APruiCAT1vir FIELm nUMlviAtcY Fvauv1 " PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Chadboum WQ Permit #: WQ0001934 Field #: 10 Acres Utilized: 15.42 Owner: Raymond Butler Annual Dry Tons Applied: 10.84 Site #: 1 Acres Permitted: 15.42 Operator: Raymond Butler Predominat Soil Series NoB Cation Exchange Capacity (non 503): NA Crop 1 Name: Soybeans Crop 1 Max PAN: 161.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A C7 o ?; 0 '> Specify Totals Per Acre o /o Solids As Decimal Volume Applied per Acre DT/Ac Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc.)Wet, Site Cond. D (Dry, Moist) Precip. Past 24 firs. Inches d �, �. a w o o ro �; * Ir � m * # ° TKN m Z E o0 o @ w m Nitrate and Nitrite m PAN Applied (lbs/acre) Must Select Crop 1 or Crop 2 Gal. Cu.Yd. ` <: Report Totals in Gal. Crop 1 Crop 2 Crop 1 Crop 2 :> Mar-14 130,000 8,431 2.00 0.70 wn of Chadboum WW S 0.50 0.30 12,850 336 4 5.52 X TOTALS: 8,431 :r AS Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.01 0.00 0.04 0.15 0.04 0.00 0.01 0.01 0.01 0.45 6.26 5.52 0.00 Date lbs/ac Current Cumulative lbs/r ac e 0.01 0.00 NA 0.15 0.04 0.00 NA 0.01 0.010.45 0.00 00 .o 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 36 34NA 1,338 267 IS NA 37489 2,498 161.001 Prior Years Cumulative lbs/acre e Permitted C. P. L. R. *** N AN Limit 1st/ 2nd Cro Perm PAp "I certify, under penalty of law, that this document was prepared under my direction or supervision m accormance witn a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and 'imprisonment for knowing violations." �✓�� ����/ C *Application Method: S -Surface, IN ®Injection, INC -Incorporation **Volitilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2, Aerobically Digested - 0.3, Raw Sludge - 0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) RESIDUAL ANALYSIS LAB SHEETS ��dor�o����� alp ��c�oQpoQa�c�d DrinkingWater SDr 3771E k` Wastewater IDs 10 P.O. BOX 7085, 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH (not to be used for reporting) 7.3 02/25/14 TRB 4500HB-00 Aluminum, (dry wt. basis), mg/kg 20792 03/05/14 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 6 03/18/14 MEL 3113B-04 Calcium (dry wt. basis), mg/kg 9807 03/05/14 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg <0.5 03/26/14 MEL 3113B-04 Copper (dry wt. basis), mg/kg 106 03/05/14 LFJ EPA200.7 Chromium, T.(dry wt. basis),mg/kg 29 03/05/14 LFJ EPA200.7 Lead (dry weight basis), mg/kg 32 03/31/14 MEL 3113B-04 Magnesium (dry wt. basis), mg/kg 1529 03/05/14 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.13 03/10/14 ADD 245.1 113-94 Nickel (dry wt. basis), mg/kg 9 03/07/14 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 1862 03/05/14 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 03/25/14 MEL 311313-04 Sodium (dry wt. basis), mg/kg 2323 03/19/14 MTM 311113-99 Zinc (dry wt. basis), mg/kg 317 03/10/14 ADD 3111B-99 Total Solids, % 2.51 02/26/14 MDD 254OG-97 TKN (dry wt.), mg/kg 12850 03/03/14 ANO 351.2 R2-93 Ammonia Nitrogen (dry •rjt.),mg,lkg 336 02/27/14 ANO 350.1 112-93 Phosphorus, T. (dry wt.), mg/kg 4455 03/03/14 ALB 365.4 -74 Nitrate -Nitrite (dry wt.), mg/kg <3.65 02/28/14 ANO 353.2 R2-93 Plant Available Nitrogen, mg/kg 3922 03/06/14 SEJ Molybdenum (dry wt. basis), mg/kg <5.0 03/05/14 LFJ EPA200.7 ID#: 853 C DATE COLLECTED: 02/25/14 DATE REPORTED : 04/02/14 REVIEWED BY: Environment 1, Inc. P.O. Box 7085, 114 Oakmont Dr. Greenville. NC 27858 CHAIN OF CUSTODY RECORD Page 1 of I Phone (252) 756-6208 • Fax (252) 756-0633 DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION CHLORINE CLIENT: 853 C Week: 9 pH CHECK (LAB) UV ❑dNONE P P P P P P P CONTAINER TYPE, P/G TOWN OF CHADBOURN MR. CLINT WARD A A A A A A A CHEMICAL PRESERVATION 602 NORTH BROWN STREET CHADBOURN NC 28431 A -NONE D-NAOH m zo (910) 654-3045 E w" z w Cl) 2 b .