NCS000007_MONITORING INFO_20060802

i
-------STORMVUATER-DIVISfON"CODINGSHEET - -- -
PERMIT NO.
� GS 00000�
DOC TYPE
❑FINAL PERMIT
N�MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ (J 6pi,ri 1
YYYYMMDD

f
1
Aug. 2. 2006 12:07PM WH IE No-0386 P. I
hronC-hemical
WRS 305 Amherst Road
U Ma unNon, NC 28W5
voice; (M) 438-4M
Injiyubwcture & EimronmM4 Inc.
AUG - 2 2005 Pax: (8n) 437-1155
¢r4
WATER QUALITY SECTION
ASHEVILLE REGIONAL OFFICE
FAX
812106
DATE:
NCOENR
TO - COMPANY:
_
Larry Frost
ATTENTION;
828-299-7043
FAX NUMBER:
Greg, Garrison
FROM:
16
NUMBER OF PAGES INCLUDING COVER: _
COA17*ENTS: LC — 60 Results from samplecollected directly from the fracs.
The water from these frace have been pumped to the POTW. The water currently in
Fracs Is from other storm events and slnce the sample was collected the site has
Changed waste has been cleaned and removed from the site, The water currently
Stared Is cleaner than the Initcial storm water collected

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AUG - 2 2006 Do
WATER QUALITY SECTION
ASI-IEVILLE REGIONAL OFFiCrc

Aug. 2. 2006 12:0 M WRS[E No-0386 "P. 3
Ti3IMM= SPEARMAN-XMWER METKOD% VERSYQN 1.5
DATE: 6/10/06 TWT NUZ43ER1 nURATIdN_ 96 h
T=:[C WT $ynthmn Pile FT-07
SPEC_ IES : Cariodaphnia dubia _
RAW DATA: e03mr-a 'oration Number Mortalities
-- -- (W.) Exposed
.00 20
6.25 20 0
12.50 20 2
25.00 20 5
50.00 20 9
10D.00 20 20
SPBAFiyvw-KARBSR TRIM
$$EARNhN-KARSER LSTIMATFB: LC50; 42.23
95t L )M CQi9FIDSNCB: $3.96
95* UPPER CWFIDZNCN I 52.S2
NOTE- MORTALITY PROPORTIONS WS9.8 b= MONOTOMCALLY =CRRABING.
AWUS KMrXS WADE V=E PRIOR TO BPBAW=- KPXMM TBTIMATIM .

Aug. 2. 2006 12:03PM WWI E
TRXMMM SPEARMAN-WMER METHOD. VMMICN 1-5
DATE: 6/10/06 TEST BR: R
TOXICANT Synthron Pire FT�-08
SPECIES: Ceriodaphnia dubia
RAW DATA Concentration Number
--- -- -- ($) Rxosed
N©-0386 P. 4"
DURATION; 96 h
mortalities
. a0 20 1
5.29 20 0
12.50 20 1
25.00 20 3
5a.00 20 1
100,00 20 17
9pM RAN-KUB2R TRIM: IS.384
38SARMAN-KAR88R ESTaMTES: LC50: 73-20
95$ LOWER C'Gl+ lDMZCS s 66.67
9 3 t UPPER CONE IDENCE : 8 0.3 7
NOTE.- MORTALITY PROPORTIONa WERE NOT MONOTONICALLY INCREASING .
ADJUSTURNTS WXRE MADE PRIOR TO SPSARMAX-XAR99R ESTIMATION.
`IRIMMM SVEARXAN-XAX3M METRDT}_ VERSION 1.5
DATE: 6/10/06 TEST =90Me 3 DURAtIONt 96 h
TOXICA= Synthron Fire PT-09
SPECIES; Cerioda:phniat dubia
RAW DATA: Concentration Number Mertalitiea
--- --�� (t) F14poaed
.00 20- 1
9,25 20 Z
12.50 20 5
25.00 20 2
$0.00 20 1
3.00.00 20 17
SPB AN-KARBER TRZXz 15.79t
SPEA.RMAN-PULBMER ESTIMATES; LC50: 73.03
950 LGWM CDNFIDENCR- 66.2-5
95t UPPER WNFIDEXCH; 80.90
Nom . MORTALITY PROPORTIOtNB WOW NOT MONOTONICALLY INCREASIM .
An3VSTb=TS 4RM MAKE PRIOR TO SPEARMAV-KARBER ESTIMATION7.
-----------__------_--------------..-.---w..---w-��--�ti-
TR±MMRI3 SPEAP14KN-XAMMR METHOD. VERSION 1.5

Aug. 2. 2006-12:09PM WRSIE --- - No•0386' =P• 5
DAZE; 6/10/06 TRAs NUMBER! 5 13UMTIONa 96 h
TOXICANT :. $Iyntrlron Fite PT-11
SPEGTE9 s CeriWa:phnia dubia
RAW DATA: Con.aentrAti= Number mortalities
---- ---- i40 Exposed.
.00 20 1
6.25 20 9
I2.S0 20 4
25.00 20 10
50 .00 _ 20 19
1oo.ao 20 20
SVZAR:4AN-KPMZR TRIMi 21.05%
rpVEA9X=-KA3WHR•ESTrMTES: LCSOs 24_22
a5vs La"M CQNFIDSKc8 : 16.38 ,
95$' UPQRR CONFIDENCE: 31-94
NOTE: MORTALITY PROPORTIORS WMtE NOT. MONOTONICALLY •INC MSING.
ADiTUSZDMNTS WERE MADE •PRXOR TO 9PEAPJQN-10UUM ESTIMATION.
------------- --------------- .-------------------------------------- __---------

Aug' 2. 2006 1219MA WRS[E
No-0386 'P. 6
EWXZUXM
JAMARY 19"
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Aug. 2. ME 12:IOPM WRSIE
No•0386 'P• 8
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Re: [Fwd: [Fwd: Synthron Chemical water treatment results]]
Subject: Re: [Fwd: [Fwd: Synthron Chemical water treatment results]]
From: Ken Pickle <[e-mail]>
Date: Fri, 28 Jul 2006 10:09:27 -0400
To: Larry Frost <[e-mail]>
CC: Bradley Bennett <[e-mail]>
Larry,
a) I note that there were hits on barium, cadmium. I don't know the significance
of the levels reported.
b) Intuitively I believe that the BOD report of <2.0 ppm is innocuous.
c) I note that the test data presented does not include some of the analytes that
were previously present in frac tanks 7-12. Many of the metals were not tested for
this time. Organics present in frac tanks 7-12, but not even tested for in this
data include 4-methylphenol, acetone, methyl acetate, carbon disulfide, and
2-butanone. I don't have enough of a water chemistry/water pollution background
to know if these omissions are significant, or not.
d) Our starting perspective is that the explosion resulted in a hazardous waste
spill. Runoff that has contacted a hazardous waste is hazardous waste, and cannot
be discharged under the current site stormwater permit. So, I think that as long
as the runoff can be considered to have been in contact with hazardous wastes it
cannot be discharged under our permit.
e) Now, moving on to: What about a cleaned up site? I think our preferred posture
is this: Synthron has a permit, and they're still responsible for the runoff from
the site. We tell other people that abandon a site that they continue to be
responsible for runoff under the permit until they have removed any potential
exposure of wastes or process materials. Once that exposure, or potential
exposure, is removed we can rescind the permit at a closed or abandoned industrial
site, if the permittee will request it. I think that applies here. We typically
ask the RO to visit the site and confirm that the clean up has been accomplished as
part of the recission process. I think that ARO site confirmation is especially
important in this case.
f) It seems to me that we may need some contact with the NC DWM folks to know what
the federal and state rules require in this sort of situation.
Ken
Larry Frost wrote:
Ken
Bradley is out, will look over the following and give me your thoughts.
Larry
Larry Frost - [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: [phone]
Fax: [phone]
1 of 3 7/31 /2006 8:22 AM

Re, [Fwd: [Fwd: Synthron Chemical water treatment results]]
Subject:
[Fwd: Synthron Chemical water treatment
From:
Larry Frost <[e-mail]>
Date:
Fri, 28 Jul 2006 08:13:24 -0400
To:
Jeff Poupart <[e-mail]>,
<[e-mail]>, Sandy Mort
results]
Bradley Bennett
<[e-mail]>
To:
Jeff Poupart <[e-mail]>, Bradley Bennett
<[e-mail]>, Sandy Mort <[e-mail]>
CC:
Roger Edwards <[e-mail]>
Guys
As you may or may not remember EPA contractors have been cleaning up the
Synthron Chemical Plant site for the last 2 months and since the explosion that
destroyed the plant they have been collecting all runoff from the plant in
tanks. They have been discharging this contaminated water to the City of
Morganton WWTP at a very low flow rate to ensure no pass through at the WWTP.
They are concerned that with the on going rain events they continue to add more
tanks and get further behind, also tank rental is expensive and they continue to
add tanks (currently 16). Recently the contractors brought in a filtration unit
consisting of progressive filtration and activated carbon bed . They ran a test
of the system on 7/20/06 with the attached results. Their desire is to continue
to collect all runoff, filter all of what is collected (all fire suppression
water has been discharged to the WWTP) and discharge to the stream, with some
sort of monitoring (possibly weekly effluent SOD, COD, TSS RCRA metals semi
VOC's and VOC's) reported to ARO.
Please review the attached results and give me your comments/thoughts.
Thanks
Larry
Larry Frost -- [e-mail]
North Carolina Dept. of Environment and Natural Resources
Asheville Regional Office
Division of Water Quality - Water Quality Section
2090 U.S. 70 Highway
Swannanoa, NC 28778
Tel: B28-296-4500
Fax: B28-299-7043
Subject:
Synthron Chemical water treatment results
From:
"Greg Garrison" <[e-mail]>
Date:
Thu, 27 Jul 2006 16:43:39 -0400
To:
<[e-mail]>
To:
<[e-mail]>
CC.
< au han. err @e a.cov>, <[e-mail]>
Mr. Frost,
2 of 3 7/31/2006 8:22 AM

Re: [Fwd: [Fwd: Synthron Chemical water treatment results]]
I have attached the analytical results from the water treatment system effluent
sample. Please review for discharge into the storm water ditch on the south side
of the site or per Synthron's NPDES permit discharge point. If approval for
discharge can be expedited it would be greatly appreciated, the frac tanks are
quite expensive and we would like them off -site ASAP.
Thanks for you assistance in this matter,
Greg Garrison
Project Manager
WRS Infrastructure & Environment, Inc.
813-684-4400 (WRS Office)
828- 448-4888 ( Site Phone)
813-917-2542 ( Cell?
3 oi'3 7/31/2006 8:22 AM

TestAmerica
ANALYTICAL TESTING CORPORATION
July 27, 2006
Client: WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn: Greg Garrison
SAMPLE IDENTIFICATION
W WT 072006
2960 Foster Creighton Road Nashville, TN 37204' 600-765-0960' Fax [phone]
Work Order:
NPG2609
Project Name:
Synthron Chemical RUSH
Project Nbr.
US > PA Region 4 - Synthron Chemical Fire/106150
P/O Nbr.
74110248
Date Receivcd:
07/21/06
LAB NUMBER COLLECTION DATE ANDTIME
NPG2009-01 07/20/06 16:00
An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum
to this report. If you have any questions relating to this analytical report, please contact your I-aboratory Project Manager at
1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's aceredidation.
This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is
privileged and confidential. if you are not the intended recipient, or the employee or agent responsible for delivering this material to the
intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you
have received this material in error, please notify us immediately at 615-726-0177.
North Carolina Certification Number: 387
The Chain(s) of -Custody, 2 pages, are included and are an integral part ofthis report.
These results relate only to the items tested. This report shall not be reproduced except in fill] and with permission of the laboratory.
Report Approved By:
gwu /, ("w-
Roxanne Connor
Senior Project Manager
Page 1 of 22

TestAmerica
ANALYTICAL TESTING CORPORATION 2960 Foster Creighton Road Nashnlla, TN 37204' 800-765-0980 • Fax [phone]
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Ann Greg Garrison
Work Order.
NPG2609
Project Name:
Synthron Chemical RUSH
Project Number:
US EPA Region 4 - Synthron Chemical Fire/I U6150
Rdceived:
07/21/06 08:00
A,NAL1" rICAL REPORT'
Analyte Result Flag Units
Sample ID: NPG2609-01 (WWT 072006 - Waste Water) Sampled: 07/20/06 16:0(
General Chemistry Parameters
BOD - 5 Day
2.00 <
mg/L
ROD - 5 Day
2.01) <
mg/L
Chemical Oxygen Demand
ND
mg/L
Total Suspended Solids
ND
mg/L
Total Metals by EPA Method 601 OB
Arsenic
ND
mg/L
Barium
0.17-S
mg/L
Cadmium
0.00130
mg/L
Chromium
ND
mg/L
Lead
ND
mg/L
Selenium
ND
mg/L
Silver
ND
mg/L
Mercury by EPA Methods 747OA/747IA
Mercury
ND
Ing1L
Purgeable Organic Compounds by EPA Method
624
Acrolein
ND
ug/L
Acrylonitrile
ND
ug/L
Benzene
ND
ug/L
Bromodichloromethane
ND
ug/L
Bromofonn
ND
ug/L
Bromomethastc
ND
ug1L
Carbon Tetrachloride
ND
ug/L
Chlorobenzene
ND
ug/L
Chlorodibromometh3ne
ND
ug/L
Chloroethane
ND
ug/L
Chloroform
ND
ug/l-
Chloromethane
ND
ug1L
1,2-Dichlorobenzene
ND
ug/l-
1,4-Dichlorobcnzene
ND
ue1L
0-Dichlorobenzene
ND
ug/L
Dichlorodilluoromethane
ND
ug/L
1,2-D-sschloroethane
ND
ug/L
1, 1 -Dichloroethane
ND
ug/L
cis-L2-Dichloroethene
ND
ugll,
trans-1,2-Dichloroethene
ND
ug/L
1,1-Dichloroethene
ND
ugll.
1,2-Dichlorupropane
ND
ug/L
cis-1,3-Dichloropropene
ND
ug/L
trans-0-Dichloropropene
ND
ug/l.
Ethylbenzene
ND
ug/L
Methylene Chloride
ND
u0L
1,1.2.2- ietrachloroethane
ND
ug/L
Dilution Analysis
A'IRL Factor Daterl'ime Xlethod Batch
2,00
1 07/26/06 22:30
EPA 405.1
6073832
2.00
1 07/26/06 22:30
SM 5210B
6073832
10.0
1 07/21/06 12:14
EPA 410.4
6073730
2.00
1 07/21/06 19:01
EPA 160.2
6073835
0,0100
l 07/24/06 16:46
SW846 601OB
6074122
0,0100
l 07124/0616:46
SW846601OB
6074122
0.00100
1 07/24/06 16:46
SW846601OB
6074122
0.00500
l 07/24/06 16:46
S W 846 601 OB
6074122
0,00500
1 07/24/06 16:46
SW846 601OB
6074122
0.0100
1 07/24/06 16:46
SW846 601OR
6,074122
0.00500
1 07/24/06 16:46
SW846 601OR
6074122
0.000200
1 07/26/06 13:18
SW846 7470A
6074086
50.0
1 07/22/06 t 9:40
EPA 624
6074013
10.0
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
I.00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1,00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1 00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1.00
$ 07/22106 19:40
EPA 624
6074013
1.00
1 OW22106 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19A0
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19A0
EPA 624
6074013
l _00
1 07r22106 19:40
EPA 624
0074013
Loo
1 07/22/06 19:40
EPA 624
6074013
L00
1 07/22/06 19:40
EPA 624
6074013
1.00
1 07/22/06 19:40
EPA 624
6074013
LOO
1 07/22/06 19:40
EPA 624
6074013
1,00
1 07/22/06 19:40
EPA 624
6074013
1,()()
1 07/22/06 19:40
EPA 624
6074013
5.00
1 07/22/06 19:40
EPA 624
6074013
1,00
1 07/22/06 19:40
EPA 624
6074013
Page 2 of 22

r
Test merlca
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 3360
Atin Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax [phone]
Work Order:
NPG2609
Project Name:
Synthron Chemical RUSH
Project Number.
US EPA Region 4 - Synthron Chemical Fire1106150
Received:
07/21/06 08:00
ANALYTICAL REPORT
Analyte Result Flag units NIRL
Sample 1D: NPG2609-01 (WWT 072006 - Waste Water) - cont. Sampled: 07/20/06 16:00
Purgeable Organic Compounds by EPA Method 624 - cont.
Tetmchloroethene
ND
ug/l,
1.00
Toluene
ND
ug/L
1.00
1,1,2-Trichloroethane
ND
ug/l,
1.00
1,1,1-1'richloroethane
ND
ug/L
1.00
Trichloroethene
ND
ug/L
1.00
Trichloroftioromethane
ND
ug/L
1.00
Vinyl chloride
ND
ug/l.
1.00
Xylenes, total
ND
ug/L
2,00
Sum 1,1-Dichloroelhane-d4 (81-116%)
89 %
Surr.• Dibromafbroromerhane (88-110%)
103 %
Sum Toluene-& (85-130%)
105 %
Sum 4-Broraafhioroben_ene (80-114%)
94 %
Acid and Base/Neutral Extractables by EPA
Method 625
Acenaphthcnc
ND
ug/L
10,7
Acenaphthylene
ND
ug/L
10.7
Anthracene
ND
ug/l.
f0.7
Benzo (a) anthracene
ND
ug/L
10,7
Benzo (a) pyrene
ND
ue)L
i0.7
Benzo (b) fluoranthcne
ND
ug/l.
10.7
Benzo (g,h,i) perylene
ND
ug/L
10.7
Benzo (k) tluoranthene
ND
ug/L
10.7
4-Bromophenyl phenyl ether
ND
tig/L
10.7
Butyl benzyl phthalate
ND
ug/l,
10.7
4-Chloro-3-methyl phenol
ND
ug/L
10.7
Bis(2-chlorocthocy)methane
ND
ug/L
10.7
Bis(2-chloroeth),l)ether
ND
ug/l'
10.7
Bis(2-chloroisopropyl)ether
ND
ug/L
10.7
2-Chloronaphthalene
ND
ug/l,
10.7
2-Chlorophenol
N D
ug/L
10.7
4-Chlorophenyl phenyl ether
ND
ug/l,
10.7
Chryscuc
N D
ug/L
10.7
Dibenz (a,h) anthracene
ND
ug/L
10.7
Di-n-butyl phthalate
ND
ug/L
10.7
1,3-Dichlorobenzene
ND
ug/L
10.7
1,4-Dichlorohenz4ne
ND
ug/L
10.7
1,2-Diclilorobenzene
ND
ug/L
10.7
33-Dichlorobenzidine
ND
ue1L
10.7
2,4-Dichlorophenal
NI)
ug/L
10.7
Diethyl phthalate
ND
uelL
10.7
2,4-Dimethylphenol
ND
ug1L
10.7
Dimethyl phthalate
ND
ug/L
10.7
4,6-Dinitro-2-methyl phenol
ND
ug/L
26.7
2,4-Dinitrophenol
ND
ug/l,
26.7
Dilution Analysis
Factor Dateft'ime Method Batch
1 07/22/06 19A0
EPA
624
6074013
1 07/22/06 19A0
EPA
624
6074013
1 07/22/06 t9 40
EPA
624
6074013
1 07/22/06 19A0
EPA
624
6074013
1 07/22/06 19:40
EPA
624
6074013
1 07/22/06 19:40
EPA
624
60740 t 3
1 07/22/06 19:40
EPA
624
6074013
1 07/22/06 19:40
EPA
624
6074013
07122106 19:40
EPA
624
6074013
07122106 19:40
EPA
624
6074013
07122106 19:40
EPA
624
6074013
07122106 19:40
EPA
624
6074013
1 07/25/06 20:06
EPA
625
6073897
1 07125/06 20:00
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20-06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
t 07/25/06 20:06
EPA
625
6073997
t 07/25/06 20:00
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
l 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20:06
EPA
625
6073897
1 07/25/06 20-06
EPA
625
6073897
1 07125/0fi 20:06
EPA
625
6073897
Page 3 of 22

TestAmerica
ANALYTICAL. TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Greg Garrison
2%0 Fester Creighton Road Nashville, TN 37204' 800-765-0980' Fax [phone]
Work Order: NPG2609
Project Name: Synthron Chemical RUSH
Project Number: US EPA Region 4 - Synthron Chemical Fire/106150
Received: 07/21/06 08:00
ANALYTICAL REPORT
Dilution Analysis
Analvie Result Mal; Units MIZI, Factor Date/time Method Batch
Sample I1): 1NPG2609-01 (WWT 072006 - Waste Water) - cont. Sampled: 07/20/06 16:00
Acid and Base/Neutral Extractables by EPA Method 625 - cont.
2,6-Dinitrotoluene
ND
ug/L
10.7
2,4-Dinitrotoluene
ND
ug/L
103
Di-n-octyl phthalate
ND
ug/L
10.7
13is(2-ethy1hcxyl)phthalate
ND
ug/L
10.7
Fluoranthene
ND
ug1L
10.7
Fluorene
ND
ug/L
10.7
Hexachlorobenzene
ND
ug/L
103
Hexachlorobutadie:ne
NJ)
ug/L
103
Hexachlorocyclopentadiene
ND
ug/L
10.7
Hexachloroethane
ND
ug/L
10,7
Indeno (I 2,3-cd) pyrene
ND
ug/L
10.7
lsophorone
ND
ug/L
10.7
Naphthalene
ND
ug/I-
10,7
Nitrobenzene
ND
ug/L
10.7-
2-N i tropheno I
ND
ug11-
10.7
4-N i tro pheno I
N D
ug/L
26.7
N-Nitrosodirwhylalnine
ND
uol-
10.7
N-Nitrosodiphenylamine
ND
ug/I-
10.7
N-Nitrosudi-n-propylamine
ND
ug L
10.7
Pell tachIOro phenoI
ND
ug/L
26.7
Phenanthrene
ND
ug/1'
10.7
Phenol
ND
ug/L
10.7
PYTMe
N D
ug/L
10.7
1,2,4 frichlorobenzene
ND
ugfL
10.7
2,4,6- Trichlorophenol
ND
ug1L
10.7
2-Methylnaphthalene
NI)
ug/L
10.7
Surr: Terphe)0414 (34-116%)
71 %
Surr: 2,4,64-rlhronropherrol (16.130/)
57 Yo
Surr. Phenol-rl5 (10-66%)
Ij %
Surr: ?-FluorohipheiiN (32-99%)
69 %
Surr: 2-FLrorophenol (10-81 %)
19 %
Surr: hirroben ene-d5 (19-116%)
70 %
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07125I06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/00 20:06
EPA 625
6073997
1 07/25/00 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20-06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
1 07/25/06 20:06
EPA 625
6073897
07125106 20:06
EPA 625
6073897
07/25106 20:06
EPA 625
6073897
07125106 20:06
EPA 625
6073897
07125106 20.06
EPA 625
6073897
07125106 20:06
EPA 625
6073897
07125106 20:06
EPA 625
6073897
Page 4 of 22

Testl�merica
ANALYTICAL 'TESTING Cd PPORATION
2960 Foster Creighton Road Nashville, TN 37204 ' 800-765.0980' Fax [phone]
Client WRS (3166)
Work Order:
NPG2609
221 Hobbs Street, Suite 108
Project Name:
Synthron Chemical RUSH
Fam11a, FL 33619
Project Number: US EPA Region 4 - Synthron Chemical Fire1106150
Ann Greg Garrison
Received:
07/21/06 08:00
SAMPLE Ex'r11AC-PI0N DATA
W I/ V of
Extraction
Parameter
Batch
Lab Nuntber
Extracted Extracted
Vol Date
Analyst
Method
Acid and Base/Neutral Extractables by EPA
Mctkwd 625
EPA 625
6073897
NPG26V)-Ot
935.00
1.00 07/24/06 15:59
CEC
EPA 625
General Chemistry Parameters
EPA405.1
6073332
NPG2609-0I
300.00
MOM 07/21/06 2F.55
JTH
BODICBOD
SM 5210B
6073932
NPG2609-01
300.00
300,00 07/21/06 21:55
M]
SODICBOD
Mercury by EPA Methods 7470A/7471A
SW8467470A
6074066
NPG2609-0t
30.00
-10.00 07/24/0604:47
AMB
EPA7470
Total Metals by EPA Method 6010B
SW946601OB
6074122
NPG2609-01
50.00
50.00 07/24/06 10:40
JLS
EPA 3010A
SW846601013
6074122
4PG26D9-0l
50.00
50.00 07/24/06 10:40
JLS
EPA 3010A
SW9466010B
6074122
NPG26D9-01
50.00
50.00 07/24/06 10:40
JLS
EPA3010A
SW846601013
6074122
NPG2609-01
50.00
50.00 07/24/06 10:40
JLS
EPA3010A
SW8466010B
6074122
NlIG2609-01
50.00
50,00 07/24/06 IDAO
JLS
EPA3010A
SW84660106
6074122
14PG2609-01
50.00
50,00 07/24/06 1040
JLS
EPA3010A
SW8466030B
6074122
NPG2609-01
50.()o
50A0 07/24/1)6 10:40
JLS
EPA3010A
Page 5 of 22

TestAm'erica
ANALYTICAL TESTING CORPORATION 296D Foster Creighton Road Nash✓He, TN 37204. 800-765-0980' Fax 615-72&3404
Client WRS (3166) Work Order: NPG2609
221 Hobbs Street, Suite t08 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number. US EPA Region 4 - Synthron Chemical Fire1106150
Attn Greg Garrison Received: O7f21106 08:00
Analyte Blank Value
General Chemistry Parameters
6073730-BLK1
Chemical Oxygen Dernand <5.50
6073832-BLK1
BOD - 5 Day
<LOO
BOD- 5 Day
<IAO
6073835-BLKI
Total Suspended Solids
<0,500
6073835-BLK2
Total Suspended Solids
<{5,500
Total metals by EPA Method 6010B
6074122-BLK1
Arsenic
<0.004(,D
Barium
<0.00100
Cadinium
<0-000401)
Chromium
<0.00150
Lead
<0-00240
Selenium
<0,00820
Silver
<0.00190
Mercury by EPA Methods 7470A/7471A
6074086-BLKI
1\IMLK3•
<0, 000100
Purgeable Organic Compounds by EPA t\Icthod 624
6074013-BLKI
Acrolein
<1.18
Acrylonitrile
<0.520
Benzene
<0.290
Brontodiehloromethene
<0.:70
Brmnoform
<0.140
Bramosnethane
<0-320
Carton Tetrachloride
<0.150
Chlorohenzene
<0,110
ChlorodibrOlmmnethane
<0. 130
Chloroedrane
<0, 170
Chlorofonn
0. 130
Chloromethane
<0,1 10
1,2-Diehlorobenzene
<0, 170
1.4-Dichlorobenzene
<0,310
PROJECT QUALITY CONTROL DATA
Blank
V Units Q.0 Batch Lab Number Analyzed Datmffime
mgJL
6073730
6073730-BLK1
07/21/06
12:14
.+rg)L
6073832
6073832-BLK)
07/26/06
22:30
mrJL
6073832
6073832-BLKI
07/26/06
223D
ingJL
6073835
6073835-BLKI
07/21106
19:01
mgJL
6073835
6073835-131,1<2
07/21/06
19:01
mg/L
6074122
61174 122-BLK 1
07/24/06
16:05
ngVL
6074122
6074122-BLK1
07/24/06
16:05
mglL
6074122
6074122-BLK1
07/24/06
16:05
mg1L
6074122
6074122-BLK1
07/24/06
16:05
mglL
6074122
6074122-BLK1
07/24/06
16:05
mg1L
6074122
6074122-BLK1
07/24/06
16;05
mg1L
6074122
6074122-BLKI
07/24/06
16:05
mg1L 6074i186 6074086-BLKI 07/26/06 13:02
ueJL
607401,
6074013-131-KI
07/22706 15:23
LI �JL
6074013
6074013-BLK1
07/22/06 15:23
ugl-
6074013,
6074013-111-K1
07/22/06 15:23
utJL
607403
6074013-BLKI
D7122106 15:23
ugjL
60740L3
6074013-BLKI
07/22/06 B523
ug%L
6074013
6074013-BLK l
07122106 15:23
u51L
6074013
6074013-BLK1
(17/22106 15:23
ng11-
6074013
007401 ;-BLK 1
07/22/06 15:2.1
ugll.
6074013
6074013-BLKI
07/22/06 15:23
ug/L
6074013
60740t3-111-KI
07/22/06 15:23
uc/L
6074011
607400-131-KI
07/22/06 15:23
uc/L
6074013
6074013-BLKI
07/22/06 15:23
ugit.
6074013
60740t3-BLK1
07/22/06 15:23
❑�1L
6074013
6074013-BLKI
07/22/06 15:23
Page 6 of 22

TestA-merica
ANALYTICAL TLS7ING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
'Pampa, FL 33619
Atin Greg Garrison
2960 Foster Creighton Road Nashville, -TN 37204 ' 800-765-0980' Fax [phone]
Work Order: NPG2609
Project Name: Synthron Chemical RUSH
Project Number. US EPA Region 4 - Synthron Chemical Fire/106150
Received: 07/21/06 08:00
PR0,1EC1' QIIALI'I'2' CO\-1.110L DA-I-A
131:utk - Cont.
Aualyle
Blank Value I)
Purgeable Organic Compounds
by EI"A Method 624
6074013-BLK1
1,3-Dichlorobenzene
<0. 120
Dichlorodi➢uoroinethanc
<0.470
1,2-Dichloroethene
<0, 560
1,1-Dichloroethene
<0.310
cis-1,2-Dichloroethene
<0.130
trnns-1,2-Dich loroelhenc
<0.130
1,1-Dichloroethene
<0.100
%2-Dichloropiopaue
<0. 150
cis-1.3. Dich loropropcne
<0.250
trans- L,-Dicltloropropcnc
<0.100
Ethylbenzene
<0.2 30
kletlMene Chloridc
<0.210
1,1,42- Felrachloroethane
<0.130
Tetrachloroethene
<0.1 10
Toluene
<0.280
1.1,2-Trichloroethane
<0.240
1,1,1-Trichloroetltane
<0.1 10
Trichloroetllenc
<0.100
Trichlorofluoromclhanc
<0. 120
Vinyl chloride
<0.370
Xvlencs. total
<0.68u
,1&rrogwe: 1, 2-UirLlnrwfhunc.d4
90%
Surroyale: 1Jrhmmr+Jhrorunrrlhunc
104%
Surnrt ie: Tolnrnc-dN
105%
Surm,vcae: 4-13ronu fhiomben-eni
94%
Acid and Base/Neutral Extractables by EPA Method 625
6073897-BLK1
Acenaphthene
<2.90
Acenaplrthylene
<3.00
Anthracene
<2.80
13enxa(a) anthracene
<2.60
Benzo (a) pyrene
<2.80
Benzo (b) ➢uoranthene
<3.00
Benzo (g,h,i) petylene
<2.90
Benzo (k) fluorartthene
< 1,70
4-Bromophenyl phenyl etlter
<2.20
Butyl beazyl pinlinlate
<2.70
4-Chloro-3-methylphenol
<2.40
Bis(2-chloroethoxy)1net1a1e
<3.40
Bis(2-chloroedtyl )ether
< 1.90
Units
Q.C. Batch
Lab Number
Analyzed Dale/fine
ugfL
6074013
0074013-BLKI
07/22/06 15:23
ug/L
6074013
6074013-BLKI
07/22l06 15:23
ug/L
6074013
6074013-BLKI
07/22/06 1523
ug1L
6074013
6074013-BLKI
07122106 15:73
ugIL
6074013
6074013-BLKI
07/22/06 15:23
ug1L
6074013
6074013-BLKI
07/22/06 15;23
ugJL
6074013
6074013-BLKI
07/22/06 15:23
ug1L
6074013
6074013-BLK1
07122106 15:23
ugJL
6074013
6074013-➢LKI
07/22106 15:23
ug/L
6074013
6074013-BLKI
07/22/06 15:23
uglL
6074013
6074013-BLKI
07/22/06 15:23
ug/L
6074013
6074013-BLK1
07/22106 15:23
ug/L
6074013
6074013-BLKI
07/22/06 15:23
ug/L
607401.1
6074013-BLKI
07/22/06 15:23
ug/L
6074011
6074013-BLKI
07/22/06 15:23
ug/L
L074013
6074013-BLKI
07/22l06 15:23
ug/L
6074013
6074013-13LK1
07/22/06 15:23
ovl-
60740L3
6074013-BLKI
07/22/06 15:23
ug/L
6074013
6074013-BLK1
07/22/06 15:23
ugJL
6,074013
6074013-13LK1
07122106 15:23
ugJL
6074013
6074013-BLKI
07/22/06 15:23
6074013
6074013-BLK1
07/22/06 15:23
6074013
6074013-BLKI
O7/22106 15:23
6074013
6074013-BLK1
07/22106 15:23
6074013
6074013-BLK1
07122/06 15:23
ugJL
6073897
6073897-BLK1.
07/25106 M44
uglL
6073897
6073897-BLK€
07/25/06 ISA4
uglL
6073897
6(173897-BLK)
07/25/06 18:44
ugll.
6073897
6073897-BLKI
07/25/06 18:44
uIVL
6013N97
6073897-BLK1
07/25/06 18:44
ug/L
6073897
6073897-BLKI
07/25106 18:44
ugJL-
6073897
6073997-BLKI
07/25/06 18.44
ue1L.
0073897
60731397-BLK1
07/25/06 18:44
ugA.
6073897
6073997-BLK I
07/25/06 18:44
ugJL
6073897
6073897-BLK 1
07/25/06 18:44
ug1L
6073897
6073897-BLK 1
07/25/06 18:44
ug/L
6073897
6073897-BLK I
07/25/06 18:44
ug/L
6073897
6073997-BLK 1
07/25/06 18:44
Page 7 of 22

TestAimerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 1lobbs Street, Suite 108
Tampa, FL 33619
Attn Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204' 800-765-098D' Fax [phone]
Work Order:
NPG2609
Project Name:
Synthron Chemical RUShi
Project Nulnber:
US EPA Region 4 - Synthron Chemical Fire1106150
Received:
07/21/06 08:00
PROJECT QUALITY CONTROL DATA
Blank- cont.
Analyte Blank Value
Acid and Base/Neutral Extraclahles by EPA Method 625
6073897-BLKI
Bis(2-chloroisopropyl)ether
<4.50
2-Chloronaphlltalene
<3.00
2-Chlorophennl
<2.00
4-Chlorophenyl phenyl ether
<2.50
Cltrysene
<2A0
Dibenz (a,h) arnhracene
<2.90
Di-n-buryl phthalate
<2.60
1,3-Dichlorobenzene
<L50
1,4-Dichlorobenzene
<1.70
l,2-Dichlorobeuzene
<1.70
3,Y-Dich lorobenzidine
<2.70
2.4-Dichloropltenol
<3.10
Diethyl phthalate
<2.60
2,4-Dime1hylphenol
<5.20
Dimethyl phthnlate
<2,46
4,6-Diuioo-2-tnethylpheno1
<3_3i1
2.4-Dinicrophenal
<2.90
46-Dinitrotoluene
<2.80
2,4-Dinitrotoluene
<2.50
Di-n-mty] phthalate
<2.80
Bis(2-ethylhexyl)phthalnte
4.50
FI uorant3tenc
<2.50
Fluorene
<2.70
HcxaAlorobenzer c
<2.40
Hexachlorobutadiene
<.3.2U
Hcxachlorocyclopemadiene
<5.50
HexachloroeOmne
<1.80
ladcuo (1,2, 3-cd) pyrene
<2.90
lsophorone
<2.40
Naphthalene
<2.90
Nitrobenzene
<4.50
2-Nitrophenol
<2.50
4-Nitrophenol
<4.50
N-Nitrosodimethylatnine
<3.70
N-Nitrosodiphenylamine
<3.80
N-N i lrosodi-u-propylandne
6.4 G
11entachlorophenol
<3,00
Phenanthmne
<2.40
Phenol
<4.60
Pyrcne
<2.7V
1,2,4-Tricklorabeitzeue
<2.70
2,4,6-Trichlorophca01
<2.90
Q Units
Q.C. Batch
. .
Lab Number
....................
Analyzed Dal&Time
....... ._..................
ug/L
6073897
6073897-BLKI
07125106
I8:44
uglL
60.1897
6073897-BLKI
07/25/06
18:44
ug/L
6073897
6073897-13LKI
07/25106
19:44
ug/L
6073897
6073897-BLK 1
07/25/06
18:44
ug/L
6073897
6073897-BLK 1
07/25/06
18:44
ug/L
6073897
6073897-BLK I
07/25/06
18:44
ug1L
6073897
6073897-BLKI
07/25/06
18:44
ug/L
6073897
6073897-BLK I
07/25/06
18:44
ug/L
6073897
6073897-BLKI
07/25/06
18W4
ug/L
6073897
6073897-BLKI
07125/06
18:44
uV/L
6073897
6073897-BLK I
07/25106
19:44
ugJL
6073897
6073897-BLK1
07/25106
18:44
ug/L
6073897
6073897-BLK1
07/25/06
18:44
uglL
6073997
6073997-BLK1
07/25106
18:44
ug/L
6073897
6073897-BLKI
07125/06
]8:44
uglL
6073897
607;89?-BLK1
D7125106
19:44
ug/L
6073897
6073897-BLK1
07/25106
18:44
ug/L
60 -1897
6073897-t3LK 1
07/25/06
18:44
uglL
6073897
6073897-BLKI
07/25/06
18:44
ug/L
6073897
6073897-BLKI
07/25106
18:44
utJL
607,3897
6073997-BLKI
07/25/06
19:44
ug/L
6073897
6073997-BLK1
07/25/06
18:44
ub1L
6073897
6073897-BLKI
07/25/06
18:44
ug/L
6073997
6073897-BLKI
07/25/06
18:44
uglL
6073897
6073897-BLKI
07/25/06
18:44
ug/L
6073897
6073897-BLKI
07/25/06
18:44
tgll-
6073,897
6073897-HLKI
07125/06
18:44
urjL
6073897
6073897-BLKI
07/25/06
18:44
u�1L
073897
6073897-BLK1
07125106
18A4
u0t.
6073897
6073897-BLKI
07125106
I8:44
ugL
6073897
6073897-BLK1
07125100
18:44
ug1L
6073897
6073997-BLK1
07/25/06
18:44
u6di-
6V738')7
6073897-BLKI
07/25/06
18:44
ug1l.
6073897
6073997-BLKI
07/25/06
18:44
ugll,
fi073897
6073897-BLKI
07/25/06
18:44
ug/L
6073897
6073897-BLK1
07/25106
18:44
ug/L
6073897
6073897-BLKI
07/25/06
18:44
uglL
6073897
6073897-BLK1
07/25/06
18:44
ag/l,
6073897
6073897-BLK1
07/25/06
18:44
aglL
6073897
6073997-BLKI
07/25/06
18:44
uglL
6D73897
6073897-BLKI
07Y25/06
18:44
ugll-
64173897
6073397-BLKI
07/25/06
18:44
Page 8 of 22

Testl�--.merica
ANALYTICAL TESTING CORPORATION 2960 Foster Creighton Road Nashville, TN 37204 - 800-765-0980 - Fax [phone]
Client WRS (3166) Work Order: NPG2609
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number: US EPA Region 4 - Synthron Chemical Fire/] 06150
Alm Greg Garrison Received: 07/21/06 08:00
PIZO.IEC'1'
QIIALI'I'Y CONTROL DATA
Blank - Cont.
Analyte
blank Value Q
Units
Q.C. B;'101
Lab Number
Analyzed DatcrTintc
Acid and Base/Neutral Extractables by
EI'A Melhod 625)
6073897-BLK9
Benzidine
<34,0
ugjt-
6073897
6073897-BLKI
07/25/06 18A4
1,2-Dipheny1hydrazine
a2.90
ugJL
6073897
6073897-BLKI
07125106 18'A4
2-Methy1naphmhalene
<L50
ugJL
6073897
6073897-BLKI
07/25/06 18:44
Surm are: Terphenvl-d14
72%
6073897
6073897-BLKI
07/25/06 18:44
Surrogate, 2.4.0.Trihrewwphenof
75%
6073997
6073897-BLKI
07/25106 18:44
.Surrogate: Phew! d5
25%
6073897
6073897-BLK I
07/25/06 19:44
S'urrggare.—-Jgrjimrhiphen)'1
64%
6073897
6073897-BLK 1
07/25/06 18:44
.Surnrl,wfe: 2-14uumphemd
36%
607.1897
6073897-BLK 1
07125106 19:44
,Surn;gare: Nirrohemene-di
63%
6t173897
6073897-BLK 1
07/25/06 18:44
Page 9 of 22

Testl�-,merica
ANALYTICAL TESTING C0RP0RAitC1N 2960 Faster Creighton Road Nashville, TN 37204.800.765-0980 - Fax [phone]
Client WRS (3166) Work Order: NPG2609
221 1lobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number: US EPA Region 4 - Synthron Chemical FirellOM 50
Attu Greg Garrison Received: 07121 /06 08:00
Analyse
General Chemistry Parameters
6073730-DU P1
Chemical Oxygen Demand
6073832-DUP1
BOD - 5 Day
BOD- 5 Dav
6073835-DUP1
Total Suspended Solids
6073835-DUP2
Total Suspended Solids
PIiO.IEC-I' Qt)AL1'I'1' CON'I'IZOL DATA
Duplicatc
Sample Analyzed
Orig. Val. Duplicate Q Units RI'D limit Batch Duplicated Date/Time
ND ND
90,9 90,2
9U.9 902
15400 14000
5.00 4.75
mg1L
10
6073730
NPG2609-01
07/21/06 12:14
mg/L
0,8
20
6073832
NP62562-01
07/26/06 22:30
mg1L
0.8
20
6073832
NPG2562.01
07/26/06 22:30
ntg/L
10
20
6073835
NPG2628.01
07/21/06 19:01
mgll-
5
20
1.073835
NPG2636.01
07/21/06 19:01
Page 10 or 22

T A.Bhst I lmeric a
ANALYTICAL TESTING, CORPORATION
2960 Foster Creighton Road Nashville, TN 37204.800-765-0980' Fax [phone]
Client WRS (3166)
Work Order: NPG2609
221 Hobbs Street, Suite 109
Project Name: Synthron
Chemical
RUSH
Tampa, FL 33619
Project Numly-r. US EPA
Region 4
- Synthron Chemical Fire/106150
Attn Greg Garrison
Received: 07121 /06 08:00
PROJE,C]' QUALITI' C:ON-I-ROL DATA
LCS
Target
Analyzed
Analyfe
Known Val.
Analyzed Val
Q Units
%Rec.
Range
Batch
Date/Time
General Chemistry Paranteten
6073730-BS1
Chemical Oxvgen Demand
20.0
20.7
UWLnL
104%
90- 110
6073730
07/21/06 12:14
6073832-BS1
BOD - 5 Day
198
189
uglmL
95%
85 - 1 l5
6073832
07/26/06 22:30
BOD - 5 Day
OR
198
ug1mL
95%
85 - t l5
6073832
07/26/06 22:30
6073835-BS 1
Total Suspended Solids
100
97,0
mg1L
97%
90 - 1 l0
6073835
07/21/06 19:01
Total Metals by EPA Method 6010B
6074122-BSI
Arsenic
0.0500
f1.0532
mg/L
106%
80- 120
6074122
07/24/06 16:10
Barium
211O
2.07
ing/L
104%
80 - 120
6074122
07/24/06 16:10
Cadmium
0-0500
0.0520
11ogJ1.
104%
80 - 120
6074122
07/24/06 16:10
Chromium
0.200
0.196
mglL
98%
80 - 120
6074122
07/24/06 16:10
Lcad
00500
0.0511
mg[L
t 02%
80 - 120
6074122
07/24/06 16:10
Selenium
0.0500
0.0529
nrg/L
t06%
80 -120
6074122
07/24/06 16:10
Silver
0.0500
0.054E
ntg l-
108 %
SO- 120
6074122
07t24106 16:10
117ercui-y by EPA Methods 7470i I7471A
6074086-BS1
b1ercun
0 OOtOO
0.00108
mg/L
108%,
78 -124
6074086
07/26/06 1104
Purgcable Organic CotnlroundS brEPA Mcthod
624
6074013-BSI
Acrolein
250
359
ugJL
144%
19- 196
6074013
07/22/06 13:46
Acrylonitrile
250
239
uglL
960 .
73 - 132
6074013
07/22/06 13:46
Benzene -
50,0
54.9
ug/L
1 10%
37 - 151
6074013
07/22/06 13:46
Bromodichloromethane
Soo
51.2
ug/L
102%
35 • 155
6074013
07/22106 13:46
Brotnofonn _
50,1E
55.3
ug1L
111
45 - 169
6074013
07R2/06 13:46
Brantomethane
50.0
554
ug1L
I 1 t%
1 - 242
6074013
07/22/06 13:46
Carbon'retrachloride
50A
49.5
ugil.
99°/,
70- 140
6074013
D7122106 13:46
Chlarobenzene
50.0
51-6
ug1L
103 %
37. 160
6074013
07122/06 13:46
Chlorodibromomethane
50.0
54.9
ug1L
110%
53- 149
6074013
07122/06 13:46
Chlormthane
50.0
55.4
ug/L
Ili%
14 - 230
6074013
07122106 13:46
Chloroform
50.0
51.6
ug/L
103%
51 - 138
6074013
07/22/06 13:46
Chloromelhmic
501E
37.6
ugll.
75%
1 - 273
6074013
07/22/06 13:46
1,2-Dichlorobenzcne
50.0
50.8
uclL
102 %
18 • 190
6074013
07/22106 13:46
1,4-Dichtmobeuzene
50.0
47.7
ug1L
95%
Is- 190
6074013
07/22/06 13:46
1,3-Dichloro6cnzcne
50-0
49.6
ugll-
991/.
59. 156
6074013
07/22106 13:46
Dichlarodifluoromethane
50.0
27.1
ug1L
54%
33 • 142
6074013
07/22/06 13:46
1,2-Dichloroethane
50.0
46.4
ug1L
93%
49- 155
6074013
07122106 13:46
Page l l of 22

TestAimerica
ANALYTICAL TESTING CORPORATION
2960 Faster Creighton Road Nashville, TN 37204 ' 800-765-0980 - Fax [phone]
Client WRS (3166)
221 l lobbs Street, Suite 108
Tampa, FL 33619
Atm Greg Garrison
WOA- Order.
Project Name:
Project Number:
Received:
NPG2609
Synthron Chemical RUSH
US EPA Region 4 - Synthron Chemical Fire/106150
07121/0608700
PROJECT QUAL11'1' CONI'ROL DA"1-A
LCS - Cont.
Target
Analyzed
Analyte
Known Val.
Analvzed Val Q
Units
%Rec.
......
Range
.. ...........
Batch
.....
DaIdTimc
...... ,... -.
Purgcal lc Organic Compounds by EPA
Method 624
6074013-BS 1
l,t-Dichloroetliane
50.0
50.4
ug1L
101%
59- 155
6074013
07122/06 13:46
cis-1,2-Dichloroethene
5W)
47.4
ug/L
95%
54 - 136
6074013
07/22/06 13:46
trans•1,2-Dichlomeihene
50.0
49.2
uglL
98%
54 - 156
6074013
07/22/06 13:46
LI-Dichloroethenc
So it
S4,6
ug/L
109%
1-234
6074011
07/22/06 13:46
1,2-Dichloropropanc
50.0
54.0
ug/L
IO8%
1- 210
6074011
07/22/06 13:46
cis. 1,3-Dichloropropene
50.0
45.0
ug/L
90%
1 - 227
607401-1
07/22/06 13:46
tracts-1,3-Dichloropropene
50.0
45,1
ug/L
90"/
17 - L83
6074013
07/22/06 13:46
Ethylbcnzcne
50.0
50,6
ug/L
101%
37- 162
6074013
07/22/06 13:46
Methylene Chloritfe
50.0
54.8
ug/L
1 10 %
1 - 22 t
6074013
07/22/06 13:40
1,1,2,2-Tetmchloroethane
50.0
46,7
ug/L
93%
46- L57
6074013
07/22/06 13:46
Tetrachloroethene
50.0
53,6
uglL
107%
64 - L48
6074013
07/22/06 13:46
Toluene
50.0
52.6
ug/L
105 %
47 - 150
6074013
07/22/06 13:46
1,1.2=rrichloroethane
50.0
54A
ug/L
109%
52- 150
6074013
07/22/06 13:46
I,1,1-Ti icldorocthane
50.0
51.1
ug/L
102%
52 - 162
6074013
07/22/06 13:46
Tricitloroulleae
50.0
58,8
ug/L
119%
71 - 157
6074013
07/22/06 13:46
Trichlorofluoromethane
50.0
45.5
ug/L
91%
17- lel
6074013
07122106 13:46
Vinyl c11106de
50.0
45,6
ug/L
91 %
1 - 25L
6074013
07/22/06 13:46
xylenes, total
ISO
155
ug/L
103%
80- L25
6074013
07/22/06 13:46
S•urnrgulr: 1,2-Dirh1oroelhune-d4
30.0
26.3
88%
81 - 126
6074013
07/22/06 13:46
Sum,guie: Uihronrr flrunomerhune
30.0
31.2
104 %
88 - L 20
6074013
07/22/06 13:46
Surmgule: 7irlucm-dti
30.0
11.0
103%
85- 130
(.074013
07/22/06 13:46
S•urrgqure: 4-Bmnsoj1unrohemene
30.0
27.9
93%
80- L24
6074013
07/22/06 13:46
Acid and Base/Neutral Extractidles by EPA Method 625
6073897-BSI
Acenapltthene
50.0
425
MNRI
ug/L
85%
47- 145
6073997
07/25/06 19:12
Acenaphthylene
50.0
4).3
MNRI
ug/L
81%
33- 145
6073897
07/25/06 19:12
Anthraccne
50.0
47.5
MNRI
uglL
95%
27 - 133
6073897
07/25/06 19:12
Bcnzo(a)anthracene
50,0
46.4
MNRI
ug/L
93%
.33-143
6073897
07/25106 19;12
Benzo (a) pyrene
50.0
51.6
MNRI
ug1L
103%
17 - 163
6073997
07/25/06 19:12
Beuzu(b) fluoranthene
SO,O
12A
MNRI
ugll,
105%
24 - 159
6073897
07/25/06 19:12
Benzo (g,hj)lmylene
50.0
44.3
MNRI
uglL
89%
1-219
607.1897
07/25/06 19:12
Benzo (k) lluoranihene
50.0
41.0
MNR I
ug/L
82%
It - 162
6073897
07/25/06 19:12
4-Bmmophenyl phenyl ether
5O.0
40A
MNRI
ug/L
81%
53 - 127
6073897
07/25/06 19:12
Butyl benzy] phthalate
$0.0
46.8
MNR l
uglL
94%
1- 152
6073897
07/25106 19:12
4-Chloro-3-mcdrylphenol
50.0
35.7
MNRI
ugll,
71%
22- 147
6073897
07/25/06 19:12
Bis(2-chlotmtlroxy)mc8tail e
50.0
40.7
MNR[
siglL
81%
33- 184
6073897
07/25/06 19:12
1is(2-cldoscethy1)e1her
50.0
42.0
MNRI
uglL
84%
12-158
6073897
071251D6 19:12
Bis(2-chloroisopropy))ether
50.0
44.5
AgNRI
nldL
89%
36- 166
6073897
07/25/06 19A2
2-Chloronaphthalene
50.0
42.2
1<9Nit I
ug./L
84 %
60 - its
6073897
07/25/06 19:12
2-0110rophcnol
50.0
',T6
MNRI
ug/L
75%
2 3 - 134
6073897
07/25/06 19:12
Page 12 of 22

Testl�merica
ANALYTICAL TESTING,, CORPORATION 2960 Foster Creighton Road Nashville, TN 37204.800-765.0980 - Fax [phone]
Client WRS (3166)
221 Hobbs Street, Suite 108
'ramps, FL 33619
Attu Greg Garrison
Work Order:
Project Name:
Project Number.
Received'
NPG2609
Synthron Chemical RUSI4
US EPA Region 4 - Synthron Chemical Fire(106150
07/21/0608:00
PROJECT
QUAIATY CONTROL DATA
LCS -
Conl.
Target
Analyzed
Analyte
.... ............... ....... . .. ..
Known Val.
.. .
Analyzed Val
-
Q
- .. ...
Units
...................-....................._..--
% Rec.
Range
Batch
Dattrrime,
......
Acid and Base/Neutral Extraclables by
EPA Method 625
6073897-BSI
4-Chlorophenylpbenylerher
50.0
42.7
MNRI
ug/L
85%
25-158
6073897
07/25/06 19:12
Chrysenc
50,0
433
MNRI
ug/L
86%
17- 168
6073897
07/25/06 19:12
Dibettz (a-h) anthracene
%D
48.5
MNRI
ug/L
97%
1 - 227
6073897
07/25106 19:12
Di-n-huryl phthalate
50,0
48.2
MNRI
ug)L
96%
1- 118
6073897
07/25/06 19:12
0-Dichlorobenzene
50.0
38.7
MNRI
ug/L
77%
1-172
60733897
07/25/06 19:12
1,4-Dichlorobenzcne
50.0
39.4
MNRI
ug/L
79%
20- 124
6073897
07/25/06 19:12
1,2-Dicldorobenzene
50.5
41.8
N1NR1
ug1L
83%
32-129
6073897
07/25/06 19:12
3,3'-Dichtorobenzidine
50.0
47.7
MNRI
ug/L
95%
1 - 262
6073897
07/25/06 19:12
2,4-Dich1orophenol
50.0
36.9
MNRI
ug l-
74%
39 - 135
6073897
07125/06 19:12
Diethyl phthalate
50.0
37.0
MNRI
ug1L
74%
1- 114
6073897
07/25/06 M12
2,4-Dimethylphenol
50.0
31A
MNRI
ug/L
64%
32-I19
6073897
07/25/06 19:12
Ditnethyl phthalate
50.0
22,6
hINRI
ug7L
45%
1- 112
6073897
07/25/06 19:12
4,6-Dinitro-2-n1eihylphcnol
50.0
42.2
A1NR1
ug/L
84%
1- 181
6073897
07/25/06 19:12
2.4-Dinitrophenol
50.0
2T8
MNRI
ug/L
56%
1- 191
6073897
07/25/06 19:12
2,6-Dinitrotaluene
50.0
47.5
,\-INRI
ug/L
95%
50- 158
6073997
07125106 19:12
2,4-Dinitrotaluene
50.0
47.6
MNRI
ug/L
95%
39- 139
6073897
07/25/06 19:12
Di-n-aclylphthalate
50.0
52,7
MNKI
ug/L
105%
4- 146
6073897
07/25/06 1%12
Bis(2-elhylhexyl)phthalate
50.0
52.2
MNRI
ug/L
104%
8- 158
6073897
07/251D6 t9:12
Fluoranthenc
50.0
47.1
MNRI
ugIL
94%
26- 137
6073897
07/25/06 19:12
Fluorenc
50.0
42.7
MNR I
ug/L
85%
59 - 121
6073897
07/25106 19:12
Hexachlorobcnzcnc
50.0
45.0
%1NR1
ug)L
90%
1- 152
6073897
07/25/06 19:12
Hexachlorobutadiene
50.0
36,4
NINR1
ug/L
73%
24-110
6073897
07/25/06 19:12
Hexachlorocyclopentadiene
50.0
36.4
MNRI
vWL
73%
23 - 86
6073997
07/25/06 19:12
Hexachlorocthane
50.0
38.3
MNRI
ug/L
77%
40 - 113
6073897
07/25/06 19:12
Indeno (1,2.3-cd) pyrene
50.0
46,7
MNRI
ug/L
93%
1- 171
6073897
07/25/06 19:12
Isophorone
50.0
4L5
MNRI
ug1L
83%
21 - 196
6073897
07/25/06 19:12
Naphthalene
50.0
35.3
MNRI
ugIL
7l %
21- 133
6073897
07/25/06 19:12
Nitrobenzene
50.0
39.2
MNRI
uglL
76%
35-180
6073897
07/25/06 19:12
2-A'itrophenol
50.0
39.2
MNRI
ugll,
76%
29-182
6073897
07125/06 19:12
4-Nitrophenol
50.0
16-5
MNRI
ug/L
33%
1. 132
6073897
07/25/06 19:12
N-Mirosodintedtylatnine
50-0
23.6
MNRI
ug11-
47%
23-69
6073897
07/25/06 19:12
N-Nirrosodiphcnylamine
50.0
70.2
L. MNRI
ug1L
140%
42- Ill
6073897
07/25/06 19:12
N-Nitrosodi-n-propylamine
50.0
46.2
MNRI
uWL
92%
1 - 230
6073897
07/25/06 19:12
Pentachlaropltcnol
50.0
53.1
MNRI
ag/L
106%
14- 176
6073897
07/25/06 19:12
Phenanthrene
50A
44.4
MNRI
ug/L
89%
54- 120
6073897
07/25/06 19:12
Phenol
5U.0
20.3
MNRI
ug/L
41%
5- 112
6073897
07/25/06 19;12
Pyrcne
50,0
45.8
MNRI
tg/L
92%
52- 115
6073897
07/25/06 19:12
1,44-Trichlorobenzenc
50.0
36.4
MNRI
ug/L
73%
44- 142
6073897
07/25/06 19:12
2,4,6-Trichlorophenol
50.0
42.0
MNRI
ug/L
84%
37- 144
6073897
07/25/06 19:12
Benzidine
50,0
21.3
MNRI
ug/L
43%
1- l22
6073897
07/23/06 19:12
I,2-Diphcnylhydrazine
50,D
47.9
MNRI
ug11-
86%
47- 117
073897
07/25/06 19:12
Page 13 of 22

TestAimerica
ANALYTICAL TESTINGCORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Atm Greg Garrison
2960 Foster Creighton Road Nashville, Thl 37204 ' 800-765-0980' Fax 615-72&3404
Work Order:
NPG2609
Project Name:
Synthron Chemical RUSH
Project Number:
US EPA Region 4 - Synthron Chemical Firel106150
Received:
07121/06 08:00
PROJECT
QUALITY CONTROL DATA
LCS - Cont.
Target
Analyzed
Analyte
Known Val, Analyzed Val Q Units
%Rec-
Range
Batch
Date/Tirne
Acid and Base/Neutral Extractables by
E1'A Method 62-5
6073897-BS 1
2-Methylnaphthalenc
50,0
39.0 NINR I uWL
78%
34 - 110
6073897
07/25106 19:12
Surrei ale: Terphenyl-d1J
50.2
42.2
84%
34 - 116
6073897
07/25/06 19:12
Surrogate: 2,4,6-Trihramophened
50.2
43.5
87%
16- 130
6073897
07/25106 19:12
Surroxaie; Phened-dS
50.2
16.6
33%
10 - 66
6073997
07125106 19:12
Surr igale: 2-Fhxrrohiphenyl
50.2
37.4
75 %
32 - 99
6073897
07/25/06 19:12
Surrcrgaie: 2-1-1ouniphenol
50.2
21.3
42 %
10 - 81
6073897
07125/06 19:12
Surrogate; Xanihen.ene-d5
50.2
34.6
69"/
19 - 116
6073897
07125/06 19:12
Page 14 of 22

TestLmerica
ANALYTICAL TESTING CORPORATION 2960 Foster Creighton Road Nashville, TN 37204' 800-765-0990' Fax [phone]
Client WRS (3166) Work Order: NPG2609
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Pampa, FL 33619 Project Number: US EPA Region 4 - Synthron Chemical Fire/106150
Alin Greg Garrison Received; 07/21/06 08:00
PRO.IECI' QUALITY CONTROL DATA
LCS Dup
Analytc
General Chemistry Parameters
6073832•BSD1
BOD - 5 Day
ROD - 5 Day
6073835-BSD1
Total Suspended Solids
Total Metals by EPA Method 6010B
6074122-BSD1
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Spike Target Swuple Analyzed
Orig. Val. Duplicate Q Units Conc %Rec. Range RPD Limit Batch Duplicated Date/Time
198 uglntL 199 1011% 85 -113 5 20 6073,832 07126I06 22:30
198 uc/mL 198 1Ut)% 85-115 5 20 6073832 0712610622:30
106 tng1L 100 106 % 90 - 110 9 20 6073835 07/21/06 19:01
0.0524
nrgJL
0.0500
105°5
SO- 120
2
20
6074122
07124/06 16: 14
2.06
mg1L
200
10 3%
80 - 120
0.5
20
6074122
07/24/06 16:14
0.0518
ntg1L
0.050D
104 %
SO- 120
0.4
20
6074122
07124106 16:14
0.195
mg/L
0.200
97%
80 - 120
0.5
20
6074122
07/24/06 16:14
0.0508
mglL
00500
102 %
80 - 120
0.6
20
6074122
07/24/06 16:14
0.0549
mgJL
00500
110%
80- 120
4
20
6074122
07/24/06 16:14
0.0532
mg1L
00500
106 %
80 - 120
2
20
6074122
07/24/06 16:14
Mercury by EPA Nlcthuds 7470A/7471A
6074086-BSD1
Mercury 0 001 15
Acid and Base/Neutral Extractahles by EPA Method 62-
6073897-BS D1
Acenaphthene
40.2
Acenaphthylene
37.3
Anthracene
42.6
Benzo (a) anilimcene
42.5
Benza (a) pyrene
44.4
Benzo(b) Buoranlhene
42,5
Benzo (g,h,i) pcoylene
37.4
Benzo (k) tluoranthene
3U
4-Bromophenyl phenyl ether
36.3
Butyl benzyl phthalate
440
4-Chloro•3-1tethylphenol
33.8
Bis(2-chloroelhoxy)ntethmre
325
Bis(2-chloroethyl)e1her
38.7
Bis(2-chloroisopropy))ether
41.2
2-Chloronaphth ileac
39.4
2-Cltloroplrcnal
34.0
4-Chlorophenylphenylelher
39.6
Cluysene
40.5
Dibenz (a,h) awltmcene
41.4
ntgJL 0.00100 1 15 % 78 - 124 6 22 6074086 07/26/06 13:07
tig/L
50,0
80%
47. 145
6
41
6073897
07/25/06
19:39
ug/L
50.0
75%
33 - 145
10
33
6073897
07/25/06
19:39
og/L
50,0
85 %
27 - 133
11
38
6073897
07125106
M19
ug/L
%0
85%
33 - 143
9
35
6073897
07/25/06
19:39
„%/L
Soo
89%
17- 163
15
37
6073897
07/25106
19:39
ttg1L
50.0
85%
24 - 159
21
37
6073897
07125106
19:39
%t�JL
Soo
75 %
1 - 219
17
36
6073897
07/25100
1939
110,
Soo
78%
11 - 162
4
40
6073897
07/25/06
M39
ugrL
50.0
73%
53 - L27
11
35
6073897
07/25/06
1939
mlL
50 0
88 %
1. 152
G
37
6073897
07/25/06
0:39
ug/L
50.0
6H%
22- 147
5
38
6073997
07/25/06
19:39
ug/L
S0_o
79°/
33 - 184
-,
34
6073897
07/25/06
19;39
ug/L
50.0
77%
12 - 159
8
44
6073997
07/25/06
19:39
ng�L
50.0
82%
36- 166
8
40
6073897
07/25/06
19:39
ug/L
50.0
79%
60 - 119
7
41
6073997
07/25/06
19:39
uglL
500
69%
23 • 134
l0
59
6073997
07/25/06
19:39
ug/L
50.0
799/6
25 - 159
8
38
6073897
07/25/06
19:39
rig/L
50.0
81 %
17- 168
6
35
6073997
07/25/06
19:39
„g/l,
50.0
83 %
I - 227
16
41
6073997
07/25/06
19:39
Page 15 of 22

