NCS000037_Compliance_20101202

'SCW
T C
SCR Catalyst Management & Regeneration Services
December 2, 2010
Mr. David Caldwell
Water Quality Supervisor
Charlotte -Mecklenburg Storm Water Services
700 North Tryon Street
Charlotte, NC 28202
Subject: Spill Response Report
Noveiirboi 17, 2010 Spill
NRC Report #960103
Dear Mr. Caldwell:
4n November 29, 2010 Mr. Andrew Martin conducted a compliance inspection of the spill site.
He was satisfied with the remediation and only requested the manifests of the clean up material.
shipped to the CMS landfill for disposal. Those four manifests (non-RCRA materials) were sent
to him by e-mail at 10:23 a.m. today.
Upon discovery of the spill at 4:50 a.m. on November 17, 2010 all loading activities were
immediately discontinued. Absorbent pigs and pads were immediately put into the stormwater
ditch to prevent any further spread of the spill. Monarch was contracted to supply a vacuum
truck to remove all the contaminated liquids from the ditch and had removed approximately 1200
gallons of liquid from the ditch (the spill volume was calculated to be approximately 1100
gallons) by 1:300 p.m. on November 17, 2010-the same day. This material was held on site until
analysis was completed and the material was deterniined not to be characteristic hazardous for
Arsenic (the primary metal contaminant). The material was shipped of for final treatment at the
Clariant facility on Mt. Holly road
The National Spill Response Center was contacted, CMUD was contacted, NCDENR was
contacted, Charlotte -Mecklenburg Storm 'Seater Services was contacted, and the Norfolk
Southern Railroad was contacted. Mr. Andrew Martin from your group and Bill Ointert from
CMUD both conducted a site inspection after the contact.
An initial determination was made to remove the top 3"-5" of soil from all the impacted areas to
minimize potential impact. The effort was completed by 5:00 p.m. Friday November 19, 2010.
The impacted soil (approximately 40 tons) was held on site in four 30 yard roll off containers
until analysis was completed. Samples of the impacted area prior to remediation and after the
soil remediation were picked up by Pace analytical services for analysis. All sample results were
finally received the following Wednesday, November 23, 2010.

Steven Ball of the EPA, Gilbert Turner from the Norfolk Southern Railroad, and Andrew :Martin
of Charlotte-Mecklinburg Storm Water Services were kept informed of our clean up progress
either by phone conversation or messages left on the phone (due to the Holiday).
The initial samples of the contaminated soil had Arsenic levels significantly less than 5mg/kg
and were used to profile the soils into the CMS landfill for disposal.
The soil samples taken at 10 foot intervals and composited by groups of 10 came back ,non
detect for Arsenic except for one result which was 0.65 mg,/kg (see attachments).
An investigation was launched to determine the root cause of the spill and identify deficiencies
in the procedures.
We believe the Driver failed to adequately observe and manage the loading operation and the
Operator did not adequately supervise the Driver. Because the existing loading hoses did not
reach the containment area, the Driver and Operator chose to load the tanker outside of
containment. These actIons resulted in a spill from the tanker which flowed to the ditch because
it occurred outside of the loading containment. The Operator received corrective action and will
be re-trained, particularly on the loading procedures. In additon, a checklist was developed
which includes specific pre -loading and post -loading instructions for both the Driver and the
Operator (see attachments).
A new Procedure and checklist have been developed which include additional preventative
actions such as; Tankers will now only be loaded in a containment area designed for truck
loading ( additonal hoses have been purchased to reach a tanker to be loaded with waste water in
the containment area). The Driver will be temporarily issued a radio for communications. An
operator will be assigned to stay with the load during loading at all times. The Driver will be
trained on `Driver responsibilities` prior to loading every tanker. A pre -loading and posting
loading inspection will be conducted for each load. A manual shut-off valve will be attached to
the end of the hose when ever loading is done through the top dome.
Planned preventative measures include putting a roof over the containmet area and `hard piping`
the loading line to the tanker and the line from the top of the tanker to a valve and camlock
connection at the rear bumper of the tanker.

