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HomeMy WebLinkAboutWQ0001318_Sludge/Compost Annual Report 2018_2019022640 CFR Part 503 Class A Sludge/Compost Annual Report for 2018 FEB � 6 2019 Lexington Regional WWTP — NCO055786 Compost Production Facility — WQ0001318 500 Glendale Road Lexington, NC Davidson County Permittee: Mr. Kim Burkhart City of Lexington 28 West Center Street Lexington, NC 27292 Non_plsch unit CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0001318 FACILITY NAME: City of Lexington Regional WWTP Compost Facility PHONE: 336-240-8316 COUNTY: Davidson OPERATOR: Kim Burkhart FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) p Distribution and Marketing (complete Parts A, B, and C) Was the facilitv in oneration durine the Dast calendar veer? Yes 0 No ❑ -► If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volumed tons Recipient Information Amen men Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January waste activated sludge 67.15 342.2 Individuals & businesses 61.4 lawns, February from NCO055786 48.19 336.4 Names and intended uses are 10.5 landscaping, March 38.49 394.9 on file at the Regional WWTP 159.7 soil April 69.22 377.3 573.3 conditioning, May 89.39 339.3 212.9 & bioremediation June 111.21 301.3 131 July 108.1 368.6 72.5 August 84.36 397.8 126.9 September 88.86 383.2 133.4 October 79.26 327.6 81.9 November 101.93 313 60.8 December 73.32 163.8 0 Total from FORM DMSDF (sup) Totals: Annual (dry tons):, 0 959.48 4045.4 1624.3 Amendments used: I Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 71 Part C: Facility was compliant during the past calendar year with all conditions of the land application permit p Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No --► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of P rmittee Date **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) gna r par (if differe fro ermittee) ,� -do a Date DENR FORM DMSDF (12/2006) Page Intentionally Blank ANNUAL RESIDUAL SAMPLING "SUMMARY FORM Please note that your -permit may -contain, additional parameters. to be analyzed. The- parameters can :be reported .in FORM RSSF - B WQ Permit Number: WQ000131.8 . Laboratory: 1) Environment l Facility Name: City ofLexington WWTP Compostfacility 2) :. Residual Source. WQ # or NC0055786/WQ000131&.. 3). NPDES #: : 4)- WWTP Name: Lexington Regional WWTP -5) Residual Anal sis Data Ceiling Sam 1e or Coin osite: Date - . Parameter (mpg) Conn Limit 2/6/18, 4/3/.18 7/10/18. 8/7/18 :10/3/18 '.12/5/18', Percent'Solids {% NA 48:6. 56.72 . 61:22 ° '. 43.33. 71.15 : 35.74 Arsenic 75 11 5.4. 4.4' 6.3 8.1.... $.6 Cadmium 85 10.96 .0.64 0.59 0.65 0.69 A.8 :Copper 4,300. 227 127 ' 133- 167 152 166 Chromium NA Lead 840- 47 .26 30. 53 61. 38 Mercury 57. 0-.83: 0.56 0:46: .. 0.47 0.53 0.57 Molybdenum ' 75 <5 0 <5.0 <5.0 <5A <5.0' <5.0 Nickel 420 11 7 .9 10' 7 9 . Selenium. 100 <5.0 <5.0 <5.0 . <5.0 <5.0 ..55.0 " Zinc . 7,500 589 370 '_ 378_ 466 451 `513 Total Phos horus ... NA 1-3640. 9148 10270 :.1,1800 . 4290 12390 TKN NA 2916.0. 20090..25500. `.230610. 38530 24830._ Ammonia -Nitrogen :: NA. 237.3 . 1684 - - . 2440 1332 2012 .. . 14.73: ; Nitrate and Nitrite. NA 464:6 : 20.9 6.97 5.96 17 250.217 'Tor -surface disposal facilities -the ceiling, concentration -limits listed in this form,arenot applicable: Reference the.individual peraut,for metals limits. "I certify,, under penalty of law, ahat.thb document was: prepared under- my direction,.or supervision in accordance -with a :system: designed to assure that qualified .personnel properly gathered and evaluated the information submitted. I am aware that:there are significant; , penalties for submitting false information, including. the possibility of fines and imprisonment for knowing:violations:' . . ....... Si e p * Date- - *Preparer .is defined in 40 CFR Part 503.9(r) and TSA NCAC 2T :1102 (26) _ �"� ,DENR.FORM RSSF (1V2006). . CITY OF LEXINGTON WWTP MS. GISELE COMER 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt, basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 6.2 02/19/18 KDS 4500HB-11 10720 02/20/18 LFJ EPA200.7 11 02/21 /18 MTM 3113B-04 14931 02/20/18 LFJ EPA200.7 0.96 02/20/18 MTM 311311-04 227 02/20/18 LFJ EPA200.7 47 02/19/18 MTM 311313-04 3573 02/20/18 LFJ EPA200.7 0.83 02/27/18 MTM EPA7471B 11 02/20/18 LFJ EPA200.7 4761 02/20/18 LFJ EPA200.7 <5.0 02/22/18 MTM 3113B-04 < 1250 02/20/18 LFJ EPA200.7 589 02/20/18 LFJ EPA200.7 48.60 02/09/18 KDS 2540G-II c 29160 02/22/18 CML 351.2 R2-93 c 2373 02/20/18 CML 350.1 R2-93 c 13640 02/22/18 DTL 365.4-74 c 464.6 03/09/18 NIF 353.2 R2-93 4330 03/12/18 SEJ <5.0 02/20/18 LFJ EPA200.7 Dr-iaking Water ID: 37715 Wastewatez ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 636 DATE COLLECTED: 02/06/18 DATE REPORTED : 03/13/18 REVIEWED BY: V ;1�e;4 c Uncertified data, DWR does not offer non -aqueous certification for thia analytical procedure. C! Envirnvment 1, mc. %- Aii. OF %-uSTUj., j(R u^—JR,, P.O. Box 7085, 114 Oakmont Dr. Page I of i r-:.,m,...:ne wr l'yQaQ DIStNFECnON . . 1' 1. ■CHLOWNE ' ■UV 011001110 soonNONE • • V• • • •. . ` .1 ==Now n� mv MM;i3ffl0qknq00E ■■�■■■■■■■■■■■■■■■■■■■ CHAIN OF CUSTODY DURING SHIPMENT/DELIVERY `_ ,�..71 ► , . CA PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C' forcomposite sample or a'G'for FORM N5 Grab sample in the blocks above for each parameter requested. N G 343534 Orlando, FI The results set forth herein are provided by SGS North America Inc. e-HQIY%CUpy 2. Aulomufed Report Technical Report for Environment 1, Inc City of Lexington WWTP; 28 W Center St, Lexington, NC 636 SGS Job Number: FA51716 Sampling Date: 02/06/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard @environment 1 inc. com ATTN: Deedee Woolard Total number of pages in report: 9 j - Test results contained within this data package meet the requirements Caitlin Brlce, M.S. General Manager of the National Environmental Laboratory Accreditation Program and/or slate specific certification programs as applicable. Client Service contact: Sue Bell 407-425-6700 Certifications: FL.(F.83510), LA(03051). KS(E-10327), iL(200063), NC(573), N.)(F1.002), NY(12022), SC(96038001) Doll EL.AP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, 1A, KY, MA, MS, ND, Nll, NV, OK, OR, U`F, WA, WV This report shall not be reproduced, except In Its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • let: 407-425-6700 • fax: 407-425-0707 SUS is the sole authority for authorizing edits of modifications to this document. Unauthorized Unauthorized modification of this report is strictly prohibited. _tr �(+`Q9 6 Review, standard terms at: http'//u-Aiv.sgs.com/enitemis-atld-wnditions 1 of g FAS1716 ' i o F A677.78 -SGS Orlando, FIL Section 3 Sample Results Report of Analysis SG 5 of r 10 FAS1711 tsener4 Chemistry Analyte ... Re�alt RI: Units 'DF Analyzed Ay `.Method Coicosivity as; -pH 7 3 su:02(13/18.14.10 - VK SWkG CHAP7'• " Cyatude Reactivity <,: 7' 2.7 ing/kg, . - 1. "62%21/-18' 17:15 KH SW846,CHAP7`.. Ignitaliility',(Flashpoint) a 200 . Deg;:F:. 1 62124/1'810 6 tW' : SW8491010• Solids; Percent _:. 54:7_' " . ,- % 1 .. 02/12/18 13s06 Jc°"" 5tvtis'i54bc Sulfide: Reactivity <89: = 89 ing/kg 1 02/19/18 ,18:00. 13GV; 9WW CHAP7 .. RL = 'Reporting 41mit e ot.9 • KA67?1fi' 11 GS 12 Misc. Forms.. Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 7ofF FA51711 SGS $ample Receipt Summary J6GIu'mbe -FM17,16, Chi i t:.ENV:7 Prriject . CITY 0 LEXINGTON WWTP Date!TimeRee6l6ed:0l0/20109t300,AM _ bill y,Wlethcd:-TED.EX, .Airbill#,'ae."100j893$5,136000328110042004b46 988; .' Therm ID:-CE:.0.4; #,of Cooloc4: ;1 Coo1er7dmps•(RawMOApuredj'C:- Coolef1; (4.4);. Cooler Temps (Corrected) •CE 'N.: 4 ' ' Sainole -'tr Cooterintormatiori Y or 1,; Custody Seals Present ®' N I�, : Informal/on or 1. Semple latiels present on bottles ® N1A . ❑ '2. Custody Seals Intact;, ® 0: 2. Srimples preseived'pfoperly, ;® El3..Tamp'oiiteri6 addeved ® ❑ I. Sutfdeni volumelcontainers recvd for analysis: 'G ❑ 4, Coolerterrmp verfiaatfori jB Cjlp` 4. Condi, an of sample . Irifact 5, Cooler media • Ice feaot r . .ol 5.:Sample rec4d evl0)in HT . .:•® "6,. Datesliimesn6s on COC match Sample Label ® ❑.. T�Io•Rlank•Iniormatlon V or' N - 7: VOCs have head¢paae , t. TAp Blank preseritl.cooler [] :. [j . (� " _ 8. Bbtfle5 feceived forunspecAied tests Q- „_.. 2. Trip Blank Usted on'COC I]; ; [] .® 9: Compositinu instructions clear, - IN -a f ::3 N!A 10, Voa SoiliCits/Jars reeeivetl'past;48hrs?" ' ❑ ❑ ®. 3iType;OiT6'Receided ❑ ®.' flAhSolldsJar:recelved7 ❑• „ ❑. Id 12. Residual,Chlodne-Present? ' . Mlsc:•Inforrimatlon = hiinibei'af Encores: 25-Gam - 5-Gram Number of 5035 Field Ialsi Number of Lab Filtered Metals: . Test Stitp'Lot iR4 OHM 230315 , 'pH 1042 219613A : Older (Specify) ' Residual Chlodho.Test Strip Lot*. Comments , svr Technician; SAY, - ReS.DeaSRa�tT Date: 2/.10/20189:30AOAM. '-Reviewer.-SP' _ Dater 2l1012018 " .. jR'k5l!4.6. Chain of Cu§tod" "Pik, - edai2 9 tS q 1 4 FA517 16 Er�viror�r�ierlt1, Iricorlor�ted GREENVILLE, N.C, 27835-7085 CITY OF LEXINGTON WWTP MS. GISELE COMER 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Lead (dry weight basis), nlg/kg Magnesium (dry wt. basis), mg/lig Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), nlg/kg Zinc (dry wt. basis), mg/Icg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),ntg/kg Phosphorus, T. (dry wL), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 5.8 04/06/19 HI1i1l1 4500HB-11 5944 04/16/18 LFJ EPA200.7 5.4 04/ 18/ 18 MTM 3113B-04 12829 04/16/18 LFJ EPA200.7 0.64 04/23/18 MTM 3113E-04 127 04/16/18 LFJ EPA200.7 26 04/20/18 MTM 3113B-04 2776 04/16/18 LFJ EPA200.7 0.56 04/12/18 LFJ EPA7471B 7 04/16/18 LFJ EPA200.7 4286 04/16/18 LFJ EPA200.7 <5.0 04/19/18 MTM 3113E-04 <1250 04/17/18 ONS 3111B-11 370 04/16/18 LFJ EPA200.7 56.72 04/06/18 JMT 2540G-1I c 20090 04/10/18 CLO 351.2 112-93 c 1684 04/12/18 TLH 350.1 R2-93 c 9148 04/10/18 114E 365.4-74 c 20.90 04/12/18 DTL 353.2 R2-93 2704 04/17/18 SEJ <5.0 04/16/18 LFJ EPA200.7 FAX (252) 756-0633 ID#: 636 DATE COLLECTED: 04/03/18 DATE REPORTED : 04/26/18 REVIEWED BY: c Uncortified data. DWR does not offer non -aqueous certification for this analytical procedure. 15 Enviromneat 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 7085, 114 Oakmnt Dr. Page 1 of n..m.,.;n. mr iiuSa DISINFECnON ■CHLORINE i x ■UVNONE ■■■■■.■■■■.■,.■■ « . C4184M PFESERVATX)N _. . .... _ B-HNE-H .. .. .. ==mmmrrrrFEEEEEEEE ASSFOTIOR- M w. DRWNGWATER ��■�aoa����ooae�■■■■■ NCJGW DURING SHIPMENT/DELIVERY �i'�'•i ' v : c ate AT,ffA • .� : '� , —I a FA 0 1 .• PLEASE READ Instructions for completingthis form on the reverse side. Sampler must place a C for composite sample or a 'G' for NO 3 3 9 5 2 B w FORM •5 Grab sample in the bW*s above for each parameter requested. It— _SGS-, Orlando, FL The results set forth herein are provided by SGS North America Inc. Hardcopy 2. D Automated Report Technical Report for Environment 1, Inc City of Lexington WWTP; 28 W Center St, Lexington, NC 636 SGS Job Number: FA53171 Sampling Date: 04/03/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentlinc.com ATTN: Deedee Woolard Total number of pages in report: 9 Test results contained within this data package meet the requirements Caitlin Bnce, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification program as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022). SC(96038001) DoD ELAP(ANA$ L2229), AZ(AZ0806), CA(2937), TX(TI04704404), PA(68-03573), VA(460177), AK, AR, IA. KY, MA. MS, ND. NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced. except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. - 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel; 407-425-6700 • fax; 407-425-0707 SUS is the sole authority for autharizinp edit.. or maditic.ations to this dovutnent. Please share your ideas about Unauthorized modification of this report is strictly prohibited, how we can serve you better at: _ Rcvic++ �dmidard terms at: h[tp:t/w+4l+tsgs.com: etu`letms-and-cvnaitiuns EHS.US.CuqomrrCarvQwsgs.com 1 of 9 V171 .-SGS. Orla Sample Results Report of Analysis Section 3 w 5Of9 213171 Client Saraple.ID;, . BED 'lI :PILE>2Q3 BONE 0 Lab .$ample ID FA53171-1 Date'$4Wi led: 04); -9' IvTatcix:. S0: = :Sludge Date• Ikeceivede 64/07/18 Percent Solids: 48.9 Project: :city of Lexington WWTP: 28 W,Center St, ,Lexington, NC General:ChemWrq Anal e; yt Result ' RL , Units -DF-. ::-Analyzed By Method: ggrrwiviiy as pH 8;0 su .:: 1 '04/09/18 12:15 Sk Svirsas.CHAP! Cyanide Reactivity 3.Q. - . mg/lig 1,.• .. 04/19/18 18:36 ]x ; sws4s cxarT - Igtutahilitylastipoinf) a > 20Q ; Deg. `F. .::1 04/23/18 1620 _Bw Sws4s ioto' Solids; Percent. 