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HomeMy WebLinkAboutWQ0010528_Residual Annual Report 2018_20190218It ANNUAL SLUDGE DISPOSAL REPORT :QI�WR L0 nac9e � cc.Ri��tti'�9 Vnt SUMMARY OF THE LAND APPLICATION PROGRAM FOR THE TOWN OF RAMSEUR RFC`t=i1�F� FEB 1 8 2019 prepared by DWR SECTION INFORMATION PROCESSING UNIT SUEZ Clemmons, North Carolina (336) 766-0270 CLASS WQ PERMIT #: NNUAL DISTRIBUTION AND MARKETING/ SUK., ,%ZE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ0010528 PHONE: 336-824-3939 FACILITY TYPE (please check one): FACILITY NAME: COUNTY: Randolph OPERATOR: Town of Ramseur Town of Ramseur i l Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) J Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes !d No J —► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February March WWTP - NCO026565 0.03 0.05 0.08 April May WTP 27.55 27.55 June July August September October November December Total from FORM DMSDF (sup) Totals: Annual (dry tons): 0.03 27.6 1 27.63 0 Amendment(s) used: Lime Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) Part C: Facility was compliant during the past calendar year with all conditions of the land application permit 0 Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: IJ No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Per ittee Date Signature df Preparer** (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM DMSDF (12/2006) ANNUAL RESIDUAL Si-xiviPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data WQ0010528 Town of Ramseur �CKIZI . •1.�T.� Ramseur WWTP Laboratory: 1) Environment 1 2) SGS Accutest 3) 4) 5) Parameter • I- - ,' 1 ------- Molybdenum Total Phosphorus ' For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." r Signature of Pr9lparer 1-T ( -11 Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) 0 OAKMONT DRIVE EENVILLE, N.C. 27858 SUEZ WATER (RAMSEUR WWTP-SLUDGE) NADINE BLACKWELL P.O. BOX 1279 CLEMMONS ,NC 27012 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH, Units 6.9 12/07/18 HMM 4500HB-11 Arsenic (dry wt. basis), mg/kg <2.5 12/19/18 MTM 311313-04 Chromium, T.(dry wt. basis),mg/kg 58 12/12/18 LFJ EPA200.7 Nickel (dry wt. basis), mg/kg 8 12/12/18 LFJ EPA200.7 Total Solids, % 0.38 12/05/18 KDS 2540G-11 Wastewater IV: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 965 DATE COLLECTED: 12/04/18 DATE REPORTED : 12/26/18 REVIEWED BY: Environment 1, Inc. CHAIN OF C i T`'TODY RECORD P.O. Box 7( 14 Oakmont Dr. Page 1 Greenville, 7858 environment 1 inc.com DISINFECTION Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE NEUTRALIZED AT COLLECTION Fi CHLORINE pH CHECK (LAB) CLIENT:965 Week: 7 Fi UV p p p p p p G G G G G I I CONTAINER TYPE, P/G UEZ WATER (RAMSEUR WWTP-SLUDGE) ❑ NONE fADINE BLACKWELL .O. BOX 1279 CHEMICAL PRESERVATION 'LEMMONS NC 27012 A A A A A A A A A A A E o A -NONE D-NAOH 536)766-0270 z J L zo z a o e R :R w C B-HNO E-HCL o of c_ = H Uj Z v) a LU C - H zSO F -ZINC ACETATE/NAOH w COLLECTION J¢ < 0o¢ o O x :° � o ro o a U Q" a U a U a U a U G- NATHIOSULFATE as SAMPLE LOCATION DATE TIM a. s G4 .. U E� E� Sl udge Sample 09Q8 .... ..: Ir G CLASSIFICATION: WASTEWATER (NPDES) DRINKING WATER DWQ/GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY N SAMPI FS'Cl7TECTED BY: (Please Print) 1 SAMPLES 4CEIVED IN LAB AT�°C RE INQUI ED BY (SIG.) (SAMPLER) II)ATUTIME RECEIVED B G.) I A`T,ETIME , COMMENTS: ( �� Nz� e c-vr D I1 J RELINQUISHED BY (SIG.) DATE/TIME RECEIVED BY (SIG. DATE/TIME RELINQUISHED BY (SIG.) DATE/TIME I RECEIVED BY (SIG.) DATE/TIME I I i PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for FORM #s Grab sample in the blocks above for each parameter requested. N 2 3 4 2 A 01 SGS Orlando, FL The results set forth herein are provided by SGS North America Inc. eHardcopy 2.0 Automated Report Technical Report for Environment 1, Inc Suez Water, Ramseur WWTP; Clemmons, NC 965 SGS Job Number: FA60021 Sampling Date: 12/04/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentIinc.com ATTN: Deedee Woolard Total number of pages in report: 14 Test results contained within this data package meet the