NCS000258_MONITORING INFO_20160608

---STORMWATER DIVISION CODING -SHEET
PERMIT NO.
/\,j C. ow )S7
DOC TYPE
❑ FINAL PERMIT
1� MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ 0--DIW�DQ
YYYYM M D D

Pickle, Ken
From:
Pickle, Ken
Sent:
Wednesday, June 08, 2016 3:46 PM
To:
'Gary Wooten'
Cc
Georgoulias, Bethany; Bennett, Bradley
Subject:
RE: Stormwater Permit Application NCS000258
Hi Gary,
Yes, Glycotech should continue to abide by the provisions of your NPDES stormwater discharge permit, NCS000258,
even after it expires. Your authorization to discharge continues after expiration.
1. First item, regulatory status: Federal rules (40 CFR 122.26 and following) administered in North Carolina by
NCDEQ's Stormwater Permitting Program provide specifically for our current circumstances: If the permittee
makes timely application for renewal (we consider your renewal application to be timely), and if the permitting
agency (us) is late in delivering the requested authorization to continue discharging, then the expired permit
continues in effect as long as the permittee continues to abide by the provisions of the expired permit. As long
as the permittee abides by the expired permit, he is protected from 'discharging without a permit.' Federal
rules specifically anticipate our current situation and protect the permittee from liability caused solely by the
agency's delay.
2. Second item, suitability of current permit for new manufacturing: Your site stormwater discharges into Alligator
Branch, a class C, Sw water in the Cape Fear River Basin. Your current permit requires stormwater monitoring
for pH and COD. You report below a change in manufacturing to a manufacturing process to produce oils used
in cosmetics, medicines, and foods, and featuring only hydrocarbons (squalane — C301-162; farnesene -- C151-124;
and IPA — C31-180). My opinion is that these hydrocarbons will be readily measured by the COD analysis, and it
should be an adequate test method even for your new manufacturing process. Your site has some history of
low pH measurements, and so pH continues to be relevant.
Please contact me with any questions.
Ken Pickle
Stormwater Program Specialist
DEMLR Stormwater Permitting Program
Department of Environmental Quality
919 807 6376 office
[e-mail]
1612 Mail Service Center, Raleigh, NC 27699-1612
512 N. Salisbury St, Raleigh, NC 27604
l ��''Notihing Compares,
w
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Gary Wooten [mailto:[e-mail]]
Sent: Friday, June 03, 2016 10:50 AM
To: Pickle, Ken <[e-mail]>
Subject: Stormwater Permit Application NCS000258
Mr. Pickle
Thank you for your assistance during our phone conversation this morning, concerning renewal of Stormwater Permit
No. NC5000258 for Glycotech, Inc. located at 2271 Andrew Jackson Hwy, Leland NC 28451. Based on information you
provided, there is a significant backlog of permit renewals being processed, and Glycotech can expect the Permit
renewal to occur after the expiration date of the existing Permit, which is July 1, 2016.
Based on information I provided you about our current manufacturing of Squalane at the Glycotech site, with the use of
Farnesene (Sugar Cane Fermented/Distilled Raw Material) and Isopropyl Alcohol (solvent), your initial assessment is that
the current permit appears to adequately address environmental risks, at least for the short term until further
investigation may be conducted as part of the Permit renewal process.
Per your recommendation, Glycotech is to continue to comply with the parameters of the existing Stormwater Permit
NCS000258, which expires July 1, 2016 until such time DWQ issues the renewed Permit.
Glycotech is to continue with all currently permitted sampling, reporting, & payment of fees. Submission of all required
Permit Application Forms, including a detailed description of relevant changes of the current manufacturing process
versus the previous processes existing when the last application for renewal was submitted in 2011, will be completed
during the next calendar week.
The purpose of this e-mail is to request written confirmation that Glycotech has contacted NC DWQ, discussed these
matters, and that Glycotech, having submitted a complete Permit Renewal Application, has permission to continue
discharging stormwater past the expiration date of existing Stormwater Permit NCS000258 .
Thank you again for your assistance!
Gary Wooten, CSM
Environmental, Health, Safety Manager
Glycotech Inc.
910-371-2234 x32 Office
910-231-3204 Cell
910-371-9158 Fax

41J a �c
U4
November 7, 2014
C9
Glycotech
2271 Andrew Jackson Hwy, NE
PO Box 1956
Leland, N.C. 28451
910-371-2234
ATTENTION: Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: Fall Stormwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc., under permit #NCS000258 has performed the Fall 2014
qualitative monitoring of the designated point source discharge Outfall 002. Under this
permit, Glycotech, Inc. is required to perform storm water sampling and subsequent
analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD was
103 mg/L, versus the benchmark value of 120. The pH was 5.8, with a recorded Rain -
gage pH of 5.9, therefore the benchmark values of 6.0 to 9.0 do not apply (per the
permit).
If any questions or comments arise concerning either the visual monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very truly yours,
Gary Wooten, CSM
EHS Manager
Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http://Rortai.ncdenr.ors/web/wg/ws/sulnydessw#tab4
Permit No.: Njg 10/0IQI2-151T l
Facility Name: "LVCdfrrW
County: >Q uN e.J d t�
Inspector:
Date of Inspection-, 9 /
Time of Inspection:
or Certificate of Coverage No.: NICIGI_l_I_l_l 1 1
Phone No. -qLD --M-
Total Event Precipitation (inches): P. 51 ,,i,X.e-r
Was this a Representative Storm Event? (See information below) y
Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this sign re I certif that this report is accurate and complete to the best of my knowledge:
(Signature of Perkittee or Designee)
1. Outfall Description: ,
Outfall No. WZ Structure (pipe, d'tch, etc.} 31 7Cq
Receiving Stream: LL1 64TblZ An-0C 4 1010A rIM2 RlUil?_1�StM
Describe the industrial activities that occur within the outfali drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
- ��UN I C-
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): NO►j r
Page 1 of 2
5WU-242-20120613

4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids. Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
i 2 3 4 5
7. Is there any foam in the stormwater discharge?. Yes No
8. Is there an oil sheen in the stormwater discharge? Yes CN)
9. is there evidence of erosion or deposition at the outfall? Yes CNo)
10. Other Obvious Indicators of Stormwater Pollution:
List and describe No
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may
be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-20120613

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS OW Z 58 or
Certificate of Coverage Number: NCG
FACILITY NAME L CofiFC14 I /V C
PERSON COLLECTING SAMPLE(S) Qeiale O-SaTaA
CERTIFIED LABORATORY(S) Edwoka COMM, Lab # ci IV
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 20N-
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receivers the sampling results from the laboratory.)
COUNTY U a U PJ St.) I C
PHONE NO. (Qto_) 3 2
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
s
Date
Sample
Collected
Flow (if Opp.)
. ,
.
i M
IWA9 TAWINFaf-,
OW-yal /+*E1rI."J.•�L�
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes $o
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitorine Requirements
Outfall
No:
Date
Sample
Collected
50050 '
00556 1 .
ill
00530
00400
Total Flow
(if applicable)
Total!Rainfall
Oilr&Grease
(if ,appl.) , 3
iO&G/fPH
1 i .
i on -polar
`(Metliod' 1664
SG'I'-HEM) ; if
�a` 1.
Total
Suspended
Solids
pH
New Motor Oil
Usage
mold r
MG
inches
;mgtl
m
Units
(allmo
Form SWU-246, lust revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date 9 h(
Total Event Precipitation (inches): . S
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the'system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
Including t ssibility of fines and imprisonment for knowing violations."
�r 7 C�
(Signature of Pe ittee) (Date)
Form SWU-246, last revised 21212012
Page 2 of 2

■
6�L�
ANALYTICAL & CONSULTING
CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • (910) 392=4424 (Fax)
710 $owsertown Road • Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DLS CERTWICATE #37729
Glycotech, Inc. Date of Report: Sep 23, 2014
PO Box 1956 Customer PO #: 5326
Leland NC 28451 Customer ID: 09060025
Attention: Gary Wooten Report #: 2014-11237
Project ID: Stormwater
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-27570 Site: Outlall 002 9/6/2014 2:00 PM Water Client
Test Method Results Date Analyzed
COD
SIN 5220D
Comment:
Reviewed
103 mg/L 09/18/2014
Report #:: 2014-11237 Page 1 of 1

i
ENVIRONMENTAL CHEMISTS, INC OFFCE:9r1f10-3924=11l Way FAX 910.NC
2�$24
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION 0 37729 info®envlronmentalchemlaft.com _
COLLECTION,AWCHAIN OF CUSTODY
CLIENT: L Ca 1-1cclw //V c-
PROJECT NAME: FALL 2-61'f STZ(ZIInw &'rVZ
REPORT NO: 3
ADDRESS: 2 Z"? ( 4ND"2 k) A4*soJ
CONTACT NAME:
PO NO: z%
1-6L A-YO f aC— 2ATYrSl
REPORT TO: pia UdTF.
PHONE/FAX:
COPY TO: C =
emai• , �CCA inc, co.J
Sampled By: SAMPLE TYPE: I = influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae. Other:
Sample Identification
I
MM
M
ANALYSIS REQUESTED
M-�-
M.
mum/amm
0-1
N
WE—
1010100
ME
aE
milli
1111NINIENNE!
077
Relinquished By:
Temperature when
Delivered By;
cc A,c
pD 532-&