48 9: :: % 1 04/13/181Z:52- M SM19 254bG • .. Sulfide Reactivity <:100 : 100. mg/kg 1 04/14/18 10:55 'B{N SW896'CHAP7, (a)-N6t ignitable:.. RL := Reporting Limit al 22. FA`a371 Orlando, FL_ Section 4 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody 1� r of 9 MITI ESiylrunmetit 1, Inc; � CHAIN OE' CLISTO�Y I2EC0 P:OrBoz7A8S;:114 0akrtioritDr. Page 1 of 1 I�1C27858 CRV1COnmelitlinc.com, DISlNPECTION Phafik( kj1$64.09%Fax,(252)75f+0633' fk1LQR�NENEI1TRAl CHLORiN5 ¢EDATOOUFGTION CIdE)VT: .636' 'Week:'19 r-y QV: pHCHECk{lhBp :PPYOFL7LVVGTONV VWR. �••i NONE P• . P- P -1°. P. sP P k. 'P.. P CQNfAfNERT/PEPG. _ .... . MI6: mmm COMER B WEST CEPI CEB'ST: ❑ CHBXALP(MERVATILIN MMGMNNC27292 - . AA A , A, A' - •,•A A A A- A a l' 336) 357•7889 ' 9�F16; • E•FIC! F-aNCACETATFli1407i COI.LECtTON" t5 a -� _ . ,� � ;� G�kATHiOSULFATE saMLoc;An� nritE; 4.0 1 J 6' 1s a y t C1AS�F�AISON -2M` 4 - . l - y/%/P P • .. - WASIEWATEA(NQDES). Ll oRWNowATER , ' so>.OwnsiESEgrIDN C1iA1N OP CISSTOIIY (SEAL).MAIMAINED .. " DURING SHIPMENT/DELIVERY , • C� N SMdPLMCOU.ECTE_DBY: Sloe{,gvsN.ET' SAMPLESRECETIIEDWLABA'f !� Z-�C REU BY(SIC�(SAMPIER) DAWME BY ) PAW17 COMMEtifS Ram ULSRenytSG) DAMWE ) I TE/iYJE 4Tow" RECENEDBY .J DATElRMe: 0� %7 - 24 �� 24 �� a- .'Of t FA53Y7Z SG$: 5amp[e',RceipfS:ummary JoTi.Numbe�; FA53171 CI(ent ;ENV,1 P'roject:-. CITYi01=-LEXINGTON. " Date! Time;iteceived 9/7I2Di8 9:15;UO AM_ t)elnrery Metfioils FED. E)C ; Aililll #'s: 271940433480,_ Therm ID9 dR•1;. Theim CE 0:4;- #ofCooters 1, Cog10 Terttps (Rav i MeaLstfre °C; Poo ler:l; (4;2);. Cnolei Temps (Coirecfed)-"CE _ Cooier'1;`(d;8)p " Cooler InforrnaElon, Y or' N Samele Information: Y -,or N NIA 1, CgstodySeais_Pres6nt ® 1, Sample labels presenVon bottles `2 buslody Seals Intsci. ® 0 I. Samples preserved properly ® Q 3: Temp:critsrie ,achieved: ® Q 3..SunictegEvoluine/containers r'ecvtJ, for analysis: a, 4. Cooler tegip Ver111catiojl IR Giin. 4. Condipon of s"ample 1!', S. doolermed'ia Ice tang)5. Sample.recvd vdthin,HT ® p. `6. Dat..M.=ADs on 666 mach Sample Label ® ❑; Trio"Blank'Information Y or `N N1A 7. V.OGs liarfe;6eadspace [] Q 1'; Trip t3lank;present'Gcooler p Q 0 `8. Bottltpsretelyeil,forJnspeall(edytests ❑ Q 2.81a1it k.s SidnTn9 Instructions: clear" ❑ %®'' 10. Yoa Sail kitsfJars. ieeeived:past"48ti"'I ❑ �'.. 11.9G'Sotidsjar' receiVed? 13 Ij �. 3: TYPj# dt E Reaeived o Ea / .1?. Resfduai. Chlorine present? Q I1flisc:•Information Numbepof Encores:, '2SG�am 5-Gram.. tJumb'er.",of-5035 Field Kits: NOfriber-of Lab FilCeied Metals: Tesl.Strip ,Lolfls: pH`0=3 230315:. pH 10=12'"- 219813A, oiher:r(Spedfy) Residual Chloiine Te§t Strip_ Lol it: Comrrients .. ��docro��c��� �lfl Q�c�o�poQa��d P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 Drinking Water 1D: 3771, Wastewater ID: 14 *** THIS IS A CORRECTED COPY OF PREVIOUSLY REPORTED DATA *** ID#: 636 CITY OF LEXINGTON WWTP MS. GISELE COMER 28 WEST CENTER ST. LEXINGTON ,NC 27292 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH, units 6.4 07/13/18 JTH 4500HB-11 Aluminum, (dry wt. basis), mg/kg 8367 07/13/18 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 4.4 07/16/18 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 13736 07/13/18 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 0.59 07/19/18 MTM 311313-04 Copper (dry wt. basis), mg/kg 133 07/13/18 LFJ EPA200.7 Lead (dry weight basis), mg/kg 30 07/20/18 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 3280 07/13/18 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.46 07/24/18 LFJ EPA7471B Nickel (dry wt. basis), mg/kg 8 07/13/18 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 4510 07/13/18 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 07/18/18 MTM 311313-04 Sodium (dry wt. basis), mg/kg <1250 07/13/18 LFJ EPA200.7 Zinc (dry wt. basis), mg/kg 378 07/13/18 LFJ EPA200.7 Total Solids, % 61.22 07/12/18 KDS 2540G-11 WON (dry wt.), mg/kg c 25500 07/24/18 TLH 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg c 2440 08/06/18 BLD 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 10270 07/24/18 BLD 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 6.97 07/18/18 DTL 353.2 R2-93 Plant Available Nitrogen, mg/kg 3533 08/08/18 SEJ Molybdenum (dry wt. basis), mg/kg <5.0 07/13/18 LFJ EPA200.7 PHONE ✓o.�;«c FAX (252) 756-0633 DATE COLLECTED: 07/10/18 DATE REPORTED : 08/08/18 REVIEWED BY: ALLL__ e Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. 26 EmMormum t h(nno' OQTo P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 CITY OF LEXINGTON WWTP MS. GISELE COMER 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/I:g Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 6.4 07/13/18 JTH 4500HB-11 8367 07/13/18 LFJ EPA200.7 4.4 07/16/18 MTM 3113E-04 13736 07/13/18 LFJ EPA200.7 0.59 07/19/18 MTM 311311-04 133 07/13/18 LFJ EPA200.7 30 07/20/18 MTM 311313-04 3280 07/13/18 LFJ EPA200.7 0.46 07/24/18 LFJ EPA7471B 8 07/13/18 LFJ EPA200.7 4510 07/13/18 LFJ EPA200.7 <5.0 07/18/18 MTM 311313-04 < 1250 07/13/18 LFJ EPA200.7 378 07/13118 LFJ EPA200.7 2.46 07/12/18 KDS 254OG-11 c 25500 07/24/18 TLH 351.2 112-93 c 2440 08/06/18 BLD 350.1 R2-93 c 10270 07/Z4/18 BLD 365.4-74 c 6.97 07/18/18 DTL 353.2 112-93 3533 08/08/18 SEJ <5.0 07/13/18 LFJ EPA200.7 Drinking Water IDc 31115 wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 636 DATE COLLECTED: 07/10/18 DATE REPORTED : 08/08/18 REVIEWED BY: c Uncertified data. DWR does not offer non-agueous certification for this analytical procedure. 27 mnlronmulli 10 Inc. P.().40x--7-035-. Or U Ncn* 1 Ile _1C'2-7&58.1 Pi! ,,, � 1 tie - I T--7 — 7564)63:3' CH._h MEMIM,rk LLE0ti: 0 - -W(252) :PH*EGK(i ABA CLIENT:: Meek.-.17 UY CCr,Y'0F;1EMf.T0N WWTP MW -'P :-P P: -P P P. P. P WMAMIEFITYPERIG U&MSELEICOMER' -A G., 11CAL HE-1 -PRESEEMMnM -28 NMr CENTER Sr. NC A A A-AME- 'D-NA0H -'g. (330,35,74M cfj B-;HN0 E-HCL UJ U.1 F - ZINCACETA-FEEPHAOM OOLLECTION 0 G-NAMV J-7 i a .0s, 'A SAMPkELt7GAMON DATE TIME 6. G"MCCATIGNi- --6 '711011 SC JDVIASTESEC IOU j 7 MHAII-4 OF CUSTODY (SEAL) IVIMMAIMED- D IGSHIPMENTIDELIVERY URM SAMPUS COUCTED BY.: w S kNIPLESBECEIVEMN LABAB—!Q-.- WED. SIG SWPLER) DAMME 'RECEMDBY(SIGJ' DATEMME OOMMENTS. -T � A PX IM'0UISHEUiW.,(&a)' MT MW FECEwWBY'L(SIr--) TE ME. DATEMME FjEcE�y(sje DATEMME FOPUT45 PLEASEM Rinstructions-for zom'01Ptin i�Odwon'th- I g th e, reverse side. Sampler must place a."C`fdr compositersample or a-V for 00 Grab sample in .the blocks above',for each parameter requested: N2 3561:20 k., fi.0rlando, FL t, r The results set forth herein are provided by SOS North America Inc. Technical Report for Environment 1, Inc City of Lexington WWTP; 28 W Center St, Lexington, NC 636 SGS Job Number: FA55825 Sampling Date: 07/10/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard @environment 1 inc . com ATTN: Deedee Woolard Total number of pages in report: 9 e-Hardc'oly 2.0 Automated Report } J qe - Test results contained within this data package meet the requirements Caitlin Brice, M.S. General Manager of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051). KS(E-10327), IL(200063), NC(573), N](FL002), NY(12022). SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806). CA(2937), TX(r104704404), PA(68-03573), VA(460177), AK. AR. IA, KY, MA, MS. ND, NH. NV, OK. OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, Ft. 32811 • tel: 407-425-6700 • fax: 407-425-0707 SUS is the sole authority for authorizing edits or mudificatious to thi do:mnent. Please share your ideas about �° i Unauthorized modification of this relxin is strictly prohibited. how we can serve you getter at. __SGS,_ Review stmidard terms at: httpJ/ww�v.sRs.colnten/terms and amditiotts FHS.I)S.Custo uerc are: sgs.cam Of 9 LW925 • - S��$i®IflS $ t ® VAX ,e� s Section 1: Sample Sumtnary..:.:.:..:.::.:.........:..::.:.:..:..:...:::...1.::...:..:;:.::....:.:..................:::...::.. 3 4 SecfionlSummary-®f /pry (y/� �,. (etiy.�y m■y'� /y yp�y((�`■■BgI �^ I.,J Yr4��ilftt � �+Jf6YAl iJ �'4 .ROL�3 �G434� . ............... I........ \.:........ ji...f........ .��I�.s...16..s.i�...Y.......... f ..1..:............... .Z: FA55,$25-1: BED EL PILE 2061,ZCONE.1 . ..,.... .......................... ....... Sect"ion 4s NLsc., Forms •.. ................ .......:..N.: M•H........:....:..�i... :.....N....:.:......::oo....... .:: 4:T..Chain of Custiody ... .::... . ...:. .... ....... .. .........:,.... 2 of 30 - - PA55825 32 SummaryHits; of Hi lob Number: FA5588' Account: 'Eny1rpament"l,-Inc. Project. City of Lekioit6n 28 W-- CenterS!-,.Le PoM40. '0.7/10./18 Lab 0*0*10 ID Ogmt Sample 11 D I Resu . W Analyfe Qy4al . RL bmb- UAfts Ivlethod FA55825-1 BED IL TILE 2Qff ZONE.1 IC qFrQsWity-'as,bH loitait hp y (FW oin!) 4> 20 'Not 1&itAble. §u SW846 CHAP?' F SW846. ffiol -Page i of i M _SGS, 4 of FA55-825 r. 't a IN� ate K —SI Orlando, FLU`. Section 3 Sample Results g, Report of Analysis 5of9 SG'S,Nbrth.-Aifi&ica Iric.- Report of Analysis Cm&dt SgimVle ID-. BED IL PILE, -206', ZONE I Lab SA&ple ID: FA55825-1 Date. Sampled: 07/.10/18 Matt -ix: SO 4 -Sludge e uc,�M4: 'Oh h8 V.'qr.i;6nt Solids: OQ; Citrof Lexikrtofi..WW.TP, 28 WCeriter S Lexington; exfogtonj NC dencril dhemisiry Anilyto, Corrcisfvity'-,a$ -ph .Cyanide; Reactivity xgn't4iliv (Fla 4gint) 84dsi Percent.Sulfide ReacftVifv {a)'Not ignitable. RL..= Reporting Lid( Result bp su, mg/kg I.. > D.eg. F 1. - %1. 4 .74 T�g/kg I Pago i of I .Analyzed- By Method -Bier SW846' C'H"7. 07/24Y19 i61bi. jK SW8 -PHAP7 O7/26" 18 11:24' BAF, $W846-1040 OT/.- 14i1$14`35,'M' ; M19 84OG- 0/24/18 1146 BW 'SW'A6,PHAF7 34 0 e 11 SO ax4 4 G Orlando, FL ; Section 4 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody 7 of 9 ..,Ts7sla7l._ 88829 Blot lir'. cliv lu" pil't, CrFY,qFUMNr,TOX-WWM Off F P. t,pl r 29MAMr-COMER ULWGMN:NC;T;n A (i36),3S77889 7- :From 7[PIWEREAD'Idstrucflonsf6�comploungthis, fdb-on'th6 ravel DY.Rr-WoRAS ti � Y 4r C4ipRAHEidElfi41REDTfcOUECi1fMiA ,A, ,L A� . OURAY16N:. R,9 55 G-f*T!03ULFATF` 4, .19-:1010, oupiNG"mmiurukay" b&ri ESFWCEM to eirqui;placepV0 r c*oskeisaroplci Orb t" ki, GrabrO sample Ia the Wadi abue tot each parameter requisl6d; FA5$82-5,.' C' h a ill 0 f Ci UAOY; Phge I of I 221 8 of 'Clid V,.ENV.1, Joh,N n Piojiicl, PITYOF Date 14, a Al T!m Rec�IiTd; P�!!�. ry I�etho�. f ipl I;X MerTn'jD:4R, I"' i OfCocilos: A Coibler re jG06-ler TOWS (pk e -(4 'd016i .or :N 8. praden t-6niottles 1 13 2. Custody sobisintdoi d'd properly Oent vq!um"qtalnars re rana!ysfls.,. ertemp,verification. lliStln .4:.Cofi.ditibn of sample law 5.,'C66ltr thedfa Ice HT' match Sim Le I V16,61ank 106finatibb Y' `or N _HA_ "i.-V668 6w6ad I so . ace, 2jrip [jank!Nted'OwCOC 0 'D M 9.;CaTpqsitlng Instmetigns. clear b Ni ill- � S'/Jqrs receVedpaA 46rsf 3. tipe Oft84keoeive-d'i 'j 12' JRo orl sl,dual.-Chl no:FNsent? El El K4mbif6f 614*i' . 15-G Fini :'5-dram - kumpep of. 605 Fie'ld kit *666er, of Lib 'FifieradMetals: , Tebt'SJtdp Lot,#s, pt !'O3 230315 pH 10�12 210813N, (Spqciry) Residual Chiorin -a Test Strip LoW, Comments T�6ifnjcjifhE - SHAYLAP Wd: WWA' Fiiviewer bate". Rev. Dole WNW ......... FA5,5825,. ChAin of Cxfstoo),i fiage 2.- o.f 2 37625 ElMoTmEw Rio kw Mho P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 CITY OF LEXINGTON WWTP MS. GISELE COMER 28 WEST CENTER ST. LEXINGTON ,NC 27292 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH, Units 6.1 08/10/18 JTH 45001IB-1I Aluminum, (dry wt. basis), mg/kg 10431 08/22/18 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg 6.3 08/21/18 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 15242 08/22/18 LFJ EPA200.7 Cadmium (dry wt. basis), mg/kg 0.65 08/29/18 MTM 311313-04 Copper (dry wt. basis), mg/kg 167 08/22/18 LFJ EPA200.7 Lead (dry weight basis), mg/kg 53 08/24/18 MTM 311313-04 Magnesium (dry wt. basis), mg/kg 3982 08/22/18 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.47 08/31/18 MTM EPA7471B Nickel (dry wt. basis), mg/kg 10 08/22/18 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 3803 68/22/18 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 08/30/18 MTM 311313-04 Sodium (dry wt. basis), mg/kg < 1250 08/22/18 LFJ EPA200.7 Zinc (dry wt. basis), nig/kg 466 08/22/18 LFJ EPA200.7 Total Solids, % 43.33 08/09/18 JMH 2540G-11 TKN (dry wt.), mg/kg c 23060 08/14/18 BLD 351.2 112-93 Ammonia Nitrogen (dry wt.),mg/kg c 1332 08/21/18 TLH 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg c 11800 08/14/18 TLH 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg c 5.96 08/22/18 TLH 353.2 R2-93 Plant Available Nitrogen, mg/kg 2845 08/24/18 SET Molybdenum (dry wt. basis), mg/kg <5.0 08/22/18 LFJ EPA200.7 Drinking Water ID: 3771! Wastewater ID: to PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 636 DATE COLLECTED: 08/07/18 DATE REPORTED : 09/17/18 REVIEWED BY: t c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. 38 environment 1, Inc. CHAIN OF CUSTODY MC:URU O. B 7085,114 Oakmont Dr. Page 1 of X,_ KTr•'I'lOrO • ., • DimmcnON ■CHLORINE ■UV■■�®i®i�i■■■■�■i■ NONE t . - eeeeeeoi000■�■■■ .