requirements Caitlin Brice, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about �� Unauthorized modification of this report is strictly prohibited. how we can serve you better at: Review standard terms at: http://wwtiv.sgs.cotii/en/terms-and-conditions EHS.US.CustomerCare Casgs.com 1 of 14 FA60021 Table of Contents -1- Section1: Sample Summary................................................................................................... Section2: Summary of Hits.................................................................................................... Section3: Sample Results........................................................................................................ 3.1: FA60021-1: SLUDGE SAMPLE.................................................................................. Section4: Misc. Forms............................................................................................................ 4.1: Chain of Custody........................................................................................................... Sections: 3 4 5 6 12 13 2of14 FA60021 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA60021 Suez Water, Ramseur WWTP; Clemmons, NC Project No: 965 Sample ; Collecfed- ': - _ Matrix Client Number Date Time By Received Code Type Sample ID FA60021=1- ; 12/04/18 09:50 TL 12/08/18 SO Sludge SLi1DGE;SEIMPLE ; Soil samples reported on a dry weight basis unless otherwise indicated on result page. 3of14 ��� FA60021 Summary of Hits Job Number: FA60021 Account: Environment 1, Inc Project: Suez Water, Ramseur WWTP; Clemmons, NC Collected: 12/04/18 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA60021-1 SLUDGE SAMPLE Corrosivity as pH su Ignitability (Flashpoint) a ">200:`';W Deg. F (a) Not ignitable. Page 1 of 1 , SW846 CHAP7 SW846 1010A MOD 4 at 14 FA60021 I- I -9•} x Orlando, FL *"' Sample Results'' Report of Analysis Section 3 rA 5of14 FA60021 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60021-1 Date Sampled: 12/04/18 Matrix: SO - Sludge Date Received: 12/08/18 Method: SW846 8260B SW846 1311 Percent Solids: 0.5 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 C0129136.1) 10 12/13/18 02:26 SO 12/11/18 14:45 OP72982 VC5125 Run #2 Purge Volume Run #1 5.0 ml Run #2 VOA TCLP List CAS No. Compound Result HW# MCL RL 71-43-2 Benzene ND D018 0.50 0.010 78-93-3 2-Butanone (MEK) ND D035 200 0.050 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 108-90-7 Chlorobenzene ND D021 100 0.010 67-66-3 Chloroform ND D022 6.0 0.010 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.010 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 75-35-4 1,1-Dichloroethylene ND D029 0.70 0.010 127-18-4 Tetrachloroethylene ND D039 0.70 0.010 79-01-6 Trichloroethylene ND D040 0.50 0.010 75-01-4 Vinyl Chloride ND D043 0.20 0.010 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 100% 83-118% 17060-07-0 1,2-Dichloroethane-D4 101% 79-125% 2037-26-5 Toluene-D8 97% 85-112% 460-00-4 4-Bromofluorobenzene 98% 83-118% TCLP Leachate method SW846 1311 MDL Units Q 0.0031 mg/1 0.020 mg/1 0.0036 mg/1 0.0020 mg/1 0.0030 mg/1 0.0026 mg/1 0.0031 mg/1 0.0032 mg/1 0.0022 mg/1 0.0035 mg/1 0.0041 mg/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound _SGS_ 6of14 FA60021 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60021-1 Date Sampled: 12/04/18 Matrix: SO - Sludge Date Received: 12/08/18 Method: SW846 8270D SW846 3510C Percent Solids: 0.5 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 -7 M File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X064217.1) 1 12/13/18 21:19 MV 12/13/18 08:45 OP73016 SX2650 Run #2 Initial Volume Final Volume Run #1 100 ml 1.0 ml Run #2 ABN TCLP List CAS No. Compound Result HW# MCL RL 95-48-7 2-Methylphenol ND D023 200 0.050 3&4-Methylphenol ND D024 200 0.050 87-86-5 Pentachlorophenol ND D037 100 0.25 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.050 88-06-2 2,4,6-Trichlorophenol ND D042 2.0 0.050 106-46-7 1,4-Dichlorobenzene ND D027 7.5 0.050 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.050 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 