Gr
Glycotech
2271 Andrew Jackson Hwy, NE
PO Box 1956
Leland, N.C. 28451
910-371-2234
May 19, 2014
ATTENTION: Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: Spring Stormwater Discharge Monitoring Report
To whom it may concern:
coV
RECEIVE,)
MAY 2 2 2014
CENTRAL FILES
DWQ/80G
Glycotech, Inc., under permit #NCS000258 has performed the Spring 2014
qualitative monitoring of the designated point source discharge Outfall 002. Under this
permit, Glycotech, Inc. is ' required to perform storm water sampling and subsequent
analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD was
82 mg/L, versus the benchmark value of 120. The pH was 5.7, with a recorded Rain -gage
pH of 5.8, therefore the benchmark values of 6.0 to 9.0 do not apply (per the permit).
If any questions or comments arise concerning either the visual monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very truly yours,
AmMaret Collins
wner
Glycotech, Inc.
CC:
Gary Wooten — Safety Health Environmental Manager- Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 006 Z S19� or
Certificate of Coverage Number: NCG
FACILITY NAME r11►►�
PERSON COLLECTING AMPLE(S)
CERTIFIED LABORATORY(S) a.,j Caj. a Lab"
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2Z
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the samplingresults from the laboratory.)
COUNTY _ 61Zjf,j- ci
PHONE NO. (q(,0,
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
1
DateII
Sample-
Collectedi
I
i
: i
i
y ;
1
/
r
t
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes Ko
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitorine Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
'Total Flow
(ifapplicable)
Total Rainfall
Oil &:Grease
(ifappl.)
Non -polar
O&G/I'PH
(Method 1664
,SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor Oil
Usage
mo/dd/ r.
MG
inches
01911
mg1l
Units
al/mo
Form SWU-246, Iasi revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date is
Total Event Precipitation (inches): Q- % q
Event Duration (hours): (only if applicable —see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours); (only if applicable —see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information,.the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines a imprisonment for knowing violations."
store o Pe itt (Date)
Form SWU-246, last revised 21212012
Page 2 of 2

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this farm. please visit: http://portal.ncdenr.orglweb/wu/ws/su/n2dessw#tab-4
Permit No.: N/C/ Sl0/ 0/0 f2-1 SlXl or Certificate of Coverage No.: NICIGI_I_I 1 I 1_I
Facility Name: GtYLOTECH INC
County: _1
Inspector:
Date of Inspection:
Time of inspection: D f OQ
Total Event Precipitation (inches): 6.99
Phone No.
Was this a Representative Storm Event? (See information below) Yes ❑ No
3Z
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signk t , I certify that this report is accurate and complete to the best of my knowledge:
of Pe or Designee)
1. Outfall Description: -bl rc#
Outfall No. bO?— Structure (pipe, ditch_, etc.)
Receiving Stream: ,f sr+u
Describe the industrial activities that occur within the outfall drainage area:
Cyf_V XAL 114-7VUr c fV41 JG
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
7'/,f-,NNi L - LI Gq7 f3Rvr��J '%i XjT
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): �D N
Page 1 of 2
SWU-242-20120613

4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy: �'�
(1 ) 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
f 1) 2 3 4 5
b. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
S. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes DNo
10. Other Obvious Indicators of Stormwater Pollution:
List and describe _ _ . no Pi;
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may
be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
swu-242-20120613

41 Environmental Chemists, Inc.
envirochw 6602 Windmill Way • Wilmington, NC 28405
(910) 392-OM (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYnCAL & CONSULTING
CHENSTS NCDENR.- DWQ CERTIFICATE #94. DLS CERTIKCATfi #37729
Glycotech, Inc. Date of Report: Apr 28, 2014
PO Box 1956 Customer PO #: 4913
Leland NC 28451 Report #: 2014-04448
Attention: Gary Wooten Report to: Gary Wooten
Project ID: Stormwater
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
14-10698 SfEe: Outfall 002 4/15/2014 1:00 AM Water Gary Wooten
Test
COD
Method
sM szxao
Comment: I '
Reviewed by:
Results Date Analyzed
82 mg/L 04/2312014
RepmM 2014-MM Page 1 of I

ENVIRONMENTAL CHEMISTS, INC fl�FFICE:910 Wad WF1AnX910-M2844
Analytical & CDnsulUng Chemists NCDENR: DWG CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info®envlronmentalchemists aom
All 4Ill IN►1.1►1*I93:EliiIh]3F14--1to] oYJ
CLIENT: Ly t i,kC
PRO.IECT NAME: S ►ru ZO S'R3/LukLuwvZ
REPORT NO;
ABC
ADDRESS: Z2'7( AwDIipi-3ACACSo&1 9wY
CONTACT NAME:
PO NO: l 3
Lz- kr.j D L(r I
REPORT TO: Aa o s�l
PHONVFAX: R i 0 - 37(- Z Z3 � 3 z
COPY TO: L S u'�
email• .W00 �5 1Yc0AVL6. ifc . CO �x
Sampled By: (zSAMPLE 'TYPE: I = influent, E = Effluent, W W Well, ST = Stream, SO c Soil, SL = Sludge, Other:
Sample Identification
NMI
Millis
11111100�0
Temperature when
Delivered By:
4 Z.0
L ' G E r-LATt -.) Qo L Za
po o-4g13

Gr
Glycotech
February 5, 2014
2271 ANDREW JACKSON HWY NE . LELAND, NC 28451
ATTENTION: Steve Pusey
NCDENR — DEMLR — Stormwater
Wilmington Regional Office
127 Cardinal Drive Extension
Wilmington, NC 28405-2845
Subject: SDO Annual Summary Data Monitoring Report 2013
To whom it may concern:
FEB 0 7 20f4
Glycotech, Inc., under permit #NCS000258 has performed the required
monitoring of the designated point source discharge Outfall 002 for calendar year 2013.
Under this permit, Glycotech, Inc. is required to perform storm water sampling and
subsequent analytical testing Semi -Annually.
Enclosed please find the original and a copy of the completed SDO Annual
Summary Data Monitoring Report 2013.
I any questions or comments arise concerning this report please do not hesitate to
contact me at [phone].
Very truly yours,
Alan Stout
Vice President
Glycotech, Inc.
CC:
Gary Wooten — Safety Health & Environmental Manager — Glycotech, Inc.
Enclosure: SDO Annual Summary Data Monitoring Report — 2013
Phone [phone] Fax [phone]

Individual NPDES Permit No. N
Certificate of Coverage (COC) No. N
STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)
Calendar Year 2613
or
This monitoring report summary of the calendar year should be kept on file on -site with the facility SPPP.
Facility Name: .
County:
Phone Number:
0
Total no. of SDOs monitored
Outfall No. oa Z
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No
Was this outfall ever In Tier 2 (monitored monthly) during the past year? Yes ❑ No
If this outfall was In Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWo to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No
Total
Rainfall,
lnchet;�
Parameter, units
Cob
f �/
QA, nrG a AGE
pN
Benchmark
NIA
17A A 4
6-9
N 14
1Date�Sarnple
Collected,
mnUddlyy
o 113
0,13
o
S;7''�
09 fp
f
//
&Ac�mark /0/'( %Im [fo /taT 0.PP�� cli+� �o I'Q"n �lf.��q�
p l4 1 I ,[�r -/- e P 1C r m�. i*. J J
SW U-264-Generic-13Dec2012

Additional Outfall Attachment
Outfall No.
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑
I.Total
inches
Benchmark N/A
Date :Sample
Collected,Ell
mrrilddlyy
Parameter
SW U-264-Generic-1 3 Dec2012
J1

"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and. imprisonment for knowing violations."
Signature _
Date Z - -5--- /
For questions, contact your local Regional Office:
DWQ Regional Office Contact Information:
SHEVILLE REGIONAL QFI -
OYE'I7'EYILLEREGIONAL OFFI ►
T OORESVILLFE REGIONALXOFFI
225 Green Street
610 East Center Avenue/Suite 301
2090 US Highway 70
Swannanoa, NC 28778
Systel Building Suite 714
Mooresville, NC 28115
(828) 2964500
Fayetteville, NC 28301-5043
[phone]
[phone]
' ;EIQH REGIONAL OFFI
ASHINGTONIREGIONAL OFFIC
I' INGTON REGIONAL OFFIG
943 Washington Square Mall
127 Cardinal Drive Extension
3800 Barrett Drive
Raleigh, NC 27609
Washington, NC 27889
Wilmington, NC 28405-2845
[phone]
[phone]
[phone]
STON'SAEEMIREGIONAL OFFIC
ITAM52FFIq
1617 Mail Service Center
Raleigh, NC 27699-1617
(919)'807-6300
"Topreserve,• PratedWinston-Salem,
andeMence
W,NOIM Ca drira*0Wr._.
585 Wau htown. Street
8
NC 27107
[phone]
SW U-264-Generic-13Dec2012

Glycotech
2271 Andrew Jackson Hwy, NE
PO Boa 1956
Leland, N.C. 28451
910-371-2234
February 19, 2013
ATTENTION: Linda Willis ��' E �'�,/E
NCDENR Division of Water Quality
Wilmington Regional Office MAR 0 4 2o13
127 Cardinal Drive Extension
Wilinington, NC 29405-2845 BY.
—
Subject: SDO Annual Summary Data Monitoring Report 2012
To whom it may concern:
Glycotech, Inc., under permit #NCS000258 has performed the required
monitoring of the designated point source discharge Outfall 002 for calendar year 2012.
Under this permit, Glycotech, Inc. is required to perform storm water sampling and
subsequent analytical testing Semi, -Annually.
Enclosed please find the original and a copy of the completed SDO Annual
Summary Data Monitoring Report-2012.
If any questions or comments arise concerning this report, please do not hesitate
to contact me at [phone].
Very truly yours,
Alan Stout
'a�e' '4>c-�
Vice President
Glycotech, Inc.
CC:
Linda Willis — Surface Water Protection Section — Wihnington Regional Office
Gary Wooten — Safety Health 8t Environmental Manager- Glycotech, Inc.
Enclosure: SDO Annual Summary Data Monitoring Report-2012

