WQ0039053_Modification_20190320

INITIAL REVIEW
Reviewer
Project Number*
Thornburg, Nathaniel
WQ0039053
SUBMITTAL DATED: 3/20/2019
Project Contact Information
Rease provide information on the person to be contacted by NDB Staff regarding electronic subrrittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Martin Mabe
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
r
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number WQ0039053
currently has project
Permittee * Bio-Nomic Services, Inc.
Facility Name * Bio-Nomic Services DCAR
Phone Number*
336-312-1396
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Permit modification to add Greenville Utilities WTP (2,000 DT's/Yr). Check for $395.00 modification fee to be included
with paper copy being mailed out today by UPS.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Hans, Specifications, Calculations, Etc.)
Bio-Nomic Services Class A Permit Modification 3-
4.6MB
20-19.pdf
upload only 1 HDF docurrent. IVLltiple documents rrust be combined into one HDFfile.

For nein and modif cation permit applications, the paper copy is required to be submitted to the
Di, risiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ging:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,vision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942M
512 N_ Salisbury St_ Raleigh, NC 27644
For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
*140 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 3/20/2019

APPLICATION FOR
DISTRIBUTION OF CLASS A RESIDUALS
PERMIT MODIFICATION
BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
Willcox & Mabe Soil Solutions, PLLC Project No. 15-18
Prepared for:
Bio-Nomic Services, Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Prepared by:
Willcox & Mabe Soil Solutions, PLLC
7231 B Summerfield Road
Greensboro, North Carolina 27358
willcax&mate
SOIL SOLUTIONS
March, 2019

March 20, 2019
NCDEQ/DWR
Water Quality Permitting Section
512 N. Salisbury Street
9M Floor, Office #942W
Raleigh, North Carolina 27604
Attention: Non -Discharge Permitting Unit
willcox&mabe
SOI L SOLUTIONS
Reference: Modification for Distribution of Class A Residuals
Bio-Nomic Services, Inc. WQ0039053
Willcox & Mabe Soil Solutions, PLLC Project No. 15-18, Phase: I 1
Non -Discharge Permitting Unit:
Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting the enclosed application to
modify the existing Distribution of Class A Residuals permit WQ0039053 for Bio-Nomic
Services, Inc. (BNS) on behalf of BNS. The application package includes information for
adding one Class A source at this time: Greenville Utilities - 2,000 Dry Tons.
It should be noted that Greenville Utilities WTP is an industrial source with no domestic
contribution to the waste stream. Fecal coliform sampling has demonstrated that the
residuals meet Class A requirements (all 7 individual samples were below 1,000 MPN/g).
Per 15A NCAC 02T. I 106A and .1107.c vector attraction reduction should not be required
for this source.
If there is any further information required or questions regarding this application please do
not hesitate to contact Bio-Nomic's, Mr. Vaughn "Buck" Stevenson at [phone] or
WMSS's Mr. Martin Mabe at 336-312-1396 for further assistance.
Sincerely,
Willcox & Mabe Soil Solutions, PLLC
Martin Mabe
Agronomist
cc: Bio-Nomic Services, Inc.
Rob Willcox, L.S.S.
Licensed Soil Scientist
SharedlWMSS Projects\2015\15.18 Bio-Nomics\Phase 09 - Class A Permitr2019 Permit Modification (GUC)115-18 Bionomics Distribution of
Class A Residuals Application Package.doc
Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road 1 Summerfield, NC 273581 Rob 336.339.9128 or
Martin 336.312.13961 www.willcoxmabesoil.com

APPENDIX I
DISTRIBUTION OF CLASS A RESIDUALS
APPLICATION FORM (DCAR 06-16)

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T.1 100 — DISTRIBUTION OF CLASS A RESIDUALS
INS'T'RUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two copies of the application and
stipportipg documentation
For more infortnation, visit the Water Quality Permitting Section's � (� ii, l il,15chcrrge Pe. irriltirrg Zlnil websile
General —This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under l5A NCAC 02"l .1 100,
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-I6) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
® The project name should be consistent on the plans, specifications, etc.
® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 1.5A_NCAC 02T .0106(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in .1.5A
NCAC.023.--, 0,1110160).
E] If this project is for a modification of an existing permit, submit one copy of the existing permit.
El Please submit this application form at. least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification New Permit Major Modification
I
Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395
Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245
' - A major modi#ication shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications,
C. Cover Letter (All Application Packages)
® List all items included in the application package, as well as a brief description of the requested permitting action.
INS`T'RUCTIONS FOR FORM: DCAR 06-16 Page 1 of 3

D. Program Information (All Application Packages)
® Provide a narrative explaining the following:
® How the materials will be handled and transported from where the residuals were produced to where it will be treated.
® How the residuals will be processed/treated (attach process flow diagram).
® How leachate collection will be handled,
® Where the residuals will be stored until processed.
® How the final product will be distributed (packaging, bulk, etc.)
® What nutrients or other constituents (i,e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
® Name and address of the person who prepared the residual that is sold or given away.
® A statement that application of the residuals to the land shall be in accordance with the instructions oil the label or
information sheet.
® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters,
® Information on all applicable setbacks in accordance with 15A, NCAC.02T...1.108(b}.
® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
Submit detailed plans and specifications that have been signed, scaled, and dated by a NC Professional Engineer per 15A
NCA.C_02.'I'..J.104.(a).. Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
❑ Plans must include the following minima n items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minhnum separations required in .,l_5A.NCAC 02"T'_.1_108(a) on the plans.
F-1Specificationsmust include, at a minimurn, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 021'_._1 104(4)(2),(Q),, including leakage and pressure testing as appropriate.
Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02'1_'
T I.04(a).
C. Environmental Assessments (May be Required — See 15A NCAC I,C_.0300)
Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
F] For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
® Submit the O&M Plan in accordance with .1..5A..N.CAC_02"lT , ].1 1.0 and include at a minimum:
® Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
® Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
® Safety measures; may include safety training program, manuals, signs, etc.
® Spill response plan; including control, containment, remediation, emergency contact information, etc.
® Inspection plan including the following information;
® Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
® Sampling and monitoring plan including the following information;
® Names and titles of personnel responsible for conducting the sampling and monitoring.
® Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of

DWR
State of North Carolina
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T.1 100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 06-16
1. APPLICANT INFORMATION:
1. Applicant's name: Bio-Nornic Services, Inc
Applicant type: ❑ Individual ® Corporation General Partnership Q Privately -Owned Public Utility
F Federal ❑ State El Municipal ❑ County
Signature authority's name per i.. 5_A.NCAC.._92-1.'...0.106: Mr. Vaughn Stevenson Title: Assistant Vice President
Applicant's mailing address: 530 Woodlawn Street
City: Belmont State: NC Zip: 28012 -
Telephone number: [phone] Ernail Address: vstevenson(bio-nomic.com
2. Consultant's narne: Martin Mabe License Number (for P.E.):
Affiliation: ❑ On Staff ® Retained (Firm: Willcox & Mabe Soil Solutions, PLIX)
Consultant's ,nailing address: 7231B Summerfield Road
City: Suninierfield State: NC Zip: 27358 -
Telephone number: (3.36) 312-1396 Email Address: martina wil€coxmabesoil.com
3. Fee submitted: $395.00 (See Instruction B)
11. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, 0 renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WQ0039453
Date of most -recently issued permit: March 22_2017
Date of most -recently certified Attachment A (if different than the permit): January 14, 2019
III. FACILITY INFORMATION:
1, Name of residuals processing facility: Bio-Nomic Services, Inc.
City: Belmont State: NC Zip: 28012-
Coordinates: Latitude: 350 16' 32" Longitude: 81' 3'7"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
County where facility is located: Gaston
2. Facility contact (person familiar with residuals preparation):
Name: Vaughn "Buck" Stevenson Title: Assistant Vice President
Mailing address: 530 Woodlawn Street
City: Belmont State: NC Zip: 28012 -
Telephone number: [phone] E-mail address: vstevenson a bio-nomic.com
FORM: DCAR 06-16 Page] of 3

3. Is the residual process facility also the generator'? ❑ Yes; ® No
If No, please specify delivery frequency and quantity of residual to be processed: NIA
4. Length of residuals storage at facility: N/A days (Note: the Division requires minimurn 30 days storage in units that are separate
from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
I. Specify how these residuals will be distributed:
0 sold or given away in bags or other containers; C] lawn (bull:); [] home garden (bulk);
® other (explain); Land Application
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less,
z. Complete the following if residuals are to be mixed with other materials:
Amounts to be added
Type of Materials ner 1.0 dry ton of residuals (dry ton)
3. Approximate amounts of the residuals received and processed at the facility: NIA dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: NIA dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): N/A
6. Does the facility have a stormwater managernent plan? El Yes; ® No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: N/A
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
CIf
Residuals Source
Certification
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
, attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions ofthis submittal package
may have been developed by other professionals, inclusion of these materials under my signature and sea] signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Sea], Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 1 A..NCAC...02"T...0.1.OS.
® Yes E] No, Explain;
I, Vaulln_Stevenson Assistant Vice President
(Signature Authority's Name — PLEASE PRINT) ("Title)
attest that this application for _ _ ,_.._Bio_Nornic Services, Inc. -- Distribution of Class_A Residuals
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. l understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. 1 will make no claim against the Division of Water
Resources should a condition of this permit be violated, 1 also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation,
Signature:
Date
,3-,,-2c) - i q
FORM: DCAR 06-16 Page 3 of 3

APPENDIX II
FORM DCAR 06-16 (ITEM D. - PROGRAM INFORMATION)

FORM DCAR 06-16 (ITEM D. PROGRAM INFORMATION)
D. Program Information (Bio-Nomic Services Class A Residuals)
Currently, Bio-Nomic Services is proposing to add one source: McCall Farms, Inc.
W WTP (in association with closing out several of the existing lagoons on site.
How the materials will be handled and transported from where the residuals
were produced to where it will be treated.
The operational functions of this program involve removing Class A Residuals from the
respective WWTP and beneficially recycling the biosolids to land application sites which
meet NCDEQ-DWR regulatory requirements. Class A Residuals will be land applied at
or below agronomic rates.
How the residuals will be processed/treated (attach process flow diagram).
The Class A Residuals will be tested at the respective treatment plants prior to hauling for
land application.
• How leachate collection will be handled.
Leachate will not be generated
• Where the residuals will be stored until processed.
Class A Residuals will be stored at the respective treatment plants
• How the final product will be distributed (packaging, bulk, etc.)
Class A Residuals will be land applied, not distributed
What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum,
calcium, etc.) are used or recommended as the limiting parameter for
determination of residuals loading rate to ensure that it does not overload the
soil and cause contravention of surface water or groundwater standards, limit
crop growth, or adversely impact soil quality.
Product Information Labels and Application Information Sheets are Attached.
• Attach a marketability statement detailing destinations and approximate
amounts of the final product to be distributed.

D. Program Information (Bio -Noetic Services Class A Residuals) Page 2
Product Information Labels and Application Information Sheets are Attached
Provide either a label that shall be affixed to the bagged Processed residual or an
information sheet that shall be provided to the person who receives the
processed residual. The label or information sheet shall contain, at a minimum,
the following information:
• Name and address of the person who prepared the residual that is sold or given
away.
• A statement that application of the residuals to the land shall be in accordance
with the instructions on the label or information sheet.
• A statement that the residuals shall not be applied to any site that is flooded,
frozen or snow-covered.
• A statement that adequate procedures shall be provided to prevent surface runoff
from carrying any disposed or stored residuals into any surface waters.
• Information on all applicable setbacks in accordance with I5A_NCAC_OXIF
_l.l QS(h)..
• A statement that the residuals shall be applied at agronomic or recommended rates
for intended uses.
Product Information Labels and Application Information Sheets are Attached

BIO-NOMIC SERVICES PRODUCT INFORMATION LABEL
Prodsced/L.and Applied By., Preparer:
Bio-Nomic Services, Inc. Respective WWTP's and WTP's
530 Woodlawn Street
Belmont, North Carolina 28012
For information on these products contact Bio-Nomic Services, Inc.
Vaughn "Buck" Stevenson, Assistant Vice President [phone]
The Bio-Nomic Services Class A Residuals are WTP Plant Residuals and WWTP Biosolids that
meet NCDEQ-DWR Class A land application requirements. The Bio-Nomic Services Class A
Residuals and Biosolids contain varying values of Nitrogen, Phosphorus and Potassium. Each
permitted Source will have a laboratory sample analyzed, with current nutrient values made
available prior to land application of the product.
Provisions for Application
Application of the Bio Nomic Services Class A Residuals are prohibited except in accordance with
the provisions specified in the Application Information Sheet. Application must conform to
standards identified in Pernut WQ0039053 and include but are not limited to:
Setback Description
Setback
(feet)
Private or public water supply sources
100
Surface waters (streams — intermittent and perennial, perennial waterbodies,
and wetlands)
25
Surface water diversions (ephemeral streams, waterways, ditches)
0
Groundwater lowering ditches (where the bottom intersects the SHWT)
0
Wells with exception to monitoring wells
100
Bedrock outcrops
0
Bio-Nomic Services Class A Residua3 Product Information label

Application Information Sheet
1. Bio-Nomic Services Class A Residuals are intended for use as a fertilizer product.
Applications of Bio-Nomic Services Class A Residual should be made in accordance with
approved application standards and WQ0039053 permit conditions.
2. Bio-Nomic Services Class A Residuals shall not be applied to flooded, frozen, or snow
covered areas.
3. Application and storage of Bio-Nomic Services Class A Residuals must be conducted in
such a way as to prevent runoff from the application or storage site to any surface water.
4. Applications and loading rates of Bio-Nomic Services Class A Residuals shall be
applied at agronomic or recommended rates.
Contact Bio-Nomic Services for a copy of the most recent Class A Residuals analysis and
loading rates.
Bio-Nomic Services Class A Residual Product Information Label