TestAmerica
ANALYTICAL TEST04G CORPORATION 2960 Foster Creighton Road Nashville, TN 37204 • BOD-765-0980' Fax [phone]
Client WRS (3166) work Order: NPG2609
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number: US EPA Region 4 - Synthron Chemical Fire/106150
Anri Greg Garrison Received: 07/21106 08:00
PROJECT QUALITY CO\TROL DATA
LCS Dup - Cont.
Spike
Target
8lunple Analyzed
Analyte
Orig. Val. Duplicate Q
Units
Conc % Rec.
Range
RPD Limit
Batch
. ..............
Duplicated Date/Time
.... .........
Acid and Base/Neutral Extractables by
EPA Method 62i
6073897-BSD9
Di-n-butyl phthalate
43.4
ug1L
Soo
87%
1- 118
t0
35
6073897
07/25/06 19:39
I-3-Dichlorobcazeae
34,2
ug/L
50.0
68%
[- 172
12
55
6073897
07/25/06 19;39
IA-Dichlorobenzeae
33.4
ug/L
Soo
67%
20- 124
16
57
6073897
07/25/06 19:39
1,2-Dicttlorobenzene
36,0
ug/L
50.5
71%
32 - 129
15
55
6073897
07125M 19:39
3,3'-Dichlorobenzidine
43.3
uglL
S0.0
87%
1 - 262
t0
44
6073897
071251D6 19:39
2,4-Dichlorophenol
34.2
ug/L
Soo
68%
39.135
8
57
6073897
07/25/06 19:39
Diethyl phthalate
34.0
ug/L
Soo
69%
1- 114
8
38
6073897
07/25/06 19:39
2,4-Ditne1hylphen0l
29.3
ug/L
500
59°/
32 - 119
8
73
6073897
07/25/06 19:39
Dimethyl phthalate
17.9
ug l-
500
36%
1- 112
23
36
6073897
07/25/06 19:39
4,6-Dini1r0-2-me1hylphenol
41.1
ug/L
500
82l
I- IS]
3
59
6073897
07/25/06 19:39
2,4-Dinitrophea0l
3 4, 2
ugll-
500
68%
1- l91
21
35
6073897
07/25106 19:39
2,6-Dinitrotoluene
43.2
ug/L
50.0
96%
50-15S
9
40
6073897
07/25/06 19:39
2,4-Dinitrotoluene
45.0
=ig/L
50.0
90%
39 - 139
6
36
6073897
07/25/06 19:39
Di-n-octyt pluhalaie
46.7
uglL
50.0
93,V.
4- 146
12
44
6073897
07/25/06 19:39
Bis(2-ethylhesy1)plahaIaIe
45.6
ug/L
Soo
91 %
9- 158
13
37
6073897
07/25/06 19:39
Fluoranlhene
42.4
ug/L
50,0
85%
26 - 137
11
34
6073897
07/25/06 19:39
Fluorene
39.4
uglL
50,0
791/6
59- 121
8
36
6073897
07/25/06 19:39
Hexadtlorobenzene
41.1
ugll-
Soo
82%
1 - 152
9
34
6073897
07/25/06 19:39
Hexachlorobti adienc
33.0
ug/L
500
66%
24 • 116
10
55
6073897
07/25/06 1939
Hexachlorocyctopenladiene
32.7
ug/L
50.0
65%
23 - 86
11
55
6073897
07/25/06 19:39
Hexachloroethnne
34.4
ugll.
500
69%
40-113
11
59
6073897
07/25/06 19:39
Indeim (1.2,3-ed) pyrene
39.5
ug/l.
50,0
79%
1 • 171
l7
41
6073897
07/25/06 19:39
Isophorone
39.3
ug1L
50.0
7W/6
21.196
5
33
6073897
07/25/06 1939
Naphthalene
30.7
ug1L
50.0
61%
21 - 133
14
44
6073897
07/25/06 19:39
Nilrobcnzene
32.6
ug/L
500
65%
35- ISO
l6
35
6073997
07/25/06 19:39
2-Nitrophenul
36,0
ugJL
50.0
72%
29 - 182
6
55
6073997
07/25/06 19:39
4-Nitrophenot
15.2
ug1L
500
30%
1- 132
8
48
6073897
07/25/06 19:39
N-Nilrosodimeshylamine
20,0
ug/L
50.0
40%
23 - 69
17
51
6073897
07/25/06 19:39
N-Nitrosodiphcnylanine
63,1 L
ug/L
50,a
126%
42 - 1 l I
11
32
6073897
07/25/06 19:39
N.Nitrosodi-a-propylatniae
410
ug/L
500
82%
1-230
12
47
6073897
07/25/06 19:39
Pentachlorophenal
47.4
ug/L
50.0
95%
14 - 176
11
47
6073897
07/25/06 19:39
Phenaathrene
40.8
uglL
509
82%
54 . 120
8
39
6073997
07/25/06 19:39
Phenol
17.5
ug/L
500
35%
5 • 112
15
54
6073897
07/25/06 19:39
Pyrene
41.7
ug/L
50.0
830%
52 - 115
9
35
6073897
07/25106 19:39
1,2,4-Trichlorobenzenc
31.8
ug1L
50.0
64%
44 - 142
13
50
6073897
07/25/06 19:39
2,4,6-Trichlorophenot
40.3
ug/L
50.0
81 %
"+7 - L44
4
62
6073897
07/25/06 19:39
Bepzidine
ND L2
ug1L
50.0
0%
1 - 122
85
6073897
07/25/06 19:39
1,2-Diphenylhydrazitic
41.6
ug/L
50.0
83%
47-117
3
36
6073897
07/25/06 19:39
2-Methy1naphthrilene
,S.4
ug1L
Soo
71%
34 - 110
10
41
6073897
07/25/06 19:39
Nurrogeire: 'Perpherryd-dI4
40.2
ug/L
50.2
80%
34 - 116
6073897
071251D6 19:39
.SurreiKrnc: 1.4, 6-Trihraruophenol
40.6
kitA
50.2
81 %
16 - 130
6073897
071251D6 19:39
Page 16 of 22

Test,A-merica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 ' BOD-785-0960 " Fax [phone]
Client WRS (3166) Work Order: NPG2609
221 Hobbs Street, Suite 108 Project Name- Synthron Chemical RUSH
Tampa, FL 33619 Project Number: US EPA Region 4 - Synthron Chemical FireA06150
Atm Greg Garrison Received: 07/21/06 09:00
I'ROJEC'I' QLIAI.fI'1' CON'I'ROI. DATA
I.CS Dup - Cont.
Spike 'rarget Sample Analyzed
Analyte Orig. Val. Duplicate p Units Cone %Rec. Range RPD Limit Bntch Duplicated Daterrime
Acid and Base/Neutral Extractables by EPA Alctliod 625)
6073897-BSD1
Surmguae, Phunn1-d5 14.7
Sara, ate. 2-1.7unmhiphenyl 35.9
Surrogate: 2-Muumphenol 199
Surrogate.- Nivahen_ene-d5 31.9
116A.
50.2
29%
10 - 66
6073897
07/25/06 19:39
ug1L
50.2
72 %
32 - 99
6073897
07/25/06 19:39
uglL
50.2
40%
10 - 81
6073897
07/25/06 19:39
ugil-
50.2
64%
19- 116
6073897
07/25/06 19:39
Page 17 of 22

0
TestAimerica
ANALYTICAL TESTING CORPORATION!
2960 Foster Creighton Road Nashville, TN 37204 ' B00.765-0980' Fax [phone]
Client WRS (3166) Work Order: NPG2609
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number: US EPA Region 4 - Synthron Chemical Fire/106150
Ann Greg Garrison Received: 07121106 08:00
PROJECT QUALITY CONTROL DATA
Nlatrix Spike
Target Sample Analyzed
Auatyte Orig. Val. MS Val Q Units Spike Conc %Rec. Range Batch Spiked Dalerrime
. ....-...--
General Chemistry Parameter
6073730-MS1
Chemical Oxygen Demand
Total Nletals by EPA Nlethod 6010B
6074122-M S 1
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
28,9 72,9 MR ug/mL 50,0 88% 90-110 6073730 NPG2326-01 07/21/06 12:14
0.00620
0.0596
mglL
0.0500
0.212
2.31
mg1L
2.00
0.000700
0.0519
mg/L
0.0500
0,00170
0.195
mttJL
0.200
ND
0.0515
m81L
0,0500
NI)
0.0555
mg/L
(10500
ND
0.059
mg/L
0.0500
107%
75- 125
6074122
105%
75-125
6074122
102%
75. 125
6074122
97 %
75 - 125
6074122
103%
75 - 125
6074122
111%
75 - 125
6074122
1 12 %
75 • 125
6074122
N P G 2 5 90-01
0 7/ 24 /06 l 6: 2 8
NPG2390-01
07124106 W28
NPG2590-01
07124106 16:28
NPG2390-01
07/24106 16:28
NPG2590-01
07/24/06 W28
NPG2590-01
07/24106 16:28
NPG2590-01
07124106 W28
Mercury by EPA Methods 7470A17471A
6074086-MS1
Mercury 0.000251 0.00113 nlg1L 0.00100 89% 63- 138 6074086 NPG2590-01 07/26/06 13:11
Purgeable Organic Compounds by EPA Mcthod 624
6074013-MS1
Acrolein
ND
Acrylonitrile
ND
Benzene
ND
Broluodichloratnethmte
ND
Bromofonn
ND
Bromomethane
ND
Carton Tetrachloride
ND
Chlorobenzene
ND
Chlorodibrotnomcthane
ND
Chloroethane
ND
Chlorofonn
ND
Chloromethaic
ND
1,2-Dichlorobenzcne
ND
1,4-Dichlorobcizene
N 1)
1,3-Dichtowbenzene
ND
Dicldorodiiluoromethane
ND
I ,2-Dichloroelhnne
ND
1,1-Dichloraethane
ND
cis-1,2-Dichloroelltene
ND
trans- 1,2-Dichloraethene
N D
330
ug1L
250
132%
L9- L96
6074013
226
ug/L
250
90%
73- 132
6074013
5 3.4
uglL
Wo
107 %
37 - 151
6074011
48.9
ug/L
50.0
98%
35- 155
6074013
47.4
ug/L
50.0
95%
45- L69
6074013
61.8
ug/L
50,0
124%
1 - 242
6074013
51.0
ug/L
50,0
102%
70- 140
60740L3
49.6
ug/L
50.0
991/6
37 - 160
6074013
46.8
ug/L
50.0
94%
53 - 149
6074013
61.3
Ug/L
50.0
123%
L4 - 230
6074013
49.7
u61L
50.0
"/a
51 - 138
6074013
43.4
ug/L
50.0
87%
1 - 273
6074013
46,7
ug1L
50.0
9,%
18-190
6074013
46, 1
ug/L
50.0
92%
18 - 190
6074913
47.3
ug/L
50.0
95%
59- 156
6074013
43.7
ug/L
50.0
97%
33 - 142 -
6074013
43A
ug/L
50.0
87%
49- 155
6074013
50,1
ug/L
50.0
100 %
59 - 155
6074013
47A
u1JL
50.0
95%
54 - 156
6074013
50,8
ug)L
50.0
L02%
54. 156
6074013
NPG1923-04
07122/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07122/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07122/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07/22/06 22:21
NPG1923-04
07122/06 22:21
NPG1923-04
07/22/06 22:21
NPGt923-04
07f22106 22:21
NPG1923-04
07/22/06 22:21
NPG1923.04
07/22/06 22:21
NP01923-04
07/22/06 22:21
NPG1923-04
07/22/06 22:21
NP01923-04
07/22/06 22:21
NPG1923-04
07/22/06 22:21
Page 18 of 22

Testli r .+erica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
AM Greg Garrison
2960 Foster Creighton Road Nashvilte, TN 37204 . 800-766-09W 'Fax [phone]
Work: Order:
NPG2609
Project Name:
Synthron Chemical RUSH
Project Number:
US EPA Region 4 - Synthron Chemical Firell06150
Received:
07/21/06 08M
1r120JE CC QUALI'I.1' CO\7-R0L DATA
Matrix Spike - Cont.
Target Sample Analyzed
Analyze Orig. V11. MS Vol Q Units Spike Conc %Rec. Range Balch Spiked DatelTime
Purgeable Organic Compounds by EPA Method 624
6074013-MS1
1, 1 -Dichloruethene
ND
1,2-Dichloropropone
N D
Cis- 1,3-Dichlorupropene
ND
trans- I,3-❑ichl-propcnc
N D
Ethylbenzene
ND
Methylene Chloride
ND
1,1,2.2-Tetrachlormthane
N D
Tetrachloroethene
N D
Toluene
ND
1,1,2-Trichlaroethane
ND
I,I,1-Trichloroethane
ND
Trichloroetlrcne
N D
TrichloroRuoromcthane
ND
Vinyl chloride
ND
Xylcnes, total
ND
Surnigate: 1. 2-Uich1 orrx theme-d a
Surrol;ate Uihronrnjluurunrrlhum
Surnrgule: Toluene-eAl
Surn+,gaie: 4-14mmo Jluarohvnrene
60.1
uglL
50.0
120%
1 - 234
6074013
NPGi923-04
07/22/06
22:21
50.0
ug ]-
50.0
100%
1 - 210
6074013
NPG 1923-04
07/22106
22:21
40.7
ug11.
50.0
81%
1 - 227
6074013
NPG1923.04
ON22106
22:21
38,7
ug/L
50.0
77%
17-193
607-1013
NPG1923-04
07/22/06
22:21
49.4
ug1L
50.0
99'/•
37 - 162
6074013
NP01923.04
07l22/06
22:21
53,3
uglL
50.0
107%
1 -221
6074013
NPGt923-04
07/22/06
22:21
41.5
uWL
50.0
93°%
46-157
6074013
NPGL923.04
07/22/06
22:21
54,6
uglL
50.0
1091/6
64 - 149
6074013
NPG1923-04
07/22/06
22:21
48.3
ug/L
50-0
97%
47. 150
6074013
NPG1923-04
07/22/06
22:21
46.8
ug1l.
50.0
94%
52-150
6074013
NPGL923.04
07/22/06
22:21
51.5
ug/L
50.0
103%
52 - 162
6074013
NPG1923-04
07/22/06
22:21
57.9
ug11.
50,0
116%
71 - 157
6074013
NPG1923-04
07/22/06
22:21
5.3.G
uglL
50.0
107%
17-181
6074013
NPG1923-04
07/22/06
22:21
53.7
ng/L
50.0
107%
1-251
6074013
NPG1923-04
07/22/06
22:21
15L
uplL
150
101%
80- 125
6074013
NPG1923-04
07/22/06
2211
27.0
ug/L
30.0
90%
8l - 126
6074013
NP01923.04
07/22/06
22:21
31.8
ug/L.
30.0
106%
88-120
6074013
NPG1923-04
07122/0622:21
29,8
ug/L
30.0
99%
85 - 130
6074013
NPG1923-04
07/22/06
22:21
27.2
ug/L
30,0
91%
80. 124
6074013
NPG1923-04
07/22/06
22:21
Page 19 of 22

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Faster Creighton Road Nashville, TN 37204 ' 800-765-0980' Fax [phone]
Client WRS (3166)
Work Order:
NPG2609
221 Hobbs Street, Suite 108
Project Name:
Synthron Chemical RUSH
Tampa, FL 33619
Project Number:
US EPA Region 4 - Synthron Chemical Firetl06150
Ann Greg Garrison
Received:
07/21/06 08:00
I'ROJEC'I- QtIALI'I'1' CONTROL DATA
Matrix Spike Dup
Spike 'Target Sample Analyzed
Analyte Orig. Val. Duplicate Q Units Coic % Rec. Range RPD limit Batch Duplicated DateJTime
General Chemistry Parameters
6073730-MSD1
Chemical Oxygen Demand 28,9 72.5 NB ugltnL Soo 87% 90 - 110 0.6 10 6073730 NPG2326-01 07/21/06 12:14
Total Metals by EPA method 601013
6074122-MSD1
Arsenic
0.00620
0.0579
mg1L
0.0500
103%
75-125
3
20
6074122
NPG2590-01
0712006 16:32
Barium
0.212
2.31
mglL
2.00
105 %
75 - 125
0
20
6074122
NPG2590-01
07/24/06 16:32
Cadmium
0.000700
0.0523
mglL
00500
10'%
75-125
0.8
20
6074122
NPG2590-01
07/24/06 16:32
Chromium
0,00170
0.196
mglL
0.200
97%
75 - 125
0.5
20
6074122
NPG2590-01
07/24/06 16:32
Lead
ND
0.0521
mg1L
0.0500
104%
75 - 125
1
20
6074122
NPG2590.01
07/24/06 16:32
Selenium
ND
0,0562
ntg1L
0.0500
112i6
75 -125
1
20
6074122
NPG2590-01
07/24/06 16:32
Silver
ND
0.0366
mg11-
0.0500
113%
75-125
1
20
6074122
NPG2590-01
07/24/06 16:32
Mercury by EPA Methods 7470A/7471A
6074086-MS D1
I<lercury 0A00251 0.00117 mg/L 0.00100 92% 63-138 3 22 6074096 NlIG2590-01 07/26/06 13:16
Page 20 of 22

TeSty�i merica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 31204' 600-7%-0960' Fax [phone]
Client WRS (3166)
Work Order:
NP62609
221 Hobbs Street, Suite 108
Project Name:
Synthron Chemical RUSH
Tampa, FL 33619
Project Number:
US EPA Region 4 - Synthron Chemical Fire1106150
Attn Greg Garrison
Received'
07/21/06 08:00
CER'I'IF[CA110N
SUMNIIARY
TcstAtnerica - Nashville. 'l'N
Method Matrix
AIHA
Nelac
North Carolina
EPA 160.2 Water
NIA
X
X
EPA 405.1 Water
NIA
X
X
EPA 410.4 Water
NIA
X
X
FPA 624 Water
NIA
X
X
EPA 625 Water
NIA
X
X
SM 5210B Water
NIA
X
X
SW8460010B Water
NIA
X
X
SW846 7470A Water
NIA
X
X
Page 21 of 22

TestAmerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
'Pampa, FL 33619
Aun Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204 ' 800-765-0980' Fax [phone]
Work Order: NPG2009
Project Name: Synthron Chemical RUSH
Project Number: US EPA Region 4 - Synthron Chemical Fire/106150
Received: 07/21/06 08:00
DATA QUALIFIERS AND DEFINITIONS
< Result is less than the stated value.
L Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the acceptance limits. Analyte not
detected, data not impacted.
L2 Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was below acceptance limits.
1%18 The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS)-
MNR1 There was no MS/MSD analyzed with this batch due to insufficient sample volume. See Blank Spike.
METHOD MODIFICATION NOTES
COD 410.4 M - M = COD method modified for use of Hach method 8000.
Page 22 of 22

TestAmerica, 07/2810616:00 07/28/0616:00
ANAtYTI UI iES11NG CpppOpATION 1
Nashville Division
COOLER IMCETPT FORM BC#
NPG2609
Cooler Received/Opened On 7121/06 _8:00
1. Indicate [lie Airbill Tracldng Number (last 4 digits for hedex only) and lame of Courier below: L/
Fed-1G UPS Velocity DHL Route Off-street Misc.
r Q
2. Temperature of representative sample or temperature blank when opened: - I Degrees Celsius
(indicate IR Gun IDit)
NA A00466 A00750 AO1124 100190 10I282
102594
3. Were custody seals on outside of cooler%...........................................................................
)0 .... NO .... NA
j
If how f'�0i C
a. yes, many and where: _ I " -
4. Were the seals inlact, signed, and dated correctly?.............................................................
&... NO ... NA
5. Were custody papers inside cooler?................................................................................
j!qS....NO...NA
1 certify that 1 o ened the cooler and answered queslirins 1-5 intinl............................ I.................
xz"
6. Were custody seals an containers: YES W and lutact
YES NO 'AA
were these signed, and dated correctly?......................................................
YES —NO...
7. What kind of packing used? Hu lely . p Peanuts Vermiculite
Foam Insert
gmmaterial
l!a rft'v� Paper Other None:
y
S. Cooling process: Ie/) Ice -pack Ice (direct contact) Dry ice
Other None
9. Did till containers arrive in good condition f unbroken)? ......................... --............ ............. .......
..N0... NA
10. Were all container labels complete (#, date, signed, pres., etc)? ........ ....................................
S...NO... NA
11. Did all contaiitter labels and tags agree with custody papers? ................................................
7 CS...NO...NA
} 12. a. Were VOA vials received?... ...................................................................................
i
YES ... NO...NA
b. Was there any observable head splice present hiany VOA vial? ................................................
YES..& ... NA
1 eertify that I unloaded the cooler and answered questions 6-12r(fntinh.....................................
13. :t. On preserved bottles did the p1-1 test strips suggest that preservation reached the correct pH level?
4V..NO.. q('T ,
04
b. Did the bottle labels indicate that the correct preservatives were used ......................
1�..,NO.,.NA
If preservation in-house was needed, record standard 11) of preservative used here
14. Was residual chlorine present?........................................................................................
YES..*D... NA
1 certify that I checked for chlorine and oli,,is per SOP surd answered uuestions 13-14 fintiall.........
i15. Were custody papers properly filled out (ink, signed, etc)? .................................................
I. 16. Did you sign the custody papers in the appropriate place?...........
NO NA
ff NO ... NA
17. Were correct containers used for the analysis requested? ...................................................
NO ... NA
18. Was sufficient amount of sample sent in each contaiacr?.....................................................
... NO ... NA
I certify that I entered this proiect into LIMS and answered questions 15-18 fintial).......................
-TL.—
I certify that 1 attached a label with the unique LIMS number to each container (iutial)...................
_
19. Were there Non-Coufortuance issues tit login YES 9 Was a PIPE generated YES
NO #
BIS = Broken in shipment
Cooler Receipt Form LF-1
Revised 319/06
End of Form

Testj�,mericar
Client N" %.11 l� s Client* 3 1 ao G
Address:_ Zz.l 9
CitylStot67ip Code: 7a _ - iG . . r 9 �
Prood Manager f'tw G^-- _..1•
Telephone Nu~. $z9 Y3 � �$ff� - — Fax.—Z4_'$f37
i'nnt Name}" V IZp
Satnp�er Nerve: t
Sampler Signature:
ut�tr;Y arnearvation s # of Contain
To easiat us in v*kV Me proper and fiethods,
ig'hia *Vl* beiflq conducted for mgukbry lw ?
Compliance MonAodng
Project Name: U.S E :arj y
Project #:---
Site/Location ID:
Report To: — t jl�•S a Ld �1
Invoke To: $
Quote #: PO#: `f 4 1 jQ Z
fAiStandard �14 L
1 1
$ '
l .
read rolaf PA 010 Mercury
To
5da)
W
o'
Selenium Total EPA b^Silv�r
d
J
f Rush {surcharges may apply}
y
4
.:
N y
Pl'77•' `%•
C
cn o
Dote Needed: ��
L)
e y 1
S1)
it
�r
d N
p
rn `�
iL
.2
y3
°x
"
SAMPLE ID
1
�S
(7�itti'T 07Z"--
�g$c►I�S �� qp G 7Caalto'
Spec1�11mtructlons: a�Mur' �
C# to TA L--
-I. Zd I6 c C:
Bale: Time:
Date: Tlme:
#? -Time'. -
ry�f
_' None -
.4
Level
1
Level 3
Level 4
o
Other:
�
r
J REIAP.Kn�
LABORATORY COMMENTS:
Init Lab Temp:
Rec Lab Temp:
Date: —'rime! Custody Seals: Y N N/A
Bottles Supplied by Test America: Y N
Date: Time:
Method of Shipment:

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-07
Project: Synthron Inc.
Collection Date: 5/11/2006
8:15:00
AM
Lab ID: 0605766-001
Matrix: SURFACE
WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchlD
Dilution
Factor
Date Analvzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW35108)
Analyst: MM
4,4'-DDD
BRL
0.10
pg/L
70940
1
5/15/2006 9:26 PM
4,4'-DDE
BRL
0.10
pg1L
70840
1
5/15/2006 9:26 PM
4,4'-DDT
BRL
010
pg11-
70840
1
5/15/2006 9:26 PM
Aldrin
SRL
0.050
pglt
70B40
1
5115/2006 9:26 PM
alpha-BHC
BRL
0.050
pg/L
70940
1
5/15/2006 9:26 PM
alpha -Chlordane
BRL
0.050
pg1L
70840
1
5/15/2006 9:26 PM
beta-BHC
BRL
0.050
pg/L
70940
1
5/15/2006 9:26 PM
delta-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 9:26 PM
Dieldrin
BRL
0.10
pg/L
70840
1
5/15/2006 9:26 PM
Endosulfan I
BRL
0.050
pg1L
70840
1
5115/2006 9:26 PM
Endosulfan 11
BRL
0.10
pg1L
7OB40
1
5115/2006 9:26 PM
Endosulfan sulfate
BRL
0.10
pg/L
70840
1
5/15/2006 9:26 PM
Endrin
BRL
0.10
pg1L
70B40
1
5/15/2006 9:26 PM
Endrin aldehyde
BRL
0.10
pg/L
70840
1
5/15/2006 9:26 PM
Endrin ketone
BRL
0.10
pg1L
70940
1
5/15/2006 9:26 PM
gamma-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 9:26 PM
gamma -Chlordane
BRL
0.050
pg1L
70B40
1
5/15/2006 9:26 PM
Heptachlor
BRL
0.050
pg/L
70840
1
5/15/2006 9:26 PM
Heptachlor epoxide
BRL
0.050
p91L
70840
1
5/15/2006 9:26 PM .
Mothoxychlor
BRL
0.50
pg/L
70840
1
5/15/2006 9:26 PM
Toxaphene
BRL
5.0
p91L
70840
1
5/15/2006 9:26 PM
Surr: aecachlorobiphenyl
21.1
17.9-122
%REC
70840
1
5/15/2006 9.26 PM
Surr: Tetrachloro-m-xylene
107
18.9-119
%REC
70840
1
5/15/2006 9:26 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
4.79
0.200
mg1L
70835
1
5/15/2006 5:02 PM
Antimony
0.0770
0.0200
mg1L
70835
1
5/1512006 5:02 PM
Arsenic
BRL
0.0500
mg/L
70835
1
5/15/2006 5:02 PM
Barium
0.0405
0.0200
mg1L
70835
1
5/1512006 5:02 PM
Beryllium
BRL
0.0100
mg/L
70835
1
5/15/2006 5:02 PM
Cadmium
BRL
0.0050
mg/L
70835
1
5/15/2006 5:02 PM
Calcium
18.7
0.100
mg/L
70835
1
5115/2006 5i02 PM
Chromium
0.0254
0.0100
mg1L
70835
1
5/15/2006 5:02 PM
Cobalt
BRL
0.0200
mg1L
70835
1
5/15/2006 5:02 PM
Copper
0.0827
0.0100
mg/L
70835
1
5/1512006 5:02 PM
Iron
8.53
.0.100
mg/L
70835
1
5115/2006 5:02 PM
Lead
0.0560
0.0100
mg1L
70835
1
5/1512006 5:02 PM
Magnesium
3.08
0.100
mg1L
70835
1
5/1512006 5:02 PM
Manganese
0.419
0.0050
mg/L
70835
1
5/15/2006 5:02 PM
Molybdenum
BRL
0.0500
mg/L
70835
1
5/1S/2006 5:02 PM
Mickel
0.0367
0,0200
mg/L
70835
1
5/15/2006 5:02 PM
Potassium
T27
0.500
mglL
70835
1
5/1512006 5:02 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
tl Holding times for preparation or analysis exceeded
N Analyze not NELAC certified
B Analyze detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 1 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-07
Project: Synthron Inc.
Collection Date: 5/11/2006
8:15:00
AM
Lab ID: 0605766-001
Matrix: SURFACE
WATER
Analyses
Result
Reporting Qual
Units
BatchlD
Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg/L
70835
1
5/15/2006 5:02 PM
Silver
BRL
0.0100
mg/L
70835
1
5/15/2006 5:02 PM
Sodium
42.5
1.00
mg/L
70835
1
5/15/2006 5:02 PM
Thallium
BRL
0.0200
mg/L
70835
1
5/15/2006 5:02 PM
Tin
0.0896
0.0500
mg/L
70835
1
5/15/2006 5:02 PM
Titanium
0.253
0.0500
mg/L
70835
1
5/15/2006 5:02 PM
Vanadium
0.0448
0.0100
mg/L
70835
1
5/15/2006 5:02 PM
Zinc
2.27
0.0200
mg/L
70835
1
5/15/2006 5:02 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0.00020
mg/L
70883
1
5/16/2006 2:30 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2,4,5-Trichlorophenol
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
2,4,6-Trichlorophenol
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2,4-Dichlorophenol
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2,4-Dimethylphenol
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2,4-Dinitrophenol
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
2,4-Dinitrotoluene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
2,6-Dinitrotoluene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2-Chloronaphthalone
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2-Chlorophenol
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
2-Methylnaphthalene
BRL
10
pg/L
70832
1
5115/2006 7:06 PM
2-Methylphenol
BRL
10
pg1L
70832
1
5/15/2006 T.06 PM
2-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 7:05 PM
2-Nitrophenol
BRL
10
pg/L
70832
1
5/16/2006 7:06 PM
3,3'-Dichlorobenzidine
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
3-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 7:06 PM
4,6-Dinitro-2-methylphenol
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
4-Bromophenyl phenyl ether
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
4-Chloro-3-methylphenol
BRL
10
pg/L
70832
1
5/15/2006 T.06 PM
4-Chloroaniline
BRL
10
pg/L
70832
1
5/15/2006 T06 PM
4-Chlorophenyi phenyl ether
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
4-Methylphenol
66
10
pg/L
70B32
1
5/15/2006 7:06 PM
4-Nitroaniline
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
4-Nitrophenol
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
Acenaphthene
BRL
10
pg/L
70B32
1
5/15/2006 7:06 PM
Acenaphthylene
BRL
10
pg/L
7OB32
1
5/15/2006 7:06 PM
Acetophenone
BRL
10
pg/L
70B32
1
5/15/2006 7:06 PM
Anthracene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Atrazine
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 2 of 30

F/
Analytical Environmental Services, Inc.
Date: 22-Mav-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-07
Project: Synthron Inc.
Collection Date: 5/11/2006 8:15:00
AM
Lab 1D: 0605766-001
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
QuaI Units
BatcblD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
10
pglL
70832
1
5/1512006 7:06 PM
Benzaldehyde
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Benzo(a)pyrene
BRL
10
pg1L
70832
1
5115/2006 7:06 PM
Senzo(b)fluoranthene
BRL
10
pglL
70B32
1
511512006 7:06 PM
Benzo(g,W)perylene
BRL
10
pglL
70B32
1
5/15/2006 7:06 PM
Benzo(k)fluoranthene
BRL
10
pg1L
70832
1
511512006 7:06 PM
Bis(2-chloroethoxy)methane
BRL
10
pglL.
70832
1
5/1512006 7:06 PM
Bis(2-chloroethyl)ether
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Bis(2-chloroisopropyl)ether
BRL
10
pg/L
70832
1
511512006 7;06 PM
Bis(2-ethylhexyl)phthalate
22
10
pg1L
70832
1
5/15/2006 7:06 PM
Butyl benzyl phthalate
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Caprolactam
BRL
10
pg/L
70832
1
5/1512006 7:06 PM
Carbazole
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Chrysene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Dibenz(a,h)anthracene
BRL
10
pglL
70832
1
5/1512006 7:06 PM
Dibenzofuran
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Diethyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 T06 PM
Dimethyl phthalate
BRL
10
pglL
70B32
1
5/15/2006 T06 PM
Di-n-butyl phthalate
BRL
10
µg1L
70832
1
5/1512006 7:06 PM
Di-n-octyl phthalate
BRL
10
pglL
70832
1
5/1512006 T06 PM
Fluoranthene
BRL
10
pg1L
70832
1
5115/2006 7:06 PM
Fluorene
BRL
10
pglL
70832
1
5115/2006 7:06 PM
Hexachlorobenzene
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Hexachlorobutadiene
BRL
10
pg1L
70832
4
5/1512006 7:06 PM
Hexachlorocyclopentadiene
BRL
10
pglL
70832
1
511512006 7:06 PM
Hexachloroethane
BRL
10
pglL
70832
1
5/15/2006 T06 PM
Ind eno(1,2,3-cd)pyrene
BRL
10
pglL
70832
1
5115/2006 7:06 PM
Isophorone
BRL
10
pglL
70632
1
5/1512006 7:06 PM
Naphthalene
BRL
10
pglL
70832
1
5115/2006 7:06 PM
Nitrobenzene
BRL
10
pglL
70832
1
5/1512006 7:06 PM
N-Nitrosodi-n-propylamine
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
N-Nitrosodiphenylarnine
BRL
10
µglL
70832
1
511512006 7:06 PM
Pentachlorophenol
BRL
25
pglL
70832
1
5/1512006 7:06 PM
Phenanthrene
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Phenol
36
10
pglL
70832
1
511512006 7:06 PM
Pyrene
BRL
10
pglL
70832
1
5/1512006 T06 PM
Surr: 2,4,6-THbromophenol
68.8
64.8-129
%REC
70832
1
6115/2006 7:06 PM
Surr: 2-Fluorobiphenyl
68.8
58.2-115
%REC
70832
1
5/1512006 T.06 PM
Surr: 2-Fluorophenol
56.6
24.4-115
%REC
70832
1
5/15/2006 7:06 PM
Surr: 4-Terphenyl-d14
60A
58.3-115
%REC
70B32
1
5/1512006 7:06 PM
Sum Nitrobenzene-d5
64.2
51.8-115
%REC
70832
1
5/15/2006 7:06 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E Estimated (Value above quantitation range)
BRL Below Reporting Limit
S Surrogate
Recovery outside accepted rccovcfy limits
H Holding times for preparation or analysis exceeded
Narr Sec Case Narrative
N Analyte not NELAC certified
NC Not
Confirmed
B Analyte detected in the associated Method
Blank
Page 3 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client
Sample ID: FT-07
Project: Synthron Inc.
Collection
Date: 5/1
1/2006 8:15:00
AM
Lab ID: 0605766-001
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Units
BatchlD Dilution
Date Analyzed
Limit
Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-dS
53.4
17.9-115
%REC 70832
1
5/15/2006 7:06 PM
TCL VOLATILE OR
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70849
1
511312006 7:28 AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70849
1
511312006 7:28 AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
511312006 7:28 AM
1,1-Dichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70849
1
511312006 7:28 AM
1,2,4-Trichoorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,2-Dichlorobenzene
BRL
5.0
pq/L
70849
1
5/13/2006 7:28 AM
1,2-Dichloroethane
BRL
5.0
pq/L
70849
1
5/13/2006 7:28 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,3-Dichlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
1,4-Dichlorobenzene
BRL
5.0
pq/L
70849
1
5/13/2006 7:28 AM
2-Butanone
BRL
50
pg/L
70849
1
5/13/2006 7:28 AM
2-Hexanone
BRL
10
pg/L
70849
1
5/13/2006 7:28 AM
4-Methyl-2-pentanone
BRL
10
pg/L
70849
1
5/13/2006 7:28 AM
Acetone
110
50
pg/L
70849
1
5/13/2006 7:28 AM
Benzene
BRL
5.0
pg/L
70B49
1
5/13/2006 7:28 AM
Bromodichloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Bromoform
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Bromomethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Carbon disulfide
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Carbon tetrachloride
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Chlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 7:2B AM
Chloroethane
BRL
10
pg/L
70849
1
5/13/2006 7:28 AM
Chloroform
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Chloromethane
BRL
10
pg/L
70849
1
5/13/2006 7:28 AM
cis- 1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
cis- 1,3-Dichloropropene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Cyclohexane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Dibromochloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Dichlorodifluoromethane
BRL
10
pg/L
70849
1
5/13/2006 728 AM
Ethylbenzene
BRL
5.0
pg/L
70849
1
5/13/2006 T.28 AM
Freon-113
BRL
10
pg1L
70849
1
5/13/2006 7:28 AM
Isopropylbenzene
BRL
5 0
pg/L
70849
1
5/13/2006 7:28 AM
m,p-Xylene
BRL
10
pg1L
70849
1
5/13/2006 7:28 AM
Methyl acetate
BRL
5.0
pg/L
70B49
1
5/1312006 7:28 AM
Methyl tert-butyl ether
BRL
5.0
pg/L
70B49
1
5/13/2006 7:28 AM
Methyfcyclohexane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
l l I lolding times for preparation or analysis
exceeded
Narr
See Case Narrative
N Analyte not NELAC cLytified
NC
Not Confirmed
B Analyte detected in the associated
Method Blink
Page 4 of 30

Analytical Environmental Services, Inc.
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-001
Date: 22-Mav-06
Client Sample 1D-. FT-07
Collection Date: 5/1 1/2006 8:15:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg1L
70849
1
5113/2006 7:28 AM
o-Xylene
BRL
5.0
}tg1L
70849
1
5/13/2006 7.28 AM
Styrene
BRL
5.0
pglt
70849
1
5/13/2006 7:28 AM
Tetrachloroethene
BRL
5.0
pg1L
70849
1
5/1312006 7:28 AM
Toluene
BRL
5.0
pglL
70849
1
5/13/2006 7:28 AM
trans-1,2-Dichloroethene
BRL
5.0
p91
70849
1
5/13/2006 7:28 AM
trans- 1,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/1312006 7:28 AM
Trichloroethene
BRL
5.0
pglL
70849
1
5/13/2006 7:28 AM
Trichtorotluoromethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Vinyl chloride
BRL
2.0
pglL
70849
1
5/13/2006 7:28 AM
Surr: 4-Bromofluorobenzene
97.5
63.7-115
%REC
70849
1
5/13/2006 7:28 AM
Surr: Dibromofluoromethane
94.2
70.4-123
%REC
70849
1
5/13/2006 7:28 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849
1
5/13/2006 7:28 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
Biochemical Oxygen Demand 61.4 50.0
CHEMICAL OXYGEN DEMAND (COD)
Chemical Oxygen Demand 604 10
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
I I I loldinb times for preparation or analysis exceeded
N Analyte not NELAC certified
13 Analytc detected in the associated Method Blank
E405.1 (E405.1) Analyst: CAM
mg1L 70797 10 5112/2006 10:50 AM
E410.4 (E410.4) Analyst: EK
mg1L 70814 1 5112/2006 3:45 PM
E Estimated t Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 5 of 30

Analytical Environmental Services, Inc.
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-002
Date: 22-May-06
Client Sample ID:tFT-08-
Collection Date: 511.112006-8.35:00 AM
Matrix: SURFACE WATER ` J
J--
Analyses
Result
Reporting
Qual Units
BatchlD Dilution
Date Analyzed
Limit
Factor
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4--DDD
BRL
1.0
pglL
70840 1
5/15/2006 10:02 PM
4,4--DUE
BRL
1.0
pg1L
70840 1
5/15/2006 10:02 PM
4,4"-DDT
BRL
1.0
pglL
70840 1
5/15/2006 10:02 PM
Aldrin
BRL
0.50
pg1L
70840 1
5/15/2006 10:02 PM
alpha-BHC
BRL
0.50
pglL
70840 1
5/15/2006 10:02 PM
alpha -Chlordane
BRL
0.50
pglL
70a40 1
5/15/2006 10:02 PM
beta-BHC
BRL
0.50
pglL
70840 1
5/15/2006 10:02 PM
delta-BHC
BRL
0.50
pglL
70840 1
5/15/2006 10:02 PM
Dieldrin
BRL
1.0
pg1L
70840 1
5/15/2006 10:02 PM
Endosulfan I
BRL
0-50
pglL
70840 1
5/15/2006 10:02 PM
Endosulfan II
BRL
1.0
pglL
70840 1
5/15/2006 10:02 PM
Endosulfan sulfate
BRL
1.0
pglL
70840 1
5/15/2006 10:02 PM
Endrin
BRL
1.0
pglL
70840 1
5/15/2006 10:02 PM
Endrin aldehyde
BRL
1.0
pglL
70840 1
5/15/2006 10:02 PM
Endrin ketone
BRL
1.0
pglL
70840 1
5/15/2006 10:02 PM
gamma-BHC
BRL
0.50
pglL
70840 1
5/1512006 1U2 PM
gamma -Chlordane
BRL
0.50
pglL
70840 1
5115/2006 10:02 PM
Heptachlor
BRL
0.50
pglL
70W 1
6/16/2006 10:02 PM
Heptachlor epoxide
BRL
0.50
pglL
70840 1
5/15/2006 10:02 PM
Methoxychlor
BRL
5.0
pg1L
70840 1
5/15/2006 10:02 PM
Toxaphene
BRL
50
pglL
70840 1
5/15/2006 10:02 PM
Surr: Decachlorobiphenyl
22.3
17.9-122
%REC
70840 1
5/15/2006 10:02 PM
Surr: Tetrachloro-m-xylene
84.2
18.9-119
%REC
70840 1
5/15/2006 10;02 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
h Aluminum
4.47�
0.200
mg1L
70835
1
5/15/2006 5:08 PM
Y�,Antimon
LO 04-
0.0200
mg/L
70835
1
5/15/2006 5:08 PM
Arsenic
BRL
0.0500
mg1L
70835
1
5/15/2006 5:08 PM
Bari�m_�
0_04L1
0.0200
mg/L
70835
1
511512006 5:08 PM
Beryllium
BRL
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Cadmium
BRL
0.0050
mg1L
70835
1
5/15/2006 5:08 PM
Calcl- i=
222
0.100
mg1L
70835
1
5/15/2006 5:08 PM
-
Chromium-
C0.0316
0.0100
mg1L
70835
1
5/15/2006 5:08 PM
Coba�
C20318
0.0200
mg1L
70835
1
5/15/2006 5:08 PM
Copper_,
OL o818,
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Iro, n-�
Llj
0.100
mg/L
70835
1
5/15/2006 5:08 PM
[Lest
C0 0816�
0.0100
mg1L
70835
1
5/15/2006 5:08 PM
% Magnesium---.
2:83
0.100
mglL
70835
1
5/15/2006 5:08 PM
Mangan se
C0.9�
0.0050
mg1L
70835
1
5/15/2006 5:08 PM
Molybdenum
BRL
0.0500
mglL
70835
1
5/15/2006 5:08 PM
tNickel
0.0631
0.0200
mglL
70835
1
5/15/2006 5:08 PM
Potassium-
fi
0.500
mg/L
70835
1
5/15/2006 5:08 PM
Qualifiers: Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
11 Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analytc detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 6 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc. ` Client Sample ID- FT-2D
Project: Synthron Inc. Collection Date: 511-172006'$.35:00 AM
Lab ID: 0605766-002 Matrix: SURFACEVATER_�)
Analvses Result Reporting Qual Units BatchlD Dilution Date Analyzed
Limit Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: 138
Selenium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:08 PM
Silver
BRL
0.0100
mg1L
70835
1
5115)2006 5:08 PM
tSodiu—r—n:�:;7
63.8
1.00
mg1L
70835
1
5/15/2006 5:08 PM
Thallium
BRL
0.0200
mglL
70835
1
5/1512006 5:08 PM
�; irTin'
Z0.0688
0.0500
mg1L
70835
1
5/1512006 5:08 PM
Ti{anium 7
�0.154
0.0500
mg/L
70835
1
511512006 5:08 PM
;��Vanadiu�
i0.0460?
0.0100
mglL
70835
1
5/1512006 5:08 PM
Zinc
L2 34-':�;7 0.0200
mg1L
70835
1
5/15/2006 5:08 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0.00020
mg1L
70883
1
5M612006 2:32 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
100
pg1L
70632
1
511512006 7:34 PM
2,4,5-Trichlorophenol
BRL
250
pg1L
70832
1
511512006 7:34 PM
2,4,6-Trichlorophenol
BRL
100
pglL
70832
1
5115/2006 7:34 PM
2,4-Dichlorophenol
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
2,4-Dimethylphenol
BRL
100
pg1L
70832
1
5/1512006 7:34 PM
2,4-Dinitrophenol
BRL
250
NgIL
70832
1
5/15/2006 7:34 PM
2,4-Dinitrotoluene
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
2,6-Dinitrotoluene
BRL
100
pg1L
70832
1
5/1512006 7:34 PM
2-Chloronaphthalene
BRL
100
pglL
70832
1
5115/2006 7:34 PM
2-Chlorophenol
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
2-Methylnaphthalene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
2-Methylphenoi
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
2-Nitroaniline
BRL
250
pglL
70832
1
5/15/2006 T34 PM
2-Nitrophenol
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
3,3'-Dichlorobenzidine
BRL
100
pglL
70832
1
5/.15/2006 T34 PM
3-Nitroaniline
BRL
250
pg1L
70832
1
5/15/2006 7:34 PM
4,6- Dinitro-2-m ethyl phenol
BRL
250
pg1L
70832
1
5/15/2006 7:34 PM
4-Bromophenyl phenyl ether
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
4-Chloro-3-methylphenol
BRL
100
pglL
70832
1
5115/2006 7:34 PM
4-Chloroaniline
BRL
100
pglL
70832
1
5/1512006 7:34 PM
4-Chlorophenyl phenyl ether
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
4-Methylphenol
BRL
100
pglL
70832
1
5115/2006 7:34 PM
4-Nitroaniline
BRL
250
pglL
70832
1
5/1512006 7:34 PM
4-Nitrophenol
BRL
250
pglL
70832
1
5/15/2006 7:34 PM
Acenaphthene
BRL
100
pg1L
70832
1
5115/2006 7:34 PM
Acenaphthylene
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
Acetophenone
BRL
100
pg1L
70832
1
5115/2006 7:34 PM
Anthracene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Atrazine
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
13RL Below Reporting Limit
S
Surrogate Recovery outside
accepted recovery limits
H ]-folding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method Blank
Page 7 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT=08�
Project: Synthron Inc.
Collection Date: S11 1/2006�t
AM
Lab ID: 0605766-002
Matrix: SURFACE -WATER
Analyses
Result
Reporting
Qual Units
BatchID Dilution
Date Analyzed
Limit
Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Benzaldehyde
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Benzo(a)pyrene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Benzo(b)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Benzo(g,hJ)perylene
BRL
100
pg/L
70832
1
5/1512006 7:34 PM
Benzo(k)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Sis(2-chloroethoxy)methane
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Bis(2-chloroethyl)ether
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Bis(2-chloroisopropyl)ether
BRL
100
pg/L
70832
1
5/15/2006 7734 PM
Bls(2-ethylhexyl)phthalate
100-100
pg/L
70832
1
5/1512006 T34 PM
Butyl benzyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Caprolactam
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Carbazole
BRL
100
pg/L
70832
1
5/15/2006 T34 PM
Chrysene
BRL
100
pg/L
70632
1
5/15/2006 7:34 PM
Dibenz(a,h)anthracene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Dibenzofuran
BRL
100
pg/L
70832
1
5/1512006 7:34 PM
Diethyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Dimethyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Di-n-butyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Di-n-octyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Fluoranthene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Fluorene .
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Hexachlorobenzene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Hexachlorobutadiene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Hexachlorocyclopentadiene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Hexachloroethane
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Indeno(1,2,3-cd)pyrene
BRL
100
pg/L
70832
1
5/1512006 7:34 PM
lsophorone
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Naphthalene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Nitrobenzene
BRL
100
pg/L
70832
1
5/1512006 7:34 PM
N-Nitrosodi-n-propylamine
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
N-Nitrosodiphenylarnine
BRL
100
pg/L
70B32
1
5116/2006 7:34 PM
Pentachturophenol
BRL
250
pg/L
70832
1
5115/2006 7:34 PM
Phenanthrene
BRL
100
pg/L
70832
1
5115/2006 7:34 PM
Phenol
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Pyrene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Surr: 2A,6-Tribromophenol
92.8
64.8-129
%REC
70B32
1
5/15/2006 7:34 PM
Surr: 2-Fluorobiphenyl
87.4
5B.2-115
%REC
70832
1
5115/2006 7:34 PM
Surr: 2-Fluorophenol
73.7
24.4-115
%REC
70832
1
5/15/2006 7:34 PM
Surr: 4-Terphenyl•dl4
73.5
58.3-115
%REC
70832
1
5/15/2006 7:34 PM
Surr: Nitrobenzene-d5
91.4
51.8-115
%REC
70832
1
5/15/2006 7:34 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyle detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Conlinned
Page 8 of 30

Analytical Environmental Services, Inc. Date: 22-Muv-06
CLIENT: Tetra Tech EM Inc. Client Sample lD: FT-08
Project: Synthron Inc. Collection Date: C511;172006--8'.35:00 AM
Lab ID: 0605766-002 Matrix: 'SURFACE.WATER
Analyses
Result
Reporting Qua,
Limit
Units BatchID Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
74.0
17.9-115
%REC
70832
1
5115/2006 7:34 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg1L
70849
1
511312006 7:54 AM
1,1,2,2-Tetrachtoroethane
BRL
5.0
pg1L
70949
1
5113/2006 7:54 AM
1,1,2-Trichloroethane
BRL
5.0
pglL
70849
1
5113/2006 7:54 AM
1,1-Dichloroethane
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
1,1-Dichloroethene
BRL
5.0
pglL
70849
1
St13/2006 7:54 AM
1.2,4-Trichlorobenzene
BRL
5.0
pglL
70849
1
5/13/2006 7:54 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
1,2-Dibromoethane
BRL
5.0
pg1L
70849
1
511312006 7:54 AM
1,2-Dichlorobenzene
BRL
5.0
pglL
70849
1
5/1312006 7:54 AM
1,2-Dichloroethane
BRL
5.0
pglL
70849
1
5113/2006 7:54 AM
1,2-Dichloropropane
BRL
5.0
pglL
70849
1
5113/2006 7:54 AM
1,3-Dichlorobenzene
BRL
5.0
pglt
70849
1
5113/2006 7:54 AM
1,4-Dichlorobenzene
BRL
5.0
pglL
70849
1
5113/2006 7:54 AM
2-Butanone
BRL
50
pglL
70949
1
5/1312006 7:54 AM
2-Hexanone
BRL
10
pglL
70849
1
5113/2006 7:54 AM
4-Methyl-2-pentanone
BRL
10
pg1L
70849
1
5/13/2006 7:54 AM
Acetone
12D
50
pglL
70849
1
511312006 7:54 AM
Benzene
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Bromodichloromethane
BRL
5.0
pg1L
70B49
1
5113/2006 7:54 AM
Bromotorm
BRL
5.0
pglL
70849
1
5113/2006 7:54 AM
Bromomethane
BRL
5.0
pg1L
70B49
1
5/13/2006 7:54 AM
Carbon disulfide
BRL
5.0
pg/L
70849
1
5113/2006 7:54 AM
Carbon tetrachloride
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Chlorobenzene
BRL
5.0
pglL
70B49
1
5113/2006 7:54 AM
Chloroethane
BRL
10
pg1L
70849
1
5/13/2006 7:54 AM
Chloroform
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Chloromelhane
BRL
10
pglL
70849
1
511312006 7:54 AM
cis-1,2-Dichloroethene
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
cis- 1, 3-Dichloropropene
BRL
5.0
pg1L
70849
1
5113i2006 7:54 AM
Cyclohexane
BRL
5.0
pg1L
70949
1
5/13/2006 7-54 AM
Dibromochlorom ethane
BRL
5.0
pg1L
70849
1
5113/2006 7:54 AM
Dichlorodifluorom ethane
BRL
10
pg1L
70849
1
5/1312006 7:54 AM
Elhylbenzene
BRL
5.0
p91L
70849
1
5/1312006 7:54 AM
Freon-113
BRL
10
pg1L
70849
1
5/1312006 7:54 AM
Isopropylbenzene
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
lm;p--X� ylene--�
1=4
10
pg1L
70849
1
5/1312006 7:54 AM
\ / Methyl acetate
CZ-TE-P
5.0
pglL
70849
1
5/1312006 7:54 AM
Methyi tert-butyl ether
BRL
5.0
pgll-
70849
1
5/1312006 7:54 AM
Methylcyclohexane
BRL
5.0
pglL
70849
1
5/1312006 7:54 AM
Qualifiers: . Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H Bolding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyze not NGLAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method Blank
Page 9 of 30

Analytical Environmental Services, Inc.
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab 1 D: 0605766-002
Date: 22-May-06
Client Sample ID: FT 08
Collection Date: t57]']72006-9-35:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Units
BatchlD Dilution
Date Analyzed
Limit
Factor
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
o-Xylene
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Styrene
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
Tetrachloroethene
BRL
5,0
pglL
70849
1
5/1312006 7:54 AM
Toluene
11
5.0
pg11-
70B49
1
5/1312006 7:54 AM
trans-1,2-Dichloroethene
BRL
5.0
pg1L
70849
1
5/1312006 7;54 AM
trans-1,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
Trichloroethene
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
Trichlorofluoromethane
BRL
5.0
pg1L
70849
1
5/1312006 7:54 AM
Vinyl chloride
BRL
2.0
pglL
70849
1
5/1312006 7:54 AM
Surr: 4-Bromofluorobenzene
99.0
63.7-115
%REC
10849
1
5/1312006 7:54 AM
Surr: Dibromofluoromethane
94.4
704-123
%REC
70849
1
5/1312006 7:54 AM
Surr: Toluene-d8
101
73.4-115
%REC
70B49
1
5/1312006 7:54 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical.Oxygeri,Demand
113
50.0
mg1L
70797
10
5/1212006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
CI eicica�' 1 Oxygen Demand
774
10
mg/L
70814
1
5/120006 3:45 PM
Qualifiers: s Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 10 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID- FT-09
Project: Synthron Inc,
Collection Date: 5/11/2006
8:55:00 AM
Lab ID: 0605766-003
Matrix: "SURFACE WATER
Analyses
Result
Reporting
Qual Units
I3atchlD
Dilution
Date Analyzed
Limit
Factor
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW351013)
Analyst: MM
4,4'-DD0
BRL
0,10
pg1L
70840
1
5115/2006 10:14 PM
4,4'-DDE
BRL
0.10
pglL
70840
1
5/1512006 10:14 PM
4,4'-DDT
BRL
0,10
pg1L
70840
1
5115/2006 10:14 PM
Aldrin
BRL
0.050
pg1L
70840
1
5/1512006 10:14 PM
alpha-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
alpha -Chlordane
BRL
0.050
pg1L
70840
1
5/1512006 10:14 PM
beta-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
delta-BHC
BRL
0.050
pg1L
70W
1
5115/2006 i0:14 PM
Dieldrin
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
Endosulfan I
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
Endosulfan Il
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
Endosulfan sulfate
BRL
0,10
pglL
70840
1
5/15/2006 10:14 PM
Endrin
BRL
0.10
pg1L
70B40
1
5/1512006 10:14 PM
Endrin aldehyde
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
Endrin ketone
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
gamma-BHC
BRL
0.050
pg1L
70B40
1
5/15/2006 10:14 PM
gamma -Chlordane
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
Heptachlor
0.69
0.050
pg1L
70B40
1
5/1512006 10:14 PM
Heptachlor epoxide
BRL
0.050
pg1L
70840
1
5115/2006 10:14 PM
Methoxychlor
BRL
0.50
pg1L
70W
1
5/15/2006 10:14 PM
Toxaphene
BRL
5.0
pg1L
70a40
1
5/15/2006 10:14 PM
Surr: Decachlorobiphenyl
38.2
17.9-122
%RFC
70840
1
5/15/2006 10A4 PM
Surr: Tetrachloro-m-xylene
172
18.9-119
S %REC
70940
1
5115/2006 10:14 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
22.3 "1
0.200
mg/L
70835
1
5115/2006 5:13 PM
'Antimony
0.21.1 .
0.0200
mg1L
70835
1
5/15/2006 5:13 PM
Arsenic
BRL
0,0500
mg1L
70835
1
5/15/2006 5:13 PM
Barium
0.214 '
0,0200
mg1L
70835
1
5/15/2006 5:13 PM
Beryllium
BRL
0.0100
mg/L
70835
1
5/15/2006 5:13 PM
Cadmium
BRL
0.0050
mg1L
70835
1
5/15/2006 5:13 PM
r Calcium 7
27.0
0.100
mg1L
70835
1
5/15/2006 5:13 PM
Chromium
0.0815
0.0100
mg1L
70835
1
5/15/2006 5:13 PM
Cobalt
` 0.0359
0.0200
mg/L
70835
1
5/15/2006 5:13 PM
\
Copper
0.258
0.0100
mg/L
70835
1
5/15/2006 5:13 PM
Iron
34.4
0.100
mg1L
70835
1
5/15/2006 5:13 PM
;Lead
0.133
0,0100
mg/L
70835
1
5115/2006 5:13 PM
Magnesium '
8.33
_ 0.100
mg/L
70835
1
5/15/2006 5:13 PM
Manganese
' 1.06
0.0050
mg/L
70835
1
5115/2006 5:13 PM
Molybdenum
BRL
0.0500
mg1L
70835
1
5/15/2006 5:13 PM
;Nickel
%0.0740
0,0200
mglL
70835
1
5115/2006 5:13 PM
Potassium
11.6
0,500
mg1L
70835
1
5/15/2006 5:13 PM
Qualifiers: Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
I: Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page I I of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample IDr..FT-09�
Project: Synthron Inc.
Collection Date: 5/11/2006
8:55;00 AM
Lab ID: 0605766-003
Matrix: SURFACE WATER.
Analyses
Result
Reporting Qual
Units BatchID Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:13 PM
Silver
BRL
0.0100
mglL
70835
1
5/15/2006 5:13 PM
Sodium
60.4
1.00
mg1L
70835
1
5/15/2006 5:13 PM
Thallium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:13 PM
Tin
0.430
0.0500
mg1L
70835
1
5/15/2006 5:13 PM
Titanium
1.12
0.0500
mg1L
70835
1
5/15/2006 5:13 PM
Vanadium
0,117
0.0100
mg1L
70835
1
5/15/2006 5:13 PM
Zinc
4.34
0.0200
mglL
70835
1
5/15/2006 5713 PM
MERCURY, TOTAL
SV 7470A
(SW7470A)
Analyst: LKW
Mercury
;0.00038
, 0.00020
mg1L
70883
1
5/16/2006 2:34 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
SRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2,4,5-Trichlorophenol
BRL
25
pg/L
70832
1
5/15/2006 8:00 PM
2,4,6-Trichlorophenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2,4-Dichlorophonol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2,4-Dimethylphenol
BRL
10
pg/L
70832
1
5/15/2006 8;00 PM
2,4-Dinitrophenol
BRL
25
pg/L
70832
1
5/15/2006 8;00 PM
2,4-Dinitrotoluene
BRL
10
pg/L
70832
1
5/15/2006 8;00 PM
2,6-Dinitrotoluene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Chloronaphthatene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Chlorophenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Methylnaphthalene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Methylphenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Nitroaniline
BRL
25
pg/L
70832
1
5/15/2006 8:00 PM
2-Nitrophenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
3,3"-Dichlorobenzidine
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
3-Nilroaniline
BRL
25
pg/L
70832
1
5/15/2006 8:00 PM
4,6-Dinitro-2-methylphenol
BRL
25
pg1L
70832
1
5/15/2006 8:00 PM
4-13romophenyl phenyl ether
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
4-Chloro-3-methylphenol
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
4-Chloroaniline
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
phenyl ether
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Y4-Chlorophenyl
4-Methylphenol
21
10
pg/L
70832
1
5/15/2006 8:00 PM
4-Nilroaniline
BRL
25
pg/L
70832
1
5/15/2006 8:00 PM
4-Nitrophenol
BRL
25
pg/L
70832
1
5/15/2006 8:00 PM
Acenaphthene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Acenaphthylene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Acetophenone
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Anthracene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Atrazine
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Qualifiers: Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation range)
13RL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H I lolding times for preparation
or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 12 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT:
Tetra Tech EM Inc.
Client Sample 16:.FT-09
;
Project:
Synthron Inc.
Collection Date:
5/11/2006 8:55_00 AM
Lab ID:
0605766-003
Matrix:
SURFACE WATER
4.
Analyses Result Reporting Quai Units BatchlD Dilution Date Analyzed
Limit Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Benzaldehyde
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Benzo(a)pyrene
BRL
10
pg1L
70832
1
5/16/2006 8:00 PM
Benzo(b)iluoranthene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Benzo(g,h,i)perylene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Benzo(k)tluoranthene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Bis(2-chloroethoxy)methane
BRL
10
pg1L
70832
1
6/15/2006 8:00 PM
Bis(2-chloroethyl)ether
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Bis(2-chloroisopropyl)ether
BRL
10
pg/L
70832
1
5115/2006 8:00 PM
Bis(2-ethylhexyl)phthalate
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Butyl benzyl phthalate
BRL
10
pglL
70832
1
5/1512006 8:00 PM
Caprolactam
BRL
10
pglL
70832
1
5/1512006 8:00 PM
Carbazole
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Chrysene
BRL
10
pg1L
70832
1
5/1512006 8:00 PM
Dibenz(a,h)anthracene
BRL
10
pg1L
70832
1
5/1512006 8:00 PM
Dibenzoturan
BRL
10
pglL
70832
1
5115f2006 8:00 PM
Diethyl phthalate
BRL
10
pglL
70832
1
511512006 8:00 PM
Dimethyl phthalate
BRL
10
pglL
70832
1
5/15f2006 8:00 PM
Di-n-butyl phthalate
BRL
10
pg1L
70832
1
6/1512006 8:00 PM
Di-n-octyl phthalate
BRL
10
pg1L
70832
1
6/1512006 8:00 PM
Fluoranthene
BRL
10
pglL
70832
1
5/15/2006 8:00 PM
Fluorene
BRL
10
pg1L
70832
1
5/1512006 8:00 PM
Hexachlorobenzene
BRL
10
pg/L
7OB32
1
5/1512006 8:00 PM
Hexachlorobutadiene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Hexachlorocyclopentadiene
BRL
10
pg1L
70832
1
5/1512006 8:00 PM
Hexachloroethane
BRL
10
pg/L
70B32
1
5/15/2006 8:00 PM
Indeno(1,2,3-cd)pyrene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Isophorone
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Naphthalene
BRL
10
pglL
70832
1
5/1512006 8:00 PM
Nitrobenzene
BRL
10
pg1L
70832
1
5/1512006 8:00 PM
N-Nitrosodi-n-propylamine
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
N-Nitrosodiphenylarnine
BRL
10
pglL
70832
1
5/15/2006 8:00 PM
Pentachlorophenol
BRL
25
pg1L
70832
1
5/15/2006 8:00 PM
Phenanthrene
BRL
10
pglL
70832
1
5/15/2006 8:00 PM
`Phenol
20
10
pglL
70832
1
5/15/2006 8:00 PM
Pyrene
BRL
10
pglL
70832
1
5/15/2006 8:00 PM
Surr: 2,4,6-Tribromophenol
35.1
64.8-129
S
%REC
70832
1
5/15/2006 8:00 PM
Surr: 2-Fluorobiphenyl
37.0
58.2-115
S
%REC
70832
1
5/15/2006 8:00 PM
Surr: 2-Fluorophenol
27.9
24.4-115
%REC
70832
1
5/1512006 8:00 PM
Su rr: 4-Terphenyl- d 14
33.7
58.3-115
S
%REC
70832
1
5/1512006 8:00 PM
Surr: Nitrobenzene-d5
37.2
51.8-115
S
%REC
70832
1
5115/2006 8:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H fielding times for preparation or analysis exceeded
N Analyte not NELAC certifted
B Ana lyte detected in the associated Method Blank
E Estimated (Value above quantitation ranee)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 13 of 30