I
Individual NPDES Permit No. NC
Certificate of Coverage (COC) No. NC
STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)
Calendar Year Z-O 1 2
or
This monitoring report summary of the calendar year should be kept on file on -site with the facility SPPP.
Facility Name: 9L y eOreo4 TkC
County:
Phone Number: Qr O J 3 7/- 2 Z 3 4
Total no. of SDOs monitored 1
Outfall No. 00 2-
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No
Was this outfall ever in -Tier 2 (monitored monthly) during the past year? Yes ❑ Nox
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWO to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No
lu
Total;
Rainfall;
Inch"es'
paraMbter,. unfts
COD
rn L
N
RAW 6uAG
P N
Benchmark
N/A
2 DD-
Dato ample;
Collected;,
mmkldlyy
19 rz
, SZ
33
6, o
2 25 I2.
O. 4t
35
(o,
VOILUM-MAY
EXTRq 4
is Z ,z
0.49
" 00
�_5-45
5-
SW U-264-Generic-13 Dec2012

Additional Outfall Attachment
Outfall No.
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No ❑
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No ❑
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ❑ No ❑
- MMMMMMM
1EM - =0
S W U-264-Generic-13 Dec2012

ti
" I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Sign
Date
For questions, contact your local Regional Office:
DWQ Realonal Office Contact Information:
HEY LE R G IONNUIOEVC-14
PAN, EY[LLE REGIONAL O ICPAOORESVAlffLtEMG,10—NWL!LOFF,[EEI
225 Green Street
610 East Center Avenue/Suite 301
2090 US Highway 70
Swannanoa, NC 28778r
Systel Building Suite 714
Mooresville, NC 28115
[phone]
Fayetteville, NC 28301-5043
[phone]
910 433-3300
MIr9fGftjW6fCFNArTflTOF,#fG_Q
WASHINGTON REGIONAL OFI+[C
ILMINGTON REGIONAL OFF'IC
943 Washington Square Mali
127 Cardinal Drive Extension
3800 Barrett Drive
Raleigh, NC 27609
Washington, NC 27889
Wilmington, NC 28405-2845
(919)°791-420..0
[phone]
[phone]
INSTON-SALEM REGIONAL OFFIC
-ENTRAL OFF1C
1617 Mail Service Centeno,,:{
Raleigh, NC 27699-1617
919) 807-6304
a»d;enharnae
` Aiarth Cara�tira�s'warer:s""
585 Waughtown Street
Winston-Salem, NC 27107
336 771-5000
SW U-264-Generic-13Dec2012

cl- I �
Glycotech
2271 Andrew Jackson Hwy, NE
PO Bog 1956
Leland, N.C. 28451
910-371-2234
November 29, 2010
ATTENTION: Central Files RE C E IV E D
Division of Water Quality DEC - 9 2010
Surface Water Protection Section
1617 Mail Service Center information /BOssing Unit
pWQIBOG
Raleigh, N.C. 27699-1617
Subject: Fall Stormwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc.,. under permitz#NCS000258has performed the Fall qualitative
monitoring of the designated point source discharge Outfall 002. Under this permit,
Glycotech, Inc. is required to perform storm water sampling and subsequent analytical
testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD is
150, versus the benchmark value of 120. The pH was 5.7 versus the benchmark of 6 to 9,
similar to the site's previous eight outfall samples/reports, in which we reported pHs of
4.7, 4.9, 5.2, 4.8, 4.9, 5.4, 5.7, and 5.4 respectively.
Please note that on July 6, 2006, this facility requested a modification to the
existing Stormwater Permit in regard to lowering the pH Benchmark Values. This
request was based on a number of samples taken for pH of the stormwater on site as well
as adjacent waters and rainwater as collected in a rain gauge. These analysis show that
all waters including rainwater are below the lower benchmark value specified in the
current permit.
If any questions or comments arise concerning either the visual monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very truly yours,
Alan Stout
Vice President
Glycotech, Inc.

CC:
Linda Willis — Surface Water Protection Section -- Wilmington Regional Office
Gary Wooten — Production Manager- Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. http://h2o.enr.state.nc-us/su/Forms Doc uments.htnAmisciorms
Permit No.: NIC/S/ 01010/21 SI 91 or Certificate of Coverage No.: N/C/G/
Facility Name: _ Ca L Yl'oTECFf , ZAI C
County: Poem NS wrcle Phone No. 9/O 3 71- Z Z 3
Inspector: i o a-T
Date of Inspection: /O
Time of Inspection: / .5 b O
Total Event Precipitation (inches):
0.4sj
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
G.
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. O Z Structure (pipe, ditch, etc.) b
Receiving Stream: 4441G4ioge .19A24.1VCF1 C9io,5 6E U RIAVCrt RAJ , n1
Describe the industrial activities that occur within the outfall drainage area:
e 4FIn t csfc. W ^ur.¢c-r 1&NC,
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
--�ryNi C
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): /VbN E -
Page 1 of 2
SWU-242-112608

R
r
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
O 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
(9 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where l is n��o�� solids and 5 is extremely muddy:
10 J 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
& Is there an oil sheen in the stormwater discharge? Yes No
9. is there evidence of erosion or deposition at the outfall? Yes oNo
10. Other Obvious Indicators of Stormwater Pollution:
List and describe N 0 ME -
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS O 0O Z SAS or
Certificate of Coverage Number: NCG
FACILITY NAME 4�9L y do TFc Z1 c
PERSON COLLECTING SAMPLE(S).
CERTIFIED LABORATORY(S) o r 14 bK Lab 0/ 3 S Z 2-
Lab 0
Part A: Speeiflc Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2 b 10
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY B,eKNSI, t C k
PHONE NO. ( rb) 3-7r— 2.23V
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Date
CollectedSample
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes Xno
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(f applicable)
Total Rainfall
OR & Grease
(if appl.)
Non -polar
O&GYTPH
(Method 1664
SGT-HEM), if
a 1.
Total
Suspended
Solids
pH
New Motor Oil
Usage
mold r
MG
inches
mgA
MWA
Units
galtmo
Form SWU-246-062310
Page 1. of 2

STORM EVENT CHARACTERISTICS:
Date 1%S/16 it
Total Event Precipitation (inches): 0 •
Event Duration (hours): is (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the Information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Information,
Including the possibility of fines and imprisonment for knowing violations."
29 /o
(Signature of Permittee)
(Date)
Form SWU-246-062310
Page 2 of 2

enroche
ANALY11CAL & CONSUUM
CFEEU WS
Environmental Chemists, Inc.
66M W-usdmM Way • Wdmingbnn, NC 28405
--- — (910) 392-UM (Lab)-*-[phone]'(Faz)
710 Bowsert+own Road • Manteo, NC 27954
[phone]
NCDENTL DWQ CERTIFICATE #94 DIS CERTIFICATE #37729
Glycohwk hm Date of Report Nov 01, 2010
PO Box 1956 Comer PO M. 1372
Leland NC 28451 Report 9: 2010-10790
Attention: Gary Wooten Report to: Gary Wooten
Project ID:
Lab ID Sample ID: OuBafl 002 Collect DateIT'me Matrix Sampled by
10-27029 Site: - 10252010 3:00 PM Water - Cary Wooten
Test Method Results Date Analyzed
COD 150 mg►L 102SM10
Comment:
Reviewe by_ 1 _
Report 6:: 2010-10790 Page 1 of 1

ENVIRONMENTAL CHEMISTS, INC 6602 Windmill way
Wilmington, NC 29405
SamW—e-Collection andChainu Phone. (910) 39M23
�Y(OTC-CH � c P. 0 . '� 1:37 Z ` Fax [phone]
Co1le.&A Rv! C" Anv oaT G-" 1 Renort No! le M 10 M
bmak •
.
Sample Idendflestion
i
Collectionb
a
SERVATION
ANALYSU REQUUM
DATZ
THU
TRW
. du-TFA LL 002
.1v7-91
la S o
So
AmB
sT
X
COD SlaotwA-MR
. �
G
C
G
G
C
P
I
G I
G
i.
C I
P
I
.G I.
G
i
C
p
'.
G
G
C
P
G
G
C
P
'G
G
'C
P,
G
G
C
P
G
G
C
P
G I
G
NO- ,CE_- DUHL[) UNAMON t Samples for Ammonia, TKN, Cyanide, Phenol, &no
0.2 m * less in the field at the time of collection. See reveres side for instructions.
Bacteria must be dechlorinated
Transfer
t
Relinquished By:
DatelTime
elved By:
Date/Time
r2.6
-Temperature when Received: 'Accepted: Reject
: Roa
ple Requpstpd:
Delivered By:
Cbmmenta: AW � Z .