The pictures attached to this document show the before and after condition of the remediation
efforts. They also clearly show the careful efforts made to maintain the smooth flow of the
drainage ditch and the minimize impact to the area along side the ditch.
We have made every effort to promptly remediate the spill area and have been done our best to
communicate and share our progress.
Let us know if there is anything else we need to do to be in compliance.
Sincerely,
Brad Cummock
Manager of Projects and EHS
C.'oaLogix
Cc: Andrew Martin, CMSWS
Lon Snider, NCDENR
Gilber Turner, Norfolk Southern Railroad

10riainated bv: IBrad Cummock I
Type of incident:
spill, injury, etc.)
Non Regulated Waste
Water -Spill
Date of incident:
11/17/2010
Time of incident:
4:50 a.m_
Location of incident:
Tanker Loading area
lBrief description of incident
At 4:50 a.m. while loading the 5th and final truck with pre-treated waste water to haul to another waste water
treatment fac1lity for additional treatment, the driver (Alfred ,Johnson from Monarch Trucking) ohserved spillage on
the ground next to the loading area. The driver inforrned Justin Toumberlin, the Shift Supervisor, who further
investigated the spill and discovered the spill had gone into the storm water drainage ditch next to the railroad
tracks on the south side of the building. Absorbent socks and pads were immediately put in the ditch to stop any
further spread of the spill. Managment was notified at 5:00 a.m., who then contacted CMUD, Mecklenburg Water
Quality Division, the National Spill Response Center (Report #960103), NCDENR, and the Norfork Southern
Railroad. The immediate containment prevented the spill reaching the local creek and which facilitated a quicker
clean up and remediation. By 1:30 pm that same day all the liquids were removed from the ditch (1200 gallons). A
mini excavator and a back hoe were brought on site the next day to scrape and remove the top three to five inches
of soil where ever the spill had contacted the ground. The soil removal was completed by around 5:00 p.m. Friday
I I/19110. All soil was put Into 30 yard roil orr boxes and Iield on site until airalytical results could be obtained ror
the contaminated soil. Approximately 40 tons of soil were removed and later disposed in a subtitle C landfill under
an approved profile specifically for this material once the analytical results were obtained (see attachment).
Cause
Approximately 1,100 gallons were spilled by apparent overfilling of the tanker by the Driver Alfred Parks. The j
truck was staged outside of containment and the the driver was not paying close enough attention to the loading
operation. Furthermore, the material was being loaded through the top hatch by a hose secured in place by the
driver. The operator did not adequately supervise the driver and allowed infrequent monitoring of the loading
process which resulted in a spill. The driver did not seethe spill or just failed to report the spill until the after' the
next truck was loading. Once truck driver reported the spill, the Supervisor immediately assessed the situation, put
containment in place, and notified management. Containment and clean up action began immediately (around
5:15 am).
In the case of a spill
pH: 7-7.3
Volume Released: 1100 gallons
*estimates
Contaminant Approx. cone. (ppm)
Arsenic (As)
1.079
Molybdenum (Me)
0.098
Vanadium (V)
0.589
Tungsten W
0
Absorbent Use (including socks and pads
Disposal
Type Amount Used: Location:
socks 10-3 ft units Iroll off box
pads 10 pads I roll off box

Corrective actions taken
All liquids were picked up, analyzed, and properly sent for final treatment and disposal. All areas where the spill
occurred were remediated by removing 3%5" of soil down from the surface. The cleaned up liquid and the soil
were tested for Arsenic . The results for the solids were below TCLP limits for Arsenic, and the liquid was well
below the RQ limits for Arsenic. T-ie materials were properly profiled for disposal afid shipped offsite to the
approved disposal sites. Samples were then taken of the soil at the cleaned up site and analysis completed.
Seven of the eight samples had analytical results below the detection limits for EPA method 6010, with the one
remaining sample results of 0.65 mg/kg(see attachment).
Preventative actions for future
The fallowing changes have been made: All bulk loading/unloading operations must be conducted in containment.
An operator must be in attendance and observing the operation with the driver the whole time loading/unloading is
occurring. A pre-loading/unloading and post loading/unloading inspection must be conducted and signed by both
the operator and driver. A manual shut off valve must be attached to the hose whenever loading is through the top
dome and not directly connected to a 'hard piped' loading line connected to the tanker All operators will he trainod
on the now SOP and Chocklist (soo attachmont). In addition, an enclosure is being planned to go over tho lording
containment area, along with a hard piped loading system for the waste water .
Follow-up Results
Date: 11 /23/2010
The sample results for the soils came back non RCRA, so the soil could be sent to a subtitle C landfill. Obtained a
profile for disposal at the C:MS landfill. l he sample results from the samples of the 'cleaned up area' indicated the
Arsenic levels were 'non detect' in all but one sample. However, the one sample was below significantly below
regulatory limits for Arsenic.
EHS manager: Date: Z& a,
Plant Manager: Date: ja -a j 6

NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST
S;r�i't19EE'S,1AIC.
if waster €s dstseStds waste,curnpleta:5ectlurts 1,11, 11l and IV
if waste is NOt asbestos was#e cdmplate Sections 1,11'and ill
!, GENERA -OR ,(enerat r completes 1a-r.} 3#j {
a. Generators US EPA ID Nurriker 6, Manifest Dbetiment Number
c Page 4 of
d, Generator''s'filameand LaraUon:
d
e Oeneratdes Melling Addre,ss-
io
r
f. Phones.z
!3 Phone
If owner,dithe generaffing fedtt .drffers: orn the generator, provit#e
h,.O ners,Name'
I. € oRr's Phona.,Ro.:
j, Waste Profile #
"k. Exp; ,Date
h Waste Shipping Name and
m. a detainers
n. Total
0, Unit
No.'
I Type
Description
quant
i yoi
i Y L
GENERATOR,'S GERT€FICATION` I hereby certify'that the above named material is not a hazardous waste as defineds16y-40 CM,261 or any applicable
state,law, has been properly described, classified and packaged, and is in proper condiflon-tor transportation according to applicable regulations; AND, if this
waste is a Ireatment'rgsidue of a:pri vioiisly rest icte i hazardous waste subject to the Land Disposal Restrictions, "I certify -and warrant That the waste has
been treated in accordance with the requirements of`40 CFR.268 and is no longer a hazardous waste as defined by A 0 CFi2 261.
p:.Gertsrator>Ai?thoHzeii`A eni M13arrie Print). 'I
q, Signature
r. faate
it completes lle=e
f f ,
T � 9
e: Date
te.`complates 111d=g}
Discrepancy lei€cation Space:
A; r
ow0 e .
Xf
,,,.' d
Date
.te<IVg-i)
a. Operator's Name.aiid Address;
Responsible Agency Name and Address.
T��'Phone!
b.: Phone.
B. Special Handling Insttuctians and A3ditional inforTnation:
f. El Friable ❑ Nan -Friable 0 Both % Friable % Non -Friable
OPERATOR'S CERTIPICATiON: € hereby declare that the contents of this consignment are fully and accurately described above by proper shipping name
and are classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable international and
national governmental regulations,
O erator's Name and Tille Print h Signature i. Date
'Operalur refers to the company which owns, leases, operates, controls, or supervises f66 aor Bing ernolishe�a or renovated, cis the demolltion or
renovation operation or both
REV 10/01 GENERATOR RETAIL RS-I'll

DL ff C NON -HAZARDOUS SPECIAL WASTE & ASBESTOS MANIFEST
SERVICES' INC �
If waste Is asbestos waste, complete Sections 1, II, 111 and IV_ > '
If waste Is NOT asbestos waste, complete Secflons 1, 11 and III
4 I
t
1. GENERATOR (Generator comnlefes la-r)
a Genomtor's US EPA ID Numbor
b Manifest Document Number
n ragn 1 of
d. Generator's Name and t_ocatiom
e. Generator's Mailing Address:
f Phons: ,.44
g, Phone:
If owner of the gerierating facility differs from the generator, provider
h. Owner's Nams
i., Owners Phone No,
1. Waste•Profile #
k, Exp. Date
1, Waste Shipping Name and
m. Gontaiheis
m Total
o Unit
No,
Type
Description
Quantity
WtA/ol
39
�3
GENERATOR'S. CERTIFICA T ION: I hereby certify that the above named material is not a hazardous waste as defined by 40 GFR 261 or any applicable
state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this
waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has
been treated ih accordance with the requirements of 40 CFR 268 a0d=Js no longer a hazardous waste as defined by 40 CFR 261.
p, Gen6ratorwAuthorized A eni Name. Print
q. Si hafure
r. Date
a. dperato4s name and Address:
b. Phone,
c, Aesponsibie Agency Name and Address:
(i Phone:
e. Special Handling Instructions and Additional Information:
f. ❑ Friable © Non -Friable El Both °!o Friable % Non -Friable
OPERATOR'S CERTIFICATION: 1 hereby declare,that the contents of this consignment are fully and accurately described above by proper shipping name
and "are classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable intemafi4nal and
national governmental regulations.
Operator's Name and Title Print
h. Signature
1, Date
"Operator refers to the aornpany which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or he derrtciirtion or
renovation operation or both
REV 10101 GENERATOR RETAIN R81.F11

