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HomeMy WebLinkAboutWQ0001347_Residual Annual Report 2014_20150123MI.IIerCoOe:S'- 863 E Meadow Road . Eden, NC 27288-3636 . January 15, 2015 CERTIFIED MAIL . RETURN RECEIPT REQUESTED Mr. Ed Hardee NCDENR Division of Water Quality Aquifer Protection Section 1636 Mail Service Center Raleigh, NC 27699-1636 RE: Annual Distribution and Marketing/Surface Disposal Certification and Summary Distribution of Process Residuals Permit Number WQ0001347 MillerCoors LLC, Eden, NC Dear Mr. Hardee: Please find enclosed the Annual Distribution and Marketing/Surface Disposal Certification and Summary for MillerCoors LLC located in Eden, Rockingham County, North Carolina. Three copies of the following forms have been included: 1:) Annual Distribution and Marketing/Surface Disposal Certification and Summary (Form DMSDF) 2) Annual Residual Sampling Summary Form (Form RSSF) 3). Annual Residual Sampling Summary Form (Form RSSF-B) 4) List of Recipient Information 5) 3 Copies of Lab Residual Analysis Results Please contact me if you should have any questions or comments at 336-627-2136 or via e-mail at eric.tillman(a-)-millercoors.corri Sincerely, "7 Eric Tillman Environmental & Sustainability Engineer PC: Mike Van Foots Audrey Templeton —Milwaukee, WI Jim Smith Mike Lozano Matt Toms RECEIVEDIIDEN.RWR JAN S wat®I Queli Pemil##lin9 seclion c ANNUAL DISTRIBUTION.AND MARKETING/ SURFACE DISPOSAL CERTIFICATION:AND SUMMARYNORM PERMIT #: WQ0001347 FACILITY NAME: MillerCoors LLC PHONE: 336-627-2100 COUNTY: Rockingham OPERATOR:-MillerCoors LLC FACILITY TYPE (please check one): 13 Surface Disposal (complete Part A (Source(s) and -'.'Residual: In" Volume only) and Part C) 0 Distribution and Marketing (complete Parts A, B; and C) . Was the facility in operation durin! the east calendar *ear?. 0 Yes OM) No If No, skip parts A,=B, C and certify form below ...... __.. � ..... Part A*: ... .... ...- .. .... Part.B*: .:::... Month (include NPDES. # if Sources(s) (i applicable) Volume (dry tons) Recipient Information Admendment/ Bulking Agent Residual In Product Out Name(s) Volume(dry tons): Intended.use(s) January_ :. NCO029980 9 . 31.7.38 326.38 -. S:ee-Attached_Sheet -. . February NCO029980 - 5.2 183.03 188.23 -See Attached Sheet; March - NCO029980 7.4 :.: 261.28 268.68 See Attached Sheet APeil::: NC0029980 = ::5.4 182.26: - 187.36 ::':'See Attached Sheet. May .. NC0029980 .... 3.9. .... 138.61 ..142.51... See Attached Sheet June NCO029980 4.5 :.. :160.28 164.78. See Attached Sheet July NCO029980 6.6::_ .- .233.15 239.75.... See Attached Sheet ... August : NCO029980 5 = -175..99 180.99 SeeAttached Sheet September NCO029980 2.8 100.35 103.15 See Attached Sheet October NCO029980 4.5 157.7 162.2 See Attached Sheet November NC0029980 7.1 = 249.99 257.09 See Attached Sheet December. NCO029980 5.9 20.8.79 214.69 . See Attached- Sheet Totals: Annual (drytons)::.. 67 . : 2368.81 2435.81: ............................ :::::::::::::::::::::::::::::::::::::::::::::::: : 0: .................... Admendment s used I None' :: = = Bulking Agent(s) used::::: :. = :.Lime * If more space than given is required, lease attach'additional information sheets : R Check box if additional sheet s ' are attached p g q �p (). .. Part C: Facilitywas com hantAurin calendar year. 2014:-.. with all: conditions of the' permit (including but. not limited to items: below issued.b the: P� g .... Y ... P. (� g )� Y Division of Water Quality. 21: Yes. 0 : No If No, please provide a written description why -the facility was not compliant. 1. All monitoring was done in accordance with the permit and -reported for the year as required and three (3) copies of certified laboratory results are attached. .:2.:All operation and maintenance requirements were compiled :with or, in the case of a deviation, prior authori2ation was received .from the: Division of Water _. _. __. _. .. ... Quality.. . - 3. No contravention of Ground Water: Quality. Standards. occurred -at'a monitoring well. "I certify, under .penalty of law, that the above information is; to the best of in Y. knowledge :a belief, true, :accurate and complete._ I am: aware th ,here are significant penalties for submitting false informaiton, iricludin the oss' ili of fines and imprisonment for knowing violations." :. . nature -of Permittee , Date. Signature of Preparer** Date ... (i different a ee) * *Preparer' differe from=P rmitt, arer is defined in 40 CFR Part 503.9 r -. p ......... DENR�FORM DMSDF: (5/2 003) ...... ... ...: ANNUAL RESIDUAL SAMPLING SUMMARY FORM t Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001347 Facility Name: NPDES # or WQ#: WWTP Name: Residual Analysis Data MillerCoors LLC NCO029980 NA Laboratory: 1) 2) 3) U, ©, Meritech, Inc Sample or Composite Date 2/3/14 4/1/14 6/2/14 8/1/14 10/2/14 12/1/14 Percent Solids 17.7 14.4 13 11.8 14.4 14.2 Arsenic NA NA NA NA NA NA Cadmium 0'.594 <.694 <.769 <.847 <.694 <.704 Chromium NA NA NA NA NA NA b Copper 57..2 69.4 66.4 38.1 26.1 32.5 ?� Lead 8.56 11.1 12 7.64 7.15 3.63 Mercury NA NA NA NA NA NA CD CD Molybdenum NA NA NA NA NA NA Nickel 17.7 15.5 12.5 8.12 4.45 5.43 tQ- Selenium NA NA NA NA NA NA Zinc 163 215 298 231 207 202 Total Phosphorus 7,000 7,638 9,154 9,580 9,100 47310 TKN 11,700 33,600 11,000 44,900 195500 37,500 ]Eli Ammonia -Nitrogen 369 2930 6180 6640 1120 37820 Nitrate and Nitrite <56.5 1 <69.4 1 <76.9 <84.7 <69.4 —F—I <70.4 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Date DENR FORM RSSF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001347 Laboratory: 1) Meritech, Inc Facility Name: NPDES # or WQ#: WWTP Name: Residual Anal sis Data MillerCoors LLC NCO029980 NA 2) 3) 4) 5) Sample or Composite Date 2/3/14 4/1/14 6/2/14 8/1/14 10/2/14 12/1/14 pH 6.8 6.6 9.2 7.5 7.4 7.5 Nitrogen, Total 14,436 33,669 11,077 44,985 19,569 37,570 PAN 3,370 72,137 - 24,407 203,919 16,563 103,253 Aluminum, Total 7,440 7,777 3,792 1,960 840 496 Calcium, Total 8,670 22,638 38,846 36,900 40,100 8,100 b Magnesium, Total 1,940 2,270 3,354 2,530 23,100 2,840 Potassium, Total 3170 3,188 3462 3030 31900 4,310 Sodium, Total 3760 3,514 6846 4490 3,970 5,620 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for ubmitting false information, including the possibility of fines -and