• . .. . t • • NATHK)SULFATE. .. .. • • -G _ - - - ..: ==MMMLLLLLLLLLLLMMDURING ■■■ .. . CHAIN OF CUSTODY (SEAL) MAINTAINE SHIPMENT/DEL[VERY u l._� J TT ' ff', tMat f L1 ' cwc Sampler must place a'C" for composite sample or a V for p- 3 3 7 6 9 7 ".s PLEASE READ Instructions for completing this form on the reverse side. Grab sample in the blocks above for each parameter requested. N SGS r. V0 Orlando, FL Tlie restitta sei forth herein are providced by SGS North Anie tica Inc. e-HartiCopy 2.0 Atttonrated Report Technical Report for Fnvironment 1, Inc City of Lexington WWTP; 28 W Center St, Lexington, NC 636 SGS Job Number: FA56695 Sampling Date: 08/07/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard @ environment 1 inc. com ATTN: Deedee Woolard Total number of pages in report: 9 r.�? - Test results contained within this data package ►neel the requirements Caitlin Brice, M.S. General Manager of the National Environmental Laboratory Accreditation Program andlor state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), 1L(200063), NC(573), NJ(FLO02), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZO806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY. MA. MS, ND. NH. NV, OK, OR, UT, WA. WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 - tei: 407-425-6700 - fax: 407-425-0707 "l;S is th, wAe dttilt;k mtN 1 r a,ut uai n� ,lit r fn l,I,t'atmi} to, thi:, document. Pleaae shate ..our ideas about I11mathorired ,r,illic:tl,on,at III]',w1wirl is taiit,ti: Tw- ttihil.d holy we Can servt; you bcact at: I zwkiatt!:i,, aItp+t %t.,.+lnc4(r HIS l �.t ❑lt,ritlt7t ifra(�!`3gs.iarn t of FAS669.. 6 e''s, Section L-Sikinple Summary , ,...:...............................:.::....:::.:.:..: 3 - $ection.Z:. Sumnn:avy of :T3its::...............:.:....:........::::::..:o.::- ..... 4 Sed2 ion 38: ml le, ....... :...+........:............... i.e:.:.e.e.•.c.:r.:p....�.... 3.3 : FA56695-1: TI BED PILE 2U6_ZONE'S b Sei tiQ 4:1Vii c. dorms : •............a ....... :f..n.• , 4.1: Chain of.Custody ....,::.............:...:..........:::..,:::: ,:.:' 8 . i ,SG:S.Nortl America.Iiic. Sample. $umm:ry Emko' htiierit 1, Inc City of.Lexington VUWTP; Z$ W Centor St;1exingfon1VG Project No:" '63fi. Sample Collected_ Matrix. Client Number Date Time By Received Code Type Sample ID' .rA5669571 0 WII& 14:55 SF 08114/18' SO" SIudge BED IIPME-206.ZONE;5, Summaxy of Hits Job Number: ' FA56695 Accounts Environment 1, 3nc Project:;' . City of Uxin&h W .TP 28•W'Cent6f St;.LeWingtdh, NC: Collected:. 08%07I18 Lab: Sample ID: Client Sample 1 - R®sult/ Anal}!t® Quin RL IML Uriifs Methoid. FA56695=1' BED II.EILE. 266 ZONE` 5 :. Corrosijiity as pH 8:1: Ignita6ility:'(Plasli0in ). a _ > 26 'Sulfide Reactivity' 110 (a); Not. ignitable. 'su- :SW846; CHAP? Deg, F _SW846-161QA. ntg*g: §W846-,CHAP7 i ..�.... SGS- Orlando, F Sample Results Report of Analysis i 44 SS 5 of FAS6690 SGS North, America Inc. Report Of Anal, Page. is 6f I . Client Sainpla ID: • BED II PILE 206;70NE, 5. Lab ^Sample ID. FA566954 Date Sampled; 08/01118. - Matrix: SO :.Sludge Date Received: 0, L44/14 Percent Solids: 44:9 Project . .City Of Leiungton Wl!VTO 2$ W:Center �St. L'eiungton; NC: General:.Chemistry Anatyte, Result: IZI: Units DF: Analysed By Method C&rosivity as: pH 8:1 su 1 0$116/1815 27' Bh SW89G:CNAPZ Cyaiud a Reactivity- a < 3'. Z :: 3.3 .::ing/kg 1. 68/22/18 1040 .A, gl V 46 CHAP7: Ignitability,( lashpoi O b >'200 . 1)'eg.T- .::1; 08/271/8 11:53: _131N' ,'SW84610'10A. Solids, I?ercent .44.9 %., 1:. 08/2411810., 6 - I R "SM19.2540 `, SU-B& Reactivity. 689 110 ':mg/k A 08/23/18 15:45, B1N sviWs46 CHAP : (a). Sample aiialyied beyond heldainie :(0): Not.igiutable.. '°,•„+�€i4 r a ..-SGS Orlando, FL r x Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 [A Ell SGS7 of 1 FAassas . •' 'Bngli'olimentl,Ine. CHAIN OFCUSTOD'�RECORD �:. .�.. . ... • • " , ::drr�6vi11e, i3�C.27858 . ' , . ' • � .. _: ' eny1ronmen)11na'xoin . D1StNFECiIO1J : Cji0F11�TdElftAllil7/fll1TQOIlECif�j ' .. CHCORitd6 •. ' �iiTY.ORLi�I1±iC�TON.WV,Y►� : ; " .. � �NQ� .p; :"P P' "..t�ryfAlt�AiYPl:;�i%' • 114B::6IS61.8 COMBR- 28"WBST-C6iPiE88r: `LEXIIVGTONI4C�.1292.. • . j-j '.+..a� A A A - ;- 'CFPOCAPR . . A=NONE 040 � - 357f/889. 9'FYdt1, • E'=Hp. 71NGA*rEtAiEINgQl1 i .. 'COLIECfWN • �a - �" G,-.NATt�IAFATE', SANTIfI{ICiagf�' .... : .f�!AE' . •'�-.. �'o �a ' ;6fu Sample. 6 ol CLJICNION �.t. tr,;P'k?.a�!z� "�:7 f �"� ' • tP3 Z - �•: J •.� . �' WAStEYJ+tI�(NPP>�S) . ;DWC7GW .. - .. _ CkWIN.UF,C11fiTOpY.ISFAI•i.MA1NilUHED .. �UiUNGSHIP.gViENi(OEL EAY:'+ . _SM�lESCdlt�61�9Y:; - - 6Aldt�SAEC�VEDWLAfIAi, y �—.L"� ' :)) OATE�IYaE " - • . . RECENED Yjsw3.) r (A.11f�1Tff.• RBAOJS OYM, DAtERNAB IV ESfffD .(SKi},' , OATEI►IA� yy,, p( - _ • BIEASEREAD lnstniionsdor com' le Uiis Lorin on:the r�versB's�de: ' ; " V Sampler mvslpl a'torcompos sample ora `Q, ter " .,- 8 " ' 33,7097 : -cam same m"me blocks �a for eaen oammeter rosp,oslsa. . ,�, . , . . PAO 1,101 .tQ . SO$ SampleRece$t'Sutlnmary b044er7v M5 95:_ Client:-ENVIRONMENTI INC.,, P�oJect: 836 pafe;!'Tlme Rec@Ived: ;811'412418.9:t)p:t]O:AM •• dellvery.Method.. FX; Alitilll#s::"100i8977398600632@110043%02138t)5 Tfieiin.ID: IR' 1; Tfierm, M:: qil- *'Of oleic; .1 Coolei7einps..(Ra4v'Nteasuredj.°C. Gooler.;lt.(d;aj; CbClet-Temps (Corrddted):'C:::Cooler 6661erdnfoimat16ri:' :- Y '6` ..N- - ' ' : Saritole iriformat)on Y 'or .. N -- - NIA. t: G`usttidy $sale Preserd • �� "" Q 1; ;Semple labels'preaenbon bottles; ?Xuitady-, Seals, lnldci; ®• ... .. - .. 2. Samples"preserved P.raPedY �I. - 3,Temp'aiteria'actiieSetl. ":®' :�']• " „ 3iSutficientirohiine/coniairiersrecvd`forarietysts ®_ 0 i:Coolel fempVerifca'tioli'' • • ."ur 4', Co'ndltdbn ofsainPle Intel.. - 5; Coolertp"edia, Ce" , a 5; Sample recv4.wilhimH7 G.. Date s>rmesAOs on COC match "Sainpte Label'•• ®'- 'Trio"b 6ikd6forryia6dw Y • -o►<• N NlA 7 VQCshaGe'1%ead§pace Fjiip 81aak:preterit I tooter' ❑ . �, ® 8.. Bottles iecelved'fot• unapecilied tests -. Q . ®', . 1,7rip.13lenklisted:on`000:: �_ )]; `Compositing " ` clear " :.. m:insfructions 80:VoaSii11,, plop m 610edPa9t4@hrs2. p .. Q` 3: Type Of T9;3eceivgd` • ' ." . : 11 jar'rec�lved? '%;Solids". 12: Residual,Cfiloiine Present? INi'sc:'Iriformafion, Numb.?�t`ALMC r 25;Gram> .. S Gram Number ot-5035field Nits:.: ' . - - Npmtiec6t leb ggqed Melals:, Tesl S p" NpH 0 3.• "230315 :pH 1Ua2 .21981.3A .Oth'ec (Speafy} Residual Cfiloririe Test,S'tdq_Lut # ' : - ' nvrronment 1, Incorporated 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OP LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt, basis), mg/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 5.9 10/04/18 JMS 4500HB-11 10198 10/10/18 LFJ EPA200.7 8.1 10/08/18 MTM 311311-04 13442 10/10/18 LFJ EPA200.7 0.69 10/09/18 MTM 3113B-04 152 10/10/18 LFJ EPA200.7 61 10/10/18 MTM 3113B-04 3822 10/10/18 LFJ EPA200.7 0.53 10/22/18 MTM EPA7471B 7 10/10/18 LFJ EPA200.7 4651 10/10/18 LFJ EPA200.7 <5.0 10/05/18 MTM 3113B-04 <1250 11/09/18 AKS 3111B-11 451 10/10/18 LFJ EPA200.7 71.15 10/04/18 JMH 254OG-11 c 38530 10/11/18 DTL 351.2 122-93 c 2012 10/12/18 BLD 350.1 112-93 c 4290 10/11/18 CLO 365.4-74 c 17.00 10/09/18 DTL 353.2 112-93 4675 10/15/18 SEJ <5.0 10/10/18 LFJ EPA200.7 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) la6-61'U8 FAX (252) 756-0633 ID#: 636 DATE COLLECTED: 10/03/18 DATE REPORTED : 11/16/18 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. 49 nument 1, Inc. CnAIN vjr'CXjb-.t0Dy XECqjXD P.O. Box 7085,114 Oakmont Dr. Page 1 of I DIS&FECMON '11 Tin -W CHLOME ■ UV ■■,�r�■■,■■■■,■ NONE eeeeeee■eee■■■■■ CHEMICALPRESERVATION -NW D-NADH IF f n _A _ HU C-HS0, F-MCACETATENAOHI: .... _ G-NATHIMLFATE F ■■■■■ CLASSIFICATION: ,,■■■■■■e I WASTEWATERMDES) . _ .■rye■aa■■■■■■■■■■■■■ ■�■■■■■■■■■■■■■■■■■■■■■ ■ 1RWWjWATER DWI" SOLID WASTE SECTON ��■■■■■■■■■■■■■■■■■■■ CHAIN OF CUSTODY (SEAL) MAINTAINED SHIPMENT/DELIVERY -�■■■■■■■■■■■■■■■■DURING NOR 0 N "I *-Ike X"OH291 I_ 11011101■■■■■■■■■■■■■■■■■■■ • «> >. MEN N 17: = PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a 'C for composite sample or a "G" for Q FORM#5 Grab sample in the blocks above for each parameter requested. N! 361149 Orlar The results set forth herein are provided by SGS North America Inc. Technical Report for Environment 1, Inc City of Lexington WWTP; 28 W Center St, Lexington, NC 636 SGS Job Number: FA58206 Sampling Date: 10/03/18 Report to: Environment 1, Inc dwoolard@environment 1 inc .com ATTN: Deedee Woolard Total number of pages in report: 10 e-Hardcopy 2.0 Autoinated Report A - Test results contained within this data package meet the requirements Caitlin Brice, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510). LA(03051), KS(E-10321), IL(200063), NC(573), NJ(FL002). NY(12022), SC(96038001) DoD F.1.AP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA. MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety. without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. - 4405 Vineland Road - Suite C-15 - Orlando, Fl. 32811 - tel: 407-425-6700 - fax: 407-425-0707 SGS is the, sole authority for authorizing edits or modifications to this document. Please share your ideas about (�(�(� Unauthorized modification of this repots is strictly prohibited how we can serve you better at: auJ Review standard terms at: http:I!wwtv.ses.cotn/en'temrs-and-conditions EHS.LIS.Cu__tomer(.are(t1 sgs.com 1of10 tiA11f206 October 26, 2018 Ms. Deedee Woolard Environment 1, Inc PO Box 7085 Greenville, NC 27835 RE: SGS North America Inc. - Orlando job FA58206 Reissue Dear Ms. Woolard, The final report for job number FA58206 has been edited in response to your recent data inquiry. The revised report contains the following changes; The reported value for Ignitability has been corrected. SGS North America Inc. - Orlando apologies for any inconvenience this may have caused. Please feel free to contact us if we can be of further assistance. Sincerely, SGS North America, Inc. - Orlando Cc: Florida ♦ 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 ♦ tel: 407 425-6700 ♦ fax: 407 425-0707 52 2of1 PAWL- bh 0f C:anteuts Section 1 Sample Sumuiaay:.::::::.:.:...........:.:::.:....:::..:.:.......::......:::.:..:::::::::::::::...:... ...:..... S.ecfion 2: S'uth iary �of Hits .,::..:.::.::................:....:.:.::.:.:.::::.::.;.:.:...:.;..::.:.:.:.�..:..:...::.....:.:.: 5 Scetioii3i Sam pie R6,010...:.:...::.::...:::....::.:....:.....:.:......:..:.::..:...::.:... 3.1:. FAS 20.6-1: BED-11 PTCE 307. ZONE. 4....a.:...:......... ................................. ................ 7 Sectnon4: M16e. Foams .........................................::..........:................................................... S: 41: Chain of Custody ......... ........ .......... - _. .......... ,of40 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA58206 City of Lexington WWTP; 28 W Center St, Lexington, NC Project No: 636 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA58206-1 10/03/18 08:30 JL 10/06/18 SO Solid BED II PILE 307 ZONE 6 Soil samples reported on a dry weight basis unless otherwise indicated on result page. A%^ ' a of i 54 FA58206 Siii ary-of "Hits:.. - 7ob,Numbert. FA5820 '' Account: Environment 1, Inc Project:. City of Lexington "WWTP; 28 W Ceritcr St; Lexington,; NC: Collected. 10/03/18 Lab'Samoie ID 04"t inogID ResnIt/ Analyte Qiial RI> IVIDL Units .IVlethbd Orlando, F!, Sample Results aR 1 r`.x Report of Analysis Section 3 0 56 ` FA58206 r L._; Client Sample ID BED II PILE 3VZON_ E.6 . . Lail Sample ID . FA58206=1 :: Date' Sampled: ;10/03/18 Matrix: SO - S61id Date.Reaeived: 10/06/18 Percent Widss �60..3 Erojed City of exington WWTB; 28 W .Center St, Lexington; NC. :GeneiAl Chemistry ApAlyte Result RL, Units DF Analyzed ;By, Method .Coito§Wlt' -as, Z:.3 „ , . sn i .10%22118 16:25. sW SW.84s.CxAp7 Cyanide Reactivity SN.' : 2;5 mg%kg 1 1:01$/18 15t:02 .1$10:27 _�K ' sv+i84s::cHAe7 tgnitaliihty tElashpof.nt) a > 200 Deg. F. 1 10/1 13W SW846;1010A Solids; Percent. ; 6Q:3 % 1 10/0�%18.11:55 AG. SM19 2590G, Self de;Reactivity ` <$1- = °;" `81. mg/kg 1_ 10%17 IR 14 08 W SW896 CHAP7 a _ Not i nitable RI. =Reporting; Limit 7of10 S.G-9,- feG�820E C ✓h -7 rT" Orlando, FL 4 . Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 58 Sofi �� - FA582W It. . Z -Eiifiifintiptjjin&, Dr. CRAINPYCUSTODY'RECORD ;Jn I LCF. er-vlllp If KLGJM; o Ik A e�ee�ee■ee��®■®®■ �. . . ..... ==won[ 211 U1311 go 11 11 al V Uri OMMUMMOMMI;.. Upffieffisom _ . I -a V� (NPPR- DfrNMGWAIM RM!'"Mraml e■®®■■■■■e■■■®■■■■■■■■ W. .I , RIN UW MR -On" m RX!mm I PLEASE READ.Idstr6dionslorcor�pldft this aft on ttLe*iev0s6 M& 1 dbsamMeinft'b1cc4mab—'ZF",a,� '"equ4st T'Dp tV )9/4 Ila 1cw --Zt, Gr 0110 le Z=-'w id FA-58206:'ChAin, of Custo pAge i of 2 SGS Sample Receipt Summary Job Number. FA58200 Merle ENVIROMENT 1, INC Projed: on Delia / Tuns Reoalvad: 10AW201510:00:0o AM Delivery Marlrod: FED Ex AlrbM #s: 1001 8933507600032M f 0048'1155081050 Therm ID: IR 1; Therm CF: -0.2; *of Coolers: 1 Cooler Temps (Raw Measursd)'C: Cooler 1: (2.2); Cooler Too" (Corroded)'C: Cooler 1: (2.0); ®�pE Y or N Y or N -Wh- 1. cUdody Sale PreaM 0 ❑ 1. Sample labels preserrt on boBNa ® ❑ 2. Custody Seals kdad 0 ❑ 2. Samples preserved property 0 ❑ 3. Temp orkerle achieved 0 ❑ 3. SuA dwd wlumakorAbMNrs aovd for Mhdyaie: 0 ❑ 4. Cooler hemp vwNWWon 1110w 4. CorAkm of wnWk k= 5. Cooler media Imam 5. Semple reavd vAOdn HT 0 ❑ 5. DMesITImeWs on COC mooch Sample Label 0 ❑ Y or N JWd 7. VOGa hove headspace ❑ ❑ 0 1, Top Blank p usel t / cooler ❑ 0 ❑ 8. BoMes malved for ham KMW WO ❑ 0 2. Trip Monk lined on COC ❑ 0 ❑ e. Composov beruck" dear ❑ ❑ 0 10. Voe Sole IOWJam waived pat 45hrv? ❑ ❑ 0 11. % Solids Jerr received? ❑ ❑ 0 3. Typo Of TS Received ❑ ❑ ® 12. Rsdduel CNwkw Present? ❑ ❑ 0 Number of Encores: 25-Mam 543rom Number of 5035 Field Klb: Number alLab Filtered MsINn: Tat Strap Lot is: pH 0.3 230315 pH 10.12 219813A Ok►er: Mpo*) RaWusl CMwkw Test Strip Lot e: Commards i1g01 rw. err ssrWT.rhnidan: TMMTYM Deft: tOl MIG 10..0O:OOA Ravinvar. DNa: m FA58206: Chain of Custody Page 2 of 2 60 10 of 1 Envi onment 1, Inco pora ed 114 OAKMONT DRIVE CITY OF LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.), ng/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg +��a Drinking Water ID: 37715 Wastewater ID: 1, PHONE (252) !a6-62 U8 FAX (252) 756-0633 Sludge Analysis Method Sample Date Analyst Code 5.6 12/07/18 HMM 4500HB-11 9899 12/12/18 LFJ EPA200.7 8.6 12/19/18 MTM 3113B-04 16092 12/12/18 LFJ EPA200.7 0.80 12/16/18 MTM 3113B-04 166 12/12/18 LFJ EPA200.7 38 12/17/18 MTM 3113B-04 3441 12/12/18 LFJ EPA200.7 0.57 12/18/18 MTM EPA7471B 9 12/12/18 LFJ EPA200.7 5041 12/12/18 LFJ EPA200.7 <5.0 12/19/18 MTM 311313-04 < 1250 12/18/18 AKS 3111 B-11 513 12/12/18 LFJ EPA200.7 35.74 12/05/18 KDS 2540G-11 c 24830 12/11/18 BLD 351.2 112-93 c 1473 12/10/18 BLD 350.1 112-93 c 12390 12/11/18 TLH 365.4-74 c 250.2 12/10/18 TLH 353.2 112-93 3322 12/14/18 SEJ <5.0 12/12/18 LFJ EPA200.7 ID#: 636 DATE COLLECTED: 12/05/18 DATE REPORTED : 12/26/18 REVIEWED BY: A��L_ c Uncertified data. DWR does not offs: non -aqueous certification for this analytical procedure. 61 nnvkomnent 1,1nc. k z1LAIN tjr' Cua 100E Y AE(,%jkD P.O. Box 7085,114 Oakmont Dr. Page 1 of 1 .! 1 ■CHLORINE eeeeeee■eee■■■■■ .• - - NECHMALPFE• • • `• IACETATE/NAOFr •. LLFATE .. • n • - - - - ��...:�,,� : �■tee ..s r_� ■■■■■ «�.,� . . CHAIN OF CUSTODY (SEAL) MINTAINED DURINCIPMENTIDELIVERY ve PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G°for 'D �.s N Grab sample in the blocks above for each parameter requested. HO 357673 Orlando, The results set forth herein are provided by SGS North America Inc. e-HQl"dCIJl) f 2.0 Automaled Report Technical Report for Environment 1, Inc City of Lexington WWTP; 28 W Center St, Lexington, NC 636 SGS Job Number: FA60022 Sampling Date: 12/05/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard 9 environment 1 inc. com ATTN: Deedee Woolard Total number of pages in report: 9 -�txN Test results contained within this data package meet tire requirements Caitlin Brice, M.S. of the National Environmental Laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), 1L(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB 1.2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573). VA(460177), AK. AR, IA, KY, MA, MS, ND, NH. NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed, SGS North America Inc. - 4405 Vineland Road - Suite C-15 - Orlando, FL 32811 - tel: 407-425-6700 - fax: 407-44++255-0707 sZ�is .iris is the sole authority for authorizing edits or madifscatitais to this & cutnent, Please share vour ideas about t luatttlxxiuJ modification of this report is Strictly prohibited. how we can serve you utter at: Itevie.t ­mandsrd terms at. http:i?�t�� v.sgs.cont;en;terms-and conditiists CtiS.[1'i.('usiontzrCarei'r ks.4iam 1 of 9 163022 Sectioais: Table. of Contents _a. Section 1: Sample Summary ......::....: :............... 1.........,............:....:...........o.:.:....,..:.;.,,...,:....::: Section 2: S:ummarp of.Hits.:.::;:..:.:.....:.::...:::..:...:...::.....:.::....:.::.......::.:.:.:::..:.:::.:e�;.::.... geetiou 3_i Staple Resutts ...,;:.::..::...:..:..::...::......::::....:..>..:.,...:::.::►,,:........:.,:...:.:..:.::,:...:..... 3:1: FA60022=1: SLUDGE SAMELE _ .. 6 Section 4: Mise. Forans:.........:.:..::.:::..::.;:....:::.:.:.:.:.<.:.::::::.::::::.::::.:.......,::::.:..::::.....:.::.:.: '7 64 2 of, FA0o022 SGS-.N6tffi Affii&k Ific.. E.. nvjhmme'jq'I ,116c of L&` VvWTP; 28 W. Center St,,Le� NC: city il !Ogtou P i Oyj 6:36 Job No TA60022 SampleClient, Collected_ Number, Date Time By kccdived �'Typ6' Sample ID JI 12 Qg/ 18 SQ, 5tt!qge SLUDGE; SAIViPE X., Soil samples reported on, Ady—mi'Ios1u.nIess,,, qt4qrwise.mdicated on result page. H Summary of Hits 'Yob. Number:, . FA609124. Account: Environment 1,, Inc Pro, �i� 6.�,Lexlhgton W'WTP. 28,W.C.eiiter�'S.f.,.Lexingtbn,, NG Coll 12145/18 Lab Sam pl6,. W Client,SamplelD Resuld Ana,fyfe Q.ya I RL WD I L ullois., ;Niiih I SLUDGE CQ"rrQ$'lVJ("Y'4' PH jashpqint) 209 N6i bl' .1 n ti gl, � e. -.p4gp, I Of --i su SW846 CHAP? .Deg. IF SW84 � 6 idiOA 4.01) . . 66 .-I aoff FM0022 s � � ii.......1,�-- F .�y� -MA Orlando, FL Section 3 tom..., Sample Results` Report of Analysis 0 SG Fon SGS North AmericaInc. Rqppit of Analysis tieht Sample ID; SLODGE SAMPLE Lab B` p'le, D':'-, A60 02 Z4 Date Sainokd` I2/6 5118 M rix-, SO = S.14dg,e Pe*,.oezit Solids: 23.9 49t Project; City of'L;exingtbif WW, P�p 28 W, Ctht& St;, Leid- on? NC General .Chemistry 4alyte Result RL Codosivlty- 'as "PH 1.41, Y, Cyah-id6keactiv"it- 6.2- 1gpit.Obility (Fla§h0oifit).A >200,: -S6li&,, Pe'icent, 21.9' :Sulfid6 "Reactivity . -;<"zio 210 (a).Nqt ignitable. RL.= Repoftitig Limit Page. I,-bf I - Units bF -Aniily&d 1 y -'Mahcd .1 12/17/18 12:51 -BW SW$46 CtWl irlAg 1 :12/14/18;14--00 jK SW846 t RAP17' De-:'V. 4t 12h-01840;23 IRVV 48d6*,-1.0 I OA MOD, % Y 12113/1413:19AO' SM-A'2540dl &/kg I -.12/14118 15.-30 42 -'SW846 CHAP.7 68 ra of; I FAD= t Orlando, FLU, Section 4 Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody L of 9 169022 Environment 1,Inc. CHAIN OF CUSTODY RECORD A �OD P.O. Box 7085, 114 Oakmont Dr. Page 1 of 1 •• • .Uv NONPia �E �,� ai ���� �eee■■■■■ .• A-NONEr • B-HN-• ' : i i _G-NATHOWATE Ol ■t flU� I it .lL LLI 10000■■■■ ■■■ ■■URVICIPMENTIDELIVERY. r �1I_�Ril1�/ :1:7.I�iLir'L�31'Pt7lf��7.:'•T, PLEASE READ Instructions for com letln this form on the roverse side. crutH rs Grab sample in the Clocks above for each parameter requested 0 j F a FA60022: Chain of Custody Page 1 of 2 70 SGS 8 of FAe0022 Job Number; FA60022 -Client ENV. I 'Date l'Titpe'Received:.:1218/2018 10:00.00AM. DiflveiymeiliPq: Alifillift: '�00,1890710BOA0328ii6(j46lit669"267 ------ - Fx tih&id ID: IK I'; The . m6N _6.2;: # of Coolers: 1 Cooler Temps (Raw Measured)`C: Cooitiiei:bm; qdolei Tempe (qqftedod) IC: 'Cp6leeI!A2.0);. �oolerlriforritatiori-Y or jai6i)16 Iniatiliation Y, '--or' A I Custody Sebfs Preseht !� . O ' 1.. Sample labels present on battles - �' 2., Cuisto'dy-Seali; . I I rilact '2. Sarnpl' d'Oivp6 Pti Oqi� W 3. Temp crit.orla-achleved 3,sumaiint votari-eicontalners recvd ior 044ysis: 4. IX6066 of -sample Intact 5._CboNIrm,6dIa Aca Lga-01, 5.,Sirnpl6,jrPi:i4d within HT 6. Dal . esfftbMDs,bn 601: match Sairnple Label m El Trl&BWimJc'Infojrmi'tldn or N 7: V0'6s have fiead;pace 0 I � Tri - B Ak irese6 1 14 0 - p '! P­ coo a 0 12 A Bottles receive or unsoecifi E) 4, Trip,Blank fisted on COC Q .0 EZ q, Composiffing ldstnicfibns clear W • -or S% WA. 1V 0; Via S01.1 Vits/eJars rceived past 46rs?' 0 El W f. 4� $' ollds, '4iir received?, e fvie-d?, & b 0 :E] E2 -6 sent? 12. Residual C 6rin6 Pi 0 11 Misc. Inf6iinatl6rV Numlik-of Ericores: 264iaifi 5=t3 adi Number of Field F(ltw, k6mberof LabT . H lte red Walk. Test IStripLot ild: 230315 pwio-42,., 2191113A Other: (Specify) Residual Chi ori ne . Test Strip Lot* Comments Rev. Mte =411 7 Tddliniclan: PETERH Date; 12MaOI8-.'10!00.00A RevidiWer. Date: FA60022- Chaih of Custody T-Ag . 62 of 2 f M 'r'r ITI r`sd�� 4.eC.:' 6 '.4 e+' ` -.;,Y } .� ; 'JR ? Y �"r°•.r �,•tra �s *�i t: 4 i4lq'hf' 4:�• - '� - � `.;: s' .. �'� ., Ism-� 1 CLl ANALYSES rA q �• .y. I r � ij;,� G , j �u 7. is y� 72 � i�.. l�y2 d �' �� �� {�1•.." L4 a ,y �F � � r�, � L'�il 'a"'! ! '� ' �K "tea ;�'�d�1",u. ,�.� ,•S a r•� .�}, __SGS,. Orlando, F The results set forth herein are provided by SGS North America Inc. e-H[Irdeopy 2.0 Automated Report Technical Report for Environment 1, Inc City of Lexington WWTP; 28 W Center St, Lexington, NC 636 SGS Job Number: FA56698 Sampling Date: 08/07/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard @ environment 1 inc. com TTN: Deedee Woolard Total number of pages in report: 13 ,tea a�,Ro Test results contained within this data package meet the requirements Caitlin Brice, M.S. of the National Environmental laboratory Accreditation Program General Manager and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), iL(200063), NC(513). NI(FI.002), NY(12022). SC(96038001) DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573). VA(460177), AK, AR, IA. KY. MA. MS, ND, N11. NV, OK, OR, UT, WA. WV This report shall not be reproduced. except in Its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SOS is the aole auth<nity foi mrth"ai, utl; edit_, -n:tti I nxliiicona: m to thi, document. Please share your ideas about SO t Inauthoriaed modification of this rellort is stnctly prohibiled. how we can serve you better at, �j Review tandard tents at: bhp://%vu F1{S-US.C'ustunxr('nreursgs.crm 1of13 FA5669N 73 Sections; Seeti6n tt Simple Summary: ....... ............. .... ...... ....... ........ ...... m4w; .. 6 3 Section2- Summary, of Hits ...... ............... .......... ; ...... ii� .......... .................... Sie,dion-3: Simi le Re4tilt.4 ............. ................ ................... ....................... is FA 6608mL SLUDGE 8A W—LE 5. ................................. ........................ .......................... 6 'Section 4: Misc. Forms....., ......... ...... ! ....... ............. 4.1:,Chain. ofCustody............. ........................ ! ............... ............... ........................... 2 Of,13: SGN FASPOS 74 SGS North Ameiica 1iic: Sample Sii>Yiimary E0ironment.1 I..Ihcr Job No: FA56698 . City of Lexinigton WVIITP; :28 W Center St,: Lexington, NC. ' Project' No: 636 Saffiple Gotlecteci Matrix Client Number- Date Ti&e' -B ' Received Code Type' Sample.iD FA5.6fi9$,=1.. 08/07%18 .14:58. SF 0,8%14/18 _ SO. Sludge SL:,UD;GE;AMPiE, .. . Soil samples reported on a dry wei&tasis unless otherwise indicated on result page. so S of 0 FASOM 75 S.44i' th ary-of Hits J6 Nuinber! FA56698 Account-.. EftNiifdntfi.ei'Ht 1,- Inc Project-. City of Lexington WWTP: 28'W CO-nt6f St, Lekia&nj NC :Collected: ',08/07/18 Lab. Simple ID' Client Sampk'll).: -Result/ Analyte- Qual RL MDL Units Method FA566984 SLUDG E, SAMPLE No hi6 Te'pbrted w tfiis.'. sample. 76 NO I of 1 SENA! 10,13 FArSSFJM SGSr- NpAg Orlando, FL z=z Section 3 Sample Results Report of Analysis SGS5 of 13 FA5Gc9sJ 77 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA56698-1 Date Sampled: 08/07/18 Matrix: SO - Sludge Date Received: 08/14/18 Method: SW846 8260B SW846 1311 Percent Solids: n/a Project: City of Lexington WWTP; 28 W Center St, Lexington, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 J0993718.1) 10 08/18/18 16:23 SP 08/16/18 14:00 OP71367 V_j6017 Run #2 Purge Volume Run #1 5.0 nil Run #2 VOA TCLP List CAS No. Compound Result HW# MCL RL 71-43-2 Benzene ND D018 0.50 0.010 78-93-3 2-Butanone (MF.K) ND D035 200 0.050 56-23-5 Carbon Tetrachloride ND D019 0.50 0.010 108-90-7 Chiorobenzene ND 1)021 100 0.010 67-66-3 Chloroform ND D022 6.0 0.010 106-46-7 I A-Dichlorobenzene ND D027 7.5 0.010 107-06-2 1,2-Dichloroethane ND D028 0.50 0.010 75-35-4 1, 1 -Dichloroethylene ND D029 0.70 0.010 127-18-4 Tetrachloroethylene ND D039 0.70 0.010 79-01-6 Trichloroethylene ND D040 0.50 0.010 75-01-4 Vinyl Chloride ND D043 0.20 0.010 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromolluoromethane 102% 83-118% 17060-07-0 1, 2-Dichloroethane-D4 105`Yo 79-125% 2037-26-5 Toluene-D8 98% 85-112% 460-00-4 4-Bromofluorobenzene 97% 83-118% TCLP Leachate method SW846 1311 MDL Units Q 0.0031 mg/I 0.020 mg/I 0.0036 mg/1 0.0020 mg/l 0.0030 mg/I 0,0026 mg/1 0.0031 mg/l 0.0032 mg/I 0.0022 mg/I 0.0035 mg/I 0.0041 mgll ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 78 A ,ri59t SGS North America Inc. Report of Analysis Page I of 1 Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA56698-1 Date Sampled: 08/07/18 Matrix: SO - Sludge Date Received: 08/14/18 Method: SW846 8270D SW846 3510C Percent Solids: n/a Project: City of Lexington WWTP; 28 W Center St, Lexington, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 X062123.1) 1 08/21/18 00:48 MV 08/17/18 13:00 OP71401 SX2576 Run #2 Initial Volume Final Volume ;un #1 100 ml 1.0 ml :un #2 ABN TCLP List TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 95-48-7 2-Methylphenol ND D023 200 0.050 0.0056 mg/I 3&4-Methylphenol ND D024 200 0.050 0.0098 mg/1 87-86-5 Pentachiorophenol ND D037 100 0.25 0.050 mg/I 95-95-4 2,4,5-Trichlorophenol ND D041 400 0.050 0.0074 mg/I 88-06-2 2,4,6-Trichlorophenol a ND D042 2.0 0.050 0.0075 mg/I 106-46-7 I A-Dichlorobenzene ND D027 7.5 0.050 0.0050 mg/1 121-14-2 2,4-Dinitrotoluene ND D030 0.13 0.050 0.0081 mg/I 118-74-1 Hexachlorobenzene ND D032 0.13 0.050 0.0069 mg/I 87-68-3 Hexachlorobutadiene ND D033 0.50 0.050 0.0050 mg/1 67-72-1 liexachloroethane ND D034 3.0 0.050 0.016 mg/I 98-95-3 Nitrobenzene ND D036 2.0 0.050 0.0093 mg/I 110-86-1 Pyridine ND D038 5.0 0.10 0.020 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 22% 14-67% 4165-62-2 Phenol-d5 16% 10-50% 118-79-6 2.4,6-Tribromophenol 74% 33-118% 4165-60-0 Nitrobenzene-d5 62% 42-108% 321-60-8 2-Fluorobiphenyl 590/0 40-106% 1718-51-0 Terphenyl-d14 79% 39-121% (a) Associated BS outside control limits high. Sample was ND. ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank F.. = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound SGS7 of 13 FA56698 79 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE. SAMPLE. Lab Sample ID: FA56698-1 Date Sampled: 08/07/18 Matrix: SO - Sludge Date Received: 08/14/18 Method: SW846 8151A SW846 3510C Percent Solids: n/a Project: City of Lexington WWTP: 28 W Center St, Lexington, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC059159.1) 1 08/20/18 15:58 NJ 08/18/18 10:10 OP71408 GCC1335 Run #2 Initial Volume Final Volume Run #1 10.0 ml 5.0 ml Run #2 Herbicide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 94-75-7 2.4-D ND D016 10 0.050 0.017 mg/I 93-72-1 2,4,5-TP (Silvex) ND D017 1.0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 19719-28-9 2,4-DCAA 102% 39-135% ND = Not detected MDI. = Method Detection Limit J Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8oft? FA 5669N 80 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID: SLUDGE SAMPLE' Lab Sample ID: FA56698-1 Date Sampled: 08/07/18 a Matrix: SO - Sludge Date Received: 08/14/18 Method: SW846 8081B SW846 3510C Percent Solids: n/a Project: City of Lexington WWTP; 28 W Center St, Lexington, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 TT389243.1) 1 08/20/18 15:31 KL 08/18/18 08:30 01'71407 GTT2175 Run #2 Initial Volume Final Volume Run #1 100 ml 5.0 nil Run #2 Pesticide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 58-89-9 gamma-1311C (Lindane) ND D013 0.40 0.00010 0.000022 mg/1 12789-03-6 Chlordane ND D020 0.030 0.0010 0.00038 mg/1 72-20-8 Endrin ND D012 0.020 0.00020 0.000021 mg/l 76-44-8 Heptachlor ND D031 0.0080 0.00010 0.000026 mg/I 1024-57-3 Heptachlor epoxide ND D031 0.0080 0.00010 0.000020 mg/i 72-43-5 Methoxychlor ND D014 10 0.00020 0.000050 mg/1 8001-35-2 Toxaphene ND D015 0.50 0.0050 0.0021 Ing/l CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 877-09 8 Tetrachloro-m-xylene 78% 42-127% 2051-24-3 Decachlorobiphenyl 69% 27-127% ND = Not detected MDL = Method Detection Limit I = Indicates an estimated value MCI.. = Maximum Contamination 1-eve] (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound SGS 9 of 13 FA566 8198 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE. Lab Sample ID: FA56698-1 Date Sampled: 08/07/18 Matrix: SO - Sludge Date Received: 08/14/18 Percent Solids: n/a Project: City of Lexington WWTP: 28 W Center St, Lexington, NC Page 1 of 1 FA --1 91, Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic < 0.10 D004 5.0 0.10 mg/I 1 08/24/18 08/24/18 t.M SW846 6010D 2 SW846 3010A 4 Barium < 2.0 D005 100 2.0 mg/1 1 08/24/18 08/24/18 LM SW846 6010D 2 SW846 3010A 4 Cadmium < 0.050 D006 1.0 0.050 mg/I 1 08/24/18 08/24/18 LM SW846 6010D 2 SW846 3010A 4 Chromium < 0.10 D007 5.0 0.10 mg/I 1 08/24/18 08/24/18 LM SW846 6010D 2 SW846 3010A 4 Lead < 0.050 D008 5.0 0.050 mg/I 1 08/24/18 08/24/18 LM SW846 6010D 2 SW846 3010A 4 Mercury < 0.0050 D009 0.20 0.0050 mg/I 1 08/20/18 08/20/18 1c SW846 7470A 1 SW846 7470A 3 Selenium < 0.10 D010 1.0 0.10 mg/1 1 08/24/18 08/24/18 I.M SW846 G0101) 2 SW846 3010A 4 Silver < 0.10 D011 5.0 0.10 mg/1 1 08/24/18 08/24/18 LM SW846 6010D 2 SW846 3010A 4 (1) Instrument QC Batch: MA15141 (2) Instrument QC Batch: MA15155 (3) Prep QC Batch: MP34206 (4) Prep QC Batch: MP34226 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) SGS10 0f 1' FA56M 82 SGS. Orlan Misc. Forms �7 Custody Documents and Other Forms Includes the following where applicable: - Chain of Custody Section 4 il of 13 SGS 83 I Environment 1, Inc. CHAIN OF CUSTODY RECORD W66" P.O. Box 7085, 114 Oakmont Dr, Page 1 of ■■■■■■■■■■■■■■■■ r uV NONE CH 1 B-HN •/ ��auuuo■■■■■■■■■■■ CLASSIFICATION' WASTEWATER (NPDES) DWwW '• ' w�w �■■■■■■■■■■■ — DURING SHIPMENTMELIVERY ■■■■■■■■■■■■■■■■■■■NNEVIM WMARS _ww NO DIVA lag &M — s " I PLEASE READ Instructions for completing thislorm on the reverse side. 1 " " reouesled. W 3 4 0 2 7 4 l � (xab sample in Iha blocks above for each oerameler FA56698: Chain of Custody Page 1 of 2 SGS12 of 13 FASS698 84 -.SGS Sample Receipt _Summary Job Nam6er..FA58688 COent: ENVIRONMENT 1 INC. Pro)ect:'636 Date'/ Time Received: 8/14/2098 9:Oft:00.AM Detiyery Method: FX A rbitl fa'a;: 10g1891731960b03281100439402213905. Therm ID: IR 1;- Therm M A.1;r #'of Coolers: -1 Cooler Temps (Raw Measured) *d: Cooler 1: (4.0); Coole'rTempS:(Corrected)'Cc ..Cool0-U(j.1); Crioler hifonnation " .Y :of' ' N " Saiiible Information Y or N " NIA . 7: Custody Seals Present ❑ 1. Sample labels present on bottles ❑ 2='Custw—,,Se- S intact . ® 2. Samples preserved property 0 ❑ 1.-Temp cdima achieved ® ❑ 3. Sufficlent volume/oonid1hers redid for analysis: ® 11 4; Coolei teirip'vedfigation • Gun . . ,4. coriifitiori'of eainpie Infect S.'(;Oler iriedie Bii S. Simple; reiaWthin tiT ®' ❑ 8: DateslTlmas/IDs on &&ma_tchSample•Label ® ❑ Tr10 Blank InfortnaUdn Y or N' NIA 7. VOCs-have headspaoa:, ❑ I, Tnp 8lankpresegt /.cooler , ❑ ❑ ® S. Bottles received forun_'sp"ed. tens ❑91, 2. Up Blank-9sted on COC ❑ •❑ ® 9. Coinpositina insWeUons dear ❑ Q W on 'S' - Nam! 10;Voa.So1l10ts(Jers;raceiJedpast 48Fi7s? ❑ ❑ 3: Type Of TB Received ❑ ❑. ® t:l:°G SoUds.Jarfeceivad?„ 0 1Ii Residual Chiorina Presair!? ❑ ❑ Ga M c Inforniatiun ' Pfumberef Encores: .2SGram 5-Gram Number of 5035 Fleld Wts: Number of Lab Filtered Metals: Test Stiip'Lot Ss , pH 0 3 . 23031$, pH•10=12. 219a13A Othor, (Specify) ResiduWgG 166e Test Strip L,ot#: . Cominents srAbgi Technician: PETERH Dale: ShV2618 9:00:00 AM RkDela OWW17 Reiie r; P.H Date:' 8/14r2018" FA5608: Ch111I1 df C?1$lidDd Page'", mf,2 G . 13 1if -13 Fk5669a• 85 Environment 1, Inc. t- rinAIN Vt' CUn l'OL Y RE4-u D P.O. Box 7085, 114 Oakmont Dr. Page 1 of 1 C;reenville_ NC 27959 environment 1 ine.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 •Fax (252) 756-0633 CHLORINE CLIENT: 636 A Week: 10 pHCHECK (LAB) Ij UV G G G G G CONTAINER TYPE, PiG 'ITY OF LEXINGTON WWTP NONE AS. GISELE COMER CHEMICAL PRESERVATION t8 WEST CENTER ST. LEXINGTON NC 27292 A A A A A A - NONE D-NAOH E o 336) 357-7889 z w w z LU 9 t B- HNO3 E- HCL ¢o o 0 �Q t z a w W LU C- HZSO, F- ZINC ACETATE/NAOH COLLECTION J a F Fo o �a CL 8 W tc P4 E✓ E- v F v F J E- G- NATHIOSULFATE ii SAMPLE LOCATION DATE TIME m Sludge Sa ple 8�/i//� 2: $ � 4 CLASSIFICATION: WASTEWATER(NPDES) //� l0(o z f gf7�/�(Pl'� �02 y ✓ ✓ •� .� — R, Ile DRINKINGWATER 00 DVVGGW ❑ SOLID WASTE SECTION u-w- s 2/7� fj 2 pyr, �3' y -- /mow& zvPft a/7 , Z:SXPrY► (�D 4/ ✓ ✓ CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY N SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB AT 0-3 °C RELINO RECEIVED PY (SIG.) DATE(11ME COMMENTS: �(S�IG.)(SAMPLER) Q�PATFJIIME RELINQUISHED Y (SIG.) DATE/TIME RECEIVED BY (SIG.) DATEMME �- 10 =0a y: Zo RELINQUISHED BY (SIG.) DATE/TIME RECEIVED BY (SIG.) DATE/TIME w PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a *T for ND 340274 °O FORM #5 Grab sample in the blocks above for each parameter requested. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Lexington Regional WWTP Compost facility WQ Permit Number: _ WWTP Name: Lexington Regional WWTP Compost facility NPDES Number: _ Monitoring Period: From 1/l/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed; WQ0001318 NCO055786 Class A: Alternative 1 F1 Alternative 2 ❑_ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Altemative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost El Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion ❑ Anaerobic i b c Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ot Excee dences Frequency of Analysis Sample Type Analytical Tech - ni ue inimu Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CF27 1000 mpn per gram of total solid (dry weight) 2 3.96 189 mpn/gts 0 34/yr g multitub Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (AIL Stabilization ❑ Alt 7 (Drying - Stable) El JAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) O "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Tom Johnson Water Resources Director Preparer Name Title (type or print) v-- Signature reparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date 87 DENR FORM PVRF 503 (12/2006) Lexington Compost — Certlflcadon of Exceptional Qnality Permit # WQ0001318 Date: d • l.7 - I? Certification Period: From JA•h% a01$ to e C oo 1S Vector Attraction: Method # Ee�fails Class A Pathogen Reduction: Time/Temperature certification: (see records on file at the WWTP) /fails Coll form: (All materials are less than 1000/gm before released for sale) fails High Quality Pollutant Concentration Limits: (see attachment) meets/fails I certify that per the above that compost marketed and distributed from Lexington's compost facility meets the requirements for an exceptional quality material. r Sign: Print: C , fJLC� ?�C/ "L 'd d7ZT Title: Chief Operator S Print: JQ(An Lo, K!Y Title: Compost Supervisor Sign: Print: Title: ORC Sign: Print: o fit Jo h +moo n Title: Superintendent Sign: --Avle-J' Print: E�_n n 4 ,'newoL Title: Lab Supervisor/Pretreatment 88 .. rue ow Lone : � Date` �•- _ .... Tiaie:�'� ..- .- - � .� ,S= . .:�' _ - - .: - - ; i'atl�cgenTest=18ffi 221E: ivlPl+�Fecal-coli#'czaJ iaa l6x, ---: ?Nindeu/lOtis . � � '.. ' - - ' . �� �� ya1u���a •d�,'.amlids test�i: - � . - .Z `F�cat•CclifdmDe�sity:�__�_ ,;MPN1gT3.: .. • . Tf►e Iarge�t-�ao% is the.1a�gcst saa'�pT� volame °tined iri . , deteimiam� - the:MPNvgine,a .tbe,volnme.nsedu►the. • ,� .1QOnTs . /3; - .:. � .. • � . .�euatyms: If g/o:d� ssands=:75°.�0 iise�;i�e value 75�ia'ttter#'osm1� . • ... • . , US - ._ . ' , :.. . , lJe�tde BIIc •' _ Pa�ive�Hik�._.(1 � .. .. ./1 The.above 0 ' an is -to the best ofmy..-' edg Signed": ,• - .. . ,. -: • � � }2evaeated;by :.. .89'. . 90. :. Lexington Oegional'Wa.stewaterTreatment Plant City of LeAkiton, r1birth Caroiina �IQ00013.18 Ubaiatory Wo*Aeet For CompostAnatyses �ATiIPT F in :Batch mfg date(s). ! Collection of Sample Date Analyzed: . Aaalyst(s): Location: Bed # /d Pile Date•. z %3 hr Time. d 23 ivI ijrp . Pathogen Test=186� 3221E wet *i i' t Dish weight - gn . _ 'Sample -we" ,6; . 0 � 2.,.n to ,g i aY — lq,OmLs 5 1.OMUS /5 ; O.IMLS s -jV1pN T; N Fecal ailiform/gram 10 X: r< Z-- w' M in4Mgj 40m1 _I:ar�est voluaLe.x C( %' dry solids tested Fecal Colifamm Density. Z M SU- The. Iargestvolume, is the largest sample volume used in determining ille hdpN value, not the volume, used in the, analysis. Tf % dry spuds = 75% use the value 75 in'the formula ,not .75. AlmediumiLot#503Q`j�jSDmemlxed-c�. $:vH $-� ofDonblastreagth Date Auto a i $ pH „� ,� of 3ingie sfPeagth Nogetcve Hlk_ � /1 Po�ttivo H1k S /1 Jn3s'CDate=�T�moIn a�•20 •.� y-:,'Z ' z 'Daik +� Tuno oat_ . `� �.lo calms Total Solids - IEP 25400 - pH Dish # Wet weight: Blank Sample Dry weight grams, crams Dish weight t eiams 114 6oltds : Yn oven Dade A41 .Time Oatofovehbna ' Time. I! 1 O Notes:. The above inf ` ti " is G o the best ofmy knowledge: Sighed Date: Z Signed• 1 Date: Reviewed by. 92 l �ngto>m Regional f7Vastewater Treatment. -Plant City -af Leeringtbni North -Cat. d ina W00001318• Date�,arilyted Laboratory Wotkshect For CompostAlsalyses AnaiYstis}: a Batch mfg date(s) Collection of Sample Location: B,ed ##: - pile 4 . Z dy done .