67-72-1 Hexachloroethane ND D034 3.0 0.050 98-95-3 Nitrobenzene ND D036 2.0 0.050 110-86-1 Pyridine ND D038 5.0 0.10 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 37% 14-67% 4165-62-2 Phenol-d5 25% 10-50% 118-79-6 2,4,6-Tribromophenol 81% 33-118% 4165-60-0 Nitrobenzene-d5 68% 42-108% 321-60-8 2-Fluorobiphenyl 69% 40-106% 1718-51-0 Terphenyl-dl4 77% 39-121% TCLP Leachate method SW846 1311 MDL Units Q 0.0056 mg/l 0.0098 mg/1 0.050 mg/1 0.0074 mg/1 0.0075 mg/1 0.0050 mg/I 0.0081 mg/1 0.0069 mg/1 0.0050 mg/I 0.016 mg/1 0.0093 mg/1 0.020 mg/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound -SGS1 7 of 14 FA60021 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60021-1 Date Sampled: 12/04/18 Matrix: SO - Sludge Date Received: 12/08/18 Method: SW846 8151A SW846 3510C Percent Solids: 0.5 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1wa File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC060463.1) 1 12/14/18 16:50 RS 12/13/18 13:40 OP73025 GCC1386 Run #2 Initial Volume Final Volume Run #1 10.0 ml 5.0 ml Run #2 Herbicide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 94-75-7 2,4-D :AND,;;; D016 10 0.050 0.017 mg/1 93-72-1 2,4,5-TP (Silvex) ND :; _ `, D017 1.0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA ;;;1l04%'s:;:y^' 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8of14 FA60021 SGS North America Inc. Client Sample ID: SLUDGE SAMPLE Report of Analysis Lab Sample ID: FA60021-1 Date Sampled: 12/04/18 Matrix: SO - Sludge Date Received: 12/08/18 Method: SW846 8081B SW846 3510C Percent Solids: 0.5 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 KK92415.D 1 12/13/18 18:16 WH 12/13/18 08:30 OP73018 GKK2939 Run #2 Initial Volume Final Volume Run # 1 100 ml 5.0 ml Run #2 Pesticide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) a ND D013 0.40 0.00010 0.000022 mg/I 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin ND D012 0.020 0.00020 0.000021 mg/1 76-44-8 Heptachlor ND D031 0.0080 0.00010 0.000026 mg/1 1024-57-3 Heptachlor epoxide a ND D031 0.0080 0.00010 0.000020 mg/1 72-43-5 Methoxychlor ND D014 10 0.00020 0.000050 mg/I 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 101% 42-127% 2051-24-3 Decachlorobiphenyl 122% 27-127% (a) Associated ICV outside control limits high, however sample ND. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound CGS9of14 FA60021 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60021-1 Date Sampled: 12/04/18 Matrix: SO - Sludge Date Received: 12/08/18 Percent Solids: 0.5 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/1 1 12/11/18 12/12/18 LM SW846 6010C 2 SW846 3010A 4 Barium < 2.0 D005 100 2.0 mg/1 1 12/11/18 12/12/18 LM SW846 6010C 2 SW846 3010A 4 Cadmium < 0.050 D006 1.0 0.050 mg/1 1 12/11/18 12/12/18 LM SW846 6010C 2 SW846 3010A 4 Chromium < 0.10 D007 5.0 0.10 mg/1 1 12/11/18 12/12/18 LM SW846 6010C 2 SW846 3010A 4 Lead < 0.050 D008 5.0 0.050 mg/1 1 12/11/18 12/12/18 LM SW846 6010C 2 SW846 3010A 4 Mercury < 0.0050 D009 0.20 0.0050 mg/I 1 12/11/18 12/11/18 JC SW846 7470A 1 SW846 7470A 3 Selenium < 0.10 D010 1.0 0.10 mg/1 1 12/11/18 12/12/18 LM SW846 6010C 2 SW846 3010A 4 Silver < 0.10 D011 5.0 0.10 mg/1 1 12/11/18 12/12/18 LM SW846 6010C 2 SW846 3010A 4 (1) Instrument QC Batch: MA15458 (2) Instrument QC Batch: MA15465 (3) Prep QC Batch: MP34790 (4) Prep QC Batch: MP34791 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) SGS_ 10 of 14 FA60021 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA60021-1 Date Sampled: 12/04/18 Matrix: SO - Sludge Date Received: 12/08/18 Percent Solids: 0.5 Project: Suez Water, Ramseur WWTP; Clemmons, NC General Chemistry Analyte Corrosivity as pH Cyanide Reactivity Ignitability (Flashpoint) a Solids, Percent Sulfide Reactivity (a) Not ignitable. RL = Reporting Limit Result RL Units DF Analyzed By Method su 1 12/17/18 12:51 BW SW846 CHAP7 z_280"; '-': : ` 280 mg/kg 1 12/14/18 14:00 JK SW846 CHAP7 >,200Y '." ". Deg. F 1 12/11/18 10:23 BW SW846 1010A MOD % 1 12/13/18 11:55 AC SM19 254OG 9300 mg/kg 1 12/14/18 15:30 LR SW846 CHAP7 S11 of 14 FA60021 SGS,--- Orlan