imprisonment for knowing violations." Signature of Preparer Date DENR FORM RSSF-B (5/2003) FARM ON nISTRIRUTION 2014 NORTH CAROLINA See Farm Recl lent Tab for Locations 261 296.93 52.56 368 401.17 71.01 369 112.3 19.88 367 174.17 30.83 368 302.04 53.46 169 62.11 10.99 55 206.21 36.50 367 289 51.15 1843.93 326.38 369 499.61 88.43 169 18.00 3.19 321 545.86 96.62 1063.47 188.23 369 242.43 42.91 321 194.04 34.35 169 77.14 13.65 367 413.93 73.27 370 522.85 92.54 367 67.58 11.96 1517.97 268.68 369 321 150.06 121.44 21.61 17.49 367 389.27 56.05 169 380.49 54.79 309 206.85 29.79 370 53.01 7.63 0.00 1301.12 187.36 406 220.00 31.68 321 104.35 15.03 344 665.31 95.80 989.66 142.51 344 319 648.93 1 618.6 84.36 80.42 1267.53 164.78 319 370 1520.39 323.84 197.65 42.10 1844.23 239.75 319 321 667.83 586.67 78.80 69.23 169 96.07 11.34 329 183.23 21.62 1533.80 180.99 321 11 690.58 183.56 81.49 21.66 874.14 103.15 329 55 250.43 325.08 36.06 46.81 276 373.45 53.78 277 177.45 25.55 1126.41 162.20 329 276 580.68 349.63 83.62 50.35 1 584.80 84.21 55 270.25 38.92 1785.36 257.09 1 279 117.55 83.25 16.69 11.82 367 524.16 74.1 370 384.85 54.65 276 402.12 57.10 1511.93 214.69 16659.551 2435.82 Dry Solids Sample Date 17.7 1 2/3/2014 14.4 2 4/1/2014 13 3 6/2/2014 11.8 4 8/1/2014 14.4 5 10/2/2014 14.2 6 12/1/2014 14.3 Average North Carolina Land Application Month Total Lime In NC ProductOut VA Out Total Out %VA %NC Total Lime NC Tons Lime Jan 9.65 326.38 25.28 351.66 7.2% 92.8% 9.65 9.0 Feb 7.40 188.23 81.51 269.74 30.2% 69.8% 7.40 5.2 March 10.58 268.68 116.89 385.57 30.3% 69.7% 10.58 7.4 April 7.72 187.36 93.7 281.06 33.3% 66.7% 7.72 5.1 May 7.85 142.51 143.62 286.13 50.2% 49.8% 7.85 3.9 June 4.52 164.78 0 164.78 0.0% 100.0% 4.52 4.5 July 6.58 239.75 0 239.75 0.0% 100.0% 6.58 6.6 August 5.79 180.99 29.85 210.84 14.2% 85.8% 5.79 5.0 Sept 5.50 103.15 97.27 200.42 48.5 % 51.5 % 5.50 2.8 Oct 7.901 162.2 125.5 287.7 43.6% 56.4% 7.90 4.5 Nov 7.06 257.09 0 257.09 0.0% 100.0% 7.06 7.1 Dec 6.24 214.69 12.54 227.23 5.5% 94.5% 6.24 5.9 Total 86.8 2435.81 726.16 3161.97 23.0% 77.09e.1 86.81 66.87 2014 Purchased Lime (lbs) Purchased Lime (tons) Total NC and VA Dry Tons Tons Lime/Ton Dry 173600 86.8 3161.97 0.027451241 Plant Available Nitrogen Calculation 2014 Reporting Year mg/kg NH3-N NN TKN Organic-N Volatization Rate (V) Demineralization Factor (D) Mineralization Factor (K) Feb-14 Apr-14 369 2930 56.5 69.4 11700 33600 11274.5 30600.6 Jun-14 Aug-14 6180 6640 76.9 84.7 11000 44900 4743.1 38175.3 Oct-14 Dec-14 1120 3820 69.4 70.4 19500 37500 18310.6 33609.6 0.5 Per Derrick Denard - NCDENR on 6/30/11 0 Lime -Stabilized 0.4 Per Derrick Denard - NCDENR on 6/30/11 PAN = [AN x(1-V/100) + NN + ON x (K/100)] x (1-D/100) X 0.002 Plant Available Nitrogen 3370 72137 ' 24407 203919 16563 103253 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Andrew Lucas Report Date: 2/17/2014 Client: MillerCoors NPDES #: NCO029980 863 East Meadow Road Eden, NC 27288 Date Sample Rcvd: 2/3/2014 Meritech Work Order # 02031403 Sample: Farm On Grab 2/3/14 Parameters Result Analysis Date &porting Limit Method % Total Solids 17.7 % 2/5/14 0-100 % SM 2540B Ammonia, Nitrogen 369 mg/kg 2/5/14 10 mg/kg EPA 350.1 TKN 11,700 mg/kg 2/7/14 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen < 5 6. 