AYl. SIC NON-HAZARDOLIS SPECIAL. WASTE & ASBESTOS MANIFEST
SC�S; tflr�.
D55If waste is asbestos waste, complete Sections t, It, III and IV 55,23
if waste is NOT asbestos waste, complete Sections I, 11 and [it �
t. G NFRATOR (generator win pletos la-r)
0. Ganordtor's US ZPA ID Numbor
b, Manifest Docum®rit Number
C. Page. 1 of
d. Generator's Namee and Location;
a, Generator's Mailing Address
�.:
r z
4211
f. Phone;
g. Phon
If'owner of fhe:generaw fkflity'differs from the generator, provide:
b.,Qwner'sName:
1, Owners Phone. No-,
j. Waste Profile #
k. Exp Date
1 Waste Shipping
Name and
m, Container`s
n. Total
o, Unit
No.
Typ e
D.escn tion
Quanta
WtNo1
AIt
fr
GENFR%\`TOR'S C1=RTIFIGA i ION- (hereby oertifythat the above �nah ed material 1's not a hazardous waste as defiftad by 41T GFR 261 or anyapplicable
state law, has been properly described, classified and packaged, and is in proper condition for transportation -according to appkable•regulatrons;,AND, if this
waste is a treatment residue of a previously restricted hazardous waste subtedt to the Land Disposal Restrictions, heertifj!•arid warrant €hatthe waste has
been treated in accordance with be requirements of 4D GFR 266 and" is nb to ger a`hazardous.waste:ag,:defined b 4t1 GFl2 261,
GenerataFftuthorized Agent:Name,. Prlt
Sf` nature' r. Date
41
b, Phowa- ° _
d. Phone:
e. 5pecialrRandling instructions ir6d AdditiQbal Information;
f. El Friable ❑ Non4:nable ❑ Both % Friable % Non -Friable
OPERATOR'S CERMFICATiON: I hereby declare that the contents of thib consignment are fully and accurately described above by propel shipping name
and are classified, packed, marked and labeled and are in all respects in proper condition for transport by highway according to applicable' international and
national governmental regulations,
U i�rator s_Name and Iigq (Nntrt}
1, Sr nature
t. Date
`Operator refers to the company which owns, leases, operates, controls, or supervises the facility being demolished or renovated, or the demolition or
renovation operation or both
REV 1Q'01
GENERATOR RETAIN R,;-F1f

