NCS000173_MONITORING INFO_20171109

STORMWATER DIVISION CODING SHEET
PERMIT NO.
NG S pip n '-?>
DOC TYPE
0 FINAL PERMIT
MONITORING INFO
APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ Z0rl it 0
YYYYMMDD

PAGE 1 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
PERMIT NO. NCS000173 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
FACILITY NAME: N.C. STATE PORTS AUTHORITY PORT OF MOREHEA❑ CITY COUNTY: CARTERET
PERSON COLLECTING SAMPLES: Michael D. Mason/Kameron Smith_ - CATLIN PHONE NO. 910-452-5861
CERTIFIED LABORATORY: PACE ANALYTICAL SERVICES, INC. CERT. # 37706
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
and complete to the best of my knowledge.
PART A: Specific Monitoring Requirements
Outfall No.
Date Sample
Collected
Molddl r
Total
Rainfall
Inches
Chemical
Oxygen Demand
m IL
Total Suspended
Solids
m 1L
Total
Phosphorus
m IL
pH
(Units)
Oil &
Grease
m 1L
Permit Benchmark Values
120
100
2
6-9
15
301
11/9/2017
0.34
684
6.3
NR
6.4
<11
402
11/9/2017
0.34
69.0
17.1
NR
7.7
<1.1
506A1
11/9/2017
0.34
143
3.6
0.79
7.3
<1.1
5061131
11/9/2017
0.34
147
18.5
NR
7.2
<1.1
510
1119/2017
0.34
88.0
37.7
NR
7.9
<1.1
803
11/9/2017
0.34
810
29.8
1.0
7.2
1.3 J
907
11/9/2017
0.34
<12.5
<2.5
NR
8.2
<1.1
NR - Not Required
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

NORTH
CAROLINA
PORT'
June 5, 2017 RECEIVED
Division of Water Quality :IUN G $ 2017
GENT
Water Quality Section , RAL FILES
Attention Central Files 1)VR SECTION
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: North Carolina State Ports Authority
Spring 2017, Qualitative Storm Water Monitoring Results
Port of Morehead City, Permit No. NCS000173
Central Files:
In Keeping with the terms of storm water permit NCS000173, enclosed are two copies of
the Spring 2016, Qualitative monitoring results. This should complete the subject facility's
Spring 2016 storm water monitoring requirements.
If any additional information is needed. please call me at [phone].
Sincerelv,
NORTH CAROLINA STATE PORT AUTHORITY
Todd C. Walton
Sr. Environmental Analyst
Cc: environmental files
North Carolina State Parts Authority • 2202 Bumett Boulevard • PC Box 9002 - Wilmington, NC 28402 • www.ncports.com

Pace Analytical Services, LLC
e 9800 KinceyAve. Suite 100
ceAna"a
f Huntersville, NC 28078
F�
[phone]
r.
' s
ANALYTICAL RESULTS
Project: PORT OF MOREHEAD-202005
Pace Project No.: 92341670
Sample: 301 Lab ID: 92341670001 Collected: 05/23/17 10:05 Received: 05/23/17 16:00 Matrix: Water
Report
Parameters
Results Units Limit
MDL
OF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
NO mg1L 5.0
1.1
1
05/30117 07:11
2540D Total Suspended Solids
Analytical Method: SM 25401D
Total Suspended Solids
3.9 mglL 2.5
2.5
1
05/26/17 03:02
5220D GOD
Analytical Method: SM 5220D
Chemical Oxygen Demand
357 mg1L 25.0
12.5
1
06/01117 01:41
Sample: 402
Lab ID: 92341670002 Collected: 05123/17 10:25
Received: 05/23/17 16:00 Matrix: Water
Report
Parameters
Results Units Limit
MDL
OF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mglL 5.0
1 A
1
05130/17 07:11
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
20.3 mglL 2.5
2.5
1
05/26/17 0102
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
132 mglL 25.0
12.5
1
06/01117 01:41
Sample: 510
Parameters
Lab ID: 92341670003 Collected:
Report
Results Units Limit
05/23/17 10:45
MDL OF
Received: 05/23117 16:00 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16646
Oil and Grease
NO mglL 5.0
1.1 1
05/30/17 07:12
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.8 mg1L 2.5
2.5 1
05/26117 03:03
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
22.OJ mg1L 25.0
12.5 1
06/01/17 01:41
Sample: 506 81 Lab ID: 92341670004 Collected: 05/23117 11:15 Received: 05123/17 16:00 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease NO M91L 5.0 1.1 1 05I30/17 07:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in run,
Date: 06/0112017 07:39 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 17

NORTH
CAROLINA
P0RT�.r
qq _,�
December 13, 2016
Division of Water Quality
Water Quality Section
Attention Central Files
I617 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: North Carolina State Ports Authority
Fall 2016, Qualitative Storm Water Monitoring Results
Port of Morehead City Permit No NCS000173
Central Files:
RECEIVED
DEC 19 2016
CENTRAL FILES
DUVR SECTION
In keeping with the terms of storm water permit NCS000173 enclosed are two copies of
the fall 2016, Qualitative monitoring results. This should complete the subject facility's fall
2016 storm water monitoring requirements.
If any additional information is needed. please call me at [phone].
Sincerely,
NORTH CAROLINA S"fATE PORT AUTHORITY
Todd C. Walton
Sr. Environmental Analyst
Cc: environmental tiles
North Carolina State Ports Authority - 2202 Burnett Boulevard - PO Box 9002 - Wilmington. NC 28402 - www.ncparts.corn

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Pace Analytical Services, LLC
Mg•� fe . 9600Wnceyave, C 2 100
Jj%�] f Humers,riDe, NC 28078
wwwF2z'&G0M [phone]
SAMPLE SUMMARY
Project: 202005
Pace Project No.: 92319638
Lab 10
Sample iD
Matrix
Date Collected
date Received
92319638001
301
Water
1111411610:10
11/1411615:49
92319638002
402
Water
1111411610:25
11/1411615:49
92319638003
907
Water
11114116 10:45
11/1411615:49
92319638004
506AI
Water
1111411610:55
1111411615A9
92319638005
506B1
Water
1111411611:05
1111411615:49
92319638006
510
Water
11/14/16 11:18
11/14/16 15:49
92319638007
803
Water
1111411611:30
1111411615:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 16

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Project 202005
Pace Project No.: 92319638
Lab ID Sample ID
92319638001 301
92319638002 402
92319638003 907
92319638004 506A1
92319638005 506B1
92319638006 510
92319638007 803
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 20078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 1664E
JMS
1
PASI-C
SM 2540❑
MJS1
1
PASI-A
SM 5220D
MDW
1
PASI-A
EPA 16648
JMS
1
PASI-C
SM 2540D
MJS1
1
PASI-A
SM 5220D
MDW
1
PASI-A
EPA 1664B
JMS
1
PASI-C
SM 25400
MJS1
i
PASI-A
SM 5220D
MDW
1
PASI-A
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJS1
1
PASI-A
EPA 365.1
B RJ
1
PAS I -A
SM 5220D
MDW
1
PASI-A
EPA 1664E
JMS
1
PASI-C
SM 2540D
MJS1
1
PASI-A
SM 5220D
MDW
1
PASI-A
EPA 1664B
JMS
1
PASI-C
SM 2540D
MJ51
1
PASI-A
SM 5220D
MDW
1
PASI-A
EPA 16648
JMS
1
PASI-C
SM 25400
MJS1
1
PASI-A
EPA365.1
BRJ
1
PASI-A
SM 5220D
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 16