Misc. FormsTW Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 SGS12 of 14 FA60021 P.OBox°7085, 114 Oakmont Dr. ��lAl1 � V 1 � � y "L�vl`V VL1 • 6mZ01 Page 1 of 1 Greenville, NC 27858 1 ' DISINFECTION CHLORINE NEUTRALIZEDATCOLLECiON environmentlinc.com Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE pHCHECK (LAB) LIENT;965 Week:7 uv P P P P P P G G G G G CONTAINER TYPE,P/G IUEZ WATER M"SEUR WWTPSLUDGE) NONE IADINE BLACKWELL -.O. BOX 1279 ❑ CHEMICAL PRESERVATION 'LEMMONS NC 27012 A A A A I A A A A A A A �o A -NONE D-NAOH 336) 766-0270 0 0 22 ° pp B-HP10, E-HCL C-H,SO, F- ZINC ACETATEINAOH LLECTION ¢ o� a a a 8 �5 j j F Aj Q a VF a F ¢� G-NATHIOSULFATE SAMPLE LOCATION EDATE TIME r Cam CLASSIFlCATION: WASTEWATER(NPDES) DRINKINGWATER DWO/GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY N SAMPLES CTED BY (Please PrinQ 7Rvnq L'(cr SAMPLES 4CEIVEDINLAB ATQZ_°C RE INOIJI BY (SI AMP R) AT IM I I RECEIVED G.) I A`TEIIME COMMENTS: r, , RELINOUISHEDBY( G. ATEITIME RECEIVED BY (SIG. DATE/DME Cu W I Z?/1 /�' .r. c,., ,}1>t,l, �' c4e,v I��i II6 Il 3` NOUISHED BY (SIG.) DATE/RME RECEIVED BY (SIG.) ; tiE 17ATE/DME- kI9I1� I 9) 111ld'i61w0 PLEASE READ Instructions for completing this form on the reverse side. �v'Q zGrab sample in the blocks ampler must place ck for composite sample or a "G" for f�aM a.5 � ° � s above for each naramnter rnnuasrad. No q A ,) d n i FA60021: Chain of Custody Page 1 of 2 13 of 14 SG _ FA60021 SGS Sample Receipt Summary Job Number: FA60021 Client: ENV. 1 Project: 965 Date / Time Received: 12/8/2018 10:00:00 AM Delivery Method: FX Airbill Ws: 1001693371060003281100461155066267 Therm ID: IR 1; Therm CF: -0.2; # of Coolers: 1 Cooler Temps (Raw Measured) eC: Cooler 1: (2.0); Cooler Temps (Corrected) eC: Cooler 1: (1.8); Cooler Information Y or N Sample Information Y or N N/A 1. Custody Seals Present ® ❑ 1. Sample labels present on bottles ® ❑ 2. Custody Seals Intact ® ❑ 2. Samples preserved property ® ❑ 3. Temp criteria achieved ® ❑ 3. Sufficient vokrme/containers recvd for analysis: ® ❑ 4. Cooler temp verification IR Gun 4. Condition of sample law 5. Cooler media Ice (Bao) 5. Sample recvd within HT ® ❑ 6. Datesfrimea/lDs on CDC match Sample Label ® ❑ Trio Blank Information Y or N NIA VOCs have headspace ❑ ❑ 1. Trip Blank present / cooler ❑ ❑ ® 8. Bottles received for unspecified teats ❑ 2. Trip Blank listed on CDC ❑ ❑ ® 9. Compositlnp Instructions dear ❑ ❑ W or S N/A 10. Voa Soil Kits/Jars received past 48hrs? ❑ ❑ 11. % Solids Jar received? ❑ ❑ Ea 3. Type Of TB Received ❑ ❑ ® 12. Residual Chlorine Present? ❑ ❑ Misc. Information Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Test Strip Lot #a: pH 0-3 230315 pH 10-12 219813A Other. (Specify) Residual Chlorine Test Strip Lot #: Comments SNGRw. Mla 052N77 Technician: PETERH Date: 12/6/2018 10:00:00 A Reviewer. Date: Rev. FA60021: Chain of Custody Page 2 of 2 14 of 14 �— FA60021 ANNUAL RESIDUAL Si 'LING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0010528 Laboratory: Facility Name: Town of Ramseur Residual Source WQ # or NPDES #: NCG590019 WWTP Name: Ramseur Water Treatment Plant Residual Analysis Data 1) Environment 1 2) SGS Accutest 3) 4) 5) Parameter - - Conc.• Limit or • .• Date 1 ---------- Molybdenum e For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature 6f Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) SUEZ WATER (RAMSEUR WTP-SLUDGE) NADINE BLACKWELL P.O. BOX 1279 CLEMMONS ,NC 27012 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH, Units 3.4 05/25/18 HMM 4500HB-11 Arsenic (dry wt. basis), mg/kg <2.5 05/30/18 MTM 311313-04 Chromium, T.