DEC-01-2010 10 = 22 Ali ALLIED WASTE INC, 803 547 3197 P, 1
is tff waste `lss NO'r asbes��va�stme, co'rrrpe5e aS antis I, � n I �.
i d::��,i�S?�if387-tt?.'ort�ar•dinrr'yiPri!'SiAf�S�9.i'�' � ��, ••-. O•if
a.GeivratprSUS EPA M N=t*r
b: Manifest D ctiment bar '
o. Page I of
d, Generators.Name aril.Location: :sa," T F$
s. t3enalaiars Addr
_ Ij7f d
fa'Phow.
if over of the gm!r8 irsg'fad* dif€em from ft.Senerator, Provide: ,
h, osa rases Name.
1.Ownees Phona'No,;
J. Wsate
,[late
i. Wasta.5hippkrg Nama and
m. Contalnarn
n. Total
e. unit
Desscri "on
No.
Ginan,
WUVot
Sag tA3tttram*4 with
%004681
' l?
l t�r
-
J L.
it'--17i. }f
GENERATOR'S FICATION: I hereby certifY tigtthe above named nraiedal Is, rot a hazardsitrs waste de dsfined by 40- CFR 261 or any >ppiicab e .
state laws, has been property desoibod, classified and pedcaged, and Is In proper cordtion for transpdrWen accwift to app*;aWe n;gula tors, AND, If this,
waste is a treatment residue of a previously restr(Otsd hazardous waste su*ct to the Land Disposal Restrictfons. I certtfy and warrant that: the waste has
bash, in acewdance with.the uirsm of 40 OFR 288 and is no Igngera hazardous waste as deftnsd t5y40 CFR 261.
:f OafatAtrftxiti7sd Agent Nam' cti
..S riattrra ••
ra Date
H.' -TRANSPORTER Generator rxrm etes lis-b and Traits' rter comate-s.lic-e
.a,'f'ranaporter's[dameBndAddtess; _ � .
'.• .. r: ft Or so
1 c Dryer tdarrre d. e. Data
z tit, DEsnNAW"(Gerreratol: complete N1a-D and Destiny#on S6 tofrtpWo Illd-g)
I Facility and Site Address: c US EPA Numthar. A. DiscrePancy Indication 4ace;
\6105 MftIhnarl Rd t� t
,i,t'rt4=ilrCi, I�Ci cBfQPT
9
t
.a. "-...•,.. r.- � ax �nf ,Nary ww.enea.rn
Ittei`eb Tn im lresb ns«xsp a t
e, Nears of Aiifti need a9 5l rirttarra tiara
w: • ASBESTOS (tier ratter completes lwt dnc# typep .. ' nfpjate I` Ug ij �
a t3peratoc's Natnd arxi Address
,, ponsitle,Ager* Name and Address:
b. Phone:'
d. Phony
a. Special Handling Instrutallo ns and Additional IntbunStion:
f.0. Friabfa' 0"Nrsn Frbls .0 Scrdt % Non»Fciabla
•OpERATt3jr$' t ERi'IFICATIt7bis t hereby declare brat the contents of thia consignment are fully and •a=rat.* deaodbed above by proper $*ping name'
and ors classified, pscttsd, marked and Iahelsd arid are in all.rsspects in proper oondIfian for transport by highway according to applJoabls International and
national vernmethtai ikxls. •
is Narie and "l : •• ... i?•...!firiitfzire�.4 .. .,,..,, W ,..._... i• M
,operator ra ors' ttw t*Mpsnv Isase"w.operates, crsntrois, or sup> ryiGt+u Etta lac fl y bettX} derreoiiehed or nrsovafsd, ur the de€su3ittian ar
.renovation ouerarson cr:both . '_—
REV itiJ44 TMN8P0RtER• RETAIN i?S F1

Table 1- ICP Samples (liquid)
Testing by CoaLogix on in house ICP
Description
ICP As
ppm
Trench start near road - before cleanup
0.0
Trench near spill location - before cleanup
1.2
Trench at inlet of 1st culvert - before cleanup
0.7
Trench at outlet of 1st culvert - before cleanup
1.0
Trench at "dam" between culverts - before cleanup
2.5
Trench at outlet of 2nd culvert - before cleanup
0.0
Small stream off beyond 2nd culvert - before cleanup
0.0
Vac Truck - after liquid cleanup
1.1
Table 2 - TCLP Samples fSolids)
Prep by EPA method 3010, Analytical by EPA method 6010
(<5mg/L As for non -hazardous discharge)
Sample #
Description
TCLP As
_
-
mg/L (ppm)
S10-0872
Trench surface after 1-1" scrape
ND
510-0813
Trench surface before Scrape @ pohil. of spill
0.13
510-0874
Trench surface near point of spill (near point of spill)
ND
S10-0875
Hopper sample from initial cleanup -Top
ND
S10-0876
Hopper sample from initial cleanup -Middle
ND
510-0877
Hopper sample from initial cleanup -Bottom
ND
Table, 3 - Taal Ars .nl� Samples 9ft_Qr. Final Cle?nVP (5olidsj
Prep by EPA method 3050, Analytical by EPA method 6010
(<5mg/kg As over background for successful remediation)
Sample #
Description
Total
(EPA 6010)
-
-
rrig/1% (pprn)
S10-0914
Background S onple.
ND
(I rench near road away from splll)
Composite of samples 1-10
ND
S10-0915
(10' to 100' from spill edge)
S10-0916
Composite of samples 11-20
ND
(110' to 200' from spill edge)
S10-0917
Composite of samples 21-30
ND
(210'to 300' from spill edge)
Composite of samples 31-40
ND
S10-0918
(310' to 400' from spill edge)
S10-0919
Composite of samples 41-43
ND
(410' to 430' from spill edge - inlet of 1st culvert)
S10-0923
Composite of samples 44-53
0.65
(10' to 100' frorn ouLlet of 1SL LulverL)
S10 0924
Composite of samples 54 62
ND
(110' to 180' from outlet of 1st culvert - inlet of 2nd culvert)
12/1/2010 3:37 PM CoaLogix Confidential 1 of 1