(�Iaoe,Mal0d
wwwpacebbsctan
ANALYTICAL RESULTS
Project 202005
Pace Project No.: 923195W
Pace Anahrtical Services, LLC
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 301
Lab ID: 92319638001 Collected:
11/14/16 10:10
Received: 11/14/16 15:49 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mglL 5.0
1.1 1
11/22/16 09:37
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mglL 2.5
2.5 1
11116/16 20:07
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg1L 25.0
12.5 1
11/16/16 22:05
Sample: 402 _
Parameters
HEM, Oil and Grease
Oil and Grease
2540D Total Suspended Solids
Total Suspended Solids
522oD COD
Chemical Oxygen Demand
Lab ID: 92319638002 Collected.
11/14/16 10:25
Received: 11/14/16 15:49 Matrix: Water
Report
Results Units Limit
MDL DF
Prepared Analyzed CAS No.
Analytical Method. EPA 1664E
ND mg1L 5.0
1.1 1
11/22/16 09:38
Analytical Method: SM 2540D
3.3 mglL 2.5
2.5 1
11/16/16 20:07
Analytical Method: SM 5220D
ND mg1L 25.0
12.5 1
11/16/16 22:05
Qua[
Sample: 907
Parameters
Lab ID: 92319638003 Collected:
Report
Results Units limit
11114/16 10:45
MDL DF
Received: 11/14116 15A9 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L 5.0
1.1 1
11/22/16 09:38
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
8.2 mg1L 2.5
2.5 1
11/16/16 20:08
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
79.0 mg1L 25.0
12.5 1
11/16116 22:05
Sample: 506A1 Lab ID: 92319638004 Collected: 11/14/16 10:55 Received: 11/14/16 15:49 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1.1 1 11122/16 09:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/22/2016 03:24 PM without the written consent of Pace Analytical Services, LC. Page 5 of 16

aceAnalyfr`cal
wwwpaaqlabs.carn
Project: 202005
Pace Project No.: 92319538
Sample: 50SAl
Parameters
2540D Total Suspended Solids
Total Suspended Solids
365.1 Phosphorus, Total
Phosphorus
5220D COD
Chemical Oxygen Demand
Pace Analytical Services, LLC
9a00KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Lab ID: 92319638004 Collected:
11/14/16 10:55
Received: 11/14/16 15:49 Matrix; Water
Report
Results Units Limit
MDL OF
Prepared Analyzed CAS Nc
Analytical Method: SM 2540D
13.8 mglL 3.1
3.1 1
11/16116 20:08
Analytical Method: EPA 365.1
1.0 mg1L 0.050
0.025 1
11/18/16 2T40 7723-14-0
Analytical Method: SM 5220D
15.01 mglL 25.0
12.5 1
11/16116 22:05
Qual
Sample: 506B1
Lab 1D: 92319638005 Collected:
11/14/16 11:05 Received:
11/14116 15A9 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF Prepared
Analyzed CAS No.
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mglL 5.0
1.1 1
11/22/16 09:39
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.7 mg/L 2.5
2.5 1
11/16/16 20:08
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
171 mg1L 25.0
12.5 1
11/16/16 22;05
Sample: 510
Lab ID: 92319638006 Collected:
11/14/16 11:18 Received;
11/14/16 15A9 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF Prepared
Analyzed CAS No,
Qual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO mglL 5.0
1.1 1
11/22/16 09:39
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
3.3 mglL .2.5
2.5 1
11/16/16 20:09
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
52.0 mg1L 25.0
12.5 1
11/16/16 22:05
Sample: 803
Lab ID: 92319638007 Collected:
11/14/16 11:30 Received:
11/14/16 15:49 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF Prepared
Analyzed CAS No.
Quaff
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L 5.0
1.1 1
11/22/16 09:40
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date; 11/22/2016 03:24 PM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 16

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wffiacpacelabsmrr
ANALYTICAL RESULTS
Project: 202005
Pace Project No.: 92319638
Pace Analytical Services, LLC
9800 Kincey Ave. Suite100
kuntersviDe, NC 28078
[phone]
Sample: 803
Parameters
Lab ID: 92319638007 Collected.
Report
Results Units Limit
11114/16 11:30
MDL DF
Received: 11114/16 15:49 Matrix: Water
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
9.9 m91L 2.5
2.5 1
11116/1620:09
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
0.35 mg1L 0.050
0.025 1
11118/16 23:41 7723-14-0
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO m91L 25.0
12.5 1
11/16/16 22:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/22/2016 03:24 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16

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QUALITY CONTROL DATA
Project: 202005
Pace Project No.: 92319638
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 2ao78
[phone]
QC Batch: 337939 Analysis Method: EPA 16648
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92319638001, 92319638002, 92319636003, 92319638004, 92319638005, 92319638006, 92319638007
METHOD BLANK: 1874159 Matrix: Water
Associated Lab Samples: 92319638001, 92319638002, 92319638003, 92319638004, 92319638005. 92319638006, 92319638007
Blank Reporting
Parameter Units Result Limit MDL Analyzed qualifiers
Olt and Grease mg/L ND 5.6 1.1 11/22/16 09:37
LABORATORY CONTROL SAMPLE: 1874160
Spike LCS LCS % Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 36.4 91 78-114
MATRIX SPIKE SAMPLE: 1874161
92319638003 Spike MS MS % Rec
Parameter Units Result Cone. Result % Rec Limits Qualifiers
Oil and Grease mg/L ND 40 36.5 91 78-114
Results presented on ttds page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shad not he reproduced, except In fuSl,
Date: 11122/2016 03:24 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

acmnafAcal
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QUALITY CONTROL DATA
Project: 202005
Pare Project No.: 92319638
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 337262
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92319638001, 92319638002,
92319638003, 92319638004, 92319638005, 92319638006, 92319638007
METHOD BLANK: 1870423
Matrix: Water
Associated Lab Samples: 92319638001,92319638002.92319638003,92319638004,92319638005,92319638006,92319638007
Blank Reporting
Parameter
Units
Result Limit MDL Analyzed Qualifiers
Total Suspended Solids
mglL
ND 2.5 2.5 11/16/16 20:06
LABORATORY CONTROL SAMPLE:
1870424
Spike . LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 236 94 90-110
SAMPLE DUPLICATE 1870425
92319635001 Dup Max
Parameter
Units
Result Result RPD RPD Qualifiers
Total Suspended Solids
m91L
24.3 23.3 4 5
SAMPLE DUPLICATE: 1870426
92319678001 Dup Max
Parameter
Units
Result Result RPD RPD Qualifiers
Total Suspended Solids
mglL
7.6 7.6 0 5
Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the right of the resuiL
REPORT OF LABORATORY ANALYSIS
This report shad not he reproduced, except in fug.
Date: 1112212016 03:24 PM without the written consent of Pare Analytical Services, LLC. Page 9 of 16