Glycotech
2271 Andrew Jackson Hwy, NE
PO Boa 1956
Leland, N.C. 28451
910-371-2234
June 16, 2010
ATTENTION: Central Files
Division of Water Quality o
Surface Water Protection Section
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: Spring Stonnwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc., under permitCS00Q258'h4s_tperformed the Spring qualitative
monitoring of the designated point source discharge Outfall 002. Under this permit,
Glycotech, Inc. is required to perform storm water sampling and subsequent analytical
testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD is
within the benchmark value but the pH was 4.7 versus the benchmark of 6 to 9, similar to
the site's previous eight outfall samples/reports, in which we reported pHs of 4.9, 5.2,
4.8, 4.9, 5.4, 5.7, 5.4, and 5.8 respectively.
Please note that on July 6, 2006, this facility requested a modification to the
existing Stormwater Permit in regard to Iowering the pH Benchmark Values. This
request was based on a number of samples taken for pH of the stormwater on site as well
as adjacent waters and rainwater as collected in a rain gauge. These analysis show that
all waters including rainwater are below the lower benchmark value specified in the
current permit.
If any questions or comments arise concerning either the visual monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very truly yours,
Alan Stout
G.
Vice President
Glycotech, Inc.

FA
CC:
Linda Willis — Surface Water Protection Section — Wilmington Regional Office
Gary Wooten — Production Manager- Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfali Analytical data

U
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: htte://h2o.enr.state.nc.us/su/Forms Documents.htm#miscforms
Permit No.: NICI SI 6l 0l Q/ 2151 Vl or Certificate of Coverage No.: NIGGI I 1 I I 1 1
Facility Name: 6; ky &3z
County: d /214 Ars W I C
Inspector: G a
Date of Inspection:
Time of Inspection:
to
Total Event Precipitation (inches): 1- 1
No. Q/6 - 37 / --1 Z -7 S6
Was this a Representative Storm Event? (See information below) [Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. OutWI Description:
Outfall No. 00 2 Structure (pipe, ditch, etc.) frc Jq
Receiving Stream: 4d L.,Fjr. .s ZbA d.RWAt e A4 O-AP F FF41 Rd vFR k srnl
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(Light. medium, dark) as descriptors:
I —A Nlu j L - Lcar am krAj J I, 1-r
3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, -weak
chlorine odor, etc.): NoAvF_
Page 1 of 2
SWU-242-t 12608

rA
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
O 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
G) 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1. 22 3 - 4 5
7. Is there any foam in the stormwater discharge? Yes No
& Is there an off sheen in the stormwater discharge? Yes No
9. is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious indicators of Stormwater Pollution:
List and describe N 0 N E
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SVM-242-112M

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS_ 000 2.5k or SAMPLES COLLECTED DURING CALENDAR YEAR: 200
Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME L Co'Tl CN f4 C-
PERSON COLLECTING SAMPLE(S)
CERTIFIED LABORATORY(S) P-"jv, Ln C 04104 Lab # 22
Lab #
Part A: Specific Monitoring Requirements
COUNTY Aeu AtS c.J rC t
PHONE NO. ;- 2 7-3
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
total:�
Suspended
Sollds(TSS)
�•
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes )�no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
Outfall
N6.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total Rainfall
Oil & Grease
Total
Suspended
Solids
pH
New Motor Oil
Usage
moldd! r
MG
inches
Units
mo
Farm SWU-246-112608
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date 5 / 9//a �, 1
Total Event Precipitation (inches):
Event Duration (hours): 2— (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualifled personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible.for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
C_
(Signature of Permittee)
(Date)
Form SWU-246-112608
Page 2 of 2

Environmental Chemists, Inc.
0 1 6602 WmdmW Way • Wilmington, NC 29405
® [phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING [phone]
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DFS CERTIFICATE #37729
Customer:
GLYCOTECH, INC
PO Box 1956
Leland, NC 29451
Attn: Gary Wooten
Date Received:
Sampled By:
-REPORT OF ANALYSIS
05/21/10
Gary Wooten
Date of Report: May 26, 2010
Purchase Order No: 1312
Report Number: 104714
Sample ID
Date
Lab ID
Chemical Oxygen Demand,
Method
Date
Sampled
COD as 02 mg/L
Code
Analyzed
Outfall 002
05/19/10
# 11341
59
SM 5220 D
05/24/10
Comment:
Reviewed by: ! a¢�

ENVIRONMENTAL CHEMISTS, C
5=P 3 l Z—
Sam le Coll tion nd Chain of Custody!
G L yca 7" EC t-! , -rN c
6602 windmill way
Wilmington,'NC 28405
Phone: [phone]
Fax [phone]
Collected Br" - - G µiZy W o a7 tr � I R rt No. O — r714
ample • I m hffi
a
odgi Oth'
Sample Identification
Q
Collection
�
y
e
�
,
�
SERVATION
ANALYM nQUnMW
a
DATE
TIII!>t
TEMP
4 U'rF,ki, ©ate
1(311
! 00
AMA
5�
C
P
IX
X
C o 'Sit Rpm ww
G
G
C
P
G
G
C
P
'
G
G
C
P
.G
G
C
P
G
G
C
P
G
G
C
P
i
G
G
C
P
G
G
C
P.
G
G-
C
P
G
-G
DE RIl�iAT�ON : Samples for Ammonia, TKN,,CyanWe, Phenol, and Bacteria mint be dechiorinated
0.2ppm or Ins) in the field at the time of collection. See reverse side for Instructions.
Transfer
Relinquished By:
Datemme
i
Received By:
Date/Time
2.
'�nper�ture wh,:eieResample Requested:
'�vered By: Received _ : Date: ! -->I- l o Time: " 15
2.0 , - 0 . t317,
STIR

Glycotech
2271 Andrew Jackson Hwy, NE
PO Box 1956
lAhmd, N.C. 28451
910-371-2234
November 24, 2009
ATTENTION: Central Files
Division of Water Quality 0 1 �Qpg
Surface Water Protection Section D E C
1617 Mail Service Center
Raleigh, N.C. 27699-1617 �3`►'
Subject: Fail Stormwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc., under permit #NCS000258 has performed the Fall qualitative
monitoring of the designated point source discharge Outfall 002. - Under this permit,
Glycotech, Inc. is required to perform storm water sampling and subsequent analytical
testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD is
within the benchmark value but, the pH was 4.9 versus the benchmark of 6 to 9, similar to
the site's previous seven outfall samples/reports, in which we reported pHs of 51, 5.0,
4.9, 5.4, 5.8, 5A and 5.7 respectively.
Please note that on July 6, 2006, this facility requested a modification to the
existing Stormwaw Permit in regard to lowering the pH Benchmark Values. This
request was based on a number of samples taken. for pH of the stormwater on site as well
as adjacent waters and rainwater as collected in a rain gauge. These analysis show that
all waters including rainwater are below the lower benchmark value specified in the
current permit.
If any questions or comments arise concerning either the visual Monitoring report
or analytical report, please do not hesitate to contact me at [phone].
Very holy yours,
Alan: Stout
President
Glycotech, Inc.

.4
CC:
Linda Willis Surface Water Protection Section — Wilmington Regional Office
Gary Wooten — Production Manages Glycotech, Inc.
Enclostue: Visual Monitoring Report and 002 Outfall Analytical data

Stormwater Discharge Out&H (SDO)
Qashitative Monitoring Report
For guidmtce ain frlling out this form. please visit: httn:/Ih3aenr.state.nc.tislsta/F-orms-Document:s.lit in#ntiscforiw,
Permit No.: My S
Facility Name:
'41I.1 SI 8/ or Certificate of Coverage No.: NVg I I_/ 1 I 1
County: 13 N w cc Phone No. 9 lO — 3'71- ZZ
inspector. -9
Date of Inspection: 10 240 o q
Time of Inspection: -_ 4.O , --- _ --
Total Event Precipitation (inches):
3.7q
Was this a Represenmve Storm Event? (See information below) QrYes ❑ No
Please check your permit to verify if Qualita dve Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 mchcs of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 incites has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accrrate and complete to the best of cry knowledge:
(Signature of Permittere or
1. OuftH Damon:
Outfall No. Q U 2 _ Structure (pipe, M* etc.)
Receiving Stream: &.&-Scg t CAM HEAft
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _ Se m xs G - Ltc r -9 Rowba Tom —i
3. Odor: Describe any distinct odors that the discharge may have (Le., smells strongly of oil, weak
chlorine odor, etc.): NgtAe
Page 1 of 2
SWU-242-112=

4. Clu ty: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy: �-� .
[ 1 J 2 3 4 5
S. Floating Sander Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Steed Safids: Copse the number which best describes the amount of suspended solids in
the stormwater discharge, where I is � no solids and 5 is extremely muddy:
( 1 J 2 3 4 5
7. Is them any foam in the su mwater discharge? Yes oN()'
& Is there an off sheen in the starmwater discharge? Yes OID
9 Is there evidence of erosion or deposition at the outfall? Yes DNo
M Odxr ObvWus Indicators of Skwmvvater Fob:
Note: Low clarity, high solids, and/or the price of foam, oil sheer, or erosion/depmdon may be
indicative of pollntamt exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112M