BIO-NOMIC SERVICES CLASS A RESIDUALS RECEIPT FORM
I , (Printed name) have received
pounds and/or gallons of the Bio -Noetic Services Class A Residuals, a copy of the Bio -Noetic
Services Class A Residual product information label, and a copy of the most recent analysis of
the product (if requested). I have read these documents and agree to adhere to the directions
specified on the Application Information Shect and the Product Information Label.
Signature of Receiver• Date of Receipt
Address of Receiver
Bio-Nomic Services Class A Residual Product Information Label

APPENDIX III
FORM DCAR 06-16 (ITEM H. - OPERATION AND MAINTENANCE PLAN)

BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
I. Purpose
To put into place a plan that implements the requirements of North Carolina Department
of Environmental Quality — Division of Water Resources (NCDEQ-DWR) Permit No.
WQ0039053 for Bio-Nomic Services, Inc. (Bio-Nomic Services). Requirements are
included for the Class A source(s) (WWTP's and WTP's) and Bio-Nomic Services (land
application contractor). Class A source(s) are listed within the permit.
II. Operational Functions
The operational functions of this program involve hauling Class A Residuals from the
respective WWTP's and WTP's to land application sites which meet NCDEQ-DWR
regulatory requirements. Class A Residuals will be Iand applied at or below agronomic
rates. Bio-Nomic Services will also account for any nutrient sources the
landowner/lessee has applied. Some source(s) may be land applied as either a liquid or
cake material utilizing either pumper trucks, vacuum trucks, tractor trailer, tractor and
cake spreader and/or tractor and pull tank. Class A Residuals will be spread evenly and
at consistent rates. Class A Residuals will be land applied on fields that are used for hay
production, grazing, or row crop production harvested for animal feed. In the case where
Class A Residuals are land applied on fields utilized for grazing, applications rates will
be reduced by 25% in accordance with t1SDA-NRCS 590 Nutrient Management
Standards. Grazed fields will be determined by Bio-Nomic Services Operations Manager
oI] sIte.
The Bio-Nomic Services Class A Residuals will be monitored to confirm its compliance
with conditions in Non -Discharge Permit No. WQ0039053 to include:
• 15A NCAC 02T.1105 Pollutant Limits and nutrient analysis,
• Toxicity Characteristics Leaching Procedure (TCLP), and
• Reactivity, Ignitability and Corrosivity
III. Maintenance Schedules
Bio-Nomic Services will follow the maintenance schedule as recommended by the
manufacturer for the equipment utilized to complete the Job within the limits of the permit.
IV. Safety Measures
Bio-Nomic Services takes pride in operating in a safety conscious manner. Employees
participate in regular safety training that is designed to help employees recognize safety
issues and take steps to prevent potential accidents from occurring. Bio-Nomic Services
employees have the authority to stop operations if they thinly any aspect of the operation
is going to lead to the cause of an environmental or personal accident.
CAUsersWartinlWi€lcox and Mabe Soil Solutions\Rob Willcox - Shared\WMSS Projects=15115-18 Bio-Nomics\Phase 09 -Class A Permit12019 Permit
Modification (GUC)Tio-Nomic Services Class A O&M Plan 2018.doc 3-5-19

BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
V. Spill Response Plan
• Halt the source of the spill. Such as a ruptured line or valve, or damaged transportation
unit.
• Contain spill: Use straw bales to form a barrier. Straw or hay bales can be obtained
from several sources for this purpose. Soil near the site can also be used to form a barrier
for containment.
• Clean up: Use Class A Residuals application equipment to recover as much of the
material as possible. After the application equipment has recovered as much material as
possible, it will be land applied as per the management plan. A temporary sump pit may
be dug in the containment area and spilled material washed into it to enhance recovery.
• Final Clean up: The ultimate goal will be to restore the spill area to its original
condition if possible.
• Notification: As soon as possible after a spill occurs notify:
• Bio-Nomic Services — Home Office
704-529-0000
Andy 'Taylor
704-907-7933
Joel Coert
704-904-9704
Buck Stevenson
704-930-8886
• Department of Environmental Quality
Division of Water Resources
Applicable Regional Office (Sec Permit)
Management of clean-up efforts: The field superintendent shall take immediate charge
of the clean-up activities. Additional labor will be requested from Bio-Nomic Services as
needed.
VI. Reporting
Within 24 hours of a spill the field superintendent shall present a written report detailing the
cause of the spill and all action taken in response to the spill. Bio-Nomic Services will notify
the appropriate Regional Office as soon as possible, but not more than 24 hours after, or on the
next working day following the occurrence
VII. Inspection Plan
Inspections for the land application of Class A Residuals will be conducted at a minimum of
daily at the land application site during land application events. Inspections will consist of
inspecting the current field(s) that are being applied on, as well as inspecting random fields
that have previously received Class A Residuals applications. Inspections will be performed
by Bio-Nomic Services personnel on a rotational basis to ensure that all employees are
familiar with the inspection processes. At a minimum, these inspections will consist of the
following:
CAUsersWartir W ilcox and Mabe Soil Solutions\Rob Wi€lcox • Shared\WMSS Projectsr2015115-18 Bio-NomicslPhase 09 -Class A Permi112019 Permit
Modification (GUC)1Bio-Nomic Services Class A O&M Plan 2018.doo 3-5-18

BIO-NOMIC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
• Verify that a residuals analysis has been collected prior to land application
activities being performed and that it meets the criteria for land application.
• Verify that pathogen reduction data has been collected for the source to be land
applied and that it meets the criteria for Iand application.
• Verify the crop that is planted or is to be planted on the respective field(s).
• Confirm that the correct amount of Class A Residuals are being land applied.
• Confirm that transport and application vehicles have a copy of the spill control plan.
+ Confirm that a copy of the permit and the operations and maintenance plan are
maintained at the land application sites during land application activities.
• Check that the field has been properly flagged and that buffers are adhered to.
• Confirm that records are turned in at the end of each business day.
Inspections will also be conducted by the respective employees of the Class A Residuals
generating facilities (at the source generating facility). Bio-Nornic Services is not
responsible for inspections at the source generating facilities. These inspections
should be conducted by the respective ORC of each facility and should fall under
their own Operations and Maintenance Plans.
VIII. Sampling and Monitoring Plan
All sampling and monitoring shall be performed in accordance with curre11t Permit No.
WQ0039053, Bio -Noetic Services Class A Residuals.
Pollutant concentrations for Class A Residuals shall not exceed the following Ceiling
Concentrations or Monthly Average Concentrations (i.e., dry weight basis):
Parameter
Ceiling Concentration
(milligrains per
kilogram)
Monthly Average
Concentration
(milligrains per kilogram)
Arsenic
75
41
Cadmium
85
39
Copper
4,300
1,500
Lead _
840
300
Mercury
57
17
Molybdenum
75
n/a
Nickel
420 -��
420
Selenium
100
100
Zinc
7,500
2,800

BIO-NOM.IC SERVICES, INC.
NON -DISCHARGE PERMIT NO. WQ0039053
OPERATIONS AND MAINTENANCE PLAN
CLASS A RESIDUALS
Class A Residuals shall be analyzed to demonstrate it is non -hazardous under the Resource
Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity,
and toxicity characteristic teaching procedure (TCLP)] shall be performed prior to land
application of Class A Residuals.
TCLP analysis of Class A Residuals shall include the following parameters (the regulatory level in
milligrams per liter is in parentheses):
Arsenic (5.0)
1,4 -Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadntiurn (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Hexachlorobenzene (0.13)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Heptachlor (and its
hydroxide) (0.00$)
Toxaphene (0.5)
Chloroform (6.0)
Hexachlor -1,3-butadiene
'Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5 -Trichlorophenol (400.0)
m -Cresol (200.0) -
Lead (5.0)
2,4,6 -Trichlorophenol (2.0)
o -Cresol (200.0)
Lindane (0.4)
2,4,5 -TP (Silvex) (1.0)
p -Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
_
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone
An analysis shall be conducted on the Class A Residuals based on conditions set forth in Permit No.
WQ0039053. The analysis shall include the following parameters:
_ Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadnliunl
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
"rKN
Copper
_
pH
Zinc
Lead
Phosphorus
Magnesium
_ _
Plaut Available Nitrogen
(by calculation)
Pathogen Reduction: Per 15A NCAC 027.1 106,
For DistributionlLayLl A> >Ircation of Class A or E uivaleut:
0 A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids
4

APPENDIX IV
RESIDUALS SOURCE CERTIFICATION
APPLICATION FORM
GREENVILLE UTILITIES WTP
(FORM: RSC 06-16)

State of North Carolina
DW
Department of Environmental Quality , R
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
PIease use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one ori incl and two copies of the a lication and
stigporting documentation
For more information, visit the Water QiralydvPer»iiiiii7gSectioy7 ,v NVo1a.-I)iselagr�ePej-.nr lltt?g.!V it
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 1..5.A_NCAC._02T ._L_i_00, Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form, If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification,
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities,
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance foto
EZesidtia.ls La„nd_,Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed; and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8.
)insure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or, disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

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State of North Carolina
DW
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction 13.):
1. Facility Name: Greenville Utilities Commission
2. Facility permit holder is: El Federal, El State, 2 local Government, or El Private.
Facility permit issued by: 0 Div. of Water Resources, El Div. of Environmental Health,
or 0 Other (explain. ).
3. Facility contact person and title: Julius Patrick, WTP Superintendent
Complete mailing address: P.O. Box 1847
City: Greenville State: NC Zip: 27835-1847
Telephone number: [phone] E-mail address: patricie2guc.coin
4. Facility physical address: 1721 Waterway Road
City: Greenville State: NC Zip: 27834 -
Coordinates: Latitude: 35° 38' 26.31" Longitude: 77`23'55.47"
Datum: NAD83 Level of accuracy: Nearest hundredths of second
Method of measurement: MAP
5. Purpose ofthe facility:
treatment of municipal wastewater, 0 treatment of 100% domestic wastewater,
® treatment of potable water, 0 treatment of 100% industrial wastewater,
0 treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages:' ' % industrial and % domestic)
E] other (explain. ).
6. Does the facility have an approved pretreatment program: D Yes ® No
7. Facility permitted/design flow: 008 MGD and facility average daily flow: 6.573 MGD
8, Average amount of residuals being generated at this facility 2000. dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volurne of residuals treatment: N/A
Type and volume of residuals storage (i.e., outside of residuals treatment units): 23 acres with a depth of 14 feet frons the
invert to grade with a 3.50.000 cubic vard capacity. mm
11. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
El 40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during dornestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCA
El Biological ® Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: El yes Z no.
If yes, list the nurnber(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: M yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure ('1'CLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Test America and Date of analysis: 2/19/19
Passed corrosivity test: yes ❑ no, pl l: s.u. (2 < pH < 12.5)
Passed ignitability test: yes Q no. Flashpoint: >200 °F (> 140T)
Passed reactivity test: ® yes ono. HCN: <0.505 mg/kg (<250) & H2S: 31.7 mg/kg (<500)
TCLP Parameter
Limit
Result
TCLP Parameter
Limit
Result
Arsenic
5.0
<0.500
flexachlorobcnzene
0.13
<0.0500
Barium
100.0
<2 _
�Hexachloro-1,3-Butadiene
0.5
<0.0500
Benzene
0.5
<0200
Flexachloroethane
3.0
<0.0500
Cadmium
1.0
<0.500
Lead
5.0
<0.500
Carbon Tetrachloride
0.5
<0.200
Lindane
0.4
<0.000500
Chlordane
0.03
<0.00500
Mercury
0.2
<0.00200
Chlorobenzene
100.0
<0.200
Methoxychlor
10.0
<0.000500
Chloroform
6.0
<0.200
Methyl Ethyl Ketone
200.0
<0.200
Chromium
5.0
W <0,500
Nitrobenzene
2.0
<0.0500
m -Cresol
200.0
<0.100
Pentachlorophenol
100.0
<0.250
0 -Cresol
200.0
<0.100
Pyridine
5.0
<0.100
p -Cresol
200.0
<0.100
Selenium
1.0
<0.500
Cresol
200.0
<0.100
Silver
5.0
<0.500
2,4-D
10.0
<0.0400
Tetrachloroethylene
0.7
<0.200
1,4 -Dichlorobenzene
7.5
<0.0500
Toxaphene
0.5
<0.0400
1,2-Dichloroethane
0.5
<0.200
Trichloroethylene
0.5
<0.200
1, 1 -Dichloroethylene
0.7
<0.200
2,4,5 -Trichlorophenol
400.0
<0.0500
2,4-Dinitrotoluene
0.13
<0.0500
2,4,6 -Trichlorophenol
2.0
<0.0500
Endrin
0,02
<0.000500
2,4,5-1'P (Silvex)
LO
<0.0100
Heptachlor and its Hydroxide
0.008
<0.000500
Vinyl Chloride
0.2
<0200
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under I 5 NCAG,„021 /„105,
a. For Distribution/L(tyid Application: Pill in the following table with the results of the latest analyses (i.e,, on a dry weight
basis) for the following metal parameters:
Laboratory: Waypoint Analytical and Date of analysis: 2/20/19
Parameter
Ceiling
Concentration Limits
(Class,4 & Classl3)
(Ing/kg)
Monthly Average
Concentration Limits
(Class A Only)
(Ing/kg)
Result
(ing4g)
Arsenic
75
41
16.6
Cadmium
85
39
< I
Copper
4,300
1,500
556
Lead
840
300
12
Mercury
57
17
0.475
Molybdenum
75
n/a
< 2.5
Nickel
420
420
10.2
Selenium
100
100
< 5
Zinc
7,500
2,800
59.4
b. Tor Surface Disposal Unit (landll}: Fill in the Following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check orae)
Arsenic
(ing/kg)
Chromium
(ing/kg)
Nickel
(ing/kg)
El > 0 but < 25
30
200
210
0 > 25 but < 50
34
220
240
E ? 50 but < 75
39
260
270
0 >75 but < 100
46
300
320
El > 100 but < 125
53
360
390
El >_ 125
62
450
420
Result (rr:g/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. "Total solids: 2.79 %.
b. fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
rmcronutrrent parameters:
Laboratory: Waypoint Anal fical and Date of analysis: 2/20/19
Parameter
Result
(mg/kg)
Aluminum
140,000
Ain monia-N itrogen
3,930
Calcium
1,990
Magnesium
402
Nitrate -Nitrite Nitrogen
190
pH (Standard Unit)
6.4
Phosphorus
3,340
Potassium
310
Sodium
456
Total Kjeldahl Nitrogen
40,700
c. Using the results listed in Item It. 5b. above, calculate the sodium adsorption ration (SAR): 0.406
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g.,gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growthl.
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 20 %. This
rate is a (check one): ® default value, or 0 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
c. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (iso) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(ing/kg)
Surface
9,509
15,167
Injection/Incorporation
11,474
17,132
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: NIA
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per _1.5A NC..AC.U2'l';.I..,106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
f A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative I [ 15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
Alternative 2 [ 15A NCAC 02T.1106(b)(3)(B)] -Alkaline Treatment.
[] Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova,
El Alternative 4 [15A NCAC 021'.] 106(b)(3)(D)] -No Prior Testing for Enteric Virus/Viable HeIrninth Ova.
Ej Alternative 5 [15A NCAC 02T.] 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 0 composting, 0 heat drying, E] heat treatment,
thermophilic aerobic digestion, El beta ray irradiation,
[] gamma ray irradiation, or [I pasteurization,
b. For LandApqlication of Class B:
Alternative I [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [ 15A NCAC 02T.1 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: El aerobic digestion, 0 air- drying, 11 anaerobic digestion,
El composting, or lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item 11. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item 11. 7b. above.
F1 Exempt - If Daily Cover Alternative is chosen in Item 11,8. below [15A NCAC 021'. l 106(a)(2)].
0 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC. 027.1 107, specify how residuals will meet the VAR requirements:
E] Alternative 1 [15A NCAC 02T.] 107(a)(1) - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
Alternative 2 [ 15A NCAC 02T.1 107(a)(2)] - 40 -Day Bench Scale Test (Anaerobic Digestion).
0 Alternative 3 [15A NCAC 02T.] 107(a)(3)] - 30 -Day Bench Scale Test (Aerobic Digestion).
0 Alternative 4 [ 15A NCAC 02T.1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion),
E] Alternative 5 [15A NCAC 02'1'.1 107(a)(5)] - 14 -Day Aerobic Processes.
El Alternative 6 [ 15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
] Alternative 7 [15A NCAC 02T.1 107(a)(7)] - Drying of Stabilized Residuals.
[] Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals.
Ej Alternative 9 [15A NCAC 02'7'.1 107(a)(9)] - Injection.
Alternative 10 [ 15A NCAC 02T.1 107(a)(10)] - Incorporation.
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