# Date:: /3 . /. dime: ` 29 ARPM 'n'P� r•A� Signe _ Pathogen Test -.1�'� 9?21E •MP'N l?'eca� colfona/gra�lO x '�2—`1�iiPN index/] OQni1 16 Largest volume x 5',0 % dry solids tested wet v fight t Disli weight FeW Coliform DeaW. Z— A' M9TS _ Sample wei 0gul to iaiiiter The; laigest volume; is the largest sample volume used is determii ft ti c MW value, not the volume• used in the. 10.0pLx' 4 /5 analysis. If Jo dry solids = 75%use the value 75 in the fozmale LODES 0 /5 not.75. 0.1mLs �5 p `_�. A I tedium Ldt# SO ate�iued • dl � $ FH i1 . _ ofDonble r�+erigkh Data. Atrtoelaves2 pH of Single strength Negative sIIc I Positive Btic 5 jl WS-bMt.A Ti. N.L. 10 .. T.- 4�st N44-CDate —A Tune Oat Z Total Solids -18d 254OG Dish # sample Wtt •weight Blank t 15 Dish weight grow soar Solids An ovm Ij da Time 1 + _? • OatofovenDato T-aao fl1 0 Notes: The above inf tion is i:on'ect to the best of my lmowiedge: Signed Date,_Z Zf Af signed - Date o`Z Reviewed by. 94 Leaiingtor Regional Wastewater Tieatmnent Prat City of LWn' gton' North CArolina WQ.0001318 I,Aoratory WorksiieetF& CompostAnalyses .DateA�alyr�a: .•2 .� .L Aaalyst(s�:� Batch mfg dates) _ter .Collection 4Sample. Logation: Bed Pile # Z d3 Zoile Date•. . /,S' / Time- - /7 Ivt Type• 6 ewedi Pathogen Test -:18m' 9221E MFN Fecal colifoanlgram U inQ b ` _ Largest volume 4 % dry solids tested Wet*eiglit em Dish weight Feca1.ColifoamDewity: MPN/gTS Sampl. we` to water 1 ' The largest voltmae, is the largest sample y6lume used is determining the M V value; not the volume used lee the IO.OmLs : 0_j5 a*ysis. K° o dry solids = 75% use the value 75 in'the fomnla. 1.QinLs �5 not .75. O:lmrt.s,� 5 PN A=1 LoL# D �4 �temiued_s�s. R ofDonbleshrwgtli Dato Airtoelaved o2 p$ of single *mgth Neptive Blk l PosWm Blk I833°CDatoTimoLtij�limo0ut � ; 4S BiMIC Dato 9 i5mo Ia 3: Dato Tim, Out La Total Solids -18m 25400 PH Dish il G Wet.weight Black Sample Dryweigbt Qrams Disci weight gramgems ! MR:_ Solids-laoveaDatn A g. 'Time ouiofoves►Dato Tuno / '. .. Notes: The above" on is co to the best ofmy knowledge: Sign / Date: Z E / Signed' Date,• Reviewed by: 96 Leaim ui�i � " •'onal Wastewater Treatment plant Ciity oiFLenngton,:Nortti Croln► Q 18, �; .;c -z i �V 00013 ... . � - . � � � Date Aua'lyr�_ :..• Labcy Worlcsheet,ForCompoSEAnalysea� . - � 4aatyst(s7 - .ems z • � ;:Ilion;: Bed # it .�2v� .. • ... .3 • Pita #' •ZoneYPC PatLogea est � 18`! 9221E. ' Mm Fecal. I a�/gra 10' x :%C 'NIP'N •volume "�,� : 5 .%o ;dty soli,d`s'tested Dislvyei�: • ga i�ecaTGa�iDeasily,. -- � �_GIt�PPT/g't'S . • ta��`- ,�° _wale ' :. � � • ,... " • � . • • .- ::Thelargest volnmq:ie8ie Ia m 0:se"u. vo om� peed in - . detiea�ini� the.MPN.vatue,�not-tlewoltuni� _used ia'tiud " IO:tfmi;s'-.:��' /S. analysis: If °1o.diy solids a'.75%:nse ttu'e: vi�lue 73 iii�lti0 fo�la:. • not 75:: OaaiLs. N,. IS:. . Aptoclaved:` 'ra �-of8ingi°sttessgtli' . . :NogetvaBlk ..0 riro°'sn�i5_Ji ..' . ig35.;CDate� .�`S Q .TmtoYn ��2��fS..;Tam , __ 3:: 5• U44*0ma i.lu.TnimltiL � ' ��S Da2e iaia'Oot . I �:dO. -,Total Solids :� :18m Z54QG :. • . wet Dish s � _ Lexington Regional Wastewater Treatment Plant. City of lop to, % North , Carolina . VVQOUQx3f8 7,abaratory WoikshcetFar.ComgastAnalyses Patch jbfg &($).— Collecoon of Sampid Location: Bed Pile#. 0 3 MP'1`T.Fecat califa�au/gram'lU x � � MP'N index/lbi)tul.' _ ,_ �t� Latgtst eolumeL, 4�o dry solids tested -Fecal Colifam.Density: L .AeN/JS . i�ate.Ana)yze . Pathogen Test -_Ip. kilp, Wet weight sm Sample weigh 0. 0 0�9 to .qp ,m vvater. lO;OmU, P /5 1.Omi.s OAMLs S_J5. -I Zone # . YP Ike largest volume, is the largest saingle vale -used in iletr xbft the LON value, not &e volume used in the nnalysts..Tf %.dry'soft =.75% use the value 75 in the fomula not 31 A 1 madh= I:ot # So 30 4 5 Dais mixed pH = J ofDantile strength Date Autoclaved a.7—' L S jH ,e J ofSingle stcea�tli Naget vaEk 0 /i PoutivaBlk5—i1 L►9sc.Datn-3 .Z � Time '!'� TSmooa���t ��3!,� S In 44•C Darn �' g mum n 1 S nate„�/_y/a Time oat /R'.. _0 Total Solids -18a'25406- PH Dish 0 G S. Wetweight emps Blank elo Dry weight , Dish weight QOrams *,a Solids - In oeea Daio OateavenDate 7[Sme�I 2 _ice Notrs:� The above infomoation is com .d to the best ofmy knowledge signed Hate:.- si Hate: Reviewed. by. 98 Rl Baiclimfgdates) -gf (441 1. , i A.I" 3 Ift Colleciiea of Salriple. .. Y:ocaitiori •.Bed'#'. Pa4hogea Test - i P 9221E Lav Fecal iafomiL=6x-' G % MPATindeir/IOOr'aolimlj�fX :SS- ..%a:drysoft UmW, Dish weight Fecal C6umm Dea4 ty. L j MPNIg1 - Sample ., .... ...: Tate: ;:?te,the ie:8est• Ple vala�a�,'�ase� in: Al A /S ieiy is: If°lodrya6 =75%o':usettewatue:7S;iu.t efoimula _5 U�lmis� ��:-. 15 'A 1 �iadivan3:yi# 0 atcu�iued . Z bH ofDaiuble talrmgtli: ' bafeA.A"vad'. 3'a Q.D ofsinglestcu* ' 7n35'�Data• � Tsroe7q•..��10�Tnae;:`. 3;stS �4,�cnate T166b 1. . Totel�Solids_=18� Z � .� Dish`# �,0.. .Wet. Sli3* ' ' ::. Dish vVeight solids-inovenDade .� 15me ,j� �.!�'. ' . .. � .. .. • Outofav«i-D>td `Tie<e�a`.4.� • Lexington Regiogal WMtewat& ThAtment..Pl*. ' .. G�tp ol;ea�ngton,•Ndirtth.Caroiina ... . ' _ '' . W000.0,1318 Date..Mtyzea:_ jl Lalioratoiy.WoiCsheet Far CampostAnslyses :. Aiislyst�sj: Batchmfg date(m% . a, -- M.- S doll ectioa44amm e.. I ocaii=. Bed: # .:11 ' Pile;# 0?9 3' Zone #. ... . Ikite� .o� •.1 Timq. .;;•i'1(A-. �ypM' � .Ty'pe� 'iM:b ' Sigaai: Patttogeri'Test�l$'�922YE F6'wi orin/ rlO:xG MINindesr/1Q0iii1.. . ' iergest.voliune a , �{5 • .. % dty solids tested �Vet.wenght " - Dis�'aeigtSm :Co]ifcmoo Densty.1N�ff9 . 38mple Tine lagest valume;:is flteasrgest sample valpme used is detesmi�.the MPN velue,.not.the go�ume used in the YO:QanI.s, �. 5 analysiv: Tf edLydo, 6 = 7S%ilea lhb'vatue 75,% the'famlula A 1 mod'nimLot#$034 • -5.b, jmiyed. 3 itiuoaii< '° ofsingle ') ATogativaBlk_ /YPautiveBlk /I Ya33!CDate aue7n '12. f � '1"nae0at . �� ; f'S . In44'CDate •' Timela `� •' r • �odj2 ?d Total Solids.,= Y 0i 2540E Dish`# Cam.. Wet vyeight Blankgrms $ample ITMTMh���'LL.weiight•'pam �Soltds•7n'ovdtl?IItP• � iJWa 11�30 . 100 Lexington Regional' Wastewater Treatment Plant City of Lexington, North Carolina WQ0001318 Laboratory Worksheet For Compost Analyses Batch mfg Collection of Sample Date Analyzed: i U Analyst(s). Locatiow Bed # It Pile # soy Zone # `l �,�' I'� • L bate 4j$ Time ' 33 Type: ,i%� Since Pathogen Test -18- 9221E wN Fecal colifarnm/gram=lox wN index/100ml —10_ Largest volume x (! , y % dry solids tested Wet weight --gm Dish weight Fecal Coliform Density --4 Z MP 9TS Sample wtt 0' 'C to 4jQ_mLs water The largest volume, is the largest sample volume used in determining the MPN value, not the volume used in the I O.OniU ?0 /5 analysis. If % dry solids = 75% use the value 75 in the formula 1.OmL.s p /5 not .75. r O.l mLs �5 A 1 —di, Lot # � v 3C 9q mimed `? ] J f t `O - p -� ��—�N t� of Don61e atreugth Date Autoclaved S l i pH of Single strength Negative Bik h) /1 Positive Blk J1 Ia 3PC Data Time Ia �'. �" I-mw Out ' 20 In 44•C Date , Time In L- D DaQo s r Tim Out r', a Total Solids -18" 25400 PH Dish # 21 Q sample , 'L Wet weight Blank Dry weight Z-- Dish weight Gowns S. LI Solids - In over Data S b Tmse f '. W Out of oven Date Time t sue' Notes: The above infolmatiota is cantct to the best of my knowledge: • S,Is / , y Signed Date: Signed: Reviewed by. 101 Lexington Regional Wastewater Treatment Plant City of Lexington, North Carolina WQ0001318 Laboratory wor Wuwt For Compost .Analyses Date Amat rm& `J 1 g .Analyst(s� Batch mfg date($) 3/�a !� / 3 �� ►5 Collection of Sample Location: Beni # Pile # AJ Zone # Date: t!At /6 Time: '• M Type;_ Pathogen Test -18" 9221E b4PN Fecal coliform/gram=lO x.-e2 MPN index/100ml �rO Largest volume x,,�$. 2 - % dry solids tested wet weight gm Dish weight tmi L Fecal Colifam Density: )"N/gTS Sample . towater The largest volume, is the largest sample volume used in p determining the MPN value, not the volume used in the 10.0m1.s 5 � analysis. If % dry solids = 75% use the value 75 in the formula 1.OmLs not .75. �' O.1mLs� S N a A-1 medal- Lot # mind S � pH 'x• I of .M..h gth Date AuIa,-.d s1 'j pH _ of Single strestgth Nogetive Blk pwithm Bnr 5_n ICJ �1 In 35-C Da. Time ��. O Time out In 44T Date Time In—L�2_ Dale 5 Time 04 1 ,-,C Total Solids - 18'" 254OG pH Dish tl 61 > Wet weight Blank e Dry weight Dish weight 5grams gram 3s,z:/ Solide - In oven Date 5 Time to ! `i 10 Om of overt Date Notes: The above information is correct to the beast of my knowledge: - Signed: Date: j -- s-A fis Signed: - ~ , Date: l / l g Reviewed by. 102 Lexington Regional Wastewater Treatment Plant City of Lexington, North Carolina WQ0001318 Laboratory Workaheet For Compost Analyses Date Analyzed: g Awlysgs): Batch mfg date s) ,Z 1,tP IJ ri-- Collection of Sample Location: Bed # it Pile # Zane to Date S ht iftWpm Type:_ S' Pathogen Test -18" 9221E MPN Fecal coiiform/gram=lO x 'C2--MPN indcOOOm1 0 Largest voli % drysolids tested Wet weight gM Dish weight_ „__gm Fecal Colifolm Density -.e2 MPN/gTS Sample weigh ' to water The largest volume, is the largest sample volume used in determining the MPN value, not the volume used in the 10.0n,I.s f ' 5 analysis. If % dry solids = 75% use the value 75 in the formals I.OmLs —E-J5 not .75. O.1mI.s A-1 modicun Lot it t 3019 5DW. mined 5 ell � pH -* -L dDoublo ,U gth Date Antaclaved J t PH 4 of single sveagth Negative Bak /1 Positive BIk 25 Jl In 3 3°C Date 5 Time In, J2_ Tines 33v In 44'C Date , Time Ia Dates JETTime OutIW Total Solids - I P 25400 PH Dish # 14 SampZ Wet weight Blank 10 Dry weight FwaMs gram Dish , grams —grams . 523 Solids - In ovm Date Tads ' Out of wen Date Tiros Notes: The above information is correct to the best of my knowledge: • J (� /� `�` sib Date. f 3igned�C.� Date: �_ Reviewed by. 103 I;eaineton Regional. Wastewatei Treatment Plant City of I eafngton,'&rth Carglina W�OOb�318 Laboratory WorksheetFor Compost Anai = Datch ba% Collection of SamPle bate anaiyea:.. location: Bed # Pile # ao� done # Dstt• 5h0 Time .. � TYIx`, - Pathogen Test -10 92 1E MP'N Fecal. CalifoM/gcam=lo : _ 2._ MPN indmd QQMl I;sgest volume X S ®Jo dry solids testeii Wet weight Dfih*eigm Fecal Coll q=Densz{y: Z MPN%gTS, Sample to sister The largest volume, is the largest sample Volume, used in- detecmining.theNOON value not the voltme.used, nthe 10.0mLsJs analysis. If °/a dry solids = 75% use the.vatiie 75 inthe'farula 1,Oms A %5 .not :75• . 0: L lyp5 p,1 qq ,h f r pH i _.ofl -hie _*-9th -� A l meann1 t# SD'30 _pat..n�boed 5 g: 9 Date AtitocTaved. 5 4 L g p4 0 of Single strength Nbgativb HlkPoaiiive E k Ia35-CDala-5'O T�. In fA i Time r :t S In44TDatoS o g Tynera3`.t-5 Dam51 /2 T*oot f2 Total Solids -18" 25400' . PH Dish ff Wet weight 9-L, 2.1 Blank Sample Dry"weight Dish weight : $ Solids - Ia ovenDMe L Time l l ?_f s OutofdvenDate Tim' Notes: The above infoanation is com d to the best of my Im6wledge: Sigted• Date: 10/ r Sighted Dgee Reviewed by. . 104 �;Coliectiaa of Sample .. .. � • . ,.Lacationz '$ed. # . l.f. Fite. #- � `:Zane;#�• - .. . :� : lD �1., _ � �:.:.: �= :3'1:: i;i .: •gib � • . spa:. `.Ra$t►gea.Test-.1$�_�221B IyJPN,Fecal colifoimUgcaa�=1O at, •�2 d (�;Q��, • .. . . '$b.:i2iy'sands tesbei, vYaciiit mn -Dish �►�ei` gm .Fecal colfoaai Ieasitjr •C Z 'N�g'g iMP..isti�zt`:�im���a� aet liar zrt;;: tn% in. IO.Omis '' /S'.di�'solid�rse:ilic;.Yalrie"75 the jtf Varmuls. l:OmLs .' 15.. nct75, A 4*0 • ,Dste.At}tOclavbd- �� D '71 ' . p8�•o€Ssaglo:nttm�i. km 8� .q.4 Collec?ion of,Sample � � � . � " : • . • � . ovation:: Berl # .. _ f .: • Pile #' . �e� Ana®#".'• . Date: [0' Time: �' IVd'' .. � •., . '::�fa .' .Signed• ` Paf2toged�I'esf=,38'9221E N1P�1Fcat— tOZ•iNIPN:inder%ibOml' ;.. Wet wei . _ :. .. .., sm:.' . - • , _ • � .. - .. . . : gm Fecal:Colif i*00sity:.:.•C Tiie:laigesti-dl ist6elaigestsampkvoinme_itsed:ia.: . detamining.lheMFN�value,.aot.thevolwmensQd.mthe . 10;t)uils. - /S : atti�ly!sis.:If%,y solids_. 75%'pse the :value 75 iu tht Yc¢mula . `1N A=1.�#.'�c0:30:9Q5Dsteinired. to � g$_�.ofll'cuble&ttcng�h' Aiitoclav�d ff 'Q• �. Date ..�� ' lJ i•� , . . ,2�<. - ' :: Nog6tivaBIIc � /1PositiveBik-: :5�' �l' : � :: ... � :Yu95 CData'(�TSm�e, - . •• �� i5. _.T�ma,0oit:�.3 P f � �. , .. • In4�s'C.l�te• � T1a�e 3' i • �•Date'S 15me . • .. 2,. ., -, Total Salina = l$°i:2540,G .:.. P$ , ..oxi- W ..S' et' . . BIB* . . � . �e�� Dryweight � gams` Dish weigh S`.: 2�3 ; soli, -!!lao igg ER, kwtefs Compoy Cerfifi,qatdotAnioly'sls Lot No. P267-084/M26740A Certification Par-dmvior C6111iled PiTO16 -A (Whilbrane Filtration). utardoillopm - , Oacardo,14forhis Ecoll Total f6rMb ViC*a*i. Cb L.Poil- Sample �•A (SM- 12211) T&W.Collibrms 'F I J, Totalt ulkorms I cal Coliforrns Aha'1001 Vedfloafloh Par.pMet6r. Sample•A (MaMbrans Filtration) .Total Fecal-Coilf6rms E Coll Sample - A (SM-9223) . IfOnlf TOtal.00.1 I S. Fecal Collfofts Samp!q;- A (SM-9221) Total-,Col06rrn's Fecal.Wlforrns Emil Value, CM1160iTiL 709 636 1300 1310, MPNhO6ML 882 0' OFU m il�oikL rl Ceitiflid CFUIIOOML 1080 fog. 836 MPNIIOOmL 1300 1 180 1310 MPWIOPiPL 882 8?6 810 Wastewater , Coliform' . Mit rdWm Citalog No: 089/08!k "u"'Date-.' July 24, 2017 Z Revision biti. hial 060 Lincerw6liv :.QO PerfoOnz nce PT Oirforkn4mi Acceptance4 Acceptance Litniteg Acieptiti Lunitim! =11166MIL CIPQ11100MIL. ',2Q%,,+265% 466-:2340 '655 -.2-666 718%, +22-4 2142346 1013 =2dk +144/. 