5 mg/kg 2/6/14 56.5 mg/kg EPA 353.2 Aluminum, total 7,440 mg/kg 2/9/14 5.00 mg/kg EPA 200.7 Cadmium, total 0.594 mg/kg 2/9/14 0.200 mg/kg EPA 200.7 Calcium, total 8,670 mg/kg 2/9/14 10.0 mg/kg EPA 200.7 Copper, total 57.2 mg/kg 2/9/14 10.0 mg/kg EPA 200.7 Lead, total 8.56 mg/kg 2/9/14 2.0 mg/kg EPA 200.7 Magnesium, total 1,940 mg/kg 2/9/14 10.0 mg/kg EPA 200.7 Nickel, total 17.7 mg/kg 2/9/14 2.0 mg/kg EPA 200.7 Phosphorous, total 7,000 mg/kg 2/9/14 2.00 mg/kg EPA 200.7 Potassium, total 3,170 mg/kg 2/9/14 20.0 mg/kg EPA 200.7 Sodium, total 3,760 mg/kg 2/9/14 20.0 mg/kg EPA 200.7 Zinc, total 163 mg/kg 2/9/14 10.0 mg/kg EPA 200.7 pH 6.8 S.U. 2/4/14 1.0-14.0 S.U. SM 4500-H B I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain, of Custody Record COC Client: MillerCoors Address: 863 E. Meadow. Road Eden, NC 27288 ,E Attention: n NPDES #: NCO029980 Phone: 336-627-2592 Fax: Email: nunmhassan millercoors.com Project: POV: RITECH INC. Environmental Laboratories ~ y gy and Control • �,,,- A Division of Water Tcchnolo , Inc. 642 Tamco Rd Phone 1-336-342-4.748 Reldsville, .NC Fax: 1-336-342-1522- .27320 Email: wtclab@bellsouth.net Web Site: www.meritech=labs.com Turn Around Time* Std (10 days) L� 3 - 5 Day o 24 - 48 Hr Sample LocatiOnLiD # Sampling Dates & Times person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #' conts. qbf Tests Re uir d On Ice? ' pH'OK? C12 OK? Date Time Date Time Farm On 3 % Grab O ,Cadmium, Copper, Lead, Nickel,.Zinc, Ammonia -Nitrogen, Calcium; Magnesium, Nitrate -Nitrite -Nitrogen, pH, Phosphorus,. % Total Solids, Plant Available Nitrogen (by calculation) Potassium, Sodium, TKN, Aluminum Method of Shipment: Comments: Express results -as mglkg (Dry weight basis) [] UPS Q Fed Ex Hand Delivery ❑Other Will these results be used for regulatory purposes? Yes Yes No *RUSH work must be approved prior to submitting samples. Relinquis by: Date:, Time: 4 j x Recei d by: Date: Time: �.¢S_ ._ iN L Relinquishedb .. Date: Time: Received by: ate. 'Time: Rellnquis ed by: Date: Time: Re a y: Date Time: Meritech,' .Inc. Environmental Lab6rat6ry . ]Laboratory Certification No.165 Contact: Andrew Lucas Report Dater 4./16/2014 Client' Mi1lerCoors NPDES #: NCO029980 863 East Meadow Road Eden, NC. 27.288 Date Sample Revd; 4/2/2.014 Meritech Work Order # 04021418 Sample: Farm On Grab . .. 4_/1/14 Parameters Result Analysis Date:. ReportingiLimit Method , Total Solids 14.4 % 4/3/14. 0-100 % SM 2540B Ammonia, Nitrogen 2930 mg/kg 4/3/14 10 mg/kg EPA 350.1 TKN 33,600 mg/kg 4/7/14 20 MOT EPA 351.1 . Nitrate/Nitrite, Nitrogen <- 69.4 mg/kg 4./4/14 69.4 mg/kg EPA 35'3.2' Aluminum, total _ 7,777 mg/kg 4./7/14 5,00 .mg/kg EPA 200.7 Cadmium, total < 0.694 mg/kg 4/7/14 .0:694 .mg/kg E A:200.7 Calciunxjotal 22,638 mg/kg 4/7/14. 10.0 mg/kg. EPA -200.7' Copper, total 69.4 mg/kg 4/7/14 10.0 mg/kg EPA 200.j. Lead, total 11.1 mg/kg 4/7/14 2.0 mg/kg EPA 200.7 Magnesium, total 2,270 mg/kg 4/7/14 10.0 mg/kg EPA 200.7 Nickel, total 15.5 mg/kg 4/7/14 2.0 mg/kg EPA 200.7:: Phosphorous, total 7,638 mg/kg 4/7/14 2.00 mg/kg EPA 200.7 Potassium, total. 