BIO-NOMIC SERVICES, INC.
Specializing in today's needs for environmental protection.
530 Woodlawn Street • Belmont, North Carolina 28012 • [phone] • [phone]
GREENVILLE UTILITIES COMMISSION (GUC)
GREENVILLE UTILITIES WATER TREATMENT PLANT
Residuals Source- Generating Facility Information
- Process Flow Narrative
Greenville Utilities Commission operates an existing water treatment plant at 1721 Waterway
Road, which produces drinking water for the local community. The source of raw water
originates from the Tar River.
The Greenville Utilities Water Treatment Plant has been operational since 1985 and has a
capacity of 10.5 MGD. In 1995, the plant was upgraded to accommodate the treatment of an
additional 12 MGD bringing the plant's capacity to 22.5 MGD. The average daily flow is 10.54
million gallons per day.
Raw water from Greenville's sources is pumped into a 63 -million -gallon impoundment where it
settles for five days to facilitate sedimentation. Then the introduction of a coagulant allows
particles to clump together allowing additional sedimentation to occur with the aid of
flocculators.
Upon the completion of settled water receiving ozone for primary disinfection, clear, sediment
free water is pumped into 2 three -million -gallon storage tanks ready for distribution. The
collected sediment is discharged into a holding lagoon, GUC also utilizes eight deep
groundwater wells that have a combined capacity of 2.0 MGD which have previously been used
to meet the increasing water demands of the city.
The lagoon will hold the sediment until removal is necessary. A portable hydraulic dredge is
placed in the lagoon to pump the materials out of the basin. The floating hydraulic dredge is
advantageous as it allows the lagoon to remain in service during the process. The sediment is
pumped in slurry form to a 20,000 -gallon receiving tank. The tank is fitted with mixers to
homogenize the materials for mechanical dewatering.
The mechanical dewatering process is accomplished with a mobile belt filter press system. An
anionic or catanionic polymer is introduced to concentrate the slurry during the dewatering
process. The belt filter press further removes water by compressing the residuals between filter
belts generating a filter cake. The filtrate water resulting from the process can be returned to the
lagoon.
The filter cake, is now suitable for either onsite land application or for loading into dump trucks
for transportation to a secondary application site as a soil amendment.
- Quantitative Justification for Residuals Production Rate
A minimum of 1,250 dry tons may be removed and land applied annually.
A Carylon Company

SAMPLING PLAN
Sampling Procedures
Accurate sampling is essential for valid laboratory test results. All samples collected at the respective
Water Treatment Plant's (WTP) are grab samples, which are samples taken at selected intervals to
represent conditions at a given location at a particular point in time.
Grab samples of residuals are stored in a manner that will not alter sample characteristics. Proper
preservatives are used for specific parameters. The samples are kept under refrigeration at 4° C until
delivered to laboratory for analysis.
Sampling Log
Sampling information is recorded on a chain of custody (COC) form by Bio -Noetic Services personnel
provided by the respective laboratory that is performing the required testing required by the permit, Log
book entries include, at a rninimurn:
• Purpose of sampling
• Location of sampling point
• Type of sample (grab or composite)
• Name of person collecting samples
• Type of residuals sampled (undigested, post -digestion, post -storage)
• Number and volume of sample(s) collected
• Description of sampling point.
• Date and time of collection
The residual solids analysis will be conducted for, but not limited to, the following parameters, percent total
solids, phosphorus, lead, copper, cadmium, sodium, total Kjeldahl nitrogen, nitrate nitrogen, nitrite nitrogen,
magnesium, potassium, zinc, nickel, arsenic, mercury, selenium, molybdenum, calcium, ammonia nitrogen,
aluminum and pH on all Annual Basis, or as required by Permit Conditions based upon annual tons land
applied.

(D
�lnt.:
ANALYTICAL
3/1/2019
Bin-Nomic Servics Inc
Joel Coert
530 Woodlawn St
Belmont, NC, 28012
Ref: Analytical Testing
Report Number: 19-052-0208
Project Description: Guc #1
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 1 Fax [phone]
www.waypointaiialyticaI.com
Dear Joel Coert:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/21/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VAOJ J Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Vie'

WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
W-aypoint.(D
7621 Whitepine Road, Richmond,
VA 23237
Main 804-743-9401 ('Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Sample
Summary table
Report Number: 19-052-0208
Client Project Description: Guc #1
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
SM-2540G
WTN
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
SW-74718
WTN
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
SM-4500-NH3C-TKN
WTN
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
4500NO3F-2011
WTN
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
6010D
WTN
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
SM-4500-NH3C
WTN
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
9045D
WTN
64892
Guc #1
Solids
02/20/2019 07:00
02/21/2019
AOAC 955.01
WiN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354

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(D
Waypoint7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 ° Fax $04-271-6446
ANALYTICAL www.waypointanalytical.coni
Cooler Receipt Form
Customer Number: 45671
Customer Name: Bio -Noetic Servics Inc
Report Number: 19.052-0208
Shipping Method
Fed Ex US Postal Lab
UPS Client Courier
Other:
Thermometer ID:
Shipping container/cooler uncompromised?
+ Yes
No
Number of coolers received
F-1
Custody seals intact on shipping container/cooler?
Yes
No
Not Required
Custody seals intact on sample bottles?
Yes
No
Not Required
Chain of Custody (COC) present?
Yes
No
COC agrees with sample label(s)?
Yes
No
COC properly completed
Yes
No
Samples in proper containers?
Yes
No
Sample containers intact?
Yes
No
Sufficient sample volume for indicated test(s)?
Yes
No
All samples received within holding time?
Yes
No
Cooler temperature in compliance?
Yes
No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
No
Water - Sample containers properly preserved
Yes
No
0 NIA
Water - VOA vials free of headspace
Yes
No
NIA
Trip Blanks received with VOAs
Yes
No
NIA
Soil VOA method 5035 — compliance criteria met
Yes
No0
NIA
High concentration container (48 hr)
High concentration pre -weighed (methanol -14 d)
Low concentration EnCore samplers (48 hr)
Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Yes
No
Comments:
... ... ------- __..._.........,._
Signature: ,Brandi Watson Date & Time: 02/21/2019 14:28:47
................. .

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BIO-NOMIC SERVICES
WQ0039053
Greenville Utilities WTP
Date
Fecal Coliform
MPN per gram
Log
02/19/19
712
2.8525
02/19/19
769
2.8859
02/19/19
820
2.9138
02/19/19
826
2.9170
02/19119
758
2.8797
02/I9/19
830
2.9191
02/19/19
784
2.8943
Total 1 20.2623
Average 2.8946
Geometric Mean 785 Fecal Coliform MPN / gram
Geometric Mead of Less than 2,000,000 meets Class B - Alternative 1 Pathogen for Reduction
requirement.

Analytical Results � ATFSW QJ.
ANALY A
Bio-Nomic Service, INC
530 Woodlawn Street 4k
Belmont, NC 28012
Receive Date:
02/19/2019
Reported:
02/21/2019
For:
PO #48691
Comments:
Geometric Mean <785 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
190219-29-01
Fecal Coliforms
1
<712
MPN/g
sM9221ce-2006
02120/2019
WC
190219-29-01
Percent Solids
1
2.81
%
sM25408-201,
02/20/2019
WC
190219-29-02
Fecal Coliforms
2
<769
MPN/g
SMM210E-20os
02/20/2019
WC
190219-29-02
Percent Solids
2
2.60
%
SM254oB-2011
02/20/2019
WC
190219-29-03
Fecal Coliforms
3
<820
MPN/g
SMMICE-2006
02120/2019
WC
190219-29-03
Percent Solids
3
2.55
%
SM25409-2011
02/20/2019
WC
190219-29-04
Fecal Coliforms
4
<826
MPN/g
SM9221cE•2006
02/20/2019
WC
190219-29-04
Percent Solids
4
2.42
%
SM2540B.2011
02/20/2019
WC
190219-29-05
Fecal Coliforms
5
<758
MPN/g
SM92210E-2006
02/20/2019
WC
190219-29-05
Percent Solids
5
2.54
%
SM25408-2011
02/20/2019
WC
190219-29-06
Fecal Coliforms
6
<830
MPN/g
SM92210E-2036
02/20/2019
WC
190219-29-06
Percent Solids
6
2.41
%
SM25400,2011
02/20/2019
WC
190219-29-07
Fecal Coliforms
7
<784
MPN/g
W9221cE-2006
02/20/2019
WC
19021929-07
Percent Solids
7
2.55
%
SM25408-2011
02/20/2019
WC
Respectfully submitted,
& _VVQ.0rnt-)
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 a Statesville, NC 28687 a 704/872/4697
Page 1 of 2

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Wage 2 of 2

10 MIC SERVICES
A Catylon Company
530 Woodlawn Street - Belmont, NC 28012
[phone] - Fax [phone]
TO
PURCHASE ORDER
NO. 48691
SHOW ABOVE NUMBER ON ALL SHIPMENTS,
INVOICES AND CORRESPONDENCE
(." - /� q :/ o , i
OATE
SHIP VIA
SHIP TO;
DATE WANTED
INVOICE fN DUPLICATE
PLEASE SHIP SUBJECT TO THE CONDITIONS ON FACE AND REVERSE SIDE HEREOF
CST

Willcox & Mabe Soil Solutions, PLLC
Greensboro, North: Carolina
RESIDUAL PAN CALCULATION
Greenville Utilities WTP
TK -N=
40,700
mg/kg
NH3=
3,930
mg/kg
NO3-NO2-N=
190
mg/kg
Min Rate=
0.20
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2]
0.20 36,770 1,965 190.00
PAN= 9509.00 mg/kg
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N]
0.10 36,770 7,354
PAN= 2941.60 mg/kg remaining from 1st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N]
0.05 29,416 2,942
PAN= 1411.97 mg/kg remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N]
0.03 26,474 1,412
PAN= 835.41 mg/kg remaining; from I st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N]
0.02 25,062 835
PAN= 469.52 mg/kg remaining fi-om 1st year application
Residual PAN from years 2 thru 5 after the initial application = 5658.50 mg/kg
Application
Method
First Year PAN
(mg/kg)
Five Year Maximum
Adjusted PAN
Surface
9,509
15,167
Incorporation
11,474
17,132