� B HNO, E HCL 0 0 z Ir o z O '.sue l)_ CEr c3 4wz � �Zzza LU C - H,SO, F -ZINC ACETATE/NAOH a a w L¢ o ° QCOLLECTION G NATHIOSULFATEo SAMPLE LOCATION DATE TIME0 via alsSludge ' a a 0 Sample ,f 4A 5 • CLASSIFICATION: WASTEWATER (NPDES) DRINKING WATER DWQ/GW SOLID WASTE SECTION CHAIN OF CUSTODY MAINTAINED DURING SHIPMENT/DELIVERY Q N SAMPLES COLLECTED BY: (Please Print) %n ,nr SAMPLES RECEIVED IN LAB ATrl-f'°C RELINQUISHED BY (SIG.) (SAMPLER) DATE(TIME R CE E6Y (SIG.)( DATErnME COMMENTS: :&PM I [ r' �ZCJ RELINQUISHED BY (SIG.) DATErnME RECEIVED BY (SI DATE/TIME RELINQUISHED BY (SIG.) DATE/TIME RECEIVED BY (SIG.) DATUrIME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for N ? 2 6 3 � 71 FARM #5 Grab sample in the blocks above for each parameter reouested. P.O. BOX 7085. 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 Digester 1 Digester 2 PARAMETERS Drinking Water ID; 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 853 J DATE COLLECTED: 02/25/14 DATE REPORTED : 03/03/14 REVIEWED BY: Analysis Method Date Analyst Code Total Residue, mg/1 10967 20600 02/26/14 CMC 2540B-97 Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Town of Chadbourn Town of Chadbourn WWTP Chadbourn, North Carolina Southern Solutions Environmental Wastewater Treatment Plant 853 Cl 2/25/2014 4/2/2014 1st Third 2014 Parameter % PPM Dry Weight EPA Monthly Limits Average Solids* 2.00 Nitrogen (TKN)* 1.285 12,850.000 Phosphorus 0.446 4,455.000 Potassium 0.186 1,862.000 Sulfur Calcium 0.981 9,807.000 Magnesium 0.153 1,529.000 Sodium 0.232 2,323.000 Iron --- Aluminum --- 20,792.000 Manganese --- Copper --- 106.000 1,500 Zinc --- 317.000 2,800 Ammonia Nitrogen* 0.034 336.000 Nitrate N / Nitrite N* --- 3.650 Cadmium --- 0.500 39 Chromium --- 29.000 1,200 Nickel --- 9.000 420 Lead --- 32.000 300 Arsenic --- 6.000 41 Mercury --- 0.130 17 Selenium --- 5.000 100 pH 7.300 Calcium Carbonate Eq. (est) 0.000 Organic Nitrogen 1.251 Molybdenum --- 5.000 75 Chloride --- Boron Available P2O5 Specific Gravity 8.340 Average Solids = Solids average from sampling events during the first half of 2011 Wastewater Treatment Plant Town of Chadbourn WWTP Chadbourn, North Carolina Southern Solutions Environmental 1 st Third 2014 Date Reported: 4/2/2014 Report No: 853 Cl Note All Units in Pounds Per Dry Ton Macro Nutrients Physical Characteristics PAN Surf. 7.852 PAN Inj. 8.188 P 8.910 K 3.724 Lime (estimated) 0.000 Secondary Nutrients Calcium 19.614 Magnesium 3.058 Sodium 4.646 SAR 0.813 Chloride 0.000 Iron 0.000 Alumium 41.584 Manganese 0.000 Boron 0.000 Sulfur 0.000 Residual Nitrogen Calculation Year Min Rate PAN #/Acre % Solids 2.00 PH 7.300 Min Rate 0.300 Metals Arsenic 0.012 Cadmium 0.001 Chromium 0.058 Copper 0.212 Lead 0.064 Mercury 0.000 Molybdenum 0.010 Nickel 0.018 Seleniun 0.010 Zinc 0.634 2011 2012 2013 2014 0.30 7.51 2015 0.15 2.63 2016 0.08 1.12 2017 0.04 0.52 2018 2019 2020 d I 2021 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 PARAMETERS Total Solids, % Drinking Wager IDt 3-71.5 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 853 I DATE COLLECTED: 05/14/14 DATE REPORTED : 05/19/14 REVIEWED BY: Digester 1 Digester 2 Analysis Method Date Analyst Code 0.86 1.61 05/15/14 CMC 