3002336 460 -J760 MPN/IqOmL r2a%.'tjq°!u` 483'-'3506 6.68 r,2530 O%ii, +29% 30'5' 4576 _. 595.-234Q 4M, -30A' 658 -Add 686 -. 2490' MON1100m, L Mpkilb.cm-L -21 %,'t26% 176 1 64420 161 77,06. -211;�, + -/6 -140'r 4`600 7350, r2064o,'t266/6 I9D-'--.3446 .Prqflckincy Testing Study , 084o kic'O.V64Y 'lA n b!qanIs.M IdPntlflcatlon' OFIL1111100mL 4060, lob 38 EscheridfiI6 c6lij* ATdC.5181 3'. 760 IM 1,1 ts cheirichip call, AT'C'Mi 61 3: 836 100 26 - Eskliekl6hiaboli. AtCP51813 MPNIlOOmL 1:du Idio 80 E6chedqhla'.foll,'ATtC51813' 1190 160 82 Eschirichia soli; ATCCM M3 1310 160 1118 E scherichla coil, ATCC.5181 3 .882 100 53 Eschedchia soli,ATCC51813. 8216 1-00 64 Esclie�bhla coii.&CC -51813 810 100, , ,1,6 5 & t serichia soli, ATC61,848 dFu =-CO104 Forming Units; MPN - MoM Probable Number. SM-9223 = Mulitiple,W611m6thdds w/Enzy.Mb,Substtate-Medl6. SM-'9221 = Multiple Tube Ferri eqtition methods. ­ this product• is sold upder,two diffeirent Catalod and Lot t numbers. b I ers. The Catalog and Lot.Number that . in.ah Avis for SM-9221. Ferrilentatioh methods). REFEPJuNC9 MATERML PAODIJ '.q R . _ 1641 Table MouW n Pkwy,Goldon'COO 80403 BQO-3��4122 fax (3 421415W Page 1 Of 2 108 Ll AmdyiKsY- SAIRLE ID .Bitchi C(dectidn qf 1ca4on:: Oed.#". zotie. Date:. Time -ype Sample' • rdaht, 46 fl min *a 10 aidu [oz. -Vo dry OfDmkblo A96A. Date X Blk ........... J, b:- I P'2S46G 109 ERA A Waters 6inpar'vy ala .,c 'l ifi 'cati? of Analysis LOOP. P208483/F26670§3A Expiration Date:' 11/20118 ;Certification Pafanieter Sample. w A (Membrane Filtration) Fecal Colfforms Sample - 9223) Total CQllforms Fecal C611forths Ecoll S00110!e A-(tMT92911) Total'Col-hrms Fecal C6111orms Sample-s- Total Colliorms Fecal E.coll Analytical WrifidAtl6n Parameter S' am rnpI�e - A (Mbmbrana' Filtration) Total Coliforms Fecal do4orms tcol Sarnp16 - A (SM-9223 - Total Colffdryns Fecal CbIlfbAns: Ecoll SampleL A-(SM-91211) Total C61fforms Fecal 601dotnis E.coli Certified CFUROOmL ISO 8.1 98 MPW100mL 168' 135 171 Joe t.�L— . IQ7 ' CFUhO0mL 'Certified, Xahie 61FINI00MIL ISO .81 98 MPN/1OOmL 168 135' 1-7i, MPW10Om1L 106 117 WAtte WAtor Coliforni MicrobETIVU COW!qg No. 083/08.3A. issuebato! August?,-2017 ' ReWOriginal Date: unc4itilfiltv QC Performance PT PeqprMqncp. ACC0ptQnC0.jLIMItSj.4- Acceptance�0 Llmlta C0011106ML CFUh00mL' 4.80*.+7t3% .23- NI 21 +8.'0% 32 = 296 24 - 396 MPNI00mi. ra.PN110*nL. +51% 103-27.3 80.5-349, --.31%+4§% =; 38A 474, 84.1 -216 -34%i +61% 94.6-309 86.0-34.0 MPNI100inL MPN1I00mL -'29%,-141% 28.6- - -SO2 --'966 400A. 43°A 26.6 -'61� 6:� .. 1.�eb +41% 30.1-38 1 1 Proficiency Testing StudyP Moan Rec.PV66 % A CFUIIOOML 150 i0b 15 81 100 65 98 Idb is MPN1IOOmL Ili 8 100 24 -135 100 B 171 100 53 MIRN11100611- 106 100 23 117 100 27 107 100 9 ZIFY = Colony FormingPnits. MON = Most Probable Number. SM-92.2.3 = Multiple Well methods w/Eiizym Substrate Media. SM-9221 = Multiple a Tube Fermentation methods. Organism Ideintificatipyir itschdrichle coil'o4TC.Q51813 is.he'richla 6o'll, ATCC51813 Escherichla coil, ATdC51813 Escherichfai coll, ATIbC6181, 3 Eschei ' ichla Coll, ATCC518-13- Its,cherichl'a c6li;ATCCS'181 4 Esdherichla coil, ATCC51813 Eschbrichia coli,',ATCC51 M3 Esdharichia soli, ATCC5I813 This product Is sold Under two diffatent Catalog and Lot humbeks. The Catalog and Lot Number that'bnds In an A Is for SM-9221 (Mu'Itiole"Tube Fermentation methods), nEFXRWct MATERIAL r9oDuczR CERT 0 1539M Isul TablaMou0Zn'FKWY Golden, GO 5.0403 P.ga 1 of 2 110 Loiiagton IUgfid®9" Wasik r'Tr ee®t Plant. City. .of:I niton9 Notfi Carolianai vvCtoaoa�is Labora4oryQvo*sheetForCGM0 *21ysm Ill -Collectidn of Sample I:ocation: �,ed #:. Pile.# _3 ZOiie # Date:. 4. "Y Tune: °/ Nt Type ,g14b Signed'S Pathogen Test-1801.9221E -MPN Fecsd cc�Ij om;/ 10 ic• = nW60001id Largest volubax• I®i.ty solids tested Wet weight. Mimi - Persl ColilFa®aa.Dety.' Z' MPN%gTS. gai Sa>aple to �pnL9:wates. • Tke lslgest voluale, is tl�:brgost sample .Polume used in deteanining tlie'MPN value, not•tfie volume.used in -the. lO.OmIs ,^%5 amalysis. if 14 ds solids =.75%o use the value. 75 iei tlae faaaula LOMLs 0..,/5. not :75: O,lm►s �- 5. � A 1 riudnzm Iat # ��0 30 g pnixed-- ��p& 8 ofDonblo shreogth DateElufocla . .: .. PH Of l�Tegatava BIIc . /l Pedfiva uk $___(2 Ia35°C Date Tuns In 1 !.. TSaie Oat .. y p� rn44'C Ddaft� 1, t_.Dsw ,aea oue •1'- 1 S Tatal Solids =186 2S400 PA Dish Wetiareiglit ^p _gl�nk Dinh*eeight trams Salida a Yn ni"m nA a Tim ' 112 Lexington Regional' Wastewater Treatment Plant City of Lexington, North Carolina WQ0001318 Labaratuy Wodwheet For Compost Analyses B.meh m% COUM ism Of Sample L,o.au m: Bed # Pile # 20 G Zone # Date:AO� TM0 �' Typq Q rah Date Analyzed: 6 • AndysKsk r Pathogm Test - I r 9221E MPN Fecal eolif� gnus 'f-2 _ 0 Largest vohtme % dry solids tested Wetweizu Dish vw gm Fecal Califamm Deasity: -G 2-- Mmgn Sample to �,Q�nLe watrr The largest volume, is the largest sample vohmme Used M ddtesm WW the MPN value, not the vohune mead in the I0.0mLs p JS anablds. If % dry solids - 75% use the vabe 75 in the fc®ula 1.Omu _Lf5 na .75. 0.1mLs5 A 1 medium Lat 1< � � �'i`.�b.me a�ed�� ..(? p�� afDooble strao¢h � �P'N DSUPH ruWt eeac o P*sMMk--f--A 1n35V Dame— TM 0 ' —0 nM 0d 3, 3 3 In 44'C Demo Tb= ' -O DemqjdL�dUs aU-' •uD Total Solids - le 254OG pH Dish # s,asple wet weight LI 630 nim Blank Dry weight --grams REMB Dtsh vrwe& i � � �—gram gram Solidi - In oVm Dstrl v TAr O �► Oat of oven Dste Time Notes: The above info iyo to the bead of my lmawledge: Signe Signed Date; b 6 l'g Reviewed br: 114 Leaengtot 0gignal Wkgt City of ][Ami mgteo, NorM,'Carolina WQOO.0131 Date•Aualyaed i abnratoay Wbrkshect For Compost Analyses A:gaiyst(§). RID Be#clt CoIIeatiion Of Stipple T.00atiom Bed :# . /l Pile #• Zone #_ _.'.. �.. 8= s9: pe Paft&(e i Test=_IP'9221E . .. MI'NFad COlippian./grdZIF=i0'x Z MPIJ.:u dcx/lbdial i,srgest.voluimex S' 9Smdrysolidstested Weimm Di* weigh Colif o Dpsity: 2-Z .11dPN/gTS. to s water. The:lacgest;volusne, is tba largest sample Bol a used in deteaaWng tli®1\90 vslug, not :the volume used in the 10.0m%s O_ 5 analysis. If %o: dry solids = 7MA use the' value 75 in the formula - 1.OmLS: not :75: O.1mLs =5 . _�llpN A 1 medium Lot# 3.0 mixed A �, ofDonle strength Data Autoc]uved • �-6 pil 9 of Single stnnA Negativa Bllc - ./0� 11,1 Positive Blk- � J1 7a3sla. to_J �mmeia,.1.2;�4TmceOut TiL WC Date' Yam' �Tssne Ta Dato mom' TdW Solids =18a` 2540G P$' Dish ,# Saiuple `' Wet weigbi Blank D1� weigiif grain's Dish weight b 'lit S 2'i- 5 3 Notes:. 116 • Lexington Regional Wastewater Treatment. Plant . Cif of Lexington, -North Carotin `v 000I31.8 Laboratory WmIsheet For CbmpostAnalyses. .SAI M.E ID 'Date.Analyzed; ... 2 . $ 1 Batchrafg date(s�. ' Couedian 0. Sample . L'6640n:. abed. e # . :?'��' . S done # Date: (�(. j Tunie::</2. .., .. ► Sr. 1?afhogen Test =1 Wh-k21E. Iv]IT+T Fecal wlifoxm7granr U x iadc l00m1 .( %® dry solids tested I argent volume . _ 22 •Weiveiglrt. em .. ; . • .. . Dish v�te_i' FecalComforiiDensity hI xlm sample to .� Up largest vnlzitue; is the lftdst`sample volume used in, &ter bft the MFN va W' not the *'CUUMO used in.tba . 1 OA i" �5 aaelysis, if %dry solids = 75 %use the value 75 4a the formula. -1.0119A- --/5 i<6t:75: :. w .. A1. 144;ld3c��nj Dare = eH �. of Doubleshrength Da.w.Autoclaved - PH •/J of Single &ength ]lTogetive Blk b /1 Pomt v.c BUc = /1 1105.-CDatcl lug In 44'CDde g "T"m�e xn.�. r Data . Time Oot % 9 T6id Solids = I P 25400 PH Dish#, Wetareighi gww Blaak Dry weigIA �`� -Frams gams Dish v6dIglit 0,. r3 .5 . a .ro3 i Sofi&4iovenDAO Oiit ofoven Da2o•Tiaie� 1 71- E- .1 Wastewater ib, De 114 OAKMONT DRIVE PHONE (252) - 6-SM N.C. 27858 FAX (252)756-0633 2D#: 636 A CITY OF LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. DATE COLLECTED: 10/10/18 LEXINGTON ,NC 27292 DATE REPORTED : 10/16/18 J REVIEWED BY: Sample Sample Sample Analysis Method PARAMETERS #1 #2 #3 Date Analyst Code Total Solids, % 43.41 44.55 45.89 10/11/18 KDS 2540G11 Fecal Coliform (MPH /gram Solids 3.0 7.4 8.0 10/11/18 KDS 9221E-06 123 -- ' �?�i+'::ti r�.�i'. �' ���t:1�'r�L:�s.� I:` -L_�Z�_y ��'.�•••`}S Z � a : . - �- . ." ,..+ �lv_:, �,0.`3 -A' _::k: •?_..-_.S.' � - -. _.rw,4�.+.� - .— _ w.b._y_�+...� - ,- ..usr,+_...c,..., :�.-•.x. ti 1....u.a.-. ar.-. :b._.,:;-,._ni. �; . i• _ ,. v_. _ '.fit•.._.... �. - . � � - __ .� 28; WEST (336j'3�7.18.89 [ 's' , _ `� ,► _ .••.::<._ . •.. � - _ ;,�. ;off:. � - - 1_�+•r,.+_,FIB(/J[� n� •_�._- // r.f, ^_Y�..!-.�•'____'1..w. are �:,._ .. .. .._r. -�: r • .... �.__.... � ..�.... - •. .. a._ _.�wvr•M�..�a _.mvb..: . r_ - - . v ..-H .. .•r. k'w•.f__.•_.aw.- . .. _.. __... au_ t a._rr .. _aK�. ,r. �__ • _ ... ..._ .-. •. r•w r_ . v _..._ , , •irir.•,w.. ,/!•+ef_..r_r_Yrrr._ .�� r.i; v.,+ .._.x w ., . _ ' _ -�__rn irk •_ r • � _� . � . a _ •.. w • .., _ . _w a • • .� • r - • y _ • f _ls .. - y.i+•r-u...oi-..1._�w-b _..,... _. � -.. _ .. v> .. _. w e ., u. _— • -, __ •.«- .• rf.. ..a :�.:_.--..—.> .-_.� ...._::..•.:..� - .c.. - - � - - -- .1 .. � u, -.-. _ : — i . _ ._ 1_.... ' f....,.,:;:�._:,•-�»tea:..: •_ .. ... .� � - .._ .. . :..._ ,........ -c .. - i, r-era:'-.:.� _ .-_...... ---•.�-:9 - . 0 _. R-.RC::itz;.irrt.�.;r�r�.,: ,fir � .i ��.:.,,i� a�: s.us �:, .• . #a�� «t�a:e°,.-��:, � U::.'t�i!LSF .•'�fM �i_•,iF.fiti '4 �'i•.`:'. 1'w�r `S'}:t�i.. C'i:.i-.%,: -.� �', d'.`_';' ��1'•. i•�'•trt:n - � i i•:Y'', J�'-aye .. _ - .., r N®�CiogBilt � n_.Foeitiv+oBUc•�fll.� 7a33!CDatoT;���. T�mla . • . . _ :'Ifdne,QaL 1. --iJ16Q'V���UUI! i I 1 ' i; - Yid ,i EJ;1� i 1_)1 ,1 "-- 3REENVILLE, N.C. 27858 CITY OF LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. LEXINGTON ,NC 27292 Sample Sample PARAMETERS N4 M5 ID#: 636 K urSnkItill wet aA XP Wastewater ID. 10 1:)CA t.; !;_i 1;) 11L 1l3.5 FAX (252) 756-0633 DATE COLLECTED: 10/17/18 DATE REPORTED : 10/23/18 REVIEWED BY: Sample Sample Analysis Method K6 N7 Date Analyst Code Total Solids, % 54.68 58.03 52.54 51.21 10/18/18 KDS 254OG-11 Fecal Coliform (MPN), /gram Solids r >1,9'�M' 159 2.1 87 10/18/18 KDS 9221E-06 Ln iP4%, ?nvironment 1, Inc. CHAIN OF CUSTODY RECORD ?O. Box 7085. 114 OakmonE Dr. Page 1 of .:11. xrr- 117RSR :nvironment 1 inc.com 'hone (?S2) 756' Szva *fax (252) 756-0633 CLIENT: 636 K Week: 4 Ty OF LEXINGTON WWi7 S. EGLANTINA MINERALI WEST CENTER ST. mMGTON NC 27292 � �_7� ��y�� LLECT COLLEC t M• CO DISINFECTION ❑ CHLORINE ❑ UVp#i ❑ NONE UiOFrIN>_ NEUT'RALIEDATCOLLECTION CHECK (LAB) P P CONTAINER TYPE PtG A A CHEMkCALPRESERVATION A -NONE D.NAOH B - HAIO, E - HCL C - H=S0, F - ZINC ACETATT:MAOi W c G NATHOSULFATE a E U 3 � J - a, Cr - F� 1''-' !R � ,� c tR g a tti SAMPLE LOCATION DATE TFk Sam le #4 b/rl/6 �' �� ��i, 2 CLASSIFiCATIM WASTI=IIVATER(NPDES) ❑ ORItW(ING WATER ❑ awaGw ❑ SOUD WASTE SECTION Sample #5 10%1 T IM 2 Sample #6 1 /T� 6 r d'A 2 Sample #7 1D�17,b 9 : lark 2 . CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY C) N SAMPLES COLLECTED BY: (Please Pnnt) ✓o/4-7 z� SAMPLES RECEIVED IN LA8AT °C R BY ( ) (SAMPLER) DATEMME 10/7 9 =aa► REC BY (SIG.) DATEITWE i7 r y zS COMMENTS: NGUI ) DA7unME CENED BY (SIG.) DATEJTM PaUNQUISHED BY (SIG.) DATEMME RECEIVED BY (SIG.) DATE/TIME M PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a -C' for composite sample or a "G' for T_ MAU 05 Grab sample in the blocks above for each parameter requested. Sir% ., � „ n e •, E[Mummumn % hmpmUd 114 1 Di i!Vi_ GREENVILLE, N.C. 27858 CITY OF LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS Total Solids, % Fecal Colirorm (MPH /gram Solids Sample Analysis Method #4 Date Analyst Code 52.97 10/25/18 KDS 254OG-11 2379 10/25/18 KDS 9221E-06 Drinking S. IB! S`171: Wastewater ID: 1) )HONE (2b") r aL lj-'.i > FAX (252) 756-0633 ID#: 636 K DATE COLLECTED: 10/24/18 DATE REPORTED : 10/30/18 REVIEWED BY: 131 avironment 1, Inc. CHAIN OF CUSTODY RECORD O. Box 7085, 114 Oakmont Dr. Page t of -=.._ ,..d- 't-70co . . �� � • u 1: 1. .. a1.i .... ., . ' 'r ' ' � , • . . NONE ■..■■.■■..■■...■ ��l.:�i .`� 11;:,►,� eta �•IL�.. 111 loss Emission I.. ee■■■■■■■■■�■■■■ . �.. . ee■■■■■■■■■■■■■■ ...r .E. .. . 