Analytical Environmental Services, Inc. Date: 22-Mav-06
CLIENT: Tetra Tech EM Inc. Client Sample 1D: _ FT-09`
Project: Synthron Inc. Collection Date: 5/11/2006,$:55:00 AM
Lab ID: 0605766-003 Matrix: SURFACE WATER
Analyses Result Reporting Qua] Units BatchlD Dilution Date Analyzed
Limit Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
26.2
17.9-115
%REC
70832
1
5/15/2006 8:00 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70849
1
5113/2006 8:20 AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,1-Dichloroethane
BRL
5.0
pglL
70649
1
5/13/2006 8:20 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70649
1
5/13/2006 8:20 AM
1,2,4-Trichlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,2-Dichlorobenzene
8RL
&0
pg/L
70849
1
5/13/2006 8:20 AM
1,2-Dichloroethane
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
2-Butanone
BRL
50
pg/L
70849
1
5/13/2006 8:20 AM
2-Hexanone
BRL
10
pg1L
70849
1
5/13/2006 8:20 AM
4-Methyl-2-pentanone
BRL
10
pg/L
70849
1
5/13/2006 8:20 AM
Acetone
140
50
pg/L
70849
1
5/13/2006 8:20 AM
Benzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Bromodichloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Bromoform
BRL
5.0
pg/L
70849
1
5/1312006 8:20 AM
Bromomethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
'Carbon disulfide
12
5.0
pg/L
70B49
1
5/1312006 8:20 AM
Carbon tetrachloride
BRL
5.0
pq/L
70849
1
5/1312006 8:20 AM
Chlorobenzene
BRL
5.0
pg/L
70849
1
5/1312006 8:20 AM
Chloroethane
BRL
10
pg/L
70849
1
5/1312006 8:20 AM
Chloroform
BRL
5.0
pg/L
70849
1
5/1312006 8:20 AM
Chloromethane
BRL
10
pg/L
70849
1
5/13/2006 8:20 AM
cis- 1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
cis- 1,3-Dichloropropene
BRL
5.0
pg/L
70849
1
5/1312006 8:20 AM
Cyclohexane
BRL
5.0
pg/L
70849
1
SM3/2006 8:20 AM
Dibromochloromethane
BRL
5.0
pg/L
70849
1
5/1312006 8:20 AM
Dichlorodifluoromethane
BRL
10
pg/L
70849
1
S113/2006 8:20 AM
Ethylbenzene
BRL
5.0
pg/L
70849
1
S113/2006 8:20 AM
Freon-113
BRL
10
pg/L
70849
1
5/13/2006 8:20 AM
lsopropyl benzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
-m,p-Xylene
21
10
pg/L
70849
1
5/13/2006 8:20 AM
Methyl acetate
10
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Methyt tert-butyl ether
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Methylcyclohexane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NEL'AC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation rangel
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 14 of 30

Analytical Environmental Services, Inc.
Date: 22-Mav-06
CLIENT: Tetra Tech EM Inc_
Client Sample ID: FT-09
Project: Synthron Inc.
Collection Date: 5/11/2006
8:55:00 AM
Lab ID: 0605766-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Quat
Limit
Units
BatchID
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
Ng1L
70849
1
5/13/2006 8:20 AM
o-Xylene
5.6
5.0
NgIL
70849
1
511312006 8:20 AM
Styrene
BRL
5.0
Ng1L
70949
1
5/13/2006 8:20 AM
Teirachloroethene
BRL
5.0
Ng1L
70849
1
5/1312006 8:20 AM
Toluene
5.5
5.0
pg1L
70849
1
5/13/2006 8:20 AM
trans-1 ,2-Dichloroethene
BRL
5.0
NgIL
70849
1
5/13/2006 8:20 AM
trans- 1,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
Trichloroethene
BRL
5.0
NgIL
70849
1
5/13/2006 8:20 AM
Trichlorofluoromethane
BRL
5.0
N911-
70849
1
5/13/2006 8:20 AM
Vinyl chloride
BRL
2.0
VgIL
70849
1
5113/2006 8:20 AM
Surr: 4-Bromofluorobenzene
96.7
63.7-115
%REC
70849
1
5/13/2006 8:20 AM
Surr: Dibromofluoromethane
96.4
70.4-123
%REC
70849
1
5/13/2006 8:20 AM
Sum Toluene -dB
103
73.4-115
%REC
70849
1
5/13/2006 8:20 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
184
50.0
mg/L
70797
10
5/12/2006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand ;
1350
10
mg1L
70814
1
5/12/2006 3:45 PM
Qualifiers: IValue exceeds Maximum Contaminant Level
BRL Below Reponing Limit
I I }folding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Anatyte detected in the associated Method Blank
E Estimated ( Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 15 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-10
Project: Synthron Inc.
Collection Date: 5/1
1/2006 9:15:00
AM
Lab ID: 0605766-004
Matrix. SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMQOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
4,4'-DDE
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
4,4'-DDT
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
Aldrin
BRL
0.50
pg1L
70840
1
5/15/2006 10:25 PM
alpha-BHC
BRL
0.50
pg1L
70840
1
5/15/2006 10:25 PM
alpha -Chlordane
BRL
0.50
pg1L
70840
1
5/15/2006 10:25 PM
beta-BHC
BRL
0.50
pg1L
70840
1
5/15/2006 10:25 PM
delta-BHC
BRL
0.50
pg/L
70840
1
5/1512G06 10:25 PM
Dieldrin
BRL
1.0
pg/L
70840
1
5/15/2006 10:25 PM
Endosulfan I
BRL
0.50
pg1L
70840
1
5/15/2006 10:25 PM
Endosulfan 11
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
Endosulfan sulfate
BRL
1.0
pg1L
70840
1
5/1512006 10:25 PM
Endrin
BRL
1.0
pg/L
70840
1
5/15/2006 10:25 PM
Endrin aldehyde
BRL
1.0
pg/L
70840
1
5/15/2006 10:25 PM
Endrin ketone
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
gamma-BHC
BRL
0.50
pg/L
70840
1
5/1512006 10:25 PM
gamma -Chlordane
BRL
0.50
pg/L
70840
1
5/1512006 10:25 PM
Heptachlor
BRL
0.50
pg/L
70840
1
5115f2006 10:25 PM
Heptachlor epoxide
BRL
0.50
pg/L
70840
1
5/1512006 10:25 PM
Methoxychlor
8RL
5.0
pg/L
70840
1
5/1512006 10:25 PM
Toxaphene
BRL
50
pg/L
70a40
1
5/1512006 10:25 PM
Surr: Decachlorobiphenyl
33.0
17,9-122
%REC
70840
1
6/1612006 10:25 PM
Surr: Tetrachloro-m-xylene
30.5
18,9-119
%REC
70840
1
5/1512006 10:25 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
5.35
0.200
mg/L
70835
1
5/1512006 5:19 PM
Antimony
0,0857
0.0200
mg1L
70835
1
5/1512006 5:19 PM
Arsenic
13RL
0.0500
mg1L
70835
1
5/1512006 5:19 PM
Barium
0.0609
0.0200
mg1L
70835
1
5/1512006 5:19 PM
Beryllium
BRL
0,0100
mg1L
70835
1
5/1512006 5:19 PM
Cadmium
0.0062
0.0050
mg/L
70835
1
5/1512006 5:19 PM
Calcium
37.5
0.100
mg1L
70835
1
5/1512006 5:19 PM
Chromium
0.0470
0.0100
mg/L
70835
1
5/15/2006 5A9 PM
Cobalt
0.0243
0.0200
mg/L
70835
1
5/15/2006 5:19 PM
Copper
0,185
0.0100
mg/L
70835
1
5/15/2006 5:19 PM
Iron
10.9
0.100
mg/L
70835
1
5/15/2006 5:19 PM
Lead
0.163
0.0100
mg/L
70835
1
5/15/2006 5:19 PM
Magnesium
5.75
0.100
mg/L
70835
1
5/15/2006 5:19 PM
Manganese
0.728
0.0050
mg/L
70835
1
5/15/2006 5:19 PM
Molybdenum
BRL
0.0500
mg/L
70835
1
Sit 512006 5719 PM
Nickel
0.0636
0.0200
mg1L
70835
1
5/15/2006 5719 PM
Potassium
15.5
0.500
mg/L
70835
1
5/15/2006 5719 PM
Qualifiers: Value exceeds Maximum Contaminant Level
RRL Below Reporting Limit
0 Holding times for preparation or analysis exceeded
N Analvte not NL-LAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantization range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 16 of 30

Analytical Environmental Services, Inc. Date: 22-Mav-06
CLI ENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-004
Client Sample lD: E i-10
Collection Date: 5/1 1/2006 9:15:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting
Qual Units
BatchlD
Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg1L
70835
1
5/1512006 5:19 PM
Silver
BRL
0.0100
mglL
70835
1
5/15/2006 5:19 PM
Sodium
97.1
1.00
mg1L
70B35
1
5/15/2006 5:19 PM
Thallium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:19 PM
Tin
0.150
0.0500
mglL
70835
1
5/15/2006 5:19 PM
Titanium
0.257
0.0500
mg1L
70835
1
511512006 5:19 PM
Vanadium
0.0741
0.0100
mg1L
70835
1
5/15/2006 5:19 PM
Zinc
8.88
0.0200
mglL
70835
1
6/15/2006 5:19 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0.00020
mg1L
70883
1
5116/2006 2:36 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
100
pg1L
70832
1
5/1512006 8:26 PM
2,4,5-Trichlorophenot
BRL
250
pg1L
70832
1
5/15/2006 8:26 PM
2,4,6-Trichlorophenol
BRL
100
µg1L
70832
1
5115/2006 8:26 PM
2,4-Dichlorophenol
BRL
100
pg1L
70832
1
5115/2006 8:26 PM
2,4- Dime thy [phenol
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
2,4-Dinitrophenol
BRL
250
pg1L
70832
1
5/15/2006 8:26 PM
2,4-Dinitrotoluene
BRL
100
pg1L
70832
1
6/15/2006 8:26 PM
2,6-Dinitrotoluene
BRL
100
µg1L
70832
1
5115/2006 8:26 PM
2-Chloronaphthalene
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
2-Chlorophenol
BRL
100
pglL
70832
1
5/15/2006 8:26 PM
2-Methyinaphthalene
BRL
100
µg1L
70832
1
511512006 8:26 PM
2-Methylphenot
BRL
100
pglL
70832
1
5/15/2006 8:26 PM
2-Nitroaniline
BRL
250
µg1L
70832
1
5/15/2006 826 PM
2-Nitrophenol
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
3,3'-Dichlorobenzidine
BRL
100
pglL
70832
1
5/15/2006 8:26 PM
3-Nilroanifine
BRL
250
pg1L
70832
1
5/15/2006 8:26 PM
4,6-Dinitro-2-methylphenol
BRL
250
pglL
70832
1
5115/2006 8:26 PM
4-Bromophenyl phenyl ether
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
4-Chloro-3-methylphenol
BRL
100
pg1L
70832
1
5115/2006 8:26 PM
4-Chloroaniline
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
4-Chlorophenyl phenyl ether
BRL
100
pglL
70832
1
5/15/2006 8:26 PM
4-Methylphenol
140
100
µg1L
70832
1
511512006 6:26 PM
4-Nitroaniline
BRL
250
pglL
70832
1
6/15/2006 8:26 PM
4-Nitrophenol
BRL
250
µg1L
70832
1
5/15/2006 8:26 PM
Acenaphthene
BRL
100
pg1L
70832
1
511512006 8:26 PM
Acenaphthylene
BRL
100
pglL
70832
1
6/15/2006 8:26 PM
Acetophenone
BRL
100
pg1L
70832
1
6/15/2006 8:26 PM
Anthracene
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Atrazine
BRL
100
µg1L
70832
1
5/15/2006 8:26 PM
Qualifiers: Value exceeds Maximum Contaminant Level
BRi- Below Reporting Limit
H holding times for preparation or analysis exceeded
N Analyte not NFLAC certified
fS Analyte detected in the associated Method Blank
E Estimates! (Value above quamitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 17 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-10
Project: Synthron Inc.
Collection Date: 5/11/2006
9:15:00
AM
Lab ID: 0605766-004
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchlD
Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
SRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Benzaldehyde
BRL
100
pg/L
70832
1
5115/2006 8:26 PM
Benzo(a)pyrene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Benzo(b)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Benzo(g,h,i)perylene
BRL
100
pg1L
70832
1
511512006 8:26 PM
Benzo(k)fluoranthene
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Bis(2-chloroethoxy)methane
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Bis(2-chloroethyl)ether
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Bis(2-chloroisopropyl)ether
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Bis(2-ethylhexy1)ph1halate
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Butyl benzyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Caprolactam
BRL
100
pg/L
70832
1
5/1512006 8:26 PM
Carbazole
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Chrysene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Dibenz(a,h)anthracene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Dibenzofuran
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Diethyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Dimethyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Di-n-butyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Di-n-octyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Fluorene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Hexachlorobenzene
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Hexachlorobutadieno
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Hexachlorocyclopentadiene
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Hexachloroethane
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Indeno(1,2,3-cd)pyrene
BRL
100
pglL
70832
1
5/15/2006 8:26 PM
Isophorone
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Naphthalene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Nitrobenzene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
N-N itrosod i-n-propyla mine
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
N-Nitrosodiphenylamine
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Pentachlorophenol
BRL
250
pg1L
70832'
1
5/15/2006 8:26 PM
Phenanthrene
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
Phenol
260
100
pg/L
70832
1
5/15/2006 8:26 PM
Pyrene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Surr: 2,4,6-Tribromophenol
90.1
64.8-129
%REC
70832
1
5/1512006 8:26 PM
Surr: 2-Fluorobiphenyl
89.8
58.2.115
%REC
70832
1
5/15/2006 8:26 PM
Surr: 2-Fluorophenol
76.5
24.4-115
%REC
70832
1
5/15/2006 8:26 PM
Surr:4-Terphenyl-d14
82.9
58.3-115
%REC
70832
1
5115/2006 8:26 PM
Surr: Nitrobenzene-d5
116
51.8-115
S %REC
70832
1
5/15/2006 8:26 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
I I I lolding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantization range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 18 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-10
Project: Synthron Inc.
Collection
Date: 5/1
112006 9:15:00 AM
Lab ID: 0605766-004
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qua] Units BatchiD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
77.6
17.9-115
%REC 70832
1
5/15/2006 8:26 PM
TCL VOLATILE ORGANICS
SW8260B
(SW503013)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg1L
70849
1
5113I20068:45AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70849
1
511312006 8:45 AM
1,1-Dichloroethene
BRL
5.0
p91L
70849
1
5/1312006 8745 AM
1,2,4-Trichlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70849
1
5/1312006 8A5 AM
1,2-Dibromoethane
BRL
5.0
pg1L
70B49
1
5/13/2006 8A5 AM
1,2-Dichlorobenzene
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
1,2-Dichloroethane
BRL
5.0
pg1L
70849
1
5/1312006 8:45 AM
1,2-Dichloropropane
BRL
5.0
pg1L
70949
1
5/13/2006 8:45 AM
1,3-Dichlorobenzene
BRL
5.0
pglL
70849
1
511312006 8:45 AM
1,4-Dichlorobenzene
BRL
5.0
pglL
70649
1
5/13/2006 8A5 AM
2-Butanone
BRL
50
pg1L
70849
1
5/13/2006 8:45 AM
2-Hexanone
BRL
10
pg1L
70849
1
5/1312006 8:45 AM
4-Methyl-2-pentanone
BRL
10
pg1L
70849
1
5/13/2006 8:45 AM
Acetone
620
500
pg/L
70849
50
5/13/2006 2:42 AM
Benzene
BRL
5.0
pglL
70649
1
5/1312006 BA5 AM
Bromodichloromethane
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
Bromoform
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
Bromomethane
BRL
5.0
pg1L
70B49
1
5/13/2006 8;45 AM
Carbon disulfide
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
Carbon tetrachloride
BRL
5.0
pglL
70949
1
5/13/2006 8:45 AM
Chlorobenzene
BRL
5.0
pg1L
70849
1
5/1312006 8:45 AM
Chloroethane
BRL
10
pglL
70849
1
5/13/2006 BA5 AM
Chloroform
BRL
5.0
pg1L
70849
1
511312006 BA5 AM
Chloromethane
BRL
10
pglL
70849
1
5/13/2006 8:45 AM
cis- 1,2-Dichloroethe ne
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
cis-1,3-Dichloropropene
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
Cyclohexane
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
Dibromochloromethane
BRL
5.0
pglL
70849
1
5/1312006 8A5 AM
Dichlorodifluoromethane
BRL
10
pg1L
70849
1
5/13/2006 8:45 AM
Ethylbenzene
13
5.0
pglL
70849
1
5/13/2006 8:45 AM
Freon-113
BRL
10
pglL
70849
1
5/13/2006 8:45 AM
Isopropylbenzene
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
m,p-Xylene
52
10
pg1L
70849
1
5/1312006 SA5 AM
Methyl acetate
56
5.0
pg1L
70849
1
5/13/2006 &45 AM
Methyi tent -butyl ether
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
Methylcyclohexane
BRL
5.0
pg11.
70849
1
5/13/2006 &45 AM
Qualifiers: ' Value exceeds Maximum Coniaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H Molding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated Method
Blank
Page 19 of 30

Analytical Environmental Services, Inc. Date: 22-A4a.v-06
CLIENT: Tetra Tech EM Inc. Client Sample ID: FT-10
Project: Synthron Inc. Collection Date: 5/1 1/2006 9:15:00 AM
Lab ID: 0605766-004 Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Units
BatchlD Dilution
Date Analyzed
Limit
Factor
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
NgIL
70849
1
5/13/2006 8:45 AM
o-Xylene
15
5.0
pq/L
70849
1
5/13/2006 8:45 AM
Styrene
BRL
5.0
NgIL
70949
1
5/13/2006 8:45 AM
Tetrachloroethene
BRL
5.0
NgIL
70849
1
5/13/2006 8:45 AM
Toluene
69
5.0
NgIL
70849
1
5/13/2006 8:45 AM
trans- 1,2-Dichloroethene
BRL
5.0
NgIL
70849
1
5/13/2006 8:45 AM
trans- 1,3-Dichloropropene
BRL
5.0
NgIL
70849
1
5/13/2006 8:45 AM
Trichloroethene
BRL
5.0
NgIL
70849
1
5/13/2006 8:45 AM
Trichlorofluoromethane
BRL
5.0
NgIL
70849
1
5/13/2006 8:45 AM
Vinyl chloride
BRL
2.0
pg/L
70849
1
5/13/2006 8:45 AM
Surr: 4-Bromofluorobenzene
97.8
63.7-115
%REC
70849
1
5/13/2006 8:45 AM
Surr: 4-Bromofluorobenzene
96.0
63.7-115
%REC
70849
50
5/13/2006 2:42 AM
Sum Dibromofluoromethane
94.3
70.4-123
%REC
70849
50
5/13/2006 2:42 AM
Sum Dibromofluoromethane
96.1
70.4-123
%REC
70849
1
5/13/2006 8:45 AM
Surr: Toluene-d8
102
73.4-115
%REC
70849
1
5/13/2006 8:45 AM
Surr: Toluene-d8
101
73,4-115
%REC
70849
50
5/13/2006 2:42 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
585
50,0
mg1L
70797
10
5I1212006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
2570
100
mg1L
70814
10
5/12/2006 3:45 PM
Qualifiers; * Value exceeds Maximurn Contaminant Level
BRL Below Reporting limit
if Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
13 Analyte detected in the associated Method Blank
E Estimated (Value above yuantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 20 of 30

Analytical Environmental Services, Inc.
Date: 22-Mav-06
CLIENT: Tetra Tech EM Inc. Client Sample ID: FT-Ll
Project- Synthron Inc. Collection Date: t511'1'/2006' -35:00 AM
Lab ID- 0605766-005 Matrix: SURFACE-WATER`<j
Reporting Dilution
Analyses Result Limit Qua] Units BatchlD Factor Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
1.0
µg1L
70840
1
5/15/2006 10:37 PM
4,4'-DDE
BRL
1.0
µglL
70840
1
5/15/2006 10:37 PM
4,4'-DDT
BRL
1.0
µglL
70840
1
5/15/2006 10:37 PM
Aldrin
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
alpha-BHC
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
alpha -Chlordane
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
beta-BHC
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
delta-BHC
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
Dieldrin
BRL
1.0
µglL
70840
1
5/15/2006 10:37 PM
Endosulfan I
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
Endosulfan II
BRL
1.0
µglL
70840
1
5/15/2006 10:37 PM
Endosulfan sulfate
BRL
1.0
µg1L
70840
1
5/15/2006 10:37 PM
Endrin
BRL
1.0
µglL
70840
1
5/15/2006 10:37 PM
Endrin aldehyde
BRL
1.0
µglL
70840
1
5/15/2006 10:37 PM
Endrin ketone
BRL
1.0
µg1L
70840
1
5/15/2006 10:37 PM
gamma-BHC
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
gamma -Chlordane
BRL
0.50
µg1L
70840
1
5/15/2006 10:37 PM
Heptachlor
BRL
0.50
µglL
70840
1
5/1512006 10:37 PM
Heptachlor epoxide
BRL
0.50
µglL
70840
1
5/15/2006 10:37 PM
Methoxychlor
BRL
5.0
µglL
70840
1
5/15/2006 10:37 PM
Toxaphene
BRL
50
µg1L
70840
1
5/15/2006 10:37 PM
Surr: Decachlorobiphenyl
17.1
17.9-122 S
%REC
70840
1
5/15/2006 10:37 PM
Surr: Tetrachloro-m-xylene
49.5
18.9-119
%REC
70840
1
5/15/2006 10:37 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
n u ?
[2 62� 0.200
mglL
70835
1
5/15/2006 5:27 PM
ktion
0.05600.0200
mg1L
70835
1
5/15/2006 5:27 PM
Arsenic
BRL 0.0500
mg1L
70835
1
5/15/2006 5:27 PM
8ariurti
O7O377 ? 0.0200
m91L
70835
1
5/15/2006 5:27 PM
Beryllium
BRL 0.0100
mg1L
70835
1
5/15/2006 5:27 PM
Cadmium
BRL 0.0050
mglL
70835
1
5/15/2006 5:27 PM
Calcium y=
C29-7,7 0.100
mg/L
70835
1
5/15/2006 5:27 PM
Chromium-m
0:0414�0.0100
mglL
70835
1
5/15/2006 5:27 PM
Cobalt _ '�'i,•
2LOS 0.0200
mg1L
70835
1
5/1512006 5:27 PM
CoL ppe-�
0a29 0.0100
mg/L
70835
1
5115/2006 5:27 PM
lien
ULOD 0.100
mg1L
70835
1
5/15/2006 5727 PM
,Lead
`0�128- - 0.0100
mglL
70835
1
5/1512006 5:27 PM
Magnesium
3:84--- 0.100
mg/L
70835
1
5/15/2006 5:27 PM
Manganeses.
1,27 0.0050
mg1L
70835
1
5/15/2006 5:27 PM
Molybdenum
BRL 0.0500
mglL
70835
1
5/15/2006 5:21 PM
NiZ61E,3-
C,02676�. Z0.0200
mglL
70835
1
5/15/2006 527 PM
lPotassium
11� .7�---0.500
mg1L
70835
1
5/15/2006 5:27 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times For preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quanlitalion range)
S Surrogate Recovery outside accepted recovery limits
Narr Sec Case Narrative
NC Not Confirmed
Rage 21 of 30

Analytical Environmental Services, Inc.
Date: 22-iWay-06
_
CLIENT: Tetra Tech EM Inc.
Client SampleIDrFYI
Project: Synthron Inc.
Collection
Date: 51] ]I2006 9'35:00 AM
Lab ID-. 0605766-005
Matrix: Sl}RF.ACE WATER
Analyses
Result Reporting Qua,
Units BatchlD Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg/L
70835 1
5/15/2006 5:27 PM
Silver_
BRL
0.0100
mg/L
70835 1
5/1512006 5:27 PM
t5od umiL88.5J
1.00
mglL
70835 1
5/15/2006 5:27 PM
Thallium
BRL
0.0200
mg/L
70835 1
5/15/2006 5:27 PM
Tin
0.102
0.0500
mg/L
70835 1
5/15/2006 5:27 PM
TitL a�nium _
0.12�
0.0500
mg/L
70835 1
5/15/2006 5:27 PM
Vanadium C
w
O'0570—)
�5.71
0.0100
mg/L
70835 1
5/16/2006 5:27 PM
2inc
0.0200
mg/L
70835 1
5/15/2006 5:27 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury~ —
[-060230.00020
mg/L
70883 1
5/16/2006 2:37 PM
TCL-SEMIVOLATiLE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
100
pg1L
70832 1
5/1512006 8:51 PM
2,4,5-Trichlorophenol
BRL
250
pg/L
70832 1
5/1512006 8:51 PM
2,4,6-Trichlorophenol
BRL
100
pg/L
70832 1
5/1512006 8:51 PM
2,4-Dichiorophenol
BRL
100
pg1L
70832 1
5/15/2006 8751 PM
2,4-Dimethylphenol
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
2,4-Dinitrophenol
BRL
250
pg/L
70832 1
5/15/2006 8:51 PM
2,4-Dinitrotoluene
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
2,6-Dinitrotoluene
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
2-Chloronaphthalene
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
2-Chiorophenol
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
2-Methylnaphthalene
BRL
100
pg/L
70832 1
5/15/2006 &51 PM
2-Methylphenol
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
2-Nitroaniline
BRL
250
pg/L
70832 1
5115/2006 8:51 PM
2-Nitrophenol
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
3,3'-Dichlorobenzidine
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
3-Nitroaniline
BRL
250
pg/L
70832 1
5/15/2006 8:51 PM
4,6-Dinitro-2-methylphenol
BRL
250
pg/L
70832 1
5/15/2006 8;51 PM
4-Bromophenyl phenyl ether
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
4-Chloro-3-methylphenol
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
4-Chloroaniline
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
4-Chlorophenyl phenyl ether
BRL
100
pg1L
70832 1
5/16/2006 8:51 PM
4-Methylphenol
[140'-�
100
pg1L
70832 1
5115/2006 8:51 PM
4-Nitroaniline
BRL
250
pg/L
70832 1
5/1512006 8:51 PM
4-Nitrophenol
BRL
250
pg/L
70832 1
5115/2006 8:51 PM
Acenaphthene
BRL
100
pg/L
70832 1
511512006 8:51 PM
Acenaphthylene
BRL
100
pg/L
70832 1
5/1512006 8:51 PM
Acetophenone
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
Anthracene
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
Atrazine
BRL
100
pg/L
70832 1
5/15/2006 8:51 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
E
I:slimated (Value above quantitation range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H Holding times for preparation
or analysis exceeded
Narr
See Case narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method Blank
Page 22 of 30

Analytical Environmental Services, Inc. Date: 22-Muy-06
CLIENT: Tetra Tech EM Inc. Client Sample 1D: FT-11
Project: Synthron Inc. Collection Date: C5/I.1%2006 9 35:00 AM
Lab ID: 0605766-005 Matrix: S-URFACE-WATER
Analvses Result Reporting Qual Units BatchlD Dilution Date Analyzed
Limit Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Benzaldehyde
BRL
100
pglL
70832
1
5/15/2006 8:51 PM
Benzo(a)pyrene
BRL
100
pglL
70832
1
5/15/2006 8:51 PM
Benzo(b)fluoranthene
BRL
100
NgIL
70832
1
5/15/2006 8:51 PM
Benzo(g,h,i)perylene
BRL
100
pglL
70832
1
5/15/2006 8:51 PM
Benzo(k)fluoranthene
BRL
100
pg1L
70832
1
511512006 8:51 PM
Bis(2-chloroethoxy)methane
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Bis(2-chloroethyl)ether
BRL
100
NgIL
70632
1
5/15/2006 8:51 PM
Bis(2-chloroisopropyl)ether
BRL
100
pg1L
70832
1
5115/2006 8:51 PM
Bis(2-ethylhexyl)phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Butyl benzyl phthalate
BRL
100
pg1L
70832
1
5115/2006 8:51 PM
Caprolactam
BRL
100
pg1L
70832
1
511512006 8:51 PM
Carbazole
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Chrysene
BRL
100
pglL
70832
1
5/15/2006 8:51 PM
❑ibenz(a,h)anthracene
BRL
100
pg1L
70832
1
5115/2006 8:51 PM
Dibenzofuran
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Diethyl phthalate
BRL
100
pglL
70832
1
5/15/2006 6:51 PM
Dimethyl phthalate
BRL
100
pglL
70832
1
5115/2006 8:51 PM
Di-n-butyl phthalate
BRL
100
pglL
70832
1
5/15/2006 8:51 PM
Di-n-octyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Fluoranthene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Fluorene
BRL
100
pg1L
70832
1
5115/2006 8:51 PM
Hexachlorobenzene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Hexachlorobutadiene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Hexachlorocyclopentadiene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Hexachloroethane
BRL
100
pg1L
70832
1
5115/2006 8:51 PM
Ind eno(1,2,3-cd)pyrene
BRL
100
pg1L
70832
1
6115/20068:51 PM
Isophorone
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Naphthalene
BRL
100
pglL
70832
1
5/15/2006 8:51 PM
Nitrobenzene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
N-Nitrosodi-n-propylamine
BRL
100
Vg1L
70832
1
5/15/2006 8:51 PM
N-Nitrosodiphenylamine
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Pentachlorophenol
BRL
250
pg1L
70832
1
5/15/2006 8:51 PM
Phenanthrene
BRL
100
pg1L
70832
1
5115/2006 8:51 PM
Phenol.
= 100
pg/L
70832
1
5/15/2006 8:51 PM
Pyrene
BRL
100
pg1L
70832
1
6115/2006 8:51 PM
Surr: 2,4,6-Thbromophenol
89.7
64.8-129
%REC
70832
1
5/15/2006 8:51 PM
Surr: 2-Fluorobiphenyl
138.4
58.2-115
%REC
70832
1
5/15/2006 8:51 PM
Sum 2-Fluorophenol
72.8
24.4-115
%REC
70832
1
5115/2006 8:51 PM
Surr: 4-Terphenyl-d14
79.1
58.3-115
%REC
70832
1
5/15/2006 8:51 PM
Surr: NitrobenzeneA5
93.9
51.8-115
%REG
70832
1
5/15/2006 8:51 PM
Qualifiers: Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
11 Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
13 Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC NotConfirtned
Page 23 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc. Client Sample ID: NY 1.,
Project: Synthron Inc. Collection Date: f51.1 /2Q06.9735:00 AM
Lab ID: 0605766-005 Matrix: SURF.ACE W ETA
Analyses
Result Reporting Qua,
Limit
Units
BatchID Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
73.8 17.9-115
%REC
70832
1
5/15/2006 8:51 PM
TCL VOLATILE ORGANICS
SW8260B
(SW503013)
Analyst: NWH
11,1-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/20069A1 AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70849
1
511312006 9:11 AM
1,12-Trichloroethane
BRL
5.0
pg/L
70849
1
5113/20069:11 AM
1,1-Dichloroethane
BRL
5.0
pg/L
70849
1
5113/20069:11 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2,4-Trichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70849
1
5/1312006 9:11 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2-Dichlorobenzene
BRL
5.0
pg1L
70849
1
511312006 9:11 AM
1,2-Dichloroethane
BRL
5.0
pg1L
70849
1
511312006 9:11 AM
1,2-Dichloropropane
BRL
5.0
pg1L
70849
1
5113/2006 9:11 AM
1,3-Dichlorobenzene
BRL
5.0
pg1L
70849
1
5/1312006 9:11 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70849
1
511312006 9:11 AM
\� 2-8utanone
C-64:D
50
pg/L
70849
1
5/13/2006 9:11 AM
% 2-Hexanone
BRL
10
pg1L
70849
1
5/13/2006 9:11 AM
4-Methyl-2-pentanone
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Acetone- _S
CB60�
500
pg/L
70849
50
5/13/2006 3:08 AM
Benzene
BRL
5.0
pg/L
70B49
1
5/13/2006 9:11 AM
Bromodichloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Bromoform
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Bromomethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
disulfide_ �
r- 72
5.0
pg/L
70849
1
5/13/2006 9:11 AM
CCarbon
arbon tetrachloride
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Chlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Chloroethane
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Chloroform
BRL
5.0
pg/L
70B49
1
5/13/2006 9:11 AM
Chloromethane
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
cis-1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
cis- 1,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/13/2006 9:11 AM
Cyclohexane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Dibromochlorom ethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Dichloroditluoromethane
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Ethylbenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Freon-113
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
lsopropylbenzene
BRL
5.0
pg1L
70849
1
5/13/2006 9:11 AM
m,p-Xylene
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Methyl eta
18
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1 \ Methyl tert-butyl ether
BRL
5.0
pg1L
70849
1
5/13/2006 9:11 AM
Methylcyclohexane
BRL
5.0
pg/L
70a49
1
5/13/2006 9:11 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quanlitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 24 of 30

Analytical Environmental Services, Inc.
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-005
Date: 22-May-06
Client Sample ID: FT_7
Collection Date: S/T172006 :35.00 AM
]Matrix: SURI=ACE WAT� TER
Analyses
Result
Reporting Qua[ Units
BatchlD Dilution
Date Analyzed
Limit
Factor
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
p91L
70849 1
5/13/2006 9:11 AM
o-Xylene
BRL
5.0
pg1L
70849 1
5113/2006 9:11 AM
Styrene
BRL
5.0
pg/L
70849 1
511312006 9:11 AM
Tetrachloroethene
BRL
5.0
pg1L
70649 1
5/13/2006 9:11 AM
Toluene
BRL
5.0
pg1L
70849 1
5113/2006 9:11 AM
trans- 1,2-Dichloroethene
BRL
5.0
pg1L
70849 1
5113/2006 9:11 AM
trans- 1, 3-Dichloropropene
BRL
5.0
pg1L
70949 1
5/13/2006 9:11 AM
Trichloroethene
BRL
5.0
pg1L
70849 1
5/13/2006 9:11 AM
Trichlorofluoromethane
BRL
5.0
pg1L
70849 i
511312006 9:11 AM
Vinyl chloride
BRL
2.0
pg1L
70B49 1
5/13/2006 9:11 AM
Surr: 4-Bromofluorobenzene
99.4
63.7-115
%REC
70849 1
5/13/2006 9:11 AM
Surr: 4-Bromofluorobenzene
96.1
63.7-115
%REC
70849 50
511312006 3:08 AM
Surr. Dibromofluoromethane
95.1
70.4-123
%REC
70949 1
5/13/2006 9:11 AM
Surr: Dibromofluoromethane
93.7
70.4-123
%REC
70849 50
5/13/2006 3:08 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849 1
511312006 9:11 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849 50
5/1312006 3:08 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
215
50.0
mg1L
70797 10
511212006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen.Demand
1'440'--� 10
mg1L
70814 1
5/12/2006 3:45 PM
Qualifiers: Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
1 i Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 25 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: - FT- 12
Project: Synthron Inc.
Collection Date: 5/i
1/2006 9:55:00
AM
Lab ID: 0605766-006
Matrix: SURFACE WATER
Analyses
Result
Reporting
Qual Units $atchlD
Dilution
Date Analyzed
Limit
Factor
CHLORINATED PESTICIDES, TARGET COMPOLIN
SW8081A
(SW3510B)
Analyst: MM
4.4'-DDD
BRL
0.10
pg/L
70840
1
5/15/2006 10:49 PM
4,4'-DDE
BRL
0.10
pg/L
70840
1
5/15/2006 10:49 PM
4,4'-DOT
BRL
0.10
pg/L
70840
1
5/15/2006 10:49 PM
Aldrin
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
alpha-BHC
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
alpha -Chlordane
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
beta-BHC
BRL
0.050
pg/L
70a40
1
5/15/2006 10:49 PM
delta-BHC
BRL
0.050
pg/L
70a40
1
5/15/2006 10:49 PM
Dieldrin
BRL
0.10
pg/L
70a40
1
5/15/2006 10:49 PM
Endosultan I
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
Endosultan II
BRL
0.10
pg/L
70840
1
5/15/2006 10:49 PM
Endosultan sulfate
BRL
0.10
pg/L
70840
1
5/15/2006 10:49 PM
Endrin
BRL
0,10
pg/L
70a40
1
5/15/2006 10:49 PM
Endrin aldehyde
BRL
0.10
pg/L
70840
1
5/15/2006 10A9 PM
Endrin ketone
BRL
0.10
pg/L
70940
1
5/15/2006 10:49 PM
gamma-BHC
BRL
0.050
pg/L
70840
1
5M 5/2006 10:49 PM
gamma -Chlordane
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
Heptachlor
BRL
0.050
pg/L
70840
1
5115/2006 10:49 PM
Heptachlor epoxide
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
Methoxychlor
BRL
0.50
pg/L
70840
1
5/15/2006 10:49 PM
Toxaphene
BRL
5.0
pg/L
70840
1
5/15/2006 10:49 PM
Surr: Decachtorobiphenyl
14.1
17.9-122
S %REC 70840
1
5/15/2006 10:49 PM
Sutr: TetrachlOTO-m-xylene
104
18.9-119
%REC 70840
1
5/15/2006 10:49 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
[Aluminum
0.600
0,200
mg/L
70835
1
5/15/2006 5:42 PM
,Antimony
0.0257
0.0200
mg/L
70835
1
5/15/2006 5:42 PM
Arsenic
BRL
0.0500
mg/L
70835
1
5/1512006 5:42 PM
`Barium
0.0260
0.0200
mg/L
70835
1
5/15/2006 5:42 PM
Beryllium
BRL
0.0100
mg/L
70835
1
5/15/2006 5:42 PM
Cadmium
BRL
0.0050
mg/L
70835
1
5/15/2006 5:42 PM
Calcium
23.2
0.100
mg/L
70835
1
5115/2006 5:42 PM
Chromium
',0.0140
0.0100
mg1L
70835
1
5115/2006 5:42 PM
Cobalt
BRL
0.0200
mg1L
70835
1
5/15/2006 5:42 PM
Copper
0.0313
0.0100
mg/L
70835
1
5115/2006 5:42 PM
[Iron
13.1
0.100
mg/L
70835
1
5/15/2006 5:42 PM
Lead
0.0296
0.0100
mg/L
70835
1
5/15/2006 5:42 PM
Wagnesium
2.51
0.100
mg/L
70835
1
5/15/2006 5:42 PM
Manganese
0.787
0.0050
mg/L
70835
1
5/15/2006 5:42 PM
Molybdenum
BRL
0.0500
mg1L
70835
1
5115/2006 5:42 PM
`Nickel
0.0425
0.0200
mg/L
70835
1
5/15/2006 5A2 PM
'Potassium
8.35
0.500
mg1L
70835
1
5/15/2006 5:42 PM
Qualifiers: ' Value exceeds Maximum Contaminant
Level
F
Estimated (Value above quantization rangel
BRL Below Reporting Limit
S
Surrogate Recovery
outside accepted recovery limits
H Holding times for preparation
or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in [he associated Method Blank
Page 26 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-006
Client Sample 113" FT-12
Collection Date: 511 1/2006 9:55:00 AM
Matrix: SURFACE WATER !
Analyses
Result
Reporting Qual
Limit
Units
BatchlD
Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:42 PM
Silver
BRL
0.0100
mg1L
70835
1
5115/2006 5:42 PM
'.Sodium
57.7
1.00
mg/L
70835
1
5/15/2006 5:42 PM
Thallium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:42 PM
Tin
BRL
0.0500
mg1L
70835
1
5115/2006 5:42 PM
Titanium
BRL
0.0500
mg1L
70835
1
5/15/2006 5:42 PM
Vanadium
0.0268 '
0.0100
mg1L
70835
1
5/15/2006 5:42 PM
Zinc
1.06
0.0200
mg1L
70835
1
5/15/2006 5:42 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0,00020
mglL
70883
1
5/16/2006 2:39 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
10
uglL
70832
1
5/15/2006 9:17 PM
2,4,5-Trichlorophen ol
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
2,4,6-Trichlorophenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2,4-Dichlorophenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2,4-Dimethylphenol
BRL
10
pg1L
70832
1
5/1512006 9:17 PM
2,4-Dinitrophenol
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
2,4-Dinitrotoluene
BRL
10
pg1L
70832
1
511512006 9:17 PM
2,6-Dinitrotoluene
BRL
10
pg1L
70832
1
5/1512006 9:17 PM
2-Chloronaphthalene
BRL
10
NgIL
70832
1
.511512006 9:17 PM
2-Chlorophenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2-Methylnaphthalene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
2-Methylphenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
2-Nitrophenol
BRL
10
pglL
70832
1
5/15/2006 9.17 PM
3,3"-Dichlorobenzidine
BRL
10
pg1L
70832
1
511512006 9:17 PM
3-Nitroaniline
BRL
25
pg1L
70832
1
5/16/2006 9:17 PM
4,6-Dinitro-2-methylphenol
BRL
25
pglL
70832
1
5/15/2006 9:17 PM
4- Brom op henyl phenyl ether
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
4-Chloro-3-methylphenol
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
4-Chloroaniline
BRL
10
pglL
70832
1
5115/2006 9:17 PM
4-Chlorophenyt phenyl ether
BRL
10
pg1L
70832
1
5115/2006 9:17 PM
4-Methylphenol
BRL
10
pg1L
70832
1
5/1512006 9:17 PM
4-Nitroaniline
8RL
25
pg1L
70832
1
511512006 9:17 PM
4-Nitrophenol
BRL
25
pg1L
70832
1
5/15/2006 9:11 PM
Acenaphthene
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Acenaphthylene
8RL
10
pg1L
70832
1
5/15/2006 9:17 PM
Acetophenone
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Anthracene
BRL
10
pg1L
70832
1
5/1512006 9:17 PM
Atrazine
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Eistimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Nary See Case Narrative
NC Not Confinned
Page 27 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-006
Client Sample ID: / FT- 12
Collection Date: 5/11/2006 9:55:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting
Qual Units
BatchlD
Dilution
Date Analyzed
Limit
Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Benzaldehyde
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Benzo(a)pyrene
BRL
10
pg1L
.70832
1
5/15/2006 9:17 PM
Benzo(b)tluoranthene
BRL
10
pg1L
70832
1
6115/2006 9:17 PM
Benzo(g,h,i)perylene
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Benzo(k)fluoranthene
BRL
10
pg1L
70832
1
5/1512006 9:17 PM
Bis(2-chloroethoxy)methane
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Ris(2-chloroethyl)ether
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Bis(2-chloroisopropyl)ether
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Bis(2-ethythexyl)phthalate
31
10
pg1L
70832
1
5/15/2006 9:17 PM
Butyl benzyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Caprolactam
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Carbazole
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Chrysene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Dibenz(a,h)anthracene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Dibenzofuran
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Diethyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Dimethyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Di-n-butyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Di-n-octyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Fluoranthene
BRL
10
pg/L
70832
1
5/15/2006 9:47 PM
Fluorene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Hexachlorobenzene
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Hexachlorobutadiene
BRL
10
ttg/L
70832
1
5/15/2006 9:17 PM
Hexachlorocyclopentadiene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Hexachloroethane
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Indeno(1,2,3-cd)pyrene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
lsophorone
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Naphthalene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Nitrobenzene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
N-N itrosodi-n-propyla mine
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
N-Nitrosodiphenylamine
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Pentachlorophenol
BRL
25
pg/L
70832
1
5/15/2006 9:17 PM
Phenanthrene
BRL
10
}tg/L
70832
1
5/15/2006 9:17 PM
Phenol
BRL
10
pg1L
70832
1
5115/2006 9:17 PM
Pyrene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Surr: 2,4,6-Tdbromophenol
83.4
64.8-129
%REC
70832
1
5/15/2006 9:17 PM
Surr: 2-Fluorobiphenyi
82,6
58.2-115
%REC
70832
1
5/15/2006 9:17 PM
Surr: 2-Fluorophenol
67.7
24.4-115
%REC
70832
1
5/15/2006 9:17 PM
Surr: 4-Terphenyl-d14
68.0
58.3-115
%REC
70832
1
5/15/2006 9:17 PM
Surr: Nitrobenzene-d5
82.4
51.8-115
%REC
70832
1
5/15/2006 9:17 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated {Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 28 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID:' FT-12
Project: Synthron Inc.
Collection Date: 5/11/2006
9:55:00
AM
Lab ID: 0605766-006
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchID Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst DA
Surr: Phenol-d5
62.0
17.9-115
%REC
70832
1
5/1512006 9:17 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pglL
70849
1
511312C069:38AM
1,1,2,2-Telrachloroethene
BRL
5.0
pg1L
70849
1
5113/2006 9:38 AM
1,1,2-Trichloroethane
BRL
5.0
pg1L
70849
1
511312006 9:38 AM
1,1-Dichloroethane
BRL
5.0
pglL
70849
1
511312006 9:38 AM
1,1-Dichloroethene
BRL
5.0
pg1L
70B49
1
5113120069:38AM
1,2,4-Trichlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 9:38 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70849
1
511312006 9:38 AM
1,2-Dibromoethane
BRL
5.0
pg1L
70849
1
511312006 9:38 AM
1,2-Dichlorobenzene
BRL
5,0
pglL
70B49
1
511312006 9:38 AM
1,2-Dichloroethane
BRL
5.0
pg1L
70849
1
5/1312006 9:36 AM
1,2-Dichloropropane
BRL
5.0
pglL
70849
1
5/1312006 9:38 AM
1,3-Dichlorobenzene
BRL
5,0
pglL
70849
1
5/13/2006 9:38 AM
1,4-Dichlorobenzene
BRL
5,0
pglL
70849
1
5/1312006 9:38 AM
2-Butanone
BRL
50
pg1L
70849
1
5/13/2006 9:38 AM
2-Hexanone
BRL
10
pglL
70849
1
511312006 9:38 AM
4-Methyl-2-pentanone
BRL
10
pg1L
70849
1
511312006 9:38 AM
'Acetone
110
50
pglL
70849
1
511312006 9:38 AM
Benzene
BRL
5.0
pglL
70849
1
5/1312006 9:38 AM
Bromodichloromethane
BRL
5.0
pg1L
70849
1
5113/2006 9:38 AM
Bromoform
BRL
5.0
pg1L
70849
1
5/1312006 9:38 AM
Bromomethane
BRL
5.0
pglL
70849
1
511312006 9:38 AM
Carbon disulfide
BRL
5.0
pglL
70849
1
511312006 9:38 AM
Carbon tetrachloride
BRL
5.0
pg1L
70849
1
5/13/2006 9:38 AM
Chlorobenzene
BRL
5.0
pg1L
70849
1
511312006 9:38 AM
Chloroethane
BRL
10
pg1L
70B49
1
5/13/2006 9:38 AM
Chloroform
BRL
5.0
pg1L
70849
1
5/13/2006 9:38 AM
Chloromethane
BRL
10
pglL
70B49
1
5113/2006 9:38 AM
cis-1,2-Dichloroethene
BRL
5.0
pglL
70849
1
5M312006 9:38 AM
cis-1,3-Dichloropropene
BRL
5.0
pglL
70849
1
5/1312006 9:38 AM
Cyclohexane
BRL
5.0
pg1L
70949
1
5/13/2006 9:38 AM
Dibromochloromethane
BRL
5.0
pglL
70849
1
5/1312006 9:38 AM
Dichlorodifluoromethane
BRL
10
pg1L
70849
1
5/1312006 9-38 AM
Ethylbenzene
BRL
5.0
pglL
70849
1
5113I2006 9-38 AM
Freon-113
BRL
10
pg/L
70849
1
5/1312006 9:38 AM
Isopropylbenzene
BRL
5,0
pg1L
70849
1
511312006 9:38 AM
m,p-Xylene
BRL
10
pglL
70849
1
5113f2006 9-38 AM
Methyl acetate
BRL
5.0
pg1L
70849
1
5/1312006 9:38 AM
Methyl tert-butyl ether
BRL
5.0
pglL
70849
1
5/1312006 9:38 AM
Methylcyclohexane
BRL
5,0
pg1L
70849
1
5/13/2006 9:38 AM
Qualifiers: * Valuc exceeds Maximum Contaminant Level
BRL Below Reporling Limit
H Holding times for preparation or analysis exceeded
N Analyte not NFLAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantization range)
S Surrogate Recovery outside accepted recovery limits
Nary See Case Narrative
NC Not Confirmed
Page 29 of 30

Analytical Environmental Services, Inc.
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-006
Date: 22-Mav-06
Client Sample ID: FT-12
Collection Date: 5/1 1/2006 9:55:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual Units
BatchlD Dilution
Date Analyzed
Limit
Factor
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methyiene chloride
BRL
5.0
pglL
70849
1
5/13/2006 9:38 AM
o-Xylene
BRL
5.0
pg1L
70849
1
5/13/2006 9:38 AM
Styrene
BRL
5.0
pg1L
70849
1
5/13/2006 9:38 AM
Tetrachloroethene
BRL
5.0
pglL
70849
1
5/13/2006 9:38 AM
Toluene
BRL
5.0
pg1L
70849
1
5/13/2006 9:36 AM
trans-1,2-Dichloroethene
BRL
5.0
pglL
70849
1
5/13/2006 9:38 AM
trans-1,3-Dichloropropene
BRL
5.0
pglL
70849
1
5/13/2006 9:38 AM
Trichloroethene
BRL
5.0
pglL
70849
1
5/13/2006 938 AM
Trichlorofl uorom ethane
BRL
50
pglL
70849
1
5/13/2006 9:38 AM
Vinyl chloride
BRL
2.0
pglL
70849
1
5/13/2006 9:38 AM
Surr: 4-Bromofluorobenzene
96.5
63.7-115
%REC
70849
1
5/13/2006 9:38 AM
Surr: Dibromoflueromethane
95.0
70.4-123
%REC
70849
1
5/13/2006 9:38 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849
1
5/1312006 9:38 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst; CAM
Biochemical Oxygen Demand
._44.2
40.0
mg1L
70797
10
5/12/2006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
633
10
mg1L
70814
1
5/12/2006 3:45 PM
Qualifiers: Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N "alyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quandtation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 30 of 30

Synthron reveiw
Subject: Synthron reveiw
From: Sandy Mort <[e-mail]>
Date: Tue, 23 May 2006 16:05:27 -0400
To: Larry Frost <[e-mail]>
Attached are the spreadsheets I generated to calculate hazard quotients (HQs) based
on NAWQC and ecological screening values (per risk assessment guidelines, also
called toxicity benchmarks). HQ = chemical cone./screening value, HQ > 1.0 or
summed HQ >1.0 for toxicants acting on the same target organ, or by the same mode
of action, indicate the potential for toxic impacts. If a NAWQC value was not
available, I next used the other listed ESVs in the order listed from left to right across
the spreadsheet.
Summed HQs are shown at the bottom of the acute & chronic QQ columns.
Application of the 9% IWC dilution is also shown under the summed HQs.
calculated hardness values for each tank, as mg CaCO3/L
FT-07 59.4 mg/L
FT-08 67.1
FT-09
101.7
FT-10
117.3
FT-11
90.0
FT-12
68.3
Toxicity benchmarks for some metals are adjusted to 100 mg/L hardness. Sample
hardness <100 mg/L may indicate the potential for increased toxicity as related to the
calculated HQ.
Sandy Mort, Environmental Biologist
Aquatic Toxicology Unit
NC DENR Div. of Water Quality
location: 4401 Reedy Creek Road
Raleigh, NC 27607
phone: [phone] x242
e-mail: sandy.mortCa7ncmail.net
mail: Mail Service Center 1621
Raleigh, NC 27699-1621
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Synthron reveiw
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2 of 2 5/24/2006 12:16 PM

ECOLOGICAL SCREENING VALUES, RA
FRESHWATER SURFACE WATER
All defa in ug/L (ppb)
Ij(�
compound
CAS
rotas,
99n.
NAWQC
CMC,
awte
NAWQC
CCC,
ohrenk
USEPA
A".4,
aeufe SY �.hrowc
USEPA
Re9.4.
SV
Reg 4 net
NOAA
SQUIRT,
CMC acute
1I.AA
5QuiRT,
CCC
chronic
NOAA We
Tier II
SAY
(ORNIL)
Tier II
SCV
(OR1,L)
Lew
chronic
EC20,
fish
Law chronic
EC20,
daphnids
Sensiti s:
speeies
EC20,
dephnlds
Pain.
chronic
EC20
ACENAPHTHENE
83329
L-PAH
L70
17
2; spc
1700
5201
LOEL
acenophthykne
208968
28,000
1500
ocrokin
6.8
2.1
3,1 spc
acrylonitrik
755
75.5
4,- spc
Odin
309002
pest
3.0
3
0.3
1.5
ANTHRACENE
120127
L-PAH
13
0.73
0.035
>8 2
banzene
530
53
7; spc
2300
130
21
229
benzidine
82875 i
250
25
4,-spc
2500
70
3.9
158
68
BENZO(A)ANTHRALD,E
56553
H-PAH
0.49
0.027
BENZO(A"ENE
50328
H-PAH
024
0.014
QL99
BENZO(B)FLUORANTHENE
205992
H-PAH
bcnzo(q,hj)p lene
191242
H-PAH
BENZO(K)FLUORANTHENE
207089
H-PAH
benzoic aid
65850
740
42
7409
1259
benzYl alcohol
100516
150
8.6
550
375
BHC, a-
pest•d
500
law (phnt)
39
2.2
BHC, b-
pcft-d
5000
low
39
2.2
8HC.9- (lied-)
pest
0.95
2
0,08
_(plant)
<1.1
S1
0.11
bis(2Zethy1h I)phthalote
27
3,0
54.3
50
bu�1 bcn,z r�l phtfieSate
85687
330
22
4,2spc
940
3
LOEL. class
19
carbon tetrachloride
I80
9.8
65
224
eh lardane
57748
24
0.0043
2.4
000-431
f
1.2
0.00215
<0.25
12.1
0.50
0.71
chloroaniline. 4-
106478
250
50
LOEL, class
chloroben:ene
1100
64
1002
165
chloroform
49D
28
8400
562
chloronaphthokne, 2-
91587
1600
LOEL
ch1Fienel, 2-
95578
438
43.8
5; spc
4380
LOEL
chloropyrifosT
2921882
0.083
0.41
0.083
0.041
0.083
0.041
CHRYSENE
218019
_pelt
H-PAH
DDD, p,p- (TDE)
72548
Pest-d
0.064
0.DO64
8,-spc
0,6
LOEL
0.19
0.011
3.99
0.61
DDE, P.4 -
72559
-d
105
10.5
1,-spc
1050
LOEL
DDT, ,P-
50293
pey
LI
0.001
1.1
0001
0.55
OM05
0.013
DDT, total
st
0.35
0008
dVj2thtylhexy_I] phthalate
117817
400
360
diaziran
0.17
0.043
dibenz[a,hpnihracene
53703
dibanzofuron
132649
66
3.7
diehlar enal, 2.4-
120832
202
36.5
3.1 spc
2020
365
LOEL
dieldrin
60571
Pc#
024
0.0%
2.5
0.0019
mf-chr
0.24
0.056
1
diethyl othalate
84662
5210
521
2,•spa
940
3
LOEL. chss
t800
210
1000
d-thyl phtholate
131113
3300
330
2,.spc
940
3
LOEL, class
dimeth Iphenol, 2,4-
10567R
212
21.2
3,- spc
2120
di•n•butyl phthalate
84742
94
9-4
6,-spe
940
3
LOEL, class
190
35
270
500
251
dinitr nal
51285
230
150
LOEL.cbss
dinitrcphenol, 2,4-
62
62
3,- spc
dinitrataluerre, 2,4-
121142
310D
310
2,-spc
330
230
LOEL
di-n-ocy phtholt.
117840
940
3
LOEL, class
'100
310
1995
dipharylhydrozina, 1,2-
122667
27
2.7
2.-spc
270
LOEL
andosulfan(a 6 B)
115297
Pest
0.11
0.028
0.051
cndosulfan sulfate
1031078
endosulfon, e-
9599a8
st
0.22
0.056
0.22
0.0%
endasulfm, 6-
33213659
pest_
0.22
0,056
0.22
0.056
erdrin
72208
past
0.096
0.036
0.19
0.OD23
mf
0,086
0.036
1
endrin aldehyde
7421934
IEEF:
i
t
I
FLUORANTHEW
206M0
H-PAH
399
39.8
2,-spc
2980
LOEL
32
FLU0RENE
96767
L-PAH
7p
3.9
ESVMetalsTotal 0506,Ms 5/2412006

conpaund
CAS
mtes,
gen.
NAWQC
CMC,
cafe
NAWCIC
CCC,
chronic
USDA
Reg. 4,
ante SV
LISEPA
Reg. 4,
chronic SY
Reg 4 not
NOAA
SQUAT.
CAC awte
NOAA
SQuiRT,
CCC
chronic
NOAA mh
Tier II
SAY
{CMNL)
Tier II
SCY
{ORNL)
Lear
chronic
EC20,
fish
Low chronic
EC20,
dsphnlds
Sensitive
Wei"
EC2o,
dophnids
Popul.
chronic
EC20
heptachlor
76448
pest
0.52
0.0038
0.52
0.0030
mf-dw
0.26
0.0019
0.125
0.0069
0.86
0,0041
0.1
heptxhlar epoxide
1024573
pest-d
0.52
0.0038
0.52
0.0038
mf-chr
0.26
0.0019
hexachlorobenzere
116741
6
3,68
hcxechlerobsaodiene
87683
9
0.93
5,lspc
90
9.3
LOEL
hexochlorocyclohexone{BHC)
608731
l00
LOEL
hexochlcracthene
67721
98
9.8
5.-spc
980
540
LOEL
210
12
hexachlerepentodiene
77474
7
5.2
LOEL
hexane
28,995
hexenene, 2-
_ _ .-
-- --
_ _ -- _
16.155
_
1259
L_dene(1,2 3-ed�yrene
193395
H-PAH
isophoront
78591
117000
LOEL
hndane
58899
0,95
0.08
m lathion
121755
Port
0.1
0.1
03
methoxychlor
72435
Pest
0.03
0.03
0.03
0.019
methyl ncphtholcm. t-
37
2.1
500
31.62
METHYL NAPHTHALENE, 2-
91576
L-PAH
Lcthylphenol, 2• (o-cresol)
95487
230
13
470
74
methLphenel, 4� (p.cresol)
106445
mirex
2385855
pest
0.001
O.00t
0.-I
NAPHTHALENE
91203
L-PAH
230
62
4,Ispc
190
12
450600
1000
nitrobenzene
98953
2700
270
2,-spc
27,000
LOEL
nitropheml, 2-
3500
nitrcphcnol, 4-
100027
828
82.8
3,- spc
230
150
LOEL, class
1200
300
464
5000
60
-,tromdiphe famine
86306
5851
58.5
2,-pc
5850
3,300,000
LOEL. class
3800
210
339
40
PAHs. HMW
PAHs, LMW
PAHs, total
parathion
131
0.065
0013
0.065
0.013
parathion mixture
56382
pen
0.065
0.013
PC6.1016
PC8
0.2
0.014
7; spc
PCB-1221
PCB
02
0.014
7,- c
50
0.28
BO
10
PCB-1232
PC8
0.2
0.014
7,-sp.
IOT
0.58
I48
16
PC94242
PCB
0.2
0.014
7,-spc
1.2
0.053
<2.9
t,58
PCO-1248
I PC8
0.2
0.014
T,-spc
1.4
O.OSI
0.4
2.5
t.26
PC8.1254
PCB
0.2
0.014
T,-spc
0.60
0.033
0.52
1.2
0.63
PCB-)260
PCB
0.2
0.014
7; spc
1700
94
2.1
316
PCBs
1336363
0014
2
OD14
0.014
0.4
12
0.63
pentuchlo benzene
608935
250
50
250
50
LOEL, class
8.4
047
pentochlaropheml (PCP)
87865
19
15
20
13
4-pH
19
15
B pH 7.8, 2
PHEMANTMENE
85018
L-PAH
110
phenol
108952
1020
256
16,1 c
10.200
2560
LOEL
Q30
4467
propawl, 2-
35,381
3162
PYRENE
129000
H-PAH
TCDD,23,78-(dioxin}
1746016
0.1
0.00001
mf
•0.01
�0.00001
LOEL
tetruchlarobenzene, 1,2 4,5-
95943
250
50
250
50
LOEL, class
tetrachlareethene (PERC)
127184
YOC
529
84
5,lspc
5280
840
LOEL
830
98
500
510
50
tetrochlorophcnel, 2,3,4,6-
58902
toluene
108883
YOC
1750
175
5spc(ocu)
17,500
LOEL
120
9.8
Q6
0.0252 (LCV)
200
toxophene
8001352
0.73
0.0002
073
0.0002
mf
0.73
0,0002
triehlarebenzene, 1 2,4-
150
44.9
4,tspc
rKchloroethene (TCE)
79416
YOC
45.000
21,900
LOEL
440
47
5,758
7260 (LCV)
232
tri6lorapherol,2,4,6-
88062
32
3.2
3,-spc
970
LOEL
ESVMotal3Total_0506.)ds SIM2006