aceAnalyfical
rvwwpadelabs.cam
Project: 202005
Pace Project No.: 92319638
OC Batch: 337075
QC Batch Method: EPA 365.1
Associated Lab Samples: 92319638004, 92319638007
METHOD BLANK: 1869261
Associated Lab Samples: 92319638004. 92319638007
Parameter Units
Phosphorus mg1L
LABORATORY CONTROL SAMPLE: 1869262
Parameter Units
Phosphorus mg[L
Pace Analytical Services, LLC
980019nceyAve. Suite 100
Huntersville, NC 28078
(7D4)875-9092
QUALITY CONTROL DATA
Analysis Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed Qualifiers
ND 0.050 0.025 11/18/16 23:22
Spike LCS LCS % Rec
Conc. Result % Rec Limits • Qualifiers
2.5 2.5 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1869263 1869264
MS MSD
92319574001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Phosphorus mg/L 1.2 2.5 2.5 3.7 3.7 99 100 90-110 1 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1869265 1869266
MS MSD
92319749002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Phosphorus mg1L ND 2.5 2.5 2.5 2.5 100 100 90-110 0 10
Resutts presented on this page are In the units indicated by the "Units' column except where an alternate emit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/22/2016 03:24 PM without the written consent of Pace Analytical Services, LLC,
Page 10 of 16

ceAnalyfical
www.Pacews-coat
QUALITY CONTROL DATA
Project: 202005
Pace Project No.: 92319638
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunterswlle, NC 28078
[phone]
QC Batch: 337214 Analysis Methods SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92319638001, 92319638002, 92319638003, 92319638004, 92319638005, 92319638006, 92319638007
METHOD BLANK: 1870107 Matrix: Water
Associated Lab Samples: 92319638001, 92319638002, 92319638003, 92319638004, 92319638005, 92319638006, 92319638007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 12.5 11/16/16 22:05
LABORATORY CONTROL SAMPLE: 1870108
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand m91L 750 746 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1870109 1870110
MS MSD
92318889007 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg11- 669 750 750 1350 1350 91 91 90-110 0 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1870111 1870112
MS MSD
92319277004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Quat.
Chemical Oxygen Demand mg/L ND 750 750 748 751 100 100 90-110 0 3
Results presented on this page are in the units Indicated by the "Units" column except Mtere an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/22/2016 03:24 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

laneAnafyfical'
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QUALIFIERS
Project: 202005
Pace Project No.: 92319638
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting limit -
Pace Analytical Services, LLG
98001GnceyAve. SuKe 100
Nuntersville, NC 28o78 .
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each anatyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute,
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shag not be reproduced, except in cull,
Date: 1112212016 03:24 PM without the written consent of Paw Analytical Services, LLC. Page 12 of 16

aceAnalyhcal
www.paGeW&I mn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
202005
92319638
Analytical
Lab ED
Sample ID
GC Batch Method
QC Batch Analytical Method Batch
92319633001
301
EPA1664B
337939
92319638002
402
EPA1664B
337939
92319638003
907
EPA16648
337939
92319638004
506Ai
EPA1664B
337939
92319638005
506B1
EPA 1664 B
337939
92319638006
510
EPA1664B
337939
92319638007
803
EPA1664B
337939
92319638001
301
SM 2540D
337262
92319638002
402
SM 2540D
337262
92319638003
907
SM 2540D
337262
92319638004
506A1
SM 2540D
337262
92319638005
506B1
SM 2540D
337262
92319638006
510
SM 2540D
337262
92319638007
$03
SM 2540D
337262
92319638004
506A1
EPA 365.1
337075
92319638007
$03
EPA 365.1
337075
92319638001
301
SM 5220D
337214
92319638002
402
SM 5220D
337214
92319638003
907
SM 5220D
337214
92319638004
506A1
SM 5220D
337214
92319638005
506131
SM 5220D
337214
92319638006
510
SM 5220D
337214
92319638007
803
SM 5220D
337214
REPORT OF LABORATORY ANALYSIS
This report snail not be reproduced, except in full,
Date: 11/22/2016 03:24 PM without the written consent of Pace Analytical Services, LLC, Page 13 of 16

Sample Condition Upon Receipt{SOUR)
Page 1 of 2
Il/ c G`B/If1d�]/1`lCc7i
Document No.:
F-CAR-CS-033-Rev.01
Issuing Authority:
Pace Cluality Office
Laboratory receiving sa pies;
ASheville V Eden❑
Greenwood ❑ Huntersvilie ❑
Raleigh❑
Mechanicsville[]
' Client lVarrte: Project WOE : 92319638
.
ui �11r�_ Cll�iaaarli� __
Courier: Fed Fx ❑UPS ❑USPS ❑Client
❑ ComnierclaI ❑Pace ❑r. otheIII 11111111111111111111
92329638
Custody Seal Present? ❑Yes No Seals I ct? Dyes ❑Pio
Date/Initials person Examining Contents: 2rA?
T-17
Packing Material: ❑Bubbie Wrap Bubble Bags ❑None J ❑0ther.- /�
Thermometer: tit/
I1tGun ID: _ Type of Ice: Vet nulue ❑'lane ❑Samples on ice, cooling process has begin
Correction Factor. ter Temp Corrected ('C): �, Biological Tissue Frozen? ❑Yes ❑No ❑N/A
Temp should be above fr Ing tD 6'C A
USDA Regulated Soil ( NIA, vlater santpIa)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples angina Le from a foreign source (infernal natM1J
❑Yes QNo _ including Hawaii and Puerto Rico)? []Yes _tdo
Comm ents/Discrepancv: I
Chain of Custody Present? I e ❑N. ❑ai/A 1.
Samples Arrived within Hold Time? _ Ycs ❑Nd ❑N/A 2.
Short Hold Time Analysis 02 hr.)? ❑Yes Plo []N/A 3.
Rush Turn Around Time Requested? ❑Y o DO 4.
sufficient Volume? r / I—ia--., F-1mm s
Correct Containers Used?
-Pace Containers Used?
❑No
❑No
VVW
©,NVA
❑,V/A
6,
Containers intact?
Yes
©,
❑N/,t
_
?.
Samples Field Filtered?
❑Y s17
No
❑N/A
_8. Note If sucilment is visible in the dissolved container
9. f
{ Sample Labels Match COC? _ Yes ❑.io ❑Y/A
. _incluclesD3te/Tinie/1D/Ana sis Matrix: ifs/
Headspace In vdAVIals {>5-6mm)?
❑yes
❑No
N/
_ ---
Trip Blank Present?
Trip Blank Custody Seals Present?
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
[]Yes []No 9 f" i 11.
Date/Tinte:
Field Data Required? Dyes ❑Pio
Project Manager SCURF Review: Date: t r I S
'Y Pra}ect Manager SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will Ile sent w the Mort]; Carolina DBWIR Certlfic atfon Office (Le.
Out of hold, incorrect p(esenxstive, out of temp, incorrect containers)
Page 14 of 16