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 2 00 2 S 8 or SAMPLES COLLECTED DURING CALENDAR YEAR: 20 0 q
Certificate of Coverage Number: NCG ('This monitoring report sball be received by the Division no later than 30 days from
the date the facility receives the eampling results from the laboratory.)
FACILITY NAME C L Co C C in4C, .
PERSON COLLECTING SAMPL ) a a
('ERTWWD LABORATORY(S) _ tNefRd C f4 Ewc Lab #
Lab #
Part A: Specific Monitoring Requirements
COUNTY- .- _ -- a r`u NSW 1 C fc
PHONE NO. (a1 ! D 1 223
(SIGNATURE OF R DESIGNEE)
By this signature, I caft that this report Y accurate
complete to the beat of my knowledg&
W,7*'T*"M
R U1,
��©I,
F I m�k'
�M
Does this facility perform Vehicle Maintenance Activities using more than SS gallons of new motor oil per month? yes �/—no
(if yes, complete Part B)
Part bt Vehicle Maintenance Acdvity Momiterim Reauirements
Outfall
Na
Date
Sample
Collected
M. 0
005%
M30
00"
TOWHOW
(if applicable)
Total Rainfall
Oil & Grease
Total
Suspended
Salida
PH
New Motor Oil
Usage
moi
inches
MRA
I nwA
LUnits
ovino
�MMG
Form SWU-246-112608
Page 1 of 2

STORM EVENT CHMUCTEIWTICS:
Date , [Oqt
Total Event Precipitation (inches):
Event Duration (hours): I) (only if applicable — see permit)
(if more than one storm event was sampled)
Date
Total Event Precipitation (Inches):
Event Duration (boars): (only if applicable — see permit)
Mall original and one copy to:
Division of Water Quality
Attn: central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I cer ft, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of may knowledge and belief, true, accurate, and complete. I am aware that there are ant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
(Signature of Permitta) — (Date)
Form SWU-246-112608
Page 2 of 2

ANALYTICAL & CONSULTING
CHEMISTS
Customer:
GLYCOTECH, INC
PO Box 1956
Leland, NC 29451
Attn: Gary Wooten
Date Received:
Sampled By:
C:Z r w;A
Environmental Chemists, Inc,
66M Windmill Way • Wilmington, NC 28405
(910) 392- (YM (Lab) • (910) 3924424 (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR: DWQ CER rHCATE #94. DLS CERTIFICATE #37M
REPORT OF ANALYSIS
10/29/09
Crary Wooten
Date of Report: November 3, 2009
Purchase Order No: 1178
Report Number: 9-10294
Sample ID
Date
Lab ID
Chemical Oxygen Demand,
Method
Date
Sampled
COD as Oz mg/L
Code
Analyzed
Outfall 002-
10/26/09
# 25850
89
SM 5220 D
11/02/09
Fall
Comment:
Reviewed by: .. L

ENVIRONMENTAL CHEMISTS, INC
4WD . tlr,s
Pt amllie Coflection and Cb of Ca oa
hut: V L'! C OTE C 14 [
6602 Windmill Way .
WUmiugtou,'NC 28405
Phone: [phone]
Fax [phone]
I!It1-
: �.. .
11771WilII:
_
M_
I I II I l f .• 1
1 I ! ,I I I r I! 1[ I i 11 l i 11' 1 [.-N 41 [lid I:.1
11 II 1 �1 1, I 1 I I I (;
I
fill
� �lgpE�`9�!!
I
e1ivem l
�.
Iments:
Am pted:__�_,�___r
i � Received Bv:
!e Reques ed:
Date: a Time: t o= t 3 �4
10

G�
Glycotech
2271 Andrew Jackson Hwy, NE
PO Boa 1956
Leland, N.C. 28451
910-371-2234
July 16, 2009
ATTENTION: Central Files
Division of Water Quality J
Surface Water Protection Section U� 2 0 z0�9
1617 Mail Service Center BY,•
Raleigh, N.C. 27699-1617
Subject: Spring Stormwater Discharge Monitoring Report
To whom it may concern:
Glycotech, Inc:, under permit #NCS000258'has performed the Spring qualitative
monitoring of the designated point source discharge Outfall 002. Under this permit,
Glycotech, Inc. is required to perform storm waxer sampling and subsequent analytical
testing.
Enclosed please find the original and a copy of the completed visual monitoring
report and the original and a copy of the analytical testing. Please note that the COD is
within the benchmark value but the pH was 5.2 versus the benchmark of 6 to 9, similar to
the site's previous six outfall samples/reports, in which we relwrted,pHs of 5.0, 4.9, 5.4,
5.8, 5.4 and 5.7 respectively.
Please note that on July 6, 2006, this facility requested a modification to the
existing Stormwater Permit in regard to lowering the pH Benchmark Values. This
request was based on a number of samples taken for pH of the stormwateron site as well
as adjacent waters and mi nwater as collected in a rain gauge. These analysis show that
all waters including rainwater are below the lower benchmark value specified in the
cument,permit
If any questions or comments arise concerning either the visual. monitoring report
or analytical report;.please do not hesitate to contact me at [phone].
Very truly yours,
Alan Stout
President
Glycotech, Inc.

CC:
Linda Willis — Surface Water Protection Section -- Wilmington Regional Office
Gary Wooten — Production Manager- Glycotech, Inc.
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidfuwe on f Uing out this form, please visit: hit ://h2o.enr.state.ne.us/su/Forms Documents.htm#miseforms
Permit No.: N ! S I �j OI �!?I SI 1 or Certificate of Coverage No.: WE"— I 1—LJ 1 1
Facility N
County: _
Inspector
Date of In
Time of Inspection:
g
Total Event Precipitation (inches): /
Was this a Representative Storm Event? (See information below) CdYes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
oecucred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my lmowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. DO 2 Structure(pipe, ditch, etc.) Q /reff
Receiving Stream: RLUC •! f _ -64& F,642
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _ 7",el,v,yiL L/Gdlr C3natdn1 Ti/,u i
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): Na KC
Page 1 of 2
SWU 242-112608

4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
10 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge. where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
O 2 3 4 5
7. Is there any foam in the stornhwater discharge? Yes ONO
& Is there an oil sheen in the stormwater discharge? Yes CNq)
9. Is there evidence of erasion or deposition at the outfall? Yes Nod
10. Other Obvious Indicators of Stormwater Pollution:
List and describe DONE 6 [3,S C2 V F<l
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant expostic+e. These conditions warrant furthler investigation.
Page 2 of 2
SWU-242-112M

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 2 or SAMPLES COLLECTED DURING CALENDAR YEAR: 2ZO'Y
Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME �2Lrk a 7f of
PERSON COLLECTING SAMPLE(S) ";AAva o-rF
CERTIFIED LABORATORY(S) j;rNyrRd C4EA4 Lab # 2.2
Lab #
Part A: Spedfle Monitoring Requirements
COUNTY _ d'e uv-Se'J! CK
PHONE NO. (1/01 - �Z
ZIP2,.,_
(SIGNATURE OF PEAKRTEE OR DESIGNEE)
By this signature, I eertlfy that this report Is accurate
complete to the best of my knowledge.
�
� •. 1
• I '. I I I
t II
15: t 'a l�l .t
I I:
II2M
II I �-
I��©���
I •'
o r
©�
��
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? yes ) no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Ontfall
No.
Date
Sample
Collected
50050
00555
005"
00400
Total Flow
(if applicable)
Total Rainfall
Oil & Grease
Total
Suspended
Solids
pH
New Motor Oil
Usage
I MG
inches
nWA
I mrA
I Units
I
it
—Nil ri
Form SWU-246-112608
Page I of 2

STORM EVENT CHARACTERISTICS:
Date
Total Event Precipitation (incites):
Event Duration (hours): _3 (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Piles
1617 Mail Service Center
Raleigh. North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a
system designed to aware that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those. persons directly responsible for gathering the information, the Information subndtted is, to the best
of myknowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Information,
including the possibility of fines and imprisonment for knowing violations''
zAimz a42��.e 7-16-09
(Signature of Pe
rmlttee) (Date)
Form SWU-246-112608
Page 2 of 2

jr-'nviroc7h-
.
ANALYTICAL & CONSULTING
CHEMISTS
Customer:
GLYCOTECH, INC
PO Box 1956
Leland, NC 29451
Attn: Gary Wooten
Date Received:
Sampled By:
STORMWATER:
Environmental Chemists, Inc.
6602 WmdmiU Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (flax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR- DWQ CERTIFICATE #94. DLS CERTiF7CATE #37729
REPORT OF ANALYSIS
06/17/09
Gary Wooten
Date of Report: June 23, 2009
Purchase Order No: 1075
Report Number: 9-5402
Date
Chemical Oxygen Demand,
Method
Date
Sample ID
Sampled
Lab ID
COD as % mg/L
Code
Analyzed
Outfall 002
06/16/09
# 13822
99
SM 5220 D
06/22/09
Comment:
e �
Reviewed byc del

ENVIRONMENTAL CHEMISTS, INC
Sample Coll on and ChaMC_ps-todv
fiG
L.e Laut Z
6602 Windmill Way
Wilmington, NC 28405
Phone: [phone]
Fax [phone]
Li 5 r VMAnL WIW. V aW(&
E
. I. rar.�-? _t ._ �.�
3 _ �►
�.� I :_ , - -ram:
,...::-,
�� - ti.l
1. _
� ��
49
1 � . II - -1 , .
_► ,5M_ *!= Q ,@j: i
T_
•, I I 1les es Ammonia,i1Cyanide,Phenol, , I Bacteria must 1 ,:. , I_. 1
I- II 1 collection.1 fbr I- I 1 I
INJU ,1 !I S I I IP 1
11
"nurature when Received. Accepted: Rejected: Resemple Requested:
"..-I By Received By: ��'� G e Date: 6 o Time: ao P
P, o OgI4-e 2,0 �'