8 HNO, E HCL C-H,SO, F- ZINC ACETATE/WH _ NATI-11CISLAYATE G - _. ....: CLASSIFICATM WATEA SOUDWASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURIPMMENT/DELIVERY SAMPLES RECEIVED IN LABAT '� ME I I I r 0,09 PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a'C" for composite sample or a `G" for rrnh camnlA in the hlnrks ahnvA fnr parh naramptPr ranupsred N® 355779 M CITY OF LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS Total Solids, Fecal Coliform (MPH /gram Solids Sample Sample Sample #1 #2 #3 Drinking Water ID: 37715 Wastewater ID: 14 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 636 J DATE COLLECTED: 11/28/18 DATE REPORTED : 12/03/18 REVIEWED BY: Analysis Method Date Analyst Code 33.75 4 .52 41.27 11/28/18 KDS 254OG-11 <53 5780 89 11/29/18 KDS 9221E-06 00c) 136 Environment 1,Inc. CHAIN Off' UUS1•()0Y khCOkl) P.O. Box 7085. 114 Oakmont Dr. Page 1 of 1 Greenville, NC 27958 environment I inc.com DISINFECTION CHLORINE NEUTRALIZEDATCOLLECTION Phone (252) 756-6298-�-F�(252) 756-0633 Ij CHLORINE CLIENT: 636 J Week: 4 Ij UV pH CHECK (LAB) P P CONTAINER TYPE, P/G 'ITY OF LEXINGTON WWTP ❑ NONE IS. EGLANTINA MINERALI 8 WEST CENTER ST. CHEMICAL PRESERVATION ,EXINGTON NC 27292 A A o A -NONE D-NAOH S36) 357-7889 z o La Er .� t B- HNO, E- HCL F o� O Z v°z w C - H,SO, F -ZINC ACETATE/NAOH COLLECTION _j c <� o � C k" a 8 LL F s C7 w I G- NATHIOSULFATE SAMPLE LOCATION DATE TIME Sample #1 ' a$' ' YOA 6 c 2 ....... .... ....... ....... CLASSIFICATION: WASTEWATER(NPDES) DRINKING WATER Sample #2 $ .15A VC 2 '•••• Sample #3 ��' a$' Q O ' 63 �' 2 DWQ/GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY N SAMPLES COLLECTED BY: (Please Pdnt) jotdarl LW SAMPLES RECEIVED IN LAB AT L' °C RELINQ (SHED B (SIG.) (SAMPLER) DATEMME RECEIVED IG. / ATETIME COMMENTS: 11-a8 A Y:ODA tar I? I L1 .3 i I 1 flg'LINQUINHESIG.) DATEMME RECEIVE BY (SI DATE/i'IME RELINQUISHED BY (SIG.) DATEMME RECEIVED BY (SIG.) DATEITIME v PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "G' for composite sample or a "G" for FORM #5 Grab sample in the blocks above for each parameter requested. NO 359851 1LaeAilgton. lojud..Wa itewaterTreatment.Plant City '.O n on, North i e°®lingi . WiQO001318 IAmatory WiirksheetForCompo`stlatialyses MheLE 1D satchmfg date{sj- ).y-I . M ; 40 - ra - . Collection of"'le Loon: Bda # aiie # . a8 bate.. 49WA Pattiogen Test-18'h 9=IE' MPPI!T Fecal colifonmJgram 1'0 x NlPN mdex/1QOri� % ImSest'volume'X dry solids tasted . Wet VYCI�I$.. gin, Dish weight em ' Fetal Coliform Dms iw. MFwgTS Sample: to,GIs *OM' The laigest valuave, ;is the largest sample voMme.iised_in detwaiaing the WN vsiue,'ntot the volume used in the 10.0n" S pgysi9. If %"dry solids = 751%'use *e value 75.ih the f_opmuls . 1.OmLs --is O.1mLs T/5: A 1 mcam 14 # mmd pH_• ofDo i6Ie Wag% Da's Au ck and p� = of Single strang#ti ATegaiivo t3iic /1.Pda�ive B!k . • %1 Ia35°CDsfn Ti=I% Time6d In440CDate -- "WrA_• _Date . Tm3900t_ Total Solids =-18e' 254OG s$ Dish # Wetweight Blank S-*' Dry-viei0t mams Dishweight �._._.VMS Solids = Iaoyea Dais .. Tuns OutofavenYJsto • Tmse dete�ig'the :. - no the golwnenscdiathe S .. .. ., •_.,: anysis If °!o dry solids s",�S®Je'.iise the:valua 75'in the"1'oa�ula 1.OmIs` - ' . A+imm'%bE#� Ditnnniaz�t � ;p$ .__ofDoitiilesireagfh: - : . • Dtte'A • • , p8• • of$igeie to �iS'C1�• . 15ooe 1'�me' __ .. . :iTa'�4Y:�ato Timeia• :... Total Solids-18m25400 • #F: DisiiAD ..' ';9i%!-weft'• .. Blan{C ;Sample . - �vesBM SolIde`=7riovat`Data 1�0 � .. ,Notes: The.aboveitf'aiinatia'iscczreetto;tIiebesiofmj►:1criowiioda .. �Si�aed:.::. '.. : , ..: 'Date! :... � • ' .. � � . •S;_: � Datev :. '�R±eviteve3bjr ;_ 41 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. LEXINGTON ,NC 27292 Sample PARAMETERS #f4 Total Solids, % 33.97 Fecal Coliform (MPH /gram Solids <53 142 Sample ##5 50.43 < 36 Sample #t 6 47.45 < 38 �P,' 1 Drinking Water ID: 37715 Wastewater ID: 10 ly ice' r ib b'Lu6 FAX (252) 756-0633 ID#: 636 K DATE COLLECTED: 12/05/18 DATE REPORTED : 12/10/18 4 REVIEWED BY: Sample Analysis Method #/7 Date Analyst Code 39.45 12/05/18 KDS 2540G-11 <46 12/06/18 KDS 9221E-06 F t nient 1, Inc. CHAIN 01' UCSTUDY kr CMD P.O. Box 7085, 114 Oakmont Dr. Page 1 of 1 llroo,,.,:110 AT(''7RSSZ environment 1 inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 •Fax (252) 756-0633 Ij CHLORINE CLIENT: 636 K Week: 4 pH CHECK (LAB) UV CONTAINER TYPE,P/G ITY OF LEXINGTON WWTP ❑ NONE P P IS. EGLANTINA MINERALI 3 WEST CENTER ST. CHEMICAL PRESERVATION EXINGTON NC 27292 A A m o C/) A -NONE D-NAOH E W zo Cr cn w C B - HNO E - HCL a f36)357-7A89 Q ; � z Soo oo M w C- H,SO, F- ZINC ACETATE/NAOH COLLECTION a o o o c a G- NATHIOSULFATE a SAMPLE LOCATION DATE TIME �aIS')� ' (90G CLASSIFICATION: Sample #4 2 WASTEWATER (NPDES) Sample #5 ) �b $ 2 L�6A rdL Samizie #6 ral3�ig �+`` 2 >>. ❑ DRINKINGWATER i�'J��$ L Vt� tO'�t' Sample #7 2 DWQ/GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY Y N SAMPLES COLLECTED BY: (Please Print) J0 r`awn 1-6 SAMPLES RECEIVED IN LAB ATI r4 °C RELINQUISHED BY SIG.) (SAMPLER) DATFffIME RECEIVE B IG.) ATEMME COMMENTS: Ak 5-6 I 9 : 05ec RELINQ E G.) DATE/TIME RECEIVED BY (SIG.) DATEfnME RELINQUISHED BY (SIG.) DATE/TIME RECEIVED BY (SIG.) DATETIME w Sampler must place a "C" for composite sample or a "G" for PLEASE READ Instructions for completing this form on the reverse side. FORM. #5 Grab sample in the blocks above for each parameter requested. N p 3,99850 Lexington Regional, Wastewateir Treatidelft Plat City ®f Lesi>ngtom; l�Toe 6 Carolil�a WQ0001318 . Labaia q WoAphect For. Comaposi Analyses MW AM3iy7ea::. . Aiaiyst�s); . MMELE ID Batchmf Collection of 5ar#le I;ocatioit fed,# I.a Pile # ®$ . Zone # eZ �'abPbi Type, uP �_ siga«. Date: �a�lq.��$ Time(101 Pathogen Test -.18119221E Fecal colif_oimlgtam=l O x `MPN mde li QOmI' IAgest: Volume X %dry solids tested Wetroveighi t Dish oveig Eni Fe* Colif m Density. I+HP1V/giS -----JML. WAter . ... Tlie largest volume; is the laegest sample vnlimne ,,iW in detctaiiniag the IViFN v4ue.-not`t6 voiuIuJO its9d irk the 10 Omi s /5 enfgysis.-If % dry solids = 75 a use the value, 75 in the formula. 1UmLs. /5: mof79._ A1ict# Date ,. nH oflJorihYestxmgtii Datm Awl p$ . Of Sole etcength Nega4igeBlk /1 Pmi6veBltcsf l 7si3s'c Dafe" Tim In T= Od TAIWcDaW : TiititeIto_Date r=Out_ Total Solids-- 186 254-00 Dish # Wet weight Blank Samoa Dzy. weightgrams Dish weight gram Solids=lnovenData Tmte Outofav=D, ato T=* Notes: 144 O El omfluM Flo hCupown'%.dQ 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CITY OF LEXINGTON WWTP MS. EGLANTINA MINERALI 28 WEST CENTER ST. LEXINGTON ,NC 27292 PARAMETERS Total Solids, Fecal Coliform (MPH /gram Solids Sample Analysis Method H2 Date Analyst Code 38.83 12/19/18 KDS 2540G-11 <46 12/20/18 KDS 9221E-06 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 636 K DATE COLLECTED: 12/19/18 DATE REPORTED : 12/26/18 REVIEWED BY: 145 Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Box 7085. 114 Oakmont Dr. Page 1of ureenvnic..N�- -10-70 environment I inc.com DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252i 756-6208 • Fax (252) 756-0633 FA ('HLORINF. CLIENT: 636 K Week: L: V j ! i pHCHECK (LAB) CONTAINER TYPE.P/G ITY OF LEXINGTON WWTP ❑ INON i P P IS. EGLANTINA NHNERALI 3 WEST CENTER ST. + , CHEIVICALPRESER.VATION EXINGTON NC 27292 C A - NONE D -NAOH �= Z u v w co w C B -HNO. E -HCL I36) 357-7889 -j W zo z ?? CC v Ln Uj C - H730, F - ZINC ACETATE/NAOH COLLECTION m w o H �a w G NATHIOSULFATE o o Uj ti w SAMPLE LOCATION DATE TIME CLASSIFICATION: 'RrASTEWAT�R APDES) DRINKING WATER Sample N `� �. 2 " `' I ,+ `� I j ❑ DWQGW - SOLID WASTE SECTION I CHAIN OF CUSTODY (SEAL) MAINTAINED DURING SHIPMENT/DELIVERY Y N SAMPLES COLLECTED BY: (Please Print) jajc-tA (,,, e SAMPLES RECEIVED IN LAB AT __ C RELINQU HED BY (SI .) (SAMPLER) DATEM,, /,t/��t� RECEIVED ( 1YD TEffIME �-7 COMMENTS: RELINQUI ED BY ( DATE11ME RECEIVED BY (S ATETIME RELINQUISHED BY (SIG.) DATEMME RECEIVED BY (SIG.) DATEMME i V PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "T for FAQ„ S5 Grab sample in the blocks above for each parameter requested. Lin o c n n c NCme 9C. S-Aafdnomlc.Division -Phone: (919)731-2e55. 'WebSite: < rtcagr:govfagrorioMU-- Report No FY16=1N006934' Pi@diCtive =Client_ Joseph'..Shafi°er .Advisor.-JordanLakey. Lexittgton=Wastevvatec 500: Glendale -Road-' 500'Gledale Rd-0 Lexington; NC 27282 RepoftaLexingtan; PiC 27292 p Davidson .County "R $aMpted: 05/OW1 018 LinScs.t®:4iLie-LUI Infl6 naldn - Received:r.05f14/2018: PAl:3#:43741i#' ParnD: LEXIPIGTON. PAdS lnfornatin 'Other Results NutrientWsurementsare gien:in-nitsofpais permillinm; unlesstherwise-OWed.sample :ID:201:H 1. Nitrogen (N) �. P K: Ca. :Mg S: Fe: -Mn Zn Cu B Nto �; C. Al Na CI C®der i3Ca Total N: 23700 , - 10560 . '431:0. 13000 2630 '1t390. 10200:. 'ti52 280 1?8 21 1 ' � `.3t30000 8760, 491 - Description: Inorganic'. _ . Biosolids,.Gomposted- NNa=N ( SS EC. pH_ 'BD. CCE -SALE' :CN+ DM' Giower Comments: NotPrcivided NOs-N -, .S !.(.10 S/cm) (mSLcm) (Unitless) (tb/yd'), (%) (tons} (lJnitless) (%o) - 162 "1.82: 56,93 - - - 16,0 1 4,71, Estimate:of Nutrients- Available for,First Year miton): Other Resuf fS (Ibltonj Applleatioei,.Method: N . PzOs KzQ : Ca Mg, S Fe Mn Zn'du B, 'Mo I Al, No, CI Broadcast 22:6. 14:3 4 93 124 25't 1.81 .9.71 :0.62 0:27 0:12 0.02_. - 8 36. 0,47 - agronomist's Comments: Insufficient infomrtation.is_ available _regarding -the first;year•availability of-nutrierits imthis:material. The nut rsent, availability: reporte6here:is, therefoae°:th'e.TOTAL nutrients in the_mgtenal.'Sam_ pies°submftted.prior to 2016 reported, an estimated value•rather.than:total nutrient leveis:. Please. -contact me if:you.have any.questions. Sample^ Inforrroation Nutrient MOastiremdrits are.given in units of parts.per million (pprn),. unless:uthe�wise specifed. Otit�er'fResultS Nltroaen (N) P K Ca_ . Mg S F®: Mn . Zn Cu 13 :Mo. `C Ai Na Gi Gode:. NCO Total N: 25200: 1- 6360 4110 12800 2870 1,91.0: 101.0-0 644 283 124' 205 - �`39Q000- 730,6 434: - Description: -Inorgariic: :Biosolids;.,Composted NH4-N. SS EC pH `Bb CCE . AL.E. C.`N DM. Grower.:Gomments• . Not RrovWed � NOs-, N I oeS,icm): (mSlcrri) (Unitiess). (Ib/yd3,) (%o) ,(tons) (WItless) .(7 221 95:5-;1 52;8 E6tirti9te of'Nutriettts Availabfle:for First:.Year:(Ib/ton)- -'Othet'Results (lb/ton)' Applfeation Method:. N PsOs' 'K20 'Ca Mg. 'S. Fe':' Mn Zn Cu :B Mo. At -Na: -CI. Broadcast .26.6: �1&4� 5.21 13.5 2:82` 2;01 10:6 t}:68` 0:30 0;1'3. 0.02 -. 7.70,' 0.:46 - North-. Carolina Reprogramming. of the laboratory -information -management. system that' makes -this report possibleU-.being fdhded: ' 4h"rough" a; grant from ttie North Carolina �Tobacco:Trust Furid,Corrimission.- ,;�� ..� Tharrlc. you for. -:using agronomic serviees to wrange. nartrients curd safeguard eny romnental qublity:_ _ t4aeco7iust`Nfid Commission = .Sfeye;Trorltr,..Co»tritissioner'o ` rculture:. 4 - h NCOA&CS'Agronomic Division Phone: ,,($119) 733-26W' Website: vww ncagr govlagronomi/ Report No. FYI8&W006934 Joseph 5ttafier Sampled: 05107/2018 j Received.-05/1412018 I :Completed:.05118/2018 Page 3 of'3 Understanding the Waste. Report. ,Nutrient- concentrations and other data on•this report are provided so thafwaste materials can' be applied at agronomic rates, thereby supplementingor reducing fertilizer -application.ar4preventing.environmental contamination' In reading the Laboratory Results:sedtion, remember that materials with < 15% dry matter (generally liquids) are - analyzed as received; all othee.wastes are".dried first.VValues.in the.Estimats of Nutrients Available for First Crop:section:are-based, on theaype of waste and method of application you • specify_ 'aiid. reflects the .fact chat .oNy.40.60% of the nitrogen becomes available. within one year of application. -The remainder. may orma v not ever'become Available.: -ALE is Agricnhural Lime Equivalence.. The ALE Diii .4 js percent Dry Matter [for semi -solid and Al = Aluminum Cu. == Copper NH4-N =-Ammonium.-N indicates. theamourit.of the -waste material that -solid waste, this value facilitates conversion of -As =Arsenic . Fie = Iron NI = Nickel, provides a limiting,effect.equivatent;to one'.ton of dry -basis concentrations (ppm)backto .B = Boron- K = Potassium NOa-N = Nitrate -N agricultural grade limestone. wet=basis of original sample]., Ca = Calcium Mg = Magnesium P = Phosphorus, 13a,is Oulk Density;in lblyd'. EC (Electrical Conductivity) measures Cd = Cadmium Mn = Manganese Pb- = Lead ,COE is Calcium Carbonate. Equivalence and'is salinity; or soluble salts (SS). Cl =Chloride, Mo = Molybdenum S = Sulfur ,used -'to, determine ALE.'. pH measures.basicity/acidity: Cr = Chromium N = Nitrogen se = Selenium - :G:N ratio. ts:theiAarbon:Nitrogen ratio.. Na = Sodium meq/L'= milliequivalent'per Men, Ins = millisiemens; ppin = parts per million or mg/L; S = siemens; T = trace (<0.005 lblunit) Additional -information: _NMM_nc_'a__ aoy/anrono ni/odifiles/uwaste.pdf'8�wwvv:ncarar.,g viacironomilpdffiles/wasteauidg.odf