Flq�,racTr�iyouFFNIN6 VALUES, RA I I I ! I
I
I
I
I
fRSSHWATER SURFACE WATER � Sum metals in all Frac Tanks FT�07-th^r�u- FT- i�2, s1-m
95/23/06
compound
site cone,
ug/L
acute
HQ
chronic
HQ
NAWQC
CMC,
acute (1)
NAWQC
CCC,
chronic
(1)
NAWQC
notes
USEPA
Reg. 4,
acute SV
USEPA
Reg. 4,
chronic SV
Reg 4
note
NOAA
SQuiRT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
USEPA
Tier II
SAV
(ORNL)
USEPA
Tier II
SCV
(ORNL)
Low
chronic
EC20, fish
Low
chronic
EC20,
dophnids
Sensitive
species
EC20,
dophnids
Popul.
chronic
EC20
METALS,_gg/L (pD_b)
aluminum
40,130
53,51
461,26
750
87
pH 6.5.9.0
750
87
pH 6.5-9.0
756
87
pH
4700
540
75
antimony
495
0.38
3.10
1300
160
88
30
180
30
2310
1900
79
arsenic, total
0.00
0.00
340
150
340
150
d
arsenic•3
360
190
2130
633
55
1995
arsenic +5
950
66
3.1
1500
�932
185
barium
420
3.82
105,05
110
4.0
beryllium
0.00
0.00
16
0.53
130
5.3
LOEL
35
0.66
1:48
3.8
21
cadmium (h)
6.2
1.44
2.82
4.3
2.2
1.79
0.66
h
4.3
2.2
h,d
1.8
0.75
0.013
4.3
chromium, total
241
0,42
3.26
chromium •3 (h)
570
74
994.32
117.32
h
570
74
h,d
89
8.44
126
chromium •6 (h)
16
11
16
11
h
16
11
d
1
51
&5
0,266
316
cobalt
127
0.08
5.51
15001
23
810
<4.413.98
capper (h)
768
59.06
85.31
13
9.0
9.22
6.54
h
13
9
h,d
5
0.205
0.26
8.6
+ron
118.600
118.60
118.60
1000
1000
1000
16
lead (h)
591
9.10
236.48
65
2.5
3378
1.32
h
65
2.5
h,d
22
0.35
71
lithium
0.00
0.00
260
14
magnesium
22,628
manganese
5,235
2,28
43,63
2300
120
1270
<1100
112
mercury
0,610
0.44
O.79
1.4
0.77
2.40
OrM
1.4
0.77
d
mercury, inorganic or total
1.30
0.87
0,87
0.18
0,32
mercury, methyl
0.099
0.0028
<0.03
0,87
O.28
molybdenum
16,000
370
360
nickel
348
0.74
6.68
470
52
1
789.00
57,71
h
470
52
h,d
62
45
Il
215
selenium
0.00
0.00
5.0
20.00
5.00
40
25
2.60
selenium, total
186
5
d
silver
3.4
1.23
O.OI2
h
1.7
0.12
h,d
0.36
0.20
<0.561
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
110
12
81
64
67
tin
540
0.31
11.51
2700
73
tin as T$T
24;480
-204.00
204-00
0.46
-120
0,063
(26-
b5:04
0.026
58:91
0.46
120
0.063
120
21
80
zinc
-F--
47
hardness, as CaCO3, mg/L
hardness, calculated, mg/L
Ina onics mist /L
cyanide
22
5222
5.2
22
5.2
5.3
1.17
11
chlorine
19
11
fluorine
�
5336
3706
1
1080
SUM HQs
,apply97.IWC
1454,176
1 40.4
12811
115.4
i
ES VMletalsTotal 0508.1. x l S

RE�i H� Y N6 VAl.F1�S RA
� Frac Tanks FT-07 thrul FT-12,�slIm 5/3�/061
FRESHWATERSURFACE WATER Highest �each [M] in
compound
site cant.,
ug/L
acute
HQ
chronic
HQ
NAWQC
CMC,
acute (1)
NAWQC
CCC,
chronic
(1)
NAWQC
notes
USEPA
Reg. 4,
acute SV
USEPA
Reg. 4,
chronic SV
Reg 4
note
NOAA
SQuiRT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
USEPA
Tier 11
5AV
(ORNL)
USEPA
Tier II
SCV
(ORNQ
Law
chronic
EC20, fish
Low
chronic
EC20,
daphnids
Sensitive
species
EC20,
daphnids
Popul.
chronic
EC20
METALS, %g {vob)
aluminum
22,3D0
29.73
256.32
750
87
pH 8.8-9,0
750
87
pH 6.5-9.0
750
87
pH
4700
540
75
antimony
211
0.16
1.32
1300
160
88
30
180
30
2310
1900
79
arsenic, total
0,00
0.00
340
150
340
150
d
arsenic •3
360
190
2130
633
55
1995
arsenic -5
850
1
66
3.1
1500
>932
185
barium
214
1,95
53.50
1
110
4.0
beryllium
0.00
0.00
16
0,53
130
5.3
LOEL
35
0.66
148
3.8
21
cadmium (h)
6.2
1.44
2.82
4.3
2.2
L79
0.66
h
4.3
2.2
h,d
1,8
0.75
0.013
4.3
chromium, total
81.5
0.14
1.10
chromium+3 (h)
570
74
984.32
117.32
h
570
74
h,d
89
8.44
126
chromium •6 (h)
16
11
16
II
h
16
11
d
51
0.5
0.266
316
cobalt
36
0.02
L56
1500
23
810
4A
3.98
copper (h)
258
19.85
28.67
13
9.0
9.22
6.54
h
13
9
h,d
5
0.205
0.26
8.6
iron
34,400
34.4D
34.40
1000
1000
1000
16
leod (h)
lithium
163
2.51
0.00
65.20
0.00
65
2.5
33.78
1,32
h
65
2.5
h,d
260
14
22
0.35
71
magnesium
8,330
Manganese
1,270
0.55
10.58
2300
120
1270
�1100
112
mercury
0.380
0.27
0.49
1.4
0.77
2.40
0.012
1.4
0.77
d
mercury, inorganic or total
1.30
0.87
0.87
0.18
0.32
mercury, methyl
0.099
0.0028
<0.03
0.87
0.28
molybdenum
16,000
370
360
nickel
74
0,16
1.42
470
52
789.00
87.71
h
470
52
h,d
62
45
11
215
selenium
0.00
0.00
5.0
20,00
5.00
40
25
2.60
selenium, total
186
5
d
silver
3.4
1,23
0,012
h
1.7
0.12
h,d
0.36
0.20
<0.56
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
110
12
81
64
67
tin
430
0.16
5.89
2700
73
tin as TBT
0.46
0,063
0.026
0.46
0.063
zinc
8,800
73.33
73.33
120
120
65.04
58.91
h
120
120
h
47
21
BO
hardness, as CaCO3, mg/L
hardness, calculated, mg/L
Inorganics, mist,- ug/L
cyanide
22
5.2
22
5.2
22
5.2
5.3
1,17
ll
chlorine
19
11
fluorine
5336
3706
1080
SUM HQs
164,677
536.611
--
-
apply 9%IWC
1 14.81
48.3
i
ESVMetalsHigh_0506-t .xls

FCnI,C I��I SC?F,FNIW,VALI)ES, RA I I I I I I
FRESHWATER SURFACE WATER r FT-09, s[m 5/23106
I I
I
!
I
compound
site cant.,
ug/L
acute
HQ
chronic
HQ
NAWQC
CMC,
acute (1)
NAWQC I
CCC,
chronic
(1)
NAWQC
notes
USEPA
Reg. 4,
acute SV
USEPA
Reg, 4,
chronic 5V
Reg 4
note
NOAA
SQuiRT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
USEPA
Tier II
5AV
(ORNL)
USEPA
Tier II
SCV
(ORNQ
Low
chronic
EC20, fish
Low
chronic
EC20,
daphnids
Sensitive
species
EC20,
daphnids
P.P.I.
chronic
EC20
METALS. Mg {oobl
aluminum
22300.00
29.73
256,32
750
87
pH 6.5-9.0
750
87
pH 6,5-9,C
750
87
pH
4700
540
75
antimony
211.00
0.16
1.32
1300
160
88
30
180
30
2310
1900
79
arsenic, total
0.00
0,00
340
150
340
150
d
arsenic .3
360
190
2130
633
55
1995
arsenic .5
850
66
It
1500
�932
155
barium
214.00
1.95
53.50
110
4,0
beryllium
0.00
0.00
16
0.53
130
5.3
LOEL
35
0.66
148
3.8
21
cadmium (h)
0.00
0.00
4.3
2,2
1,79
0.66
h
4.3
2.2
h,d
1.8
0.75
0.013
4.3
chromium, total
81.50
0.14
1.10
chromium -3 (h)
570
74
984.32
117.32
h
570
74
h,d
89
8.44
126
chromium •6 (h)
16
11
16
11
h
16
11
d
51
0.5
0.266
316
cobalt
35.90
0.02
1.56
1500
23
810
�4.4
3.98
copper (h)
258.00
19.85
28.67
13
9.0
9.22
6.54
h
13
9
h,d
5
0.205
0.26
8.6
iron
34400.D0
34.40
34.40
1000
1000
1000
16
lead (h)
133.00
2.05
53.20
65
2.5
33.78
1.32
h
65
2.5
h,d
22
0.35
71
lithium
0.001
0.00
260
14
magnesium
8330.00
manganese
1080,00
0.47
9.00
2300
120
1270
<1100
212
mercury
0.38
0.27
0.49
1.4
0.77
2.40
0.012
1.4
0.77
d
mercury, inorganic or total
i 130
0.87
0.87
0.18
0.32
mercury, methyl
0.099
0,0028
0.03
0.87
0.28
molybdenum
16,000
370
360
nickel
74,00
0.16
1.42
470
52
789.00
87.71
h
470
52
h,d
62
45
11
215
selenium
0,00
0.00
5.0
20.00
5.00
40
25
2.60
selenium, total
186
5
d
silver
3.4
1.23
0.012
h
1.7
0.12
h,d
0.36
0.20
0.56
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
110
12
81
64
67
tin
43D.D0
0.16
5.89
'
2700
73
tin as TBT
0.46
0.063
0.026
0.46
0.063
zinc
4340.00
36.17
36.17
120
120
65,04
58.91
h
t20
120
h
47
21
80
hardness, as CoCO3, mg/L
hardness, calculated, mg/L
Inorganics, mist., ua/L
cyanide
22
5.2
22
5.2
22
5.2
5.3
1.17
11
chlorine
19
11
fluorine
5336
3706
1080
SUM HQs
apply 9%IWC
125.52
11,30
483.04
43.47
ESVMetalsF'T09 050E-1.xls

ECOLOGICAL SCREEMNG_VALUES, RA
tIt
FRESHWATER 5URFACE WATER FT-12, sl(m 5/23/06 t
compound
site conc.,
ug/L
acute
HQ
chronic
HQ
NAWQC
CMC,
acute (1)
NAWQC
CCC,
chronic
(1)
NAWQC
notes
U5EPA
Reg. 4,
acute SV
USEPA
Reg, 4,
chronic 5V
Reg 4
note
NOAA
SQuiRT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
VSEPA
Tier II
SAV
(ORNL)
VSEPA
Tier II
SCV
(ORNL)
Low
chronic
EC20, fish
Low
chronic
EC20,
daphnids
Sensitive
species
EC20,
daphnids
Popul.
chronic
EC20
METALS. ug/L (ppb3
aluminum
600.00
0,80
6.90
750
87
pH 6.5-9.0
750
87
pH 6.5-9.0
750
87
pH
4700
540
75
antimony
25.70
0.02
0.16
1300
160
88
30
180
30
2310
1900
79
arsenic, total
0.00
0.00
340
150
340
150
d
arsenic •3
360
190
2130
633
55
1995
arsenic -5
850
66
3.1
1500
)932
165
barium
26.00
0.24
6.50
110
4.0
beryllium
0.00
0.00
16
0.53
130
5.3
LOEL
35
0.66
148
3.8
21
cadmium (h)
0.00
0.00
4.3
2.2
1.79
0.66
h
4.3
2.2
h,d
1.8
0.75
0.013
4.3
chromium, total
14.00
0,02
0.19
chromium +3 (h)
570
74
984.32
117.32
h
570
74
h,d
89
8.44
126
chromium -6 (h)
16
11
16
11
h
16
11
d
51
0.5
0.266
316
cobalt
0.00
0.00
1500
23
810
<4.4
3.98
copper (h)
31.30
2.41
3.48
13
9.0
9.22
6.54
h
13
9
h,d
5
0.205
0.26
8.6
iron
13100.00
13.10
13.10
1000
1000
1000
16
lead (h)
29.60
0,46
11.84
65
2.5
33.78
1.32
h
65
2,5
h,d
22
0.35
71
lithium
0.00
0.00
260
14
magnesium
2510.00
manganese
787.00
0.34
6.56
2300
120
1270
<1100
112
mercury
0.00
0.00
1.4
0.77
2.40
0.012
L4
0.77
d
mercury, inorganic or total
1.30
0.87
0,87
01181
0,32
mercury, methyl
0.099
0,0028
<0.03
0.87
0.28
molybdenum
16,000
370
360
nickel
42,50
0.09
0.82
470
52
789.00
87.71
h
470
52
h,d
62
45
11
215
selenium
0.00
0.00
5.0
20.00
5.00
40
25
2.60
selenium, total
186
5
d
silver
3.4
1.23
0.012
h
L7
0,12
h,d
0.36
0.20
<0.56
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
110
12
81
64
1 67
tin
102.00
0.04
1,40
2700
73
tin as TST
0.46
0,063
0.026
0.46
0.063
zinc
1060.00
8.83
8.83
120
120
65.04
56.91
h
120
120
h
47
21
80
hardness, as CoCO3, mg/L-
hardness, calculated, mg/L
Inorganics. mist., ug/L
cyanide
22
5.2
22
5.2
22
5.2
5.3
t.17
t1
chlorine
19
ll
fluorine
5336
3706
1080
SUM HQs
apply 9%IWC
I 1 2 2.37
5 5.38
ESVMetalsFT12 0506-1.xls

ECO1.06IC.AL SCREENING VALUES, RA _a
FRESHWATER SURFACE WATER FT-08, slm5/23/06
F
f�
- -
-i
1
compound
site conc.,
ug/L
acute
HQ
chronic
HQ
NAWQC
CMC,
acute (1)
NAWQC
CCC,
chronic
(1)
NAWQC
notes
USEPA
Reg. 4,
acute SV
USEPA
Reg, 4,
chronic SV
Reg 4
note
NOAA
SQuiRT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
USEPA
Tier II
SAV
(ORNL)
USEPA
Tier II
5CV
(ORNL)
Law
chronic
EC20, fish
Low
chronic
EC20,
daphnids
Sensitive
species
EC20,
daphnids
Popul.
chronic
EC20
METALS. ug/L (oob]
aluminum
4470.00
5.96
51,38
750
87
pH 6.5-9.0
750
87
pH 6.5-9-C
MO
87
pH
4700
540
75
antimony
40.00
0.03
0.25
1300
160
88
30
180
30
2310
1900
79
arsenic, total
0.00
0.00
340
150
340
150
d
arsenic •3
360
190
2130
633
55
1995
arsenic *5
850
66
3.1
1500
)932
185
barium
41.10
0.37
10,28
110
4.0
beryllium
0.00
0.00
16
0.53
130
5.3
LOEL
35
0.66
148
3.8
21
cadmium (h)
0.00
0.00
4.3 1
2,2
1.79
0.66
h
4.3
2.2
h,d
1.8
0.751
0.013
4,3
chromium, total
31.60
0.06
0,43
chromium •3 (h)
570
74
984.32
117.32
h
570
74
h,d
89
8,44
126
chromium •6 (h)
16
11
16
11
h
16
11
d
51
0.5
0.266
316
cobalt
31.60
0.02
1,38
1500
23
810
<4.4
3.98
copper (h)
81.80
6.29
9.09
13
9.0
9.Z2
6.54
h
13
9
h,d
5
0,205
0.26
8.6
iron
27100.00
27.10
27,10
1000
1000
1000
16
lead (b)
81.60
1,26
32.64
65
2.5
33,78
1.32
h
65
2.5
h,d
22
0.35
71
lithium
0.00
0.00
260
14
magnesium
2830.00
manganese
951.00
0.41
7.93
2300
120
1270
<1100
112
mercury
0.00
0,00
1.4
0.77
2.40
0,012
1.4
0.77
d
mercury, inorganic or total
1.30
0.87
0,87
0.18
0.32
mercury, methyl
0.099
0.0028
0.03
0.87
0.28
molybdenum
16,000
370
360
nickel
63.10
0.13
1.21
470
52
789.00
8711
h
470
52
h,d
62
45
11
215
selenium
0.00
0.00
5.0
20.00
5.00
40
25
2.6C
setenium, total
186
.5
d
silver
3.4
1.231
0.012
h
1.7
O.1Z
h,d
0.36
0.20
0.56
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
110
12
81
64
67
tin
68.80
0.03
0.94
2700
73
tin as TBT
0.46
0.063
0.026
0.46
0.063
zinc
2300.00
19.17
1917.
120
120
65.04
58.91
h
120
120
h
47
21
80
hardness, as CoCO3, mg/L
hardness, calculated, mg/L
Inorganics, mist., uq/L
cyanide
22
5.2
22
i.2
22
5.2
5.3
1.17
11
chlorine
19
11
fluorine
5336
3706
1080
5UM HQs
[apply 9%1WC
60.83
1 5.471
161.79
14.56
ESVMeta1sFT08 0506-t,xls

RA
FRESHWATER S1IRFACE WATERS FTrT 11.„sli 6/23/061�
compound
site cone.,
ug/L
acute
HQ
chronic
HQ
NAWQC
CMC,
acute (1)
NAWQC
CCC,
chronic
(1)
NAWQC
notes
USEPA
Reg. 4,
acute SV
USEPA
Reg. 4,
chronic 5V
Reg 4
note
NOAA
SQuiRT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
USEPA
Tier II
SAV
(ORNL)
USEPA
Tier II
SCV
(ORNQ
Low
chronic
EC20, fish
Low
chronic
EC20,
daphnids
Sensitive
species
EC20,
daphnids
Popul.
chronic
EC20
METALS. ug/L fAab)
aluminum
2620.00
3.49
30.11
750
87
pH 6.540
750
87
pH 6.5-9.0
750
87
pH
4700
540
75
antimony
56.00
0.04
0.35
1300
160
B8
30
180
30
2310
1900
79
arsenic, total
0.00
0.00
340
150
340
150
d
arsenic •3
360
190
2130
633
55
1995
arsenic .5
850
66
3.1
1500
>932
185
barium
37.70
0.34
9.43
110
4.0
beryllium
0.00
0.00
16
0.53
130
5.3
LOEL
35
0.66
148
3.8
21
cadmium (h)
6.20
1.44
2.82
4.3
2.2
1.79
0.66
h
4.3
2.2
h,d
1.8
0.75
0.013
4.3
chromium, total
41.40
0.07
0,56
chromium *3 (h)
570
74
984.32
117.32
h
570
74
h,d
89
8.44
126
chromium *6 (h)
16
11
16
11
h
16
11
d
51
0.5
0,266
316
cobalt
34.70
0.02
1.51
1500
23
810
<4.4
3.98
copper (h)
129M
9.92
14.33
13
9.0
9,22
6.54
h
13
9
h,d
5
0.205
0.26
B.6
iron
33000.00
33.00
33.00
1006
1000
1000
16
lead (h)
128.00
1.97
51.20
65
2.5
33.78
1.32
h
65
2.5
h,d
22
0.35
71
lithium
0.00
0.00
260
14
magnesium
3840.00
manganese
1270.00
0.55
10.58
2300
120
1270
<11001
Ill
mercury
0.23
0.16
0.30
1.4
0.77
2.40
0.012
1.4
0.77
d
mercury, inorganic or total
1.30
0.87
0.87
OAB
0.32
mercury, methyl
0.099
0.002B
+0.03
0.87
0.28
molybdenum
16,000
370
360
nickel
67.60
0.14
1.30
470
52
789.00
87.71
h
470
52
h,d
62
45
11
215
selenium
0.00
0.00
5.0
20.00
5.00
40
25
2.60
selenium, total
186
5
d
silver
3.4
1.23
0.012
h
1.7
0.12
h,d
0,36
0.20
0.56
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
1101
12
81
64
67
tin
102.00
0.04
1.40
2700
73
tin as T8T
0,46
0.063
0.026
0.46
0.063
zinc
5710.00
47.58
47.58
120
120
65.04
58.91
h
120
120
h
47
21
80
hardness, as CaCO3, mg/L
hardness, calculated, mg/L
Inorganics, mist., ua/L
cyanide
22
5.2
22
5.2
22
5.2
5.3
1.17
11
chlorine
19
11
fluorine
5336
3706
1080
SUM 9HQs %I
a 9X IWC
48.9
1 8.891
204.471
1818.401
E S V M eta] s FT 11 0 506-1. x l s

FRESHWATER SURFACE WATER 5'wRA slm S/2 /06 f I
I !
I
j
I
I
compound
site cone.,
ug/L
acute
HQ
chronic
HQ
NAWQC
CMC,
acute (1)
NAWQC
CCC,
chronic
(1)
NAWQC
notes
VSEPA
Reg, 4,
acute 5V
VSEPA
Reg. 4,
chronic SV
Reg 4
note
NOAA
5QuiRT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
VSEPA
Tier II
SAV
(ORNL)
VSEPA
Tier II
SCV
(ORNQ
Low
chronic
EC20, fish
Low
chronic
EC20,
dophnids
Sensitive
species
EC20,
dophnids
Popul.
chronic
EC20
METALS. uo/L (oob)
aluminum
4790.00
6.39
55.06
750
87 1
pH 6.5-9.0
750
87
pH 6.5-9.0
750
87
pH
4700
540
75
antimony
77.00
0.06
0.48
1300
160
88
30
180
30
2310
1960
79
arsenic, total
0.00
0.00
340
150
340
150
d
arsenic•3
360
190
2130
633
55
1995
arsenic -5
850
66
3.1
1500
>932
165
barium
40.50
0.37
10,13
110
4.0
beryllium
0.00
0.00
16
0.53
130
5.3
LOEL
35
0,66
148
3,8
21
cadmium (h)
0.00
0.00
4,3
2.2
1.79
0.66
h
4.3
2.2
h,d
1.8
0.75
0.013
4.3
chromium, total
25.40
0.04
0.34
chromium *3 (h)
570
74
984.32
117.32
h
570
74
h,d
89
8,44
126
chromium .6 (h)
16
11
16
11
h
16
11
d
51
0.5
0.266
316
cobalt
0.00
0.00
1500
23
810
4.4
3.98
copper (h)
82,70
6.36
9.19
13
9.0
9.22
6,54
h
13
9
h,d
5
0.205
0.26
8.6
iron
8530.00
8.53
8.53
1000
1000
1000
16
lead (h)
56.00
0.66
22,40
65
2.5
33.78
1.32
h
65
2.5
h,d
22
0.351
71
lithium
0.00
0.00
260
14
magnesium
3080.00
manganese
419.00
0,18
3.49
2300
120
1270
�11001
112
mercury
0.00
0.00
1.4
0.77
2.40
0.012
1.4
0.77
d
mercury, inorganic or total
1,30
0.87
0.87
on
0.32
mercury, methyl
0,099
0.0028
�0.03
0.87
0.28
molybdenum
16,000
370
360
nickel
36.70
0.08
0.71
470
52
789.00
87.71
h
470
52
h,d
62
45
11
215
selenium
0.00
0.00
5.0
20.00
5,00
40
25
2.60
selenium, total
186
5
d
silver
3.4
1.23
0.012
h
1.7
0.12
h,d
0.36
0.20
<0.56
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
110
12
81
64
67
tin
89.60
0.03
1.23
2700
73
tin as TBT
0,46
0,063
0,026
0.46
0.063
zinc
2270.00
18.92
18,92
120
120
65.04
58.91
h
120
120
h
47
21
80
hardness, as CaCO3. mg/L
hardness, calculated, mg/L
Inorganics, mist., ug/L
22
5.2
22
5.2
22
5.2
cyanide
5.3
1.17
11
chlorine
19
11
fluorine
5336
3706
1080
SUM HQS
apply 9%1WC
41,8
376
11.74
ESVMetalsFT07 0506-1.x15

ECOLOAICAI. SCREENING VALLIF.S, RA I
FRESHWATER SURFACE WATER T FT-30, slm 5/23/06 _
_ �
F-
44
I4I4
�I
compound
site coot.,
u9/L
acute
HQ
chronic
HQ
NAWQC
CAC,
acute (1)
NAWQC
CCC,
chronic
(1)
NAWQC
rotes
USEPA
Reg. 4,
acute SV
USEPA
Reg. 4,
chronic Sur
Reg 4
note
NOAA
SQuAT,
CMC
acute
NOAA
SQuiRT,
CCC
chronic
NOAA
note
USEPA
Tier II
SAV
(ORNL)
USEPA
Tier II
SCV
(ORNL)
Low
chronic
EC20, fish
Low
chronic
EC20,
daphnids
Sensitive
species
EC20,
daphnids
Popul.
chronic
EC20
METALS. uo/L (aab)
aluminum
5350.00
7.13
61.49
750
87
pH 6.5-9.0
750
87
pH 6.5-91
750
87
pH
4700
540
75
antimony
85.70
0.07
0.54
1300
I60
88
30
180
30
2310
1900
79
arsenic. total
0.00
0.00
340
150
340
150
it
orsenic•3
360
190
2130
633
55
1995
arsenic •5
850
66
3.1
1500
>932
185
barium
60.90
0.55
15.23
110
4.0
beryllium
000
000
16
0.53
130
5.3
LOEL
35
0.66
148
3.8
21
cadmium (h)
6.20
1.44
2.82
4,3
2.2
1.79
0.66
h
4.3
2.2
h,d
1.8
0.75
0.013
4.3
chromium, total
47.00
0.08
0.64
chromium •3 (h)
570
74
984.32
117.32
h
570
74
h,d
89
8.44
126
chromium •6 (h)
16
Il
16
11
h
16
11
d
51
0.5
0.266
316
cobalt
24.30
0.02
1.06
1500
23
810
4.4
3.98
copper (h)
185.00
14.23
2056.
13
9.0
9.22
6.54
h
13
9
h,d
5
0205
0.26
8.6
iron
20900.00
10.90
10.90
1000
1000
1000
16
lead (h)
163.00
2.51
6520
65
2.5
33.78
L32
h
65
2.5
h,d
22
0.35
71
lithium
000
0.00
1
260
14
magnesium
5750.00
manganese
728.00
0.32
6.07
2300
I20
1270
4100
112
mercury
0.00
0.00
1.4
0.77
2.40
0.012
1.4
0.77
d
mercury, inorganic or total
1.30
0.87
0,87
0.18
0.32
mercury, methyl
0.099
0.0028
.0.03
0.87
0.28
molybdenum
16,000
370
360
nickel
63.60
0.14
122
470
52
789.00
87.71
h
470
52
h,d
62
45
11
215
selenium
000
0.00
5.0
20.00
5.00
40
25
2.60
selenium, total
186
5
d
silver
3.4
1,23
0.012
h
L7
0.12
h,d
0.36
0.20
<0.56
0.14
0.32
thallium
140.00
4.00
1400
40
LOEL
110
12
81
64
67
tin
150.00
0.06
2.05
2700
73
tin as TBT
0.46
0.063
0.026
0.46
0063
zinc
8880.00
74.00
74.00
120
120
6504
58.91
h
120
120
h
47
21
80
hardness, as CaCO3, mg/L
hardness, calculated, mg/L
_
Inoraanics. misc.. uo/L
cyanide
22
5.2
22
5.2
22
5.2
531
1.17
It
chlorine
19
11
_
fluorine
5336
3706
1080
.SUM HQs
9% IWC
10.0311
.76
35a
I
ESVMeta15FT10 0506-1.xls

r
TestI�imer ica
ANALYTICAL TESTING CORPORATION
August 22, 2006
Client: WRS (3166)
221 Hobbs Street, Suite f 08
Tampa, FL 33619
Atm: Greg Garrison
SAMPLE IDENTIFICATION
WW 811206
2960 Faster Creighton Road Nashnlle, TN 37204' 800-765-0980' Fax [phone]
Work Order:
NPH 1991
Project Name:
Synthron Chemical RUSH
Project Nbr:
106105 1 Synthron Chemical RUSH
P/O Nbr.
74110248
Date Received.
09/15/06
LAB NUMBER COLLECTION DATE AND TIME,
NPH 1991 -01 08/14/06 t 4:00
An executed copy of the chain of custody, the project quality control data, and the sample receipt form arc also included as an addendum
to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at
1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accredidation.
This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is
privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the
intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you
have received this material in error, please notify us immediately at 615-726-0177.
Additional Laboratory Comments:
Received above temperature complaince at 8.8 degrees Celcius.
North Carolina Certification Number: 387
—2A0&;2di, 01Z7
I
The Chain(s) of Custody, 2 pages, are included a17Z7
These results relate only to the items tested. This'
Report Approved By:
QjtAL r�I ("
Roxanne Connor
Senior Project Manager
17 /" 0
c>)2
Page 1 of 19

TestAmerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Ann Greg Garrison
2960 Faster Creighton Road Nashville, TN 37204 • 800-765-0980'Fax [phone]
Work Order:
Project Name:
Project Number:
Received:
ANALI'TICAL REPORT
NPH 1991
Synthron Chemical RUSH
106105 1 Synthron Chemical RUSI1
08/15/06 08:00
Dilution Analysis
Analyte
Result
Flag Units
NIRI:
Factor Dalefl'ime
Method
Batch
Sample ID: NPH1991-01 (WW 811206
- Waste Water) Sampled: 08/14/06 14:00
General Chemistry Parameters
BOD - 5 Day
37.8
mg/l,
2.00
1 08/20/06 20:45
EPA 405.1
6082939
Chemical Oxygen Demand
444
mg/L
10.0
1 08/17/06 12:00
EPA 410.4
6083418
Total Suspended Solids
453
mg/L
33.3
1 08/15/06 19-07
EPA 160.2
6092943
Total Metals by EPA Method 601013
Arsenic
0.0176
mg/L
0.0100
1 08/17/06 14:25
SW846 601 OB
6083053
Barium
0,141
mg/L
0.0100
1 08/17/0614:25
SW846601OB
6083053
Cadmium
0.00390
mg/L
0.00100
1 08117/061425
SW846601OB
6083053
Chromium
0.0623
mg/L
0.00500
1 08/17/06 14:25
SW8466010B
6083053
Lead
0.11589
mg/L
0.00500
1 08/17/06 14:25
SW846601OB
6083053
Selenium
ND
mg/l,
0.0100
1 08117/0614:25
SW846601OB
6083053
Silver
ND
mg/L
0.00500
1 08/17/06 14:25
SW846 601OB
6083053
Mercury by EPA Methods 7470A/7471A
Mercury
ND
mg/L
0.000200
1 08/21/06 1 1--22
SW846 7470A
6083362
Purgeable Organic Compounds by EPA Method 624
Acrolein
NO
ug/L
50.0
1 08/22/06 10:30
EPA 624
6084149
Acrylonitrile
ND
ug/L
10,0
1 08/22/06 10:30
EPA 624
6084149
Benzene
ND
ug/L
1.00
1 08/22/06 1U0
EPA 624
6084149
Bromodichloromethane
ND
ug/L
1.00
1 09/22/06 10:30
EPA 624
6084149
Bromoform
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Bromomethane
ND
ug/L
1.00
1 08/22/06 1030
EPA 624
6084149
Carbon Tetrachloride
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Chlorobenzene
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Chlorodibromomethane
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Chloroethane
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Chloroform
ND
ug/L
1,00
1 08/22/06 10-30
EPA 624
6084149
Chloromethane
ND
uglL
00
1 09/22/06 10:30
EPA 624
6084149
1,2-Dichlorobenzene
ND
ug/L
1.00
1 09/22/06 10:30
EPA 624
6084149
1,4-Dichlorobenzene
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6094149
1,3-Dichlorobenzene
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Dichiarodilluoromcthane
ND
ug/l,
1.00
1 08/22/06 10:30
EPA 624
6084149
1,2-Dichloroethane
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
1,1-Dichloroethane
ND
ug/L
1.00
1 09/22/06 10:30
EPA 624
6084149
cis-1,2-Dichloroethcne
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
trans-1,2-Dichloroethene
ND
ug/L
1.00
1 08122106 10:30
EPA 624
6084149
1,1-Diehl oroethene
ND
ug/L
1.00
1 08/22/06 10.30
EPA 624
6084149
1,2-Dichloropropane
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
cis-1,3-Dichloropropene
ND
ug/L
1.00
1 08/22/06 10-30
EPA 624
6084149
trans-1,3-Dichloropropene
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Ethylbenzene
2.57
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Methylene Chloride
ND
ug/L
5,00
1 08/22/06 10:30
EPA 624
6084149
1,1,22-Tetrachloroethane
ND
ug/L
1,00
1 08/22/06 10.30
EPA 624
6084149
Tctmchloroethene
ND
ug/L
1-00
1 08/22/06 10:30
EPA 624
6084149
Page 2 of 19

TestAimerica
ANALYTICAL TESTING C0001 ATIQN 2960 Foster Creighton Road Nashville, TN 37204 ' 600-765-0960' Fax [phone]
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Greg Garrison
Work Order:
Project Name:
Project Number:
Received:
NPH1991
Synthron Chemical RUSE!
106105 / Synthron Chemical RUSH
08/15/0608:00
ANALYTICAL REPORT
Dilution Analysis
Analyte
..........
Result Flag
..............
Units
. ..........
',%iRL
.... .....I -
Factor Date/Time
- .... -............. ......---...........
Method
Batch
Sample ID: NPH1991-01 (WW 811206
- Waste Water) -
cont. Sampled:
08/14/06 14:00
Purgeable Organic Compounds by EPA Method
624 - cant,
Toluene
5.13
ug/L
1,00
1 08/22/06 10:30
EPA 624
6084149
1,1,2-Trichloroethane
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6094149
1,1,1-Trichloroethane
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6094149
Trichloroethene
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6094149
Trichlorofluoromethane
ND
ug/L
1.00
1 08/22/06 10:30
EPA 624
6084149
Vinyl chloride
ND
ugh
1.00
1 08/22/06 10:30
EPA 624
6084149
Xylenes, total
13.4
ug/L
2.00
1 08/22/06 10:30
EPA 624
6084149
Surr: 1,2-Dichloroethane-d4 (81-1261.)
103 %
08122106 10:30
EPA 624
6084149
Surr. DibromaJluoromethane (88-12091a)
105 %
08/22/06 10:30
EPA 624
6084149
Surr: Toluene-d8 (85-13091o)
100 %
08122106 10:30
EPA 624
6084149
Surr: 4-BromoJluorobenzene (80-12491.)
101 %
08122106 10:30
EPA 624
6084149
Acid and Base/Neutral Extractables by EPA Method 625
Acenaphthene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Acenaphthylene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082933
Anthracene
ND
ug/L
10.9
1 08/l7/06 02:23
EPA 625
6082833
Benzo (a) anthracene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Benzo (a) pyrene
ND
ug/1-
109
1 08/17/06 02:23
EPA 625
6082833
Benzo (b) fluoranthene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Benzo (g,h,i) perylene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6092833
Benzo (k) fluoranthene
ND
ug/L
10.9
1 09/17/06 02:23
EPA 625
6092833
4-Bromophenyl phenyl ether
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6092833
Butyl ben'zyl phthalate
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
4-Chloro-3-methyl phenol
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Bis(2-chloroethoxy)methane
ND
ug/L
10.9
l 09/17/06 02:23
EPA 625
6082833
Bis(2-chloroethy!)ether
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Bis(2-chloroisopropyl)ether
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
2-Chloronaphthalene
ND
ug/L
10.9
1 08/1710602:23
EPA 625
6082933
2-Chlorophenol
ND
ugA,
10.9
1 08/17106 02 :23
EPA 625
6092933
4-Chlorophenyl phenyl ether
ND
ug/L
10.9
1 09/17/06 02:23
EPA 625
6082833
Chrysene
ND
ug1l.
10.9
1 08/17/06 02:23
EPA 625
6082833
Dibenz (a,h) anthracene
ND
ugl1,
10.9
1 08/17/06 02:23
EPA 625
6082833
Di-n-butyl phthalate
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6092933
1,3-Dichlorobenzene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
1,4-Dichlorobenzene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6092933
1,2-Dichlorobenzene
ND
ug/L
10.9
1 09/1710602:23
EPA 625
6082833
3,3'-Dichlorobenzidine
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
2,4-Dichlorophenol
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Diethyl phthalate
ND
ug/L
10-9
1 08117/0602:23
EPA 625
6082833
2,4- D imethyl phenol
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Dimethyl phthalate
ND
ug/L
10.9
l 08/17/06 02:23
EPA 625
6092833
4,6-Dinitro-2-methylphenol
ND
ug/L
27.2
1 08/17/060223
EPA 625
6082833
2,4-Dinitrophetiol
ND
ug1L
27.2
1 08117/0602723
EPA 625
6082933
2,6-Dinitrotoluene
ND
ug/l.
10.9
1 08/l7/0602:23
EPA 625
6082933
Page 3 of 19

Testl- r .erica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 • 800-165-0980' Fax [phone]
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Aan Greg Garrison
Work Order:
Project Name:
Project Number:
Received:
NP111991
Synthron Chemical RUSH
1061051Synthron Chemical RUSH
08/15/06 08:00
ANA1,YTICAL REPORT
Dilution Analysis
Analyte
.......................
Result Flag
........ . ...........
units
...I........
NIRI..
.-......-1..........
Factor Daterrime
. ........................
Method
. ............-.
Batch
Sample ID: NPH1991-01 (WW 811206
- Waste Water) - cont. Sampled:
08/14/06 14:00
Acid and Base/Neutral Extractables by
EPA Method 625 - cont.
2,4-Dinitrotoluene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082933
Di-n-octyl phthalate
ND
ug/L
10.9
l 09/17/0602:23
EPA 625
6092833
Qis(2-ethylhexyl)phthalate
1 t.4
ugll-
10.9
l 08/17/06 02:23
EPA 625
6082833
Fluoranthene
ND
ug/L
10.9
l 08/17/06 02:23
EPA 625
6082833
Fluorene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Hexachlorobenzene
ND
ug/L
10-9
1 08/17/06 02:23
EPA 625
6082833
Hexachlorobutadiene
ND
ug/L
10-9
1 08/17/06 02:23
EPA 625
6082833
Hexachlorocyclopentadiene
ND
ug11'
10.9
1 08/17/06 02:23
EPA 625
6082833
Hexachloroethane
ND
ug1L
10.9
1 08/17/06 02:23
EPA 625
6082833
Indeno (1,2,3-ed) pyrene
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Isophorone
ND
ug/l,
10.9
I 08/17/06 02-23
EPA 625
6092833 '
Naphthalene
ND
ug/L
10.9
1 09/17/0602:23
EPA 625
6092833
Nitrobenzene
ND
ugA.
109
1 08/1710602:23
EPA 625
6082833
2-Nitrophenol
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
4-Nitrophenol
ND
ug/L
27.2
1 08/17/06 02:23
EPA 625
6082833
N-N itrosodimethy lam ine
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082933
N-Nitrosodiphenylamine
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
N-Nitrosodi-n-propylamine
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
Pentachlorophenol
ND
ug/L
27.2
1 08/17/06 02-23
EPA 625
6082833
Phenanthrene
ND
r1o,
10.9
l 08/17/06 02:23
EPA 625
6082833
Phenol
ND
ug/L
10,9
1 OR/17106 02:23
EPA 625
6092833
Pyrene
ND
ug/L
10.9
l 08/17/06 02:23
EPA 625
6082833
1,2,4-Trichlorobemmne
ND
ug/L
109
l 08/17/06 02:23
EPA 625
6082833
2,4,6-Trichlorophenol
ND
ug/L
10.9
l 08/17106 02-23
EPA 625
6082833
1,2-Diphenylhydrazine
ND
ug/L
10.9
1 08/17/06 02:23
EPA 625
6082833
2-Methyl naphthalene
ND
ug/L
10.9
1 08l17106 02.23
EPA 625
6092833
Surr: Terphetti-1414 (34-116%)
77 %
08117106 02:23
EPA 625
6082833
Surr. 2,4,6-Tribromophenol(16-130%)
90%
08117106 02:23
EPA 625
6082833
Surr: Phenol-d5 (10-6691.)
39 %
08117106 02:23
F,PA 625
6082833
Surr: 2-Fluorobiphenyl (32-99%)
77 %
08/17/06 02:23
F,PA 625
6082833
Surr: 2-Fluorophenol (10-81 %)
48 %
08/17106 02:23
EPA 625
6082833
Surr: Nitrobenzene-d5 (19-11691.)
77 %
08117106 02:23
EPA 625
6082833
Page 4 of 19

Testl�-merica
ANAtYnCAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Aun Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax [phone]
Work Order:
NPHi991
Project Name:
Synthron Chemical RUSH
Project Number:
1061051 Synthron Chemical RUSH
Received:
08/15/06 08:00
SAMPLE EXTRACTION DATA
WUVot
Extraction
Parameter
Batch
Lab Number
Extracted
Extracted Vol
Date
Analyst
Method
Acid and Base/Neutral Extractables by EPA Method 625
EPA 625
6082933
NPH1991-01
920.00
1,00
08115/06 12:20
KLG
EPA 625
General Chemistry Parameters
EPA405-1
6082938
NPH1991.01
300.00
300.00
08115/06 22:16
JTH
RODICBOD
Mercury by EPA Methods 7470AY7471A
SW8467470A
6083362
NP111991-01
30,00
30.00
08/27/06 0834
LTB
EPA 7470
Total Metals by EPA Method 6010E
SW8466010B
6083053
NPH1991-01
50.00
50.00
08/16/06 08:12
AMB
EPA3010A
SW8466010B
6083053
NPH1991-01
50.00
50.00
08/16/06 D8:12
AMB
EPA3010A
SW8466010B
6083053
NPH1991-01
50.00
50oo
08/16/06 08.12
AMB
EPA 3010A
SIA18466010B
6083053
NPH1991-01
50.00
50-00
08/16/0608:12
AMB
EPA3010A
SW8466010B
6083053
NPH1991-01
50.00
50.00
08116/0608:12
AMB
EPA3010A
SW9466010B
6093053
NPH1991-01
50.00
50.00
08/16/0608;12
AMB
EPA301DA
SW8466010B
6083053
NPH1991-01
50.00
50.00
08/16/06 08:12
AMB
EPA 30IDA
Page 5 of 19

•
Te.,-St merica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204' B00-165-0980' Fax [phone]
Client WRS (3166) Work Order: INPH1991
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number: 1061051 Synthron Chemical RUSH
Attu Greg Garrison Received: 08/15/06 08:00
PROJECT QUAl,1 IT CONTROL DA-FA
Blank
Analyie
[clank Value
Q Units
Q.C. Batch
Lab Number
Analyzed Daterrimc
General Chemistry Parameters
6082938-BLKI
BOD - 5 Day
<1 00
m8fl,
6092939
6092938-BLKI
OW20/06 20:45
6082943-BLK1
Total Suspended Solids
<0.500
mg1L
6082943
6082943-BLKI
08/15106 L9:07
6083418-BLK1
Chemical Oxygen Demand
<5.50
mg1L
6083418
6093418-131-K1
08/17/06 12:00
Total Metals by CPA Method 6010B
6083053-BLKI
Arsenic
<0.00460
mg1L
6083053
6083053-BLK1
09/17/06
14:16
Barium
<0.00100
mg1L
6083053
6083053-BLKI
08/17/06
14:16
Cadmium
<0.000400
mg1L
6083053
6083053-BLK1
08117/06
14:16
Chromium
<0.00150
mglL
608303
6083053-BLKI
08117l06
14:16
Lead
<0.00270
mg11,
6083053
6083053-BLKI
08/17106
14:16
Selenium
<0.00820
mgli-
6083053
6083053-BLKI
08/17106
14:16
Silver
<0.00190
mg/L
6083053
6083053-BLK1
08/17/06
14:16
Mercury by EPA Methods 7470AI7471A
6083362-BLKI
Mercury <O.M0100
Purgeable Organic Compounds by EPA Method 624
6084149-BLKI
Acrolem
<L 18
Acrylonitrile
<0.520
Benzene
<0.290
Bromodichioromethane
<0, 370
Bromoform
<0.140
Bromomethane
<0.320
Carbon Tetrachloride
<0.150
ChIm obcnzene
40.3 to
Chlorodibrarnomethane
<0.130
Chloroethane
<0.170
Chloroform
<0.130
Chloromethane
<0.110
l,2-Dichlorabenzene
<0.170
1,4-Dichlorabenzene
<0.310
1.3-Dichlorabenzene
<0. 120
Dicldurodifluoromethane
<0.470
1.2-Dichloroethane
<0.560
1.1-Dichloroethane
<0.310
mglL 6093362 6083362-BLKI 08121/06 i t:12
ug1L
6094149
6084149-BLK1
08/22106 10:05
ug1L
6084149
6084149-BLK1
08122106 10:05
uglL
6084149
6084149-iiLK1
09/22/06 10:05
uwl-
6084149
6084149-BLK 1
08122/06 10:05
ug/L
6084149
6094149-13LKI
08/22/06 10:05
ug1L
6084149
6084149-BLKI
O8122106 10:05
ug/L
6084149
6084149-BLK1
08/22106 10:05
ugJL
6084149
6084149-BI.K1
08/22106 10:05
ug1L
6084149
6084149-BLK1
08/22106 10:05
ug1l.
6084149
6D84149-BLK I
OR122106 10:05
uglL
6084149
6094149-BLK1
08/22/06 10:05
u61L
6084149
6084149-BLKI
08/22/06 10:05
uBJL
6084149
6084149-BLKI
08/22/06 10:05
u&/L
6084149
6084149-BLKI
08/22/06 10:05
ug1L
6084149
6084149-BLKI
08/22/06 10:05
ug1L
6084149
6084149-BLKI
08/22106 10:05
ug1L
6084149
6084149-BLKI
08/22/06 10:05
ug1L
6084149
6094149-BLKI
08/22106 10:05
Page 6 of 19

Testl��merica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road NashMe, TN 372C4' 800-765-0980' Fax [phone]
Client WRS (3166)
Work Orden
NPH1991
221 Hobbs Street, Suite 108
Project Name:
Synthron Chemical RUSH
Tampa, FL 33619
Project Number:
106105/ Synthron Chemical RUSH
Alm Greg Garrison
Received:
08/15/06 08:00
PROJECT QUALl-l'1' CONTROL nA-1-A
Blank -Cont.
Analyte Blank Value Q Units Q.C. Batch Lab Number Analyzed Daterime
Purgeable Organic Compounds by EPA Melhod 624
6084149-BLKI
cis-1,2-Dichloroethene
<O.130
ug1l,
6084149
6084149-BLKI
09/22/06 I0:05
trans-1,2-Dichloructhene
<O.130
ug1L
6084149
6084149-BLKI
08/22/06 10:05
1,I-Dichloroetheste
<O.IDO
ug/L
6084149
6084149-BLK]
08122106 10:05
1,2-Dichloropropane
<0,150
ug/L
6084149
6084149-BLKI
08122/06 10:05
cis-1,3-Dichloropropene
<0.250
ug/L
6084149
6084149-BLKI
08/22/06 10:05
trans-1,3-Dichloropropene
<0.100
ug1L
6094149
6084149-BLKI
08122/06 10:05
Ethylbenzene
<0.230
ug/L
6084149
6094149-BLKI
08/22/06 10:05
Methylene Chloride
<0.210
ug/L
6084149
6084149-BLKI
08/22/06 10:05
1,1,2,2-Tetrachloroethane
<0.130
ug/L
6084149
6084149-BLKI
08/22/06 10:05
Tetrachloroethene
<O.110
ug/[.
6084[49
6084149-BLKI
08122/06 10:05
Toluene
<0.280
ug/L
6094149
6084149-BLKI
08/22/06 10:05
1,1,2-Trichloroethane
<0,240
ug/L
6084149
6094149-BLKI
08122/06 10:05
I,I,I-Trichloroethane
<0.110
ug/L
6094149
60S4149-BLKI
08/22/06 10:05
Trichloroethenc
<0,100
ug/L
6084149
6084149-BLKI
08/22/06 10:05
Trichlorofluoromethane
<0.120
uglL
6084149
6084149-BLKI
08/22/06 10-05
Vinyl chloride
<0.370
ug1L
6084149
6084149-BLKI
08/22/06 10:05
Xyienes,total
<0.680
ug/L
6094149
6084149-BLKI
08/22/06 10:05
Surmgate:l,2-Dr0rlartxlhane-d4
101%
6084149
6094149-BLKI
08/22/06 10:05
Surrogate: UrhrumrJiuurornelhane
103%
6084149
6084]49-BLKI
08/22/06 10:05
Surmgaw 7aluene-dx
100%
6094149
6084149-13LKI
08/22/06 IP.05
,i'rrrrogare; 4-Hromgtfuoroher_ene
l01°%
6084149
6084149-BLKI
08/22106 10:05
Acid and Base/Neutral Extractables by EPA Method 625
6082833-BLKI
Acenaphthene
<2.90
Acenaphthylene
<3.00
Anthracene
<2.80
Benzo (a) andtncene
<2.60
Benzo (a) pyrene
<2.80
Benzo (b) fluoranthene
<3-00
Benzo (g,h,i) perylene
<2.90
Benzo (k) fluoramhene
<3.70
4-Bromophenyl phenyl ether
<2.20
Butyl benzyl phthalate
<2.70
4-Chloro-3-ntcthylpltenol
<2.40
B i s(2-chlorocthoxv)tuethane
<3.40
Bis(2-chloroe1hyl)e0her
<1.90
Bis(2-chloroisopropyl)ether
<4.50
2-Chloronaphthalcne
<3 00
2-Chlorophenol
<2 00
4-Chlorophenyl phenyl ether
<2.50
ug/L
6082933
GOR2833-13LKI
08/17/06
00:59
ug1L
608283"
6082833-13LK1
08/17/06
00:59
ug/L
6082833
6082833-BLKI
08117/06
00:59
ug1L
6082833
6082833-BLKI
os/17106
00:59
unJL
6082833
6082833-BLK 1
08/17/06
00:59
ugll.
6082833
6082833-BLK1
08/17/06
00:59
uglL
6082933
6082833-BLK I
08/17/06
00:59
ug/L
6082833
6082873-BLKI
08117/06
00:59
ug/L
6082833
6082933-13LKI
O81]7106
00:59
ugJL
6082833
6082833-BLKI
08/17/06
00:59
ug/L
6082833
6082833-BLK1
08/17/06
00:59
ue1L
6082833
6082833-BLKI
09/17/06
00:59
ug/L
6082833
6082833-BLK1
08/17/06
00:59
ug/L
6082833
6082833-BLK 1
08/17106
00:59
ug/L
6082933
6092833-BLK I
08117/06
00:59
ug/L
6082833
6082833-131.K I
DR117J06
00:59
110,
6082833
6082833-BLK1
09/17106
00:59
Page 7 of 19

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 ' 800-765-0980' Fax [phone]
Client WRS (3166) Work Order: NPH1991
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number: 106105 / Synthron Chemical RUSH
Atm. Greg Garrison Received: 08/15/06 08:00
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Analyte Blank Value Q Units Q-C. Batch Lab Nurnber Analyzed Datefror e
Acid and Base/Neutral EYtractables by EPA Method 625
6082833-BLKI
Chrysene
<2.40
ug/L
6082833
6082933-BLKI
09117/06 00:59
Dibenz (a h) anthracene
<2.90
ug7L
6082833
6082833-BLKI
09/17/06 00:59
Di-n-butyl phthalate
<2.60
ug/L
6082833
6082833-BLKI
08117/06 00:59
1,3-Diehlombenxene
<1.50
ug/L
6092833
6082833-B1-K1
08/17/06 00:59
1,4-Dichlorobenzene
<1.70
ug1L
6082833
6082833-BLKI
08/17/06 00:59
1,2-Dichlorobenzene
<L70
ug/L
6082833
6082833-BLKI
o8117106 00:59
3,Y-Dichlorobenzidinc
<2.70
ug/L
6082833
60S2833-BLKI
08/17/06 00:59
2,4-Dichlorophenol
<3.10
ug/L
6082833
6082933-BLKI
o8117/06 00:59
Diethyl phthalate
<2.60
ug/L
6082833
6082833-BLKI
08117/06 00:59
2,4-Dirne1hylphenol
<5.20
ug/L
6082833
6082833-BLKI
08117106 00:59
Dimethyl phthalate
<2.40
ug/L
6082833
G082833-BLKI
08/17/06 00:59
4,6-Dinitro-2-tnetbAphenol
<3.30
ug/L
6082833
6082833-B1.Kl
08/17/06 00:59
2,4-Dinitrophcnol
<2.90
ng[L
6082833
6082833-B],Kl
09/17/06 00:59
2,6-Dinitrotoluene
<2.80
ug/l,
6082833
6082833-BI.KI
09/17/06 00:59
7,4-Dinitrotoluene
<2.50
11wl.
6082833
6082833-BLKI
08117/06 00:59
Di-n-octyl phthalate
<2.80
uWL
6082833
6082833-BLKI
09/17/06 00:59
Bis(2-cthylhexyl)phthnlate
<1.50
ug/L
6082833
6082833-BLKI
08117/06 00:59
Fluoranthene
<2.50
ug/L
609283.1
6082833-BLKI
08/17/06 00:59
Fluorene
<2.70
ug/L
6082833
6082933-BLKI
08117/06 00:59
Hexachlombenzene
<2,40
ug/L
6082833
6082833-BLKI
08117/06 M59
Hexachlorobutadienc
<3,20
ug/L
6082833
608283i-BLKI
U3117/06 00:59
Hexachlorocyclopentadiene
<5.50
ug/L
6082833
6082833-BLKI
08/17/06 00:39
Hexachloroethane
<I.80
ug/L
6082833
6082833-131-KI
08/17/06 00:59
]ndeno(l,2 3-cd) pyrene
<2.90
ug/L
6082833
6082833-131-KI
08/17/06 00:59
Isophorone
<2A0
ug/L
6082833
6082833-BLK1
08/17/06 00:59
Naphthalene
<2.90
ug/L
6092833
6082833-BLKI
08/17/06 0059
Nitrobenzene
<4.50
uglt-
6082833
6082833-13LK1
08/17/06 00:59
2-Nitrophenol
<2.50
ug/L
6082833
6082833-RLKI
08/17106 00:59
4-Nitrophenol
<4,50
u61L
6082833
6082833-BLKI
09/17/06 00:59
N-Nitrosodirnelhylarnine
G.70
ug/L
6082833
6082833-BLKI
08/17/06 OD59
N-Nitrosodipheuylamine
<3.80
ug1L
6082833
6092833-BLKI
WPM 0059
N-Nirrosodi-n-propylarninu
<2.00
ug11.
6082833
6092833-BLKI
08/17106 00:59
Pentachlorophenol
<3,00
ug11'
6082833
6082833-BLKI
08117/06 00:59
11henanthrem
<2A0
ugll-
6082833
6082833-BLKI
08/17/06 00:59
Phc1101
<4.60
ug/L
6082833
6082833-B1,KI
08/17/06 00:59
pvrene
<2.70
ug/L
6082833
6082833-BLKI
08/17/06 00:59
1,2,4-Trichlorobenzene
<2.70
ug/L
6082833
6092933-BLKI
08/17106 00:59
2,4,6-Trichlorcphen0l
<2.90
ug/L
6082833
6082833-BLKI
08117/06 W59
] 2-Diphenylhydrazine
<2.90
ug/L
6082833
6092833-BLKI
08/17106 W59
2-Methylnaphthalene
<1.50
ug/L
6082933
6092833-BLKI
081t7/06 00;59
Surrogale: 7'cr1,1rcn)4-d14
114%
6092833
6092833-BLKI
08117106 00:59
Surrogate: 2,J,(;-7'rihr0nr0J)henn1
105%
6092833
6082833-BLKI
08117/06 00:59
Page 8ofl9

0
Testl.,merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Flobbs Street, Suite 109
Tampa, FL 33619
Attn Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204 ' 800-765-0980' Fax [phone]
Work Order:
NPH1991
Project Name:
Synthron Chemical RUST{
Project Number:
106105 / Synthron Chemical RUSH
Received;
08/15/06 08:00
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Analyte Blank Value Q
Units Q.C. Batch
Lab Number
Analyzed Datellirac
Acid and Base/Neutral Extractables by EPA Method 625
6082833-BLK1
Surmgaie: Phenol-d5 35%
6082833
6082833-BLKI
09/17/06 00:59
Surmgaie: 2-1-7uorabiphenyl 81%
6082833
6082833-BLKI
OSIl7l06 00:59
Surrogale; 2-GIrromphenol 45%
6082833
6082833-BLKI
09117/06 00:39
Surrogaw Nu—&-mein-dS 80%
6082833
6082833-BLKI
08/I7I06 00:59
Page 9 of 19

0
Testl�imerica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 • 800-765-0980' Fax [phone]
Client WRS (3166) Work Order: NPH1991
221 l lobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number; 106105 1 Synthron Chemical RUSH
Alm Greg Garrison Received: 08/15/06 08:00
PROJGCr QUALITY CONTROL DATA
Duplicate
Sample
Analyzed
Analyte
Orig. Val.
Duplicate Q
Units
RPD Limit Batch Duplicated
Date/Time
Ceneral Chemistry Parameters
6082938-DUP1
ROD- 5 Day
37.9
45.8
rng1L
I9 20 6082938 NPH1991-01
08/20/06 20:45
6082943-DUP1
Total Suspended Solids
184
175
mglL
5 20 6082943 NPH 1954-01
08/15106 19.07
6083418-DUPI
Chemical Oxygen Demand
ND
NO
mg1l,
10 6083419 NPH1192-05
08/17/06 12:00
Page 10 of 19

Testl�.merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
22I Hobbs Street, Suite 108
Tampa, FL 33619
Attn Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204.800-765.0980' Fax [phone]
Work Order:
NPH1991
Project Name:
Synthron Chemical RUS1d
Project Number:
106105 1 Synthron Chemical RUSH
Received:
08/15/06 08:00
PROJEC1' QUALITY CON'rROL DATA
LCS
Target
Analyzed
Analyte
Known Val
Analvzed Val Q
Units
%Rec.
Range
Batch
Daierrime
General Chemistry Parameters
6082938-BS1
ROD - 5 Day
198
228
uglmL
115%
85. 115
6082938
08/20106 20:45
6082943-BSI
Total Suspended Solids
100
96,0
mglL
%%
90 - 110
6082943
08/15/06 19:07
6083418-BS1
Chemical Oxygen Demand
20.0
20.0
ug1mL
100%
90 - 110
6083418
08117/06 12:00
Total Metals by EPA Method 601013
6083053-SS1
Arsenic
0.0500
0.0486
mg/L
97%
80 - 120
6083053
09/17/06 14:21
Barium
2.00
2 21
mg1L
110%
80. 120
6081053
08/17/06 14-21
Cadmium
0.0500
0,0545
mg1L
ID9%
RD- 120
6083053
08/17/06 14:21
Chromium
0.200
0.202
131gll-
101 %
8o- 120
6083053
08/17/06 14:21
Lead
0.0500
0.0507
mg1L
toM
80- 120
608305",
08/17/06 14:21
Selenium
0,0500
0.0506
mgfL
101%
80- l20
6n83053
08/17/o6 14:21
Silver
0.0500
0,0499
mg1L
100%
SO- 120
6083053
08/17/06 14:21
Mercury by EPA Methods 7470A/7471A
6083362-BS1
Mercury 0,00200
Purgeable Organic Compounds by EPA Method 624
6084149-BSI
Acrolein
250
Acrvlanitrile
250
Benzene
Soo
Bromodichlaromethane
50.0
Bromoform
50.0
Bromomethane
50.0
Carbon Tetrachloride
50.0
Chlorobenzene
50.0
Chlorodibromomeftne
50.0
Chioraeilrane
50.0
Chloroform
50.o
Chloromelhme
50.0
1,2-Dichlarobcnzene
50.0
1,4-Dichlorobenzene
50.0
1,3-Dichlarobenzene
50.0
Dichlnrodi fluorrnncthane
50.0
1,2-Dichlcroethane
50.0
[,I-Dichlorocthane
50.0
0,00192 utPJL 91 % 78 - 124 6083362 08121 /06 I 1 c 14
209
ugIL
84%
19- 196
6084149
081221D6
09:14
199
ugfL
80116
73 - 132
6094149
08/22106
09:14
48, 3
ug1L
97%
37 - 151
6084149
08/22/06
09:14
52,3
nWL
105%
35 - 155
6084149
09/22106
09:14
55.0
u8/L
110%
45 - 169
6084149
08/22106
09: 14
92.4
ug1L
185%
1- 242
6094149
08/22106
09:14
54.2
ugll,
1 OS%
70 - 14D
6094 i49
08/22/06
09t 14
50.0
u8/l,
100%
37- 160
60R4149
08/22106
09:14
55.3
ug/1-
111%
53 - 149
6094149
08122/06
09:14
45.2
ug/L
90%
14 - 230
6084149
081221D6
D9:14
47.9
ug1L
96%
51 - 138
6094149
08122/06
09:14
31.6
ug1L
63%
1 - 273
6094149
08/22106
09:14
53.6
ug1L
107%
Is- 190
6094149
08/22/06
09:14
50.8
ug/L
102%
is- 190
6084149
08/22/06
09:14
519
ut/L
108%
59 - 156
6084149
08/22/06
09:14
64.8
uglL
130%
33 - 142
6084149
08/22/06
09:14
49,0
ug(L
98 %
49 - 155
6084149
08/22/06
09:14
45.3
ug1L
91%
59-155
6084149
08/22/06
09:14
Page I 1 of 19