3,188 mg/kg 4%7/14 20A mg/kg. EPA 200:7 Sodium, total 3,514 mg/kg 4/7/14 20.0 mg/kg EPA 200.7 Zinc, total 215 mg/kg -4/7/14 10.0 mg/kg EPA 200.7 pH 6:6 S-.U. 4/4/14 1.0=14.0 S.U. SM 4500-14 B I hereby i certthat I have. reviewed and a certify -that pprove these data. Laborat®ry Representative 642 'Tarmco ]toad, l8eidsvdle; North Carolina 27320 teL(910)342-4748 fax..(910)342-!IS22 Chain. of Custody Record (COC) Client': 'MillerCoors Address. 863 E. Meadow Road -Eden-, -NC.272aa Attention: Hassan Nunn NPDES M NCO029980 Phone: 336-627-2692 Fax, Email: nunn;hassan(amilfercoors.com Project PO #; MERITECHINCO 'Environmental Laboratories A Division; of Water Technology and Control, Inc. 642 Tamco Rd Phone 1-336-342-474 8 Reidsville. N.0 Fax: 1-336-342;-1522 .27320 Email., wtclab(ftellsouthi net Web'Site: www.meritech-labs.COM Turn Around Time* Std(lodays) . 3-SDay 24 -48 Hr Sample Location/ID # SamplingDates & Times Person Taking.Sample (Signature): I9y Lab Use Only START END Comp? Grab? #of Conts. Tests Required On Ice? pH OK? C1 2 OK? Date Time Date Time Farm On, ML/ Grab. ,5¢--tr Cadmium, Copper, Lead, Nickel, Zinc, Ammonia-Nit-rogen,,Calcium,.Magnesium, Nitrate -Nitrite -Nitrogen, pH, Phosphorus, % Total -Solids, Plant Available Nitrogen (by calculation) Potassium, -Sodium, TKN, Aluminum Md-thod of Shipment: �Comments: Express results,as mglkg (Dry weight basis) UPS F-I.:Fed.Ex Q.Hand Delivery ❑Other Will these results be. used for regulatory purposes? Yes 1-Yes No *RUSH work must be approved prior to submitting samples. Relinquished by: Date: Time: a!P I -A Re Y: ate l Time: Relinquished by: Date: Time: Received ty' Date: Time: Relinquished by: Date: Time: JR!2b Time- b Y7 o lw e, (I Meritech, Inc. -b Environmental Laboratory Laboratory Certification No.165 +a' Contact: Andrew Lucas Client: Mi1lerCoors 863 East Meadow Road Eden, NC 27288 Report Date: NPDES #: Date Sample Rcvd: 6/16/2014 NCO029980 6/2/2014 Meritech Work Order # 06021417 Sample: Farm On Grab 6/2/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 13.0 % 6/3/14 0-100 % SM 2540B Ammonia, Nitrogen 6,180 mg/kg 6/4/14 10 mg/kg EPA 350.1 TKN 11,000 mg/kg 6/12/14 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen < 76.9 mg/kg 6/6/14 76.9 mg/kg EPA 353.2 Aluminum, total 3,792 mg/kg 6/5/14 5.00 mg/kg EPA 200.7 Cadmium, total < 0.769 mg/kg 6/5/14 0.769 mg/kg EPA 200.7 Calcium, total 38,846 mg/kg 6/16/14 10.0 ing/kg EPA 200.7 Copper, total 66.4 mg/kg 6/5/14 10.0 mg/kg EPA 200.7 Lead, total 12.0 mg/kg 6/5/14 2.0 mg/kg EPA 200.7 Magnesium, total 3,354 mg/kg 6/16/14 10.0 mg/kg EPA 200.7 Nickel, total 12.5 mg/kg 6/5/14 2.0 mg/kg EPA,200.7 Phosphorous, total 9,154 mg/kg 6/5/14 2.00 mg/kg EPA 200.7 Potassium, total 3,462 mg/kg 6/16/14 20.0 mg/kg EPA 200.7 Sodium, total 6,846 mg/kg 6/16/14 20.0 mg/kg EPA 200.7 Zinc, total 298 mg/kg 6/5/14 10.0 mg/kg EPA 200.7 pH 9.2 S.U. 6/5/14 1.0-14.0 S.U: SM 4500-H B I hereby certify that I have reviewed and approve these data. .-10 2'c Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chaln..'of CUStOd " ReCOi"d CiQ�i: Client: IVlil le`r,Cooes; Address:. 