Ws
i
SAR Calculation
Na mgll
Ca mgll
Mg mgll
12.7224
55.521
11.2158
Na Ca Mg SAR
0.553 2.776 0.935 0.406
Na mil eq
Ca mil eq
Mg mil eq
0.553
2.776
0.935
Enter.
Enter .% TS
2.79'
Data
Na mg/kg
456
Ca mg/kg
1990.
Mg. mglkg
402:
Job Name. Greenville Utilities WTP
Page 2

NX - , Z'0011MINEWMENMERE W___
THE LEADER IN ENVIRONMENTAL- TESTING
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-168891-1
Client Project/Site: Greenville WTP
Revision: 2
For:
Bio-Nomics Services., Inc.
530 Woodlawn Street
Belmont, North Carolina 28012
Attn: Vaughn Stevenson
Authorized for release by. -
311912019
y.3/19/2019 12:40:16 PM
Ken Hayes, Project Manager 11
[phone]
ken. [e-mail]
The test results in this report meet all 2003 NELAC and 2003 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Bio -Noetics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Table of Contents
CoverPage ..............................................
1
Table of Contents .........................................
2
Sample Summary .........................................
3
Case Narrative ...........................................
4
Definitions ...............................................
5
Client Sample Results ......................................
6
QC Sample Results ........................................
8
QC Association ...........................................
20
Chronicle................................................24
Method Summary .........................................
25
Certification Summary .................................. I ...
26
Chain of Custody ..........................................
27
Receipt Checklists .........................................
30
Page 2 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)

Sample Summary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Lab Sample ID Client Sample ID Matrix Collected Received
490-168$91-1 006 Siudge 02!7911912:00 02/2111908:55
TestAmerica Nashville
Page 3 of 30 3/19/2019 (Rev. 2)

Case Narrative
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Job ID. 490-168891-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-168891-1
REVISED REPORT: Revised to report Cyanide, Sulfide, and PCBs without dry weight conversion. This report replaces the one generated
on 03/08/19 @ 1653.
Comments
While TA Pittsburgh carries South Carolina certification for 8260D and 8270E, the referenced matrix "Sludge", is causing the report to
indicate the lab as not certified for these.
No additional comments.
Receipt
The sample was received on 2/21/2019 8:55 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 3.0° C.
GUMS VOA
Method 8260D: The continuing calibration verification (CCV) analyzed in batch 180-271299 was outside the method criteria for the
following analyte: 2-Butanone. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is
considered estimated.
No additional analytical or quality issues were noted, other than those described above or in the Definition slGlossary page
GCIMS Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 101 OA: Method 1010A is applicable only to liquid matrix. This method has been modified to incorporate soil/ solid matrices of the
following sample: GUC (490-168891-1).
Method 9034—Calc: Sample GUC (490-168891-1) was analyzed for Sulfide. Sulfide as H2S level is calculated at 1303.8 mg/Kg,
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Geotechnical
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
Method 351OC: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicatelsample duplicate
(MS/MSDIDUP) associated with preparation batch 180-271274 and 180-271365.
Method 35100: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicatelsample duplicate
(MSIMSDIDUP) associated with preparation batch 180-271274 and 180-271367.
Method 8151 A: Insufficient sample volume was available to perform a matrix spikelmatrix spike duplicatelsample duplicate
(MSIMSDIDUP) associated with preparation batch 180-271274 and 180-271391.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestArnerica Nashville
Page 4 of 30 3/19/2019 (Rev. 2)

Definitions/Glossary
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Qualifiers
GCIMS Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
13 Listed under the "b" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metafstanion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 30 3/19/2019 (Rev. 2)

Client Sample Results
Client: Bio-Nomics Services., Inc.
Result Qualifier
RL
MDL Unit
TestAmerica Job ID: A90-168891-1
Project/Site: Greenville WTP
Dil Fac
Chlordane (technical)
ND
0.00500
mglL
02126/19 11:00
Client Sample ID: GUC
1
Endrin
ND
Lab Sample
ID: 490-166891-1
Date Collected: 02/19/19 12:00
02/2711916:03
1
gamma -BHC (Lindane)
ND
Matrix: Sludge
Date Received: 02/21/19 08:55
02/26/19 11:00
02/27/19 16:03
1
Heptachlor
ND
0.000500
Method: EPA 8260D - Volatile Organic Compounds
by GCIMS - TCLP
0212711916:03
1
Heptachlor epoxide
ND
Analyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Dil Fac
1,1-Dichloroethene
ND
0.200
mgiL
1
0212611909:23
1
1,2-Dichloroethane
ND
0.200
mglL
1
0212611909:23
1
2-Butanone (MEK)
ND
0.200
mglL
0212611909:23
1
Benzene
ND
0.200
mglL
02/26/19 09:23
1
Carbon tetrachloride
ND
0.200
mglL
02/26/19 09:23
1
Chlorobenzene
ND
0.200
mg1L
02/26/19 09:23
1
Chloroform
ND
0.200
mglL
02/26/19 09:23
1
Tetra chloroethene
ND
0.200
mg1L
02/26/19 09:23
1
Trichloroethene
ND
0.200
mglL
02/26/19 09:23
1
Vinyl chloride
ND
0.200
mg1L
02/26/19 09:23
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
1,2-Dichloroethane-d4 (Surr)
$9
7j-143
02126119 08:23
1
4-Bromofluorobenzene (Surr)
81
61-123
02/26/19 09:23
1
Dibromofluoromethane (Surr)
106
68-128
02/26/19 09:23
1
Toluene -d8 (Surr)
100
75-124
02/26/19 09:23
1
Method: 8270E - Serriivolatile Organic Compounds
(GC/MS) - TCLP
Anatyte
Result Qualifier
RL MDL
Unit
D Prepared
Analyzed
Dil Fac
1,4 -Dichlorobenzene
ND
0.0500
mglL
02/26/1912:10
0212711917:24
1
2,4,5-Trichforophenoi
ND
0.0500
mg1L
0212611912:10
0212711917:24
1
2,4,6 -Trichlorophenol
ND
0.0500
mg1L
02126/1912:10
0212711917:24
1
2,4-Dinitrotoluene
ND
0.0500
mg1L
0212611912:10
0212711917:24
1
Hexachlorobenzene
ND
0.0500
mglL
0212611912:10
0212711917:24
1
Hexachtorobutadiene
ND
0.0500
mglL
02126/1912:10
0212711917:24
1
Hexachloroethane
ND
0,0500
mglL
02/26/19 1210
0212711917:24
1
Nitrobenzene
ND
0.0500
mglL
02126119 1210
0212711917:24
1
Pentachlorophenol
ND
0.250
mglL
02/28119 12:10
0212711917:24
1
Pyridine
ND
0.100
mglL
02/26/19 12:10
0212711917:24
1
Cresols
ND
0.100
mglL
02/26/19 12:10
0212711917:24
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
76
25- 112
02126119 12:10
02127119 17:24
1
2-Fluorophenol (Surr)
91
61-105
02/26/19 12:10
02127119 17:24
1
2-Fluorobiphenyl
93
62-105
02126119 12:10
02127119 1724
1
Nitrobenzene -d5 (Surr)
94
64-105
02126119 12:10
02/27/19 17:24
1
Phenol -d5 (Surr)
85
47-105
02126119 12:10
02127119 17:24
1
Terphenyl-d14 (Surr)
84
45-130
02126119 12:10
02127119 17:24
1
Method: EPA 8081B - Organochlorine Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
Chlordane (technical)
ND
0.00500
mglL
02126/19 11:00
02127/19 16:03
1
Endrin
ND
0.000500
mglL
0212611911:00
02/2711916:03
1
gamma -BHC (Lindane)
ND
0.000500
mglL
02/26/19 11:00
02/27/19 16:03
1
Heptachlor
ND
0.000500
mglL
0212611911:00
0212711916:03
1
Heptachlor epoxide
ND
0.000500
mglL
02/26/19 11:00
02/27/19 16:03
1
Methoxychlor
ND
0.000500
mglL
0212611911:00
0212711916:03
1
Toxaphene
ND
0.0400
mglL
0212611911:00
0212711916:03
1
TestAmerica Nashville
Page 6 of 30 3/19/2019 (Rev. 2)