0
s.
C.T. SPECIALTY PROPERTIES, LLC
2271 Andrew Jackson Hwy, NE
PO Box 1956
Leland, N.C. 28451
910-371-2234
October 24, 2008
ATTENTION: Central Files
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: 2008 Fall Stormwater Discharge Monitoring Report
To whom it may concern:
}ZECEIV-MD
OCT 2 9 2008
C.T. Specialty Properties, LLC, under permit #NCS000258 has performed the Fall
qualitative monitoring of the designated point source discharge Outfall 002. Under this
permit, C.T. Specialty Properties is required to perform storm water sampling and
subsequent analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring report
and the original and a copy of the analytical testing. Please note that the COD is 59 and
within the benchmark value but the pH is 4.8 versus the benchmark of 6 to 9, similar to
the previous five outfall samples/reports in which we reported pHs of 5.4, 5.8, 5.4, 5.7,
and 4.9 respectively.
Please note that on July 6, 2006, this facility requested a modification to the existing
Stormwater Permit in regard to lowering the pH Benchmark Values. This request was
based on a number of samples taken for pH of the stormwater on site as well as adjacent
waters and rainwater as collected in a rain gauge. These analysis show that all waters
including rainwater are below the lower benchmark value specified in the current permit.
If any questions or comments arise concerning either the visual monitoring report or
analytical report, please do not hesitate to contact me at [phone], ext 20.
Very truly yours,
.T. Spec
�cLawialty Properties, LLC
�C
Jhorn
Plant Manager

CC:
Kenneth Carlton - CEO, Nekekim Corporation (CT Specialty Properties, LLC owner)
Aisha Lau - NC Division of Water Quality
Linda Willis - Surface Water Protection Section - Wilmington Regional Office
Gary Wooten - Operations Support Leader, CT Specialty Properties, LLC
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

Permit No.: NK- Sl
Facility Name: C
County: -
hvecto
Date oflnon: _
Stormwater Discharge Oatfall (SDO)
Qualitative Monitoring Report
0/0i2-iSi Yr
SPEclAO-1
or Cerd icame of Covemp No.: NI�IGI 1 1 1 1 1 1
PP-oPMT7FS _ L i- c
By this siDw u r, I certify that this rqmt is a=wW* and complete to the best of my knowledge:
of or Designee)
1. Ouftll Daw%dion
Outfail No. 062- SbrnctGffe (pipe, ditch, dr-) J rrC
Receiving Stream: t4[.ca GA -?DR 1794-juc #4 , CAS A e-_ ��r � _ .� t J'A/
Describe the uxbn&W activities that occur within the 66M drainage area:
2. Color
Describe the color of the disdwp using basic Colors (red, kvwn, bloc, etc.) wd tint OMK media,
dark) as desat*x : L j CR R= V&jLY=,OW Tint
3. Odor
Daa%c any disc n ct odors that the &MhmW may bane (Le., smells strongly of od, weak chlorine odor,
etc.) /VO Al E
4. CIO*
Choose the number which best the dadW of the dim where I is clear and 10 is very
Clowdj .
C
2 3 4 5 6 7 S 9 10
Page 1
•
swu-242-1015"

5. Ftoating Sands
Choose the matcher which best descriles the amoamt of floating solids in the staamwater discharge where
1 is no solids and 10 is the mirface covered with floating solids:
( DI 2 3 4 5 6 7 8 9 10
6. Sided Solids
Choose the number which best describes the an curt of suspended solids in the shmnwater discharge
where 1 is no solids and 10 is exbumely muddy:
1 2 3 4 5 6 7 8 9 10
7. Foam
Is there any foam in the stornmda discharge? Yes DNo'
S. OD Sheen
Is them an oil sheen in the stormwater discharge? Yes No
9. Other Obvious indleaftn of Sbormwater Pollfion
�, L VE a<s
Nott Low clarity, high solids, and/or the presence of foam or o0 sheen may be indicative of pollutant
exposure.. These conditions may warraat fup hivestigation.
Pap 2
swU-242�1015W

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NC S ODd 2 53 .� or
Certificate of Coverage Number: NCG
FACILITY NAME T SP irr C zX Af,z77C"f LLC
PERSON COLLECTING SAMPLE(S)
CERTIFIED LABORATORY(S) c:. efgC44
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 7-00 8
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sa piing results from the laboratory.)
COUNTY v R1S rurc
P NFLNO. Q!o - Z 2
(SZNAMM OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes no
(if yes, complete Part B)
Part n: veoicie Maintenance AC
moauorft
ReQuIrements
On":. ,.:..', :
Date::.:.:.: :.:.
SOEI�O; ` ::..
00556', -` ::` .
= 00 .
No: -:
Sample;; : '
,Total Flow _
:.OII and
Total :;'=:.;;:. °•
pH ..`
New;Niobor:
Collected
Grease:: .:
S.ospon
646. age
Solids
....
.a�oJddlvr:� : �.�::
,MG,'�:�.:.;'..�.'::�m�!!
�:::.; •� -
�::mr11:::�:�.� ��� ::..
'ualt.:.�.:-- :-:..:gaVtao''�
Form SWU-246-051100
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date 9 2G o $
Total Event Precipitation (inches): 41.50
Event Duration (bona): Z R -
(if more than one storm event was sampled)
Date
Total Event Precipitation (Inches):
Event Duration (hours):
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and ail attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my Inquiry of the person
or persons.who manage the system, or those persons directly responsible for gathering the information, the information submitteel is, to the best
of my knowledge and belief; but, accurate, and complete. I am swats that there are significant penalties for submitting Use information,
Including the posslbWty of flues and imprisonment for knowing violations."
C
���-?= Q 8
re Permittee) (Date)
Form SWU-246-051100
Page 2 of 2

Environmental Chemists, Inc.
66M VVIndmill Way •VAhninghm,NC2M
(910) 392-= (ms) •: (na) 3924424 (Fax)
710 Bowwrk wm Road = �r�o. NCa.79AS
ANALYrOAL a oo*MMA31,q (= 473'
CHEMI rs Kcna : DWQ COUVICATE Ma, cxs CEUVICATE RVM
cush)M r:
CT SPECIALTY P"PERT>ZS; LLC
PO Box 19%
Le1arK NC 2"51
AM: Gary Wootm
Deis Decefv & 09/29M
Sampled By: Cary Wootm
FALL'OS SMTIMWATER:
Dais or IUPM* ocwtw 4, 2=
Purchm Order No:
Report Number: 9-9162
Report To: Gary Woo>m
Prate
Sample ID
Date
Lab ID
Cbm1 O Dc==d,
Mc&W
Date
Sampled
COD M8%
Cods,
A
OvjftU OR
%24"
# 21784
59
SM S22O D .
10/06M .
Comment:
Radewed br.
J
pi
2.d. dips MD 8D C2 zoo

-.- �l( Sj
C.T. SPECIALTY PROPERTIES, LLC
2271 Andrew Jackson Hwy, NE
PO Bog 1956
Leland, N.C. 28451
910-371-2234
April 25, 2008
ATTENTION: Central Files
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: Spring Stormwater Discharge Monitoring Report
To whom it may concern:
ZZ19: CP���
�P� 2 zoos
C.T. Specialty Properties, LLC, under permit #NCS000258 has performed the Spring
qualitative monitoring of the designated point source discharge Outfall 002. Under this
permit, C.T. Specialty Properties is required to perform storm water sampling and
subsequent analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring report
and the original and a copy of the analytical testing. Please note that the COD is within
the benchmark value but the pH was 4.9 versus the benchmark of 6 to 9, similar to the
previous four outfall samples/reports in which we reported pHs of 5.8, 5.4, 5.7, and 5.4
respectively.
Please note that on duly 6, 2006, this facility requested a modification to the existing
Stormwater Permit in regard to lowering the pH Benchmark Values. This request was
based on a number of samples taken for pH of the stormwater on site as well as adjacent
waters and rainwater as collected ' in a rain gauge. These analysis show that all waters
including rainwater are below the lower benchmark value specified in the current permit.
If any questions or comments arise concerning either the visual monitoring report or
analytical report, please do not hesitate to contact me at [phone], ext 20.
Very truly yours,
. Specialty Properties, LLC
Jimmy f�cLawhorn
Plant Manager

CC:
Kenneth Carlton — CEO, Nekekinn Corporation (CT Specialty Properties, LLC owner)
Aisha Lau -- NC Division of Water Quality
Linda Willis -- Surface Water Protection Section — Wilmington Regional Office
Gary Wooten — Operations Support Leader, CT Specialty Properties, LLC
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

Stormwater Discharge -Outfall (SDD)
Qualitative Monitoring Report
Permit No.: N I C I sl D D O12 / S S/ or Certificarte of Coverage No.: N/ C/ G I I I
Facility Nam Or t L c
County: u w l ck Phone No. 9/0 - 3 7 ! - 'Z 7-3
Inspector: I rc! e+-eN
Date of Inspection: I o
By this signature, I certify that this report is accurate and oomplete to the best of my knowledge:
avy-I'M4 C
M64
Permittee or Designee)
1. Outfall Description
Outfall No. 00 Z . Structure (pipe, ditch, etc.) 0 / TC rl
Receiving Stream: AL r ca"Q %S"N c tf, AP9�f3M9 R.oczz 2551AI.
Describe the industrial Aptivifies that ocaff within the o-Wall &ainage area
H��trc,Q.�. f�R-oaESS r�Cs
2. Color
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium,
dark) as d=:riptors: L. / Gfl T YELLo ed T/AIT
3.Odor
Describe any distinct odors that the discharge may have (Le., smells strongly of oil, weak chlorine odor,
etc.)No At 6
4. Clarity
Choose the number which best desc nbes the clarity of the discharge where 1 is clear and 10 is very
cloudy:
1 2 3 4 5 6 7 8 9 10
Page 1 • •
5WU-242-101599