QUALITY MANAGEMENT PROCEDURE
Subject: Work Instructions
Loading Waste Water into a Bulk Tanker at the Steele Creek
Facility
1. Responsibility
1A. The Supervisor is responsible to ensure:
NUMBhk:
Issue Date: I Revision Level: I Revision Date:
12-01-10 1 New
Approved By
1.1.1. All operators are aware of the risks and consequences of not following this procedure when
loading waste water into a bulk tanker.
1 1 2. All operators are trained on how to properly and safely load tankers with waste water.
1.1.3. The operator assigned to load has been given instructions on what to load, from where to load
it, how much to load, the hazards of the material and the required PPE.
1.2. All CoaLogix Operators are responsible to ensure:
1.2.1. They have received and understand training on waste water loading procedures and transfer
equipment operation.
1.2.2. They understand the instructions on what to load, from where to load it, how much to load,
the hazards of the material and the required PPE.
1.2.3. Wheel chocks are in place before loading a truck with waste water
1.2.4. They communicate the driver's responsibilities to the driver, including the following:
1.2.4.1. The driver trust have a radio while the truck is loading
1.2.4.2. The driver must continuously watch the loading operation until oomploted or stopped.
1.2.,,1.3. Tho driver must participate in the pro loading and post loading inspections and sign
off on [lie completed inspection sheet.
1.2.4.4. The driver must wear appropriate PPE including `fall protection' if necessary.
1.2.5. Driver has the proper paperwork signed and placards (if necessary) for each load
2. Procedure
2.1. Load Preparation
2,1.1. Have driver back into the proper position for loading in the containment bay.
2.1.2. Chock the trailer.
Page 1 of 3
This document belongs to SCR Tech, Inc, It cannot be reproduced or transmitted without authorized approval,

SCR Tech, Inc.
QUALITY MANAGEMENT PROCEDURE
NUMBER:
Issue Date:
Revision Level:
Revision Date:
12-01-10
New
Subject. Work Tnstnictionr;
Approved Rv:
Loading Waste Water into a Bulk Tanker at the Steele Creek
Facility
2.1.3. Get loading instructions from the Supervisor.
2.1.4. Obtain a truck loading inspection sheet and conduct the pre -loading inspection with the
driver (the operator and driver should sign inspection certification).
2.1.5. Determine the maximum loading capacity of the truck. Plan to load no more than 90°r0 of the
truck capacity or 5,500 gallons, whichever is less.
2.1.6. Determine the tank measurement or truck fill level before beginning to prevent overfilling.
2.1.7. Plan to document on the truck loading inspection sheet the start time, the tank #, start and
finish levels, the trailer #, the finish level, the finish time
2.1.8. Give the driver a radio to use during the loading operation and instruct the driver on the
driver's responsibilities during the loading process.
2.1.9. Put on the proper PPE and hook up the hose from the appropriate line (as instructed by the
Supervisor) to the tanker. if the hose is to be secured inside the top dome, make sure all other
valves are closed, open the dome, have the driver place the hose approximately two feet inside
the dome, ensure that the driver has properly secured it and attaches a manual shut off valve to
the end of the hose (make sure it is in the open position).
2.1.10. Have the driver do a radio check and get positioned at the dome to watch the flow of the
material into the truck.
2.2. Loading
2.2.1. Start the transfer operation as instructed by the supervisor and wait for Coll firination by the
driver that a steady flow is goring into the tanker and the hose is remaining securely in place.
2.2.2. Continuously watch the loading process (approximately 1 hour) and tanker fill level every 5
minutes or sooner when close to full.
2.2.3. When the tanker is close to full, have driver continuously observe at the dome until full or
flow is shut off.
2.2.4. Once the tanker is full or the loading is completed turn off the pump and shut the valve, then
have the driver close the manual valve.
2.3. Load completion
Page 2 of 3
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SCR 'Tech, Inn.
QUALITY NIANACEMENT PROCEDURE
Subject: Work Instntctions
Loading Waste Water into a Bulk Tanker at the Steele Creek
Facility
NUMBER:
Issue Date: Revision Level: Revision Date:
12-01-10 1 New
Approved Ry-
2.3.1. Help the driver bring the hose to ground level and drain the hose into a bucket, remove the
manual valve and cap the hose.
2.3.2. Set the hose back in the containment where it cannot get run over.
2.3.3. have the driver close; and secute the tanker doine, and check the other lanket uk. cialigs to
make sure they are fully closed and capped.
2.3.4. Remove the wheel chocks.
2.3.5. Complete the loading information on the inspection sheet.
2.3.6. Conduct a final area inspection with the driver and sign the completion certification.
2.3.7. Complete the Manifest and have the driver sign it. Keep the front copy and get the remaining
copies to the driver.
2.3.8. Clean up the area as needed.
3. Quality Records
3.1. Inspection sheets and Manifests listed in this document will be stored and retained as specified in
QMY 4.2.4.
4. Record of Revisions
Page 3 of 3
This document belongs to SCR Tech. Inc. It camtot be reproduced or transmitted without authorized approval.