Client Sample Results
Client: Bio -Noetics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Client Sample ID: GUC Lala Sample ID: 490-168891-1
Date Collected: 02/19119 12:00 Matrix: Sludge
Date Received: 0.2121119 08:55
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
DCB Decachlorobiphenyl (Surr) 95 62-150 02126119 11:00 02127119 16:03 1
Tetrachloro-m-xylene 91 54-136 02126119 11:00 02/27/19 16:03 1
Method: BPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dif Fac
PCB 1016
ND _
16.4 .....
...... ... ug/Kg ..
02/27/19 09:52
02128/19 15:46
.......1
PCB -1221
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB -1232
ND
16.4
ug/Kg
0212711909:52
0212811915:46
1
PCB -1242
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB -1248
ND
16.4
ug1Kg
02127/19 09:52
02/28/19 15:46
1
PCB -1254
ND
16.4
ug/Kg
02/27/19 09:52
02/28/19 15:46
1
PCB -1264
ND
16.4
uglKg
02/27/19 09:52
02/28/19 15:46
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Tetrachloro-m-xylene (Surr)
8i
51- 116
02127119 09:52
02128/19 15:46
1
DCB Decachlorobiphenyl (Surr)
87
44-116
(CVAA) - TCLP
02127119 09:52
02/28/19 15:46
1
Method: BPA 8151A - Herbicides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed
Dil Fac
2,4-0
ND
0.0400
mg
02)26/1914M
02/28/19 01:14
20
Silvex (2,4,5 -TP)
ND
0.0100
mg/L
02/26/1914:30
02/281190114
20
2,4,5-T
ND
0.0100
mg/L
02/26/19 14:30
02/28/19 01:14
20
Surrogate
%Recovery Qualifier
Limits
mglL
Prepared
Analyzed
Dil Fac
2,4-Dichlorophenylacefic acid
73
20- 105
0.500
02126119 14:30
02128119 01:14
20
Method: BPA 6010D - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dif Fac
Arsenic
ND
0.500
mg/L
02/26/19 12:20
02127119 09:13
1
Barium
ND
2.00
mg/L
02/26/19 12:20
02127119 09:13
1
Cadmium
ND
0.500
mglL
02/26/19 12:20
02127119 09:13
1
Chromium
ND
0.500
mglL
02/26/19 12:20
02/27/19 09:13
1
Lead
ND
0.500
mglL
02126/19 12:20
02127/19 09:13
1
Selenium
ND
0.500
mglL
02/26119 12:20
02/27/19 09:13
1
Silver
ND
0.500
mglL
02126/19 12;20
02/27/19 09:13
1
Method: EPA 7470A - Mercury
(CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Mercury
ND
0.000200
mg1L
02/26/19 11:05
0212611916:17
1
General Chemistry
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
.....
Cyanide, Total
ND
0.505
mg/Kg
03/01/19 12:40
03/01/19 19:32
......
Total Sulfide
31.7
30.0
mg/Kg
0212611909:35
02/26/19 11:20
1
Analyte
Result Qualifier
RL
RL
Unit
D
Prepared
Analyzed
Dil Fac
Flashpoint
X200
1.00
Degrees F
03/01/19 17:29
1
Percent Moisture
97.4
0.1
%
02/27/19 08:43
1
Percent Solids
2.6
0.1
%
02/27/19 08:43
1
pH
6.6 HF
0.1
SU
02127/19 12:00
1
TestAmerica Nashville
Page 7 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
TestAmerica Job ID: 490-168891-1
Lab Sample ID: LCS 180-27129913
Sample Sample
Spike
MS MS
Client Sample ID: Lab Control Sample
Matrix: Solid
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Prep Type: Total/NA
Analysis Batch: 271299
ND
1.60
1.556
mg/L
97
57-135
1,2-Dichloroethane
ND
1.60
Spike
LCS
LCS
69-127
2-Butanone (MEK)
%Rea
Analyte
0.8771
Added
Result
Qualifier
Unit
D %Roe
Limits
1,1-Di6hioroethene
0.0400
0.04011
m g I L
100
57 - 135
1,2-Dichloroethane
0.0400
0.03331
mg/L
83
69-127
2-Butanone(MEK)
0.0400
0.02829
mg/L
71
36-150
Benzene
0.0400
0.04064
mg/L
102
66-124
Carbon tetrachloride
0.0400
0,04205
mg/L
105
69-130
Chlorobenzene
0.0400
0.04443
mg/L
111
72-122
Chloroform
0.0400
0.03950
mg/L
99
69-119
Tetrachloroethene
0.0400
0.04642
mg1L
116
73-129
Trichloroethene
0.0400
0.04744
mg/L
119
75-122
Vinyl chloride
0.0400
0.03919
mg1L
98
57-132
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr) 80
73-143
4-Bromofluorobenzene (Surr) 97
61-123
Dibromofluoromethane (Surr) 105
68-128
Toluene -d8 (Surr) 103
75-124
Lab Sample ID: LB 180-27131211-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271299
LB LB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
.........................
1,1-Dichioroethene
ND
0.0500
mg1L
02/26/19 09:01 i
1,2-Dichloroethane
ND
0.0500
mg/L
02/26/19 09:01 1
2-Butanone (MEK)
ND
0.0500
mg/L
02/26/19 09:01 1
Benzene
ND
0.0500
mg/L
02/26/19 09:01 1
Carbon tetrachloride
ND
0.0500
mg/t-
02/26/19 09:01 1
Chlorobenzene
ND
0.0500
mg/L
02/26/19 09:01 1
Chloroform
ND
0.0500
mg/L
02126/19 09:01 1
Tetra chloroethene
ND
0.0500
mg/L
02/26/19 09:01 1
Trichloroethene
ND
0.0500
mg/L
02/26/19 09:01 1
Vinyl chloride
ND
0.0500
mg/L
02/26/19 09:01 1
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed til Fac
i12-D1ch1or6ethane-d4 (Surr)
85
73-143
02126119 09:01 1
4-Bromofluorobenzene (Surr)
82
61-123
02126119 09:01 1
Dibromofluoromethane (Surr)
102
68-128
02/26/19 03:01 1
Toluene -d8 (Surr)
104
75-124
02/26/19 09:01 1
Lab Sample ID: 490-168891-1 IVIS
Matrix: Sludge
Analysis Batch: 271299
Client Sample ID: GLIC
Prep Type: TCLP
TestAmerica Nashville
Page 8 of 30 3/19/2019 (Rev. 2)
Sample Sample
Spike
MS MS
%Ree.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
1,1-Dichloroethene
ND
1.60
1.556
mg/L
97
57-135
1,2-Dichloroethane
ND
1.60
1.409
mg1L
88
69-127
2-Butanone (MEK)
ND
1.60
0.8771
mg/L
55
36-150
TestAmerica Nashville
Page 8 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 8260D - Volatile Organic Compounds by GCIMS (Continued)
Lab Sample ID: 490-168891-1 MS Client Sample ID: GUC
Matrix: Sludge prep Type: TCLP
Analysis Batch: 271299
Method: 8270E - Semivolatile Organic Compounds (GCIMS)
Lab Sample ID: MB 180-27136711-A Client Sample Ila: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271438 Prep Batch: 271367
Analyte
.............. ..
1,4 -Dichlorobenzene
2,4,5-TricNorophenol
2,4,6 -Trichlorophenol
2,4-Dinitrotoluene
MB MB
Result Qualifier
ND
ND
ND
ND
RL
Sample
Sample
Spike
MS
MS
mglL
02/26/19 12:10
%Rec.
1
0.0500
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
0.0500
mg1L
Benzene
ND
1
1.60
1.613
mg/L
101
66-124
Carbon tetrachloride
ND
1.60
1.711
mglL
107
0-130
Chlorobenzene
ND
1.60
1.768
mglL
111
72-122
Chloroform
ND
1.60
1.638
mglL
102
69-119
Tetrachloroethene
ND
1.60
1.815
mglL
113
73-129
Trichloroethene
ND
1.60
1.869
mg/L
117
75-122
Vinyl chloride
ND
1.60
1.383
mg/L
86
57-132
MS
MS
Surrogate
%Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
85
7j-143
4-Bromofluorobenzene (Surr)
98
61-123
Dibromof7uoromethane (Surr)
104
68-f28
Toluene -d8 (Surr)
101
75-124
Lab Sample ID: 490-168891-1 MSD
Client
Sample
Ila:
GUC
Matrix: Sludge
Prep
Type: TCLP
Analysis Batch: 271299
Sample
Sample
Spike
MSD
MSD
%Rec.
RPD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
D %Rec
Limits
RPD
Limit
1,1 Dichloroethen.e....
ND
1.60
1.702
mg1L ......
106
....57-135
9
35
1,2-Dichloroethane
ND
1.60
1.434
mg1L
90
69-127
2
16
2-Butanone (MEK)
ND
1.60
0.9013
mglL
56
36-150
3
35
Benzene
ND
1.60
1.638
mglL
102
66-124
2
16
Carbon tetrachloride
ND
1.60
1.689
mg1L
106
69-130
1
17
Chlorobenzene
ND
1.60
1.798
mg/L
112
72-122
2
15
Chloroform
ND
1.60
1.639
mglL
102
69-119
0
16
Tetrachloroethene
ND
1.60
1.882
mg/L
118
73-129
4
15
Trichloroethene
ND
1.60
1.879
mglL
117
75-122
1
15
Vinyl chloride
ND
1.60
1.558
mglL
97
57-132
12
21
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
1,2-Dichloroethane-d4 (Surr)
87
73-143
4-Bromofluorobenzene (Surr)
99
61-123
Dibromofluoromethane (Surr)
106
68-128
Toluene -d8 (Surr)
105
75-124
Method: 8270E - Semivolatile Organic Compounds (GCIMS)
Lab Sample ID: MB 180-27136711-A Client Sample Ila: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271438 Prep Batch: 271367
Analyte
.............. ..
1,4 -Dichlorobenzene
2,4,5-TricNorophenol
2,4,6 -Trichlorophenol
2,4-Dinitrotoluene
MB MB
Result Qualifier
ND
ND
ND
ND
RL
MDL Unit
D Prepared
Analyzed
Dii Fac
0.0500
mglL
02/26/19 12:10
02127119 139:11
1
0.0500
mglL
02/26/19 12:10
02/27/19 09:11
1
0.0500
mg/L
02/26/19 12:10
02/27/19 09:11
1
0.0500
mg1L
02/26/19 12:10
02/27/19 09:11
1
Page 9 of 30
TestArnerica Nashville
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nornics Services., Inc. TestArnerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: 8270E - Sernivolatile Organic Compounds (GCIMS) (Continued)
Lab Sample IIT: MB 180-27136711-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
MB
MB
Analyte Result
Qualifier
RL
MDL Unit
D Prepared
Analyzed Dit Fac
Hexachlorobenzene
ND
0.0500
mglL
02126/19 12:10
02127/19 09:11 1
Hexachlorobutadiene
NO
0.0500
mg1L
02126/19 12:10
02/27/19 09:11 1
Hexachloroethane
NO
0.0500
mg1L
02126/19 12:10
02127119 09:11 1
Nitrobenzene
ND
0.0500
mg1L
02/26/19 12:10
02127/19 09:11 1
Pentachlorophenol
NO
0.250
mg1L
02/26/19 12:10
02127/19 09:11 1
Pyrid€ne
NO
0.100
mg1L
02/26/19 12:10
02127/19 09:11 1
Cresols
NO
0.100
mg1L
02/26/19 12:10
02127/19 09:11 1
MS
MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed bit Fac
2,4,6-Tribromophenol (Surr)
83
25. 112
02/26/79 12:10
02/27/19 09:11 1
2-Fluorophenol (Surr)
87
61-105
02/26/19 12:10
02127119 09:11 1
2-Fluorobiphenyl
83
62-105
02126119 12:10
02127119 09:11 1
Nitrobenzene -d5 (Surr)
83
64-105
02126119 12:10
02127179 09:11 1
Phenol -d5 (Surr)
86
47-105
02/26/19 12:10
02127119 09:11 1
Terpherlyl-04 (Surr)
75
45-130
02126119 12.10
02/27/19 09:11 1
Lab Sample ID: LCS 180-27136712-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Tota!/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
1,4 -Dichlorobenzene
0.250
0.2277
mglL
91
... ..........
57.100
2,4,5 -Trichlorophenol
0.250
0.2157
mglL
86
58-100
2,4,6 -Trichlorophenol
0.250
0.2096
mglL
84
57-100
2,4-Dinitrotoluene
0.250
0.2023
mglL
81
40-100
Hexachlorobenzene
0.250
0.1527
mglL
61
38-100
Hexachlorobutadiene
0.250
0.2146
mg1L
86
53-105
Hexachloroethane
0.250
0.2352
mg/L
94
57-100
Nitrobenzene
0.250
0.2299
mglt.
92
56.103
Pentachlorophenoi
0.250
0.1630
J
mg1L
65
16-100
Pyridine
0.250
0.2391
mg1L
96
51-107
Cresols
0.750
0.6754
mg1L
90
54.103
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
2,4,6-Tribromophenol (Surr) 88
25- 112
2-Fluorophenol (Surr) 90
61-105
2-Fluorobiphenyl 86
62-105
Nitrobenzene -d5 (Surr) 90
64-105
Phenol -d5 (Surr) 90
47-105
Terphenyl-d14 (Surr) 69
45-130
Lab Sample ID: LCSD 180-27136713-A
Client
Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits RPD Limit
1,4 -Dichlorobenzene
0.250
0.2220
.....
mg/L.......
89
.3 1.5
57-100
2,4,5 -Trichlorophenol
0.250
0.2095
mg1L
84
58-100 3 16
TestAmerica Nashville
Page 10 of 30 3/19/2019 (Rev, 2)
11