5. Floating Solids
Choose the number which best describes the amount of floating solids in the stormwater discharge where
t is no solids and 10 is the surface covered with floating solids:
( 1 J 2 3 4 5 6 7 8 9 I0
6. Suspended Solids
Choose the number which best describes the amount of suspended solids in the stormwater discharge
where 1 is no solids and 10 is extremely muddy:
( l J 2 3 .4 5 6 7 8 9 10
7. Foam
Is there any foam in the stormwater discharge? Yes Flo J
8. Oil Sheen
Is there an oil sheen in the stormwater discharge? YeslNo
9. Other Obvious Indicators of Stormwater Pollution
List and describe Alo ov E 04314XVEM
Note: Low clarity, high solids, and/or the presence of foam or oil sheen may be indicative of pollutant
exposure. These conditions may warrant furdw investigation.
Page 2
SWU-242-101599

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NC 5 600 2 S $ or
Certificate of Coverage Number: NCG
FACILITY NAME VZCx4cwej6 Le, C
PERSON COLLECTING SAMPLE(S). a
CERTIFIED LABORITORY(S) kAhliAO C04f t Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: ZCV g
(This monitoring report shall be recelved.by the Division no later than 30 days from
the date the facility recexll the sampling results from the laboratory.)
COUNTY Aj-g J 1 Ck
P NF�NO. ! 7 - Z 3
(S NATURE OF PERMITTEE OR DESIGNEE)
Bf this signature, I certify that this report is accurate
Complete to the best of my knowledge.
-Outfall Date S001}5fl
No: Sample .
. , 'Collected '; Fl wI . . , � .
h 6 2 11 / o St S'4'
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ,_,,,Yes _no
(if yes, complete Part B)
0
Part H: vetaicie Maintenance Monitoring Requirements
Oatfall
Date
500Mh ,
OOSSfi .
00530 ..:
?:
Nn
Sample
Total Flow :
' O1Cead
-Total -
pH
New Motor;
Collected
- =
Grease ,
Suspended
OihUsage
Solids
malditr,
;:MG'
mgll
mtJl..
ianlf
�aUma

STORM EVENT CHARACTERISTICS:
Date Y//Z,ozr
Total Event Precipitation (inches); 1. r
Event Duration (hours): 30 .
(if more than one storm event is sampled)
Date
Total Event Precipitation (inches): ------------
Event Duration (hours);
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Services Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a
System designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my Inquiry of the person
Or persons who manage the system, or those persons directly responsible for gathering the Information, the Information submitted Is, to the best
Of my knowledge and belief, true and complete. I am aware that there are significant penalties for submitting false information,
to eluding the possibility of fines and Imprisonment for knowing violations."
2Sb8
(Da e) ..
Form SWU-246-051100
Page 2 of 2

Op —
Environmental Chemists, Inc.
ree&nvi.wch 6602 Windmill Way - Wilmingwn. NC 2MW
(910) . 2-CM (Lab) - [phone] (Fax)
si.
710 &imwrhma n Rcmd Mantra, NC 27954
(252) 473-5M
ANALYTICAL A CONSULTING
CFISlll IM VCDEM. VWQCERTIFICATE O%. DL'*CER1 RCATEOT!V
customer:
CT SPECIALTY PROPER13M LLC
PO Box 1956
Leland, NC 29451
Attu: Gary Wooten
Date Received:
Sampled By:
S'MTLMWATWR-
RMOAT OF ANALYSIS
04/01/09
Gary Wooten
Date of Report: April T, 2009
Purchase Order No:
Report Nexuber. 3-2999
Report To: Gary Wooten
Project:
Sample ID
!
Sampled
Lab ID
Dawad,
COD mgjL
Boa
Cade
Dad
Analyzed
ChsOM 002
f"IM
6 6389
58
SM
5= D
04ld1: M
Commence
Reviewed by
i-d ba1HP26EOTS Q84ROJJnu3 dva :ao 80 ea ,add

(EM)
lientt C T S e e
a
Sample Identifitation
O uT Fd LL 002-
P0 s4
,LTV AZOP
LN VMONMENTAL CHEMISTS, INC
602 Windmill Wa)
Wgmington, NC 2940a
rho: [phone]
Fa: (910) 3192.4424
*-MRMWA,TJJZ QOA eW,+NC_E-,5PP,NG og
eWnvAnon
COD
n w
-- D TKN s Samples for Ammonia, , C�►an(�fd% Phenol, and Bacterla must be dechiorinated
0.2 am or fens in the field at the time of collection. See reverse side hr leetructionL
Transfer ReNe By. Dat*mme Received By: DateMme
.M- } 2 ISM
2.
Temperature when Received:, Aeeepiedi__`____�_ Rejected: Resample Requested:
Delivered s Date: Time:
. By Received By: _- _ _ ,.�
Comments: PCo

C.T. SPEC IA' PROPERTIES, LLC
2271 Andrew Jackson Hwy, NE
PO Boa 1956
Leland, N.C. 28451
910-371-2234
November 14, 2007
ATTENTION: Central Files
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: Fall 2007 Stormwater Discharge Monitoring Report
To whom it may concern:
RECEIVED
BY:
Nov 1 6 2007
C.T. Specialty Properties, LLC, under permit #NCS000258 has performed the Fall
qualitative monitoring of the designated point source discharge Outf dl 002. Under this
permit, C.T. Specialty Properties is required to perform storm water sampling and
subsequent analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring report
and the original and a copy of the analytical testing. Please note that the COD is within
the benchmark value but the pH was 5.4 versus the benchmark of 6 to 9, similar to the
previous three Stormwater Reports, which had pHs of 5.8, 5.4, and 5.7 respectively.
Please note that on July 6, 2006, this facility'requested a modification to the existing
Stormwater Permit in regard to lowering the pH Benchmark Values. This request was
based on a number of samples taken for pH of the stormwater on site as well as adjacent
waters and rainwater as collected in a rain gauge. These analysis show that all waters
including rainwater are below the lower benchmark value specified in the current permit.
We continue to monitor the pH of the rainfall and it is consistently less than the lower
benchmark value.
If any questions or comments arise concerning either the visual monitoring report or
analytical report, please do not hesitate to contact me at [phone], ext 20.
Very truly yours,
C.T. Specialty Properties, LLC
Gf
T y Mc orn - Plant /l Manager

CC:
Kenneth Carlton -- CEO, Nekekim Corporation (CT Specialty Properties, LLC owner)
Aisha Lau — NC Division of Water Quality
Linda Willis — Surface Water Protection Section — Wilmington Regional Office
Gary Wooten — Operations Support Leader, CT Specialty Properties, LLC
Enclosure: Visual Monitoring Report and 002 Outfall Analytical data

Permit No.: k! I C / s
FacE ty Name: C'
.
Dade of In
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
10 Q12 / S/ 81_ or Certificate of Coverage No.: N I C/ G 1 l l l l l l
sprc-im-x PRoPCRTr F S . L.LC
rick .Phone No. 9/6— 37/ ZZ34-
By this signabu+e, I certify that this report is made and complete do the best of my knowledge:
nn C
or Designee)
1. Outfall Description
Outfall No. ©o L . Structure (pipe, dit* etc-) U/7
Receiving 34eam- Li
Describe the hWkMUW aefivities that o0mr V400 the odWI drai�ge area:
2. Color
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium,
dark) as descr#tors: _ GIGHt A—eeow _ `rill i
3.Odor
Describe any dim odors that the dischuge may have (U. , smeEls saw* of o% weak chlonne odor,
etc.) O
a clarity
Choose the nwnber which best describes the clarity of the discharge where I is clear and 10 is very
cloudy_
1 ( 2/ 3 4 5 b 7 8 9 10
��// Page 1 .
swu-2 2-tots"

S. moats Solids
Choose the number which best describes the amount of floating solids is the stormwa#er discharge where
1 is no solids and 10 is the surface covered with floating solids:
( 1 J 2 3 4 5 6 7 9 9 10
6. Suspended Solids
Choose the nuranber which best desc ilm the amount of suspended solids in the stormwater discharge
where 1 is no solids and 10 is extremely muddy:
1 3 4 5 6 7 9 9 10
7. imam �//
Is there any foam in the stormwater discharge? Y No
L Oil Sheen
Is there an oil sheen in the stormwater discharge? Yes No
9. Other Obvious Indicators of Stormwater PolluMon
List and describe to DNE QB.f Egel Eta
Now Low clarity, high solids, and/or the presence of foam or oil sheen may be indicative of pofttant
exposure. These conditions may warrant fiat% brvestigatim
Page 2
sw13-242-1019N

Permit Number: NC S 4000 Z54'
Certificate of Coverage Number: NCG
or
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
FACILITY NAME CIA 47 d FRT7 FJ i. C
PERSON COLLECTING SAMPLE(S) a
CERTIFIED LABORATORY(S) O Lab #
Lab #
Part A: Specific Mouitorlug Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR:
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY— RrrNS wick
P NO. !O Z 7
(S NATUA OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
I
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓0
(if yes, complete Part B)
Part V: Vehicle Maintenance Activity Monitoring Requirements
OuKall
No.
Date
Sample
Collected
30050
00556
00530
80400
Total Flow
ON and
Grease
Total
Suspended
Solids
pH
New Motor
Oil Usage
mold
MG
m
unit
RMTO
-TA
Form SWU-246-051100
Page ].of 2