Testl- rmerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Alin Greg Garrison
2950 Faster Creighton Road Nashville, TN 37204' B04165-0980' Fax [phone]
Work Order:
NPH1991
Project Name:
Synthron Chemical RUSH
Project Number:
106105 / Synthron Chemical RUSH
Received:
08/15/06 08:00
PROJECT QUAIATY CONTROL DATA
LCS - Cont.
Target
Analyzed
Annlyte
Known Val.
Analyzed Val
Q Units
%Rec.
Range
Batch
DmeJTime
Purgeable Organic Compounds by
EPA Method 624
6084149-BSI
cis-1,2-Dichloroethene
50.0
47.8
ug/L
96%
54 -156
6084149
08/22/06 09:14
irons-1,2-Dichloroethene
50.0
46.6
ug/L
93%
54 - t56
6084149
08/22/06 09:14
1,1-Dichloroethene
50.0
50,1
ug/L
1!00%
1 - 234
6084149
08/22/06 09:14
1,2-Dichloropropane
50.0
46.8
ug1L
94%
] - 210
6084149
08/22/06 09:14
cis-1,3-Dichlornpropene
50.0
51. I
ug/L
102 %
1 - 227
60R4149
08122/06 09;14
trans-1,3-Diehloropropene
50.0
54.2
ug/L
108%
17-183
6084149
OW22/0609:14
Ethylbenzene
50,0
52.7
ug/L
105%
37 - 162
6084149
08122106 09:14
Methylene Chloride
50.0
47.9
ug1L
96%
1- 221
6084149
09/22/06 09:14
1,1,2,2-Tetrachloroethane
50,0
40.9
ug1L
R2%
46- 157
6084149
08/22106 09:14
Tetrachloroethene
50.0
54.4
ug/L
109%
64 -148
6084149
08/22/06 09:14
Toluene
50.0
52.5
ug11'
105%
47- 150
6084149
08122/06 09:14
1,1,2-Trichloroethane
50.0
48.1
ug/L
96%
52 - 150
6084149
08122/06 09:14
1,1,1-Trichloroethane
50.0
51.5
ug/L
10.1%
52. 162
6084149
08/22/06 09:M
Trichloroethene
50.0
52.9
nglL
106%
71 - 157
6084149
08/22/06 09:14
Tric6loroIluorotnethanc
50.0
54.9
t:gl[.
110%
17 - 181
60R4149
08/22/06 09:14
Vinyl chloride
50.0
49.6
ug/L
991/6
l - 251
6084149
08/22/06 09A4
Xylenes, total
150
161
up][,
107%
80, 125
6084149
09/22/06 09:14
Surrogate: 1, 2-Dichloroethene-d4
30.0
29.9
96%
81 - 126
6D84149
08/22/06 09:14
Surrogare: Dihronrnfluommerhane
30.0
29.8
991/6
88 - 120
6084149
08/22/06 09:14
.4urrogore: Toluene,A
30.0
29,3
98%
85 - 130
6084149
08122/06 09:14
Surre>gare: 4-8rorwfluorohencene
30.0
28.1
94%
80 -124
6084149
08122l06 09;14
Acid and Base/Neutral Fstractables by EPA Method 62.5
6082833-BSI
Acenaphthene
50.0
Acenaphthylene
50.0
Anthracene
50,0
Benzo (a) anthracene
50.0
Benzo (a) pyrene
50A
Benzo (b) tluoranthene
50,0
Benzo (g,h,i) perylene
50.0
Benzo (k)fluoranthene
50.0
4-Bromophenylphenyl ether
50.0
Butyl benzyl phthalate
50,0
4-Chloro-3-methylphenol
50,0
Bis(2-chIorocthoxy)mcthane
5o, D
Bis(2-chloroethyl)ether
50,0
Bis(2-chlor0i50prapyl)ether
5 0, 0
2-Chloronaphihalenc
50.0
2-Chlorophcnol
50.0
4-Chlorophenyl phenyl ether
50.0
40.4
ug/L
91%
47 - 145
6092833
09/17/06
17:50
41.0
ug/L
82%
33- 145
6082831
08117/06
17:50
45.6
uglL
91 %
27 - 133
6082833 '
08/17/06
17:50
42.5
ug1L
85%
33- 143
608283;
08/17/06
17:50
44.9
ug/L
90%
17 - 163
60828-13
08117/4)6
17:50
43.4
uglt.
87%
24 - 159
6082833
08/17/06
17:50
39.1.
ug/L
78%
1-219
60R2833
08/17/06
17;50
45.1
ug1L
90%
1 ] - 162
6082833
08/17106
IT50
39.8
ug1L
80%
5 3 - 127
6082833
08/]7106
17:50
39.3
ug/L
79°/a
1- 152
6082833
09/17/06
17:50
38.3
ugll-
77%
22 - 147
6DS2933
08/17/06
17:50
35.5
ug/L
71%
33 -184
6082933
09/17/06
17:50
32.2
ug/L
64%
12 - 158
6082833
08117/06
17:50
34.3
ug/L
69%
36 - 166
60N2933
09/17/06
17:50
38.0
uglL
76%
60- 118
6082833
08/17/06
17:50
30,4
uglL
61%
23- 134
6082R33
081]7106
17:50
447
11g1L
891%
25 - 158
6082833
08117/06
17:50
Page 12 of 19

0
TestA-merica
ANALYTICAL TES71NG CORPORATION
2960 Foster Creighton Road Na5hvAe,
TN 37204.80o-765-0980 - Fax [phone]
Client WRS (3166)
Work Order:
NPH1991
221 Hobbs Street, Suite 109
Project Name:
Synthron Chemical
RUSH
Tampa, FL 33619
Project Number
106105 / Synthron
Chemical RUSH
Attn Greg Garrison
Received:
08/15/06 08:00
PROJECT QUALITY CONTROL DATA
LCS - Cont.
Target
Analyzed
Analyze
Known Val.
Analyzcd Val Q
Units
%Roe.
Range
Batch
DatelTirne
Acid and Base/Neutral Extractables by EPA Method 625
6082833-BSI
Chrysene
50.0
45.6
ug/L
87%
17.168
6082833
08/17/06 17:50
Dibenz (a,h) anthracme
50.0
38.8
ug/L
78%
1 - 227
6082913
08/17/06 17:50
Di-n-butyl phthalate
50.0
42.4
ug/L
85%
1- 118
6082833
OSf17106 17:50
0-Dichlorobenzene
50.0
30.1
ug/L
60%
1- 172
6082833
08/17/06 17:50
1,4-Dichlorobenzene
50.0
29.1
ugIL
58%
20 - 124
6082833
08/17/06 17:50
1,2-Dichlorobenzene
50,5
30.0
ug/L
59%
32 - 129
6082833
08117/06 17:50
3,3'-Dichlorobenzidine
50.0
42,7
uglL
85%
1-262
6082833
08MA16 IT50
2,4-Dichlorophenol
50.0
36,8
ugIL.
74%
39-135
6082833
08/17/06 I7-50
Diethyl phthalate
50.0
31A
ug/L
62%
1- 114
6082833
08/17/06 17:50
2,4-Dimethylphcnol
50.0
29. ,
ug/L
591%
32 - 119
6082933
08/17/06 17:50
Dintethyl phthalate
50.0
15.0
ug/L
30%
1 - 112
6082833
08/17/06 17:50
4,6-Dinitro-2-nwhylphenol
50.0
44.3
ug/L
891%
1 - 181
6082833
08117/06 17:50
2,4-Dinitraphenol
50.0
45.8
ug/L
92%
1- 191
6082833
09117/06 17:50
2,6-Dinitrotoluene
50.0
47.5
ug/L
95 %
50 - 158
6092813
08/17/06 17:50
2,4-Dinitrotoluene
50.0
49.3
110,
99%
39.139
6082833
081[7l06 17:50
Di-n-octyl phthalate
50.0
41.0
u&IL
82%
4- 146
6092833
08117/06 17:50
Bis(2-ethylhexyl)phthalate
50.0
43.7
ug/L
87%
8- 158
6082933
08/17/00 17:50
Fluoranthene
50.0
43.8
ug/L
88%
26 - 137
60828 33
08/17/06 17:50
Fluorene
50.0
43.6
ug/L
87%
59 - 121
6082833
08/17/06 17:50
Hexachlorobenzene
50.0
46.3
ug/l,
93%
1. 152
6082833
08/17/06 17:50
Hcxachlorohutadiene
50.0
34.3
ug/L
691%
24 - 116
6082833
08117/06 17:50
Hexachlorocyclopentadicne
50.0
24.6
ug/L
49%
23 -86
6082833
08/17/06 17:50
Hexachterocthanc
50.0
28.8
ug/L
58%
40- 113
6092833
09117/06 17:50
lndeno(t,2.3-cd) pyrene
50.0
40.0
ug/L
80%
1- 171
6082833
08117106 17:50
Isophorone
50.0
40.3
ug/L
81%
21- 196
6092833
OR/ t7/06 IT50
Naphthalene
50.0
32.2
ug/L
64%
21 - 133
6092833
08/17106 t7:50
Nilrohenzene
50.0
34.2
upfL
69%
35- 180
6082833
OR/ [7/06 17:50
2-Nitrophenol
50.0
33.6
ug/L
67%
29- 182
6082833
09/17/06 t7:50
4-Nitrop3ienol
50.0
25.2
ug/L
50%
1 - G2
6082833
08/17/06 17:50
N-Nitrosodimethytatnine
50.0
17.9
ugll,
36%
23 - 69
6082833
08/17/06 17:50
N-Nitrosodiphenylamine
50.0
64.9 L
ug1l.
130 %
42 - I t 1
6082833
08117106 17:50
N-Nitrosodi-n-propylamino
50.0
35.2
ug/I,
70%
1-230
6092833
08/17/06 17:50
Pentachlorophenol
50.0
466
no-
93%
14 - 176
60S2833
08/17/06 17:50
Phenanthrene
50.0
-43.3
ug/L
87%
54 - 120
6082833
08/17/06 17:50
Phcnol
50.0
14.0
ug/L
28%
5 - 112
6082833
08/17/06 17:50
Pyrene
50.0
44.1
ug/L
88%
52-115
6082833
08/17/06 17:50
1,2,4-Trichlorohenzene
50.0
31.9
ugIL
64%
44 - 142
6082833
08/17/06 17:50
2.4,6-Trichlorophenol
50.0
40.4
ug/L
8l %
37 - 144
6082933
08/17/06 17:50
1,2-DiphenyIhydmzine
50.0
43 9
ug1L
88%
47 - 117
6082833
08117/06 17:50
2-Methylnaphthalene
50.0
37.3
ug/L
75%
34 - 110
6082833
09/17/06 17:50
.Surrugale: Terphenyl-J14
50.2
43.6
87%
34 - 116
6082833
08117/06 17:50
Page 13 of 19

•
Testl merica
ANALYTICAL TESTING CORPORATION 2960 Foster Creighton Road Nashville, TN 37204 ' 800-765-0980' Fax [phone]
Client WRS (3166) Work Order: NPH 1991
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical RUSH
Tampa, FL 33619 Project Number: 106105 / Synthron Chemical RUSH
Attn Greg Garrison Received: 08/15/06 OR:00
PROJECT QUALITY CONTROL DATA
LCS Cont.
Target
Analyzed
Analyze Known Val.
Analyzed Val
Q Units % Rec.
Range
Batch
Datv7irne
Acid and Base/Neutral Extractables by EPA Method 625
6082833-BS1
Surrogme: 2.4.6 7'rihmmopheno! 50.2
43.1
845
16 - 130
6082833
08/17/06 17:50
,4urrogarc: Phcned-0 50.2
13.6
27%
10 - 66
6082833
08117/06 17:50
Surmgale:2dYuamhrphenyl 50.2
35.4
71%
32-99
6082833
08/17/06 IT50
,vurmgare:2-7.7uorophennf 50.2
19.9
39%
10-81
6082833
08/17/06 17:50
.4rermgare: Nirrohenzene-d5 50.2
32.6
65%
19- 116
6082933
08/17/06 17:50
Page 14 of 19

Testl,. merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204 ' 800.765-0980' Fax [phone]
Work Order: NPH1991
Project Name: Synthron Chemical RUSH
Project Number: 106105 / Synthron Chemical RUSH
Received: 09/15/06 08:00
PROJECT QUALITY CONTROL DATA
LCS Dup
Spike Target Sample Analyzed
Analyze Orig. Val. Duplicate Q Units Cone %Kee. Range RPD Limit Batch Duplicated Datefl'ime
General Chemistry Parameters
6082943-BSD1
Total Suspended Solids 95-9 mglL 104 95% 90 - 110 1 20 6032943 08/15/06 19:07
Mercury by EPA Methods 747OtV7171A
6083362-BSD1
Mercury 0.00184 mg/L o-O0200 92% 78 - 124 1 22 6083362 08/21/06 11:19
Page 15 of 19

Testl�smerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 l lobbs Street, Suite 108
Tampa, FL 33619
Attu Greg Garrison
296D Faster Crelghton Road Nashville, TN 37204 • 800-765-0980 • Fax [phone]
Work Order: NPH1991
Project Name: Synthron Chemical RUSH
Project Number' 106105 1 Synthron Chemical RUSH
Received: 08/15/06 08:00
PROJECTQUALITY CONTROL DATA
Matrix Spike
Target Sample Analyzed
Analyte Orig. Val, MS Val Q Units Spike Cone % Rec. Range Balch Spiked Date/Time
-- -- ..------ ....... ........... ....... ....... .--------- ........ ....... -..... .--------- ............... -- ..'...'---'-- " - " --- "
General Chemistry Parameters
6083418-MS1
Chemical Oxygen Demand 48.1 102 uglmL 50.0 1081/. 90 - 110 6083418 NPHI 192-01 08(17106 12:00
Total Metals by EPA Method 6010B
6083053-MS1
Arsenic
0,0176
0.0640
mglL
0.0500
93%
75-125
6083053
NPH1991-01
08/17/06 14:30
Barium
0.141
2.33
mg1L
2.00
109%
75-125
60S3053
NPH1991-01
08/17106 14:30
Cadmium
0,00390
0.0585
mglL
0.0500
109%
75- 125
6083053
NPH1991-01
09/17/06 14:30
Chromium
0.0623
0.254
mg/L
9200
96%
75- 125
6083053
N111f1991-01
08/17106 14:30
Lead
0.0589
0,103
mglL
0.0500
88%
75- 125
6083053
NPH1991.01
08/17/06 14:30
Selenium
ND
0.0481
mg)L
0.0500
96%
75- 125
6083053
NPH1991-01
08/17/06 14:30
Silver
ND
O.D522
mglL
0.0500
M4%
75- 125
6083053
NPH1991-01
08117/06 14:30
Mercury by EPA Methods 7470Al7471A
6083362-MS1
Mercury
ND
0.00188
mg1L
0.00200
94%
63 - 138
6083362
NPH2O17-01
08/21/06 I1:26
Page 16 of 19

Test merica
ANALYTICAL, TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
'Tampa, FL 33619
Attn Greg Garrison
2960 Faster Creighton Road Nashville, TN 37204' 800-765.0960' Fax [phone]
Work Order: NPH 1991
Project Name: Synthron Chemical RUSH
Project Number: 106105 / Synthron Chemical RUSH
Received: 08/15/06 08:00
PRO,IEC'I' QIJAI,1'1'1' CON'l-ROL DATA
Matrix Spike Dup
Spike Target Satnple Analyzed
Analyte Orig. Val. Duplicate Q Units Cone %Rec. Range RPD Limit Batch Duplicated Date/Time
General Chemistry Parameters
6083418-MSD1
Chemical Oxygen Demand 48,1 102 uglmL 500 108% 90-110 0 10 6083418 NPH1192-01 08/17/06 12:00
Total Metals by EPA Method 601011
6083053-MSD1
Arsenic
0.0176
0.0669
mg1L
0.0500
99%
75 - 125
4
20
6083053
NPH1991-01
08/17/06 14:34
Barium
0.141
2.36
mg1L
200
111%
75 - 125
1
20
6083053
NP141991-01
OS117106 1434
Cadmium
0.00390
0.0589
mgli.
0ON
110%
75- 125
0.7
20
6093053
NP141991-01
06117/06 14:34
Chromium
00623
0,256
mgfL
9.200
97%
75 • 125
0.8
20
6D83053
NPH1991-01
08/17/06 14734
Lead
0,0599
0.105
mgfL
0.050a
92%
75- 123
2
20
608N"
NPH1991-01
08/17/06 1434
Selenium
ND
0.0495
mgfL
0.0500
99%
75- 125
3
20
6083053
NIIH1991-01
08117/06 14:34
Silver
ND
0.0526
mg1L
0,0500
105%
75-123
0.8
20
6083053
NPH1991-01
08/17/06 14:34
Mercury by EPA Methods 7470AJ7471A
6083362-MSDI
Mercury ND 0.00218 mg/L 0.00200 109% 63 - 138 15 22 600362 N142O17-01 08121/06 11:29
Page 17 of 19

TestAimerica
ANALYTICAL TESTING CORPOPATtON
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Greg Garrison
TestAmerica - Nashville, TN
2960 Foster Creighton Road Nashville, TN 37204 ` 800-765-0980' Fax [phone]
Work Order:
NPH1991
Project Name:
Synthron Chemical RUSH
Project Number:
1061051 Synthron Chemical RUSH
Received:
09/15/06 08:00
CERTIFICATION SUMA1ARY
Method
Matrix
AIHA
Nelac
North Carolina
EPA 160,2
Water
NIA
X
X
EPA 405.1
Water
NIA
X
X
EPA 410.4
Water
NIA
X
X
EPA 624
Water
NIA
X
X
EPA 625
Water
N/A
X
X
SW8466016B
Water
NIA
X
X
SW846 7470A
Water
NIA
X
X
6
Page 18 of 19

Testl�merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Arm Greg Garrison
2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax [phone]
Work Order: NP111991
Project Name: Synthron Chemical RUSI I
Project Number: 106105 / Synthron Chemical RUSH
Received: 08/15/06 08:00
DATA QUALIFIERS AND DF,FINITiOT'S
L Laboratory Control Sample and/or Laboratory Control Samplc Duplicate recovery was above the acceptance limits. Analyte not
detected, data not impacted.
METHOD,UODIFICA'nON NOTES
COD 410.4 M - M = COD method modified for use of Hach method 8000.
Page 19 01-19

TestAmerica
ANALYTICAL TESTING CO0.PORAFION
Nashville Division
COOLER RECEIPT FORM BC#
NPhi1991
Cooler Received/Opened On: 8 15/2006 8:00 �� i.
1. Indicate the Airbill Tracking Number (last 4 digits for Fedex only) and Name or Courier below:_ i
FED -EX
Temperature of representative sample nrtemperatnre blank when opened: Degrees Celsius
(indicate TR Gun TD#)
101507
3. Were custody seals on outside of cooler?.............................................................................. YES...NO....NA
a. If yes, how many and where: I `C `j-
4. Were the seals intact, signed, and dated correctly?............................................................. YFS ..N0_NA
5. Were custody papers inside cooler?................................................................................ ES.. O... NA
I certify that I opened the cooler and answered questions 1-5(intiall.............................................. 6.J-3
6. Were custody seals on containers: VF.S ONO and Intact YES NO NA
were these signed, and dated correctly?... ............. YES...NO. NA
7. What kind of packing material used? Bubblewra Peanuts Vermiculite Foam Insert
Plastic bag Paper Other None
S. Cooling process: [ce Ice -pack Ice (direct contact) Dry ice Other None
9. Did all containers arrive in good condition ( unbroken)?............................................................. /YES,(.NO—NA
10. Were ail container labels complete (#, date, signed, pres., etc)? ............................................ F.5 .NO ... NA
11. Did all container labels and tags agree with custody papers? ................................................ OES
.NO...NA
12, a. Were VOA vials received?...................................................................................... .NO...NA
b: Was there any observable head space present in any VOA vial?... ............................................. YES.
,r 0 ..NA
I certify that I unloaded the cooler and answered nuestions 6-12(intiall......................................
13. a. On preserved bottles did the p1l test strips suggest that preservation reached the correct pH level? ES ..NO...NA
b. Did the bottle labels indicate that the correct preservatives were used ...................... ES ..N0... NA
If preservation in-house was needed, record standard ID of preservative used here
14. Was residual chlorine present?........................................................................................ YES. .,NA
1 certify that I checked for chlorine and off as per SOP and answered questions 13-14 fintiall.._..__ U
15. Were custody papers properly felled out (ink, signed, etc)? ................................................. VE ...NO ... NA
16. Did you sign the custody papers in the appropriate place? ................................................. ES...NO...NA
17. Were correct containers used for the analysis requested? ................................................... ES..NO...NA
18. Was sufficient amnunt of sample sent In each container"..................................................... ES ..NO ... NA
f certify that I entered this nroiect into LIMS and answered questions 15-18 (intial).......................
I certify that I attached a label with the unique LIMS numher to each container (intial)...................
19. Were there Non -Conformance issues at login YES a Was it PIPE generated YFS NO d
DIS — Broken in shipment
Cooler Receipt Form LF-1 Revised 319106
End oi' Form

CHAIN O USTODY RECO}3,
N
NashvilleTN Qayton, ON [� Indianapolis, 1N To assist us in using the proper analytical
Test mericaOrland., FL Watertown, WI methods, is this work being conducted for
ANALYTICAL TESTING CORPORATION Cedar Fails, IA Pontiac. MI regulatory purposes? NC State
dlient NamelAccount #:WRS 13166 N P H 1991 Compliance Monitoring? No
Address: 221 Hobbs St., Suite 108 08/18/06 23:59 Enforcement Action? No
CitylStatefZip:Tampa, FL, 33619 y �+ Report To: WRS via Email- gacquaro2wrsie.corn
Project Manager: Greg Garrison Invoice To: WRS
Telephone Nurnber:828 438 4888 ' Fax No.: TA Quote #:
Sampler Name -.(Print) Gary Acquaro Project ID: US EPA Reg 4, Synthron Chemical
Sampler Signature: Project #: 106105
Preservative Matrix I Analvze For:
a
ID
r-
m
3
O
o
w
CON
to
,s
20
m
c
.-.
mIn
2
In
F-
.�
E
E
m
e
v
W
m
._
�'
s
a
g
m
N
i�
OCDQ
m
r
r
m
3
rn
rn
U
o
ti
a
a
c7
nto
c
m
7
a
r
I
°
m
0
U
°
E
O
2
Sample ID 1 Description
`°
❑
E
r
°
Z
O
—
z
T
c�
=
z
z
o
z
r
o
°�m
3
0`
u
m
o
O
m
t7
a]
O
V
rn
U
N
WW 811206
8114
14:00
8
Y
IYI
1
3
Ill
131X
X
I X
X
X
X
X
I
I
X
Special Instructions:
Laboratory Comments:
PO# 74110248 RUSH 5 DAY TAT Date Needed 8118
Temperature Upon Receipt:
Method of Shipment: FEDEX
VOCs Free of Headspace?Y N
Relinquished by:
Date
Time
Received by.
Date
Tme
��4.va
I4ao
Relinquished by:
Date
Time
Recei tRme
Date
Time
I .
g�bo

Environmental Testing Solutions, Inc.
PO Box 7565 Phone: [phone]
Asheville, NC 28802 Fax: [phone]
E-mail: [e-mail]
August 31, 2006
Mr. Gary Acquaro
WRS Infrastructure & Environment, Inc.
305 Amherst Road
Morganton, NC 28655
RE: ETS PROJECT NUMBER: 2720
Dear Mr. Acquaro:
Enclosed are toxicity test results for samples from WRS Infrastructure & Environment, Inc.
received by Environmental Testing Solutions, Inc. August 16, 2006.
Sample
Name
Test Procedure
EPA Method Final Result
I Number
SWF
North Carolina Phase II Chronic Whole
Effluent Toxicity Test Procedure —
EPA-821-R-02-013 ChV = 35.4%
July 1991, Revised: February 1998
(Ceriodaphnia Full -range Toxicity Test)
SWNF
North Carolina Phase II Chronic Whole
Effluent Toxicity Test Procedure —
EPA-82 I -R-02-013 ChV = 8.8 %
July 1991, Revised: February 1998
(Ceriodaphnia Full -range Toxicity Test)
Note: ChV = Chronic Value. A numeric value representing the geometric mean of the highest
concentration having no detectable impairment of survival or reproduction and the lowest concentration
that does have a detectable impairment of survival or reproduction.
If you have any questions concerning these results, please feel free to contact me.
Sincerely,
Jim umner
Laboratory Director
This report should not be reproduced, except in its entirety, without the written
consent of Environmental Testing Solutions, Inc.
North Carolina Certificate Numbers: Biological Analyses: 37, Drinking Water: 37786, Wastewater: 600
South Carolina Certificate Number: Clean Water Act: 99053-001

Environmental Testing Solutions, Inc.
PO 130x 7565 Phone: [phone]
Asheville, NC 28802 Fax: [phone]
E-mail: 7irnSumner@aol. corn
Effluent Aquatic Toxicity Report Form - Phase 11 Chronic Ceriodaphnia dubia Date: August 31, 2006
Facility: WRS Infrastucture & Environment, Inc. NPDES #: NC- NA Pipe #: SWF County, Burke
Synthron, Inc.
Laboratory Perforrrsng Test: EnNironrnentaI Testing Solutions, Inc. Conirnnts: One mrTic used for entire
Signature of Operator in Responsible Cbarge: test eriod-
SigmtureofLaboratorySupervisor-. ��( � Project 272D
Samples'. 06CS 16 03
Mail Original To: North Carolina Department of EUVironrrent and Natural Resources
DWQ/ Environnxntal Sciences Branch
1621 Mail Service Center Start date: End date: Stan lime: Fndtime:
9a8C 27699Raleigh, N
Sample Information
Collection start date:
Grab:
Composite duration:
A➢mliaity (mVL CaCO,):
Hardness (nsWL. Cs0O,)r
Conductivity (p-hos?-)r
Total residual chlorine (m#Lj
Sample Temp. at Receipt (°CX
Simple
5ample2
Control
Test information
Treatment:
Initial pH (SLOT.
Final PH (SUO
Indisl DO (mWLj:
Final DO (mglL}
InWal Temp. CC).
Final Temp. (°C):
08-15-06
3f
u
_ _
31
-_
-
43
341
15y, 1", Im
3.7
sw
R-W I
K-J ]
S-
P-t r
R.,_d 3
75%
75%
75%
Control
Control
Control
7.55
7.63
7.56
7.01
7.22
7,25
7.61
7.59
7.49
7.19
7.02
7.06
7.3
7.7
79
9.1
go
8.0
81
8.0
9.0
7.9
7.9
7.8
25.1
2a.9
24,8
24.7
2C6
24.7
25-0
25.1
24.8
25.1
24S
11
Organism Number
Control Organism% 1 2 3 4 5 6 7 8 9 10 nr n
FNu;;W., fYoung Produced 134 133 3132 137 134 135 130 135 132 1 33.3
Adult Survival: ve, ead I L I L L I L I L I L I L I L I L I L
Effluent Percentage E9
Treatment 2 Organism 1 2 3 4 5 6 7 8 9 10 stun
Nun-bCT ofYoung Produced
1321
38
135
136
137
136
1 34
1 3
334 36
1 353
Adult Survival: ive, (D ead
I L
I L
I L
I L
I L
I L
I L
I L
I L
I L
1 -7.2
x R.�w
Effluent Percentage H9
Treatment 3 Organisms 1 2 3 4 5 6 7 8 9 10 aR.
Number of Young Produced
1 36138
135133
1 37
1351351
40
39 35
36.3
Adult Survival: (L)ive, (D)cad
I L
I Li
Lj
L
I L
I L I L
I L
I L I L
1 -9.0
xxraueW
Effluent Percentage 2E%
Treatment 4 Organisms 1 2 3 4 5 6 7 8 9 10 rrr>n
Number of Young Produced 1
37
38
31137
38
135 1
34
401361
361
36.2
Adult Survival: (L)ive, (D)ead
I L
L
L
I L
L
I L
I L
L
L I
L
1 -8.7
7i R.L.Gw
Effluent Percentage sa%
Treatment 5 Organisms 1 2 3 4 5 6 7 8 9 10 1a
Nurrircr of Young Produced 1
261
261201
4 1221291
19 141
7 1
20
18.9
Adult Survival: L ivc, D end
I L
I L I L
I L L
I L
L L
I L
I L
1 43.2
Effluent Percentage 75
Treatment 6 Organisms 1 2 3 4 5 6 7 8 9 10 l> n
Number of Young Produced
3
1 U 1 3
1 0 0
1 2
1
D
1 0 1 2
1 Ll
Adult Survival• L ive, (D)cad
L
I L I L
I L L
I L
L
L
I L I L
1 96.7
%Rrdectiwi
Effluent Percentage 1007
Treatment 7 Organisms 1 2 3 4 5 6 7 8 9 10 aim
Number ofYonng Produced 0
1 U 1 0
1 0 0
1 0 0 0
1 0 1 0
0.0
Adult Survival: (L)ive, (D)cad D
I D I D
I D D
I D f D D
I ll Lp
L 100.0
%R'-w
Overall Analysis:
Result: LOEC: 50% NOEC: 25% ChV: 35.4o/a
Chronic Test Results
Final control Mortality (Y.):
0
%Control with 3rd Broods:
100
Control Reproduction CV:
6.3
48 Hour Mortality
Control
o
of
l0
lwc.
NA
Of
10
Sigaifwanl7:
NA
Final Mortality S4mifi and ar:
WrA
Reproduction Analyses
Reproduction LOP.C-
50•A
Reproduction NOEC:
25
Overall Method:
Steers Many
Normal Distnbalion:
No
Method:
Kohnoborov D
Statistic:
1 A 16
Critical Value:
L035
Equal Variances:
No
Method:
Eartictrs Test
Statistic:
46.449
Critical Vahm-
t5.086
Non-Panmetrie Analysis (if applicable)
Method:
Steers Many One
EfDucnt %
Rank Sum
Critical Sum
6.251Y.
135.5
75.0
12.5%
140.0
75.0
25%
137.5
75.0
5cry.
55.0
75.0
75%
55.0
75,0
I00'ti
This data package contains the loxicify rest results summarized on this form and includes a Cover Page,
AT-3 Form, Laboratory BenchsheetS Statistical Analyses, Chain -of -Custody Forms and Quality Control Charts.
DiVQ form AT-3 (8/9I) Rev. 1119-5

Environmental Testing Solutions, Inc.
PO Box 7565 Phone: [phone]
Asheville, NC 28802 Fax: [phone]
E-mail: [e-mail]
Effluent Aquatic Toxicity Report Form - Phase ll Chronic Ceriodaphnia dubia Date: August 31, 2006
Facility: WRS Iafraslucture & Environment, Inc. NPDES #: NC- NA Pipe #: SWNF County: Burke
Synthron,Inc.
Laboratory Performing Test Environmental Testing Solutions, Inc. Conirrrents: One.sarnpIcumdforcritirc
Signature of Operator in Responsible Char e: test mod
Signature of Laboratory Supervisor: Project- 2720
Samples: 060816.04
Matz Original To: North Carolina Department ofEnvirorurlent and Natural Resources
DWQI EnvironnCntal Scicnoos Branch
1621Mail SeniceCentrr Sfastdate, Rnddatc Starttime: Endtimc:
Raleigh, NC 27699-1621 08-16-06 08.23.06 1320 0955
Sample Information
Collect= start date:
crab:
Compoaste duration:
Maliady (mg/L CHCOrx
Hardness (mg/L CKC04
Ceadvctwo 6-hW-Y
Total residual ehlorme (mgrLk
Sample Temp. at Receipt CCT
,:
ae
ea
e �
®a
Test Information
Treatment
Initial pH (Sll}
FaralpH (SM
lnital DO (mW-x
Final DO (mpLY
instill Temp. CcC
Foul Temp. CC):
Slit
RmewJ I
RmMal l
51a1
Reaew�ll
Rmexd ]
12.5%
125%
12.5%
Control
Control
Cmuat
7.86
7.89
7.60
7.01
7.22
7.25
7.49
7.47
7.36
7.20
7.01
TO
8.0
&0
8.1
8.1
8.0
8.0
9.1
8.0
7.6
1 90
9.0
7-8
24.8
24.7
25.0
2A.7
24.6
24.9
2A.8 1
25.1 1
25.0
25.1 1
24.9
24.9
Organism Number
Control Organisms 1 2 3 4 5 6 7 8 9 10 aa.�
mher of You Produced 32 Nu30 34 1 341 31 33134 134133 132 1 72 7
Adult Survival: I-'ve, Dead L L L L L L L L L L
Effluent Percentage 6.29 i
Treatment 2 Organisms 1 2 3 4 5 6 7 8 9 10 m.
d1' cr ofYo Produced 138
131
1
33 38
1 32 1
33 1
32
33 1
37
1 33 1
34.0
Adult Survival: Live, Dead
L I
L I
L L
L
L
I L
I L I
L
I L 1
-4.0
xa.e�a�
Effluent Percentage 1as
Treatment 3 Organisms 1 2 3 4 5 6 7 8 9 10 as
Number ofYoang Produced
3 j 10 1
15 4
7 0 1 i7
17 D
3 6.6
Adult Survival (L)ice, D cad I
L I L I
L I L I
L I D I L
I L I D I
L 1 79.8
x R.4ixc�
Effluent Percentage 2s°o
Treatment 4 Organisms 1 2 3 4 5 6 7 8 9 10 edn
Furnber ofYoung Produced 1 0 1
0 0 1
0
1 0 1 0
1 0
1 0 1 0
1 0 0.0
Adult Survival: (L)ive, (D)ead D
I D D I
D
D D
I D
I D I D
I D I1 na.o
x R.a�eaa
Effluent Percentage 5ai
Treatment 5 Organisms 1 2 3 4 5 6 7 8 9 10 ,
Narrtber of Young Produced
0
0
0 1
0
1 0
0
1 0
0 0
1 0 1 0.0
Adult Survival: )ive, D cad
ll
D
D
ll
D
D
D
D D
D 100.0
x R.4uim
Effluent Percentage 75%
Treatment 6 Organisms l 2 3 4 5 6 7 8 9 10 �a
Nttmber ofYourig Produced
0 0
0
1 0
1 0
0 1 0 0
0 0
0.0
Adult Survival: (L)ive, (ll)cad
I D I D
I D
1 D
1 D
D I D I D
I D D
1n0.0
%Reaucern
Effluent Percentage 1oa i
Treatment 7 Organisms 1 2 3 4 5 6 7 8 9 10
Number ofYoung Produced
1 0
1 0
1 0
1 0
1 0
1 0 0 0
0
0
0.0
Adult Survival: ivc, cad
D
ll
D
D
D
D D D
D
D
100.0
xRa�ri�
Overall Analysis:
Result: LOEC: 12.5% NOEL: 6.25% ChV: 8.8%
Chronic Test Results
Final Control Mortality 0/4
0
%Cantrolwith 3rd moods:
100
Control Reproduction CV:
4.3
49 Hour Mortality
Control
0
of
10
IWC:
NA
of
IO
Signiticant7:
NA
Final Mortality Sipurwaul at:
25 h
Reproduction Analyses
Reproduction LOEC:
125 %
Reproduction NOEC:
6.25%
Gve U Method:
Steers Many
Narmal➢atntmtion:
Yes
Method:
Shapiro Wilks
Statistic:
0.934
CriLical Value.
0.900
Equal Variances:
No
Method:
Hadletrs Test
Statistic:
15.929
Critical Value,
9.210
Non-Pararnethc Analysis (if applicable)
Method:
Steers Many One
Effluent %
Rank Sum
Critical Sum
6.25%
112.5
79.0
12.5%
550
790
"'
SOY.
75 %
loan.
This date package contains the toxicity test results summarized on this farm and includes a Cover Page,
AT-3 Form, Laboratory Benchsheets, Statistical Analyses, Chain -of -Custody Forms and Quality Control Charts.
D iVQ form AT-3 (8191) Rev. 11195

Environmental Testing Solutions, Inc. Page 1 of
North Carolina Phase tl Chronic Whole Effluent Toxicity Test
(EPA-821-R-02-013 Method 1002.0, NC Modification- February, 1998)
Species: Ceriodaphnia dubia
Client:
LAW5,
NPDES #: Nc
n A
Facility:
5rJT8R-OrIJ INC.
Outfall/Pi e:
NA 5tjF-
County:
'8UP-V(2-
IWC:
NA
Comments:
Test organism information:
Test information:
Organism age:
< 24-hours old
Randomizing template:
19u2QL'Q.
Date and times organisms
were born between:
Oe- %5-d, %5%48 1-0 Zmcy
Incubator number and
shelf location:
2 eZ
Organism source:
O 8-ol -olo A - ti
YCT batch:
8-07--Ob
Transfer bowl information:
i-i=7.?ISU Temperature =zq.e°C
Selenastrum batch:
08•01-Olo
Dilution nrenaration information: Samnle collection information -
Concentration
V•ZS
12•S
ZS
I Sb
75
Jcm
I
Sample I
Sample 2
Sample
volume (ml
+2•S
ZS
SO
lCO
15p
zw
Collection start
date:
O&- iS-0
Diluent
volume (MI)
1$l S
rl S
1So
Ib0
eye
O
Collection end
time:
1 OOp
Total volume
(ml)
��
ZC�
200
ZOO
7�
Grab/Composite
duration):
C7t2A�
Temperature (°C)
3 C
upon receipt:
Physical
PALE TP04
characteristics:
G. OM
ETS project
number;
zi2[)
ETS
066 7(o 03
number:
number: er•
Daily renewal information:
1 .
1Test
initiation,Control
renewal, feeding,
batch used
used
terminationor
'� ,_
..
+.�:
�►
•. � —
�
army;
p
':l "fit;' R•IFVL/y7 Y,
�:�rt�CS•'d,w�:r,y%, �c;,tfs�t�,{s�S•�,
] �` ' �{:, i'lpL:"..�'�:N S
`.�''rs� - b�t'r� ., r
fI
:,3�J',w Ss-
���F�I:i•+.."tG �,�..� �t�'���-F��f;f�
i 3N
t.�zSi:�,�.:«.iw,SSF'„j,:�...T✓,i».7;�'.:7'u"a
� `4�'�Y_.�/- y�
G
r
Control information:
Acceptance criteria
Summary of test endpoints.
% of Male Adults:
j ,
s 20%
7-day LC50
% Adults having 3"Broods:
I c t.
a 80%
NOEC
a5'
% Mortality:
b' l .
5 2Q%
LOEC
Mean Offs rin Female:
3a -3
>_ 15.0 offspringlfemale
ChV
(.
% CV:
(9.3- (.
<40.0 %
IC25
$tn.le to

0
I
Environmental Testing Solutions, Inc. Page 2 of 7
Species: Ceriodaphnia dubia
Client: SA n1r kctp J lw ` SWF-
CONTROL
Date:cc -16-plo
Survival and Reproduction Data
Replicate number
1
2
3
4
1 5
6
7
1 8
9
1 to
Day
2
Adult mortality
(L = live, D = dead)
5
Young produced
"1
lbzb
ISL6
tstd
ZJ5
��
US
I`i
We)
t�
cs7.6
I(n
RZ-8
Ito
Adult mortality
(L = live, D =dead)
L
6 or 7
Young produced
Total young produced
3Li
33
3l
3Z
3-1
3(4
35
30
35
3Z
Final Adult Mortality
L
(L = live, D = dead)
X for 3`d Broods
X
X
X
x
x
Note: A 213 i:r the upper right corner of the number of young produced indicates the presence of two broods.
Concentration: la .2S 07c,
Control:
% Mortali :
Mean Offspring/Female:
Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
'10
2
Adult mortality
{L = live, D =dead}
L
L
L
5
Young produced
Z$
it'
1 b,
} I Zb
�o
I & 2
z8
is z
1� 2B
1 gt�
ZOt$
Adult mortality
(L — live, D = dead)
L
L
L
6 or 7
Young produced
16
ZQ
19
20
1
{Q
19
IG
I g
Total young produced
32
3
3 S
Jo
3-1
3�-
3`4
31
3`i
38
Final Adult Mortality
(L = live, D = dead)
Note: A 2B in the upper right corner of the number of young produced indicates the presence of two broods.
Test Concentration:
% Mortality:
Mean Offspring/Female:
3
% Reduction from Control:
—�•Z'i`.

r
i
1
_7
I
7��
J
Environmental Testing Solutions, Inc. Page 3 of 7
Species: Ceriodaphnia dubia
Client:
Concentration: 12 -solo
Date: 0:-110-0l0
Survival and Reproduction Data
Replicate number
1
2
3
4
5
6
7
$
9
14
Day
2
Adult mortality
(L = live, D = dead)L-
5
Young produced
1.12$
Ig 2_8
Ipt�
1 g �
� �26
1� z$
f {px8
tC3
192,
"A
Adult mortality
L
L
6 Or 7
Young produced
19
11
1
IS
1.1
1 ^1
1 /S
�1
7-1
Zd
48
(L = live, D =dead)
Total young produced
31.
3 8
35
33
37
35
35
N b
3cG
35
Final Adult Mortality
L�
L
L
L_
(L = live, D = dead)
Note: A 213 in the upper right comer of the number of young produced indicates the presence of two broods.
Concentration: 75%,
Control:
% Mortality:
Mean Offspring/Female:
30.3
% Reduction from Control:
Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
10
2
Adult mortality
(L = live, D =dead)
L
5
Young prodj
18 z�
lit"
17
191"
1 �'
1 b
IS
ZOZ$
18,z
I g:
Adult morta
{L =live, D =
L
L
L
L
6 or 7
Young produced
Total young produced
31
38
3 l
31
39
35
y b
3f­
3(-
Fin-at Adult Mortality
(L = live, D = dead)
L
L
L
L
L
L
L
L
L
Note: A 2B in the upper right comer of the number of young produced indicates the presence of two broods.
Test Concentration:
% Mortality:
Mean Offs rin Female:J+p.Z
%Reduction from Control:
43,? .

r
d
i
d
0
Environmental Testing Solutions, Inc. Page 4 of 7
Species: Ceriodaphnia dubia
�
Client. S`l► n\Vzt7n] tt.1C. —SU3F Date: g.�_ab
Concentration: —,n7 Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
10
2
Adult mortality
{L = Five, D =dead}
5
Young produced
Iz
�176
ax
13Z
rJ
1
O
R i8
Adult mortality
(L = live, D = dead)
6 or 7
Young produced
I b
1 Jr
1 Z
i (0
1
2'-t
I a
-1
!
Total young produced
zs
7-6zo
�
zz
zq
Ig
I�-I
�
zo
Final Adult Mortality
(L = live, D = dead)
L
L--
Note: A 2B in the upper right comer of the number of young produced indicates the presence of two broods.
C'nnrentrntinn:
Control:
% Mortality:
61,
Mean Offspring/Female:
16 �9
% Reduction from Control:
3_2.1,
Survival and Reproduction Data
Day
Replicate number
1
2
3
4 1
5
1 6
7
8
9
10
2
Adult mortality
(L =live, D = dead)
5
Young produced
Q
Q
Adult mortality
(L = live, D = dead)
L
L
L
t—
6 or 7
Young produced
3
Q
3
O
Z
l
0
Z
Total young produced
3
0
3
0
0
-L-
Final Adult Mortality
(L = live, D = dead)
L
L
L
L
�—
Note: A 2B in the upper right corner of the number of young producep indicates the presence or two Droops.
Test Concentration:
Mortah
Mean Offs rip emale:
I . i - t.
% Reduction from Control:
. 9 1.
r

�t
r
d
0
Environmental Testing Solutions, Inc. Page 5 of 7
Species: Ceriodaphnia dubia
Client: -_ 5��i.1 t it.1C. " 5 V7
Concentration: 10007a
Date: 0a-1 -aL,
Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
10
2
.
Adult mortality
(L = live, D = dead)
y�
ll
D
5
Young produced
Adult mortality
(L = live, D = dead)
6 or 7
Young produced
Total young produced
O
O
O
O
O
d
C
�
Final Adult Mortality
(L = live, D = dead)
�
�
1�!)
.Note: A 2B in the upper right comer of the number of young produced indicates the presence of two broods.
Crine'en txntinn-
Control:
% mortality:
UU'/
Mean Offspring/Female:
6.0
% Reduction from Control:
1 pp' -
Survival and Reproduction Data
Day
Replicate number
2
3
4
5
6
7
8
9
l0
2
lity
Adult;D—
(L = livdead)
5
Young produced
Adult mortality
{L = live, D = dead)
6 or 7
Young produced
Total young produced
Final Adult Mortality
(L = live, D = dead)
Note: A 2B in the upper right comer of the number of young proauceo lnelcaLcS u�c P-11 . — -•----
Test Concentration:
% Mortali :
Mean Offs rin emale:
% Reduction from Control;

Environmental Testing Solutions, Inc. Page 6 of 7
Species: Ceriodaphnia dubia
Date: O k-O.-C)6
Client: ?-aN Ltl-sw F-
Concentration: Survival and Reproduction Data
Day
Replicate number
1
3
4
5
6
7
8
9
10
2
Adult mortality
(L = live, D = dead)
5
Young produced
Adult mortality
= live, D = dead)
6 or 7
Young produced
Total young produced
Final Adult Mortality
(L = live, D = dead)
More, A 2B in the upper right comer of the number of young produced indicates the presNee of two broods.
Control:
% Mortality
Mean Offs rut Female:
% Reduction from Control:

Environmental TestinZ Solutions. Inc. Page 7 of 7
Species: Ceriodaphnia dubia
Client: 1�
+3 V:
Date:

Environmental Testing Solutions, Inc.
Statistical Analyses
_
Ceriodaphn_ia_S_ urvival nndReproduction Test -Reproduction
Start Data
8/16/2006
Test ID:
CDFRCRNC
Sample ID:
WRSInfrasWcture-SWF
End Date:
EnV2006
Lab ID:
SIS-Environ. Testing Sol.
Sample Type:
DMR-Discharge Monitoring Report
Sample Date;
Protocol:
CHRONIC-EPA-821-R-D2.013
Test Species:
CD-Ccriodaphnia dubia
Comments:
Conc-%
1
2
3
4 5
6
7
8
9 10
D-Contral
34.000
33.000
31.000
32.000 37.000
34.000
35.000
30.000
35.000 32.000
6.25
32.000
39.000
35.000
36.000 37.000
36.000
34.000
37.OD0
34.000 38.000
12.5
36.000
38.000
35.000
33.000 37.000
35.000
35.000
40.000
39.OD0 35.000
25
37.000
39.000
31.000
37.000 39.000
35.000
34,OW
40.000
36,000 36.000
50
28.000
26.000
20.000
4.000 22.000
29.000
19.000
14.0Do
7.000 20.000
75
3.000
0.000
3.0D0
0,000 0.000
2.000
Low
0.000
01000 2.000
100
0.000
0.000
0.000
o.o00 0.000
0.000
0.000
0.D00
0.000 0.000
Transform: Untransformed
Rank
1-failed
Isotonic
Conc-%
Mean
N-Mean
Mean
Min
Max
CV %
N
Sum
Critical
Mean
N-Mean
D-Control
33.300
1.0000
33.300
30.000
37.000
6.339
10
35.375
1.0DW
6.25
35.700
1.0721
35.700
32.000
38.000
5.452
10
135.00
75.00
35.375
Lo000
12.5
36.300
1.0901
36.300
33.000
40.000
5.959
10
140.00
75.00
35.375
LOD00
25
36.200
1.0971
36.200
31.000
40.000
6.866
10
137.50
75.00
35.375
1.0DW
•50
18.900
0.5676
18.900
4.000
29.000
44.440
10
55.00
75.DD
18.900
0.5343
•75
Llo0
0.0330
1-100
0.0M
3.000
116.971
10
55.00
75A6
L100
Omit
100
0.000
0.0000
0.000
0.0D0
0.000
0.000
10
0.000
0.0000
Auxiliary Tests Statistic Critical Skew Kurt
KolmogarovD Test indicates non-noraul distribution (p <= 0.01) 1.41580651 1.035-1.0140709 5.72595493
Bartlett's Test indicates unequal variances (p = 7.361~09) 46.4496198 15.0962722 -_
Hypothesis Test (1-tail, 0.05) NOEC LOE?C ChV TU
Steeps Many -One Rank Test 25 50 35.3553391 4
Treatments vs D-Control
Linear Interpolation (200 Resamples)
Pain[ `fa S❑ 95%(L Skew
1C05 27.684 0.592 26.790 28.748-0.9874
IC10 30.368 1.000 28.831 32.496 0.5794
IC15 33.052 1.462 30.790 36.244 0.7275 1,0
IC20 35.736 1.931 32.720 39.992 0.7705 0.9
IC25 38.420 2.404 34.650 43,740 0.7972 0 6
IC40 46.472 3.271 40.903 52.686 0.2132
IC50 51.703 3.187 45.252 56,726-0.2087 0.7
0, 6
h 0.5
c
a.o,a
u 0.3
0.2
0.1
0.0
.0.1
•0.2
Dos; -Response Plot
46
40
35
30
0
0 25
v
0 20
a
Y
15
10
0 p
O` N N N ul r O
C �
O
U
O
20 40 60 80 100 12D
Dose %
wxs SV F 08-76-06

Environmental Testing Solutions, Inc.
Statistical Analyses
PMSD Calculation Only.
Ceriodaphnia Sunival and ReproductionTest-Reproduction
Start Date:
8/16/2006
Test ID:
CDFRCRNC
Sample 1D:
WRS Infrastructure - SWP
End Daze;
V2312006
Lab ID:
ETS-Environ. Testing Sol.
Sample Type:
DMR-Discharge Monitoring Report
Sample Date:
Protocol:
CHRONIC-EPA-821-R-02-013
Test Species:
CD-Ceriodaphnin dubin
Comments:
Corte•%
1
2
3
3 5
6
7
8
9 10
D-Control
34,000
33,000
31.000
32000 37.000
34.000
35.000
30.000
35.000 32000
6.25
31000
38.000
35.000
36.000 . 37.000
36.000
34.000
37.000
34.000 38.000
125
36,000
38.000
35.000
33.000 37.000
35.000
35.000
40.000
39.000 35.000
25
37.000
38.000
31.000
37.000 32.000
35.000
34.000
40.000
36.000 36.000
50
28.000
26.000
20.QOO
4.000 22,000
29.000
19.000
14.000
7.000 20.000
75
3.000
0,000
3.000
0.000 0.000
2-NO
1.000
0.000
0.000 2.000
100
0.000
0.000
0.000
0,000 0.000
0.000
0.000
0.000
0.000 0.000
Transform: Untransfomied
1-Tailed
Untindr.
Conc-%
Mean
N-.Mean
Mean
Min
Max
CV%
N
t-Scat
Criticni
MSD
Mean
N-Mesm
D-Control
33.300
1.0000
33.300
30.000
37.000
6.339
10
35.375
1.0000
6.25
35.700
1.0721
35,700
32.000
38.000
5.452
LO
-1.376
2.287
3.989
35.375
1.0000
12-5
36,300
1.0901
30,300
33.000
40.000
5.958
10
-1.720
2.287
3.989
35.375
1.0000
25
36.200
1,0871
36.200
31.000
40,000
6.866
10
-1.662
2.287
3.989
35.375
IbO00
•50
18.900
0.5676
18.900
4,000
29,000
44.440
10
8.254
2287
3.999
18.900
0.5343
173
1.100
0.0330
MOO
0.000
3,000
116.971
10
18.458
2.257
3.989
1.100
0.0311
100
0.000
0.0000
0.000
O'000
ROW
ROW
10
0.000
0.0000
Auxiliary Tests
Statistic
Critical
Skew Kurt
Kolmogorov D Test indicates nw-normal distribution (p <= 0.01)
1.415806532
1.035
-1.01407087 5,725954933
Baracirs Test indicates unequal variances (p =736E-09)
46.44861994
15.08627224
hypothesis Test (1-tail, 0.05) NOFC LOEC
ChV TU
MSDu h1SDp
.ISB .1SE
F-Proh df
Dunne0's Test 25 50
35.35533906 4
3.989124729 0.119793535 2045.716667 15.21666667
3AE-29 5,54
Treatments vs D-Cmdrol
Linear Interpolation (200 Resatnples)
Point % SD 95% CL
Skew
IC05 27.684 0.508 26.639 28.730
O.000I
]CIO 30.368 0.931 28.994 32.683
0.5044
iC15 33.052 1.394 31.086 36.649 0.5994 1.0
IC20 35.736 1.845 33.115 40.600 0.6385 0.9
IC25 38.420 2,309 35.287 44.670 0.6605
0.6
IC40 46.472 3.152 41,459 53,228 0.0185
IC50 5L703 3.050 45.574 57.022-0.3963 0.7
0.6
fj
'A 0.5
c
a a4
9 03
0:
0.2
0.1
0.0
-0.1
-0.2
Dose -Response Plot
45
40
35
c 30
0
25
v
o 2
a0
m
tr 15
10
0
N 04 N
N
C �D
U
20 40 60 60 100 120
Dose %
1-tail, 0.05 level
of significance
WRS S1VF 08-16-06

Client:
Test dates:
Environmental 'heating Solutions, Inc.
Chronic Whale Effluent Toxicity Test (EPA-821-R-02-013, Method 1002.0)
Species: Ceriodaphnia duhia
Quality Control
Verification of Data Entry, Calculations, and Statistical Analyses
1VRS lhlfrastructure & Envirorurtent, Inc. - SR'F
August 16 - 23, 2006
Project number: 2720
Reveiwed by:
Cotceutralion
(%)
Day
Replicate number
Survival
(%)
Average
repruductlon
Co l icient of
v.riwlon (%)
Percent redaction from
control (%)
1
2
3
4
5
6
7
8
9
10
Control
5
19
16
15
15
18
17
19
16
18
16
100 1
33.3
6.3
Not applicable
7
l5
17
16
17
19
17
16
14
17
16
Total
34
33
31
32
37
34
35
30
35
32
6.25 %n
5
16
18
16
16
18
19
15
18
18
20
100
35.7
5.5
-7.2
7
16
20
19
20
19
17
1 19
19
16
18
Total
32
38
35
36
37
36
34
37
34
38
12.517a
5
17
19
19
18
18
18
16
19
19
17
100
36.3
6.0
-9.0
7
19
19
16
1S
19
17
19
21
20
18
Total
36
38
35
33
37
35
35
40
39
35
2517b
5
18
19
17
19
19
16
15
20
18
18
100
36.2
6.9
-8.7
7
19
19
14
18
19
19
19
20
18
18
Total
37
38
31
37
38
35
34
40
36
36
SO %
5
12
11
8
0
11
13
5
4
0
9
100
18.9
44.4
43.2
7
16
15
12
4
11
16
14
10
7
11
Total
28
26
20
4
22
29
19
14
7
20
75%
5
0
0
0
0
0
0
0
0
0
0
t0o
1.1 1
117.0
96.7
7
3
0
3
0
0
2
1
0
0
2
Total
3
0
3
0
0
2
1
0
0
2
100%
5
0
0
0
0
0
0
0
0
0
0
0
0.0
0.0
to0.0
7
0
0
0
0
0
0
0
0
0
0
Total
1 0
0
0
0
0
0
0
10
0
Q
Dtuhnett's NISD value: 3.989 MSD = Minimum Significant Difference
PMSD: 12.0 PMSD = Percent Minimum Significant Difference
l ,,MSD is a measure of test precision. The PMSD is the minimum percent difference between die control and treatment that eau be declared
statistically significant in a whole effluent toxicity test. On average, a significant difference occurs for Environttiental Testing Solutions, Inc.
chronic toxicity tests when a toxicant reduces Ceriodaphnia reproduction by 9.6% from the control.
Lower PMSD bound determined by USEPA (10Ih percentile) = 11 %.
Upper PMSD bound detennined by USEPA (90t" percentile) = 37%.
The lower and upper bounds were calculated by the USEPA using 393 tests conducted from 33 laboratories for Ceriodaphnia reproduction in
chronic reference toxicant tests.
USEPA. 2000. Understanding and Accounting for Method Variability in Whole Effluent Toxicity Applications Under the National Pollutant Discharge Elirnination Program. FPA 833-R-00-003. US Fnvirohunental Protection Agency,
Cincinnati, OR
ll'RS Sl1'F 08-16-06

Environmental Testing Solutions, Inc. Page 1 of 7
North Carolina Phase II Chronic Whole Effluent Toxicity Test
(EPA-821-R-02-013 Method 1002.0, NC Modification- February, 1998)
Species: Ceriodaphnia dubia
Client:
ut Q Tt)2 E�1� t2au�.keai—\
NPDES 4: NC
Mk
Facility:
!tm A 6,0 N C
Outfall/Pi e:
NA OfJ;:--
Count :
wa
IWC:
rJA
Comments:
Test organism hiformation:
Test in ormation:
Organism age:
¢ 24-hours old
Randomizing template:
Date and times organisms
were born between:
oa-t5'a6 ts�14 TO zo[R
Incubator number and
shelf location:
-2C`
Organism source:
0&-o8•a 6 A- lA
YCT batch:
0%-6Z-o(o
Transfer bowl information:
H=1.11SU Temperature =214•2'C
Selenastrum batch:
U-01-06
Dilution nrenaratinn information: Samnle collection information:
Concentration
t,.2S
q.S
z5
So
15
IpO
t
I
Sample 1
Sample 2
Sample
volume ml
IZ" 5
ZS
Sp
100
1
��
Collection start
date:
0� t5-plo
Diluent
181•S
I1S
1 Sv
Iori
So
Collection end
1D�
volume(ml
time:
Total volume
20D
-2w
Wo
ZCO
Z W
Grab/Composite
C'
(ml)
(duration):
Temperature (°C)
^� • C
upon receipt:
Physical
charaeteristirs:
OPAQae
PAtZS1
ETS project
'Z
number:
ETS sample
OV I)i 16, 0
number:
Daily renewal information:
Day
Date
Test initiation,
renewal, feeding,
or termination time
0
t1g-1b•oe
I'uGadon
13Z0
1
4ci•1'1-06
Feeding
613U
2
18''OL
Renewai 1 M C ^
V , JlJ
3
$-I�l�to
Feeding
OP'13
4
bg-ZO-tjo
Feeding W
5
4 a- 7 t t .
Renewal 2
8c3�t
6
0Q-'LZ-ot�
Feeding
bpzc.
7
48-Z2 ck
T,,,, mwian
6955
Control water Sample numbers
balch used used
08-A-m. 1 060316.
01- N-oe I oloal6.aq
68 1�I-off j abo� l(�. oil
Analyst
Control information:
Acceptance criteria
Summary of test andpoints:
% of Male Adults:
(,
5 24%
7-day LC50
16, 4' f ,
% Adults having 3` Broods:
1,
z 90%
NOEC
(0.251,
Mortali
p•
°
s 20 /°
LOEC
Mean Offspring/Female:
3 a
>_ 15.0 offspring/female
ChV
°
IC25
13-2'{.

r'
Environmental Testing Solutions, Inc. Page 2 of
i
' Species: Ceriodaphnia dubia
Client: GVt,�"o. itr1C.
F CONTROL
J.
i
i
Date: 6& i6-oto
Survival and Reproduction Data
Replicate number
1
2
3
4
5
1 6
7
8
9
10
Dav
2
Adult mortality
(L = live, D =dead)
5
Young produced
1-1'e
ISM
I'i1$
Ilo2
Irjl
ISs6
pr�
t-iz°
I(a�
ISM
Adult mortality
(L = live, D =dead)
L-
6 or 7
Young produced
1
1 s
is
1-
j k
l
g
j '1
IS
! 1
I
Total young produced
32
3o
M
3q
31
3 3
3y
3q
33
32_
Final Adult Mortality
1,
L
L-
L
= live, D = dead
X for 3rd Broads
x
x
%C
X
X-
/<—
/-
Note: A 2D in the upper right corner of the number of young produced indicates the presence of two broods.
Control:
% Monali
Mean Offs ring Female: 3 '�
Concentration: G - S1. Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7 1
8 1
9 1
10
2
Adult mortality
(L = live, D = dead)
L
5
Young produced
jq
2g
z6
26
26
t5
24
!`f
Z6
r j
I (o
l8
2a
IS
Adult mortality
(L = live, D = dead)
L
L
U
L
L
6 Or 7
Young produced
14
1 ('
I"+
(�
I 1
Q
p
Total young produced
U
31
33
3 Z
33
3Z
3 3
3`1
33
Final Adult Mortality
(L = live, D = dead)
t�
L
Note: A 2B in the upper right comer of the number of young produced indicates the presence of two broods.
Test Concentration:
% Mortality:
Y.
Mean Offspring/Female:
34•0
% Reduction from Control:
_q y

Environmental Testing Solutions, Inc. Page 3 of 7
Species: Ceriodaphnia dubia
Client: L"'r—
Concentration: i2.S�10
Date: 09• f(d-ab
Survival and Reproduction Data
Day
Replicate number
1
2
3
4
1 5
1 6
7
8
9
10
2
Adult mortality
(L =live, D = dead)
�--
L
+
L-
5
Young produced
O
Z
O
C)
f pQ
I
C
Adult mortality
L
L
6 Or 7
Young produced
(L = live, D = dead)
3
8
!s
3
Total young produced
3
10
f $
^-1
I -J
`1
C
3
Final Adult Mortality
(L = live, D = dead)
L
L
L
L
Mole= A 2B in the upper right comer of the number of young produces indicates the presence of two nroocs.
C'nnrentrntinnr 25%
Control:
% Mortality:
6' l
Mean Offspring/Female:
{y
% Reduction frorn Control:
e, .
Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
10
2
Adult mortality
{L = live, D =dead)
5
Young produced
Adult mortality
L =live, D = dead)
6 or 7
Young produced
Total young produced
O
d
O
O
U
O
O
0
Final Adult Mortality
(L = live, D = dead)
b
'J
h'ore: A 2B in the upper right comer of the number of young produced indicates the presence of two orooas.
Test Concentration:
% Mortality:
OO 1
Mean Offs rin Female:
0.0
% Reduction from Control:
b- .