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AG1U-1 iimrAmbor Unpreserved (N/A) (CI•)
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AM-250 mLAmber Unpreserved jN/A) (CI-)
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Section A Section B Section C
Page. of a
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Mark Blake_, P.E.
Director of Enaineerinu and Maintenance
Mark Blare, P.E.
Director of Engineering and Maintenance
May 18, 2016
Division of Water Quality
Water Quality Section _ _
Attention Central Files REF%-'f-
1617 Mail Service Center
Raleigh, N.C. 27699-1617 h�AY 2 3 2g16
CENTRAL FILES
Subject: North Carolina State Ports Authority D%P!R SECTION
Spring 2016, Qualitative Storm Water Monitoring Results
Port of Wilmington Permit No NCS000174
Port of Morehead City, Permit No. NCS000173
Central Files:
In Keeping with the terms of storm water permit No. NCS000174 and Permit No.
NCS000173, enclosed are two copies of the Spring 2016, Qualitative monitoring results.
This should complete the subject facility's Spring 2016 storm water monitoring
requirements.
If any additional information is needed, please call me at [phone].
Sincerely,
NOI 1:I`H CAROLINA STATE PORT AUTHORITY
Todd C. Walton
Sr. Environmental Analyst
Cc: environmental files
North Carolina State Ports Authority - 2202 Burnett Boutevard • PO Box 9002 • Wilmington, NC 28402 • www.ncports.com

if
Mq y 2 ��fl
N17 i � 3 2416
R SFC �pNS
PAGE 1 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
PERMIT NO. NCS000173 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
FACILITY NAME: N.C. STATE PORTS AUTHORITY PORT OF MOREHEAD CITY COUNTY: CARTERET
PERSON COLLECTING SAMPLES: Corey Futral/Bill Miller - CATLIN PHONE NO. 910-452-5861
CERTIFIED LABORATORY: PACE ANALYTICAL SERVICES. INC. CERT. # 37706
PAS
NR — Not Required
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
and complete to the best of my knowledge.

PAGE 2 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ X yes no
(If yes, complete Part B) -
PART B: Vehicle Maintenance Activity Monitoring Requirements
Outfall No.
Date Sample
Collected
(Molddtyr)
Total Rainfall
(Inches)
Oil & Grease
(mglL)
Total
Suspended
Solids
(mg1L)
pH
jUnits)
New Motor
Oil Usage
(gallmo)
301
502016
1.51
<5.0
72.7
8.9
>55
402
5/3/2016
1.51
<5.0
21.1
8.9
>55
506A1
5/3/2016
1.51
<5.0
28.2
8.7
>55
506131
5/312016
1.51
<5-0
7.6
8.3
>55
510
51312016
1.51
<5.0
119
8.4
>55
803
5/312016
1.51
<5.0
15.5
8.4
>55
907
5/3/2016
1.51
<5.0
20.0
7.7
>55

I vy
PAGE 1 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
RECEIVED
140V 16 2015
CENTRAL FILES
DWI: SECTION
PERMIT NO. NCS000173 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
FACILITY NAME. N.C. STATE PORTS AUTHORITY PORT OF MOREHEAD CITY COUNTY:CAR
PERSON COLLECTING SAMPLES: Mike D. Mason/Corey Futral - CATLIN PHONE NO. 910-452- 861
CERTIFIED LABORATORY: PACE ANALYTICAL SERVICES, INC. GERT. # 37706
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report Is accurate
and complete to the best of my knowledge.
PART A: Specific Monitoring Requirements
Outfall No.
Date Sample
Collected
(Molddlyr)
Total
Rainfall
(Inches)
Chemical
Oxygen
Demand
(mg1L)
Total
Suspended
Solids
(mglL)
Total
Phosphorus
(mglL)
pH
(Units)
Oil &
Grease
(mglL)
301
9/24/2015
1.31
36.0
2.6
0.10
8.0
<5.0
402
9124/2015
1.31
55.0
6.0
0.24
7.4
<5.0
506A1
9/24/2015
1.31
<25.0
<5.0
0.47
8.3
1 <5.0
50681
9/24/2015
1.31
18.0 J
10.3
1.2
8.2
<5.0
510
9/24/2015
1.31
<25.0
4.4
0.37
8.6
<5.0
803
9/24/2015
1.31
<25.0
6.9
1.1
8.2
<5.0
807
9/24/2015
1.31
20.0 J
15.9
0.73
7.7
<5.01
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
C-.8Z
Li.I;T
..J
L.L.

PAGE 2 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
Farm SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X as no
(if yes, complete Part B)
PAKI b: venicie maintenance Activity monitoring KGgUirements
Outfall No.
Date Sample
Collected
(Molddlyr)
Total Rainfall
(Inches)
Oil & Grease
(mg/L)
Total
Suspended
Solids
(mg/L)
pH
(Units)Oil
New Motor
Usage
(gallmo)
301
9/24/2015
1.31
<5.0
2.6
8.0
>55
402
9/24/2015
1.31
<5.0
6.0
7.4
>55
506A1
9/24/2015
1.31
<5.0
<5.0
8.3
>55
5061211
9/24/2015
1.31
<5.0
10.3
8.2
>55
510
9/24/2015
1.31
<5.0
4.4
8.6
>55
803
9/24/2015
1.31
<5.0
6.9
8.2
>55
907
9/24/2015
1.31
<5.0
15.9
7.7
155

PAGE 3 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
STORM EVENT CHARACTERISTICS:
Date: 9124/2015
Total Event Precipitation (inches): 1.31
Event Duration (hours): 17
(if more than one storm event was sampled)
Date:
Total Event Precipitation (inches):
Event Duration (hours):
Mail original and one copy to:
Attn: Central Files
DENR
Division of Water Quality
1617 Mail Service Road
Raleigh, NC 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the Information submitted. Based on my Inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the Information, the information submitted Is, to the best of
my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations." (Signature of permittee)(Date)