863: E. Meadow: Road . Eden;.:NC 27288, Attention: - NPDESVa- NC0029980 , Phone: 336-627=2597 Fax: Email: nunn:hassan millembors_com Prg1ect:. Pol#:> - MERIT° H a1� C _:w. _ 'Enviroximental Laboratories A Division of Water Technology aiid.Control,;Tnd.: 642 Tamco Rd: Phon`e. 1-336-342-4748 Reidsville, NC. Fax: C-13.6--3424.522 .:2-732Q Email: wtclab bellsouth.not:.. .::. Web.Site: .www.meritech-labscons Turn Around'Time* :;34t 90 days), 1 -6 Day, 24;-4$ Hr Sample p LocationllU ;.Sampling Dates &Times: p g r440, Person Taking Sample.(Signaiure):.14 Lab use:only :;9_TART TEND 4omp? Grab? #:of Cents. Tests, Re dined Cl - On -160 pH;.OK? -C12OK?. .. Date Time' Date `Time Farm On. �: per, .2<.sz 2 �' S Grab 'Cadmium, :copper, Lea(O; Nickel, Zinc, Altmmoriia=Nitrogen, Calcium, _Magnesium, Nitrate-Nitrite-Mtrogen, pH, Phosphorus, ..... .. _ .. °I T ids, -Plant Available Nitrogen- o. otahSol (by calculation) Potassium;;Sodiumi ..... TKN, Aluminum Method: of Shipment: Comments:.. -' Express. results'.as,mgft (Dryweight basis) Q UPS Q Ped' Ex. [] Hand: Delivery. QO.ther . Will these.results be used for,rggulatory purposes? Yes Yes Na *RUS H work"must he approved prior to-Lsubmiftingsamp►es. . Relinquis b,� Date: Time:+ tA� `: �r\ R' ed Date,: Time f'' .: �'' K Relinquished by:: Date: lime:- Neeived'by: 'Date: Time: Relinquishedby Date: T(me:: ved., a b . Date•, I Contact-: Matthew Toms Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Merftech, Inc. Environmental Laboratory Laboratory Certification No.165 Report Date: 8/25/2014 NPDES #: NCO029980 Date Sample Rcvd: 8/2/2014 Meritech Work Order # 08021403 Sample: farm On Grab 8/1/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 11.8 % 8/4/14 0-100 % SM 2540B Ammonia, Nitrogen 6,640 mg/kg 8/4/14 10 mg/kg EPA 350.1 'TKN 44,900 mg/kg 8/20/14 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen < 84.7 mg/kg 8/6/14 84.7 mg/kg EPA 353.2 'Aluminum, total 1,960 mg/kg 8/18/14 5.00 mg/kg EPA 200.7 Cadmium, total < 0.847 mg/kg 8/18/14 0.847 ing/kg EPA 200.7 Calcium, total 36,900 mg/kg 8/18/14 10.0 ing/kg EPA 200.7 Copper, total 38.1 mg/kg 8118/14 10.0 ing/kg EPA 200.7 Lead, total 7.64 mg/kg 8/18/14 2.0 mg/kg EPA 200.7 Magnesium, total 2,530 mg/kg 8/18/14 10.0 mg/kg EPA 200.7 Nickel, total 8.12 ing/kg 8/18/14 2.0 mg/kg EPA 200.7 Phosphorous, total 9,580 mg/kg 8/18/14 2.00 mg/kg EPA 200.7 Potassium, total 3,030 mg/kg 8/18/14 20.0 mg/kg EPA 200.7 Sodium, total 4,490 mg/kg 8/18/14 20.0 mg/kg EPA 200.7 Zinc, total 231 mg/kg 8/18/14 10.0 111g/kg EPA 200.7 pH 7.5 S.U. 8/4/14 1.0-14.0 S.U. SM 4500-H B I hereby certify that I have reviewed and approve these data. 6 , gx Laborato►y Representative 642 Tanrco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record CiOCi Client: MillerCoors Address: 863 E. Meadow Road Eden, NC 27288 Attention: or"Aw reyrr NPDES#: NCO029980 Phone: 336-627-2592 Fax: ' Email: nunn.hassan mil{ercoors.com Project PO#: E TECi INC. Environmental Laboratories A Division of water Technology and Control, Inc. 642 Tamco Rd Phone 9-336-342-4748 Reidsville, NC Fax: 1-336-342-1622 27320 Email: ' wtclab(&belisouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) r__= 3 - 5 Day 0 24 -48 Hr 0 Sample Location/1D # Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END Comp? Grab? #of Conts. Tests Required q On lee? pH OK? C12OK? Date Time Date Time Farm On Grab _ _-V Cadmium, Copper, Lead, Nickel, Zinc, Ammonia -Nitrogen, Calcium, Magnesium, Nitrate -Nitrites Nitrogen, pH, Phosphorus, { % Total Solids, Plant Available Nitrogen l (by calculation) Potassium, Sodium, TKN, Aluminum Method of Shipment: Comments: Express results as mglkg (Dry we"aght basis) ED UPS Fed Ex Q Hand Delivery Wiii these results be used for regulatory purposes? Yes Yes No *RUSH work must be approved prior to submiffing samples. Relinquished by: Date: Time: 2� f '� Receiv by Date: Time: �..<-� �Z`� Red Date: B / Time: 3i�s Received by: Date: oTme: Relinquished by: Date: Time: . Received at lab by: Date: Time: Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Matthew Toms Client: MillerCoors 863 East Meadow Road Eden, NC 27288 Report Date: NPDES #: Date Sample Rcvd; 10/24/2014 NCO029980 10/3/2014 Meritech Work Order # 10031416 Sample: Farm On Grab 10/2/14 Parameters Result Analysis Date Reporting Limit Method % Total Solids 14.4 % 10/16/14 0-100 % SM 2540B Ammonia, Nitrogen 1,120 mg/kg 10/21/14 10 mg/kg EPA 350.1 TKN _ 19,500 mg/kg 10/20/14 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen < 69.4 mg/kg 10/16/14 69.4 mg/kg EPA 353.2 Aluminum, total 840 mg/kg 10/13/14 5.00 mg/kg EPA 200.7 Cadmium, total < 0.694 mg/kg 10/13/14 0.694 mg/kg EPA 200.7 Calcium, total 40,100 mg/kg 10/13/14 10.0 mg/kg EPA 200.7 Copper., total 26.1 mg/kg 10/13/14 10.0 mg/kg EPA 200.7 Lead, total 7.15 mg/kg 10/13/14 2.0 mg/kg EPA 200.7 Magnesium, total 23,100 mg/kg 10/13/14 10.0 mg/kg EPA 200.7 Nickel, total 4.45 mg/kg 10/13/14 2.0 mg/kg EPA 200.7 Phosphorous, total 9,100 mg/kg 10/13/14 2.00 mg/kg EPA 200.7 Potassium, total 31,900 mg/kg 10/13/14 20.0 mg/kg EPA 200.7 Sodium, total 3,970 mg/kg 10/13/14 20.0 mg/kg EPA 200.7 Zinc, total 207 mg/kg 10/13/14 10.0 mg/kg EPA 200.7 pH 7.4 S.U. 10/13/14 1.0-14.0 S.U. SM 4500-H B I hereby certify that I have reviewed and approve these data. ��✓Cz Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record (COC) Client: MillerCoors Address: 863 E. Meadow Road Eden; 4C 27288: Attention: NPDES#:, NCO029980 Phone: 336-627-2692 Fax: Email: nunn.hassan(a)millercoors.com Project:, PO M MERETECH INCO Environmental Laboratories A.Division: of Water Technology and Control, Inc. .MW 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtdlabObellsouth.net Web Site: www.meritech-labs.com- Turn Around Time* :Std (10 da ys) 3 - 5 Day 24 - 48 Hr Sample 4ocatioh1lD# Sampling Dates & Times Person Taking Sample (Signature): Lab Useonly START END Camp?, Grab? #'Of Conts. Tests. Required On pH OK? C12 OK? Date Time -Date Time Farm On 5�,11910PV Grab _,r, v - Cadmiz, Copli4r,.Le Nickel, Zinc, Ammonia-NitrqAen, Ca'lc),um Magn, sium... Nitrate-Nitride-Nfirogen, pH� i PhospGrus, % Total Solids, Plant Available Nitrogen (by calculation) Pota 50um Sodium, TW, Alumind� Method :of Shipment: Comments: Express results as mglkg (Dry