Ste 9 �'e , E',, " er TaIiik'i' Ci n .;
Manifest #:
Date:
Operator:
Time:
Driver:
Tanker Capacity:
From (Tank #)
To (Trailer #)
Start Time
Start Level
Finish Time
Finish Level
Pre -loading Inspection;
Iyes
INo
initials
Initials
Trailer in containment
Wheels chocked
Reviewed Lei ivei's responsibililie.s w4h driver
Driver has a radio
All valves on trailer properly closed and capped
Evidence of spill inside or outside of containment i
yes, report to supervisor and clean up prior to loading
tanker)
Evidence of spills on tanker (if yes, report to
supervisor document and take picture)
The containment sump empty
The hose is good shape
The hose been properly and securely put in place
The manual valve has been attached to the hose
Tank# WW is coming from and Trailer# WW is going
to recorded
Wearing proper PPE
Post -loading Inspection:
IYes
INo
lnitiais
11nitials
Evidence of spill inside or outside of containment (if
yes, report to supervisor and clean up prior to loading
tanker)
Evidence of spill on tanker (if yes, report to supervisor
document and take picture)
Hose properly disconnected, drained, capped, and
stored
Dome properly closed and secured
All valves properly closed and capped
Chocks removed
Radio returned
Trailer properly placarded (if necessary)
All paperwork properly completed
Manifest signed and issued
Containment area clean and sump empty (if not clean
area and empty sump)

A(�T)N
SCWTECH
A CouLogir», Compaep
SCR Catalyst Management & Regeneration Services
Before and After Pictures of 11/17/10 Spill Remediaton
Before
After

` SCTECH
A O)aLogir- Cotnpa-t�v
SCR Catalyst Management & Regeneration Services
Before and After Pictures of 11/17/10 Spill Remediation
Before
After

' CO A ;
Collection System SSO 24-Hour Notification
Collection System: Number and Name WQCS# (C\jC
Incident Number from BIMS
Incident Reviewed (Date):
Incident Action Taken: BPJ
NOV-2010-DV
.......................................................................
Spill Date + I p Time � 'p�� / prri
Reported Date I' It-) Time (;' am/ pm
Reported To SWP Staff or EM Staff
Reported By :� /44 .� Phone
Address of Spill
County City
Cause of Spill
Total Eslimaled Galluns Est. Gal to Stiealri
Stream Fish Kill: Yes No Number Species
Non Required Information and other comments relating to SSO incident:
Response time minutes lone Mar (quad
M