2540G-97 S, ZK' I L Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Town of Chadbourn Town of Chadbourn WWTP Chadbourn, North Carolina Southern Solutions Environmental Wastewater Treatment Plant 853 C2 5/16/2014 5/16/2014 2nd Third 2014 Parameter % PPM Dry Weight EPA Monthly Limits Average Solids* 1.61 Nitrogen (TKN)* 1.285 12,850.000 Phosphorus 0.446 4,455.000 Potassium 0.186 1,862.000 Sulfur Calcium 0.981 9,807.000 Magnesium 0.153 1,529.000 Sodium 0.232 2,323.000 Iron --- Aluminum --- 20,792.000 Manganese --- Copper --- 106.000 1,500 Zinc --- 317.000 2,800 Ammonia Nitrogen* 0.034 336.000 Nitrate N / Nitrite N* --- 3.650 Cadmium --- 0.500 39 Chromium --- 29.000 1,200 Nickel --- 9.000 420 Lead --- 32.000 300 Arsenic --- 6.000 41 Mercury --- 0.130 17 Selenium --- 5.000 100 pH 7.300 Calcium Carbonate Eq. (est) 0.000 Organic Nitrogen 1.251 Molybdenum --- 5.000 75 Chloride --- Boron Available P2O5 Specific Gravity 8.340 Average Solids = Solids average from current application event. F.0, BOX 7085, 114 OAKMON T DRiVF GREENVILLE, N.C. 27835-7085 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 PARAMETERS Total Solids, % S' U 111 Digester 1 Digester 2 Drinking Water Ill: 3771!, Wastewater IDs 10 (252) 755-6203 FAX (252) 756-0633 ID#: 853 I DATE COLLECTED: 08/25/14 DATE REPORTED : 09/02/14 01 REVIEWED BY: Analysis Method Date Analyst Code 1.49 0.84 08/29/14 CMC 2540G-97 I �b 000 Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: Town of Chadbourn Town of Chadbourn WWTP Chadbourn, North Carolina Southern Solutions Environmental Wastewater Treatment Plant 853 C3 8/25/2014 9/2/2014 3rd Third 2014 Parameter % PPM Dry Weight EPA Monthly Limits Average Solids* 1.49 Nitrogen (TKN)* 1.285 12,850.000 Phosphorus 0.446 4,455.000 Potassium 0.186 1,862.000 Sulfur Calcium 0.981 9,807.000 Magnesium 0.153 1,529.000 Sodium 0.232 2,323.000 Iron --- Aluminum --- 20,792.000 Manganese --- Copper --- 106.000 1,500 Zinc --- 317.000 2,800 Ammonia Nitrogen* 0.034 336.000 Nitrate N / Nitrite N* --- 3.650 Cadmium --- 0.500 39 Chromium --- 29.000 1,200 Nickel --- 9.000'- 420 Lead --- 32.000 300 Arsenic --- 6.000 41 Mercury --- 0.130 17 Selenium --- 5.000 100 pH 7.300 Calcium Carbonate Eq. (est) 0.000 Organic Nitrogen 1.251 Molybdenum --- 5.000 75 Chloride --- Boron Available P2O5 Specific Gravity 8.340 Average Solids = Solids average from current application event. TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT TCLP FOR THIS FACILITY IS REQUIRED ON A ONCE PER PERMIT FREQUENCY ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION The Town of Chadbourn met pathogen reduction and vector attraction reduction requirements through fecal coliform density and Specific Oxygen Uptake Rate (SOUR). The annual certification form is marked accordingly to reflect the methods of meeting pathogen reduction and vector attraction reduction. The Town of Chadbourn will continue to collect 1 — 2 samples at each application event to verify both fecal and SOUR. — ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Chadbourn WQ Permit Number: WQ0001934 WWTP Name: Town of Chadbourn WWTP NPDES Number: NC0021865 Monitoring Period: From 1/l/2014 To 12/31/2014 iogen Reduction (15A NCAC 02T .1 Class A: Alt. A (time/temp) ❑ Alt.D (No Prior Test) 1plicable to alternative performed (Cla apost ❑ Heat Drying i Ray ❑ Gamma Ray ❑ Class B: I Alt. (1) Fecal Dc pplicable to alternative perforn ke Stabilization bic Di Elzero Digestion g [pplicable to alternative perfi Allowable Level Parameter in Sludge 