W
0=1
�i
CMJ
PAGE 1 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES G7
Form SWU-246-112608 DIVISION OF WATER DUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
PERMIT NO. NCS000173 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
FACILITY NAME: N.C. STATE PORTS AUTHORITY PORT OF MOREHEAD CITY COUNTY: CARTERET
PERSON COLLECTING SAMPLES: Corey FutgpllBill Miller - CATL.IN PHONE NO. 910-452-5861
CERTIFIED LABORATORY: PACE ANALYTICAL SERVICES. INC. CERT. # 37706
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
and complete to the best of my knowledge.
Outfall No.
Date Sample
Collected
(Molddlyr)
Total
Rainfall
(Inches)
Chemical
Oxygen
Demand
(mg/L)
Total
Suspended
Solids
(mg1L)
Total
Phosphorus
(mg1L)
pH
(Units)
Oil &
Grease
(mglL]
301
5/11/2015
1.27
149
<2.5
NR
7.8
<5.0
402
5/11/2015
1.27
159
<5.0
NR
7.8
<5.0
506A1
5/11/2015
1.27
<25.0
<2.5
0.56
8.0
<5.0
506131
5/11/2015
1.27
76.0
2.6
NR
7.8
<5.0
510
5/11/2015
1.27
<25.0
6.1
NR
7.3
<5.0
803
5111/2015
1.27
609
13.5
2.0
6.5
2.2J
907
5111 /2015
1.27
185
24.0
NR
7.2
<5.0
NR - Not Required
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

PAGE 2 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Does this facility perform Vehicle Maintenance Activities using more than 66 gallons of new motor oil per month? X ves no
(If yes, complete Part B)
PART B: Vehicle Maintenance Activity Monitoring Requirements
Outfall No.
Date Sample
Collected
(Molddlyr)
Total Rainfall
(Inches)
Oil & Grease
(mg/L)
Total
Suspended
Solids
(mg/L)
pH
(Units)Oil
New Motor
Usage
(gal/mo)
301
5/11/2015
1.27
<5.0
<2.5
7.8
>55
402
5/11/2015
1.27
<5.0
<5.0
7.8
>55
606A1
5/11/2015
1.27
<5.0
<2.5
8.0
>55
506B1
5/11/2015
1.27
<5.0
2.6
7.8
>55
610
5/11/2015
1.27
<5.0
6.1
7.3
>55
803
5/11/2015
1.27
2.2J
13.5
6.5
>55
907
5/11/2015
j 1.27
j <5.0
j 24.0
7.2
j >55

PAGE 3 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
STORM EVENT CHARACTERISTICS:
Date: 5111 /2016
Total Event Precipitation (inches): 1.27
Event Duration (hours): 6
(if more than one storm event was sampled)
Date:
Total Event Precipitation (inches):
Event Duration (hours):
Mail original and one copy to:
Attn: Central Files
DENR
Division of Water Quality.
1617 Mail Service Road
Raleigh, NC 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision In accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the Information, the information submitted Is, to the best of
my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, Including
the possibility of fines and imprisonment for knowing violations." (Signature of permittee)(Date)

dr
C.MOLJNA
Mark Blake, P.E.
Director of Engineering and Maintenance
Mark Blake, P.E.
Director of Engineering and Maintenance
.tune 19, 2015
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh, N.C_ 27699-1617
RECEIVED
JUN 2 4 2015
CENTRAL FILES
DWR SECTION
Subject: North Carolina State Ports Authority
Spring 2015, Qualitative Storm water Monitoring Results
Port of Morehead City, Permit No. NCS000173
Central Files:
In keeping with the terms of storm water permit NCSOOO173, enclosed are two
copies of the Spring 2015 Qualitative monitoring results. This should complete the
subject facilities' Spring 2015 storm water monitoring requirements.
If any additional information is needed, please call me at [phone].
Sincerely,
NORTH CAROLINA STATE PORTS AUTHORITY
Todd C. Walton
Environmental Supervisor
Cc: enviro files
North Carorma Stale Parts Authadty • 2202 Bunw t Baulavard • PO Box 9002 - Wilmington, NC 2M2 • www.ncparmcam

NoIM
cARounw
poars ,
Marl: Blake, P.E.
Director of Engineering and Maintenance
Mark Blake, P.E.
Director of Engineering and Maintenance
April 22.2014
Central Files
Division of Water Quality
1617 Mail Service Center
Raleigh. N.C. 27699-1617
Subject: North Carolina State Ports Authority
Spring 2014. Qualitative Storm water Monitoring Results
Port of Morehead City, Permit No_ NCS000173
Central Files:
�"-Yyv
J�fo
RECEIVED
APR 2 4 2014
CENTRAL FILES
DWQ/B4G
;Po~
f�
Lid
LAm
In keeping with the terms of storm water permit NCS000173, enclosed are two
copies of the Spring 2014, Qualitative monitoring results. This should complete the
subject facilities' Spring 2014 storm water monitoring requirements.
If any additional information is needed. please call me at (9I 0) 251-5678.
Sincerely,
NORTH CAROLINA STATE PORTS AUTHORITY
'r 'e //-
Todd C_ Walton
Environmental Supervisor
Cc: enviro files
Forth Carolina State Ports Authority • 2202 Burnett Boulevard • PO Box 9002 • Wilmington, NC 28402 • www.ncparts.com

walton, .todd
From: Dimitri Talbert ([e-mail]
Sent: Monday, April 21, 2014 1:38 PM
To: walton, todd
Cc: Rick Garrett
Subject: Results form MHC Stormwater Monitoring
Attachments: CATLIN-NCSPA MHC-14-03528-3-25-14.pdf
Todd,
Please find attached the results from the latest Port of Morehead City (25MAR14) stormwater monitoring results.
Couple of things to note:
Oil & Grease sample for 301 was inadvertently destroyed (dropped) by the lab. Since we have not had a
historical precedent for O&G issues here, we feel that the lab report narrative and an explanation on the results
table for the missing data should suffice. Let us know otherwise.
COD results from Newport River (2,730 mg/L) and Bogue Sound (30,900 mg/L) were high and exceeded the
COD permit benchmark limit of 120 mg/L. These results support our theory that tidally influenced waters are
influencing site COD stormwater results. The samples were collected right off of the wharves, as far away as
possible from any nearby stormwater discharge points.
The COD for 907 (741 mg/L) exceeded the COD permit benchmark limit. This was the only sample that was
collected from waters that were tidally influenced. All others were collected at low tide (rising) conditions with
outgoing flow observed or from surface flows into the respective features. There was no other way to sample
this feature (manhole with 8-10 foot vertical drop to bottom of feature) without waiting for low tide and
continued rain, etc. We may want to explore other options for collecting representative samples from this
location.
Give me a call or email if you have any questions. Thanks.
Dimitri Talbert
CATLIN Engineers and Scientists
PO Box 10279
Wilmington, NC 28404-0279
910-452-5861 (office)
910-452-7563 (fax)
[e-mail]