QC Sample Results
Client: Bio-Nomics Services,, Inc.
Project/Site: Greenville WTP
Method: 8270E - Semivolatile Organic Compounds (CC/MS) (Continued)
TestAmerica Job Ila: 490-168891-1
Lab Sample ID: LCSD 180-27136713-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271438
Prep Batch: 271367
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
0 %Rec
Limits RPDLimit
2,4,6-Tr€chlorophenol
0.250 ..
0.2135
._..... ....
rn L
_ ... 85 ....57-940 2
15
2,4-Dinitrotoluene
0.250
0.1977
mg/L
79
40-100 2 15
Hexa chloro benzene
0.250
0.1553
mg/L
62
38-100 2 16
Hexachlorobutadiene
0.250
0.2085
mglL
83
53-105 3 15 �
Hexachloroethane
0.250
0.2259
mg/L
90
57-100 4 18
Nitrobenzene
0.250
0.2141
mg1L
86
56-103 7 15
Pentachlorophenol
0.250
0.1462
3
mg/L
58
16-100 11 24
Pyridine
0.250
0.2257
mglL
90
51-107 6 18
Cresols
0.750
0.6719
mglL
90
54-103 1 17
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
66
25-112
2-Fluorophenol (Surr)
86
61-105
2-Fluorobiphenyl
86
62-105
Nitrobenzene -d5 (Surr)
84
64-105
Phenol -d5 (Surr)
86
47-105
Terphenyl-d14 (Surr)
68
45- 130
Lab Sample ID: LB 180-271274/1-D
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271438
Prep Batch: 271367
LB LB
Analyte
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
1,4 -Dichlorobenzene
ND
0.0500
mglL
02/26119 1Z 10
0212711911:33 1
2,4,5 -Trichlorophenol
ND
0.0500
mglL
02126119 12:10
02/2711911:33 1
2,4,6 -Trichlorophenol
ND
0.0500
mg1L
02/26/19 12:10
0212711911:33 1
2,4-Dinitrotoluene
ND
0.0500
mglL
02/26/19 12: 10
0212711911:33 1
Hexachloro benzene
ND
0.0500
mg/L
02/26/19 12:10
02/2711911:33 1
Hexachlorobutadiene
ND
0.0500
mg/L
02/26/19 12:10
02/2711911:33 1
Hexachloroethane
ND
0.0500
mg/L
02/26/19 12:10
02/2711911:33 1
Nitrobenzene
ND
0.0500
mg/L
0212611912:10
0212711911:33 1
Pentachlorophenol
ND
0.250
mg/L
0212611912:10
02/2711911:33 1
Pyridine
ND
0.100
mg/L
0212611912:10
02/2711911:33 1
Cresols
ND
0.100
mg/L
0212611912:10
02/2711911:33 1
LB LB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4,6-Tribromophenol (Surr)
8$
25- 112
02/26/19 12:10
02127/19 11:33 1
2-Fluorophenol (Surr)
85
61-105
02/26/19 12:10
02127/19 11:33 1
2-Fluorobiphenyl
85
62-105
02/26/19 12:10
02/27/19 i 1:33 1
Nitrobenzene -d5 (Surr)
87
64-105
02126119 12,10
02/27/19 11:33 1
Phenol -d5 (Surr)
87
47-105
02/26/19 12:10
02/27/19 11:33 1
Terphenyl-d14 (Surr)
74
45-130
02/26/19 12.10
02127119 11:33 1
TestAmerica Nashville
Page 11 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville V TP
Method: EPA 8081 B W Organochlorine Pesticides (GC)
Lab Sample ID: MB 180-27136511-A
Matrix: Solid
Analysis Batch: 271475
Analyte
Chlordane (technical)
Endrin
gamma -BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogate
DCB Decachlorcbiphenyl (Surr)
Tetrachloro-m-xylene
MB MB
Client Sample ID: Method Blank
Result Qualifier
RL
ND
0.00500
ND
0.000500
ND
0.000500
ND
0.000500
ND
0.000500
ND
0.000500
ND
0.0400
MB MB
02127/1913:14 1
%Recovery Qualifier
Limits
94
V- 150. .
91
54-138
Lab Sample ID: LCS 180-27136512-A
Matrix: Sofid
Analysis Batch: 271475
Analyte
Endrin
gamma -BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Page 12 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)
Client Sample ID: Method Blank
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271365
MDL Unit
D Prepared
Analyzed Oil Fac
mg/L
0212611911:00
02127/1913:14 1
mglL
02126119 11:00
02127/1913:14 1
mglL
0212611911:00
02127/1913:14 1
mglL
0212611911:00
02127/1913:14 1
mglL
0212611911:00
0212711913:14 1
mglL
0212611911:00
02127/1913:14 1
mglL
0212611911:00
0212711913:14 1
66.127
Prepared
Analyzed Dil Fac
mglL
02/26119 11: oo
02/27/19 1314 9
0.0100
0212611911:00
0212711913:14 1
Page 12 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)
LCS LCS
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Recovery Qualifier
Limits
Prep Batch: 271365
Spike
LCS LCS
95
62- i50
%Rec.
Added
Result Qualifier
Unit
17 %Rec
Limits
0.0100
0.009924
mg1L
99
71- 134
0.0100
0.008481
mglL
85
66.127
0.0100
0.009290
mglL
93
66-134
0.0100
0.008870
mglL
89
65-141
0.0100
0.01001
mg1L
100
59-131
Page 12 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)
LCS LCS
Surrogate
%Recovery Qualifier
Limits
DCS Decachlorobi'phenyt (Surr)
95
62- i50
Tetrachloro-m-xylene
96
54-138
Lab Sample ID: LCSD 180-27136513-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271475
Prep Batch. 271365
Spike
LCSD LCSD
%Rec. RAD
Analyte
Added
Result Qualifier Unit
D %Rec
Limits RPD Limit
Endrin
0.0100
0.009900
mglL
99
71-134 0 18
gamma -BHC (Lindane)
0.0100
0.008743
mglL
87
66-127 3 15
Heptachlor
0.0100
0.009428
mgll-
94
66.134 1 15
Heptachlor epoxide
0.0100
0.008791
mglL
88
65-141 1 15
Methoxychlor
0.01 DD
0.009889
mglL
99
59-131 1 28
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
DC8 Decachlorobiphenyt (Surr)
95
62-150
Tetrachloro-m-xylene
93
54-138
Page 12 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio -Noetics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 80818 - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LB 180-271274116-E
Matrix: Solid
Analysis Batch: 271475
Analyte
Chlordane (technical)
Endrin
gamma -BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychior
Toxaphene
LB LB
Result Qualifier
ND
ND
ND
ND
ND
ND
ND
TestAmerica Job ID: 490-168891-1
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 271365
RL
MDL Unit
D Prepared
Analyzed
0.00500
mglL ..........
02/28/19 11:06
02/27/19 14:15
0.000500
mglL
0212611911:00
0212711914:15
0.000500
mg1L
0212611911:00
0212711914:15
0.000500
mglL
0212611911:00
02/27/1914:45
0.000500
mglL
02/26/19 11:00
0212711914:15
0.000500
mglL
0212611911:00
0212711914:15
0.0400
mglL
0212611911:00
02127119 14: 15
Dil Fac
1
1
1
1
1
1
LB LB
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
DCB Decachlorobiphenyl (Surr) 98 62- 150 02126119 11:00 02127119 14:15 1
Tetrachloro-m xylene 92 54-138 02125119 11:00 02127119 14:15 1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Lab Sample ID: MB 180-271476/1-A
Matrix: Solid
Analysis Batch: 271567
Analyte
PCB -1016
PCB -1221
PCB -1232
PCB -1242
PCB -1248
PCB -1254
PCB -1260
Surrogate
Tetrachloro-m-xylene (Surr)
DCB Decachlorobiphenyl (Surr)
MB MB
%Recovery Qualifier Limits
91 51-116
94 44-116
Lab Sample ID: LCS 180-271476/2-A
Matrix: Solid
Analysis Batch: 271567
Analyte
PCB -1016
PCB -1260
Prepared Analyzed DI! Fac
02127/19 09:52 02128119 13:54 1
02127119 09:52 02128119 13:54 1
Client Sample ID: Lab Control Sample
Client Sample 1D: Method Blank
Prep Type: Total/NA
Prep Type: Total/NA
Spike
LCS LCS
%Rec.
Added
Prep Batch: 271476
MS MB
1330
1090
ug/Kg 82 57-114
1330
Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dit Fac
ND
16.7
ug/Kg
02127/19 09:52
02128/19 13:54 1
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
ND
16.7
ug/Kg
02/27/19 09:52
02128119 13:54 1
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
ND
16.7
ug/Kg
02/27/19 09:52
02/28/19 13:54 1
MB MB
%Recovery Qualifier Limits
91 51-116
94 44-116
Lab Sample ID: LCS 180-271476/2-A
Matrix: Solid
Analysis Batch: 271567
Analyte
PCB -1016
PCB -1260
Prepared Analyzed DI! Fac
02127/19 09:52 02128119 13:54 1
02127119 09:52 02128119 13:54 1
LCS LCS
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Surr) '85 51-116
DC8 Decachlorobiphenyl (Surr) 87 44-116
TestArnerica Nashville
Page 13 of 30 3/19/2019 (Rev. 2)
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 271476
Spike
LCS LCS
%Rec.
Added
Result Qualifier
Unit D %Rec Limits
1330
1090
ug/Kg 82 57-114
1330
1059
uglKg 79 55-112
LCS LCS
Surrogate %Recovery Qualifier Limits
Tetrachloro-m-xylene (Surr) '85 51-116
DC8 Decachlorobiphenyl (Surr) 87 44-116
TestArnerica Nashville
Page 13 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
TestAmerica Job ID: 490-168891-1
Method: EPA 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)
Lab Sample ICI: 490-168890-B-1 -J MS
Matrix: Solid
Analysis Batch: 271567
Sample Sample
Spike
Analyte Result Qualifier
Added
N.p .... ...
1330
PCB -1260 NO
1330
MS MS
Surrogate %Recovery Qualifier
Tetrachloro-m-xylene (Surr) 66
DC8 Decachlorobiphenyl (Surr) 72
Lab Sample ID: 490 -168890 -B -1-K MSD
Matrix: Solid
Analysis Batch: 271567
Method: EPA 8151A - Herbicides (GC)
Lab Sample ID: MB 180-27139111-A
Matrix: Solid
Analysis Batch: 271555
Analyte
2,4-D
Silvex (2,4,5 -TP)
2,4,5-T
Surrogate
2 Q bichlorophenylacetic acid
Limits
51_116
44-116
Sample Sample
Analyte
Result Qualifier
PCB -1016
NO
PCB-1260
ND
Prep Batch: 271476
MSD MSD
Surrogate
%Recovery Qualifier
Tetrachloro-m-xylene (Surr)
64
DCB Decachlorobiphenyl (Surr)
71
Method: EPA 8151A - Herbicides (GC)
Lab Sample ID: MB 180-27139111-A
Matrix: Solid
Analysis Batch: 271555
Analyte
2,4-D
Silvex (2,4,5 -TP)
2,4,5-T
Surrogate
2 Q bichlorophenylacetic acid
Limits
51_116
44-116
Limits
51-116
44-116
MB MB
Result Qualifier RL
ND 0.0400
ND 0.0100
ND 0.0100
Ma MB
%Recovery Qualifier Limits
....
71 20-105
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271391
MDL Unit
D Prepared
Client Sample ID: Matrix Spike
Oil Fac
mglL
Prep Type: Total/NA
02/27/19 20:57
26
Prep Batch: 271476
MS MS
MSD MSD
%Ree.
Result Qualifier
unit
D %Rec Limits
908.3
ug/Kg . ..
_ _ 68 57-114
933.1
ug/Kg
70 55-112
Limits
51-116
44-116
MB MB
Result Qualifier RL
ND 0.0400
ND 0.0100
ND 0.0100
Ma MB
%Recovery Qualifier Limits
....
71 20-105
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271391
MDL Unit
D Prepared
Client Sample ID: Matrix Spike Duplicate
Oil Fac
mglL
Prep Type: Total/NA
02/27/19 20:57
26
Prep Batch: 271476
Spike
MSD MSD
%Rec. RPD
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
1290
831.7
ug/Kg 64 57-114 9 34
1290
837.2
uglKg 65 55-112 11 16
Limits
51-116
44-116
MB MB
Result Qualifier RL
ND 0.0400
ND 0.0100
ND 0.0100
Ma MB
%Recovery Qualifier Limits
....
71 20-105
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 271391
MDL Unit
D Prepared
Analyzed
Oil Fac
mglL
02/26/1914M
02/27/19 20:57
26
mglL
02126/19 14:30
02/27/19 20:57
20
mglL
02/26M914:30
0212711920:57
20
Prepared
Analyzed
Dil Fac
02126119 14:30
02/27/19 20:57
20
Lab Sample ID: LCS 180-27139112-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271555
Prep Batch: 271391
Spike
LOS LOS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
2,4-D
0.200
0.1340
mglL
67
10 - 100
Silvex(2,4,5-TP)
0.0500
0.03454
mglL
69
23-109
2,4,5-T
0.0500
0.02981
mglL
60
11-101
LOS LOS
Surrogate %Recovery Qualifier
Limits
2,4-bichlorophenylacetic acid 67
20- 105
Page 14 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCSD 180-27139113-A
Client Sample ID: Lab
Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271555
Prep Batch: 271391
Spike
LCSD LCSD
%Ree. RPD
Analyte
Added
Result Qualifier
Unit
D %Ree
Limits RPD Limit
2,4-D
0.200
0.1578
mg/L
79
10 -100 16 35
Silvex (2,4,5 -TP)
0.0500
0.04003
mg/L
80
23-109 15 35
2,4,5-T
0.0500
0.03558
mg1L
71
11-101 18 35
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
2,4-6i6hlarophenylacetic acid 78
20-105
Lab Sample ID: LB 180-271274/16-G
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271555
Prep Batch: 271391
LB LB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
2,4-D ND
0.0400
mg/L
02/26/19 14:30
02/27/19 22:24 20
Silvex (2,4,5 -TP) ND
0,0100
mg1L
02/26119 14:30
02/27/19 22:24 20
2,4,5-T Nn
0.0100
mg/L
02/26/19 14:30
02!27!19 22:24 20
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4-Dichlorophenylacetic acid 60
20 - 105
02/26/19 14:30
02/27/19 22:24 20
Method: EPA 6010D - Metals (ICP)
Lab Sample ID: MB 180-27135511-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271499
Prep Batch: 271355
MB MB
Analyte Result Qualifier
RL
MDL Unit
D Prepared
Analyzed Dil Fac
Arsenic ND
0.0500
mg/L
02/26/19 12:20
02/27/19 07:50 1
Barium ND
0.200
mg/L
02126119 12:20
02/27/19 07:50 1
Cadmium ND
0.0500
mg1L
02126119 12;20
02/27/19 07:50 1
Chromium ND
0.0500
mg1L
02/26/19 12:20
02/27/19 07:50 1
Lead ND
0.0500
mg/L
02/26/19 12:20
02/27/19 07:50 1
Selenium ND
0.0500
mg/L
02126/19 12:20
02/27/19 07:50 1
Silver ND
0.0500
mg/L
02126119 l2:20
02/27/19 07:50 1
Lab Sample ID: LCS 180-27135512-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271499
Prep Batch: 271355
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Arsenic
0.500
0.5281 ........ .....
mglL.
.. .. 106
80-120
Barium
2,00
2.051
mg/L.
103
80-120
Cadmium
0.0500 0.05449
mg/L
109
80-120
Chromium
0.200
0.2054
mg/L
103
80-120
Lead
0.500
0.5102
mg1L
102
80-120
Selenium
0.500
0.5558
mg&
111
80.120
Silver
0.0500 0.05381
mg/L
108
80-120
TestAmerica Nashville
Page 15 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nornics Services., Inc.
TestAmerica Job ID: 490-168891-1
Prcject/Site: Greenville 1NTP
Method: EPA 6010D - Metals (ICP)
(Continued)
Lab Sample ID: LB 180-271274/1-C
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271499
Prep Batch: 271355
LB LB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed oil Fac
Arsenic
ND
0.500 mg/L
02/26/19 12:20 02/27/19 08:00 1
Barium
ND
2.00 mg/L
02/26/19 12:20 02/27/19 08:00 1
Cadmium
ND
0.500 mg/L
02126/99 12:20 02/27/19 08:00 1
Chromium
ND
0.500 mg/L
02/26/19 12:20 02/27/19 08:00 1
Lead
ND
0.500 mg/L
02126119 12:20 02/27/19 08:00 1
Selenium
ND
0.500 mg/L
02/26119 12:20 02/27/19 08:00 1
Silver
ND
0.500 mg/L
02/26/19 12:20 02/27119 08:00 1
Method: EPA 7470A - Mercury (CVAA)
Lab Sample ID: MB '180-27134211-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271395
Prep Batch: 271342
MB MB
Analyte Result Qualifier
RL MDL Unit
D PreAnalyzed Dil Fac
Mercury
Nil
0.000200 mg/L
1 11.pared
0212611 9 1 1:05 0212611916:00 1
Lab Sample ID: LCS 180-27134212-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271395
Prep Batch: 271342
Spike LOS LOS
%ROC.
Analyte
Added Result Qualifier
Unit D %Rec Limits
Mercury
0.00250 0.002605
mg1L 104 80-120
Lab Sample ID: LB 180-27127411-B
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
LB LB
Analyte Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fac
Mercury
ND
0.000206 mglL.
621M/1911:05 0212611916:02 1
Lab Sample ID: 180-86915-A-1-1 MS
Client Sample ID: Matrix Spike
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample
Sample
Spike MS MS
%Rec.
Analyte Result
Qualifier
Added Result Qualifier
Unit D %Rec Limits
Mercury ND
0.00500 .... 0.005020 .......
mglL ... __...100 ...75.125
Lab Sample ID: 180 -86915 -A -1-J MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 271395
Prep Batch: 271342
Sample
Sample
Spike MSD MSD
%Rec. RPD
Analyte Result
Qualifier
Added Result Qualifier
Unit D %Roo Limits RPD Limit
Mercury ND
0.00500 0.005026
mg/L ....... 101 75-125 0 20
TestAmerica Nashville
Page 16 of 30 3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: 1010A - Ignitability, Pensky-(Martens Closed -Cup
Method
Lab Sample ID: MB 490-57837211
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
MB MB
Analyte Result Qualifier
RL
RL Unit D Prepared Analyzed Dil Fac
Flashpoint > 1. 200
1.00
Degrees F 03/61/19 17:29 1
Lab Sample ID: LCS 490-57837212
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Spike LCS
LCS %Rec.
Analyte
Added Result
Qualifier Unit D %Rec Limits
Flashpoint
81.0 81.20
Degrees F 100 94-106
Lab Sample ID: LCSD 490-578372114
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Spike LCSD
LCSD %Rec. RPD
Analyte
Added Result
Qualifier Unit D %Rec Limits RPD Limit
Flashpoint _
81...0 83.4fl
..... Degrees.F 1.03 .9.4 106 3 20
Lab Sample ID: 280-120182-A-1 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 578372
Sample Sample
DU
DU RPD
Analyte Result Qualifier
Result
Qualifier Unit D RPD Limit
Flashpoint 128
134.3
Degrees F 5 10
Method: 2540G - SM 2540G
Lab Sample ID: 180-86358-B-20 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271450
Sample Sample
DU
DU RPD
Analyte Result Qualifier
Result
Qualifier Unit D RPD Limit
Percent Moisture 26.5
28.2
...... .. .......... 6 ...1.0
Percent Solids 73.5
71.8
% 2 10
(Method: EPA 9012B - Cyanide, Total ardor Amenable
Lab Sample ID: MB 180-27176014-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
MB MB
Analyte Result Qualifier
RL MDL Unit D Prepared Analyzed Dil Fac
Cyanide, Total ND
0.500
M9 9 03/01/19 12:40 03101/19 19:23 1
Lab Sample ID: HLCS 18027176012-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Spike HLCS
HLCS %Rec.
Analyte
Added Result
Qualifier Unit D %Rec Limits
cyanide, Total
0.250 0.2479
mg/Kg 99 90-110
Page 17 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method: EPA 90128 - Cyanide, Total andor Amenable (Continued)
TestAmerica Job ID: 490-168891-1
Lab Sample ID: LCS 180-27176013-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total
190
114.2
mg/Kg 60 26 -139
Lab Sample ID: LLCS 180-271760/1 -A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271809
Prep Batch: 271760
Spike
LLCS LLCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Cyanide, Total
0.0500
0.04970
mg/Kg 99 90 - 110
Lab Sample ID: 180 -87076 -D -1-B MS
Matrix: Solid
Analysis Batch: 271809
Sample Sample
Analyte Result Qualifier
cyanide, Total 0.655
Lab Sample ID: 180 -87076 -D -1-C MSD
Matrix: Solid
Analysis Batch: 271809
Spike MS IVIS
Added Result Qualifier Unit
5.05 5.182 .... mg?Kg
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 271760
%Rec.
D %Rec Limits
90 75-125
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 271760
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
Cyanide, Total 0.655 5.05 5.268 mglKg 91 75-125 2 20
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)
Lab Sample ID: MB 180-27131911-A Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Sulfide ND 30.0 mg/Kg 02/2611909:35 02/25/19 11:15 1
Lab Sample ID: LCS 180-27131912-A Client Sample ID: Lab Control Sample
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 271334 Prep Batch: 271319
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
Total Sulfide 150 144.3 mg/Kg 97 85-115
Lab Sample ID: 490 -168890 -B -1-C MS
Matrix: Solid
Analysis Batch: 271334
Sample Sample Spike
Analyte Result Qualifier Added
Total Sulfide 57.0 150
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 271319
MS MS %Rec.
Result Qualifier Unit D Rec Limits
223.2 mg/Kg 111 75.125
Page 18 of 30
TestAmerica Nashville
3/19/2019 (Rev. 2)