(dry wt. basis),mg/kg 8 06/04/18 LFJ EPA200.7 Nickel (dry wt. basis), mg/kg 26 06/04/18 LFJ EPA200.7 Total Solids, % 6.44 05/23/18 JMT 2540G-11 ID#: 950 DATE COLLECTED: 05/22/18 DATE REPORTED : 06/15/18 REVIEWED BY: Environment 1. Inc. CHAIN OF C7 T"TODY RECORD P.O. Box,70: 4 Oakmont Dr. Greenville,) 858 Page 1 environment 1 inc .com DISINFECTION Phone (252) 756-6208 • Fax (252) 756-0633 CHLORINE NEUTRALIZED AT COLLECTION Ij CHLORINE pH CHECK (LAB) CLIENT:950 Week: 7 UV p p p IP p p G G G G G I I CONTAINER TYPE, P/G UEZ WATER (RAMSEUR WTP-SLUDGE) ❑ NONE TADINE BLACKWELL '.O. BOX 1279 FA CHEMICAL PRESERVATION 'LEMMONS NC 27012 A A A A A A A A A A A m o ECl) C/) A -NONE D-NAOH 336) 766-0270 _j ur0 z w .d ? Uj t B - HNO3 E - HCL _ cc w cn y 4. ��, W w C - H,SO4 F -ZINC ACETATE/NAOH COL_ECTION J a Q o w � o a o U_ x °' ° °�' [ c a U a U a U a U a U < G NATHIOSULFATE Q SAMPLE LOCATION DATE TIME Sludge Sample' _r lOa 8 ,; CLASSIFICATION: FA WASTEWATER(NPDES) Ij DRINKING WATER DWO/GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY cD N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB AT °C RELI O ISHED BY SIG.) DATE/TIME VED BY SIG.) DATE/TIME COMMENTS: Aw .S _Z2-, P �3o Z� �� —t S —2 -2-, P I /2 o o INOUISHED BY (SIG.) DATE TIME RECEIV D Y (SIG.) DATE/TIME f sir iy RELINO ISHED BY (SIG.) DATE/TIME RECEIVED BY (SIG.) DATE/TIME Sampler must place a "C" for composite sample or a "G" for PLEASE READ Instructions for completing this form on the reverse side. FORM us Grab sample in the blocks above for each parameter requested. N _0 3 4 2 ,4 1 % Orlando, FL The results set forth herein are provided by SGS North America Inc. eHardcopy 2.0 Automated Report Technical Report for Environment 1, Inc Suez Water, Ramseur WWTP; Clemmons, NC 965 SGS Job Number: FA54556 Sampling Date: 05/22/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environment 1 inc. corn TTN: Deedee Woolard Total number of pages in report: 15 e Test results contained within this data package meet the requirements Caitlin Brice, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about � Unauthorized mG modification of this report is stricth, prohibited. how we can serve you better at: Review standard terms at: http://wxvN%.sgs.coni-en/terms-and-conditions EHS.US.Customert:are t7sgs.com i of 15 FA54556 Sections: Table of Contents -1- Section1: Sample Summary................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 4 Section3: Sample Results........................................................................................................ 5 It: FA54556-1: SLUDGE SAMPLE.................................................................................. 6 3.2: FA54556-IA: SLUDGE SAMPLE............................................................................... 7 3.3: FA54556-IL: SLUDGE SAMPLE............................................................................... 8 Section4: Misc. Forms............................................................................................................ 13 4.1: Chain of Custody........................................................................................................... 14 2of15 _ SGS. _ FA54556 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA54556 Suez Water, Ramseur WWTP; Clem coons, NC Project No: 965 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA54556-1 05/22/18 10:20 MJ 05/29/18 SO Sludge SLUDGE SAMPLE FA54556-IA 05/22/18 10:20 MJ 05/29/18 AQ Water SLUDGE SAMPLE FA54556-IL 05/22/18 10:20 MJ 05/29/18 SO Sludge SLUDGE SAMPLE Soil samples reported on a dry weight basis unless otherwise indicated on result page. 1� 3of15 __SGS FA54556 Summary of Hits Job Number: FA54556 Account: Environment 1, Inc Project: Suez Water, Ramseur WWTP; Clemmons, NC Collected: 05/22/18 Page 1 of 1 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA54556-1 SLUDGE SAMPLE Ignitability (Flashpoint) a > 200 FA54556-IA SLUDGE SAMPLE Corrosivity as pH 6.8 FA54556-IL SLUDGE SAMPLE No hits reported in this sample. (a) Not ignitable. Deg. F SW846 1010 su SW846 CHAP? 4of15 SGS' FA54556 CGS Orla Sample Results Report of Analysis Section 3 cc 5of15 FA54556 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA54556-1 Date Sampled: 05/22/18 Matrix: SO - Sludge Date Received: 05/29/18 Percent Solids: 6.8 Project: Suez Water, Ramseur WWTP; Clemmons, NC General Chemistry Analyte Result Cyanide Reactivity a < 21 Ignitability (Flashpoint) b > 200 Solids, Percent 6.8 Sulfide Reactivity a < 710 (a) Sample analyzed beyond hold time. (b) Not ignitable. RL = Reporting Limit Page 1 of 1 RL Units DF