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wiilmmgtrm, NC 28405
(910)392-= (Lab) • [phone] (Fax)
® 710 Bowsestown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING [phone]
CHEMISTS NICDENR: DWQ CM=CATE #94. DLS CER'MCATE 937729
Catlin Engineers & Scientists
Post Office Sax 10279
Wilmington NC 28404-0279
Attention: Dimitri Talbert
Lab ID Sample ID:
14-08601 Site:510
Test
Method
Date of Report:
Apr 17, 2014
Customer PO #:
140326-1
Report #:
2014-03528
Report to:
Dimitri Talbert
Project ID: NCSPA
MHC
Collect DatelTime Matrix
Sampled by
3/25/2014 12:05 PM Water
Dimitri Talbert
Results Date Analyzed
Oil & Grease (O&G) EPA 1664 <5 mg/L 04/03/2014
Residue Suspended (TSS) sup 2540 D 7.6 mg/L 03/28/2014
COD SM 52ME) < 20 rng/L 03/28/2014
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-08602 Site: 803 3/25/2014 11:10 AM Water Dimitri Talbert
Test Method Results Date Analyzed
Oil & Grease (O&G) EPA 16CA <5 mq/L 04/0212014
Residue Suspended (TSS) SM 2540 D 11.9 mq/L 03/28/2014
Total Phosphorus SM 45M P P 20.5 mg/L 04/15/2014
COD SeA52X0 42 mg/L 03/28/2014
Lab ID Sample ID: Collect DaterTime Matrix Sampled by
14-08603 Site: 907 3/25/2014 5:40 PM Water Dimitri Talbert
Test
Oil & Grease (O&G)
Residue Suspended (TSS)
COD
Lab ID Sample ID:
14-08604 Site: Newport River
Test
Method
EPA 1664
SM 2540 D
SM 5220D
Method
Results Date Analyzed
Collect Date/Time Matrix
3/25/2014 11:40 AM Water
<5 mg1L 0410212014
15.5 mg/L 03/2812014
741 mg/L 03/28/2014
Sampled by
Dimitri Talbert
Results Date Analyzed
COD SM 52200 2730 mg/L 03/28/2014
Report #:: 2014-03528 Page 2 of 3

CAROUNA
�oRrs
Mark Blake. P.E.
Director of Engineering and Maintenance
Mark Blake, P.E.
Director of Engineering and Maintenance
January 12, 2014
Central Files
Division of Water Quality
16I7 Mail Service Center
Raleigh, N.C. 27699-1617
Subject: na State Ports Authority
Fall!20litative Storm water Monitoring Results
rt oore
City, Permit No. NCS000173
Central Files:
go
JAN 14 2015
CENTRAL FILES
DWR SECTION
In keeping with the terms of storm water permit NCS000173, enclosed are two
copies of the Fall 2014, Qualitative monitoring results. This should complete the subject
facilities' Fall 2014 storm water monitoring requirements.
If any additional information is needed, please call me at [phone].
Sincerely,
NORTH CAROLINA STATE PORTS AUTHORITY
l' z/zg
/,'Z-
Todd C. Walton
Environmental Supervisor
Cc: enviro files
North Caronna State Ports Authority - 2202 Burnett Boulevard • PO Box 9002 • Wilmington. IBC 2802 • www.nr-parts.com

id
ceAnalJ/[Tcaf
www!p3MIa63c=
SAMPLE SUMMARY
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92231272001
301
Water
1212411411:50
12/3011410:45
97231272002
402
Water
12124114 12:00
1213011410:45
92231272003
506A1
Water
12/24114 11 :35
1213011410:45
92231772004
50681
Water
1212411411:20
1213011410:45
92231272005
510
Water
1212411410:50
1213011410:45
92231272006
603
Water
12124/1412:15
1213011410A5
92231272007
907
Water
1212411412:35
12/3011410:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19

ce fII cal •
wrre•�
ANALYTICAL RESULTS
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 301
Parameters
LabID: 92231272001 Collected:
Report
Results Units Limit
12124/14 11:50
MDL OF
Received: 12/30114 10:45 Matrix: VWater
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L 5.0
1.1 1
01/07115 07:20
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
8.5 mg1L 2.6
2.6 1
12J30114 15:00
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
282 mg1L 25.0
12.5 1
01/06/15 13:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/07/2015 02:22 PM without the written consent of Pace Analytical Services, Inc,. Page 5 of 19

Pace Analytical Services, Inc.
t!
��i �� 9800 Kincey Ave. Suite 100
1Jj/•�'/ Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: NCSPA MHC 202005
Pace Project No.: =31272
Sample: 402 Lab ID: 92231272002 Collected: 12/24114 12:00 Received: 12130/14 10:45 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease ND mg1L 5.0 1.1 1 01/07/15 07:20
25400 Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg1L 2.6 2.6 1 12I30/14 15:00
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 279 mg1L 25.0 12.5 1 01/06/15 13:15
REPORT OF LABORATORY ANALYSIS
This feport shall nct be reproduced, except in full,
Date: 01/07/2015 02:22 PM without the written consent of Pare Analytical Services, Inc.. Page 6 of 19

ANALYTICAL RESULTS
Project NCSPA MHC 202005
Pace Project No.: 92231272
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Sample: 506A1
Parameters
La61D: 92231272003 Collected:
Report
Results Units Limit
12124114 11:35
MDL DF
Received: 12/30/1410:45 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L 5.0
1.1
1
01/07/15 07:20
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
2.8 mg/L 2.6
2.6
1
12/30/14 15:00
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
0.072 mglL 0.050
0.025
1
01/05/1510:53 7723-14-0
5220D COD
Analytical Method: SM 52200
Chemical Oxygen Demand
273 mg/L 25.0
12.5
1
01/06/15 13:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Hate: 01/07/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 19

Pace Analytical Services, Inc.
eAm "a 5800 nceyAve. Suite 1111'�•7 Huntersvi3fe. NG 28078
078
+FCC+ [phone]
ANALYTICAL RESULTS
Project: NGSPA MHC 202005
Pace Project No.: 92231272
Sample. 50681 Lab ID: 92231272004 Collected: 12/24/14 11:20 Received: 1213GI14 10A5 Matrix: Water
Parameters
HEM, Oil and Grease
Oil and Grease
2540D Total Suspended Solids
Total Suspended Solids
52200 COO
Chemical Oxygen Demand
Date: 01/07/2015 02:22 PM
Report
Results Units Limit MDL DF Prepared Analyzed CAS No Qual
Analytical Method: EPA 1664B
ND mg/L 5.0 1.1 1 01/07/15 07:21
Analytical Method: SM 2540D
13.9 mgtL 2.6 2.6 1 12/30/14 15:01
Analytical Method: SM 5220D
54.0 mg1L 25.0 12.5 1 01/06/15 13:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fuEl,
without the written consent of Pare Analytical Services, Inc._
Page 8 of 19

Pace Analytical Services, tric.
��jJ)�/•+�j
i 1 _� • 9800 Kincey Ave. Suite 100
Huntersvifle, NC 28078
rh wmagebsc= [phone]
ANALYTICAL RESULTS
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Sample: 510 Lab ID: 92231272005 Collected: 12/24/14 10:500 Received: 12/30/14 10AS Matrix: Water
Report
Parameters Results Units limit MOL DF Prepared Analyzed CAS No. 4ual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg1L 5.0 1.1 1 01/07/15 07:21
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 60.2 mg1L 6.2 6.2 1 12/30/14 15:01
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 79-0 mgfL 25.0 12.5 1 01/06/15 13:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fun,
Date: 01/07/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 19