36) - Please indicate level achieved and alternative performed: Alt B (Alk Treatment) ® Alt. C (Prior Testing) Process to Further Reduce Pathogengs ❑ A only) indicate "Process to Further Reduce Pathogens": Heat Treatment ❑ Thermophilic Pasteurization .... . ty ST Alt. (2) Process to Significan (Class B only) indicate "Process to Signi Air Drying ❑ Composts .ed Class A or Class B complete the Pathogen Density inimurJ Geo. MeanMaximuni Units 2 x 10 to the MPN 2,135 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry Jmonella bacterial 3 MPN per 4 grams (in lieu of fecal total solid (dry aptly Reduce Pathogens": ® Aerobic Digestion ❑ .............................. [lowing monitoring data: um er ot I Frequency I Sample a ytic Excee- Tech - A —` of Analysis IType niaue 21,995 I 171,435 I MPN/ Gram I 0 Annually Grab I SM18 9221E t 7__L..-. ♦ u......a:..-. D..dv..ti.... !1 C A ivir A!' fi'fT 11 fill _ planed- intliente alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) Rl Alt. 5 (14-Day Aerobic) ® Alt. 6 (Alk. Stabilizatioi❑ Alt 7 (Drying - Stable) ❑ JAR. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ® Alt. 10 (Incorporation) ® No vector attraction reduction alternatives were performed ❑ CENFIL ' LUA IUA a l A I hNIZ1N 1 (please C11CCK ine cipprupriaLV BLU Mu"Ll El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if ❑ you check this statement attach an explanation why you have not met one or both of the` requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Daniel C. Ward, Chadbourn WWTP ORC Preparer eand Title (type or print) Z-16-1S Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The Town of Chadbourn met pathogen reduction and vector attraction reduction requirements through fecal coliform density and Specific Oxygen Uptake Rate (SOUR). Documentation is attached to reflect pathogen reduction and vector attraction reduction options. The Town of Chadbourn will continue to collect 1 — 2 samples at each application event to verify both fecal and SOUR. Town of Chadbourn Town of Chadbourn WWTP WQ0001934 2014 Enviroment 1, Inc Lab # Date Analyzed Fecal Coliform MPN per gram Log 1 2/26/ 14 52,260 4.718 2 2/26/ 14 4,187 3.622 3 4/23/14 7,874 3.896 4 7/23/14 2,135 3.329 5 8/27/14 30,393 4.483 6 8/27/14 171,435 5.234 7 10/17/14 129,936 5.114 Totall 30.396 Averagel 4.342 Most Probable Number / Gram 21,995 Fecal Coliform/gram Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction requirement Data provided in this summary have been used for the values and geometric means reported on the Annual Pathogen and Vector Attraction Reduction Form for this land application event. 11 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 Drinking Water TD: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 853 D DATE COLLECTED: 02/25/14 DATE REPORTED : 03/03/14 REVIEWED BY: Sample Sample Analysis Method PARAMETERS #1 #2 Date Analyst Code Total Residue, mg/l 10333 22800 02/26/14 CMC 2540B-97 Fecal Coliform (MPH /gram Solids 52260 4187 02/26/14 CMC 9221E-06 EIMUQMBPE4 % �[@C@ oQshd P.O. BOX 7085, 114 OAKMONT GREENVILLE, N.C. 27835-7085 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 Sample PARAMETERS #3 Total Residue, mg/l 10033 Fecal Coliform (MPH /gram Solids 7874 Drinking Seater ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 853 E DATE COLLECTED: 04/22/14 DATE REPORTED : 05/01/14 REVIEWED BY: Sample Analysis Method #4 Date Analyst Code 16900 04/23/14 LW 2540B-97 2135 04/23/14 LW 9221E-06 P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 