Analyzed By Method 21 mg/kg 1 06/09/18 12:19 KH SW846 CHAP? Deg. F 1 06/14/18 13:49 BW SW846 1010 % 1 06/07/18 13:51 JC SM19 2540G 710 mg/kg 1 06/09/18 14:15 BW SW846 CHAP7 SGS_ 6of15 FA54556 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA54556-1A Date Sampled: 05/22/18 Matrix: AQ - Water Date Received: 05/29/18 Percent Solids: 6.8 Project: Suez Water, Ramseur WWTP; Clemmons, NC General Chemistry Analyte Result RL Units DF Corrosivity as pH 6.8. su 1 RL = Reporting Limit Page 1 of 1 Analyzed By Method 06/11/18 BR SW846 CHAP? 7 —SGot15_ FA54556 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA54556-IL Date Sampled: 05/22/18 Matrix: SO - Sludge Date Received: 05/29/18 Method: SW846 8260B SW846 1311 Percent Solids: 6.8 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 M0103337.1) 10 06/05/18 14:18 AB 06/04/18 12:45 OP70327 VM4454 Run #2 Purge Volume Run #1 5.0 ml Run #2 VOA TCLP List CAS No. Compound Result HW# MCL RL 71-43-2 Benzene ND D018 0.50 0.010 78-93-3 2-Butanone (MEK) ND D035 200 0.050 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 108-90-7 Chlorobenzene ND D021 100 0.010 67-66-3 Chloroform ND D022 6.0 0.010 106-46-7 IA-Dichlorobenzene ND D027 7.5 0.010 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 75-35-4 1,1-Dichloroethylene ND D029 0.70 0.010 127-18-4 Tetrachloroethylene ND D039 0.70 0.010 79-01-6 Trichloroethylene ND D040 0.50 0.010 75-01-4 Vinyl Chloride ND D043 0.20 0.010 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 102% 83-118% 17060-07-0 1,2-Dichloroethane-D4 103% 79-125% 2037-26-5 Toluene-D8 101% 85-112% 460-00-4 4-Bromofluorobenzene 94% 83-118% TCLP Leachate method SW846 1311 MDL Units Q 0.0031 mg/1 0.020 mg/1 0.0036 mg/I 0.0020 mg/1 0.0030 mg/1 0.0026 mg/1 0.0031 mg/I 0.0032 mg/i 0.0022 mg/1 0.0035 mg/I 0.0041 mg/I ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound _SGS 8 of 15 FA54556 SGS North America Inc. Report of Analysis :lient Sample ID: SLUDGE SAMPLE ,ab Sample ID: FA54556-1L Date Sampled: 05/22/18 Ratrix: SO - Sludge Date Received: 05/29/18 Rthod: SW846 8270D SW846 3510C Percent Solids: 6.8 roject: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 61701197.1) 1 06/04/18 18:11 NJ 06/02/18 08:45 OP70324 S6F45 Run #2 Initial Volume Final Volume '.un #1 100 ml 1.0 ml '.un #2 ABN TCLP List CAS No. Compound 95-48-7 2-Methylphenol 3&4-Methylphenol 87-86-5 Pentachlorophenol 95-95-4 2,4,5-Trichlorophenol 88-06-2 2,4,6-Trichlorophenol 106-46-7 1,4-Dichlorobenzene 121-14-2 2,4-Dinitrotoluene 118-74-1 Hexachlorobenzene 87-68-3 Hexachlorobutadiene 67-72-1 Hexachloroethane 98-95-3 Nitrobenzene 110-86-1 Pyridine CAS No. Surrogate Recoveries 367-12-4 2-Fluorophenol 4165-62-2 Phenol-d5 118-79-6 2,4,6-Tribromophenol 4165-60-0 Nitrobenzene-d5 321-60-8 2-Fluorobiphenyl 1718-51-0 Terphenyl-d14 Result HW# MCL RL ND, . '-, . D023 200 0.050 D024 200 0.050 D037 100 0.25 D041 400 0.050 D042 2.0 0.050 D027 7.5 0.050 D030 0.13 0.050 ND-; `; ; , ' D032 0.13 0.050 D033 0.50 0.050 D034 3.0 0.050 2.0 0.050 :ND',': 4'r-`-:° D038 5.0 0.10 Run# 1 Run# 2 Limits '27% -.:,' . t" 14-67% ,16%' 10-50% 33-118% 42-108% 40-106% 39-121% TCLP Leachate method SW846 1311 MDL 0.0056 0.0098 0.050 0.0074 0.0075 0.0050 0.0081 0.0069 0.0050 0.016 0.0093 0.020 Units Q mg/l mg/1 mg/l mg/1 mg/1 mg/1 mg/I mg/1 mg/1 mg/1 mg/1 mg/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 9of15 FA54556 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA54556-11 Date Sampled: 05/22/18 Matrix: SO - Sludge Date Received: 05/29/18 Method: SW846 8151A SW846 3510C Percent Solids: 6.8 Project: Suez Water, Ramseur WWTP; Clemmons, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC058449.D 1 06/04/18 21:43 NJ 06/02/18 11:45 OP70326 GCC1299 Run #2 Initial Volume Final Volume Run #1 10.0 nil 5.0 ml Run #2 Herbicide TCLP Leachate CAS No. Compound 94-75-7 2,4-D 93-72-1 2,4,5-TP (Silvex) CAS No. Surrogate Recoveries 19719-28-9 2,4-DCAA TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q D016 10 0.050 0.017 mg/1 ND D017 1.0 0.0050 0.0013 mg/1 Run# 1 Run# 2 Limits 73% 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound —S-Gtflofl5 FA54556 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA54556-11 Date Sampled: 05/22/18 Matrix: SO - Sludge Date Received: 05/29/18 Method: SW846 8081B SW846 3510C Percent Solids: 6.8 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 KK89515.D 1 06/04/18 11:16 KL 06/02/18 10:30 OP70325 GKK2858 Run #2 Initial Volume Final Volume Run #1 100 ml 5.0 ml Run #2 Pesticide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result RW# MCL RL MDL Units Q 58-89-9 gamma-BHC (Lindane) ND D013 0.40 0.00010 0.000022 mg/I 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin ND D012 0.020 0.00020 0.000021 mg/1 76-44-8 Heptachlor ND D031 0.0080 0.00010 0.000026 mg/1 1024-57-3 Heptachlor epoxide ND D031 0.0080 0.00010 0.000020 mg/1 72-43-5 Methoxychlor ND D014 10 0.00020 0.000050 mg/I 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09-8 Tetrachloro-m-xylene 105% 42-127% 2051-24-3 Decachlorobiphenyl 76% 27-127% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound __SGS' 11 of 15 FA54556 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA54556-11 Date Sampled: 05/22/18 Matrix: SO - Sludge Date Received: 05/29/18 Percent Solids: 6.8 Project: Suez Water, Ramseur WWTP; Clemmons, NC Page 1 of 1 Metals Analysis, TCLP Leachate SW8461311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 010:. .' D004 5.0 0.10 mg/1 1 ' 06/07/18 06/07/18 LM SW846 6010D Z SW846 3010A 4 Barium <;2:0 D005 100 2.0 mg/1 1 06/07/18 06/07/18 LM SW846 6010D 2 SW846 3010A 4 Cadmium - 0,QmX,: ', D006 1.0. 0.050 mg/I 1 06/07/18 06/07/18 LM SW846 6010D Z SW846 3010A 4 Chromium a ;01'Q=. - D007 5.0 0.10 mg/1 1 06/07/18 06/07/18 LM SW846 6010D Z SW846 3010A 4 Lead ;< 0050s _;` D008 5.0 0.050 mg/1 1 06/07/18 06/07/18 LM SW846 6010D Z SW846 3010A 4 Mercury ' <'0' 0050: �:, D009 0.20 0'.0050 mg/1 1 06/04/18 06/04/18 Jc SW846 7470A 1 SW846 7470A 3 Selenium c;O`a'O'`;,, ` ; DO10 1.0 0.10 mg/1 1 06/07/18 06/07/18 LM SW846 6010D 2 SW846 3010A 4 ,��.. Silver:,. D011 5.0 0.10 mg/1 1 06/01/18 06/07/18 LM SW846 6010D Z SW846 3010A 4 (1) Instrument QC Batch: MA14944 (2) Instrument QC Batch: MA14956 (3) Prep QC Batch: MP33830 (4) Prep QC Batch: MP33852 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 711/11) 12of16 FA54556 SGS Orlar Section 4 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody SG� 13 of 15 a FA54656 P.O. Box 7085, 114 Oakmont Dr. Greenville, NC 27858 environment I inc.com Phone (252) 756-6208 • Fax (252) 756-0633 FECTION HLORINE FLI CLIENT950 Week. 7 . V I IUEZ WATER (RAMSEM WTP-SLUDGE) ❑ NONE °lAD1NE BLACHWELL Y.O. BOX 1279 CLEMMONS NC 27012 ❑ �z Eo (336) 766-0270 z COLLECTION a Weo8 4� U 6 � ul SAMPLELOCA110N DATE TIME o¢ as-ru 1W0 0 r BY(SIG.) DATERIME v PLEASE READ Instruct - FOR 125 ions for completin � 18 l0'30 r. CHAIN OF CUSTODY RECORDS44 5 `6 I�ro CLASSIFICATION: lm 12110 WASTEWATER(NPDES) DRINIONGWATER ❑ ❑ ❑ DWO/GW SOLIDWASTESECTION ❑, CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY C9 N SAMPLES COLLECTED BY.(Please Prim) CHLO, pHCHECI �O °tenet P P P P P P G G G G G OONTAINER', A A A A A A A A A A CHEMICALPflE� - � A -NONE D-NAOH e •a, a w 8-HNO, E-HCL C-HzSO, F-ZINCACETATEMAOH NATHIOSULFATE F a I on the reverse side. ezwAep SAMPLES RECEIVED INLA13AT V ' Y -C " ""� COMMENTS: 1300 0 DATEMME lie sq Sampler must place a "C" for composite sample or a "G" for Grab sample in the blocks above for each parameter requested. N2 342417 FA54556: Chain ®f Custody Page 1 ®f 2 rkf%ot1 14 of 15 _buk FA54556 SGS Sample Receipt Summary Job Number: FA54556 Client: ENV 1 INC Project: 950 Date / Time Received: 5/29/2018 9:00:00 AM Delivery Method: FX Airbill 99: 1001891783790003281100439402209589 Therm ID: IR 1; Therm CF: 0.4; # of Coolers: 1 Cooler Temps (Raw Measured)'C: Cooler 1: (20.4); Cooler Temps (Corrected) IC: Cooler 1: (20.8); Cooler Information Y or N Samole Information Y or N NIA 1. Custody Seals Present ® ❑ 1. Sample labels present on bottles ® ❑ 2. Custody Seals Intact ® ❑ 2. Samples preserved property ® ❑ 3. Temp criteria achieved ❑ ® 3. Sufficient volume/containers recvd for analysis: ® ❑ 4. Cooler temp