STORM EVENT CHARACTERISTICS:
Date ID zS%7
Total Event Precipitation (inches): Z Z
Event Duration (hours): _ 24
(if more titian one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours);
Mail Original and one copy to:
Division of Water Quality
Attn, Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I eer ft under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my Inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the Information submitted h4 to the best
of my knowledge and belief', true, accurate, and complete. I am aware that there are significant penalties for submitting false Information,
including the possibility of fines and imprisonment for knowing violations."
QVW� -- a /O/,z
(S tore of ermittee) (Date)
Form SWU-246-051100
Page 2 of 2

customw.
Cr SPECIALTY PROPERTIES~ LLC
PO Box 1956
Leland, NC 28451
Attn: Gary Wooten
Date Pjxxived:
Sampled By:
REPORT OF ANALYSIS
10/26/07
Gary Wooer
Data of Report: October 31, 2007
Pie Order No:
ReportNumber.: 7-10548
Report To: Gary Wooten
Project:
Sample ID
Date
ID
Cal Oxygen Demax4
Method
Date
SampledLab
COD mg/L
Code
Anab7Ad
Outlaii M
IOR.SM
# 23766
29
SM �
10129/07
comment
Reviewed by

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ENVIRONMNTAL MISTS: INC
"02 Wind" Way
Who, Nc zw
Phm (910) 3924M
F u (910 39L"24
f i .; f � �___. � ,_,!•�du3�:L'��;�M:�iT.1�.�.�'t
."V'Ihl.1l�:.WA
;�11 � ►; �
i R; -K�1. �!.:!! _►','L��nf: i,� ] R��I�].lil
it �,-
ME
:
ll '!'ti:
=mmcm'
I
r��r�rrrrrr���r��■
i �. Ilf II _;" �1 it li'•I!;
7F31.11,l I- f Ili:l I II}: ,1
l / II 1 �f � :�'ae l I - :V
:Ili I
II III,1 I i e li-.
lop
T�p�r'a�re wh�no��v�: �° A�►t�ds a end• Resawple R�questeds
D�iv�red B�!s �_� Ihre� Bps � Dates' t'a• '�m�
Com -- al l i,�

C.T. SPECIALTY PROPERTIES, LLC
2271 Andrew Jackson Hwy, NE
PO Box 1956
Leland, N.C. 28451
910-371-2234
June 1, 2007
ATTENTION: Central -Files
Division of Water Quality
Surface Water Protection Section
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: Spring Stormwater Discharge Monitoring Report
To whom it may concern:
C.T. Specialty Properties, LLC, under permit #NCS000258 has performed the Fall
qualitative monitoring of the designated point source discharge Outfall 002. Under this
permit, C.T. Specialty Properties is required to perform storm water sampling and
subsequent analytical testing.
Enclosed please find the original and a copy of the completed visual monitoring report
and the original and a copy of the analytical testing. Please note that the COD is within
the benchmark value but the pH was 5.7 versus the benchmark of 6 to 9, similar to the
2006 Spring and Fall samples, which had pHs of 5.8 and 5.4 respectively.
Please note that on July 6, 2006, this facility requested a modification to the existing
Stormwater Permit in regard to lowering the pH Benchmark Values. This request was
based on a number of samples taken for -pH of the stormwater on site as well as adjacent
waters and rainwater as collected in a rain gauge. These analysis show that all waters
including rainwater are below the lower benchmark value specified in the current permit.
If any questions or comments arise concerning either the visual monitoring report or
analytical report, please do not hesitate to contact me at [phone], ext 20.
Very truly yours,
C.T. Specialty Properties, LLC
Jimmy McLawhorn
Plant Manager

CC:
Kenneth Carlton — CEO, Nekekim Corporation (CT Specialty Properties, LLC owner)
Aisha Lau — NC Division of Water Quality
Linda Willis — Surface Water Protection Section — Wilmington Regional Office
Gary Wooten — Operations Support Leader, CT Specialty Properties, LLC
Enclosure: Visual Monitoring Report and 002 OutfaIl Analytical data

0
5. Floating Solids
Choose the number which best descn-W the amount of floating solids m the stormwater discharge where
1 is no solids and 10 is the surface covered with floating solids:
co 2 3 4 5 6 7 8 9 10
6. Suspended Solids
Choose the number which best describes the amount of suspended solids in the stormwater discharge
where 1 is no solids and 10 is extremely muddy.-
1 2 3 4 5 6 7 9 9 10
7. Foam
Is there any foam in the stormwater discharge? Yee
E_aEO-liM �.
Is there an oil sheen in the stormwater discharge? Yes@
9. Other Obvious indleatora of Storowater Pollution
List and describe 0 Q s ca V gm
------------
Note: Low clarity, high solids, and/or the presence of foam or oil sheen may be indicative of pollutant
exposure. Tbese conditions may warrant further investigation.
Page 2
swu M-1015"

Permit No.. 13
Facility Names:
�r—B
Inspo—
Date of lnsped
Aroma
Stormwater Discharge Out -fall (SDO)
Qualitative Monitoring Report
-/S 10/ 0I0/Z l5/ 8 / or Cericate of Coverage No.: N / C / G_ / l _ _L I
_TSPEcrRcr� RapF72-r+ES -, LtC
WA' t cad CA . Phone No.
By this signature, 1 certify did this report is accurate and complete to the best of my knowledge:
or Designee)
1.Ontfall Dearrlpdm
Outlhil No.---0�—�— Structure (pip dU etc.) I T
Receiving gtr+eam: _ _ HtuG4r�rz RA�ucs� CAAE .tR2 t•,E�2 phi wl
Describe the industrial activities that occur within the ouifali drainage area:
Cdc'"ir'AL P&0 c.FS-rrNC' -
2. Color
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium,
darks) as descriptors: IM tr b O u m _ r ad-AW Ti w?r
3. Oder
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor,
etc.) &D nl E
4. Clarity
Choose the number which best describes the clarity of the discharge where l is clear and 10 is very
cloudy:
1 2 03
4 5 6 7 8 9 10
Page 1

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number. NC S 0 00 ZS S . or
Certif Bate of Coverage Number: NCG
FACILITY NAME C T SPECc L C
PERSON COLLECTING SAMPLE(S)
CERTIFIED LABORTTORY(S) E', yr 2c CueAw Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR:
(Tbb. monitoring report shell be received by the Division no later than 30 doys from
the date the facift recta es the sanipliog result from the laboratory.)
COUNTY
PH NO.3-7/-23394
C
(SICNATURE OF PERMITPEE OR DESIGNEE)
By this signature, I certify that this report b accurate
Complete to the best of my knowledge.
f.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ,_Yes 3Gno
(if yes, complete Part B)
Purl Re Vwhielo Mnintrnwnro.Mnnitnrinv Rmnirwrtmwntn
Ootfall
No.
Date
Sample
Collected
500050
00556
00530
0M
Total Mow
Oil and
Green
Total
Suspended
Solkls
pH
New Motor
On Usage
moldd/yr
MG
so
Mal
unit
Anumo
Form SWU-246-051100
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date 5 18 017
Total Event rticipitation (inches):
Event Duration (hours): lZ .
(if more than one storm event is sampled)
Date
Total Event Precipitation (Inches):
Event Duration (boor'):
Mall Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Services Center
Raleigh, North Carolina 27694-1617
*1certity, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
System designed to auure that qualified personnel properly gather and evaluate the Information submitted. Haled on my inquiry of the person
Or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted 1% to the best
Of my knowledge and belie!, true and complete. I am aware that there are significant penalties for submitting false information,
In clading the possibility of fines and Imprisonment for knowing vialatlons."
t'c l 2�0
(Date)
Form SWU-246-051100
Page 2 of 2

NOW00— E al Ch ' 4-In
F7
L enviroehe,17
ANALYMAL & CONSULTING
CHEMISTS
Customer:
CT SPECIALTY PROPERTIES, LLC
Pp Box 1956
Leland, NC 28451
Attu: Gary Wooten
Date Received:
Sampled By:
CTORMWATERe
05/19/07
Gary Wooten
nvaronment emir s, c.
6602 Windmill Way • WAn ngton, NC 28405
.(910) 392-oz2°23 (Lab) • [phone] (Fax)
710 Sowsertown Road • Manteo, NC 27954
[phone]
WREN& DWQ CERTMCATE 094. DLS CEMRCATE #37729
'.a 7 SpRi46 Sioo wwwfM SJm ok E
Date of Report: May 23, 2007
Purchase Order No: 5/ of
Report Number: 74369
Report To: Gary Wooten
Project:
Sample ID
Date
Lab ID
C%a°iw Omen Demand,
Date
Sampled
COD mg/L
Analyzed
Outfall 002
05/1V07
# 9224
66
5/21/07
Comment:
Reviewed by t

e r
I
6M WiodmM Way
Wbmmgton, NC 28403 B .
Phone: [phone]
Fu (910) 392A424 7
r
i. Ifl l! l� I! I '. 1 :� I
II'-i! , W7.1 N I, 1 1 - I Y LI
li L 1411 L . *•I I "- I . s I : 1 !I .I I al 1 I''
MAN
OWN
Temperetore when eds__ Acxepted:
, Rample Requested:
hYR�Date: By:l
mmrce7
Comments: goo s Q.N