Pace Analytical Services, Inc.
s 9800 1Gncey Ave. Suite 100
un e a Hunteisville. NC 28078
Pamms cm (704)a75-9092
ANALYTICAL RESULTS
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Sample: 803 Lab 10: 92231272006 Collected: 12124114 12:15 Received: 12130114 10:45 Matrix: Water
Parameters
HEM, Oil and Grease
Oil and Grease
2540D Total Suspended Solids
Total Suspended Solids
365.1 Phosphorus, Total
Phosphorus
52201) COD
Chemical Oxygen Demand
Date: 01/0712015 02:22 PM
Report
Results Units Limit
MDL
DE
Prepared Analyzed CAS No. Qua[
Analytical Method: EPA 1664E
NO mg1L 5.0
1.1
1
01/07/15 07:22
Analytical Method: SM 2540D
5.6 mg1L 3.3
3.3
1
12/30/14 15:01
Analytical Method: EPA 365.1
1.2 mg/L 0.050
0.025
1
01/05/15 10:55 7723-14-0
Analytical Method: SM 5220D
183 mg1L 25.0
12.5
1
01106/ 15 13:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in tutl,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 19

Cr{+/"1O"ca •
ww�rpanrlab&COM
ANALYTICAL RESULTS
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 907
Lab ID: 92231272007 Collected:
12/24/14 12:35
Received: 12/30/14 10:45 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Oual
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
ND mg/L 5.0
1.1 1
01/07/15 07:22
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
8.3 mglL 3.6
3.6 1
12/30/14 15:01
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
338 mg1L 25.0
12.5 1
01/06/15 13:15
Date: 01/07/2015 02:22 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in M,
without the written consent of Pace Analytical Services, Inc..
Page 11 of 19

ceAWr,af
QUALITY CONTROL DATA
Project: NCSPA MHC 202005
Pace Project No_: 92231272
Pace Analytical Services, Inc.
9600 Kincey Ave- Suite 100
Huntersvitle, NC 28078
[phone]
OC Batch: GCSV/19987 Analysis Method: EPA 1664B
OC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92231272001, 92231272002, 92231272003, 92231272004, 92231272005, 92231272006, 92231272007
METHOD BLANK: 1364598 Matrix: Water
Associated Lab Samples: 92231272001, 92231272002, 92231272003, 92231272004, 92231272005, 92231272006. 92231272007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg1L
N❑ 5.0 01/07115 07:18
LABORATORY CONTROL SAMPLE & LCSD: 1364599 1364600
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers
Oil and Grease mg1L 40 38.1 36.9 95 92 7&114 3 30
Results preserttad an this page are in the units tndicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shah not be reproduced, except in full,
Date: 01/07/2015 02:22 PM without the written consent of Pace Analytical Services, Inc._
Page 12 of 19

ceArtalytical
QUALITY CONTROL DATA
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: WET/35023 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Anaysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92231272001, 92231272002. 92231272003, 92231272004, 92231272005, 92231272006, 92231272007
METHOD BLANK: 1361442 Matrix: Water
Associated Lab Samples: 92231272001, 92231272002, 92231272003, 92231272004. 92231272005, 92231272006, 92231272007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 12/30/14 14:58
LABORATORY CONTROL SAMPLE: 1361443
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 246 98 90-110
SAMPLE DUPLICATE: 1361444
92231226001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 348 208 50 10 D6
SAMPLE DUPLICATE: 1361445
Parameter
Total Suspended Solids
92231228001 Dup
Units Result Result
mg/L ND ND
Max
RPD RPD Qualifiers
10
Resu is presented an this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull.
Date: 0110712015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 19

ceAnaytica�.
Project NCSPA MHC 202005
Pace Project No.: 92231272
OC Hatch: WETAr21477
DC Batch Method: EPA 365.1
Associated Lad Samples: 92231272003, 92231272006
METHOD BLANK: 1363113
Associated Lad Samples: 92231272003, 92231272006
Parameter Units
Phosphorus mggL
QUALITY CONTROL DATA
Analysis Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.050 01IM1510:46
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1363114
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phosphorus mg/L 2.5 2.6 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1363115 1363116
MS MSD
92231352001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Phosphorus mg/L 0.26 2.5 2.5 2.8 2.8 100 101 90-110 1 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1363117 1363118
MS MSD
92231353004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RPD RPD Qua]
Phosphorus mg/L 280 2.5 2.5 285 281 179 46 W110 1 10 M6
Results presented on Ws page are in the unite incracated by the -Un ts' calumm except whom an alternate unit Is presented to Me right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 01/07/2015 02:22 PM without the written consent of Pace Ana"cal Services, Inc..
Page 14 of 19

eARWcal
QUALITY CONTROL DATA
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Pace Analytical Services, Inc.
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: WETA121491 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92231272001, 92231272002, 92231272003, 92231272004, 92231272005, 92231272006. 92231272007
METHOD BLANK: 1363608 Matrix: Water
Associated Lab Samples: 92231272001, 92231272002, 92231272003, 92231272004. 92231272005, 92231272006, 92231272007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand m9fL ND 25.0 01/06/15 13:15
LABORATORY CONTROL SAMPLE: 1363609
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 774 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1363610 1363611
MS MSD
92231264001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L 34.0 750 750 729 735 93 93 90-110 1 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1363612 1363613
MS MSD
92231272007 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % ReC Limits RPD RPD Qual
Chemical Oxygen Demand mg/L 338 750 750 1050 1060 97 96 90-110 1 3
Remits presented on this page are In the units Indicated by the'tlnita' column except n3eere an alternate emit is presersted to the right or the mull
REPORT OF LABORATORY ANALYSIS
This report shag not be reproduced, except in U.
Date: 01107l2015 02:22 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 19

ce p.
QUALIFIERS
Project: NCSPA MHC 202005
Pace Project No.: 92231272
DEFINITIONS
Pace Analytical Services, Inc_
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL - Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Repotting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
OUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE 13UALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 01/07/2015 02:22 PM without the written consent or Pace Analytical Services, Inc.. Page 16 of 19