verification IR Gun 4. Condition of sample IOtasd 5. Cooler media Ice (Bao) 5. Sample recvd within HT ® ❑ S. Dates/fimes/IDs on CDC match Sample Label ® ❑ Trio Blank Information Y or N N/A 7. VOCs have headspace ❑ ❑ 1. Trip Blank present / cooler ❑ ❑ ® S. Bottles received for unspecified tests ❑ 10 2. Trip Blank listed on CDC ❑ ❑ ® 9. Compositing instructions dear ❑ ❑ W or S N/A 10. Voa Soil Kits/Jars received past 48hrs? ❑ ❑ 11. % Solids Jar received? ❑ ❑ 12 3. Type Of TB Received ❑ ❑ ® 12. Residual Chlorine Present? ❑ ❑ Misc. information Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Test Strip Lot #s: pH 0-3 230315 pH 10-12 219813A Other. (Specty) Residual Chlorine Test Strip Lot #: Comments RECEIVED 5 BOTTLES CDC READS 5,TEMPERATURE CRITERIA NOT MET snout Ray. Date 05R//17 Technician: JORGEC Date: 529/2018 9:00:00 AM Reviewer. Date: FA54556: Chain of Custody Page 2 of 2 15 Of 15 FA54556 CHAIN OF CUSTODY Sample Location: (W a I Z f C Sample Collection Date: S -A P, - ) Sample Collection Time: t D• Z D n Person Collecting Sample Name/Signature M WlS C fOs ,, Parameter Analysis Time Result I Analyst Name Analyst Sig ature pH /a O 7 ►V-Osr Temperature Samples Sent to Laboratory for additional analyses? OYES NO Comments: Attach copy of commercial lalmratory Chain of Custody to this form ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Ramseur WWTP Name: Ramseur WWTP WQ Permit Number: NPDES Number: WQ0010528 NCO026565 Monitoring Period: From 1/1/2018 To 12/31/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment)❑ Alt. C (Prior Testing).. A1t.D (No Prior Test) J Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment L1 Therrnophilic Beta Ray ❑ Gamma Ray ❑ Pasteurization r] Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ' 1 If applicable to alternative performed (Class B only) indicate "Process to Significantly_ Reduce Pathogens": Lime Stabilization R) Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- n Frequency of Analysis Sample Type Analytical Tech - nia Minim Geo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) 'ector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) F1 Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization P-1 Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ; l Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed [.3 CERTIFICATION STATEMENT (please check the appropriate statement) C! "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." err �tw o•� lM ��. Preparer ame and Title (type or print) gnatu of Preparer* Land Applier Name and Title (if applicable)(type or print) 1-3/-tq Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Jan.24.2019 05:59 PM Ramseur WWTP 3368243939 PAGE. 4/ 13 a �t (_ LIMB LOS SHEET' Month 11 � o-V-(' � year z r8 DATE GAL. WAgYkb Initial TEMP ■C imit'1111 pN, SU 6.5 18S OF LIME o b Q TIME PH, 5U MP � 5 Temp Correctod PH, 5U p aftvr2M TEMP "C; wfter 2 ARS amp Mrocted p , , t .ass PH elFtar 94 HR9 ?j MP'C after 24 HRS Temp Corra ted ph, su H Correction Trim C Correction 4 P Ys 0.4 5 39 Pus 0,42 515 rlus 13.19 37 Plus 0,36 36 Plus 0,33 35 Plus 0.30 1210.0 0.27 Yri 0.2h 32 Plus 0.21 31 us . 3 u1, 8.15 29 t, 3, 7 Z Plus 0.09 28 27 Plus 0.05 26 �d25 .� Plus 0,03 U A-4 Minue 0.03 38 Minus 0106 22 Minus 0,09 3). Minus 0.1.2 _ ZG Mh1Y5 0,15 '" ip Minur+ o,ao 18 Minus 0.21 17 Minus 0.24 16 Minus 0.27 1S Minut; 0, 14 Inur0.33 13 Minus 0.36 32 Minus 0.39 11 Mlnut 0.42 10 Mlnua 0.45 "I certify, tinder peneity of low, that the Cis6s 9 pathogen requlrements in 4n (,rn, part sna,a7.th1 hmm hen 1nuL arid tale vector attraction raduetlon requirement in 40 CVIL part 503,33113)14) Raft (f,) 11eu11. I,cn111,,,ot. Tltly detvrminiMon hlit bias mad& unt lar My direatien and nupervixton In accarderic4 with thw bv&Lvm desig►red to eitsure. that aualified pomonnal propedy gather and 1evalwao. u,M IrI ftq�Iptlon vied to dearmina pt3r tho pothuren and vector attraction roductlan trqulre►mnts pawn lisom nut. I vie+ swore thn there era alAnlficont penalties tof frlA& aeltifleetiein Irtrl"1Nny (lufp, earl lotptlNU 111 11t. " PrinwU Name & Title 311sn,Itut e rz� KM