Dranki.ng Water ID+ 37715 Wastewater ID: 10 PHONE t252) 756-6208 FAX (252) 756-0633 ID#: 853 F DATE COLLECTED: 08/26/14 DATE REPORTED : 08/29/14 REVIEWED BY: "-0/ Sample Sample Analysis Method PARAMETERS #5 #6 Date Analyst Code Total Residue, mg/1 17767 9430 08/27/14 CMC 2540B-97 Fecal Coliform (MPH /gram Solids 30393 171435 08/27/14 CMC 9221E-06 TOWN OF CHADBOURN MR. CLINT WARD 602 NORTH BROWN STREET CHADBOURN ,NC 28431 PARAMETERS Total Residue, mg/1 Fecal Coliform (MPH /gram Solids Sample Analysis Method #7 Date Analyst Code 12317 10/15/14 LW 2540B-97 129936 10/15/14 LW 9221E-06 Drioking wale; !-- 37/1.5 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 853 G DATE COLLECTED: 10/14/14 DATE REPORTED : 10/17/14 REVIEWED BY: Town of Chadbourn Town of Chadbourn WNffP WQ0001934 2014 "19 Yi g 3/13/2014 0.78 3/12/2014 0.61 5/16/2014 0.09 5/16/2014 0.07 8/26/2014 0.11 8/26/2014 0.42 10/17/2014 0.66 10/17/2014 0.22 * SOUR = Specific Oxygen Uptake Rate Averagel. :. SOUR values are less than 1.5 mg oxygen/gram/hour and meets the 40 CFR Part 503.33 Option 4 for Vector Attraction Reduction. SOUR values provided by Town of Chadbourn Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Chadbourn wwtp Biosolids Permit Number: WQ0001934 Date: 3/13/2014 Digester Temperature: 12 Sampling Date/Time: 3/13/14/5:05 pm Sampled By: Daniel C. Ward Analysis DatelTime: 3/13/14/5:07 Analyzed By: Daniel C. Ward Total Solids: 2 % Dry Solids Beginning Temperature: 13 degrees Celsius End Temperature: _ 14 degrees Celsius Dissolved Oxygen Level Slope: 0.17 Intercept: 9.5 Correlation Coefficient: 0.95 Oxygen Uptake Rate: 10.39 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.52 mg Oxygen/hr/g Average Temperature: 14 degrees Celsius Temperature Correction Factor: 1.50 Temperature Corrected Specific Oxygen Uptake Rate:0.78 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Dry Solids grees Celsius arees Celsius 0.06 9.0 0.92 3.82 mg Oxygen/hr 0.38 mg Oxygen/hr/g 13 degrees Celsius 1.61 Temperature Corrected Specific Oxygen Uptake Rate: -- 0.61 :mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 1012312013 Specific Oxygen Uptake Rate SOUR Facility Name: Chac Biosolids Permit Number: WQ( Date: Digester Temperature: Sampling Date/Time: Sampled By: Clint Analysis Date/Time: 5/16� Analyzed By: Clint Total Solids: Beginning Temperature: End Temperature: Time Dissolved Oxygen Level (minutes) (mg/l) 0 8.67 1 8.58 , 2 8.48 3 8.43 4 8.41 5 8.39 6 8.37 7 8.37' 8 8.38 9 8.37 10 8.36 11 8.37 12 8.35 13 8.35 14 8.36 15 8.35 , 001934 5/16/201 23. 0.86 % Dry Solids 23.8 degrees Celsius 23.4 degrees Celsius Slope: 0.02 Intercept: 8.5 Correlation Coefficient: 0.78 Oxygen Uptake Rate: 0.90 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.10 mg Oxygen/hr/g Average Temperature: 24 degrees Celsius Temperature Correction Factor: 0.82 Temperature Corrected Specific Oxygen Uptake Rate: 0.09�mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Chadbourn m Biosolids Permit Number: WQ0001934 Date: 5116 Digester Temperature: Sampling Date/Time: 5-16-14/12:0 Sampled By: Clint Ward Analysis Date/Time: 5-16-14/12:0 Analyzed By: Clint Ward Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 24. 