Environmental Testing Solutions, Inc. Page 4 of 7
Species: Ceriodaphnia dubia
Client:
Date: _ b8- Ila-O 6
_ Syni71�((toeJ I,I.�C. '�J�� -'
Concentration: Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
10
2
Adult mortality
(L = live, D =dead)
5
Young produced
Adult mortality
(L = live, D = dead)
6 or 7
Young produced
Total young produced
O
0
O
0
0
Q
a
O
O
Final Adult Mortality
(L = live, D = dead)
Node: A 2B in the upper right corner of the number of young produced indicates the presence of two broods.
Cnncentration- -c-7
Control:
Mortality:
Mean Offs rip emale:
p.
% Reduction from Control:
/CQ /
Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
10
2
Adult mortality
(L = live, D =dead)
5
Young produced
Adult mortality
(L = live, D = dead)
6 or 7
Young produced
Total young produced
O
O
O
O
O
Q
O
0
a
O
Final Adult Mortality
(L = live, D = dead)
Nore: A 213 to the upper rrgnt comer of the numoer or young proaucea mmcmes me presence ur twu uruuu.
Test Concentration:
Mortality:
Mean Offspring/Female:
d a
% Reduction from Control:

a
a
I
i
I
Environmental Testing Solutions, Inc. Page 5 of 7
Species: Ceriodaphnia duhia
Client: GgNTN2014, rt- C( - SuitJi-7
Concentration: I no'?
Date: _0A-16-00
Survival and Reproduction Data
Day
Replicate number
I
1 2
1 3
1 4
1 5
6
7
8
9
10
2
Adult mortality
(L = live, D =dead)
`J
5
Young produced
Adult mortality
(L = live, D = dead
6 or 7
Young produced
Total young produced
d
O
0
O
O
O
0
O
O
Final Adult Mortality
(L = Live, D = dead)
D
Note: A 213 in the upper right corner of the number of young produced indicates the presence of two broods.
Concentration:
Control:
% Mortali :
,Mean Offs rine/Female:
6.
% Reduction from Control:
Survival and Reproduction Data
Day
Replicate number
1
2
3
4
5
6
7
8
9
10
2
Adult mortality
(L,= live, D = dead)
5
Young produced
Adult mortality
(L — live, D = dead)
6 or 7
Young produced
Total young produced
Final Adult Mortality
(L = live, D = dead)
More: A 2B in the upper right comer of the number of young prooucea motcates the presence of two orc"
Test Concentration:
% Mortality
Mean Offspring/Female:
% Reduction from Control:
I

a
a
Environmental Testing Solutions, Inc. Page 6 of 7
Species: Ceriodaphnia dubia
Client: , ggNWWUQ , Ii3(, Date: 8-16-06
Concentration: Survival and Reproduction Data
Da
Replicate number
1
2
3
4
5
6
7
S
9
10
2
Adult mortality
(L = live, D = dead)
L-- I
I
I
I
5
Young produced
Adult mortality
(L = live, D = dead)
6 or 7
Young produced
Total young produced
Final Adult Mortalitv
(L = live, D = dead)
Note: A 2H in the upper right comer of the nuMbet of young proaucea inarcates the presenc`ot two br000s.
Control:
% Mortality:
Mean Offs rin emale:
% Reduction from Control:

Environmental Testing Solutions, Inc,
Statistical Analyses
_
Ceriodaphtlia S_un'iv_al and Reproduction Test-7 Day Sun'lval
Start Date:
9/16/2006
Test 1D:
CD17RCRNC
Sample ID:
WRS Infrastructure - SWNIF _ -
End Date:
S/d nM6
Lab ID:
ETS-Envirm. Testing Sol.
Sample Type:
DMR-Discharge Monitoring Report
Sample Dme:
Pratocol:
CHRONIC-EPA-921-R-02-013
Test Species:
CD-Ceriodaphnia dubia
Comments:
Conc-%
1
2
3
4 5
6
7
S
9 10
D-Control
LOOM
LOWO
1.0000
i.0000 1,0000
1.0000
LOM
1.0000
1.D000 1.0000
6.25
1.0000
1.0000
1.0000
1.0000 1.0000
1.0000
1.0000
1.0000
1.0000 1.0000
12-5
1.0000
1.0000
1.0000
LOD00 L0000
O.D000
LOODO
1.00D0
0.0000 1.0000
25
0.0000
0.0000
0.0000
O,0D00 �OMNI
O.DODO
0.0000
0.0000
0.0000 0.0000
50
0.0o00
0.0000
0.0000
O.OD00 0.0000
O.ODDO
0.0000
0.0000
0.0000 0.0000
75
OA000
0.0000
0.0000
O.00DO 0.0000
O.ODW
0.0000
0.0000
0.0000 0000
too
0.00M
0.0000
O.o00D
0.0000 a0000
0.0000
0.0000
0.0000
0.0000 0.0000
Not
Fisher's
1-Tailed
Number
Total
Corte-%
Mean
N-Mean
Resp
Rasp
Total
N
Exact P
Critical
Resp
_Number_
D-Control
1.00W
1.0000
0
10
10
10
0
10
6.25
1.0000
1.0000
0
10
10
10
LOWO
0.0500
0
10
125
0.8000
0.9000
2
8
10
10
0.2369
O.0500
2
10
25
0.0000
O.ODOo
10
0
10
10
10
10
50
0.0000
0.0000
10
0
10
10
10
10
75
0.0000
0.0000
10
0
10
10
10
10
100
0.0000
0.0000
10
0
10
10
10
10
Hypothesis Teal (I -tail, 0.05)
NOEC LOEC
ChV TV
Fishers Exact Test
115 25
17,67766953 8
Treatments vs D-Control
Trintnted Spearman -Barber
Trim Level EC50
95%
CL
0.0% 15.389
12.914
19.339
5.0% 15.692
12.841
19.177
10.0% 15.949
11485
20.375
1.4
20.0% 16.210
14.135
19.591
Auto-0.0% 15.399
12.914
18.339
Ds
0_8
03
m Q.fi
N
C
C0D5
0,4
03
0.2
0.1
0.0
Dose -Response Plat
0.9
0.8
0.7
0.6
z
to 0,5
T
60.4
n
0.3
0.2
0.1
10 100
Dose %
{yRS SWNF 08-16-06

Environmental Testing Solutions, Inc.
Statistical Analyses
Ceriodaplinin Survival and Reproduction Test -Reproduction
Start Date:
9/16/2006
Test ID:
CDFRCRNC
Sample ID: ---
- --
WRS Infrastructure - SSVNF
End Date-.
8/23/2006
Lab ID;
ETS-Environ. Testing Sol.
Sample Type:
DMR-Discharge Monitoring Report
Sample Date:
Protocol:
CHROMIC-EPA-821-R-02-013
Test Species:
CD-Ceriodaphnia dubia
Comrtxnts-
Conc-%
1
2
3
6 5
6
7
8
9 IO
D-Control
37-000
30.000
34,000
34.000 31.000
33.000
34.000
34.000
33.ODO 32000
5,25
38.000
31.000
33,000
38.000 32-000
33.000
32000
33.000
37.000 33.000
12.5
3.000
10.000
15.000
4.000 7,000
0.000
17.000
7.000
0.000 3,000
25
0.000
0.000
0.000
0.000 0,000
0.000
0,000
0.000
0.000 0.000
50
0.000
0.000
0.000
0.000 0,000
0.000
0.000
0.000
0.000 0.000
75
0.000
0.000
0.000
0.000 0.000
0,000
0.000
0.000
0.000 0.000
100
0.000
0.000
0.000
0.000 0,000
0.000
0.000
0,000
0,000 0.000
Traruiurm:
Colic-% Mean N-Aiean
Swn Critical Mean N-Aiean
altrol
32700
1.0000
32700
30.000
34.000
4,337
t0
33.350
LODOO
US
34.000
1.0398
34.000
31.000
38.000
7,720
t0 112,50 79,00
33.350
1.0000
•125
6.600
0.2018
6.600
0.000
17,000
88.981
k0 55.00 79,00
6.600
0.1979
25
0.000
0.0000
0.000
0.000
0.000
0.000
10
0.000
RODOO
50
0.000
0.0000
0-000
0.000
0.000
O.ODO
10
0,000
0.0000
75
0.000
0.0000
0.000
0.000
0.000
0.000
10
O.ODO
0.0000
100
0.000
0.0000
0.000
0.000
0,000
0.000
10
0.000
0.0000
AuritiaryTesis
Statistic Gitical Skew Kurt
Shapiro,Wtli(s Test indicates natural distribution (p > 0.01)
0.934476674 0.9 0.86934241 L75594(i537
Bartlett's Test indicates unequal variances (p = 3.66E-04)
15.82821093 9.2103405
hypothesis Test (I 411H, 0.05) NOEC LOEC
Cliv 'I'U --
Stcel'sMany-One Rank Test 6,25 12.5
8.838834765 16
Trcatr=ts vs D-Control
Linear Interpolation (200 Resanlplcs)
Point % SD 95% CL
Skew
ICOS 6.640 0.036 6,552 6.694
-1.3512
ICiD 7.029 0.057 6921 7.138
0.1494
IC15 7.419 0.082 7.281 7.585 0.2818 I'D
IC20 7.908 0.109 7.625 8.044 0.2864 0.9
IC25 8.198 0.137 7.969 8.514 0.2918
IC40 9.367 0.221 9.000 9.R95 0.2793 0_e
IC50 10.146 0.277 9.688 10.807 0.2823 0.7
w
0.6
N
c 05
CL
0,4
0.3
0.2
O'l
0.0
-0.1
0 2D 40 60 80 100 120
Dose %
Dose -Response Plot
40
35
30
c 25
'U
'4 20
O
G.
!Z 15
10� r:
5
0
o ° IP N r g
N (V r
c m
o
U
0
IRS SWNF 08-16-06

Environmental Testing Solutions, Inc.
Statistical Analyses
PMSD Calculation OnIY.
Ceriodaphnia Survival and Reproduction Test -Reproduction
Stan Date:
U16R006
Test ID:
CDFRCRNC
Samplc ID:
WRS Infrastructure - SWNF
End Date:
8/2312006
LA1D:
ETS-Fit%iron. Tcsting Sol,
SwnpleType:
DMR-DischugeMonitoring Report
Sample Date:
Protocol;
CHRONIC-E.PA-821-R-02-013
Test Species:
CD-Ccriodaphnia dubia
Cornmeatte:
Conc-%
1
2 -
3
d 5
6
7
8
9 10
D-Control
32.000
30.000
34.000
34.000 31.000
33.000
34.000
34,000
33.000 32.OW
6.25
38.000
31.000
33.000
38.000 32.000
33.000
32.000
33.000
37.000 33.000
12.5
3.000
10.000
15.000
4.000 TOW
0.000
17.000
7,000
0.000 3.000
25
0.000
ff(W
0.000
0.000 0.000
0.000
0.000
0.000
0.000 0.000
50
0.000
0.000
0.000
0.000 0.000
0.000
0.000
0.000
0.000 0.000
75
0.000
0.000
0.000
0.000 0.000
0.000
0.000
0.000
0.000 ROW
100
0.000
0.000
0.000
0.000 0.000
0.000
0,0W
0.000
0.000 ROW
Transform: Unlransforoled
I -Tailed
Isotonic
Conc-%
Mean
N-Maul
Mean
Min
Max
CV%
N
tStat Critical
h1SD
Mean
N-Mean
D-Control
32.700
1.0000
32,700
30.000
34.000
4.337
10
33.350
1.00W
6.25
34.000
1.0398
34.OW
31.000
38.000
7.720
10
-0.764 1.999
3.400
33.350
1.0000
+12.5
6.600
0.2018
6.600
0.000
17.000
88.981
10
15.346 1,999
3,400
6.600
0.1979
25
0.000
0.0000
0.000
0.000
0.000
0.000
10
0.000
0.0000
50
0.000
0.0000
0.000
0.000
0.000
0.000
10
0,0W
0.0000
75
O.Ow
0.00D0
0.0W
0.000
0.000
0.000
10
0.000
0.0000
100
0.000
0.0000
0.000
0,000
0.000
0.000
10
0.000
0.0000
Auxiliary Tests
Statistic
_ Critical
Skew_
Kurt
Shapiro-Wilk's Test indicates normal distribution (p > 0.01)
0.93447667
_
0.9
0.86934241
1.75594654
Rankrrs Test indicates unequal muianca (p = 3.66$04)
15.8292108
9.2103405
_
Hypothesis Ted (1-tall, 0.05) NOEC LOEC
ChV TU
MSDu
MSDp MSR
11SE F-Proh
df
DutusetfsTest 6.25 12.5
8.8388347E 16
3.39963491
0,10396437 2389,43333
14.462963 7.2E-16
7,27
Treatmentsvs D-Control
Linear Interpolation (200
Resampla)
Point % SD 95%CL
Skcw
IC05 6.640 0.033 6.584 6,693
-1,1117
lClo 7.029 0.054 6.927 7.137
0,3030
IC15 T.419 0.079 1,294 7.580 0,4625 1.0
IC20 7.808 0.104 7,643 8.024 0.4849 os
IC25 8.198 0.130 7.997 8.467 0.4864
1C40 9,367 0.207 9.046 9.798 0.4806 0,8
IC50 10.146 0.2.59 9.750 10.685 0.4783 0.7
u
06
c 05
CL
n 0.4
u
a 0.3
Dose -Response Not
40
35
30
0 25
x0 15
10
0.2
0.1
20 40 60 80 100 120
Dose %
1-tail, OL05level
of significance
W7?S SWW,? OS-I6.06

Environmental Testing Solutions, Inc.
Chronic Whole Effluent Toxicity Test (EPA-821-R-02-013, Method 1002.0)
Species: Ceriodaphnia dubia
Quality Control
Verification of Data Entry, Calculations, and Statistical Analyses
Client: WRS Infrastructure & Environtnent, Inc. - S WNF
Test dates: August 16 - 23, 2006
Project fruurber: 2720
Reveiwed Ity:
Concentration
{%)
Day
Replicate nuutber
Survival
(°Ia)
Average
reproduction
Coemrtent nr
vuriatiun (90)
Percent mducttan from
control (%)
1
2
3
4V
6
7
S
9
10
Control
5
17
15
17
t6
15
17
19
16
15
100
32.7
4.3
Nat applicable
7
15
15
17
18
18
17
15
17
17
Total
32
30
34
34
33
34
34
33
32
6.25%a
5
19
15
16
19
17
15
16
18
15
I00
34.0
7.7
-4.0
7
19
16
17
19
16
17
17
19
18
Total
38
31
33
38
33
32
33
37
33
12.5%
5
0
2
0
1
0
10
1
0
0
80
6.6
89.0
79.8
7
3
8
15
3
0
7
6
0
3
Total
3
IU
15
4
U
17
7
0
3
5
0
0
0
0
0
0
0
0
0
0
0.0
0.0
100.0
7
0
0
0
0
0
0
0
0
0
Total
0
0
0
0
0
0
0
0
0
0
50%
5
0
0
0
0
0
0
0
0
0
0
0
0.0
0.0
100.0
7
0
0
0
0
0
0
0
0
0
0
Total
0
0
0
a
a
0
0
0
0
0
75 `"ia
5
0
0
0
0
0
0
0
0
0
0
0
0.0
0.0
100.0
7
0
0
0
0
0
0
0
0
0
0
Total
0
0
0
0
0
0
0
0
0
0
100%n
5
0
0
0
0
0
0
0
0
0
0
0
0,0
0.0
100.0
7
0
0
0
0
0
0
0
0
0
0
Total
U
-01
0
0
0
0
0
0
0
0
Dunnett'S MSD value: 3,400 MSD = Minimum Significant Difference
PMSD: 10.4 PMSD = Percent Minimum Significant Difference
PMSD is a measure of test precision. The PMSD is the minimum percent difference between the control and treatment that can be declared
statistically significant in a whole effluent toxicity test. On average, a siolicant difference occurs for Enviromuental Testing Solutions, Inc,
chronic toxicity tests when a toxicant reduces Ceriodaphnia reproductionby 9.6% from the control.
lower PMSD bound determined by USEPA (10"' percentile) ; 11 %.
Upper PMSD bound determined by USEPA (90"' percentile) = 37%.
The lower and upper bounds were calculated by die USEPA using 393 tests conducted from 33 laboratories for Ceriodaphnia reproduction in
chronic reference toxicant tests.
USEPA 2000. Understanding and Accounting for Method Variability in Whole Effluent Toxicity Applications Under the National Pollutant Discharge Elimination Program. EPA-833-R-00-003. US Environmental Protection Agency,
Cincinnati, OR
"S SUWF 08-l6-06

Environmental Testing Solutions, Inc.
Shipping address: Phone: [phone]
351 Depot Street Fax: [phone]
Asheville, NC 28801
Whole Effluent Toxicity Chain -of -Custody Form
Facility. WRS Infrastructure & Environment, Inc. NPDES €i: _
Synthron, Inc. Purchase order.
Species: Ceriodaphyda dubia Effluent dilution
Test type: PhaseII/Chronic Parameter code:
Sample information: (to be completed by sample collector)
Composite sample:
Start date: Time:
End date: Time:
Number of samples per hour.
Chilled during collection?
If chilled, specifyternperaturc:
Grab sample:
Date: $•1t57•06 Time: !u:c9dArvi
Pipe N: County: Burke
C..'ts,12.5 ,t5 so115,
THP3 B
Sample location: C -vt4,rsr cc
Volume collected for testing: Z k
Number of containers filled for testing: a�
Total residual chlorine (mg/L): "A_
Temperature at time of collection M:
Method of transport to laboratory. �eda
Comments: '�M-s0-1e- -4 1 - SW r
s.- f-f r -ff a - &U oJ'r
Note: DO NOT collect samples before 8:00 AM. Triple rinse sample container with sample before filling. Completely fill
tii2 sanipie cartaii.e'r ;.:t. n:. oar space. Pacl: the cc.....ine. �cn.plete:J° it: ice. Tfrc sar p:e muat'rc ..._....et! at � ,! tl°C'
An additional fee of $50.00 per sample will be charged for samples collected before 8:00 AM.
Sample custody: (to be completed by sample collector and facility personnel)
Sample collected by:
"
Itl:� t1M
Prau Sig»xe llatc and lime
Relinquished by:
I d:od Arn
Prml Sigwasre pate aid tiro,
Relinquished by:
hint sign-,.
Dom —d time
Sample receipt information: (to be completed by ETS personnel)
Relinquished to ETS by:
pre• Ib-O�
rem
Print Sig t.. Date ad time
Custody seats intact'?: F"t =
Ys Na Fot—d
Samples received in good condition?:
Received by:
Few 0&t�
Pant sivu D—"tint,
Received by:
Print Sig�aNre Dam and tune
Received at ETS by:
04 • Ib•Ob
kL
µ-r�� Oqy b
Print Siguliue Date aed twnc
Sample temperature upon receipt at ETS (°C):
tl
Ye Project number: 91610 Sample number: aU t b.
Comments: lk y OioQ(3 I

Environmental Testing Solutions, Inc.
Ceriodaphnia duhia Control Reproduction, Coefficient of Variation, and PMSD
in Sodium Chloride Chronic Reference Toxicant Tests
40
0 35
d
.� 30
o
2 -'r3b 25
Q" 20
c c
V 1.5
0 40
IN
30
A 20
a
10
North Carolina Acceptance Limit (< 40.0%)
Kentucky Acceptance Limit (< 30.0%)
USEPA Upper PMSD Bound (90'h percentile < 37.0%)
d� 05 05,05 0� 05 0� 05 �ti 0`�0`��006 O'J 06 0+1 ob 01 Ob 0s 06 O' 06 06"06 >> Ob Og 06
Test date
Control Reproduction, Coefficient of Variation (CV), or Percent Minimum Significant Difference
(PMSD) PMSD is the minimum significant difference between the control and treatment that can be
declared statistically significant.
— — Central Tendency (mean Control Reproduction, CV, or PMSD)
Control Limits (mean Control Reproduction, CV, or PMSD ± 2 Standard•De iations)

1.12
1.10
1.08
1.06
1.04
2.5
2.0
z
1.5
N
U 1.0
0.5
►.4
1.3
1.2
1.1
1.0
0.9
08
Environmental Testing Solutions, Inc.
Ceriodaphnia dubia
Sodium Chloride Chronic Reference Toxicant Control Chart
using Moderately Hard Synthetic Water
USEPA Control Limits (= 2 Standard Deviations)
USEPA Warning and Control Limits (75`h and 90th Percentile CVs)
D� D�,DOA D�.0o5 D3Ao6 D� Ao� 111 00� ,tiAo� D9Ao9 ,�,o,D O� 0 `, D� o,^, 06AO,,QAO.L Oy 00� D �.DO� 0� �DA.Da.D4� Dti.Dob D6,Do� NO D�A6
Test date
7-day IC25 = 25% inhibition concentration. An estimation of the concentration of sodium chloride
that would cause a 25% reduction in Ceriodaphnia reproduction for the test population.
— — Central Tendency (mean IC25)
— Warning Limits (mean IC25 ± SAAO or SA.75)
. .. ... .....
Control Limits (mean IC25 ± SA25, SAgo, or 2 Standard Deviations)

>a
Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-01
Project: Synthron, Inc
Collection Date: 5/10/2006
2:05:00
PM
Lab ID: 0605651-001
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET
COMPOUN
SW8081A
(SW3610B)
Analyst: MM
4,4'-DOD
BRL
0,10
pg/L
70734
1
5/12/2006 1:26 PM
4,4'-DDE
BRL
0.10
lig/L
70734
1
5/12/2006 1:26 PM
4,4'-DDT
BRL
0.10
pg/L
70734
1
5/12/2006 1:26 PM
Aldrin
BRL
0.050
pg/L
70734
1
5/12/2006 1:26 PM
alpha-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 1:26 PM
alpha -Chlordane
BRL
0.050
pg1L
70734
1
5/12/2006 1:26 PM
beta-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 1:26 PM
delta-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 1:26 PM
Dieldrin
BRL
0.10
pg/L
70734
1
5/12/2006 1:26 PM
Endosulfan I
BRL
0.050
pg/L
70734
1
5/1212006 1:26 PM
Endosulfan Il
BRL
0.10
pglL
70734
1
5/12/2006 1:26 PM
Endosulfan sulfate
BRL
0.10
pg/L
70734
1
5/12/2006 1:26 PM
Endrin
BRL
0.10
pg/L
70734
1
5/12/2006 1:26 PM
Endrin aldehyde
BRL
0.10
pg/L
70734
1
5/12/2006 1:26 PM
Endrin ketone
BRL
0.10
pg/L
70734
1
5/12/2006 1:26 PM
gamma-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 1:26 PM
gamma -Chlordane
BRL
0.050
pg/L
70734
1
5/12/2006 1:26 PM
Heptachlor
BRL
0.050
pg/L
70734
1
5/12/2006 1:26 PM
Heptachlor epoxide
BRL
0.050
pg/L
70734
1
5/12/2006 1:26 PM
Methoxychlor
BRL
0.50
pg/L
70734
1
5/12/2006 1:26 PM
Toxaphene
BRL
5.0
pg1L
70734
1
5/12/2006 1:26 PM
Surr. Decachlorobiphenyl
45.9
17.9-122
%REC
70734
1
5/12/2006 1:26 PM
Surr. Tetrachloro-m-xylene
84.0
18.9-119
%REC
70734
1
5/12/2006 1:26 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Aluminum
5.66
0.200
mg1L
70708
1
5/11/2006 8:09 PM
Antimony
0.0545
0.0200
mg1L
70708
1
5/11/2006 8:09 PM
Arsenic
BRL
0.0500
mg1L
7070E
1
5/11/2006 8:09 PM
Barium
0.188
0.0200
mg1L
70708
1
5/11/2006 8:09 PM
Beryllium
BRL
0.0100
mg1L
70708
1
5/11/2006 8:09 PM
Cadmium
BRL
0.0050
mg1L
70708
1
5/11/2006 8:09 PM
Calcium
44,0
0.100
mg1L
70708
1
5/11/2006 8:09 PM
Chromium
0.0290
0.0100
mg1L
70708
1
5/11/2006 8.09 PM
Cobalt
0A521
0.0200
mg1L
70708
1
5/11/2006 8:09 PM
Copper
0.105
0.0100
mg/L
70708
1
5/11/2006 8:09 PM
Iron
209
0.500
mg/L
70708
5
5/12/2006 1:20 PM
Lead
0.151
0.0100
mg/L
70708
1
5/11/2006 8:09 PM
Magnesium
5.80
0.100
mg/L
70708
1
5/11/2006 8:09 PM
Manganese
5.90
0,0050
mg1L
70708
1
5/11/2006 8:09 PM
Molybdenum
BRL
0.0500
mg1L
70708
1
5/11/2006 8:09 PM
Nickel
BRL
0.0200
mg/L
70708
1
5/11/2006 8:09 PM
Potassium
14.1
0.500
mg/L
70708
1
5/11/2006 8:09 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analvte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantization range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page] of'30

Analytical Environmental Services, Inc. Date: 16-Mav-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-01
Project: Synthron, Inc
Collection Date: 5/10/2006
2:05:00 PM
Lab ID: 0605651-001
illatrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Selenium
0.0250
0,0200
mg1L
70708
1
5/11/2006 8:09 PM
Silver
BRL
0.0100
mglL
70708
1
5/11/2006 8:09 PM
Sodium
224
5.00
mglL
70708
5
5/12/2006 1:20 PM
Thallium
BRL
0.0200
mg1L
70708
1
5/11/2006 8:09 PM
Tin
0,127
0.0500
mg1L
70708
1
5/11/2006 8:09 PM
Titanium
0.136
0.0500
mg1L
70708
1
5/11/2006 8:09 PM
Vanadium
0.0357
0.0100
mg1L
70708
1
5/11/2006 8:09 PM
Zinc
3.28
0.0200
mg1L
70708
1
5/11/2006 8:09 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: AO
Mercury
0.00026
0.00020
mglL
70854
1
5/15/2006 4:32 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Anatyst: DA
1X-Biphenyl
BRL
1000
pg1L
70749
1
5/122006 T04 PM
2,4,5-Trichlorophenol
BRL
2500
pg1L
70749
1
5/12/2006 3:04 PM
2,4,6-Trichlorophenol
BRL
1000
pg1L
70749
1
5/122006 3:04 PM
2,4-Dlchlorophenol
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
2,4-Dimethylphenol
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
2,4-Dinitrophenol
BRL
2500
pg1L
70749
1
5/12/2006 3:04 PM
2,4-Dinitrotoluene
BRL
1000
pglL
70749
1
5/122006 3:04 PM
2,6-Dinitrotoluene
BRL
1000
pg1L
70749
1
5/122006 3:04 PM
2-Chloronaphthalene
BRL
1000
pg1L
70749
1
5/122006 3:04 PM
2-Chlorophenol
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
2-Methylnaphthalene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
2-Methylphenol
BRL
1000
pglL
70749
1
5/122006 3:04 PM
2-Nitroaniline
BRL
2500
pg1L
70749
1
5/12/2006 3:04 PM
2-Nilrophenol
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
3,3'-Dichlorobenzidine
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
3-Nitroaniline
BRL
2500
pg1L
70749
1
5/12/2006 3:04 PM
4,6-Dinitro-2-methylphenol
BRL
2500
pg1L
70749
1
5/12/2006 3:04 PM
4-Bromophenyl phenyl ether
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
4-Chloro-3-methylphenol
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
4-Chloroaniline
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
4-Chlorophenyl phonyl ether
BRL
1000
pglL
70749
1
5/12/2006 3:04 PM
4-Methylphenol
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
4-Nitroaniline
BRL
2500
pg1L
70749
1
5/12/2006 3:04 PM
4-Nitrophenol
BRL
2500
pg1L
70749
1
5/1212006 3:04 PM
Acenaphthene
BRL
1000
pg1L
70749
1
5/1212006 3:04 PM
Acenaphthylene
BRL
1000
pg1L
70749
1
5/1212006 3:04 PM
Acetophenone
BRL
1000
pg1L
70749
1
5/122006 3:04 PM
Anthracene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Atrazine
BRL
1000
pglL
70749
1
5/122006 3:04 PM
Qualirrers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NFLAC certified
B Analyte detected in the associated Method Blank
F Estimated (Value above quantitation range)
5 Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 2 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-01
Project: Synthron, Inc
Collection Date: 5/10/2006
2:05:00
PM
Lab ID: 0605651-001
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Benzaldehyde
BRL
1000
pg/L
70749
1
51121200B 3:04 PM
Benzo(a)pyrene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Benzo(b)fluoranthene
BRL
1000
pq/L
70749
1
5/12/2006 3:04 PM
Benzo(g,h,i)perylene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Benzo(k)fluoranthene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Bis(2-chloroothoxy)methane
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Bis(2-chloroethyl)ether
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Bis(2-chloroisopropyl)ether
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Bis(2-ethylhexyl)phthalate
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Butyl benzyl phthalate
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Caprolactam
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Carbazole
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Chrysene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Dibenz(a,h)anthracene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Dibenzofuran
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Diethyl phthalate
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Dimethyl phthalate
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Di-n-butyl phthalate
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Di-n-octyl phthalate
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Fluoranthene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Fluorene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Hexachlorobenzene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Hexachlorobutadiene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Hexachlorocydopentadiene
BRL
1000
pg/L
70749
1
5/12/2006 M4 PM
Hexachloroethane
BRL
1000
p91L
70749
1
5/12/2006 3:04 PM
Indeno(1,2,3-cd)pyrene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Isophorone
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Naphthalene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Nitrobenzene
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
N-Nitrosodi-n-propylamine
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
N-Nitrosodiphenylamine
BRL
1000
pg1L
70749
1
5/12/2006 3:04 PM
Pentaohlorophenol
BRL
2500
pg1L
70749
1
5/12/2006 3:04 PM
Phenanthrene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Phenol
1600
1000
pg1L
70749
1
5/12/2006 3:04 PM
Pyrene
BRL
1000
pg/L
70749
1
5/12/2006 3:04 PM
Surr: 2.4,6-Tribromophenol
99.4
64.8-129
%REG
70749
1
5/12/2006 3:04 PM
Surr. 2-Fluorobiphenyi
91.5
58.2-115
%REC
70749
1
5/12/2006 3:04 PM
Surr. 2-Fluorophenol
46.7
24.4-115
%REG
70749
1
5/1212M6 3:04 PM
Surr. 4-Terphenyl-d14
78.9
58.3-115
%REC
70749
1
5/12/2006 3:04 PM
Sum Nitrobenzene-d5
106
51.5-115
%REC
70749
1
5112/2006 3:04 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E Estimated (Value above quantization
range)
BRL Below Reporting Limit
S Surrogate
Recovery outside accepted
recovery limits
I Holding times for preparation or analysis exceeded
Narr Sec
Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 3 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech FM Inc.
Client Sample ID: FT-01
Project: Synthron, Inc
Collection
Date: 5/10/2006
2:05:00
PM
Lab ID: 0605651-001
Matrix: SURFACE WATER
�
Analyses
Result
Reporting
Limit Qual
Dilution
Units BatchlD Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
77.9
17.9-115
%REC 70749
1
5/12/2006 3:04 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,1-0ichloroethane
BRL
5.0
pg1L
70847
1
511212006 9:28 PM
1,1-Dichloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
12,4-Trichlorobenzene
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,2-Dibromoethane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,2-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,2-Dichloroethane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,2-Dichloropropane
BRL
5.0
pg/L
70847
1
5/12/2005 9:28 PM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
2-Butanone
340
50
pg/L
70847
1
5/12/2006 9:28 PM
2-Hexanone
BRL
10
pg/L
70847
1
5/12/2006 9:28 PM
4-Methyl-2-pentanone
25
10
pg/L
70847
1
5/12/2006 9:28 PM
Acetone
16000
5000
pg1L
70847
100
5/12/2006 2:56 PM
Benzene
5.8
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Bromodichloromethane
BRL
5.0
pglL
70847
1
5/12/2006 9:28 PM
Bromoform
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
Bromomethane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Carbon disulfide
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Carbon tetrachloride
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Chlorobenzene
12
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Chloroethane
BRL
10
pglL
70847
1
5/12/2006 9:28 PM
Chloroform
BRL
5.0
pg1L
70847
1
6/12/2006 9:28 PM
Chloromethane
BRL
10
pg/L
70847
1
5/12/2006 9:28 PM
cis- 1,2-Dichloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
cis- 1,3-Dichloropropene
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Cyclohexane
20
5.6
pg/L
70847
1
5/12/2006 9:28 PM
Dibromochloromethane
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Dichlorodifluoromethane
BRL
10
pg/L
70847
1
5/12/2006 9:28 PM
Ethylbenzene
67
5.0
pg1L
70847
1
5/12/2006 9:28 PM
Freon-113
BRL
10
pglL
70847
1
5/12/2006 9:28 PM
Isopropylbenzene
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
m,p-Xylene
240
10
pg/L
70847
1
5112/2006 9:28 PM
Methyl acetate
BRL
5.0
pg/L
70847
1
5/12/2006 9:28 PM
Methyl tent -butyl ether
BRL
5.0
pg/L
70847
1
5112/2006 9:28 PM
Methylcydohexane
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
L'
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis
exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analvte detected in the associated
Method Blank
Page 4 of 30

Analytical Environmental Services, Inc.
Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-01
Project: Synthron, Inc
Collection Date: 5/10/2006 2:05:00
PM
Lab ID: 0605651-001
Matrix: SURFACE WATER
Anal ses
y
Result
Reporting
Limit Qua, Units
Batch1D
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
o-Xylene
72
5.0
pg1L
70847
1
5/12/2006 9:28 PM
Styrene
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
Tetrachloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
Toluene
350
300
pg1L
70847
100
5/12/2006 2:56 PM
trans-1,2-Dichloroethene
BRL
5,0
pglL
70847
1
5/12/2006 9:28 PM
trans-1,3-Dichloropropene
BRL
5.0
pglL
70847
1
5/12/2006 9:28 PM
Trichloroelhene
BRL
5.0
pg1L
70847
1
5/12/2006 9:28 PM
Trichlorofluoromethane
BRL
5.0
pglL
70847
1
5/12/2006 9:28 PM
Vinyl chloride
BRL
2.0
pg1L
70847
1
5/12/2006 9:28 PM
Surr: 4-Bromofluorobenzene
96.3
63.7-115
%REC
70847
100
5/12/2006 2:56 PM
Surr: 4-Bromofluorobenzene
97.9
617-115
%REC
70847
1
5/12/2006 9:28 PM
Surr: Dibromofluoromethane
95.2
70.4-123
%REC
70847
100
5/12/2006 2:56 PM
Surr: Dibromofluoromethane
95.7
70.4-123
%REC
70847
1
5/12/2006 9:28 PM
Surr: Toluene-d8
101
73.4-115
%REC
70847
100
5/12/2006 2:56 PM
Surr: Toluene-d8
102
73.4-115
%REC
70847
1
5/12/2006 9:28 PM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
1560
500
mg1L
70755
100
5/11/2006 3:00 PM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
4140
100
mg1L
70790
10
5/12/2006 10:45 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
11 Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Nair See Case Narrative
NC Not Confirmed
Page 5 of 30

Analytical Environmental Services, Inc.
Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-02
Project: Synthron, Inc
Collection Date: 5/10/2006
2:15:00 PM
Lab 1D: 0605651-002
Matrix- SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
0.10
pg/L
70734
1
5/12/2006 1:38 PM
4,4'-DDE
BRL
0.10
pg/L
70734
1
5/12/2006 1:38 PM
4,4'-DDT
BRL
0.10
pg/L
70734
1
5/12/2006 1:38 PM
A1drin
BRL
0.050
pg/L
70734
1
5/12/2006 1:38 PM
atpha-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 1:38 PM
alpha -Chlordane
BRL
0.050
pglL
70734
1
5/12/2005 1:38 PM
beta-BHC
BRL
0,050
pg/L
70734
1
5/12/2006 1:38 PM
delta-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 1:38 PM
Dieldrin
BRL
0.10
pg1L
70734
1
5/12/2006 1:38 PM
Endosulfan I
BRL
0.050
pg/L
70734
1
5/12/2006 1:38 PM
Endosulfan II
BRL
0.10
pg1L
70734
1
5/12/2006 1:38 PM
Endosulfan sulfate
BRL
0,10
pg/L
70734
1
5/12/2006 1:38 PM
Endrin
BRL
0.10
pg/L
70734
1
5/12/2006 1:38 PM
Endrin aldehyde
BRL
0,10
pg/L
70734
1
5/1212006 1:38 PM
Endrin ketone
BRL
0.10
pg/L
70734
1
5/12/2006 1:38 PM
gamma-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 1:38 PM
gamma -Chlordane
BRL
0.050
}tg/L
70734
1
5/12/2006 1:38 PM
Heptachlor
BRL
0.050
pg/L
70734
1
5/12/2006 1:38 PM
Heptachlor epoxide
BRL
0.050
pg/L
70734
1
5/12/2006 1:38 PM
Meihoxychlor
BRL
0.50
pg/L
70734
1
5/12/2006 1:38 PM
Toxaphene
BRL
5.0
pg/L
70734
1
5/12/2006 1:38 PM
Surr: Decachlorobiphenyl
45.7
17.9-122
%REC
70734
1
5/12/2006 1:38 PM
Surr: Tetrachlaro-m-xylene
49.5
18.9-119
%REC
70734
1
5/12/2006 1:38 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Aluminum
1.68
0.200
mglL
70708
1
5/11/2006 8:12 PM
Antimony
0.0560
0.0200
mg1L
70708
1
5/11/2006 8:12 PM
Arsenic
BRL
0.0500
mg1L
70708
1
5/11/2006 8:12 PM
Barium
0.0414
0.0200
mg1L
70708
1
5/11/2006 8:12 PM
Beryllium
BRL
0.0100
mg/L
70708
1
5/11/2005 8:12 PM
Cadmium
BRL
0.0050
mg1L
70708
1
5/11/2006 8:12 PM
Calcium
11.4
0.100
mg1L
70708
1
5/11/2006 8:12 PM
Chromium
0.0172
0,0100
mg/L
70708
1
5/1112006 8:12 PM
Cobalt
BRL
0.0200
mg1L
70708
1
5/11/2006 8:12 PM
Copper
0.0622
0.0100
mg1L
70708
1
5/11/2006 8:12 PM
Iron
144
0.500
mg/L
70708
5
5/12/2006 1:24 PM
Lead
0.0655
0.0100
mg/L
70708
1
5/11/2006 8:12 PM
Magnesium
2.14
0.100
mg1L
70708
1
5/11/2006 8:12 PM
Manganese
1.02
0.0050
mg/L
70708
1
5/11/2006 8:12 PM
Molybdenum
BRL
0.0500
mg/L
70708
1
5/11/2006 8:12 PM
Nickel
BRL
0.0200
mg/L
70708
1
5/11/2006 8:12 PM
Potassium
7.43
0.500
mg/L
70708
1
5/11/2006 8:12 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRI_ Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B. Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 6 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-02
Project: Synthron, Inc
Collection
Date: 5/10/2006
2:15:00
PM
Lab ID: 0605651-002
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua[
Limit
Units BatchlD
Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Selenium
BRL
0.0200
mg1L
70708
1
5/11/2006 8:12 PM
Silver
BRL
0.0100
mg1L
70708
1
5/11/2006 8:12 PM
Sodium
68.8
1.00
mg1L
70708
1
5/11/2006 8:12 PM
Thallium
BRL
0.0200
mg/L
70708
1
5/11/2006 8:12 PM
Tin
0.102
0.0500
mg/L
70708
1
5/11/2000 8:12 PM
Titanium
0.0723
0.0500
mg/L
70708
1
5/11/2006 8:12 PM
Vanadium
0,0156
0.0100
mg/L
70708
1
5/11/2006 8:12 PM
Zinc
1.14
0.0200
mg/L
70708
1
5/11/2006 8:12 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: AO
Mercury
0.00022
0.00020
mg/L
70854
1
5/15/2006 4.40 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
13
10
pg1L
70749
1
5/12/2006 3:31 PM
2,4,5-Trichlorophenol
BRL
25
pg1L
70749
1
5/12/2006 3:31 PM
2,4,6-Trichlarophenol
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
2,4-Dichlorophenol
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
2,4-Dimethylphenol
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
2,4-Dinitrophenol
BRL
25
pg1L
70749
1
5/12/2006 3:31 PM
2,4-Dinitrotoluene
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
2,6-Dinitrotoluene
BRL
10
yg1L
70749
1
5112/2006 3:31 PM
2-Chloronaphthalene
BRL
10
Vg1L
70749
1
5/12/2006 3:31 PM
2-Chlorophenol
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
2-Methytnaphthatene
41
10
pg/L
70749
1
5/12/2006 3:31 PM
2-Melhylphenol
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
2-Nitroaniline
BRL
25
pg/L
70749
1
5/12/2006 3:31 PM
2-Nitrophenol
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
3,3'-Dichlorobenzidine
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
3-Nitroaniline
BRL
25
pg1L
70749
1
5/12/2006 3:31 PM
4,6-Dinitro-2-methylphenol
BRL
25
pg1L
70749
1
5/12/2006 3:31 PM
4-Bromophenyl phenyl ether
SRL
10
pg1L
70749
1
5/12/2005 3:31 PM
4-Chloro-3-methylphenol
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
4-Chloroaniline
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
4-Chlorophenyl phenyl ether
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
4-Methyiphenol
340
50
pg/L
70749
5
5/15/2006 11:14 AM
4-Nitroanitine
BRL
25
pg/L
70749
1
5/12/2006 3:31 PM
4-Nitrophenol
BRL
25
pg/L
70749
1
5/12/2006 3:31 PM
Acenaphthene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Acenaphthylene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Acetophenone
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Anthracene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Atrazine
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Qualifiers: ; Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation
or analysis
exceeded
Narr
See Case Narrative
N Analyze not NELAC certified
NC
Not Confinned
B Analyte detected in the associated Method Blank
Page 7 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-02
Project: Synthron, Inc
Collection Date: 5/10/2006
2:15:00 PM
Lab ID: 0605651-002
Matrix: SURFACE WATER
Analyses
Result
Reporting
Qual Units
8atchlD
Dilution
Date Analyzed
Limit
Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Senz(a)anthracene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Benzaldehyde
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Senzo(a)pyrene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Benzo(b)fluoranthene
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Benzo(g,h,i)perylene
BRL
10
pglL
70749
1
5/12/2006 3:31 PM
Benzo(k)fluoranthene
SRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Bis(2-chloroethoxy)methane
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Bis(2-chloroethyl)ether
BRL
10
pglL
70749
1
5/12/2006 3:31 PM
Bis(2-chloroisopropyl)ether
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Bis(2-ethylhexy1)phthalate
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Butyl benzyl phthalate
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Caprolactam
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Carbazole
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Chrysene
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Dibenz(a,h)anthracene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Dibenzofuran
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Diethyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Dimethyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Di-n-butyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Di-n-octyl phthalate
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Fluoranthene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Ftuorene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Hexachlorobenzene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Hexachlorobutadiene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Hexachlorocydopentadiene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Hexachloroethane
BRL
10
pg/L
70749
1
5/12=06 3:31 PM
Indeno(1,2,3-cd)pyrene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Isophorone
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Naphthalene
26
10
pg/L
70749
1
5/12/2006 3:31 PM
Nitrobenzene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
N-Nitrosodi-n-propylamine
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
N-Nitrosodiphonylamine
BRL
10
pg/L
70749
1
5/1212006 3:31 PM
Pentachlorophenol
BRL
25
pg/L
70749
1
5/12/2006 3:31 PM
Phenanthrene
BRL
10
pg1L
70749
1
5/12/2006 3:31 PM
Phenol
56
10
pg1L
70749
1
5/12/2006 3:31 PM
Pyrene
BRL
10
pg/L
70749
1
5/12/2006 3:31 PM
Surr. 2,4,6-Tribromophenol
87.7
64.8-129
%REC
70749
1
5/12/2006 3:31 PM
Surr. 2-Fluorobiphenyl
82.7
58.2-115
%REC
70749
1
5/1212006 3:31 PM
Surr: 2-Fluorophenol
51.4
24.4-115
%REC
70749
1
5/12/2006 3:31 PM
Sum 4-TerphenyIA14
69.1
58.3-115
%REC
70749
1
5/12/2006 3:31 PM
Surr. Nitrobenzene-d5
76.1
51.8-115
%REC
70749
1
6/12/2006 3:31 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
L• Estimated (Value above quantitation range)
BRL Below Reporting Limit
S Surrogate Recovery
outside accepted recovery limits
H Holding times for preparation or analysis
exceeded
Narr See Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 9 of 30

Analytical Environmental Services, Inc. Date: 16-Hay-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-02
Project: Synthron, Inc
Collection Date: 5/10/2006
2:15:00
PM
Lab ID: 0605651-002
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
. Analyst: DA
Surr; Phenol-d5
51.2
17.9-115
%REC 70749
1
5/12/2006 3:31 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg1L
70847
t
5/14/2006 1:01 PM
1,1,2,2-Tetrachloroethane
BRL
5.0
µg1L
70847
1
5/14/2006 1:01 PM
1,1,2-Trichloroethane
BRL
5.0
pg1L
70847
1
5114/20061:01 PM
1,1-Dichloroethane
BRL
5.0
pg1L
70847
1
5114120061:01 PM
1,1-Dichloroethene
BRL
5.0
pglL
70847
1
5114/2006 1 :011 PM
1,2,4-Trichlorobenzene
BRL
5.0
pg1L
70847
1
5/14/2006 1;01 PM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70847
1
5114120061:01 PM
1,2-Dibromoethane
BRL
5.0
pg1L
70847
1
5/14/2006 1 ;01 PM
1,2-Dichlorobenzene
BRL
5.0
pg1L
70847
1
5114120061:01 PM
1,2-Dichloroethane
BRL
5.0
µg1L
70847
1
5114/20061:01 PM
1,2-Dichloropropane
BRL
5.0
pg1L
70847
1
5114/20061:01 PM
1,3-Dichlorobenzene
BRL
5.0
pglL
70847
1
5114/20061:01 PM
1,4- Di chloro benzene
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
2-Butanone
150
50
pglL
70847
1
5/14/2006 1:01 PM
2-Hexanone
BRL
10
pglL
70847
1
5/14/2006 1:01 PM
4-Methyl-2-pentanone
36
10
pg/L
70847
1
5/14/2006 1:01 PM
Acetone
2300
1500
pglL
70847
100
5/12/2006 8:10 PM
Benzene
9.2
5.0
µglL
70847
1
5/14/2006 1:01 PM
Bromodichloromethane
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
Bromoform
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
Bromomethane
BRL
5.0
pg1L
70847
1
5/14/2006 1:01 PM
Carbon disulfide
BRL
5.0
µglL
70847
1
5/14/2006 1:01 PM
Carbon tetrachloride
BRL
5.0
µglL
70847
1
5/14/2006 1:01 PM
Chlorobenzene
32
5.0
µglL
70847
1
5/14/2006 1:01 PM
Chloroethane
BRL
10
pg1L
70847
1
5/14/2006 1:01 PM
Chloroform
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
Chloromethane
BRL
10
pg1L
70847
1
5/14/2006 1:01 PM
cis- 1,2-Dichloroethene
BRL
5.0
pg1L
70847
1
5114120061:01 PM
cis-1,3-Dichloropropene
BRL
5.0
µg1L
70847
1
5114120061:01 PM
Cyclohexane
34
5.0
pg1L
70847
1
5/14/2006 1:01 PM
Dibromochloromethane
BRL
5.0
pg/L
70847
1
5/14/2006 1:01 PM
Dichlorodifluoromethane
BRL
10
pg1L
70847
1
5/14/2006 1:01 PM
Ethylbenzene
90
5.0
pg1L
70847
1
5/14/2006 1:01 PM
Freon-113
BRL
10
pg1L
70847
1
5/14/2006 1:01 PM
Isopropylbenzene
9.4
5.0
pg1L
70847
1
5/14/2006 1:01 PM
m,p-Xylene
320
10
pglL
70847
1
5/14/2006 1:01 PM
Methyl acetate
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
Methyl tert-butyl ether
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
Methylcydohexane
5.5
5.0
pglL
70847
1
5/14/2006 1:01 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Estimated (Value above guantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
11 Molding times for preparation or analysis
exceeded
Narr
See Case Narrative
N Analyze not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method Blank
Page 9 of 30

Analytical Environmental Services, Inc.
Date: 16-May-06
CLIENT: Tetra "Tech EM Inc.
Client Sample ID: FT-02
Project: Synthron, Inc
Collection Date: 5/10/2006 2:15:00
PM
Lab 1D: 0605651-002
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual Units
Limit
BatchlD
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pgIL
70847
1
5/14/2006 1:01 PM
o-Xylene
120
5.0
pglL
70847
1
5/14/2006 11:01 PM
Styrene
BRL
5.0
pgIL
70847
1
5/14/2006 1:01 PM
Tetrachloroethene
BRL
5.0
uglL
70847
1
5114120061:01 PM
Toluene
560
500
pglL
70847
100
5/12/2006 8:10 PM
trans•1,2-Dichloroethene
BRL
5.0
ug1L
70847
1
5/14/2006 1:01 PM
trans-1,3-Dichloropropene
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
Trichloroethene
BRL
5.0
1rgIL
70847
1
5/14/2006 1:01 PM
Trichlorofluoromethane
BRL
5.0
pglL
70847
1
5/14/2006 1:01 PM
Vinyl chloride
BRL
2.0
pglL
70847
1
5/14/2006 1:01 PM
Surr: 4-Bromofluorobenzene
99.0
63.7.115
%REC
70847
1
5/14/2006 1:01 PM
Surr: 4-Bromofluorobenzene
95.5
63.7-115
%REC
70847
100
5/12/2006 8:10 PM
Surr: Dibromofluoromethane
95.6
70.4-123
%REC
70847
1
5/14/2006 1:01 PM
Surr: Dibromofluoromethane
94A
70.4-123
%REC
70847
100
5/12/2006 8:10 PM
Surr: Toluene-d8
98.6
73.4-115
%REC
70847
1
5/14/2006 1:01 PM
Surr: Toluene-d8
102
73.4-115
%REC
70847
100
5/12/2006 8:10 PM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
431
50.0
mg/L
70755
10
5/11/2006 3:00 PM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
1370
10
mglL
70790
1
5/12/2006 10:45 AM
Qualiriers: ' Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC cerli5ed
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 10 of 30

Analytical Environmental Services, Inc. Dace: 16-Mav-06
CLIENT: Tetra Tech EM Inc,
Client Sample ID: FT-03
Project: Synthron, Inc
Collection Date: 5/10/2006
2:30:00 PM
Lab ID: 0605651-003
Matrix: SURF -ACE WATER
Analyses
Result
Reporting Qual
Limit
Units
RatchlD
Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW351013)
Analyst: MM
4,4'-DDD
BRL
0.10
pg1L
70734
1
5/12/2006 1:50 PM
4,4'-DDE
BRL
0.10
pg1L
70734
1
5/12/2006 1:50 PM
4,4'-DDT
BRL
0.10
pg1L
70734
1
5/12/2006 1:50 PM
Aldrin
BRL
0.050
pg/L
70734
1
5/12/2006 1:50 PM
alpha-BHC
BRL
0,050
pg1L
70734
1
5/12/2006 1:50 PM
alpha -Chlordane
BRL
0.050
pg1L
70734
1
5/12/2006 1:50 PM
beta-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 1:50 PM
delta-BHC
13RL
0.050
lig/L
70734
1
5/12MO6 1:50 PM
Dieldrin
BRL
0.10
pg/L
70734
1
5/12/2006 1:50 PM
Endosulfan I
BRL
0.050
pg/L
70734
1
5/12/2006 1:50 PM
Endosulfan 11
BRL
0.10
pg1L
70734
1
5/12/2006 1;50 PM
Endosulfan sulfate
BRL
0.10
y91L
70734
1
5/12/2006 1:50 PM
Endrin
BRL
0.10
pg1L
70734
1
5/12/2006 1:50 PM
Endrin aldehyde
BRL
0,10
pg1L
70734
1
5/12/2006 1:50 PM
Endrin ketone
BRL
0.10
pg/L
70734
1
5/12/2006 1:50 PM
gamma-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 1:50 PM
gamma -Chlordane
BRL
0.050
pg/L
70734
1
5/12/2006 1:50 PM
Heptachlor
BRL
0.050
pg/L
70734
1
5/12/2006 1:50 PM
Heptachlor epoxide
0.39
0.050
pg/L
70734
1
5/12/2006 1:50 PM
Methoxychlor
BRL
0.50
pg/L
70734
1
5/12/2006 1:50 PM
Toxaphene
BRL
5.0
pg/L
70734
1
5112/2006 1:50 PM
Surr: Decachlorobiphenyi
35.6
17.9-122
%REC
70734
1
5/12/2006 1:50 PM
Surr: Tetrachioro-m-xylene
35.1
18.9-119
%REC
70734
1
5/12/2006 1:50 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Aluminum
0.449
0.200
mg/L
70708
1
5/11/2006 8:16 PM
Antimony
0.0472
0.0200
mg/L
70708
1
5/11/2006 8:16 PM
Arsenic
BRL
0.0500
mg/L
70708
1
5/11/2006 8:16 PM
Barium
0.0617
0.0200
mg1L
70708
1
5/11/2006 8:16 PM
Beryllium
BRL
0.01100
mg1L
70708
1
5/11/2006 8:16 PM
Cadmium
BRL
0.0050
mg/L
70708
1
5/11/2006 8:16 PM
Calcium
19.7
0.100
mg1L
70708
1
5/11/2006 8:16 PM
Chromium
0.0406
0.0100
mg/L
70708
1
5111/2006 8:16 PM
Cobalt
BRL
0,0200
mg/L
70708
1
5111/2006 8:16 PM
Copper
0.0388
0.0100
mg/L
70708
1
5111/2006 8:16 PM
Iron
304
1.00
mg/L
70708
10
5/12/2006 4:00 PM
Lead
0.0126
0.0100
mg/L
70708
1
5/11/2006 8:16 PM
Magnesium
2.59
0.100
mg/L
70708
1
5/11/2006 8:16 PM
Manganese
2.04
0.0050
mg/L
70708
1
5/11/2006 8:16 PM
Molybdenum
BRL
0.0500
mg1L
70708
1
5/11/2006 8:16 PM
Nickel
0.0638
0.0200
mg1L
70708
1
5/11/2006 816 PM
Potassium
7.36
0.500
mg/L
70708
1
5/11/2006 8:16 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Nair See Case Narrative
NC Not Con Firmed
Page 11 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron, Inc
Lab ID: 0605651-003
Client Sample ID: FT-03
Collection Date: 5/10/2006 2:30:00 PM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Units
BitchlD
Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Selenium
0.0254
0.0200
mg1L
70708
1
5/11/2006 8:16 PM
Silver
BRL
0.0100
mglL
70708
1
5/11/2006 6:16 PM
Sodium
39.1
1.00
rngfL
70708
1
5/11/2006 8:16 PM
Thallium
BRL
0.0200
mg1L
70708
1
5/11=06 8:16 PM
Tin
0.0624
0.0500
mg1L
.70708
1
5/11/2006 8:16 PM
Titanium
BRL
0.0500
mg/L
70708
1
5/11/2006 8:16 PM
Vanadium
0.0482
0.0100
mg1L
70709
1
5/11/2006 8:16 PM
Zinc
0,534
0.0200
mglL
70708
1
5/11/2006 6:16 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: AO
Mercury
BRL
0.00020
mg/L
70854
1
5/15/2006 4:42 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
2,4,5-Trichlorophenol
BRL
25
pg1L
70749
1
5/12/2006 3:58 PM
2,4,6-Trichlorophenol
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
2,4-Dichlorophenol
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
2,4-Dimethylphenol
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
2,4-Dinitrophenel
BRL
25
pg/L
70749
1
5/12/2006 3:58 PM
2,4-Dinitrotoluene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
2,6-Dinitrotoluene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
2-Chloronaphthalene
BRL
10
ijg/L
70749
1
5/12/2006 3:58 PM
2-Chlorophenol
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
2-Methy1naphthalene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
2-Methylphenol
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
2-Nitroaniline
BRL
25
pg1L
70749
1
5/12/2006 3:58 PM
2-Nitrophenol
BRL
10 _
y91L
70749
1
5/12/2006 3:58 PM
3,Y-Dichlorobenzidine
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
3-Nitroaniline
BRL
25
pg/L
70749
1
5/12/2006 3:58 PM
4,6-Dinitro-2-methyl phenol
BRL
25
pg/L
70749
1
5/12/2006 3:58 PM
4-Bromophenyl phenyl ether
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
4-Chloro-3-methylphenol
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
4-Chlaroaniline
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
4-Chlorophenyl phenyl ether
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
4-Methylphenot
820
100
PA
70749
10
5/1512006 12:07 PM
4-Nitroaniline
BRL
25
pq/L
70749
1
5/12/2006 3:58 PM
4-Nitrophenol
BRL
25
pg/L
70749
1
5/12/2006 3:58 PM
Acenaphthene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Acenaphthylene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Acetophenone
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Anthracene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Atrazine
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H I folding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 12 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-03
Project: Synthron, Inc
Collection Date: 5/10/2006
2:30:00
PM
Lab 1D: 0605651-003
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Benzaldehyde
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Benzo(a)pyrene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Benzo(b)fluoranthene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
8enzo(g,h,i)perylene
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Benzo(k)fluoranthene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Bis(2-chloroethoxy)methane
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Bis(2-chloroethyl)ether
BRL
10
NgIL
70749
1
5/12/2006 3:58 PM
Bis(2-chloroisopropyi)ether
BRL
10
pg/L
70749
1
5112/2006 3:58 PM
Bis(2-ethylhexyl)phthalate
14
10
pg/L
70749
1
5/12/2006 3:58 PM
Butyl benzyl phthalate
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Caprolactam
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Carbazote
BRL
10
pglL
70749
1
5/12/2006 3:58 PM
Chrysene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Dibenz(a,h)anthracene
BRL
10
NgIL
70749
1
5/12/2006 3:58 PM
Dibenzoturan
BRL
10
NgIL
70749
1
5/12/2006 3:58 PM
Diethyl phthalate
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Dimethyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Di-n-butyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Di-n-octyl phthalate
BRL
10
NgIL
70749
1
5/12/2006 3:58 PM
Fluoranthene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Fluorene
BRL
10
NgIL
70749
1
5/12/2006 3:58 PM
Hexachlorobenzene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Hexachlorobutadiene
BRL
10
pg/L
70749
1
5/12/2006 3-.58 PM
Hexachlorocyclopentadiene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Hexachloroethane
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Indeno(1,2,3-cd)pyrene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Isophorone
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
!Naphthalene
BRL
10
pglL
70749
1
5/12/2006 3:58 PM
Nitrobenzene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
N-Nitrosodi-n-propylamine
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
N-Nitrasodiphenylamine
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Pentachlorophenol
BRL
25
pglL
70749
1
5/12/2006 3:58 PM
Phenanthrene
BRL
10
pg1L
70749
1
5/12/2006 3:58 PM
Phenol
68
10
pg1L
70749
1
5/12/2006 3:58 PM
Pyrene
BRL
10
pg/L
70749
1
5/12/2006 3:58 PM
Surr: 2,4,6-Tri bromo phenol
78.2
64.8-129
%REC
70749
1
5/12/2006 3:58 PM
Surr: 2-Fluorobiphenyi
78.7
58.2-115
%REC
70749
1
5/12/2006 3:58 PM
Surr: 2-Fluorophenol
62.2
24.4-115
%REC
70749
1
5/12/2006 3:58 PM
Surr. 4-Terphenyl-d14
62.5
58.3-115
%REC
70749
1
5/12/2006 158 PM
Surr: Nitrobenzene-d5
71.5
51.8-115
%REC
70749
1
5/12/2006 3:58 PM
Qualiriers: Value exceeds Maximum Contaminant Level
E Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S Surrogate
Recovery outside accepted
recovery limits
H Holding times for preparation or analysis exceeded
Narr See
Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
11 Analyte detected in the associated
Method
Blank
Page 13 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-03
Project: Synthron, Inc
Collection Date: 5/10/2006
2:30:00
PM
Lab ID: 0605651-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua]
Limit
Units BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
44.5
17,9-115
%REC 70749
1
5/12/2006 3:58 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg1L
70847
1
5/13120066:36AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70847
1
511312006 6:36 AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70847
1
5/1312006 6:36 AM
1,1-Dichloroethane
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
1,1-Dichloroethene
BRL
5.0
pg1L
70847
1
5/1312006 6:36 AM
1,2,4-Trichlorobenzene
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
1,2-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/13/2006 U6 AM
1,2-Dichloroethane
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
1,2-Dichloropropane
BRL
5.0
pglL
70847
1
5/13/2006 6:36 AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
2-Butanone
330
50
pg/L
70847
1
5/13/2006 6:36 AM
2-Hexanone
BRL
10
pg/L
70847
1
5/13/2006 6:36 AM
4-Methyl-2-pentanone
57
10
pg1L
70847
1
5/13/2006 6:36 AM
Acetone
1800
1500
pg/L
70847
100
5/12/2006 8:36 PM
Benzene
5.8
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Bromodichloromethane
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Bromotorm
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Bromomethane
BRL
5.0
pglL
70847
1
5/13/2006 6:36 AM
Carbon disulfide
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Carbon tetrachloride
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Chlorobenzene
110
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Chloroethane
BRL
10
pg/L
70847
1
5/13/2006 6:36 AM
Chloroform
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Chloromethane
BRL
10
pg/L
70847
1
5113/2006 6:36 AM
cis- 1,2-Dichloroethene
BRL
5.0
pglL
70847
1
5/13/2006 6:36 AM _
cis-1,3-Dichloropropene
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Cyclohexane
11
5.0
pg/L
70847
1
5/13/2006 6:36 AM
DibromocNoromethane
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Dichlorodifluoromethane
BRL
10
pg/L
70847
1
5/13/2006 6:36 AM
Ethylbenzene
72
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Freon-113
BRL
10
pg/L
70847
1
5/13/2006 6:36 AM
Isopropylbenzene
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
m,p-Xylene
250
10
pg1L
70847
1
5/13/2006 6:36 AM
Methyt acetate
170
5.0
pg/L
70847
1
5N 3/2006 6:36 AM
Methyl tent -butyl ether
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Methylcyclohexane
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte net NELAC certified
NC
Not Confirmed
13 Analyte detected in the associated
Method
Blank
Page 14 of 30

Analytical Environmental Services, Inc.
Date: 16-May-06
CLIENT: Tetra Tech CM Inc.
Client Sample ID: FT-03
Project: Synthron, inc
Collection Date: 5/10/2006
2:30:00 PM
Lab ID: 0605651-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua,
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
19
5.0
pg/L
70847
1
5/13/2006 6:36 AM
o-Xylene
70
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Styrene
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Tetrachloroethene
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Toluene
430
300
pg/L
70847
100
5/12/2006 8:36 PM
trans-1,2-Dichloroethene
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
trans- 1,3-Dichloropropene
BRL
5.0
pg/L
70847
1
5/1312006 6:36 AM
Trichloroethene
BRL
5.0
pg1L
70847
1
5/13/2006 6:36 AM
Trichlorofluoromethane
BRL
5.0
pg/L
70847
1
5/13/2006 6:36 AM
Vinyl chloride
BRL
2.0
pg1L
70847
1
5/13/2006 6:36 AM
Surr: 4-Bromofluorobenzene
95.9
63.7-115
%REC
70847
100
5/12/2006 8:36 PM
Surr: 4-Bromofluorobenzene
97.6
63.7-115
%REC
70847
1
5/13/2006 6:36 AM
Surr: Dibromofluoromethane
93.8
70.4-123
%REC
70847
100
5/12/2006 8:36 PM
Sure Dibromofluoromethane
95.8
70.4-123
%REC
70847
1
5/13/2006 6:36 AM
Surr: Toluene-d8
101
73A-115
%REC
70847
100
5/12/2006 8:36 PM
Surr. Toluene-d8
103
73.4-115
%REC
70847
1
5/1312006 6:36 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
1240
50.0
mg/L
70755
10
5/11/2006 3:00 PM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
2620
100
mg/L
70790
10
5/12/2006 10:45 AM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
I: Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 15 of 30