QC Sample Results
Client: Bio-Nomics Services., Inc.
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Method: EPA 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)
Lab Sample ID: 490 -168890 -B -1-D MSD
Client Sample ID: Matrix Spike Duplicate
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271334
Prep Batch: 271319
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit D %Rec Limits RPD Limit
Total Sulfide 57.0
149 ...
...208..1.
m 11g .. __. .. ....._102 ...75...125 7 .....20
Method: EPA 9045D - pH -
............. ..
4
Lab Sample ID: LCS 180-27150611
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 271506
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
pH
7.00
7.0
SU 101 99.101
Lab Sample ID: 180-86977-J-1 DU
Client Sample ID: Duplicate
Matrix: Solid
Prep Type: TotallNA
Analysis Batch: 271506
Sample Sample
DU DU
RPD
Analyte Result Qualifier
Result Qualifier
Unit D RPD Limit
P H 3.6
3.6
SU 0 2
TestAmerica Nashville
Page 19 of 30 3/19/2019 (Rev. 2)

CSC Association Summary
Client: Bio-Nomics Services., Inc.
Client Sample ID
Prep Type
TestAmerica Job ID:
490-168891-1
Project/Site: Greenville WTP
490 168891.1
GUC.
TCLP
Sludge
GC/MS VOA
.................................
LB 180-271274116-E
Method Blank
TCLP
Solid
Analysis Batch: 271299
LB 180-271274116-G
Method Blank
TCLP
Lab Sample ID
Client Sample ID
Prep 'Type
Matrix
Method
Prep Batch
490 168891 1...
GtJC _
TCLP ..
Sludge
........... EPA 826013 _
- 271312
LB 180-27131211-A
Method Blank
TCLP
Solid
EPA 8260D
271312
LCS 184-27129913
Lab Control Sample
Total/NA
Solid
EPA 8260D
TCLP
490-168891-1 MS
GUC
TCLP
Sludge
EPA 8260D
271312
490-168891-1 MSD
GUC
TCLP
Sludge
EPA 8260D
271312
Leach Batch: 271312
3510C
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
EPA 1311
LB 180-27131211-A
Method Blank
TCLP
Solid
EPA 1311
490-168891-1 MS
GUG
TCLP
Sludge
EPA 1311
490-168891-1 MSD
GUC
TCLP
Sludge
EPA 1311
GCIMS Sete VOA
Leach Batch: 271274
Lab Sample ID
Client Sample 10
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC............ _
TCLP
Sludge _
EPA..1.31.1.. _ ....
LB 180-27127411-D
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 271367
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
3510C
271274
LB 180-27127411-D
Method Blank
TCLP
Solid
3510C
271274
MB 180-27136711-A
Method Blank
Total/NA
Solid
3510C
LCS 180-27136712-A
Lab Control Sample
Total/NA
Solid
3510C
LCSD 180-27136713-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Analysis Batch: 271438
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
8270E
271367
LB 180-27127411-D
Method Blank
TCLP
Solid
8270E
271367
MB 180-27136711-A
Method Blank
Total/NA
Solid
8270E
271367
LCS 180-27136712-A
Lab Control Sample
Total/NA
Solid
8270E
271367
LCSD 180-27136713-A
Lab Controf Sample Dup
Total/NA
Solid
8270E
271367
GC Semi VOA
Leach Batch: 271274
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490 168891.1
GUC.
TCLP
Sludge
EPA 1311..._...
.................................
LB 180-271274116-E
Method Blank
TCLP
Solid
EPA 1311
LB 180-271274116-G
Method Blank
TCLP
Solid
EPA 1311
Prep Batch: 271365
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
_
490-168891_1
GOC ....
TCLP
_ Sludge .... .........
3510.. .......
271274
LB 180-271274116-E
Method Blank
TCLP
Solid
3510C
271274
MB 180-27136511-A
Method Blank
TotalINA
Solid
3510C
LCS 180-27136512-A
Lab Control Sample
Total/NA
Solid
3510C
TestAmerica Nashville
Page 20 of 30 3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nomics Services., Inc.
Project/Site, Greenville V TP
CSC Semi VOA (Continued)
Prep Batch: 271365 (Continued)
TestAmerica Job ID: 490-168891-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
LCSD 1 80-27 1 365!3-A
Lab Control Sample Dup
Total/NA
Solid
3510C
Lab Control Sample Dup
Prep Batch: 271391
Solid
Lab Sample ID
Client Sample ID
490-168891-1
GUC
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC _
TCLP.......
Sludge ... ....
.. 8151A
_ 271274
LB 180-271274116-G
Method Blank
TCLP
Solid
8151A
271274
MB 180-27139111-A
Method Blank
TotaUNA
Solid
8151A
Solid
EPA 8082A
LCS 180-27139112-A
Lab Control Sample
Total/NA
Solid
8151A
LCSD 180.271391/3-A
Lab Control Sample Dup
TotallNA
Solid
8151A
Analysis Batch: 271475
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1 _
GUC ...... ..................
_ TCLP
Sludge._.
EPA808.1..B ...
271365
LB 180-271274116-E
Method Blank
TCLP
Solid
EPA 8081B
271365
MB 180-27136511 -A
Method Blank
Total/NA
Solid
EPA 8081B
271365
LCS 180-27136512-A
Lab Control Sample
Total/NA
Solid
EPA 8081 B
271365
LCSD 184-27136513-A
Lab Control Sample Dup
Total/NA
Solid
EPA 8081 B
271365
Prep Batch: 271476
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
Total/NA
Sludge
3541
MB 180-27147611-A
Method Blank
Total/NA
Solid
3541
LCS 180-27147612-A
Lab Control Sample
Tota9/NA
Solid
3541
490 -168890 -B -1-J MS
Matrix Spike
Total/NA
Solid
3541
490 -168890 -B -1-K MSD
Matrix Spike Duplicate
Total/NA
Solid
3541
Analysis Batch: 271555
Lab Sample ID
Client Sample ID
490-168891-1
G U C
LB 180-271274116-G
Method Blank
MB 180-27139111-A
Method Blank
LCS 180-27139112-A
Lab Control Sample
LCSD 180-27139113-A
Lab Control Sample Dup
Analysis Batch: 271567
Solid
Lab Sample ID
Client Sample ID
490-168891-1
GUC
MB 180-27147611-A
Method Blank
LCS 180-27147612-A
Lab Control Sample
490-168890-8-1-J MS
Matrix Spike
490 -168890 -B -1-K MSD
Matrix Spike Duplicate
Metals
Matrix
Leach Batch: 271274
Prep Batch
Lab Sample ID
Sludge
490-168891-1
......271391
LB 180-27127411-B
Solid
LB 180-27127411-C
271393
180-86915-A-1-1 MS
Solid
Prep Type
Matrix
Method
Prep Batch
TCLP...
Sludge
EPA 8151A
......271391
TCLP
Solid
EPA 8151A
271393
Total/NA
Solid
EPA 8151A
271391
Total/NA
Solid
EPA 8151A
271391
Total/NA
Solid
EPA 8151A
271391
Prep Type
Matrix
Method
Prep Batch
Total/NA
Sludge
EPA 8082A
271476
Total/NA
Solid
EPA 8082A
271476
TotaVNA
Solid
EPA 8082A
271476
TotaVNA
Solid
EPA 8082A
271476
Total/NA
Solid
EPA 8082A
271476
Client Sample ID
Prep Type
Matrix
Method Prep Batch
GUC
TCLP
Sludge _
EPA 1311
Method Blank
TCLP
Solid
EPA 1311
Method Blank
TCLP
Solid
EPA 1311
Matrix Spike
TCLP
Solid
EPA 1311
TestAmerica Nashville
Page 21 of 30 3/19/2019 (Rev. 2)

QC Association Summary
Client: Bio-Nornics Services., Inc. TestAmerica Job ID: 490-168891-1
Project/Site: Greenville WTP
Metals (Continued)
Leach Batch: 271274 (Continued)
Lab Sample ID Client Sample 10 Prep Type Matrix Method Prep Batch
180 -86918 -A -1-J MSD Matrix Spike Duplicate TCLP Solid EPA 1311
Prep Batch: 271342
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
490-1681-1
89
GUC
TCLP .....................
Sludge
7470A
LB 180-271274/1-B
Method Blank
TCLP
Solid
7470A
MB 180-27134211 -A
Method Blank
Total/NA
Solid
7470A
LCS 180-27134212-A
Lab Control Sample
Total/NA
Solid
7470A
180-86915-A-1-1 MS
Matrix Spike
TCLP
Solid
7470A
180.86915 -A -1-J MSD
Matrix Spike Duplicate
TCLP
Solid
7470A
Prep Batch: 271355
Prep Batch
271274
271274
271274
271274
Lab Sample ID
Client Sample Iia
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
3010A
271274
LB 180-27127411-C
Method Blank
TCLP
Solid
3010A
271274
MB 180-27135511-A
Method Blank
Total/NA
Solid
3010A
LCS 180-27135512-A
Lab Control Sample
TotallNA
Solid
3010A
Analysis Batch: 271395
Matrix Spike Duplicate
Total/NA
Solid
9030E
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GLIC
TCLP
Sludge
EPA 7470A
271342
LB 180-27127411-B
Method Blank
TCLP
Solid
EPA 7470A
271342
MB 180-27134211-A
Method Blank
Total/NA
Solid
EPA 7470A
271342
LCS 180-27134212-A
Lab Control Sample
Total/NA
Solid
EPA 7470A
271342
180-86915-A-1-1 MS
Matrix Spike
TCLP
Solid
EPA 7470A
271342
180 -86915 -A -1-J MSD
Matrix Spike Duplicate
TCLP
Solid
EPA 7470A
271342
Analysis Batch: 271499
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TCLP
Sludge
EPA 6010D
271355
LB 180-27127411-C
Method Blank
TCLP
Solid
EPA 601 OD
271355
MB 180-27135511-A
Method Blank
TotallNA
Solid
EPA 601 OD
271355
LCS 180-27135512-A
Lab Control Sample
Total/NA
Solid
EPA 6010D
271355
General Chemistry
Prep Batch: 271319
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-188891-1
GOC
TotaiN"'A .
.._ Sludge ..
9030B
MB 180-27131911-A
Method Blank
Total/NA
Solid
9030E
LCS 180-27131912-A
Lab Control Sample
Total/NA
Solid
9030B
490 -168890 -B -1-C MS
Matrix Spike
Total/NA
Solid
9030B
490 -168890 -B -1-D MSD
Matrix Spike Duplicate
Total/NA
Solid
9030E
Analysis Batch: 271334
Lab Sample ID
Client Sample fl)
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
Total/NA
Sludge
EPA 9034
271319
MB 180-27131911-A
Method Blank
Total/NA
Solid
EPA 9034
271319
LCS 180-27131912-A
Lab Control Sample
TotaUNA
Solid
EPA 9034
271319
490 -168890 -B -1-C MS
{Matrix Spike
Totai1NA
Solid
EPA 9034
271319
TestAmerica Nashville
Page 22 of 30 3/19/2019 (Rev. 2)

Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
General Chemistry (Continued)
Analysis Batch: 271334 (Continued)
Lab Sample ID Client Sample ID
490 168890 B 1 D MSD Matrix Spike Duplicate
Analysis Batch: 271450
QC Association Summary
TestAmerica Job IB: 490-168891-1
Prep Type
Matrix
Method
Prep Batch
TotaJINA
Solid
EPA 9034
271319
Lab Sample ID Client Sample ID Prep Type
490-168891-1 GUC Total/NA
180-86358-B-20 DU Duplicate Total/NA
Analysis Batch: 271506
Matrix Method Prep Batch
Sludge 254OG
Solid 2540G
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
490-168891-1
GUC
TotaIINA
Sludge
EPA 9045D
LCS 180-271506/1
Lab Control Sample
Total/NA
Solid
EPA 9045D
180-86977-J-1 DU
Duplicate
Total/NA
Solid
EPA 9045D
Prep Batch: 271760
Lab Sample fl)
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-16889.1-1..... ...
GUC
Total/NA ........
.. Sludge
90128.
MB 180-27176014-A
Method Blank
Total/NA
Solid
9012B
HLCS 180-27176012-A
Lab Control Sample
Total/NA
Solid
9012B
LCS 180-27176013-A
Lab Control Sample
Total/NA
Solid
9012B
LLCS 180-27176011-A
Lab Control Sample
Total/NA
Solid
9012B
180.87076 -D -1-B MS
Matrix Spike
Total/NA
Sofid
9012B
180-87076-D-1-0 MSD
Matrix Spike Duplicate
Total/NA
Solid
90128
Analysis Batch: 271809
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
TotaUNA
Sludge
EPA 90128
271760
NIB 180-27176014-A
Method Blank
Total/NA
Solid
EPA 9012B
271760
HLCS 180-27176012-A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
LCS 180-27176013-A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
LLCS 180-27176011 -A
Lab Control Sample
Total/NA
Solid
EPA 9012B
271760
180 -87076 -D -1-B MS
Matrix Spike
Total/NA
Solid
EPA 90128
271760
180 -87076 -D -1-C MSD
Matrix Spike Duplicate
Total/NA
Solid
EPA 9012B
271760
Analysis Batch: 578372
Lab Sample fD
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
490-168891-1
GUC
YOWINA
Sludge
10i0A
MB 490-57837211
Method Blank
Total/NA
Solid
1010A
LCS 490-57837212
Lab Control Sample
Total/NA
Solid
1010A
LCSD 490-578372114
Lab Control Sample Dup
TotaYNA
Solid
1010A
280-120182-A-1 DU
Duplicate
Total/NA
Solid
1010A
TestAmerica Nashville
Page 23 of 30 3/19/2019 (Rev. 2)

Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Client Sample ID: GUC
Initial
Date Collected: 02/19/19 12:00
Batch
Date Received:
02121/19 08:55
Run Factor
Batch
Batch
Prep Type
Type
Method
TCLP
Leach
EPA 1311
TCLP
Analysis
EPA 8260D
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
8270E
TCLP
Leach
EPA 1311
TCLP
Prep
3510C
TCLP
Analysis
EPA 8081 B
Total/NA
Prep
3541
Total/NA
Analysis
EPA 8082A
TCLP
Leach
EPA 1311
TCLP
Prep
8151A
TCLP
Analysis
EPA 8151A
TCLP
Leach
EPA 1311
TCLP
Prep
3010A
TCLP
Analysss
EPA 601 OD
TCLP
Leach
EPA 1311
TCLP
Prep
7470A
TCLP
Analysis
EPA 7470A
Total/NA
Analysis
1010A
TotallNA
Analysis
2540G
TotallNA
Prep
9012B
TotaYNA
Analysis
EPA 90126
Total/NA
Prep
9030E
Total/NA
Analysis
EPA 9034
Total/NA
Analysis
EPA 9045D
Lab Chronicle
TestAmerica Job ID: 490-168891-1
Lab Sample ID: 490-166891.1
Matrix: Sludge
Dii
Initial
Final
Batch
Prepared
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
269
500 mL
271392
0212611906:16
TAH
TAL PIT
1
0.125 mL
5 mL
271299
02/26/19 09:23
KLG
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
200 mL
10.0 mL
271367
02/26/19 12:10
CBY
TAL PIT
1
1 mL
1 mL
271438
02/27/19 17:24
VVP
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
100 mL
40.0 mL
271365
02/26/19 11:00
CBY
TAL PIT
1
271475
02/27/19 16:03
DFE
TAL PIT
15.2 g
20.0 mL
271476
02/27/19 09:52
BAP
TAL PIT
1
271567
02/28/19 15:46
JMO
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
100 mL
10.0 mL
271391
02/26/19 14:30
CBY
TAL PIT
20
271555
02/28/19 0114
JBF
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
5 mL
50 mL
271355
02/26/19 12:20
NAM
TAL PIT
1
271499
02/27/19 09:13
RJG
TAL PIT
100 g
2000 mL
271274
02/25/19 16:00
MTT
TAL PIT
50 mL
50 mL
271342
02/26/19 11:05
RJR
TAL PIT
1
271395
02/26/19 16:17
KAK
TAL PIT
1
578372
03/01/19 17:29
VRP
TAL NSH
1
271450
02/27/19 08:43
JMS
TAL PIT
0.99 g
50 mL
271760
03/01/19 12:40
BSH
TAL PIT
1
271809
03/01/19 19:32
JAS
TAL PIT
5.00 g
50 mL
271319
02/26/19 09:35
SES
TAL PIT
1
271334
02/26/19 11:20
SES
TAL PIT
1
20 mL
20 mL
271506
02/27/19 12:00
JMS
TAL PIT
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 24 of 30 3/19/2019 (Rev. 2)

Method Summary
Client: Bio-Nomics Services., Inc.
Project/Site: Greenville WTP
Method
Method Description
EPA 8260D
volatile Organic Compounds by GC1MS
8270E
Semivolatile Organic Compounds (GC1MS)
EPA 8081 B
Organochlorine Pesticides (GC)
EPA 8082A
Polychlorinated Biphenyls (PCBs) by Gas Chromatography
EPA 8151A
Herbicides (GC)
EPA 6010D
Metals (ICP)
EPA 7470A
Mercury (CVAA)
1010A
Ignitability, Pensky-Martens Closed -Cup Method
254OG
SM 2540G
EPA 9012B
Cyanide, Total andorAmenabie
EPA 9034
Sulfide, Acid soluble and lnsoluble (Titrimetric)
EPA 9045D
pH
3010A
Preparation, Total Metals
3510C
Liquid -Liquid Extraction (Separatory Funnel)
3541
Automated Soxhlet Extraction
5030C
Purge and Trap
7470A
Preparation, Mercury
8151A
Extraction (Herbicides)
9012E
Cyanide, Total and/or Amenable, Distillation
90308
Sulfide, Distillation (Acid Soluble and Insoluble)
EPA 1311
TCLP Extraction
TestAmerica Job ID: 490-168891-1
Protocol
Laboratory
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PET
SW846
TAL PiT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL NSH
SM22
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
SW846
TAL PIT
Protocol References:
SM22 = Standard Methods For The Examination Of Water And Wastewater, 22nd Edition
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TAL PIT = TestAmerica Pittsburgh, 301 Alpha Drive, R0C Park, Pittsburgh, PA 15238, TEL [phone]
TestAmerica Nashville
Page 25 of 30 3/19/2019 (Rev. 2)

Accreditation/Certification Summary
Client: Bio -Noetics Services., Inc.
Prep Method
TestAmerica Job ID: 490-168891-1
Project/Site: Greenville INTP
2540G
Sludge
Laboratory: TestAmerica Nashville
254OG
Sludge
The accreditations/certifications listed below are applicable to this report.
8270E
3510C
Sludge
Authority Program
EPA Region
identification Number
Expiration Date
South Carolina State Program
4
84009 (001)
02-28-19
Laboratory: TestAmerica Pittsburgh
8270E
35100
Sludge
Unless otherwise noted, all analytes for this laboratory were covered under
each accredltationlcertification below.
35100
Authority Program
EPA Region
Identification Number
Expiration Date
South Carolina State Program
4
89014
04-30-19
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method
Prep Method
Matrix
Analyte
2540G
Sludge
Percent Moisture
254OG
Sludge
Percent Solids
8270E
3510C
Sludge
1,4 -Dichlorobenzene
8270E
3510C
Sludge
2,4,5 -Trichlorophenol
8270E
3510C
Sludge
2,4,6 -Trichlorophenol
8270E
35100
Sludge
2,4-Dinitrotoluene
8270E
35100
Sludge
Cresols
8270E
351 DC
Sludge
Hexachlorobe nzene
8270E
35100
Sludge
Hexachlorobutadiene
8270E
3510C
Sludge
Hexachloroethane
8270E
3510C
Sludge
Nitrobenzene
8270E
351 DC
Sludge
Pentachlorophenol
8270E
3510C
Sludge
Pyridine
EPA 8151A
8151A
Sludge
2,4,5-T
EPA 8151A
8151A
Sludge
2,4-D
EPA 8151A
8151A
Sludge
Silvex (2,4,5 -TP)
EPA 8260D
Sludge
1,1-Dichloroethene
EPA 826DD
Sludge
1,2-Dichloroethane
EPA 8260D
Sludge
2-Butanone (MEK)
EPA 8260D
Sludge
Benzene
EPA 8260D
Sludge
Carbon tetrachlofide
EPA 8260D
Sludge
Chlorobenzene
EPA 8260D
Sludge
Chloroform
EPA 8260D
Sludge
Tetrachloroethene
EPA 8260D
Sludge
Trichloroethene
EPA 8260D
Sludge
Vinyl chloride
EPA 9012B
9012B
Sludge
Cyanide, Total
* Accreditation/Certification renewal pending - accreditationlcertification considered valid.
TestAmerica Nashville
Page 26 of 30 3/19/2019 (Rev. 2)

TestAmedca Ilililllillllllllllll IIIIIIIIII Illlllllllllllllllli
THE LEADER IN ENVIRONMENTAL TESTMC, IIIIIIIIIIIIIII1111111111[11111111111UP11111111111111111111111
Nashville, TN COOLER RECEIPT FORM 490-168891 Chain of Custody
Cooler RecelvedlOpened On 212112019 @ 8:55 _
Time Samples RemovedFromCoolerTime Samples Placed In Storage <t (2 Hour Window)
1. Tracking # / (last 4 digits, FedEx) Courier: FedEx
IR Gun ID 17960358 pH Strip Lot __Chlorine Strip Lot
2. Temperature of rep, sample or temp blank when opened: Y10 Degrees Celsius
3. If Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen?
4. Were custody seals on outside of cooler7 (I
If yes, how many and where:
YES NO..CA)
61.1NO...NA
5. Were the seals intact, signed, and dated correctly? G§ ... NO—NA
6. Were custody papers inside cooler? ..NO ... NA
certify that I opened the cooter and answered questions 1-6 intlai
7. Were custody seals on containers: YESNO and Intact YES...NO...NA
Were these signed and dated correctly? YES...NO... A
S. Packing maPl used? ubblewrap Plastic bag Peanuts Vermiculite Foam Insert Paper Other None
9. Cooling process: Ice Ice -park ice (direct contact) Dry ice Other None
10. Did all containers arrive in good condition (unbroken)? S .,NO ... NA
11. Were all container labels complete (#, date, signed, pres., etc)?
12. Did all container labels and tags agree with custody papers?
13a. Were VOA vials received?
b. Was there any observable headspace present in any VOA vial?
0 00 Larger than this.
14, Was there a Trip Blank in this cooler? YES. NO.. NA
I certify that I unloaded the cooler and answered questions 7.14 (intial}
YES ..NO ... NA
E5 ..NO ... NA
YES.: N0, .NA
YES..,NO..EA)
If multiple coolers, sequence #
15a. On pres`d bottles, did pH test strips suggest preservation reached the correct pH level? YES ... N0, NA
b. Did the bottle labels Indicate that the correct preservatives were used ES ..N0...NA
16. Was residual chlorine present? YES ... NO. N
I certify that I checked for chlorine and PH as per SOP and answered questions 15.16 fintiall `
17. Were custody papers properly filled out (ink, signed, etc)? �E ,..NO...NA
18. Did you sign the custody papers In the appropriate place?YE ...NO...NA
19. Were correct containers used for the analysis requested? YE _NO ... NA
20. Was sufficient amount of sample sent In each container? YE ...NO ... NA
I certify that I entered this protect into LIMS and.answered questions 17-20 (intial}
I certify that /_attached a label with the_unsgue LIMS, number to each conta€net (lntiai)
21. Were there Non -Conformance issues at login?(9. -�
YE ..� Was a NCM generated? CES ..NO...f4
1315 _ Broken in shilmmit
Cooler Reccipt 1`0171n.doc
LIF -1
End orrot7u
Page 27 of 30
Revised 8/23117
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Page 29 of 30 3/19/2019 (Rev. 2)
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Page 29 of 30 3/19/2019 (Rev. 2)

Login Sample Receipt Checklist
Client: Bio-Nomics Services., Inc.
Login Number: 168891
List Number: 2
Creator: Say, Thomas C
Question
Radioactivity wasn't checked or is </W background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time (excluding tests with immediate
HTs)
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MSIMSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (114").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
Job Number: 490-168891-1
SDG Number:
List Source: TestAmerica Pittsburgh
List Creation: 02/23119 11:33 AM
Answer Comment
.......................
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
True
NIA
TestAmerica Nashville
Page 30 of 30 3/19/2019 (Rev. 2)