1.61 % Dry Solids 24.6 degrees Celsius 24.2 dearees Celsius 0.02 8.5 0.98 1.41 mg Oxygen/hr 0.09 mg Oxygen/hr/g 24 degrees Celsius 0.82 Temperature Corrected Specific Oxygen Uptake Rate: = 0.07 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Chadbourn Biosolids Permit Number: W0000191 Date: 8/� Digester Temperature: Sampling Date/Time: 8/26/14/6:3 Sampled By: Clint Ward Analysis Date/Time: 8/26/14/6:3 Analyzed By: Clint Ward Total Solids: Beginning Temperature: End Temperature:--__7 Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: am o Dry Solids egrees Celsius egrees Celsius 0.03 8.4 0.94 1.91 mg Oxygen/hr 0.13 mg Oxygen/hr/g 24 degrees Celsius 0.82 Temperature Corrected Specific Oxygen Uptake Rate: a 0.11 fmg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Chadbourn wwtp Biosolids Permit Number: W00001934 Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level m 4 Dry Solids grees Celsius arees Celsius Slope: 0.07 Intercept: 8.6 Correlation Coefficient: 0.97 Oxygen Uptake Rate: 4.30 mg Oxygenlhr Ambient Specific Oxygen Uptake Rate: 0.51 mg Oxygen/hr/g Average Temperature: 24 degrees Celsius Temperature Correction Factor: 0.82 Temperature Corrected Specific Oxygen Uptake Rate: =0.42 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Chadbourn wwtp Biosolids Permit Number: W00001934 Date: 10/17/201 Digester Temperature: 2 Sampling Date/Time: 10/17/14/5:20pm Sampled By: Clint Ward Analysis Date/Time: 10/17/14/5:21 pm Analyzed By: Clint Ward Total Solids: 1.2 Beginning Temperature: 1 End Temperature: ` —___ 2 Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.14 8.8 0.98 Dry Solids grees Celsius gees Celsius 8.21 mg Oxygen/hr 0.66 mg Oxygen/hr/g 20 degrees Celsius 1.00 q0/0J0 Temperature Corrected Specific Oxygen Uptake Rate:[' 0.66 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Chadbourn.v+ Biosolids Permit Number: W00001934 Date: 10/17 Digester Temperature: Sampling Date/Time. 10/17/14/5:4 Sampled By: Clint Ward Analysis Date/Time: 10/17/14/5:5 Analyzed By: Clint Ward Total Solids: Beginning Temperature:. End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 21 o Dry Solids egrees Celsius egrees Celsius 0.03 9.3 0.92 1.93 mg Oxygen/hr 0.23 mg Oxygen/hr/g 21 degrees Celsius 0.95 Temperature Corrected Specific Oxygen Uptake Rate: � 0.22 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Updated 10/23/2013 SOIL ANALYSIS REPORTS Page 1 of 1 Report Number: 15-054-0520 Account Number: 46368 Send To: BRANCH RESIDUALS & SOILS LLC WWwaleastemcom BOB BRANCH 8646 West Market Street Suite 111 GREENSBORO NC 27409 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 2714446 Grower: Submitted By: BOB BRANCH STRICKLAND Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 n..•., n---:--A. wwv2ionir i1.fn of An.iv i.- n919d/9n1r. rhfo of Rannrf• n9/9d/9M5 -------------- Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate lbs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meq/100g 1 23460 1.2 L 67 226 VH 23 VL 104 H 717 H 6.8 0.1 4.6 NC=188 NC=12 2 23461 2.8 M 94 482 VH 32 VL 183 H 1346 H 6.7 0.4 8.7 NC=402 NC=16 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl Al Field ID ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1 11.3 VH 6.3 VH 1.3 18.8 77.9 2.9 NC=282.5 INC =315.0 2 35.3 VH 13.0 VH 0.9 17.5 77.4 4.5 NC = 882.5 1 NC = 650.