weight'basis), Oups F-1 Fed Ex ❑ Hand Delivery FlOther Will these'results be used.for purposes? regulatorY Yes yes No 1 *RUSH work must be approved prior to submitting samples. Relinquished by: Date: Time: 1 1, I L M --= C) z✓/ -t I 0 0 Received b Date: Ti--e: '/ Clg //0 0 RellhquNDate, Time: o 7-1 i 11,Y5 Received by: Date: Time: Relinquished by: Date: Time: la by: D Time: I Meritech, Inc. Environmental Laboratory. Laboratory Certification No.165 Contact: Matthew Toms Report Date: 12/12/2014 Client: MillerCoors NPDES #: NCO029980 863 East Meadow Road Eden, NC 27288 Date Sample Rcvd: 12/1/2014 Meritech Work Order # 12011402 Sample: Farm On Grab 12/1/14 Parametp, Result Analysis Date Reporting LimitMethod % Total Solids 14.2 % 12/2/14 0-100 % SM 2540B Ammonia, Nitrogen 3,820 mg/kg 12/9/14 10 mg/kg EPA 350.1 TKN 37,500 mg/kg 12/10/14 20 mg/kg EPA 351.1 Nitrate/Nitrite, Nitrogen < 70.4 mg/kg 12/3/14 70.4 mg/kg EPA 353.2 Aluminum, total 496 mg/kg 12/4/14 5.00 mg/kg EPA 200.7 . Cadmium, total < 0.704. mg/kg 12/4/14 0.704 mg/kg EPA 200.7 Calcium, total 8,100 mg/kg 12/4/14 10.0 mg/kg EPA 200.7 Copper, total 32.5 mg/kg 12/4/14 10.0 mg/kg EPA 200.7 Lead, total 3.63 mg/kg 12/4/14 2.0 mg/kg EPA 200.7 Magnesium, total 2,840 mg/kg 12/4/14 10.0 mg/kg 'EPA 200.7 Nickel, total 5.43 mg/kg 12/4/14 2.0 rng/kg EPA 200.7 Phosphorous, total 10,600 mg/kg 12/4/14 2.00 mg/kg EPA 200.7 Potassium, total 4,310 mg/kg 12/4/14 20.0 mg/kg EPA 200.7 Sodium, total 5,620 mg/kg 12/4/14 20.0 mg/kg EPA 200.7 Zinc, total 202 mg/kg 12/4/14 10.0 mg/kg EPA 200.7 pH 7.5 S.U. 12/2/14 1.0-14.0 S.U. SM 4500-H B . I herebycertify that 1 have reviewed and approve these data. / fY Pp Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(910)342-4748 fax.(910)342-1522 Chain of Custody Record COC Client: MillerCoors Address: 863 E. Meadow Road Eden NC 27288 �/-7/ -S' Attention: NPDEs#: NCO029980 Phone: 336-627-2592 Fax: Email: nunn.hassan millercoors.com Project Po #: MERI'TECH INC. Environmental Laboratories A Division of Water Tecbaology and Control, Inc. 642 Tamco Rd Phone 1-336-342-4748 Reidsville, NC Fax: 1-336-342-1522 27320 Email: wtclab ftellsouth.net Web Site: www.meritech-labs.com Turn Around Time* Std (10 days) 3 - 5 Day E I 24 -48 Hr Sample Location/ID# Sampling Dates & Times Person Taking Sample (Signature): Lab Use Only START END comp? Grab? #of Conts. Tests Required On Ice?` pH OK? C120K? Date Time Date Time Farm On "7"Oa��" Pam- -7%%04o' Grab -0 Cadmium, Copper, Lead, Nickel, Zinc, Ammonia -Nitrogen, Calcium, Magnesium, Nitrate -Nitrite -Nitrogen, pH, Phosphorus, % Total Solids, Plant Available Nitrogen (by calculation) Potassium, Sodium, TKN, Aluminum Method of Shipment: Comments: n Express results as mglkg (Dry weight basis) Q �5i k spccr`,----------- UPS D Fed Ex Hand Delivery Qother Will these results be used for regulatory purposes? Yes JYes No *RUSH work must be approved prior to submitfing samples. As Relinquished by:, � �o�� �. Y�! , ifine: o � -141 ti t Received b i Date: Time: � � 7 Relinquished by: Date: Time: Received by: ate: lime: !Rnfinujulshed p Date: Time: Rev wed a b b . .� q'te/ j. Ti l/ 0.1 e�, R.. r