[aG A ca
+nun-�s.00u�
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NCSPA MHC 202005
Pace Project No.: 92231272
Pace Analyticat Services, Inc.
9800 Kincey Ave. Suite 100
Huntersv8le, NC 28078
[phone]
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92231272001
301
EPA 1664B
GCSV119987
92231272002
402
EPA 16646
GCSV119987
97231272003
506A1
EPA 1664E
GCSV119987
92231272004
50681
EPA 1664B
GCSV119987
92231272005
510
EPA 1664E
GCSV119987
92231272006
803
EPA 1664B
GCSV119987
92231272007
907
EPA 1664B
GCSV/19987
92231272001
301
SM 2540D
WET135023
92231272002
402
SM 2540D
WET135023
92231272003
506A1
SM 2540D
WET135023
92231272004
506B1
SM 2540D
WET135023
92231272005
510
SM 2540D
WET135023
92231272006
803
SM 2540D
WET135023
92231272007
907
SM 2540D
WET135023
92231272003
506Ai
EPA 365.1
WETA121477
92231272006
803
EPA 365.1
WETA121477
92231272001
301
SM 5220D
WETA/21491
92231272002
402
SM 5220D
WETA/21491
92231272003
50SA1
SM 5220D
WETA 121491
92231272004
SOGB7
SM 5220D
WETN21491
92231272005
510
SM 52201)
WETA121491
92231272006
803
SM 5220D
WETA121491
92231272007
907
SM 5220D
WETA121491
Date: 01/07/2015 0222 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent at Pace Analytical Services, Inc..
Analytical
Batch
Page 17 of 19

FuocumeF-ASV-CS-003-my.14
nt lvame'Sample Condition Upon
CeAnalytical > SCURDocument No.:
Client Name: CIP
ant Revised: June 10, 2014
Page 1 of 2-
Issuing Authorities:
Asheville Qualitv Office
Courier (Circle). Fed E x•• UPS USPS Cfrent-
Commercial Pace Other
Custody Seal on Cooler/Box Present: ❑
yes EY�'no
Intact [] yes E] no
__,�Seals
Other
Packinj Material: ❑ Bubble Wrap Bubble Sags E3No;�et
..Thermometer Used: •1R Gun#*-130265963 Type of Ice: 1Blue None 0• Samples on Ice, cooling process has begtm
IR Gin f14 SNA44290366 -= Other:
;
Tt'mp'CoV6dI-- Factor: Add I Subtract
Cl C ? C
Corrected tooter Temp.; �.<- o
C Biological
Date and Initials of person ex Ira
Tissue Is Frozen: Yes No wA t� g
contents:
Temp should be above freezing to WC
i
Comments:
Chain of Custody Present:
Cl' -13N.
❑WA
1.
Chain of Custody Filled Out:
Glyn Efl,o
❑wA
2.
Chain of Custody Relinquished:
1734. _gRo
❑wA
3.
Sampler Name & Si nature on COC:
134' ❑No
❑wA
4.
Samples Arrived within Hold Time:
QYes Ono, QmA
6.
Short Hold Time Analysis (<72hr):
❑Yes No
. ❑wA
6.
Rush Turn Around Time Requested:
❑Ya.. $
❑NIA
7.
Sufficient Volume:
C3eir❑No
❑wA
8.
Correct Containers Used:
OYWONo
❑wA
9.
-Pace Containers Used:
E3Ya- ❑No
DNA
Containers Intact
Yes ❑tee
❑NA
6.
Filtered volume received for Dissolved tests
❑Yeses❑Na
❑
11.
Sample Labels match COC:
126es ❑No
❑WA
12.
-Includes datelEimeAD/Analvsis Matrbc__
_:if
All containers nee=9 presemuon nave been criecrreo.
cfYes ❑Na
❑WIA
13.
All coltla'uters needing preservation are found to be in
❑Ws ❑tta
[1tuA
compliance With EPA recommendation.
Y-
oxeeplions: VO& colitmm, T ;? G,�woRo hater)
❑l ei ❑No
Sam pies checked for dech if atlon:
©Yea on.
❑N%
14.
Headspace In VOA Nuts ( >6mm):
Oyes ONO
©Nrl�--
Trtu Blank Present: 1]Yca ❑No ON1A 118,
Pace Trip Blank Lot ft (if purchased):
Client NotiiIcationl Resolution:
Person Contacted: Dateirime:
Comments/ Resolution:
SCURF Review: ' Date: I a-f
SRF Review: Dater 3
Note: Whenever there Is a discrepancy affecting North Carolina
compilance samples, a copy of this form will be sent to the North
Carolina DEi-INR Certification Office (Le out of hold, incorrect
preservative, out of temp, incorrect containers)
Field Data Required? Y I N
two # 'ti92231272
MT1272... r ,
Page 18 of 19

4
i1
' CHAIN -OF -CUSTODY If Analytical Request [S'oc' "'enf
/ The Chaln.li is n LEGAL DOCUMENT. AJI relevant Holds mot bo complctcd all
c urataly.
• aceArralytiralw
Section A Section B section C
`r
1
Page.
Ral Cli Inarmal ROQYIrod Projad IntomUtiat: Invoice Irt:wrnatlea:
18 3? 2 8 1
Cwnpanlr 1
Report To,
AttantlOn;
AftM. v r
Copy TO: _
CwnRv7 Nana: ^ L� N
�'1
RE
UI.ATORY AGENCY
Addmm:
i'-
NPOP.9 i- GROUNDWATER i DRINKING WATER
V$T ,`- • RCRA OiMER
Emrrl Ttx
Pwcrrasu Order I ,..y
Aaw Qum
4
RKatnoa:
PIC4= Nerne:
Paea pe}a
SitLocation
•
STAiI?:
RQgtieit�d ikr. A
ProleQ
Pees w
�
Requested
AIRS
ysls
Fidel
(YIN)
Si O I Codas
RequlndCida hillirArerY r cone
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9
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COLLECTED
Aresarvafivos
z
i
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Driwn Waku DW
%VWW WT
• - Will Water vYW
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SAMPLE ID 04 M
phi
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Samge iDi MUST BE UwOl1E TiLiw is
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DATE
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ADDITIONAL CDMM&NTS
RELINQUISHED BY I AFFILIATION
DATE
ri
ACCEPTED iAFSILIATtON
DATE
TIME SAMPLECONDR7ONS
J r
r
r
SAMPLER NAME AND SIGNATURE
v
B.
a
K
.. ..::. to •....
S
2
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PRINT Home of SAMll
t ~!
WONA"i d SAMPLER' //Gw DATE"MillRt
'9 a
'ars>sr ne "I&I- ar •. i 1•n 1 vn M� ue -=1V 19 F]C� : NE, ;d C.e ;.^.rrn.wy •rinr : c w"w, to 4Y mrgM .a : Ss yr I`YrS rar a� uh7ips� esyl pa .lwi J6 dm I � � F•:y�y7.0IU[QV,i7:. � a•r�wy[u�
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PAGE 3 OF 3 NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
Form SWU-246-112608 DIVISION OF WATER QUALITY
STORMWATER DISCHARGE OUTFALL. (SDO)
MONITORING REPORT
STORM EVENT CHARACTERISTICS:
Date: 5/3/2016
Total Event Precipitation (inches): 1.51
Event Duration (hours): 6
(if more than one storm event was sampled)
Date:
Total Event Precipitation (inches):
Event Duration (hours):
Mail original and one copy to:
Attn: Central Files
NCDEQ
Division of Water Quality
1617 Mail Service Road
Raleigh, NC 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of
my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including
the possibility of fines and imprisonment for knowing violations." (Signature of permittee)(Date)