North Carolina Emergency Management - EM43 Reporting Page 1 of 3
North Carolina Emergency Management - EM43 Reporting
Print ( Return To List
EM Level:
NCEM Edited:
Include in Report:
4
Yes
Yes
Taken by:
Date/Time Reported:
Date/Time Occurred:
R Dail
11/17/2010 14:12:01
11/17/2010 04:00:01
Reported by:
Agency:
Phone:
NRC
USCG
800-424-8802
County:
City:
Area:
Mecklenburg
Charlotte
13
SLreel.Address.
Zip Code:
11707 Steel Creek Rd
EVENT TYPE
Type: Wastewater
Animal Disease Event Type: Bomb Threat Event Type:
Complaint Event Type:
Fire Event Type:
FNF Event Type:
FNF Class:
HazMat Event Type:
HazMat Class: HazMat Mode:
Homeland Security Event:
Non-FNF Event: Non-FNF Event Type:
Other Event Type:
SAR Type:
Transportation Event Type: Wastewater Event Type:
Other
Weather Event Type: Weather Event Name: WMD Event Type:
State Resource Request
Event Description:
NRC reported 1500 gallons of treated wastewater released from a discharge point of a local
chemical facility to a trench due to operator error. The release was secured, the soil was excavated
and cleanup operations were conducted.
Attachment
Filename: NRC 960103.docx
Deaths: Injuries: Evacuation: Radius:
0 0 0 0
Responsible Party: Responsible Party Phone:
Coalogix, 11707 Steel Creek Rd, Charlotte, 980-254-6350
NC
Point of Contact: Point of Contact Phone:
Mike Mates 980 254 6350
Latitude: Longitude:
00.000000 00.000000
https://www.ncsparta.net/eoc7/boards/board.aspx?tableid=275 &viewid=1011 &label=EM... 11 /18/2010

NATIONAL RESPONSE CENTER 1-800-424-8802
***GOVERNMENT USE ONLY***GOVERNMENT USF ONT,Y***
Information released to a third party shall comply with any
applicable federal and/or state Freedom of Information and Privacy Laws
Incident Report # 960103
INCIDENT DESCRIPTION
*Report taken by: CIV BRENT TALIAFERRO at 13:23 on 17-NOV-10
Incident Type: FIXED
Incident Cause: OPERATOR ERROR
Affected Area:
lncldenL uuuuLLt:d uii 1/ NOV 10 aL 04:00 local Liiu-LdeiiL Lime.
Affected Medium: LAND TRENCH
REPORTING PARTY
Name: MIKE MATTES
Organization: COALOGIX
Address: 11707 STEEL CREEK RD
CHARLOTTE, NC
COALOGIX reported for the responsible party.
PRIMARY Phone: [phone]
Type of Organization: PRIVATE ENTERPRISE
SUSPECTED RESPONSIBLE PARTY
Name: MIKE MATTES
Organization: COALOGIX
Address: 11707 STEEL CREEK RD
CHARLOTTE, NC
Px1MARY Phone: [phone]
INCIDENT LOCATION
11707 STEEL CREEK RD County: MECKLENBURG
City: CHARLOTTE State: NC
RELEASED MATERIALS)
CHR1S Code: OTH Official Material Name: OTHER OIL
Also Known As: TREATED WASTE WATER
Qty Released: 1500 GALLON(S)
DESCRIPTION OF INCIDENT
CALLER REPORTED A SPILL FROM THE DISCHARGE POINT DUE TO OPERATOR
ERROR.
SENSITIVE INFORMATION

INCIDENT DETAILS
Package: N/A
Building TD:
Type of Fixed Object: CHEMICAL FACILITY
Power Generating Facility: UNKNOWN
Generating Capacity:
Type of Fuel:
NPDES:
NPDES Compliance: UNKNOWN
IMPACT
Fire Involved: NO Fire Extinguished: UNKNOWN
1NJURiEs. NU huspiLaliztu: Liapl/ULUVd: L'a6ae:iiyeL;
FATALITIES: NO Empl/Crew: Passenger: Occupant:
EVACUATIONS:NO Who Evacuated: Radius/Area:
Damages: NO
Hours Direction of
Closure Type Description of Closure Closed Closure
N
Air:
N Mayor
Road: Artery:N
N
Waterway:
N
Track:
Environmental Impact: UNKNOWN
Media Interest: NONE Community Impact due to Material:
REMFDTAT, ACTIONS
EXCAVATED SOIL, CLEAN UP UNDERWAY
Release Secureu: YES
Release Rate:
Estimated Release Duration:
WEATHER
Weather: CLEAR, °F
ADDITIONAL AGENCIES NOTIFIED
Federal: NONE
State/Local: NONE
State/Local On Scene: NONE
State Agency Number: NONE
NOTIFICATIONS BY NRC
USCG ICC (ICC ONI)
17 NOV 10 13:27 (301)6603363
DHS I&A STATE AND LOCAL PRGM OFFICE (RALEIGH, NC FUSION CENTER)