Analytical Environmental Services, Inc.
Date: 16-May-06
CLIENT: 'Tetra "Tech EM Inc.
Client Sample ID: FT-04
Project: Synthron, Inc
Collection Date: 5/10/2006
2:45:00 PM
Lab ID: 0605651-004
Matrix: SURFACE WATER
Analyses
Result
Reporting Q.-al
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET
COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
0.10
pg/L
70734
1
5/12/2006 2:02 PM
4,4'-DDE
BRL
0.10
pg1L
70734
1
5/12/2006 2:02 PM
4,4'-DDT
BRL
0.10
pg/L
70734
1
5/12/2006 2:02 PM
Aldrin
BRL
0.050
pg1L
70734
1
5/12/2006 2:02 PM
alpha-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 2:02 PM
alpha -Chlordane
BRL
0.050
pg/L
70734
1
5/12/2006 2:02 PM
beta-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 2:02 PM
delta-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 2:02 PM
Dieldrin
BRL
0.10
pg/L
70734
1
5/12/2006 2:02 PM
Endosulfan I
BRL
0.050
pg1L
70734
1
5/12/2006 2:02 PM
Endosulfan II
BRL
0.10
pg/L
70734
1
5/12/2006 2:02 PM
Endosulfan sulfate
BRL
0.10
pg1L
70734
1
5/12/2006 2:02 PM
Endrin
BRL
0.10
pg/L
70734
1
5/12/2006 2:02 PM
Endrin aldehyde
BRL
0.10
pg1L
70734
1
5/12/2006 2:02 PM
Endrin ketone
BRL
0.10
pg1L
70734
1
5/12/2006 2:02 PM
gamma-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 2:02 PM
gamma -Chlordane
BRL
0.050
pg/L
70734
1
5/12/2006 2:02 PM
Heptachlor
1.3
0.050
pg/L
70734
1
5/12/2006 2:02 PM
Heptachlor epoxide
BRL
0.050
pg/L
70734
1
5/12/2006 2:02 PM
MethoxycHor
BRL
0.50
pg1L
70734
1
5/12/2006 2:02 PM
Toxaphene
BRL
5.0
pg1L
70734
1
5/12/2006 2:02 PM
Surr: Decachlorobiphenyl
44.5
IT9-122
%REC
70734
1
5/12/2006 2:02 PM
Surr: Tetrachloro-m-xylene
49.1
18.9-119
%REC
70734
1
5/12/2006 2:02 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Aluminum
0.809
0.200
mg1L
70708
1
5/11/2006 8:19 PM
Antimony
0.111
0.0200
mg1L
70708
1
5/11/2006 8:19 PM
Arsenic
BRL
0.0500
mg/L
70708
1
5111/2006 8:19 PM
Barium
0.155
0.0200
mg1L
70708
1
5111/2006 8:19 PM
Beryllium
BRL
0.0100
mg/L
70708
1
5/11/2006 8:19 PM
Cadmium
BRL
0.0050
mg/L
70708
1
5/11/2006 8:19 PM
Calcium
17.1
0A00
mg1L
70708
1
5111/2006 8:19 PM
Chromium
0.172
0.0100
mg/L
70708
1
5/11/2006 8:19 PM
Cobalt
BRL
0.0200
mg/L
70708
1
5/1112006 8:19 PM
Copper
0.0957
0.0100
mg/L
70708
1
5/11/2006 8:19 PM
Iron
203
0.500
mg1L
70708
5
5/12/2006 1732 PM
Lead
0.0642
0,0100
mg/L
70708
1
5/11/2006 8:19 PM
Magnesium
2.75
0A 00
mg1L
70708
1
5/11/2006 8:19 PM
Manganese
1.11 .
0.0050
mg/L
70708
1
5/11/2006 8:19 PM
Molybdenum
BRL
0,0500
mg/L
70708
1
5/11/2006 8:19 PM
Nickel
BRL
0,0200
mg1L
70708
1
5/11/2006 8:19 PM
Potassium
9.23
0.500
mg/L
70708
1
5/11/2006 8:19 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte net NELAC certihcd
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Con Firmed
Page 16 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron, Inc
Lab ID: 0605651-004
Client Sample ID: FT-04
Collection Date: 5/10/2006 2:45:00 PM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Units
BatchlD Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Selenium
0.0286
0.0200
mg/L
70708
1
5111/2006 8:19 PM
Silver
BRL
0.0100
mg/L
70708
1
5/11/2006 8:19 PM
Sodium
198
5.00
mg/L
70708
5
5/12/2006 1:32 PM
Thallium
BRL
0.0200
mg/L
70708
1
5/11/2006 8:19 PM
Tin
0.204
0.0500
mg/L
70708
1
5/11/2006 8:19 PM
Titanium
BRL
0.0500
mg1L
70708
1
5/11/2006 8:19 PM
Vanadium
0,0903
0.0100
mg1L
70708
1
5/11/2006 819 PM
Zinc
1.83
0.0200
mg/L
70708
1
5111/2006 8:19 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: AO
Mercury
0.00048
0.00020
mg/L
70854
1
5/15/2006 4:43 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
12
10
pg/L
70749
1
5/12/2006 4:25 PM
2,4,5-Trichlorophenol
BRL
25
pg/L
70749
1
5112/2006 4:25 PM
2,4,6-Trichlorophenol
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
2,4-Dichlorophenol
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
2,4-Dimethylphenol
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
2,4-Dinitrophenol
BRL
25
pg/L
70749
1
5/12/2006 4:25 PM
2,4-Dinitrotoluene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
2,6-Dinitrotoluene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
2-Chloronaphthalene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
2-Chlorophenol
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
2-Methylnaphthalene
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
2-Methylphenol
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
2-Nitroaniline
BRL
25
pg/L
70749
1
5/12/2006 4:25 PM
2-Nitrophenol
BRL
10
pg/L
70749
1 .
5/12/2006 4:25 PM
3,3'-Dichlorobenzidine
BRL
1 D
pg/L
70749
1
5/12/2006 4:25 PM
3-Nitroaniline
BRL
25
pg/L
70749
1
5/12/2006 4:25 PM
4,6-Dinitro-2-methylphenol
BRL
25
pg/L
70749
1
5/12/2006 4:25 PM
4-Bromophenyl phenyl ether
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
4-Chloro-3-methylphenol
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
4-Chloroaniline
BRL
10
pglL
70749
1
5/12/2006 4:25 PM
4-Chlorophenyl phenyl ether
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
4-Methylphenol
720
100
pg/L
70749
10
5/15/2006 11:41 AM
4-Nitroaniline
BRL
25
pg/L
70749
1
5112/2006 4:25 PM
4-Nitrophenol
BRL
25
pg1L
70749
1
5/12/2006 4:25 PM
Acenaphthene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Acenaphthylene
BRL
10
pg/L
70749
1
5/12/2005 4:25 PM
Acetophenone
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Anthracene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Atrazine
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H I folding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated ( Value above quantization range)
S Surrogate Recovery outside accepted recovery I imits
Narr See Case Narrative
NC Not Confirmed
Page 17 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech ENE Inc.
Client Sample ID: FT-04
Project: Synthron, Inc
Collection Date: 5/10/2006
2:45:00 PM
Lab ID: 0605651-004
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchlD
Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Benzaldehyde
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Benzo(a)pyrene
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Benzo(b)fluoranthene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Benzo(g,h,i)perytene
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Benzo(k)fluoranthene
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Bis(2-rhloroethoxy)methane
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Bis(2-chloroethyl)ether
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Bis(2-chloroisopropyl)ether
BRL
10
pglL
70749
1
5112120064:25 PM
81s(2-ethylhexyl)phthalate
24
10
pg/L
70749
1
5/12/2006 4:25 PM
Butyl benzyl phthalale
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Caprolactam
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Carbazole
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Chrysene
BRL
10
pglL
70749
1
5/12/2006 4:25 PM
Dibenz(a,h)anthracene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Dibenzofuran
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Diethyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Dimethyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Di-n-butyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Di-n-octyl phthalate
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Fluoranthene
BRL
10
pg/L
70749
1
5/12/2006 425 PM
Fluorene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Hexachlorobenzene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Hexachlorobuladiene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Hexachlorocydopentadiene
BRL
10
pg1L
70749
1
6/12/2006 4:25 PM
Hexachloroethane
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Indeno(1,2,3-cd)pyrene
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Isophorone
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Naphthalene
12
10
pg/L
70749
1
5/12/2006 4:25 PM
Nitrobenzene
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
N-Nitrosodi-n-propylamine
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
N-Nitrosodiphenylamine
BRL
10
pg/L
70749
1
5/12/2006 4:25 PM
Pentachlorophenol
BRL
25
pg1L
70749
1
5/12/2006 4:25 PM
Phenanthrene
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Phenol
300
100
pg1L
70749
10
5/15/2006 11:41 AM
Pyrene
BRL
10
pg1L
70749
1
5/12/2006 4:25 PM
Sum 2,4,6-Tribromophenol
74.3
64.8-129
%REC
70749
1
5/12/2006 4:25 PM
Sum 2-Fluorabiphenyl
83.1
58.2-115
%REC
70749
1
5/12/2006 4:25 PM
Sum 2-Fluorophenol
58.2
24.4-115
%REC
70749
1
5/12/2006 4:25 PM
Surr: 4-Terphenyl-d14
72.5
58.3-115
%REC
70749
1
5/12/2006 4:25 PM
Sum Nitrobenzene-d5
64.2
51.8-115
%REC
70749
1
5/12/2006 4:25 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
E Estimated (Value above yuantitation
range)
BRL Below Reporting Limit
S Surrogate Recovery
outside accepted
recovery limits
li Holding times for preparation or analysis
exceeded
Narr See Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
H Analyte detected in the associated
Method Blank
Page 18 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-04
Project: Synthron, Inc
Collection Date: 5/10/2006
2:45:00 PM
Lab ID: 0605651-004
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units 6atchlD
Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenoi-c15
50.9
17.9-115
%REC 70749
1
5/12/2006 4:25 PM
TCL VOLATILE ORGANICS
SW82608
(SW5030B)
Analyst: NWH
1.1.1-Trichloroethane
BRL
5.0
pg1L
70847
1
5/13/2006 7:02 AM
1,1,2,2-Teirachloroethane
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1, 1,2-Trich loroethane
BRL
5.0
pg1L
70847
1
511312006 7:02 AM
1,1-Dichloroethane
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,2,4-Tdchlorobenzene
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,2-Dichlorobenzene
BRL
5.0
pg1L
70847
1
5/13/2006 7:02 AM
1,2-Dichloroethane
12
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
2-Butanone
210
50
pg/L
70847
1
5/13/2006 7:02 AM
2-Hexanone
BRL
10
pg1L
70847
1
5/13/2006 7:02 AM
4-Methyl-2-penlanone
580
500
yg1L
70847
100
5/12/2006 9:02 PM
Acetone
3400
1500
pglL
70847
100
5/12/2006 9:02 PM
Benzene
17
5.0
pglL
70847
1
5/13/2006 7:02 AM
Bromodichloro methane
BRL
5.0
pglL
70847
1
5/13/2006 T02 AM
Bromoform
BRL
5.0
pglL
70847
1
5/13/2006 7:02 AM
Bromomethane
BRL
5.0
pglL
70847
1
5/13/2006 7:02 AM
Carbon disulfide
BRL
5.0
pglL
70847
1
5/13/2006 7:02 AM
Carbon tetrachloride
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Chlorobenzene
61
5.0
pg1L
70847
1
5/13/2006 7:02 AM
Chloroethane
BRL
10
pg/L
70847
1
5/13/2006 7:02 AM
Chloroform
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Chloromethane
BRL
10
pg1L
70847
1
5/13/2006 7:02 AM
cis- 1,2-Dichloroethene
BRL
5.0
pglL
70847
1
5/13/2006 7:02 AM
cis- 1,3-Dichloropropene
BRL
5.0
pglL
70847
1
5/13/2006 7:02 AM
Cyclohexane
29
5.0
pg/L
70847
1
5/13/2006 T02 AM
Dibromochloromethane
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Diehl orodif! uoromethane
BRL
10
pglL
70847
1
5/1312006 7:02 AM
Ethylbenzene
200
100
pglL
70847
100
5/12/2006 9:02 PM
Freon-113
BRL
10
pg1L
70847
1
5/13/2006 7:02 AM
Isopropylbenzene
BRL
5.0
pglL
70847
1
5/13/2006 7:02 AM
m,p-Xylene
820
200
pg/L
70847
100
5/12/2006 9:02 PM
Methyl acetate
88
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Methyl tert-butyl ether
BRL
5.0
pg1L
70847
1
5/13/2006 7:02 AM
Methylcydohexane
BRL
5.0
pg/L
70847
1
5/13/2006 T02 AM
Qualifiers: * Value exceeds Maximum Contaminant
Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated Method
Blank
Page 19 of 30

Analytical Environmental Services, Inc. Date: 16-A1ay-06
CLIENT:
Tetra Tech EM Inc.
Client Sample ID:
FT-04
Project:
Synthron, Inc
Collection Date:
5/10/2006 2:45:00 PM
Lab ID:
0605651-004
Matrix:
SURFACE WATER
Analyses
Result
Reporting QuaI
Limit
Units
BatchlD
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
64
5.0
pg1L
70847
1
5/13/2006 7:02 AM
o-Xylene
190
100
pg/L
70847
100
5/12/2006 9:02 PM
Styrene
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Tetrachloroethene
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Toluene
720
300
pg/L
70847
100
5/12/2006 9:02 PM
trans-1.2-Dichloroethene
BRL
5.0
pg1L
70847
1
5/13/2006 7:02 AM
trans-1.3-Dichloropropene
BRL
5.0
pglL
70847
1
51IM006 7:02 AM
Trichloroethene
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Trichlorofluoromethane
BRL
5.0
pg/L
70847
1
5/13/2006 7:02 AM
Vinyl chloride
BRL
2.0
pg/L
70847
1
5/13/2006 7:02 AM
Surr: 4-Bromofluorobenzene
96.1
63.7-115
%REC
70847
100
5/12/2006 9:02 PM
Surr: 4-Bromofluorobenzene
96.9
63.7-115
%REC
70847
1
5/13/2006 7:02 AM
Surr: Dibromofluaromethane
94.0
70.4-123
%REC
70847
100
5/12/2006 9:02 PM
Surr. Dibromofluoromethane
94.8
70.4-123
%REC
70847
1
5/13/2006 7:02 AM
Surr. Toluene-d8
99.1
73.4-115
%REC
70847
1
5/13/2006 7:02 AM
Surr. Toluene-d8
102
73.4-115
%REC
70847
100
5/12/2006 9:02 PM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
Biochemical Oxygen Demand 836 50.0
CHEMICAL OXYGEN DEMAND (COD)
Chemical Oxygen Demand 2080 50
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
l { Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E405.1 (E405.1) Analyst: CAM
mg/L 70755 10 5/11/2006 3:00 PM
E410.4 (E410.4) Analyst: EK
mg/L 70790 5 5/12/2006 10:45 AM
E Estimated (Value above quantitwion range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 20 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-05
Project: Synthron, Inc
Collection Date: 5/10/2006
3:00:00
PM
Lab ID: 0605651-005
Matrix: SURFACE
WATER
Analyses
Result
Reporting Qua
Limit
Units BatchlD Dilution
Factor
Rate Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4.4'-DDD
BRL
0.10
pg1L
70734
1
5/12/2006 2:15 PM
4,4'-DDE
BRL
0,10
ltg/L
70734
1
5/12/2006 2:15 PM
4,4'-DDT
BRL
0.10
pg/L
70734
1
5/12/2006 2:15 PM
Aldrin
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
alpha-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
alpha -Chlordane
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
beta-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
delta-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 2:15 PM
Dieldrin
BRL
0.10
pg/L
70734
1
5/1212006 2:15 PM
Endosulfan I
BRL
0.050
pg/L
70734
1
5/1212006 2:15 PM
Endosulfan II
BRL
0.10
pg/L
70734
1
5/12/2006 2:15 PM
Endosulfan sulfate
BRL
0.10
pg/L
70734
1
5/12/2006 2:15 PM
Endrin
BRL
0.10
pg/L
70734
1
5/12/2006 2:15 PM
Endrin aldehyde
BRL
0A0
pg1L
70734
1
5/12/2006 2:15 PM
Endrin ketone
BRL
0.10
pg/L
70734
1
5/12/2006 2:15 PM
gamma-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
gamma -Chlordane
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
Heptachlor
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
Heptachlor epoxide
BRL
0.050
pg/L
70734
1
5/12/2006 2:15 PM
Methoxychlor
BRL
0.50
pg/L
70734
1
5/12/2006 2:15 PM
Toxaphene
BRL
5.0
pg/L
70734
1
5/12/2006 2:15 PM
Surr: Decachlorobiphenyl
27.4
17.9-122
%REC 70734
1
5/12/2006 2:15 PM
Surr: Tetrachloro-m-xylene
0
18.9-119 S
%REC 70734
1
5/12/2006 2:15 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Aluminum
10.9
0.200
mg/L
70708
1
5/11/2006 8:22 PM
Antimony
0.252
0,0200
mg/L
70708
1
511112DD6 8:22 PM
Arsenic
0.128
0.0500
mg/L
70708
1
5/11/2006 8:22 PM
Barium
0,136
0.0200
mg/L
70708
1
5111/2006 8:22 PM
Beryllium
BRL
0.0100
mg/L
70708
1
5/11/2006 8:22 PM
Cadmium
0.0142
0.0050
mg/L
70708
1
5/11/2006 8:22 PM
Calcium
104
1.00
mg1L
70708
10
5112/2006 1:36 PM
Chromium
0.110
0.0100
mg/L
70708
1
5/11/2006 8:22 PM
Cobalt
0.0254
0,0200
mg/L
70708
1
5/11/2006 8:22 PM
Copper
0,492
0.0100
mg/L
70708
1
5/11/2006 8:22 PM
Iron
38.1
0.100
mg/L
70708
1
5/11/2006 8:22 PM
Lead
0.330
0.0100
mg1L
70708
1
5/1112006 8:22 PM
Magnesium
9.51
0.100
mg/L
70708
1
5/11/2006 8:22 PM
Manganese
1.34
0.0050
mg/L
70708
1
5/11/2006 8:22 PM
Molybdenum
BRL
0.0500
mg/L
70708
1
5/11/2006 8:22 PM
Nickel
BRL
0,0200
mg/L
70708
1
5/11/2006 8:22 PM
Potassium
23.3
0.500
mg/L
70708
1
5/11/2006 8:22 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantization range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 21 of 30

Analytical Environmental Services, Inc. Dare: 16-Alav-06
CLIENT: Tetra Tech FM Inc.
Project: Synthron, Inc
Lab ID: 0605651-005
Client Sample ID: FT-05
Collection Date: 5/10/2006 3:00:00 PM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Units
BatchlD Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Selenium
0.0390
0.0200
mg/L
70708 1
5/11/2006 8:22 PM
Silver
BRL
0,0100
mg/L
70708 1
5/11/2006 8:22 PM
Sodium
603
10.0
mglL
70708 10
5/12/2006 1:36 PM
Thallium
BRL
0.0200
mg/L
70708 1
5/11/2006 8:22 PM
Tin
0.544
0.0500
mg/L
70708 1
5/11/2006 8:22 PM
Titanium
0.420
0,0500
mg1L
70708 1
5/11/2006 8:22 PM
Vanadium
0,118
0.0100
mg/L
70708 1
5/11/2006 8:22 PM
Zinc
13.5
0,0200
mg/L
70708 1
5/11/2006 8:22 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: AO
Mercury
0,00039
0.00020
mg/L
70854 1
5115/2006 4:49 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
2,4,5-Trichlorophenol
BRL
2500
pg/L
70749
1
5/12/2006 4:52 PM
2,4,6-Trichlorophenol
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
2,4-Dichlorophenol
BRL
1000
pglL
70749
1
5/12/2006 4:52 PM
2,4-Dimethylphenol
BRL
1000
pg/L
70749
1.
5/12/2006 4:52 PM
2,4-Dinitrophenol
BRL
2500
lig/L
70749
1
5/12/2006 4:52 PM
2,4-Dinitrotoluene
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
2,6-Dinitrotoluene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
2-Chloronaphthalene
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
2-Chlorophenol
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
2-Methylnaphthalene
BRL
1000
pglL
70749
1
5/12/2006 4:52 PM
2-Methylphenol
BRL
1000
NgIL
70749
1
5/12/2006 4:52 PM
2-Nitroaniline
BRL
2500
pg/L
70749
1
5/12/2006 4:52 PM
2-Nitrophenol
BRL
1000
yg/L
70749
1
5/12/2006 4:52 PM
3,3'-Dichlorobenzidine
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
3-Nitroaniline
BRL
2500
pg1L
70749
1
5/12/2006 4:52 PM
4,6-Dinitro-2-methylphenoi
BRL
2500
pg/L
70749
1
5/12/2006 4:52 PM
4-Bromophenyl phenyl ether
BRL
1000
pg1L
70749
1
5/12/2006 4:62 PM
4-Chloro-3-methylphenol
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
4-Chloroaniline
BRL
1000
p91L
70749
1
5/12/2006 4:52 PM
4-Chlorophenyl phenyl ether
BRL
1000
pg1L
70749
1
6/12/2006 4:52 PM
4-methylphenol
12000
1000
pg/L
70749
1
5/12/2006 4:52 PM
4-Nitroaniline
BRL
2500
pg1L
70749
1
5/12/2006 4:52 PM
4-Nitrophenol
BRL
2500
pg/L
70749
1
5/12/2006 4:52 PM
Acenaphthene
BRL
1000
pg1L
70749
1
5/12MOB 4:52 PM
Acenaphthylene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Acetophenone
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Anthracene
BRL
1000
pg/L
70749
1
5/1212006 4:52 PM
Atrazine
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Qualifiers: Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NFLAC certified
B Analyte detected in the associated Method Blank
E Fstimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 22 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-05
Project: Synthron, Inc
Collection Date: 5/10/2006
3:00:00
PM
Lab ID: 0605651-005
Matrix: SURFACE
WATER
Analyses
Result
Reporting
Limit
Qua] Units
BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Benzatdehyde
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Benzo(a)pyrene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Benzo(b)tluoranthene
BRL
1000
pglL
70749
1
5/12/2006 4:52 PM
Benzo(g,h,i)perylene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Benzo(k)ftuoranthene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Bis(2-chloroethoxy)methane
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Bis(2-chloroethyl)ether
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Bis(2-chloroisopropyl)ether
BRL
1000
pg1L
70749
1
5112l2006 4:52 PM
Bis(2-ethylhexyl)phthalate
2400
1000
pg1L
70749
1
5/12/2006 4:52 PM
Butyl benzyl phthalate
BRL
1000
pglL
70749
1
5/12/2006 4:52 PM
Caprolactam
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Carbazole
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Chrysene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Dibenz(a,h)anthracene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Dibenzofuran
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
Diethyl phthalate
BRL
1000
pglL
70749
1
5/12/2006 4:52 PM
Dimethyl phthalate
BRL
1000
pglL
70749
1
5112/2006 4:52 PM
Di-n-butyl phthalate
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Di-n-octyl phthalate
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Fluoranthene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Fluorene
BRL
1000
pglL
70749
1
5/12/2006 4:52 PM
Hexach loro benzene
BRL
1000
pg1L
70749
1
5112M06 4:52 PM
Hexachlorobutadiene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Hexachlorocyclopentadiene
BRL
1000
pg/L
70749
1
5/12/2006 4:52 PM
Hexadtloroethane
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Indeno(1,2,3-cd)pyrene
BRL
1000
pglL
70749
1
5/1212006 4:52 PM
Isophorone
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Naphthalene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Nitrobenzene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
N-Nitrosodi-n-propylamine
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
N-Nitrosodiphenyla mine
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Pentachlorophenol
BRL
2500
pglL
70749
1
5/12/2006 4:52 PM
Phenanthrene
BRL
1000
pglL
70749
1
5/12/2006 4:52 PM
Phenol
4200
1000
pg1L
70749
1
5/12/2006 4:52 PM
Pyrene
BRL
1000
pg1L
70749
1
5/12/2006 4:52 PM
Surr; 2,4,6-Tribromophenol
102
64.8-129
%REC
70749
1
5/12/2006 4:52 PM
Surr: 2-Fluorobiphenyl
96.5
58.2-115
%REC
70749
1
5/12/2006 4:52 PM
Surr: 2-Fluorophenol
69.6
24.4-115
%REC
70749
1
5/12/2006 4:52 PM
Surr: 4-Terphenyl-d14
81.7
58.3-115
%REC
70749
1
5/12/2006 4:52 PM
Surr. Nitrobenzene-d5
108
51.8-115
%REC
70749
1
5/12/2006 4:52 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis exceeded
Narr See Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 23 of 30

Analytical Environmental Services, Inc. Date: 16-May-06
CLIENT: Tetra Tech FM Inc.
Client Sample ID: FT-05
Project: Synthron, Inc
Collection Date: 5/10/2006
3:00:00 PM
Lab ID, 0605651-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua,
Limit
Units BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
78.3
17.9-115
%REC 70749
1
5/12/2006 4:52 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Tdchloroethane
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
1,1,2-Trichloroethane
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,1-Dichloroethane
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,1-Dichloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,2,4-Trichlorobenzene
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
1,2-Dibromoethane
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,2-Dichlorobenzene
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,2-Dichloroethane
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,2-Dichloropropane
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
1,3-Dichlorobenzene
BRL
5.0
pglL
70847
1
5/12/2006 3:49 PM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
2-Butanone
910
500
pg/L
70847
50
5/14/2006 1:54 PM
2-Hexanone
BRL
10
pg1L
70847
1
5/12/2006 3:49 PM
4-Methyl-2-pentanone
61
10
pg/L
70847
1
5/12/2006 3:49 PM
Acetone
24000
5000
pg/L
70847
100
5/12/2006 5:33 PM
Benzene
5.4
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Bromodichloromethane
BRL
5.0
pg/L
70847
1
5112/2006 3:49 PM
Bromoform
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Bromomethane
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Carbon disulfide
BRL
5.0
pglL
70847
1
5/12/2006 3:49 PM
Carbon tetrachloride
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Chlorobenzene
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
Chloroethane
BRL
10
pg1L
70847
1
5/12/2006 3:49 PM
Chloroform
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Chloromethane
BRL
10
pg1L
70847
1
5/12/2006 3:49 PM
cis-1,2-Dichloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
cis- 1,3-Dichloroprope ne
BRL
5.0
p91L
70847
1
5/12/2006 3:49 PM
Cyclohexane
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Dibromochloromethane
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Dichlorodifluoromethane
BRL
10
pg/L
70847
1
5/12/2006 3:49 PM
Ethylbenzene
44
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Freon-113
BRL
10
pg1L
70847
1
5/12/2006 3:49 PM
Isopropylbenzene
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
m,p-Xylene
160
10
pg1L
70847
1
5/12/2006 3:49 PM
Methyl acetate
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
Methyl tert-butyl ether
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
Methylcydohexane
BRL
5.0
pglL
70847
1
5/12/2006 3:49 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E-
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
11 Holding times for preparation or analysis
exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method Blank
Page 24 of 30

Analytical Environmental Services, Inc. Date: 16-A1av-06
CLIENT: Tetra Tech EM Inc. Client Sample ID: FT-05
Project: Synthron, Inc Collection Date: 5/10/2006 3:00:00 PM
Lab ID: 0605651-005 Matrix: SURFACE WATER
Analyses Result Reporting QUA Units BatchlD Dilution Date Analyzed
Limit Factor
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pglL
70847
1
5/12/2006 3:49 PM
o-Xylene
47
5.0
pg1L
70847
1
5/12/2006 3:49 PM
Styrene
BRL
5.0
NgIL
70847
1
5/12/2006 3:49 PM
Tetra chloroethene
BRL
5.0
pg/L
70847
1
5/12/2006 3:49 PM
Toluene
130
5.0
pg1L
70847
1
5/12/2006 3:49 PM
trans-1.2-Dichloroethene
BRL
5.0
pg11-
70847
1
5/12/2006 3:49 PM
trans-1.3-❑irhloropropene
BRL
5.0
pglL
70847
1
5/12/2006 3:49 PM
Trichloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
Trichlorofluoromethane
BRL
5.0
pg1L
70847
1
5/12/2006 3:49 PM
Vinyl Chloride
BRL
2.0
pg1L
70847
1
5/12/2006 3:49 PM
Surr: 4-Bromofluorobenzene
97.9
63.7-115
%REC
70847
1
5/12/2006 3:49 PM
Surr: 4-Bromofluorobenzene
96.6
63.7-115
%REC
70847
50
5/14/2006 1:54 PM
Surr: 4-Bromofluorobenzene
06.0
63.7-115
%REC
70847
100
5/12/2006 5:33 PM
Surr: Dibromofluoramethane
96.6
70A-123
%REC
70847
1
5/12/2006 3:49 PM
Surr: Dibromofluoramethane
92.6
70.4-123
%REC
70847
50
5/14/2006 1:54 PM
Surr: Dibromofluoramethane
93.6
70.4-123
%REC
70847
100
5/12/2006 5:33 PM
Surr. Toluene-d8
101
73.4-115
%REC
70847
1
5/12/2006 3:49 PM
Surr: Toluene-d8
100
73.4-115
%REC
70847
50
5/14/2006 1:54 PM
Surr: Toluene-d8
102
73.4-115
%REC
70a47
100
5/12/2006 5:33 PM
BIOCHEMICAL OXYGEN DEMAND (BOD)-
5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
2220
500
mg1L
70755
100
5/11/2006 3:00 PM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
7130
100
mg1L
70790
10
5/12/2006 10:45 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
IT Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
G Estimated (Value above quamitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Con Firmed
Page 25 of 30

Analytical Environmental Services, Inc.
Date: 16-May-06
CLIENT: Tetra Tech FM Inc.
Client
Sample ID: FT-06
Project: Synthron, Inc
Collection
Date: 5/10/2006
3:15:00
PM
Lab ID: 0605651-006
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW35108)
Analyst: MM
4,4'•DDD
BRL
0.10
pg1L
70734
1
6/12/2006 3:58 PM
4,4'-DDE
BRL
0.10
pg1L
70734
1
5/12/2006 3:58 PM
4,4'-DDT
BRL
0.10
pg/L
70734
1
5112=06 3:58 PM
Aldrin
BRL
0.050
pg/L
70734
1
5/12/2006 3:58 PM
alpha-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 3:58 PM
alpha -Chlordane
BRL
0,050
pg/L
70734
1
5/12/2006 3:58 PM
beta-BHC
BRL
0.050
pg1L
70734
1
5/1212006 3:58 PM
delta-BHC
BRL
0.050
pg1L
70734
1
5/12/2006 3:58 PM
Dieldrin
BRL
0.10
pg/L
70734
1
5/12/2006 3:58 PM
Endosultan I
BRL
0.050
pg/L
70734
1
5/12/2006 3:58 PM
Endosultan II
BRL
0.10
pg1L
70734
1
5/12/2006 3:58 PM
Endosultan sulfate
BRL
0.10
pglL
70734
1
5/12/2006 3:58 PM
Endrin
BRL
0.10
pglL
70734
1
5/12/2006 3:58 PM
Endrin aldehyde
BRL
0.10
pg1L
70734
1
5/12/2006 3:58 PM
Endrin ketone
BRL
0.10
pg1L
70734
1
5/12/2006 3:58 PM
gamma-BHC
BRL
0.050
pg/L
70734
1
5/12/2006 3:58 PM
gamma -Chlordane
BRL
0.050
pg/L
70734
1
5/12/2006 3:58 PM
Heptachlor
BRL
0.050
pg/L
70734
1
5/12/2006 3:58 PM
Heptachlor epoxide
BRL
0.050
pg/L
70734
1
5/12/2006 3:58 PM
Methoxychlor
BRL
0.50
pg/L
70734
1
5/1212006 3:58 PM
Toxaphene
BRL
5.0
pg/L
70734
1
5/12/2006 3:58 PM
Surr: Decachlorobiphenyl
34.6
17.9-122
%REC
70734
1
5/12/2006 3:58 PM
Surr: Tetrachloro-m-xytene
0
18.9-119 S
%REC 70734
1
5/12/2006 3:58 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Aluminum
9.33
0,200
mg1L
70703
1
5/11/2006 8:25 PM
Antimony
0.261
0.0200
mg/L
70708
1
5/11/2006 8:25 PM
Arsenic
0,113
0.0500
mg/L
70708
1
5/11/2006 8:25 PM
Barium
0.228
0.0200
mg/L
70708
1
5/11/2006 8:25 PM
Beryllium
BRL
0.0100
mg1L
70708
1
5/11/2006 8:25 PM
Cadmium
0.0130
0.0050
mg1L
70708
1
5/11/2006 8:25 PM
Calcium
100
1,00
mg1L
70708
10
5/12/2006 1:46 PM
Chromium
0.101
0.0100
mg/L
70708
1
5/11/2006 8:25 PM
Cobalt
0.0665
0.0200
mg/L
70708
1
5/11/2006 8:25 PM
Copper
0.535
0.0100
mg/L
70708
1
5/11/2006 8:25 PM
Iron
29.1
0,100
mg/L
70708
1
5111/2006 8:25 PM
Lead
0.501
0.0100
mg/L
70708
1
5/11/2006 8:25 PM
Magnesium
9.30
0.100
mg/L
70708
1
5/11/2006 8:25 PM
Manganese
4.64
0.0050
mg1L
70708
1
5111t2006 8:25 PM
Molybdenum
BRL
0.0500
mg1L
70708
1
5/11/2006 8:25 PM
Nickel
BRL
0.0200
mglL
70708
1
5/11/2006 8:25 PM
Potassium
26.0
0,500
mg1L
7070E
1
5/11/2006 8:25 PM
Qualifiers; • Value exceeds Maximum Contaminant Level
1?
Estimated (Value above quantitation range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
I f Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC cenif:ed
NC
Not Confirmed
B Analyte detected in the associated
Method Blank
Page 26 of- 30

Analytical Environmental Services, Inc. Date: 16-A4ay-06
CLIENT: Tetra Tech EM Inc.
Client SampleID: FT-06
Project: Synthron, Inc
Collection
Date: 5/10/2006
3:15:00 PM
Lab ID: 0605651-006
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua[
Limit
Units BatchlD Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: VA
Selenium
0.0383
0.0200
mg/L
70708
1
5/11/2006 8:25 PM
Silver
BRL
0.0100
mg1L
70708
1
5/11/2006 8:25 PM
Sodium
757
10.0
mg1L
70708
10
5/12/2006 1:46 PM
Thallium
BRL
0,0200
mg/L
70708
1
5/1112006 8:25 PM
Tin
0.506
0.0500
mg/L
70708
1
5/11/2006 8:25 PM
Titanium
0.244
0,0500
mg1L
70708
1
5/11/2006 8:25 PM
Vanadium
0.111
0.0100
mg1L
70708
1
5/11/2006 8:25 PM
Zinc
13A
0,0200
mg1L
70708
1
5/11/2006 8:25 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: AO
Mercury
0.00124
0.00020
mg1L
70854
1
5/15/2006 4:51 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
2,4,5-Trichlorophenol
BRL
2500
pg1L
70749
1
5/12/2006 5:19 PM
2,4,6-Trichlorophenol
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
2,4-Dichlorophenol
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
2,4-Dimethylphenol
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
2,4-Dinitrophenol
BRL
2500
pg/L
70749
1
5/12/2006 5:19 PM
2,4-Dinitrotoluene
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
2,6-Dinitrotoluene
BRL
1000
pg/L
70749
1
5112/2006 5:19 PM
2-Chloronaphthalene
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
2-Chlorophenol
BRL
1000
pg1L
70749
1
5/1212006 5:19 PM
2-Methylnaphthalene
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
2-Methylphenol
10000
1000
pg/L
70749
1
5/12/2006 5:19 PM
2-Nitroaniline
BRL
2500
pg/L
70749
1
5/12/2006 5:19 PM
2-Nitrophenol
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
3,3'-Dichlorobenzidine
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
3-Nitroaniline
BRL
2500
pg/L
70749
1
5/12/2006 5:19 PM
4,5-Dinitro-2-methyl phenol
BRL
2500
pglL
70749
1
5/12/2006 5:19 PM
4-Bromophenyl phenyl ether
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
4-Chtoro-3-methylphenol
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
4-Chloroaniline
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
4-Chlorophenyl phenyl ether
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
4-Methylphenol
3800
1000
pglL
70749
1
5/12/2006 5:19 PM
4-Nitroaniline
BRL
2500
pglL
70749
1
5/12/2006 5:19 PM
4-Nitrophenol
BRL
2500
pg1L
70749
1
5112/2006 5:19 PM
Acenaphthene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Acenaphthylene
BRL
1000
pg11-
70749
1
5/12/2006 5:19 PM
Acetophenone
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Anthracene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Atrazine
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
Qualifiers; • Value exceeds Maximum Contaminant
Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
tl Holding times for preparation
or analysis
exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated Method Blank
Page 27 of 30

Analytical Environmental Services, tnc. Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron, Inc
Lab ID: 0605651-006
Client Sample ID: FT-06
Collection Date: 5/10/2006 3:15:00 PM
Matrix: SURFACE WATER
Analyses
Result
Reporting
Qual Units
BatchlD
Dilution
Date Analyzed
Limit
Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
1000
pg/L
70749
1
5/12/2006 5:19 PM
Benzaldehyde
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Benzo(a)pyrene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Benzo(b)fluoranthene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Benzo(g,h,i)perylene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Benzo(k)fluoranthene
BRL
1000
pg1L
70749
1
5112WO6 5:19 PM
Bis(2-chloroethoxy)methane
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Bis(2-chloroethyl)ether
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Bis(2-chloroisopropyl)ether
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Bis(2-ethylhexyl)phthalate
1200
1000
pg1L
70749
1
5/12/2006 5:19 PM
Butyl benzyl phthalate
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Caprolactam
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Carbazole
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Chrysene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Dibenz(a,h)anthracene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Dibenzofuran
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Diethyl phthalate
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Dimethyl phthalate
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Di-n-butyl phthalate
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Di-n-octyl phthalate
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Fluoranthene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Fluorene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Hexachlorobenzene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Hexachlorobutadiene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Hexachlorocyclopentadiene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Hexachloroethane
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Indeno(1,2,3-cd)pyrene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Isophorone
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Naphthalene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Nitrobenzene
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
N-Nitrosodi-n-propylamine
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
N-Nitrosodiphenylamine
BRL
1000
pglL
70749
1
5/12/2006 5:19 PM
Pentachtorophenol
BRL
2500
pg1L
70749
1
5/12/2006 5:19 PM
Phenanthrene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Phenol
6800
1000
pg1L
70749
1
5/12/2006 5:19 PM
Pyrene
BRL
1000
pg1L
70749
1
5/12/2006 5:19 PM
Surr: 2,4,6-Tribromophenol
82.7
64.8-129
%REC
70749
1
5/12/2006 5:19 PM
Surr: 2-Fluorobiphenyi
75.8
58.2-115
%REC
70749
1
5/12/2006 5:19 PM
Surr: 2-Fluorophenot
59.6
24.4-115
%REC
70749
1
5/12/2006 5:19 PM
Surr: 4-Terphenyl-d14
61.3
58.3-115
%REC
70749
1
5/12/2006 5:19 PM
Sum NitrobenzeneA5
89.6
51.8-115
%REC
70749
1
5/12/2006 5:19 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NLLAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery Iitnits
Narr See Case Narrative
NC Not Confirmed
Page 28 of 30

Analytical Environmental Services, Inc. Date: 16-Mav-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-06
Project: Synthron, Inc.
Collection
Date: 5/10/2006
3:15:00 PM
Lab ID: 0605651-006
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr; Phenol-d5
76.0
17.9-115
%REC
70749
1
5/12/2006 5:19 PM
TCL VOLATILE ORGANICS
SW8260B
(SW50308)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70847
1
611212006 4:15 PM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70847
1
511212 006 4:15 PM
1,1,2-Trichloroethane
BRL
5.0
pg1L
70847
1
5112/2006 4:16 PM
1,1-Dichloroethane
BRL
5.0
pg/L
70847
1
5112/2006 4:15 PM
1,1-Dichloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
1,2,4-Tdchlorobenzene
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
1,2-Dibromoethane
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
1,2-Dichlorobenzene
BRL
5.0
pg1L
70847
1
511212006 4:15 PM
1,2-Dichloroethane
BRL
5.0
pg/L
70847
1
6/12/2006 4:15 PM
1,2-Dichloropropane
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70847
1
5112/2006 4:15 PM
1,4-Dichlorobenzene
BRL
5.0
p91L
70847
1
5112/2006 4:15 PM
2-Butanone
420
250
pg/L
70847
50
5/14/2006 2:21 PM
2-Hexanone
BRL
10
pg1L
70847
1
5/12/2006 4:15 PM
4-Methyl-2-pentanone
71
10
pg1L
70B47
1
5/12/2006 4:15 PM
Acetone
13000
5000
pg/L
70847
100
5/12/2006 4:41 PM
Benzene
10
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Bromodichloromethane
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Bromoform
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Bromomethane
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Carbon disulfide
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
Carbon tetrachloride
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Chlorobenzene
BRL
5.0
pq/L
70847
1
5/12/2006 4:15 PM
Chlofoethane
BRL
10
pg/L
70847
1
5/12/2006 4:15 PM
Chloroform
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Chloromethane
BRL
10
pg/L
70847
1
5/12/2006 4:15 PM
cis-1,2-Dichloroethene
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
cis- 1,3-Dichloropropene
BRL
5.0
pg/L
70847
1
5112/2006 4:15 PM
Cyclohexane
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
Dibromochloromethane
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Dichlorodifluoromethane
BRL
10
pg/L
70847
1
5/12/2006 4:16 PM
Ethylbenzene
72
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Freon-113
BRL
10
pg/L
70847
1
5/12/2006 4:15 PM
I sopropyl benzene
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
m,p-Xylene
250
10
pg/L
70847
1
5/12/2006 4:15 PM
Methyl acetate
380
250
pg/L
70847
50
5/14/2006 2:21 PM
Methyl tert-butyl ether
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Methylcydohexane
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
DELL Below Reporting Limit
S
Surrogate Recoveryoutside accepted
recovery limits
H Holding times for preparation
or analysis exceeded
Nair
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 29 of 30

Analytical Environmental Services, Inc.
Date: 16-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-06
Project: Synthron, Inc
Collection Date: 5/10/2006
3:15:00
PM
Lab ID: 0605651-006
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua] Units
Limit
BatchlD Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
o-Xylene
78
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Styrene
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
Tetrachloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
Toluene
360
250
pg1L
70847
50
5/14/2006 2:21 PM
trans-1,2-Dichloroethene
BRL
5.0
pg1L
70847
1
5/12/2006 4:15 PM
trans-1,3-Dichloropropene
BRL
5.0
pglL
70847
1
5112120064:15 PM
Trichloroethene
BRL
5.0
pg/L
70847
1
5112/20064:15 PM
Trichlorofluoromethane
BRL
5.0
pg/L
70847
1
5/12/2006 4:15 PM
Vinyl chloride
BRL
2.0
pg1L
70847
1
5/12/2006 4:15 PM
Surr: 4-Bromofluorobenzene
98.8
63.7-115
%REC
70B47
1
5/12/2006 4:15 PM
Surr: 4-Bromofluorobenzene
97.0
63.7-115
%REC
70B47
50
5/14/2006 2:21 PM
Surr. 4-Bromofluorobenzene
96.3
63.7-115
%REC
70847
100
5/12/2006 4:41 PM
Surr. Dibromofluoromethane
94.5
70.4-123
%REC
70847
1
5/12/2006 4:15 PM
Surr: Dibromofluoromethane
93.3
70.4-123
%REC
70847
100
5/12/2006 4:41 PM
Surr, Dibromofluoromethane
92.8
70.4-123
%REC
70847
50
5/14/2006 2:21 PM
Surr: Toluene-d8
99.7
73.4-115
%REC
70847
1
5/12/2006 4:15 PM
Surr. Toluene-d8
100
73.4-115
%REC
70847
50
5/14/2006 2:21 PM
Surr. Toluene-d8
100
73.4-115
%REC
70847
100
5/12/2006 4:41 PM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
3530
500
mg1L
70755
100
511112006 3:00 PM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
9590
100
mg/L
70790
10
5/12/2006 10:45 AM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or anal vsis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 30 of 30

Analytical Environmental Services, Inc. Date: 22-Alay-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-07
Project: Synthron Inc.
Collection Date: 5/1
1/2006 8:15:00
AM
Lab ID: 0605766-001
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua]
Limit
Units
BatchlD
Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
0.10
pg1L
70840
1
5/15/2006 9:26 PM
4,4'-DDE
BRL
0.10
pg/L
70840
1
5/15/2006 9:26 PM
4,4'-DDT
BRL
0.10
pg1L
70840
1
5/15/2006 9:26 PM
Aldrin
BRL
0,050
pg1L
70840
1
5/15/2006 9:26 PM
alpha-BHC
BRL
0.050
pg/L
70840
1
5/15/2006 9:26 PM
alpha -Chlordane
BRL
0.050
pg/L
70840
1
5/15/2006 9:26 PM
beta-BHC
BRL
0.050
pg/L
70840
1
5/15/2006 9:26 PM
delta-BHC
BRL
0.050
pg/L
70840
1
5/15/2006 9:26 PM
Dieldrin
BRL
0.10
pglL
70840
1
511W006 9:26 PM
Endosulfan I
BRL
0.050
pg/L
70840
1
5/15/2006 9:26 PM
Endosulfan II
BRL
0.10
pg/L
70840
1
5115=06 9:26 PM
Endosulfan sulfate
BRL
0.10
pg1L
70840
1
5/15/2006 9:26 PM
Endrin
BRL
0.10
pg/L
70840
1
5115=06 9:26 PM
Endrin aldehyde
BRL
0.10
pglL
70840
1
5/15/2006 9:26 PM
Endrin ketone
BRL
0.10
pg1L
70840
1
5/15/2006 9:26 PM
gamma-BHC
BRL
0,050
pg1L
70840
1
5/15/2006 9:26 PM
gamma -Chlordane
BRL
0.050
pg1L
70840
1
5/15/2006 9:26 PM
Heptachlor
BRL
0.050
pg1L
70840
1
5/15/2006 9:26 PM
Heptachlor epoxide
BRL
0.050
pg1L
70840
1
5/15/2006 9:26 PM
Methoxychlor
BRL
0.50
pg/L
70840
1
5/15/2006 9:26 PM
Toxaphene
BRL
5.0
pg1L
70840
1
5/15/2006 9:26 PM
Surr. Decachlorobiphenyl
21.1
17.9-122
%REC
70940
1
511WO06 9:26 PM
Surr. Tetrachloro-m-xylene
107
18.9-119
%REC
70840
1
5/15/2006 9:26 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
4,79
0.200
mg/L
70835
1
5/15/2006 5:02 PM
Antimony
0.0770
0.0200
mg/L
70835
1
5/15/2006 5:02 PM
Arsenic
BRL
0.0500
mg1L
70835
1
'511512006 5:02 PM
Barium
0.0405
0.0200
mg/L
70835
1
5/15/2006 5:02 PM
Beryllium
BRL
0.0100
mg1L
70835
1
5/15/2006 5:02 PM
Cadmium
BRL
0.0050
mg/L
70835
1
5/15/2006 5:02 PM
Calcium
18.7
0.100
mg/L
70835
1
5/15/2006 5:02 PM
Chromium
0.0254
0.0100
mg/L
70835
1
5/15/2006 5:02 PM
Cobalt
BRL
0.0200
mg/L
70835
1
5/15/2006 5:02 PM
Copper
0.0827
0.0100
mg/L
70835
1
5/15/2006 5:02 PM
Iron
8.53
0.100
mg1L
70835
1
5/15/2006 5:02 PM
Lead
0.0560
0.0100
mg/L
70835
1
5/15/2006 5:02 PM
Magnesium
3.08
0,100
mg1L
70835
1
5/15/2006 5:02 PM
Manganese
0.419
0.0050
mg1L
70835
1
5/15/2006 5:02 PM
Molybdenum
BRL
0.0500
mg1L
70835
1
5/15/2006 5:02 PM
Nickel
0.0367
0.0200
mg1L
70835
1
5/15/2006 5:02 PM
Potassium
7.27
0.500
mg1L
70835
1
5/15/2006 5:02 PM
Qualifiers: •
Value exceeds Maximum Contaminant Level
BRL
Below Reporting Limit
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page I of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc,
Lab ID: 0605766-001
Client Sample ID: FT-07
Collection Date: 5/1 1/2006 8:15:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Units
BatchlD
Dilution
Date Analyzed
Limit
Factor
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:02 PM
Silver
BRL
0.0100
mg1L
70835
1
511WO06 5:02 PM
Sodium
42.5
1.00
mg/L
70835
1
5/15/2006 5:02 PM
Thallium
BRL
0.0200
mg/L
70835
1
5/15/2006 5:02 PM
Tin
0.0896
0.0500
mg/L
70835
1
5/15/2006 5:02 PM
Titanium
0.253
0.0500
mg/L
70835
1
5/15/2006 5:02 PM
Vanadium
0.0448
0.0100
mg/L
70835
1
5/1512006 5:02 PM
Zinc
2.27
0.0200
mg/L
70835
1
5/1 W006 5:02 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0.00020
mg/L
70883
1
5/16/2006 2:30 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
2,4,5-Trichlorophenol
BRL
25
µg/L
70832
1
5/15/2006 7:06 PM
2,4,6-Trichlorophenol
BRL
10
pg/L
70832
1
5/15/2006 7:08 PM
2,4-Dichlorophenol
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2,4-Dimethylphenol
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2,4-Dinitrophenol
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
2,4-Dinitrotoluene
BRL
10
pg/L
70832
1
5/15/2006 7:05 PM
2,6-Dinitrotoluene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
2-Chloronaphthalene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
2-Chlorophenol
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
2-Methylnaphlhalene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
2-Methylphenol
BRL
10
pg/L
70832
1
5/1512006 7:06 PM
2-Nitroaniline
BRL
25
pg1L
70832
1
5/1512006 7:06 PM
2-Nitrophenol
BRL
10
pg1L
70832
1
5/16/2006 7:06 PM
3,3'-Dichlorobenzidine
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
3-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 7:06 PM
4,6-Dinitro-2-methylphenol
BRL
25
pg1L
70832
1
5/15/2006 7:06 PM
4-Bromophenyl phenyl ether
BRL
10
p91L
70832
1
5/15/2006 7:06 PM
4-Chloro-3-methylphenol
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
4-Chloroaniline
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
4-Chlorophenyl phenyl ether
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
4-Methylphenol
66
10
pg/L
70832
1
5/15/2006 7:06 PM
4-Nitroaniline
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
4-Nitrophenol
BRL
25
pg1L
70832
1
5/15/2006 7:06 PM
Acenaphthene
BRL
10
VOL
70832
1
5/15/2006 7:06 PM
Acenaphthylene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Acetophenone
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Anthracene
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Atrazine
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quandtation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 2 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-001
Client Sample ID: FT-07
Collection Date: 5/11/2006 8:15:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting
Qual Units
BatchlD
Dilution
Date Analyzed
Limit
Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3590)
Analyst: DA
Benz(a)anthracene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Benzaldehyde
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Benzo(a)pyrene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Benzo(b)fluoranthene
BRL
10
pg1L
70832
1
5/15/2006 T06 PM
Benzo(g,h,i)perylene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Senzo(k)tluoranthene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Bis(2-chloroethoxy)methane
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Bis(2-chloroethyl)ether
BRL
10
UgIL
70832
1
5/15/2006 7:06 PM
Bis(2-chloroisopropyl)ether
BRL
10
pgfL
70832
1
5115=06 7:06 PM
Bis(2-ethylhexy1)phthalate
22
10
pg/L
70832
1
5/15/2006 7:06 PM
Butyl benzyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Caprolactam
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Carbazole
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Chrysene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Dibenz(a,h)anthracene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Dibenzofuran
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Diethyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Dimethyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Di-n-butyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Di-n-octyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Fluoranthene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Fluorene
BRL
10
pglL
70832
1
5/15/2006 7:06 PM
Hexachlorobenzene
BRL
10
UgIL
70832
1
5/15/2006 7:06 PM
Hexachlorobutadiene
BRL
10
NgIL
70832
1
5/15120067.06PM
Hexachlorocydopentadiene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Hexachloroethane
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Indeno(1,2,3-cd)pyrene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Isophorone
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Naphthalene
BRL
10
yg/L
70832
1
5/15/2006 7:06 PM
Nitrobenzene
BRL
10
yg/L
70832
1
5/15/2006 7:06 PM
N-Nitrosodi-n-propylamine
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
N-Nitro sod iphenylamine
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Pentachlorophenol
BRL
25
pg/L
70832
1
5/15/2006 7:06 PM
Phenanthrene
BRL
10
pg/L
70832
1
5/15/2006 7:06 PM
Phenol
36
10
pg/L
70832
1
5/15/2006 7:06 PM
Pyrene
BRL
10
pg1L
70832
1
5/15/2006 7:06 PM
Surr: 2,4,6-Tribromophenol
68.8
64.8-129
%REC
70832
1
5/15/2006 7:06 PM
Surr: 2-Fluarobiphenyl
68.8
58.2-115
%REC
70832
1
5115/2006 7:06 PM
Surr: 2-Fluorophenal
56.6
24A-115
%REC
70832
1
5/15/2006 7:06 PM
Surr: 4-Terphenyl-d14
60.1
58.3-115
%REC
70832
1
5/15/2006 7:06 PM
Surr: Nitrobenzene-d5
64.2
51.8-115
%REC
70832
1
5/15/2006 7:06 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
G Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 3 of 30

Analytical Environmental Services, Inc. Date: 22-Nfav-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron [ne.
Lab ID: 0605766-001
Client Sample ID: FT-07
Collection Date: 5/1 1/2006 8:15:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual.
Units
BatchlD
Dilution
Date Analyzed
Limit
Factor
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst DA
Surr: Phenol-d5
53.4
17.9-115
%REC
70832
1
5/15/2006 7:06 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70849
1
511312006 7:28 AM
1,1,2,2-Teirachloroethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
1.1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,1-Dichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,2,4-Trichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,2-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,2-Dichloroethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
1,2-Dichloropropane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
2-Butanone
BRL
50
pg/L
70849
1
5/13/2006 7:28 AM
2-Hexanone
BRL
10
pg/L
70849
1
5/13/2006 7:28 AM
4-Methyt-2-pentanone
BRL
10
pg1L
70849
1
5/13/2006 7:28 AM
Acetone
110
50
pg/L
70849
1
5/13/2006 7:28 AM
Benzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Bromodichloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Bromoform
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Bromomethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Carbon disulfide
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Carbon tetrachloride
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Chlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Chloroethane
BRL
10
pg1L
70849
1
5/13/2006 7:28 AM
Chloroform
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Chloromethene
BRL
10
pg/L
70849
1
5/13/2006 7:28 AM
cis- 1,2-Dichlo roethene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
cis-1,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Cyclohexane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Dibromochloromethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Dichlorodifluoromethane
BRL
10
pglL
70849
1
5/13/2006 7:28 AM
Ethylbenzene
BRL
5.0
pglL
70849
1
5/13/2006 7:28 AM
Freon-113
BRL
10
pg1L
70849
1
5/13/2006 7:28 AM
Isop ropyl benzene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
m,p-Xytene
BRL
10
pg1L
70849
1
5/13/2006 7:28 AM
Methyl acetate
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Methyl tert-butyl ether
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Methylcydohexane
BRL
5.0
pg/L
70849
1
5/13/2006 7:28 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H ]-folding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Biank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 4 of 30

Analytical Environmental Services, Inc.
Date: 22-Mav-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-07
Project: Synthron Inc.
Collection Date: 5/1
1/2006 8:15:00
AM
Lab ID: 0605766-001
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua]
Limit
Units
BatchlD
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg1L
70849
1
5113/2006 7:28 AM
o-Xylene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Styrene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Tetrachloroethene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Toluene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
trans-1 ,2-Dichloroethene
BRL
5.0
pg1L
70849
1
5/13/2006 7:26 AM
trans- l ,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Trichloroethene
BRL
5.0
pg1L
70849
1
5/13/2006 7:28 AM
Trichlorofluoromethane
BRL
5.0
pglL
70849
1
5/13/2006 7:28 AM
Vinyl chloride
BRL
2.0
pg1L
70849
1
5/13/2006 7:28 AM
Surr: 4-13romofluorobenzene
97.5
63.7-115
%REC
70849
1
5/13/2006 7:28 AM
Surr: Dibromofluoromethane
94,2
70.4-123
%REC
70849
1
5/13/2006 7:28 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849
1
5/13/2006 7:28 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
61.4
50.0
mg1L
70797
10
5/12/2006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
604
10
mglL
70814
1
5/12/2006 3:45 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certificd
B . Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC NotConftrmed
Page 5 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech PM inc_
Client Sample ID: FT-08
Project: Synthran Inc.
Collection
Date: 5/11/2006
8:35:00
AM
Lab ID: 0605766-002
Matrix: SURFACE
WATER
Analyses
Result
Reporting Qua[
Limit
Units SatchID Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
1.0
pg/L
70840
1
5/15/2006 10:02 PM
4,4'-DDE
BRL
1.0
pg/L
70840
1
5/15/2006 10:02 PM
4,4'-DDT
BRL
1.0
pg1L
70840
1
5/15/2006 10:02 PM
Aldrin
BRL
0.50
pg/L
70840
1
5/15/2006 10:02 PM
alpha-BHC
BRL
0.50
pg/L
70840
1
5/15/2006 10:02 PM
alpha -Chlordane
BRL
0.50
pg1L
70840
1
5/15/2006 10:02 PM
beta-BHC
BRL
0.50
pglL
70840
1
5/15/2006 10:02 PM
delta-BHC
BRL
0.50
pg1L
70840
1
5/15/2006 10:02 PM
Dieldrin
BRL
1.0
pg1L
70840
1
5/15/2006 10:02 PM
Endosulfan I
BRL
0.50
pg1L
70840
1
5/15/2006 10:02 PM
Endosulfan 11
BRL
1.0
pg1L
70840
1
5/15/2006 10:02 PM
Endosulfan sulfate
BRL
1.0
pg/L
70840
1
5/15/2006 10:02 PM
Endrin
BRL
1.0
pg/L
70840
1
5/15/2006 10:02 PM
Endrin aldehyde
BRL
1.0
pg1L
70840
1
5/15/2006 10:02 PM
Endrin ketone
BRL
1.0
pglL
70840
1
5/15/2006 10:02 PM
gamma-BHC
BRL
0.50
pg/L
70840
1
5/15/2006 10:02 PM
gamma -Chlordane
BRL
0.50
pg/L
70840
1
5/15/2006 10:02 PM
Heptachlor
BRL
0.50
pg/L
70840
1
5/15/2006 10:02 PM
Heptachlor epoxide
BRL
0.50
pg/L
70840
1
5/15/2006 10:02 PM
Methoxychlor
BRL
5.0
pg/L
70840
1
5/15/2006 10:02 PM
Toxaphene
BRL
50
pg1L
70840
1
6/15/2006 10:02 PM
Sum Decachlorobiphenyl
22.3
17.9-122
%REC 70840
1
5/15/2006 10:02 PM
Surr: Tetrachloro-m-xyleno
84.2
18.9-119
%REC 70840
1
5/15/2006 10:02 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BS
Aluminum
4.47
0.200
mg/L
70835
1
5/15/2006 5:08 PM
Antimony
0.0400
0.0200
mg/L
70835
1
5/15/2006 5:08 PM
Arsenic
BRL
0.0500
mg/L
70835
1
5/15/2006 5:08 PM
Barium
0.0411
0,0200
mglL
70835
1
5/15/2006 5:08 PM
Beryllium
BRL
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Cadmium
BRL
0.0050
mg/L
70835
1
5/15/2006 5:08 PM
Calcium
22.2
0.100
mg/L
70835
1
5/15/2006 5:08 PM
Chromium
0.0316
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Cobalt
0.0318
0.0200
mg/L
70835
1
5/15/2006 5:08 PM
Copper
0.0818
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Iron
27.1
0.100
mg/L
70835
1
5/15/2006 5:08 PM
Lead
U816
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Magnesium
2.83
0.100
mg/L
70835
1
5/1512006 5:08 PM
Manganese
0.951
0.0050
mg/L
70835
1
5/15/2006 5:08 PM
Molybdenum
BRL
0.0500
mg/L
70835
1
5/15/2006 5:08 PM
Nickel
0.0631
0.0200
mg/L
70835
1
5/15/2006 5:08 PM
Potassium
8.61
0.500
mg/L
70835
1
5/15/2006 5:08 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation range)
BRL Below Reponing Limit
S
Surrogate Recovery outside accepted recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 6 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-08
Project: Synthron Inc.
Collection
Date: 5/1
1/2006 8:35:00 AM
Lab ID: 0605766-002
Matrix: SURFACE WATER
Analyses
Result
Reporting Quzl
Limit
Units BatchlD Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg1L
70835
1
5/15/2006 5:08 PM
Silver
BRL
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Sodium
63.8
1.00
mg/L
70835
1
5/15/2006 5:08 PM
Thallium
BRL
0.0200
mg/L
70835
1
5/15/2006 5:08 PM
Tin
0.0688
0.0500
mg/L
70835
1
5/15/2006 5:08 PM
Titanium
0.154
0.0500
mglL
70835
1
5/15/2006 5:08 PM
Vanadium
0.0460
0.0100
mg/L
70835
1
5/15/2006 5:08 PM
Zinc
2,30
0,0200
mg1L
70835
1
5/15/2006 5:08 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0.00020
mg1L
70883
1
5/16/2006 2:32 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
2,4,5-Trichlorophenol
BRL
250
pg/L
70832
1
5/15/2006 7:34 PM
2,4,6-Trichlorophenol
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
2,4-0ichforophenol
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
2,4-Dimethylphenol
BRL
100
pglL
70832
1
5/15/2006 7:34 PM
2A-Dinitrophenol
BRL
250
pglL
70832
1
5/15/2006 7:34 PM
2,4-Dinitrotoluene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
2,6-Dinitrotoluene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
2-Chloronaphthalene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
2-Chlorophenol
BRL
100
p911-
70832
1
5/15/2006 7:34 PM
2-Methylnaphthalene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
2-Methylphenol
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
2-Nitroaniline
BRL
250
pg1L
70832
1
5/15/2006 7:34 PM
2-Nitrophenol
BRL
100
pg/L
70832
1
5/15/2006 T.34 PM
3,3--Dichlorobenzidine
BRL
100
p911-
70832
1
5/15/2006 7:34 PM
3-Nitroaniline
BRL
250
pg/L
70832
1
5/15/2006 7:34 PM
4,6-Dinitro-2-methylphenol
BRL
250
pg/L
70832
1
5/15/2006 7:34 PM
4-Bromophenyl phenyl ether
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
4-Chloro-3-methylphenol
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
4-Chloroaniline
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
4-Chlorophenyl phenyl ether
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
4-Methylphenol
BRL
100
pg/L
70832
1
5/1512006 7:34 PM
4-Nitroaniline
BRL
250
pg/L
70832
1
5/15/2006 7:34 PM
4-Nitrophenol
BRL
250
pg1L
70832
1
5/15/2006 7:34 PM
Acenaphthene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Acenaphthylene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Acetophenone
BRL
100
ug1L
70832
1
5/15/2006 7:34 PM
Anthracene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Atrazine
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantization
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method Blank
Page 7 of 30

Analytical Environmental Services, Inc. Date: 22-Mav-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-08
Project: Synthron Inc.
Collection Date: 5/1
1/2006 8:35:00 AM
Lab ID: 0605766-002
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Benzaldehyde
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Benzo(a)pyrene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Benzo(b)fluoranthene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Benzo(g,hJ)perylene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Benzo(k)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Bis(2-chloroethoxy)methane
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Bis(2-chloroethyl)ether
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Bis(2-chloroisopropyl)ether
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
6is(2-ethylhexyl)phthalate
100
100
pg/L
70832
1
5/15/2006 7:34 PM
Butyl benzyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Caprolactam
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Carbazole
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Chrysene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Dibenz(a,h)anthracene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Dibenzotwan
BRL
100
pg1L
70832
1
5/15/2006 T34 PM
Diethyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Dimethyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Di-n-butyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Di-n-octyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Fluoranthene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Fluorene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Hexachlorobenzene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Hexachlorobutadiene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Hexachlorocydopentadiene
BRL
100
pg/L
70832
1
5/15=06 7:34 PM
Hexachloroethane
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Indeno(1,2,3-cd)pyrene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
Isophorone
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Naphthalene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Nitrobenzene
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
N-Nitrosodi-n-propylamine
BRL
100
pg1L
70832
1
5/15/2006 7:34 PM
N-Nitrosodiphenylamine
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Pentachlorophenol
BRL
250
pg/L
70832
1
5/15/2006 7:34 PM
Phenanthrene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Phenol
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Pyrene
BRL
100
pg/L
70832
1
5/15/2006 7:34 PM
Surr: 2,4,6-Tribromophenol
92.8
64.8-129
%REC
70832
1
5/15/2006 7:34 PM
Surr: 2-Fluorobiphenyl
87.4
58.2-115
%REC
70832
1
5/15/2006 7:34 PM
Surr: 2-Fluorophenol
73.7
24.4-115
%REC
70832
1
5/15/2006 7:34 PM
Surr. 4-Terphenyl-d14
73.5
58.3-115
%REC
70832
1
5/15/2006 7:34 PM
Surr. Nitrobenzene-d5
91 A
51.8-115
%REC
70832
1
5/15/2006 7:34 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
E Estimated (Value above quantization range)
BRL Below Reporting Limit
S Surrogate Recovery outside accepted recovery limits
H Holding limes for preparation or analysis exceeded
Narr See Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
B Analyte detected in the associated
Method Blank
Page 8 of 30