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g mapmum of thirty days after testing. by: Pow'. me 60 H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. p C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 1 of 1 - Report Number: 15-054-0519� Account Number: 46368 ft Send To: BRANCH RESIDUALS & SOILS LLC wwwaleaaterncom BOB BRANCH 8646 West Market Street Suite 111 GREENSBORO NC 27409 r%-#- o....eh—A- n9/9a/9rN F rinfa Of Anniucic. n9/9A/9016 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-MG Grower: Submitted By: BOB BRANCH BUTLER Farm ID: PROJECT 2004-34 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 nafp of Ronnrt. n2/24/2n1s Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number %, Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meq/100g 1 23459 1.4 L 73 111 VH 75 M 44 M 458 M 6.1 6.88 0.5 3.3 NC=92 NC=38 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl Al Field ID % % % off, % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 1 3.8 H 1.1 M 5.8 11.1 69.4 13.7 NC=95.0 NC=55.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pod. me� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/em x 640 = ppm. Pauric McGroary 2014 APPLICATION SUMMARY TABLE LAND APPLICATION PROGRAM PERMIT NO. WQ0001934 SOUTHERN SOLUTIONS ENVIRONMENTAL 2014 APPLICATION SUMMARY ....... .... . ..... ............ . Harry R Strickland 8 1 3.3 May-14 90,000 1.83 6.04 Coastal Bermudagrass 20.29 Aug-14 40,000 0.75 2.49 Coastal Bermudagrass 2 4.5 May-14 40,000 0.60 2.69 Coastal Bermudagrass 14.44 Aug-14 90,000 1.24 5.59 Coastal Bermudagrass Raymond Butler 10 1 15.42 Mar-14 130,000 0.70 10.84 Soybeans 5.52 Number of Fields Applied to: 3 23.22 Town of Chadbourn WWTF Permit Limit ...... ....... . etric< 390000 , 27.65 25.13 200 Branch Residuals Soils, LLC Confidential 2/9/2015 Page 1 W z 0 H �a z 0 U O E� U a a� 0 N Town of Chadbourn Chadbourn, North Carolina Southern Solutions Environmental WQ0001934 1st Third 2014 Town of Chadbourn WWTP Farmer: Raymond Butler Acres: 15.42 Site/Tract: 10 Application Method: Surface Field: 1 Percent Solids: 2.00 Residual Report No.: 853 C1 Crop: Soybeans Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 3/14/14 1 40,000.0 Dry Cloudy 3/18/14 1 90,000.0 Dry Cloudy olGallviiis::::<:.:::><::; ::>:.:: 0 93 00.0..0 Town of Chadbourn Chadbourn, North Carolina Southern Solutions Environmental WQ0001934 2nd Third 2014 Town of Chadbourn WWTP Farmer: Harry R Strickland Acres: 3.3 Site/Tract: 8 Application Method: Surface Field: 1 Percent Solids: 1.61 Residual Report No.: 853 C2 Crop: Coastal Bermudagrass Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 5/24/14 1 90,000.0 Dry Sunny i0 0000 11 Town of Chadbourn Chadbourn, North Carolina Southern Solutions Environmental WQ0001934 2nd Third 2014 Town of Chadbourn WWTP Farmer: Harry R Strickland Acres: 4.5 Site/Tract: 8 Application Method: Surface Field: 2 Percent Solids: 1.61 Residual Report No.: 853 C2 Crop: Coastal Bemiudagrass Date Field No. Subfield Gallons Soil Weather Prev. 24 Hour Conditions Conditions Rainfall 5/25/14 2 40,000.0 Dry Sunny ::..T. tai..Galzons>>>::'::>:>:.. 1.0.. 0..:.. Town of Chadbourn Chadbourn, North Carolina Southern Solutions Environmental WQ0001934 3rd Third 2014 Town of Chadbourn WWTP Farmer: Harry R Strickland Acres: 3.3 Site/Tract: 8 Application Method: Surface Field: 1 Percent Solids: 1.49 Residual Report No.: 853 C3 Crop: Coastal Bermudagrass Date Field No. Subfield Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 8/26/14 1 40,000.0 Dry Clear ..::..:... .:::. ::::;:.:.::.::.::.;> ::.::.:::.::: ;:.:: Town of Chadbourn Chadbourn, North Carolina Southern Solutions Environmental WQ0001934 3rd Third 2014 Town of Chadbourn WWTP Farmer: Harry R Strickland Acres: 4.5 Site/Tract: 8 Application Method: Surface Field: 2 Percent Solids: 1.49 Residual Report No.: 853 C3 Crop: Coastal Bermudagrass Date Field No. Subfaeld Gallons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 8/27/14 2 90,000.0 Dry Clear atal.:Gallons:.: ::..; ...:9.:.:Q,U00