Analytical Environmental Services, Inc. Date: 22-Alay-06
CLIENT- Tetra Tech EM Inc.
Client Sample ID: FT-08
Project: Synthron Inc.
Collection
Date: 5/1
112006 8:35:00
AM
Lab ID: 0605766-002
Matrix: SURFACE
WATER
Analyses
Result
Reporting Qua[
Limit
Units BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
74.0
17.9-115
%REC 70832
1
5/15/2006 7:34 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70849
1
5113/20067:54AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
1,1-Dichloroethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
1,1-Dichloroethene
BRL
5.0
pg1L
70849
1
5113/2006 7:54 AM
1,2,4-Tdchlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
1,2-Dibromoothane
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
1,2-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5113/2006 7:54 AM
1,2-Dichloroethane
BRL
5.0
pglL
70849
1
5I13/2006 7:54 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
1.3-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
2-Butanone
BRL
50
pg/L
70849
1
5/13/2006 T54 AM
2-Hexanone
BRL
10
pg1L
70849
1
5/13/2006 T54 AM
4-Methyl-2-pentanone
BRL
10
pg/L
70849
1
5/13/2006 7:54 AM
Acetone
120
50
pg/L
70849
1
5/13/2006 7:54 AM
Benzene
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Bromodichloromethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Bromoform
BRL
5.0
pg1L
70849
1
5/1W006 7:54 AM
Bromomethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Carbon disulfide
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Carbon tetrachloride
BRL
5.0
pglL
70849
1
5/13/2006 7:54 AM
Chlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Chloroethane
BRL
10
pg/L
70849
1
5/13/2006 7:54 AM
Chloroform
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Chloromethane
BRL
10
pg1L
70849
1
5/13/2006 7:54 AM
cis- 1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
cis-1,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Cyclohexane
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
Dibromochloromethane
BRL
5.0
pg1L
70849
1
5/13/2006 7:54 AM
Dichlorodifluoromethane
BRL
10
pg/L
70849
1
5/13/2006 7:54 AM
Ethylbenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
Freon-113
BRL
10
pg/L
70849
1
5/13/2006 7:54 AM
[so propylbenzene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
m,p-Xylene
14
10
pglL
70849
1
5/13/2006 7:54 AM
Methyl acetate
9.8
5.0
pg/L
70849
1
5/13/2006 7:54 AM
Methyl tert-butyl ether
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
Methylcydohexane
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
Qualifiers: ; Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantization
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
I I Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analvte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated Method
Blank
Page 9 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc. Client Sample ID: FT-08
Project: Synthron Inc. Collection Date: 5/1 1/2006 8:35:00 AM
Lab ID: 0605766-002 Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchID
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg/L
70849
1
5/13/2006 T54 AM
o-Xylene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
Styrene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
Tetrachloroethene
BRL
5.0
NgIL
70849
1
5/13/2006 7:54 AM
Toluene
11
5.0
NgIL
70849
1
5/13/2006 7:54 AM
trans-1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 7:54 AM
trans-1,3-Dichloropropene
BRL
5.0
Vg/L
70849
1
5/13/2006 7:54 AM
Trichloroethene
BRL
5.0
ttg/L
70849
1
5/13/2006 7:54 AM
Trichlorofluoromethane
BRL
5.0
lrg1L
70849
1
5/13/2006 7:54 AM
Vinyl chloride
BRL
2.0
{tg/L
70849
1
5/13/2006 7:54 AM
Surr: 4-Bromoiluorobenzene
999.0
63.7-115
%REC
70849
1
5/13/2006 7:54 AM
Sum Dibromofluoromethane
94.4
70.4-123
%REC
70849
1
5/13/2006 7:54 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849
1
5/13/2006 7:54 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)-5 DAY E405.1 (E405.1)
Biochemical Oxygen Demand 113 50.0 mg1L 70797
CHEMICAL OXYGEN DEMAND (COD) E410.4 (E410.4)
Chemical Oxygen Demand 774 10 mg/L 70814
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyle not NELAC certified
B Analyte detected in the associated Method Blank
Analyst: CAM
10 5/12/2006 10:50 AM
Analyst: EK
1 5/12/2006 3:45 PM
L- Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 10 of 30

Analytical Environmental Services, Inc.
Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-09
Project: Synthron Inc.
Collection Date: 511
1/2006 8:55:00
AM
Lab ID: 0605766-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua[
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
0.10
pg/L
70840
1
5/15=06 10:14 PM
4,4'-DDE
BRL
0.10
VOL
70840
1
5/15/2006 10:14 PM
4,4'-DDT
BRL
0.10
pg/L
70840
1
5/15/2006 10:14 PM
Aldrin
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
alpha-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
alpha -Chlordane
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
beta-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
delta-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 10:14 PM
Dieldrin
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
Endosulfan I
BRL
0.050
pg/L
70840
1
5/15/2006 10:14 PM
Endosulfan II
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
Endosulfan sulfate
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
Endrin
BRL
0.10
pg1L
70840
1
5/15/2006 10:14 PM
Endrin aldehyde
BRL
0.10
pg/L
70840
1
5/15/2006 10:14 PM
Endrin ketone
BRL
0,10
pg/L
70840
1
5/15/2006 10:14 PM
gamma-BHC
BRL
0.050
pg/L
70840
1
5/15/2006 10:14 PM
gamma -Chlordane
BRL
0.050
pg/L
70840
1
5/15/2006 10:14 PM
Heptachlor
0.69
0.050
pg/L
70840
1
5/15/2006 10:14 PM
Heptachlor epoxide
BRL
0.050
pg/L
70840
1
5/15/2006 10:14 PM
Methoxychlor
BRL
0.50
pg/L
70840
1
5/15/2006 10:14 PM
Toxaphene
BRL
5.0
pg/L
70840
1
5/15/2006 10:14 PM
Surr: Decachlorobbphenyl
38.2
17.9-122
%REC
70840
1
5/15/2006 10:14 PM
Surr: Tetrachloro-m-xylene
172
18.9-119 S
%REC
70840
1
5/15/2006 10:14 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
22.3
0.200
mg/L
70835
1
5/15/2006 5:13 PM
Antimony
0.211
0.0200
mg1L
70835
1
5/15/2006 5:13 PM
Arsenic
BRL
0.0500
mg1L
70835
1
5/15/2006 5:13 PM
Barium
0.214
0.0200
mg/L
70835
1
5/15/2006 5:13 PM
Beryllium
BRL
0.0100
mg1L
70835
1
5/15/2006 5:13 PM
Cadmium
BRL
0.0050
mg/L
70835
1
5/15/2006 5:13 PM
Calcium
27.0
0.100
mg/L
70835
1
5/15/2006 5:13 PM
Chromium
0.0815
0.0100
mg/L
70835
1
5/15/2006 5:13 PM
Cobalt
0.0359
0.0200
mg1L
70835
1
5/15/2006 5:13 PM
Copper
0.258
0.0100
mg1L
70835
1
5115/2006 5:13 PM
Iron
34A
0.100
mg1L
70835
1
5/15/2006 5:13 PM
Lead
0.133
0.0100
mg/L
70835
1
5/15/2006 5:13 PM
Magnesium
8,33
0.100
mg/L
70835
1
5/15/2006 5:13 PM
Manganese
1.08
0,0050
mg/L
70835
1
5/15/2006 5:13 PM
Molybdenum
BRL
0.0500
mg/L
70835
1
5/15/2006 5:13 PM
Nickel
0.0740
0,0200
mg/L
70835
1
5/1512006 5:13 PM
Potassium
11.6
0.500
mg/L
70835
1
5/15/2006 5:13 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
F Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 1 I of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-09
Project: Synthron Inc.
Collection
Date: 5/11/2006
8:55:00 AM
Lab ID: 0605766-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units BatchlD
Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
13RL
0.0200
mg/L
70835
1
5/15/2006 5:13 PM
Silver
BRL
0,0100
mglL
70835
1
5/15/2006 5:13 PM
Sodium
60A
1.00
mg1L
70835
1
5/15/2006 5:13 PM
Thallium
BRL
0.0200
mglL
70835
1
5/15/2006 5:13 PM
Tin
0,430
0.0500
mg1L
70835
1
5/15/2006 5:13 PM
Titanium
1.12
0.0500
mg/L
70835
1
5/15/2006 5:13 PM
Vanadium
0,117
0.0100
mg/L
70835
1
5/15/2006 5:13 PM
Zinc
4.34
0.0200
mg1L
70835
1
5/15/2006 5:13 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
0.00038
0.00020
m9/L
70883
1
5/16/2006 2:34 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
2,4,5-Trichlorophenol
BRL
25
pg1L
70832
1
5/15/2006 8:00 PM
2,4,6-Trichlorophenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2,4-Dichlorophonol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2,4-Dimethylphenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2,4-Dinitrophenol
BRL
25
pg1L
70832
1
5/15/2006 8:00 PM
2,4-Dinitrotoluene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2,6-Dinitrotoluene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Chloronaphthalene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Chlorophenol
BRL
10
p911-
70832
1
5/15/2006 8:00 PM
2-Methylnaphthalene
BRL
10
pg/L
70832
1
5/15/2006 6:00 PM
2-Methylphenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
2-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 8:00 PM
2-Nitrophenol
BRL.
10
pg1L
70832
1
5/15/2006 8:00 PM
3,3'-Dichlorobenzidine
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
3-Nitroaniline
BRL
25
pg/L
70832
1
5/15/2006 8:00 PM
4,6-Dinitro-2-methylphenol
BRL
25
pg/L
70832
1
5/15/2006 6:00 PM
4-Bromophenyl phenyl ether
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
4-Chloro-3-methylphenol
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
4-Chloroaniline
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
4-Chlorophenyl phenyl ether
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
4-Methylphenol
21
10
pg/L
70832
1
5/15/2006 8:00 PM
4-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 8:00 PM
4-Nitrophenol
BRL
25
pg1L
70832
1
5/15/2006 8:00 PM
Acenaphthene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Acenaphthylene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Acetophenone
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Anthracene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Atrazine
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Fstimated (Value above civantitation
range)
BRl. Below Reporting Limit
S
Surrogate Recovery
outside accepted
recovery limits
H Holding times for preparation
or analysis
exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated Method l;lank
Page 12 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-09
Project: Synthron Inc.
Collection Date: 5/1
1/2006 8:55:00
AM
Lab ID: 0605766-003
Matrix: SURFACE WATER
Reporting
Dilution
Analyses
Result
Limit
Qual
Units
Bat.h1D
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz (a)anthracene
BRL
10
1tg/L
70832
1
5/15/2006 8:00 PM
Benzaldehyde
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Benzo(a)pyrene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Benzo(b)tluoranthene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Benzo(g,h,t)perylene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Bertzo(k)fluoranthene ,
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Bis(2-chloroethoxy)methane
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Bis(2-chloroethyl)ether
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Bis(2-chloroisopropyl)ether
BRL
10
pg/L
70832
1
6/15/2006 &00 PM
Bis(2-ethylhexyl)phthalate
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Butyl benzyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Caprolactam
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Carbazole
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Chrysene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Dibenz(a,h)anthracene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Dibenzofuran
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Diethyl phthalate
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Dimethyl phthatate
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Di-n-butyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Di-n-octyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Fluoranthene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Fluorene
BRL
10
pg1L
70832
1
5/15/2006 8:00 PM
Hexachiorobenzene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Hexachlorobutadiene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Hexachlorocyclopentadiene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Hexachloroethane
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Ind eno(1,2,3-cd)pyrene
BRL
10
pg1L
70832
1
511512006 8:00 PM
Isophorone
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Naphthalene
BRL
10
pglL
70832
1
5/15/2006 8:00 PM
Nitrobenzene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
N-Nitrosodi-n-propylamine
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
N-Nitrosodiphenylamine
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Pentachlorophenol
BRL
25
pg/L
70832
1
5/15/2006 8:00 PM
Phenanthrene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Phenol
20
10
pg/L
70832
1
5/15/2006 8:00 PM
Pyrene
BRL
10
pg/L
70832
1
5/15/2006 8:00 PM
Surr: 2,4,6-Tribromophenol
35.1
64.8-129
S
%REC
70832
1
5/15/2006 8:00 PM
Surr: 2-Fluorobiphenyl
37.0
58.2-115
S
%REC
70832
1
5M512006 8:00 PM
Surr: 2-Fluorophenol
27.9
24.4-115
%REC
70832
1
5/15/2006 8:00 PM
Surr: 4-Terphenyl-dl4
33.7
58.3-115
S
%REC
70832
1
5/15/2006 8:00 PM
Surr: Nitrobenzene-d5
37.2
51.8-115
S
%REC
70832
1
5/15/2006 8:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E Estimated (Value above quantitation range)
BRL Below Reporting Limit
S Surrogate Recovery outside accepted recovery limits
H Holding times for preparation or analysis
exceeded
Narr See Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
B Analyte detected in the associated
Method Blank
Page 13 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-09
Project: Synthron Inc.
Collection
Date: 5/11/2006
8:55:00 AM
Lab ID: 0605766-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
26.2
17.9-115
%REC 70832
1
5/15/2006 &00 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1. 1, 1 -Trichloroethane
BRL
5.0
pg/L
70849
1
5/1312006 8:20 AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pglL
70849
1
5/13/2006 8:20 AM
1,1,2-Tdchloroethane
BRL
5.0
pglL
70849
1
5/13/2006 8:20 AM
1,1-Dichloroethane
BRL
5.0
pg/L
70849
1
5113/2006 8:20 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,2,4-Tdchlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,2-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,2-Dichloroethane
BRL
5.0
pq/L
70849
1
5/13/2006 8:20 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70649
1
6/13/2006 8:20 AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
2-Butanone
BRL
50
pg1L
70849
1
5/13/2006 8:20 AM
2-Hexanone
BRL
10
pg/L
70849
1
5/13/2006 8:20 AM
4-Methyl-2-pentanone
BRL
10
pg1L
70849
1
5/13/2006 8:20 AM
Acetone
140
So
pglL
70849
1
5/13/2006 8:20 AM
Benzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Bromodichloro methane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Bromoform
BRL
5.0
pglL
70849
1
5/13/2006 8:20 AM
Bromomethane
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
Carbon disulfide
12
5.0
pg1L
70849
1
5/13/2006 8:20 AM
Carbon tetrachloride
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
Chlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Chloroethane
BRL
10
pg/L
70849
1
5/13/2006 8:20 AM
Chloroform
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Chloromethane
BRL
10
pg/L
70849
1
5113/2006 8:20 AM
cis- 1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
cis- 1,3-Dichloropropene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Cyclohexane
BRL
5.0
pglL
70849
1
5/13/2006 8:20 AM
Dibromochtoromethane
BRL
5.0
pglL
70849
1
5/13/2006 8:20 AM
Dichlorodifluoromethane
BRL
10
pg/L
70849
1
5/13/2006 8:20 AM
Ethylbenzene
BRL
5.0
pglL
70849
1
5/13/2006 8:20 AM
Freon-113
BRL
10
pg/L
70849
1,
5/13/2006 8:20 AM
lsopropylbenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
m,p-Xylene
21
10
pg/L
70849
1
5/13/2006 8:20 AM
Methyl acetate
10
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Methyl tert-butyl ether
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Methyicydohexane
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NE -LAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 14 of 30

Analytical Environmental Services, Inc.
Date: 22-A9ay-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-09
Project: Synthron Inc.
Collection Date: 5/1
1/2006 8:55:00 AM
Lab ID: 0605766-003
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchlD
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
o-Xylene
5.6
5.0
pg/L
70a49
1
5/13/2006 8:20 AM
Styrene
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
Tetractdoroethene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Toluene
5.5
5.0
pg1L
70849
1
5/13/2006 8:20 AM
trans-1,2-Dichloroethene
BRL
5.0
lag/L
70849
1
5/13/2006 8:20 AM
trans- 1,3-Dichloropropene
BRL
5.0
pg/L
70849
1
5/13/2006 8:20 AM
Trichloroethene
BRL
5.0
pg1L
70849
1
5/1W006 820 AM
Trichlorofluoromethane
BRL
5.0
pg1L
70849
1
5/13/2006 8:20 AM
Vinyl chloride
BRL
2.0
pg1L
70849
1
5/13/2006 8:20 AM
Surr: 4-Bromofluorobenzene
96.7
63.7-115
%REC
70849
1
5/13/2006 8:20 AM
Surr: Dibromofluoromethane
96.4
70.4-123
%REC
70849
1
5/13/2006 8:20 AM
Surr. Toluene -dB
103
73.4-115
%REC
70849
1
5/13/2006 8:20 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
184
50.0
mg1L
70797
10
5/12/2006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
1350
10
mg1L
70814
1
5/12/2006 3:45 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
13 Analyte detected in the associated Method Blank
G Estimated (Value above quantization range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 15 of 30

Analytical Environmental Services, Inc. Date: 22-Alay-06
CLIENT: Tetra Tech EM Inc. Client Sample ID: FT-10
Project: Synthron Inc. Collection Date: 5/1 1/2006 9:15:00 AM
Lab ID: 0605766-004 Matrix: SURFACE WATER
Analyses
Result
Reporting Qua,
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET
COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
1.0
pglL
70840
1
5/15/2006 10:25 PM
4,4--DDE
BRL
1.0
pg/L
70840
1
5/15/2006 10:25 PM
4,4"-DDT
BRL
1.0
pg/L
70840
1
5/15/2006 10:25 PM
Aldrin
BRL
0.50
pg/L
70840
1
5/15/2006 10:25 PM
alpha-BHC
BRL
0.50
pg1L
70840
1
5115t2006 10:25 PM
alpha -Chlordane
BRL
0.50
pg/L
70840
1
5/15/2006 10:25 PM
beta-BHC
BRL
0.50
pg/L
70840
1
5/15/2006 10:25 PM
delta-BHC
BRL
0.50
pg1L
70840
1
5115/2006 10:25 PM
Dieldrin
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
Endosulfan I
BRL
0.50
pg/L
70840
1
5/15/2006 10:25 PM
Endosulfan II
BRL
1.0
pglL
70840
1
5/15/2006 10:25 PM
Endosulfan sulfate
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
Endrin
BRL
1.0
pg/L
70840
1
5/15/2006 10:25 PM
Endrin aldehyde
BRL
1.0
pg1L
70840
1
5/15/2006 10:25 PM
Endrin ketone
BRL
1.0
pg/L
70840
1
5/15/2006 10:25 PM
gamma-BHC
BRL
0.50
pglL
70840
1
5/15/2006 10:25 PM
gamma -Chlordane
BRL
0.50
pg/L
70840
1
5/15/2006 10:25 PM
Heptachlor
BRL
0.50
pg1L
70840
1
5/15/2006 10:25 PM
Heptachlor epoxide
BRL
0.50
pg/L
70840
1
5/15/2006 10:25 PM
Methoxychlor
BRL
5.0
VglL
70840
1
5/15/2006 10:25 PM
Toxaphene
BRL
50
pg/L
70840
1
5/15/2006 10:25 PM
Surr: Decachlorobiphenyl
33.0
17.9-122
%REC
70840
1
5/15/2006 10:25 PM
Surr: Tetrachloro-m-xylene
30.5
18.9-119
%REC
70840
1
5/15/2006 10:25 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
5.35
0.200
mglL
70835
1
5/15/2006 5:19 PM
Antimony
0.0857
0.0200
mg/L
70835
1
5/15/2006 5:19 PM
Arsenic
BRL
0.0500
mg/L
70835
1
5/15/2006 5:19 PM
Barium
0.0609
0.0200
mg/L
70835
1
5/15/2006 5:19 PM
Beryllium
BRL
0.0100
mg/L
70835
1
5/15/2006 5:19 PM
Cadmium
0.0062
0.0050
mg/L
70835
1
5/15/2006 5:19 PM
Calcium
37.5
0.100
mg/L
70835
1
5/15/2006 5:19 PM
Chromium
0.0470
0,0100
mg/L
70835
1
5/15/2006 5:19 PM
Cobalt
0.0243
0.0200
mg/L
70835
1
5/15/2006 5:19 PM
Copper
0.185
0.0100
mglL
70835
1
5/15/2006 5:19 PM
Iron
10.9
0.100
mg/L
70835
1
5/15/2006 5:19 PM
Lead
0.163
0.0100
mg/L
70835
1
5/15/2006 5:19 PM
Magnesium
5.75
0.100
mg/L
70835
1
5/15/2006 5:19 PM
Manganese
0.728
0.0050
mg1L
70835
1
5/15/2006 5:19 PM
Molybdenum
BRL
0.0500
mg/L
70835
1
5/15/2006 5:19 PM
Nickel
0,0636
0.0200
mg/L
70835
1
5/15/2006 5:19 PM
Potassium
15.5
0.500
mg/L
70835
1
5/15/2006 5:19 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Anal yte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 16 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-10
Project: Synthron Inc.
Collection Date: 5/11/2006
9:15:00
AM
Lab ID: 0605766-004
Matrix: SURFACE WATER
Analyses
Result
Reporting Qua,
Limit
Units BatcbID Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mgR
70835
1
5/15/2006 5:19 PM
Silver
BRL
0.0100
mg/L
70835
1
5/15/2006 5:19 PM
Sodium
97.1
1.00
mg/L
70835
1
5/15/2006 5:19 PM
Thallium
BRL
0.0200
mg/L
70835
1
5/1512006 5:19 PM
Tin
0.150
0.0500
mg/L
70835
1
5/15/2006 519 PM
Titanium
0.257
0.0500
mg/L
70835
1
5/15/2006 5:19 PM
Vanadium
0.0741
0.0100
mg/L
70835
1
5/15/2006 5:19 PM
Zinc
8.88
0.0200
mg/L
70835
1
5/15/2006 5:19 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0.00020
mg/L
70883
1
5/16/2006 2:36 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2,4,5-Trichlorophenol
BRL
250
pg1L
70832
1
5/15/2006 8:26 PM
2,4,6-Trichlorophenol
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
2,4-Dichlorophenol
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2,4-Dimethylphenol
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2,4-Dinitrophenol
BRL
250
pglL
70832
1
5/15/2006 8:26 PM
2,4-Dinitrotoluene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2,6-Dinitrotoluene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2-Chloronaphthalene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2-Chlorophenol
BRL
100
pg/L
70832
1
5/1 W006 8:26 PM
2-Methylnaphthalene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2-Methylphenol
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
2-Nitroaniline
BRL
250
pg/L
70832
1
5115M06 8:26 PM
2-Nitrophenol
BRL
100
pq/L
70832
1
5/15/2006 8:26 PM
3,3'-Dichlorobenzidine
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
3-Nitroaniline
BRL
250
pg/L
70832
1
5/15/2006 8:26 PM
4,6-Dinitro-2-methyl phenol
BRL
250
pg/L
70832
1
5/15/2006 8:26 PM
4-Bromophenyl phenyl ether
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
4-Chloro-3-methylphenol
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
4-Chloroaniline
BRL
100
pg1L
70832
1
5/15/2006 8:26 PM
4-Chlorophenyl phenyl ether
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
4-Methylphenol
140
100
pg/L
70832
1
5/15/2006 8:26 PM
4-Nitroaniline
BRL
250
pq/L
70832
1
5/15/2006 8:26 PM
4-Nitrophenol
BRL
250
pg/L
70832
1
5/15/2006 8:26 PM
Acenaphthene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Acenaphthylene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Acetophenone
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Anthracene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Atrazine
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 17 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-004
Client Sample ID: FT-10
Collection Date: 5/11/2006 9:15:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual knits
BatchlD
Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Benz(a)anthracene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Bertzaldehyde
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Benzo(a)pyrene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Benzo(b)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Benzo(g,h,i)perylene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Benzo(k)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Bis(2-chloroethoxy)methane
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Bis(2-chloroethyl)ether
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Bis(2-chloroisopropyl)ether
BRL
100
pglL
70832
1
5/15/2006 8:26 PM
Bis(2-ethylhexyl)phthalate
BRL
100
ug/L
70832
1
5/15/2006 8:26 PM
Butyl benzyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Caprolactam
BRL
100
pg/L
70832
1
5/15/2006 &26 PM
Carbazole
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Chrysene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Dibenz(a,h)anthracene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Dibenzofuran
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Diethyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Dimethyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Di-n-butyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Di-n-octyl phthalate
BRL
100
pg/L
70832
i
5/15/2006 8:26 PM
Fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Fluorene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Hexachlorobenzene
BRL
100
pg/L
70B32
1
5/15/2006 8:26 PM
Hexachlorobutadiene
BRL
100
pg/L
70832
1
5/15/2006 826 PM
Hexachlorocydopentadiene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Hexachloroethane
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Indeno(1,2,3-cd)pyrene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Isophorone
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Naphthalene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Nitrobenzene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
N-Nitrosodi-n-propylamine
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
N-Nitrosodiphenylam"tne
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Pentachlorophenol
BRL
250
pglL
70832
1
5/15/2006 8:26 PM
Phenanthrene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Phenol
260
100
pg/L
70832
1
5/15/2006 8:26 PM
Pyrene
BRL
100
pg/L
70832
1
5/15/2006 8:26 PM
Surr: 2,4,6-Tribromophenol
90.1
64.8-129
%REC
70832
1
5/15t2006 8:26 PM
Surr: 2-Fluorobiphenyl
89.8
58.2-115
%REC
70832
1
5/15/2006 8:26 PM
Surr: 2-Fluorophenol
76.5
24.4-115
%REG
70832
1
5/15/2006 8:26 PM
Surr: 4-Terphenyl-04
82.9
58.3-115
%REC
70832
1
5/15/2006 8:26 PM
Surr: Nitrobenzene-d5
116
51.8-115
S %REC
70832
1
5/15/2006 8:26 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 18 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
CIient Sample ID: FT-10
Project: Synthron Inc.
Collection
Date: 511
1/2006 9:15:00 AM
Lab ID: 0605766-004
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
77.6
17.9-115
%REC 70832
1
5/1512006 8:26 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45AM
1,1-Dichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45AM
1,1-Dichloroethene
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
1,2,4-Trichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:45AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg1L
70849
1
5/13/2006 8:45AM
1,2-Dibromoethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
1,2-Dichlorobenzene
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
1,2-Dichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
2-Butanone
BRL
50
pg1L
70849
1
5/13/2006 8:45 AM
2-Hexanone
BRL
10
pg/L
70849
1
5/13/2006 8:45 AM
4-Methyl-2-pentanone
BRL
10
pg1L
70849
1
5/13/2006 8:45 AM
Acetone
620
500
pg1L
70849
50
5/13/2006 2:42 AM
Benzene
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Bromodichloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Bromoform
BRL
5.0
pg/L
70849
1
5/13/2006 8:46 AM
Bromomethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Carbon disulfide
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Carbon tetrachloride
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Chlorobenzene
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
Chloroethane
BRL
10
pg1L
70849
1
5/13/2006 8:45 AM
Chloroform
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
Chloromethane
BRL
10
pg1L
70849
1
5/13/2006 8:45 AM
cis-1,2-Dichloroethene
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
cis-1,3-Dichloropropene
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
Cyclohexane
BRL
5.0
pg/L
70B49
1
5/13/2006 8:45 AM
Dibromochloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Dichlorodifluoromethane
BRL
10
pglL
70849
1
5/13/2006 8:45 AM
Ethylbenzene
13
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Freon-113
BRL
10
pg/L
70849
1
5/13/2006 8:45 AM
Isopropylbenzene
BRL
5.0
pg/L
70849
1
5113120068:45AM
m,p-Xylene
52
10
pg1L
70849
1
5/13/2006 8:45 AM
Methyl acetate
56
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Methyl tert-butyl ether
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Methylcydohexane
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
l { Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 19 of 30

Analytical Environmental Services, Inc.
Date: 22-A1ay-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-10
Project: Synthron Inc.
Collection Date: 5/1
1/2006 9:15:00 AM
Lab ID: 0605766-004
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchlD
Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg1L
70849
1
5/13/2006 8A5 AM
o-Xylene
15
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Styrene
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Tetrachloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Toluene
69
5.0
pg/L
70849
1
5/13/2006 8:45 AM
trans-1,2-Dichloroethene
BRL
5.0
pglL
70849
1
5/13/2006 8:45 AM
trans-1,3-Dichloropropene
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Trichloroethene
BRL
5.0
pg1L
70849
1
5/13/2006 8:45 AM
Trichlorofluoromethane
BRL
5.0
pg/L
70849
1
5/13/2006 8:45 AM
Vinyl chloride
BRL
2.0
pg/L
70849
1
5/13/2006 8:45 AM
Surr: 4-Bromofluorobenzene
97.8
63.7.115
%REC
70849
1
5/13/2006 8:45 AM
Surr: 4-Bromofluorobenzene
96.0
63.7-115
%REC
70849
50
5/13/2006 2:42 AM
Surr: Dibromofluoromethane
94.3
70.4-123
%REC
70849
50
5/13/2006 2:42 AM
Surr: Dibromofluoromethane
06.1
70.4-123
%REC
70849
1
5/13/2006 8:45 AM
Surr: Toluene-d8
102
73.4-115
%REC
70849
1
5/13/2006 8:45 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849
50
5/13/2006 2:42 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
585
50.0
mg/L
70797
10
5/12/2006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
2570
100
mg/L
70814
10
5/12/2006 3A5 PM
Qualifiers: i Value exceeds Maximum Contaminant Level
13RL Below Reporting Limit
H Holding times For preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 20 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample [D: FT-11
Project: Synthron Inc.
Collection
Date: 5/11/2006
9:35:00
AM
Lab ID. 0605766-005
Matrix: SURFACE
WATER
Analyses
Result
Reporting Qua[
Limit
Units BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-ODD
BRL
1.0
pg1L
70840
1
5/15/2006 10:37 PM
4,4'-DDE
BRL
1.0
pg1L
70840
1
5/15=06 10:37 PM
4,4'-DDT
BRL
1.0
pg1L
70840
1
5/15/2006 10:37 PM
Aldrin
BRL
0.50
pg1L
70840
1
5/15/2006 10:37 PM
alpha-BHC
BRL
0.50
pg1L
70840
1
5/15/2006 10:37 PM
alpha -Chlordane
BRL
0.50
pg1L
70840
1
5/15/2006 10:37 PM
beta-BHC
BRL
0.50
pg1L
70840
1
5/15/2006 10:37 PM
delta-BHC
BRL
050
pg/L
70840
1
5/45/2006 10:37 PM
Dieldrin
BRL
1.0
pg1L
70840
1
5/15/2006 10:37 PM
Endosulfan i
BRL
0.50
pg/L
70840
1
511WO06 10:37 PM
Endosulfan 11
BRL
1.0
pg1L
70840
1
5/15/2006 10:37 PM
Endosulfan sulfate
BRL
1.0
pg1L
70840
1
5/15/2006 10:37 PM
Endrin
BRL
1.0
pg1L
70840
1
5/15/2006 10:37 PM
Endrin aldehyde
BRL
1.0
pg1L
70840
1
5/15/2006 10:37 PM
Endrin ketone
BRL
1,0
pg1L
70840
1
5/15/2006 10:37 PM
gamma-BHC
BRL
0.50
pg/L
70840
1
5/15/2006 10:37 PM
gamma -Chlordane
BRL
0.50
pg/L
70840
1
5/15/2006 10:37 PM
Heptachlor
BRL
0.50
pglL
70840
1
5/15/2006 10:37 PM
Heptachlor epoxide
BRL
0.50
pg/L
70840
1
5/15/2006 10:37 PM
Methoxychlor
BRL
5.0
pg/L
70840
1
5/15/2006 10:37 PM
Toxaphene
BRL
50
pglL
70840
1
5/15/2006 10:37 PM
Surr: Decachlorobiphenyi
17.1
17.9-122 S
%REC 70840
1
5/15/2006 10:37 PM
Sum Tetrachloro-m-xylene
49.5
18.9-119
%REC 70B40
1
5/15/2006 10:37 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
2.62
0.200
mg/L
70835
1
5/15/2006 5:27 PM
Antimony
0.0560
0.0200
mg/L
70835
1
5/15/2006 5:27 PM
Arsenic
BRL
0.0500
mg/L
70835
1
5/15/2006 5:27 PM
Barium
0.0377
0.0200
mg/L
70835
1
5/15/2006 5:27 PM
Beryllium
BRL
0.0100
mg/L
70835
1
5/15/2006 5:27 PM
Cadmium
BRL
0.0050
mg1L
70835
1
5/15/2006 5:27 PM
Calcium
29.7
0.100
mg/L
70835
1
5/15/2006 5:27 PM
Chromium
0,0414
0.0100
mg/L
70835
1
5/15/2006 5:27 PM
Cobalt
0.0347
0.0200
mg/L
70835
1
5/15/2006 5:27 PM
Copper
0.129
0.0100
mg/L
70835
1
5/15/2006 5:27 PM
Iron
33.0
0.100
mg/L
70835
1
5/15/2006 5:27 PM
Lead
0.128
0.0100
mg/L
70835
1
5/15=06 5:27 PM
Magnesium
3.84
0.100
mg/L
70835
1
5/15/2006 5:27 PM
Manganese
1.27
0.0050
mg/L
70835
1
5/15/2006 5:27 PM
Molybdenum
BRL
0.0500
mg1L
70835
1
5/15/2006 5:27 PM
Nickel
0.0676
0.0200
mg/L
70835
1
5/15/2006 5:27 PM
Potassium
11.7
0.500
mg/L
70835
1
5/15/2006 5:27 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
E
I stimated (Value above quantitation range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 21 of 30

Analytical Environmental Services, Inc. Date. 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample [D: FT-1 1
Project: Synthron Inc.
Collection
Date: 5/1
1/2006 9:35:00 AM
Lab ID: 0605766-005
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units SatchlD
Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
BRL
0.0200
mg/L
70835
1
5/15/2006 5:27 PM
Silver
BRL
0,0100
mg/L
70835
1
5/15/2006 5:27 PM
Sodium
88.5
1.00
mg/1-
70835
1
511 W006 5:27 PM
Thallium
BRL
0.0200
mg/L
70835
1
5/15/2006 5:27 PM
Tin
0.102
0.0500
mg/L
70835
1
5/15/2006 5:27 PM
Titanium
0.128
0.0500
mg/L
70835
1
5/15/2006 5:27 PM
Vanadium
0.0570
0.0100
mg1L
70835
1
5/15/2006 5:27 PM
Zinc
5.71
0.0200
mg/L
70835
1
5/15/2006 5:27 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
0.00023
0.00020
mg/L
70883
1
5/16/2006 2:37 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2,4,5-Trichlorophenol
BRL
250
pg/L
70832
1
511WO06 8:51 PM
2,4,6-Trichlorophenol
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2,4-Dichlorophenol
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
2,4-Dimethytphenol
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2,4-Dinitrophenol
BRL
250
pg/L
70832
1
5/15/2006 8:51 PM
2,4-Dinitrotoluene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2,6-Dinitrotoluene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2-Chloronaphthalene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2-Chlorophenol
BRL
100
pg/L
70832
1
5/15/2006 &51 PM
2-Methyinaphthalene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2-Methylphenol
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
2-Nitroaniline
BRL
250
pg/L
70832
1
5/15/2006 8:51 PM
2-Nitrophenol
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
3,3'-Dichlorobenzidine
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
3-Nitroaniline
BRL
250
pg/L
70832
1
5/15/2006 8:51 PM
4,6-Dinitro-2-methylphenol
BRL
250
pg/L
70832
1
5/15/2006 8:51 PM
4-Bromophenyl phenyl ether
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
4-Chloro-3-methylphenol
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
4-Chloroaniline
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
4-Chlorophenyl phenyl ether
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
4-Methylphenol
140
100
pg/L
70832
1
5/15/2006 8:51 PM
4-Nitroaniline
BRL
250
pg/L
70832
1
5/15/2006 8:51 PM
4-Nitrophenol
BRL
250
pg/L
70832
1
5/15/2006 8:51 PM
Acenaphthene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Acenaphthylene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Acetophenone
BRL
100
pg/L
70B32
1
5/15/2006 8:51 PM
Anthracene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Atrazine
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Qualifiers: Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery
outside accepted
recovery limits
H Holding times for preparation
or analysis
exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated Method Blank
Page 22 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-11
Project: Synthron Inc.
Collection Date: 5/11/2006
9:35:00
AM
Lab ID: 0605766-005
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qua, Units
BatchlD Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Beriz(a)anthracene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Benzaldehyde
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Benzo(a)pyrene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Benzo(b)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Benzo(g,h,i)perylene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Benzo(k)fluoranthene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Bis(2-chloroethoxy)methane
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Bis(2-chloroethyl)ether
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Bis(2-chloroisopropyl)ether
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Bis(2-ethy1hexyl)phthalate
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Butyl benzyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Caprolactam
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Carbazole
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Chrysene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Dibenz(a,h)anthracene
BRL
t00
pg/L
70832
1
5115120068:51 PM
Dibenzofuran
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Diethyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Dimethyl phthalate
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Di-n-butyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Di-n-octyl phthalate
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Fluoranthene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Fluorene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Hexachlorobenzene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Hexachiorobutadiene
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Hexachlorocyclopentadiene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Hexachloroethane
BRL
100
pg1L
70832
1
5/15/2006 8:51 PM
Indeno(1,2,3-cd)pyrene
BRL
100
pglL
70832
1
5/15/2006 8:51 PM
Isophorone
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Naphthalene
8RL
100
pg1L
70832
1
5/15/2006 8:51 PM
Nitrobenzene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
N-Nitrosodi-n-propylamine
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
N-Nitrosod i phenyl amine
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Pentachlorophenol
BRL
250
pg/L
70832
1
5/15/2006 8:51 PM
Phenanthrene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Phenol
160
100
pg/L
70832
1
5/15/2006 8:51 PM
Pyrene
BRL
100
pg/L
70832
1
5/15/2006 8:51 PM
Surr: 2,4,6-Tribromophenol
89.7
64.8-129
%REC
70832
1
5/15/2006 8:51 PM
Surr: 2-Fluorobiphenyi
88.4
581-115
%REC
70832
1
5/15/2006 8:51 PM
Surr: 2-Fluorophenol
72.8
24.4-1 15
%REC
70832
1
5/15/2006 8:51 PM
Surr: 4-Terphenyl-d14
79.1
58.3-115
%REC
70832
1
5/15/2006 8:51 PM
Surr: Nitrobenzene-d5
93.9
51.8-115
%REC
70832
1
5/15/2006 8:51 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S Surrogate
Recovery outside accepted recovery limits
H Holding times for preparation or analysis
exceeded
Narr See
Case Narrative
N Analyte not NELAC certified
NC Not Confirmed
B Analvte detected in the associated
Method Blank
Page 23 of 30

Analytical Environmental Services, Inc. Date: 22-Alm-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-11
Project: Synthron Inc.
Collection
Date: 5/1
1/2006 9:35:00 AM
Lab ID: 0605766-005
Matrix- SURFACE WATER
Analyses
Result
Reporting Qua]
Limit
Units BatchlD
Dilution
Factor
Date Analyzed
TCL-SEN]IVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
73.8
17.9-115
%REC
70832
1
5/15/2006 8:51 PM
TCL VOLATILE ORGANICS
SW8260B
(SW6030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,12,2-Tetrachloroethane
BRL
5.0
pg/L
70849
1
5113/20069:11 AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
5113/20069:11 AM
1,1-Dichloroethane
BRL
5.0
pg/L
70849
1
5/13120069:11 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2,4-Trichiorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2-Dibromoethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,2-Dichloroethane
BRL
5.0
pg/L
70849
1
5113=06 9:11 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70849
1
5113=06 9:11 AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
1,4•Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
2-Butanone
64
50
pg1L
70849
1
5/13/2006 9:11 AM
2-Hexanone
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
4-Methyl-2-pentanone
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Acetone
860
500
pg/L
70849
50
5/13/2006 3:08 AM
Benzene
BRL
5.0
p911-
70849
1
5/13/2006 9:11 AM
Bromodichloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Bromoform
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Bromomethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Carbon disulfide
12
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Carbon tetrachloride
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Chlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Chloroethane
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Chloroform
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Chloromethane
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
cis- 1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5113120069:11 AM
cis- 1,3-Dichloropropene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Cyclohexane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Dibromochloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Dichlorodifluoromethane
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Ethylbenzene
BRL
5.0
yg1L
70849
1
5/13/2006 9:11 AM
Freon-113
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Isopropylbenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
m,p-Xylene
BRL
10
pg/L
70849
1
5/13/2006 9:11 AM
Methyl acetate
18
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Methyl tert-butyl ether
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Methylcydohexane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Not Confirmed
B Analyte detected in the associated Method
Blank
Page 24 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc. Client Sample ID: FT -I I
Project: Synthron Inc. Collection Date: 5/1 1/2006 9:35:00 AM
Lab ID: 0605766-005 Matrix: SURFACE WATER
Analyses.
Result
Reporting Qual
Limit
Units
BatchlD Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
o-Xylene
8RL
5.0
NgIL
70849
1
5/13/2006 9:11 AM
Styrene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Tetrachloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Toluene
BRL
5.0
pg1L
70849
1
5/13/2006 9:11 AM
trans-1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13120069:11 AM
trans- 1,3-Dichtoropropene
BRL
5.0
lig/L
70849
1
5/13120069:11 AM
Trichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Trichlorofluoromethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:11 AM
Vinyl chloride
BRL
2.0
pg1L
70849
1
5/13/2006 9:11 AM
Surr: 4-Bromofluorobenzene
99A
63.7-115
%REC
70B49
1
5/13/2006 9:11 AM
Surr: 4-Bromofluorobenzene
96.1
63.7-115
%REC
70849
50
5/13/2006 3:08 AM
Surr: Dibromofluoromethane
95.1
70.4-123
%REC
70849
1
5/13/2006 9:11 AM
Surr: Dibromofluoromethane
93.7
70.4-123
%REC
70849
50
5/13/2006 3:08 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849
1
5/13/2006 9:11 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849
50
5/13/2006 3:08 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
Biochemical Oxygen Demand 215 50.0
CHEMICAL OXYGEN DEMAND (COD)
Chemical Oxygen Demand 1440 10
Qualifiers: * Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NFLAC certified
B Analyte detected in the associated Method Blank
E405.1 (E405.1) Analyst: CAM
mg/L 70797 10 5/12/2006 10:50 AM
E410.4 (E410.4) Analyst: EK
mg/L 70814 1 5/12/2006 3:45 PM
F Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Con firmed
Page 25 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc_
Client Sample ID: FT-12
Project: Synthron Inc.
Collection
Date: 5/11/2006
9:55:00 AM
Lab ID: 0605766-006
Matrix: SURFACE WATER
Analyses
Result
Reporting Quai
Limit
Units BatchlD Dilution
Factor
Date Analyzed
CHLORINATED PESTICIDES, TARGET COMPOUN
SW8081A
(SW3510B)
Analyst: MM
4,4'-DDD
BRL
0.10
pg/L
70840
1
5/15/2006 10:49 PM
4,4'-DDE
BRL
0,10
pg/L
70840
1
5/15/2006 10A9 PM
4,4'-DDT
BRL
0.10
pg/L
70840
1
5/15/2006 10A9 PM
Aldrin
BRL
0,050
pg1L
70840
1
5/15/2006 10:49 PM
alpha-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 10:49 PM
alpha -Chlordane
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
beta-BHC
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
delta-BHC
BRL
0.050
pg1L
70840
1
5/15/2006 10:49 PM
Dieldrin
BRL
0.10
}tg/L
70840
1
5/15/2006 10:49 PM
Endosulfan I
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
Endosulfan II
BRL
0.10
pg1L
70840
1
5/15/2006 10:49 PM
Endosulfan sulfate
BRL
0.10
pg1L
70840
1
5/15/2006 10:49 PM
Endrin
BRL
0.10
pg1L
70840
1
5/15/2006 10:49 PM
Endrin aldehyde
BRL
0.10
pg1L
70840
1
5/15/2006 10:40 PM
Endrin ketone
BRL
0.10
pg/L
70840
1
5/1W006 10:49 PM
gamma-BHC
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
gamma -Chlordane
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
Heptachlor
BRL
0.050
pg/L
70840
1
5/15/2006 10:49 PM
Heptachlor epoxide
BRL
0.050
pg1L
70840
1
511 W006 10:49 PM
Methoxychlor
BRL
0.50
pg/L
70840
1
5/15/2006 10:49 PM
Toxaphene
BRL
5.0
pg/L
70840
1
5/15/2006 10:49 PM
Surr: Decachlorobiphenyl
14.1
17.9-122 S
%REC 70840
1
5/15/2006 10:49 PM
Sum Tetrachloro-m-xylene
104
18.9-119
%REC 70840
1
5/15/2006 10:49 PM
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Aluminum
0.600
0,200
mg/L
70835
1
5/15/2006 5:42 PM
Antimony
0.0257
0.0200
mg/L
70835
1
5/15/2006 5:42 PM
Arsenic
BRL
0,0500
mg1L
70835
1
5/15/2006 5:42 PM
Barium
0.0260
0.0200
mg/L
70835
1
5/1512006 5A2 PM
Beryllium
BRL
0.0100
mg/L
70835
1
511W006 5:42 PM
Cadmium
BRL
0,0050
mg/L
70835
1
5/15/2006 5:42 PM
Calcium
23.2
0.100
mg/L
70835
1
5/15/2006 5:42 PM
Chromium
0.0140
0.0100
mg/L
70835
1
5/15/2006 5:42 PM
Cobalt
BRL
0.0200
mg/L
70835
1
5/15/2006 5:42 PM
Copper
0.0313
0.0100
mg/L
70835
1
5/15/2006 5:42 PM
Iron
13.1
0.100
mg1L
70835
1
5/15/2006 5:42 PM
Lead
0.0296
0.0100
mg1L
70835
1
5/15/2006 5:42 PM
Magnesium
2.51
0.100
mg/L
70835
1
5/15/2006 5:42 PM
Manganese
0.787
0.0050
mg/L
70835
1
5/15/2006 5:42 PM
Molybdenum
BRL
0.0500
mg/L
70835
1
5115/2006 5:42 PM
Nickel
0.0425
0.0200
mg/L
70835
1
5/15/2006 5:42 PM
Potassium
8.35
0.500
mg1L
70835
1
5/15/2006 5:42 PM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis exceeded
Narr
See Case Narrative
N Analyte not NFLAC certified
NC
Not Confirmed
B Analyte detected in the associated
Method
Blank
Page 26 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra "Tech EM Inc.
Client Sample ID: FT-12
Project: Synthron Inc.
Collection
Date: 5/1
1/2006 9:55:00 AM
Lab ID: 0605766-006
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units BatchlD
Dilution
Factor
Date Analyzed
METALS, TOTAL
SW6010B
(SW3010A)
Analyst: BB
Selenium
SRL
0.0200
mglL
70835
1
5/15/2006 5:42 PM
Silver
BRL
0.0100
mg1L
70835
1
511WO06 5:42 PM
Sodium
57.7
1.00
mg1L
70835
1
5/15/2006 5:42 PM
Thallium
SRL
0.0200
mg1L
70835
1
5/15/2006 5:42 PM
Tin
BRL
0.0500
mglL
70835
1
5/15/2006 5:42 PM
Titanium
BRL
0.0500
mg1L
70835
1
5/15/2006 5:42 PM
Vanadium
0.0268
0.0100
mg1L
70835
1
5/15/2006 5:42 PM
Zinc
1,06
0.0200
mg1L
70835
1
5/15/2006 5:42 PM
MERCURY, TOTAL
SW7470A
(SW7470A)
Analyst: LKW
Mercury
BRL
0.00020
mg/L
70883
1
5/16t2006 2:39 PM
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
1,1'-Biphenyl
BRL
10
pglL
70832
1
5/1512006 9:17 PM
2,4,5-Tdchlorophenol
BRL
25
pglL
70832
1
5/15/2006 9:17 PM
2,4,6-Trichlorophenol
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
2,4-Dichlorophenal
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2,4 -Dimethyl phenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2,4-Dinitrophenol
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
2,4-Dinitrotoluene
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2,6-Dinitrotoluene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
2-Chloronaphthalene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
2-Chlorophenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2-Methylnaphthalene
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
2-Methylphenol
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
2-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
2-Nitrophenol
BRL
10
pg1L
70832
1
5/15=06 9:17 PM
3,3'-Dichlorobenzidine
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
3-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
4,6-Dinitro-2-methylphenol
BRL
25
pglL
70832
1
5/15/2006 9:17 PM
4-Bromophenyl phenyl ether
SRL
10
pglL
70832
1
5/15/2006 9:17 PM
4-Chloro-3-methylphenol
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
4-Chloroaniline
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
4-Chlorophenyl phenyl ether
BRL
10
pg1L
70832
1
5/15/2006 9A7 PM
4-Methylphenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
4-Nitroaniline
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
4-Nitrophenol
BRL
25
pg1L
70832
1
5/15/2006 9:17 PM
Acenaphthene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Acenaphthylene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Acetophenone
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Anthracene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Atrazine
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
E•
Estimated (Value above quantitation
range)
BRL Below Reporting Limit
S
Surrogate Recovery
outside accepted
recovery limits
Ft Holding times for preparation or analysis
exceeded
Narr
See Case Narrative
N Analvte not NELAC certified
NC
NotConftrmed
B Analyte detected in the associated
Method Blank
Page 27 of 30

Analytical Environmental Services, Inc. Date: 22-May-06
CLIENT: Tetra Tech EM Inc.
Project: Synthron Inc.
Lab ID: 0605766-006
Client Sample ID: FT-12
Collection Date: 5/1 1/2006 9:55:00 AM
Matrix: SURFACE WATER
Analyses
Result
Reporting
Limit
Qual Units
Bat,hID
Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: ❑A
Benz(a)anthracene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Benzaldehyde
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Benzo(a)pyrene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Benzo(b)fluoranthene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Benzo(g,hJ)perylene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Senzo(k)fluoranthene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Bis(2-chloroethoxy)methane
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Bis(2-chloroethyl)ether
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Bis(2-chloroisopropyl)ether
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Bis(2-ethythexyl)phthalate
31
10
pg/L
70832
1
5/15/2006 9:17 PM
Butyl benzyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Caprolactam
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Carbazole
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Chrysene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Dibenz(a,h)anthracene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Dibenzofuran
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Diethyl phthalate
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Dimethyl phthalate
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Di-n-butyl phthalate
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Di-n-octyl phthalate
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Fluoranthene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Fluorene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Hexachlorobenzene
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Hexachlorobutadiene
BRL
10
pglL
70832
1
5/15/2006 9:17 PM
Hexachlorocydopentadiene
BRL
10
pg/L
70032
1
5/15/2006 9:17 PM
Hexachloroethane
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Indeno(1,2,3-cd)pyrene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
lsophorone
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Naphthalene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Nitrobenzene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
N-Nitrosodi-n-propylamine
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
N-Nitrosodiphenylamine
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Pentachlorophenol
BRL
25
pg1L
70832
1
5/15=06 9:17 PM
Phenanthrene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Phenol
BRL
10
pg1L
70832
1
5/15/2006 9:17 PM
Pyrene
BRL
10
pg/L
70832
1
5/15/2006 9:17 PM
Surr. 2,4,6-Tribromophenol
83.4
64.8-129
%REC
70832
1
5/15/2006 9:17 PM
Surr: 2-Fluorobiphenyl
82.6
58.2-115
%REC
70832
1
5/15/2006 9:17 PM
Surr: 2-Fluorophenol
67.7
24.4-115
%REC
70832
1
5/15/2006 9:17 PM
Surr: 4-Terphenyl-d14
68.0
58.3-115
%REC
70832
1
5/15/2006 9:17 PM
Surr: Nitrobenzene-d5
82A
51.8-115
%REC
70832
1
5/15/2006 9:17 PM
Qualifiers: • Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 28 of 30

Analytical Environmental Services, Inc. Date: 22-Mrry-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-12
Project: Synthron Inc.
Collection
Date: 5/11/2006
9:55:00 AM
Lab ID: 0605766-006
Matrix: SURFACE WATER
Analyses
Result
Reporting
Qual
Limit
Units BatchlD
Dilution
Factor
Date Analyzed
TCL-SEMIVOLATILE ORGANICS
SW8270C
(SW3510)
Analyst: DA
Surr: Phenol-d5
62.0
17.9-115
%REC 70832
1
5/15/2006 9:17 PM
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
1,1,1-Trichloroethane
BRL
5.0
pg/L
70849
1
5/1312006 9:38 AM
1,1,2,2-Tetrachloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,1,2-Trichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,1-Dichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,1-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,2,4-Trichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,2-Dibromo-3-chloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,2-Dibromoethane
BRL
5.0
pg1L
70849
1
5/13/2006 9:38 AM
1,2-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,2-Dichloroethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,2-Dichloropropane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,3-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
1,4-Dichlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
2-Butanone
BRL
50
pg/L
70849
1
5/13/2006 9:38 AM
2-Hexanone
BRL
10
pg1L
70849
1
5/13/2006 9:38 AM
4-Methyl-2-pentanone
BRL
10
pg/L
70849
1
5/13/2006 9:38 AM
Acetone
110
50
pglL
70849
1
5/13/2006 9:38 AM
Benzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Bromodichloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Bromoform
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Bromomethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Carbon disulfide
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Carbon tetrachloride
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Chlorobenzene
BRL
5.0
pg/L
70849
1
5/13/2005 9:38 AM
Chloroethane
BRL
10
pg/L
70849
1
5/13/2006 9:38 AM
Chloroform
BRL
5.0
p91L
70849
1
5/13/2006 9:38 AM
Chloromethane
BRL
10
pg/L
70B49
1
5/13/2006 9:38 AM
cis-1,2-Dichloroethene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
cis- 1,3-Dichloropropene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Cyclohexane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Dibromochloromethane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Dichlorodiffuoromethane
BRL
10
pg/L
70849
1
5/13/2006 9:38 AM
Ethylbenzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Freon-113
BRL
10
pg/L
70849
1
5/13/2006 9:38 AM
Isopropyl benzene
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
m,p-Xylene
BRL
10
pg/L
70849
1
5/13/2006 9:38 AM
Methyl acetate
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Methyl tent -butyl ether
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Methylcydohexane
BRL
5.0
pg/L
70849
1
5/13/2006 9:38 AM
Qualifiers: * Value exceeds Maximum Contaminant Level
E
Estimated (Value above quantization
range)
BRL Below Reporting Limit
S
Surrogate Recovery outside accepted
recovery limits
H Holding times for preparation or analysis
exceeded
Narr
See Case Narrative
N Analyte not NELAC certified
NC
Noi Confirmed
B Analyte detected in the associated Method Blank
Page 29 of 30

Analytical Environmental Services, Inc.
Date: 22-A9ay-06
CLIENT: Tetra Tech EM Inc.
Client Sample ID: FT-12
Project: Synthron Inc.
Collection Date: 5/1 112006 9:55:00 AM
Lab ID: 0605766-006
Matrix: SURFACE WATER
Analyses
Result
Reporting Qual
Limit
Units
BatchID Dilution
Factor
Date Analyzed
TCL VOLATILE ORGANICS
SW8260B
(SW5030B)
Analyst: NWH
Methylene chloride
BRL
5.0
Ng1L
70849 1
5/13/2006 9:38 AM
o-Xylene
BRL
5.0
vglL
70849 1
5/13/2006 9:38 AM
Styrene
BRL
5.0
pg/L
70849 1
5/13/2006 9:38 AM
Tetrachloroethene
BRL
5.0
pg/L
70849 1
5/13/2006 9:38 AM
Toluene
BRL
5.0
pg/L
70849 1
5/13/2006 9:38 AM
trans-1,2-Dichloroethene
BRL
5.0
pg/L
70849 1
5113=06 9:38 AM
trans-1,3-Dichloropropene
BRL
5.0
pg/L
70849 1
5/13/2006 9:38 AM
Trichloroethene
BRL
5.0
pg/L
70849 1
5/13/2006 9:38 AM
Trichlorofluoromethane
BRL
5.0
pg/L
70849 1
5/13/2006 9:38 AM
Vinyl chloride
BRL
2.0
Vg/L
70849 1
5/13/2006 9:38 AM
Surr: 4-Bromofluorobenzene
96.5
63.7-115
%REC
70849 1
5/13/2006 9:38 AM
Surr: Dibromofluoro methane
95.0
70.4-123
%REC
70849 1
5/13/2006 9:38 AM
Surr: Toluene-d8
101
73.4-115
%REC
70849 1
5/13/2006 9:38 AM
BIOCHEMICAL OXYGEN DEMAND (BOD)- 5 DAY
E405.1
(E405.1)
Analyst: CAM
Biochemical Oxygen Demand
44.2
40.0
mglL
70797 10
5/12/2006 10:50 AM
CHEMICAL OXYGEN DEMAND (COD)
E410.4
(E410.4)
Analyst: EK
Chemical Oxygen Demand
633
10
mglL
70814 1
5/12/2006 3:45 PM
Qualifiers: ; Value exceeds Maximum Contaminant Level
BRL Below Reporting Limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated Method Blank
E Estimated (Value above quantitation range)
S Surrogate Recovery outside accepted recovery limits
Narr See Case Narrative
NC Not Confirmed
Page 30 of 30

[ wd: Synthron Wastewater Discharge]
Subject: [Fwd: Synthron Wastewater Discharge]
From: Dana Folley <[e-mail]>
f Date: Fri, 16 Jun 2006 11:03:38 -0400
To: Larry Frost <larry.frost a ncmail.net>, Matt Matthews <Matt. Matthews @ncmai 1. net>, Jeff
Poupart <Jeff.Poupart@ncmaiLnet>
CC: Ken Pickle <[e-mail]>
FYI. Jeremy and I talked on Tuesday about the status, and he said that EPA had
informed the town a few weeks ago that they were going to haul off tanks 1-6, which
we both found interesting...what had EPA learned about these tanks that we didn't
know.... but in any case, that ended the discussion about those tanks. I did ask
Jeremy to let me know if he found out where they were hauling the tanks to.
That leaves 7-12. Each 20,000 gallon tank is 0.4% of the POTW's average flow of
5MGD, and 0.025% of the receiving stream with 76.93 MGD 7Q10. I will forward you
guys the toxicity results Jeremy and I discussed on Tuesday. These showed tanks
7-12 would not cause toxicity, with the possible exception of tank 10. I did this
eval by multiplying the LC50s by 0.01 per 15A NCAC 02B .0208(a)(1) to get the
estimated chronic value. In all cases, this was higher than the tank's % in the
river, so OK - no toxicity. I went over this with Matt to verify I was doing it
right. The exception was tank 10 whose LC50 was <6.25, which times 0.01 equals
<0.065% which is not all that far off from 0.025%. The problem was - how much less
than 6.5% - so we needed EPA to re -run the test with lower concentrations.
Apparently EPA agreed to haul this tank off, so end of that problem.
Note it appears EPA never ran the ASRIT tests, but they had already done the
COD/ROD thing with this big round of testing, and tanks 7-12, except for 10, had
CODs less than 1500, some quite a bit less. I had talked to Jeremy on Tuesday
about what the ASRIT test does and how he could do somewhat of one in his own lab
by observing his bugs under the microscope. He then pointed out that with his pure
oxygen aeration basin he can essentially measure oxygen uptake in his basins as the
waste is fed in and be alerted to any oncoming inhibition. We also talked about
doing settleability tests, because he said he had done one on one of the tanks and
the solids had never settled! So it appears that he took all that, did his own
tests, and decided to forgo the ASRIT test requirement. I personally have no
problem with this, and think he will do a good job of monitoring his system.
Also FYI, I will be talking to Ken Pickle in Stormwater about ?I think when EPA
will be allowed to just start letting any new stormwater go? So more later.
-Dana
Subject: Synthron Wastewater Discharge
From: "Rees, Jeremy" <[e-mail]>
Date: Fri, 16 Jun 2006 08:27:19 -0400
To: "Dana Folley" <[e-mail]>
Dana,
We ran separate settleability tests with our mixed liquor and the calculated loading dose from each tank and
saw no difference compared with our normal mixed liquor.
We also set up a microscopic analysis with the Synthron water and our mixed liquor and saw no difference in
bug activity. We connected the microscope to a t.v, monitor and watched the bugs expire with normal conditions
observed. It took 40 - 45 min for them to dry up on the slide which is normal for us.
We talked with EPA about accepting the wastewater and they volunteered not to discharge FT-10. They will
1 or 2 6/19/2006 7:45 AM
A

Synthron Wastewater Discharge}
haul it off for disposal.
We are going to accept tanks 07,08,09,11 and 12. They are going to discharge them at a rate of 33 gpm over a
10 hour period. They will dump a tank on Monday, Wednesday and Friday.
After viewing all the lab results, settleability test and microscopic analysis, we felt pretty confident we can accept
the wastewater with no harm to the biological activity in the plant. We will continue to closely monitor the plant
over the next few weeks to look for any signs that the wastewater from the site is affecting the plant.
Jeremy E. Rees
Wastewater Superintendent
City of Morganton
Phone: [phone]
Fax: [phone]
Content -Type: messagelr&822
Synthron Wastewater Discharge
Content -Encoding: 7bit
6/19/2006 7:45 AM

Summary of the Synthron Fire 96-Hour Acute Toxicity Tests with Ceriodaphnia dubia
Sample ID
Media Lethal Concentration (%)
(LC50)
95% Confidence Limits
FT-07
42.23
33.96 - 52.52
FT-08
73.2
66.67 - 80.37
FT-09
73.03
66.25 - 80.5
FT-10
<6.25
Non calculable
FT-11
24.22
18.38 - 31.94
FT-12
> 100
NA

Testl�merica
ANALYTICAL TESTING CORPORATION
October 09, 2006
Client: WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn: Gar)' Acquaro
SAMPLE IDENT[ FICATION
S W F 92506
SWNF92506
2950 Foster Creighton Road Nashvilre, TN 37204' 8M755-0960 'Fax [phone]
Work Order:
NP13179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Nbr:
106150
P/O Nbr:
741 10248
Date Received:
09/26/06
LAB ,NUMBER COLLECTION DATE AND TIME
NP13179-01 09/25/06 14:00
NP13179-02 09/25/06 14:00
An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum
to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at
1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accredidation.
This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is
privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the
intended recipient, you are hereby notified that any dissemination, distribution; or copying of this material is strictly prohibited. If you
have received this material in error, please notify us immediately at 615-726-0177.
Additional Laboratory Comments:
The 625 blank spike duplicate (LCSD) was outside QC limits. There was insufficient sample available for
re -extraction and re -analysis.
North Carolina Certification Number: 387
The Chain(s) of Custody, 2 pages, are included and are an integral part of this report.
These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory.
Report Approved By:
(fail A Lage
Program Manager - National Accounts
Page 1 ol'24

Testl�.me'rica
ANALYTICAL TESTING CORPORATION 2960 Faster Creighton Road Nashville, TN 37204.800-765-0980' Fax [phone]
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Gary Acquaro
Work Order: NP13179
Project Name: Synthron Chemical Fire Site in Morganton, NC
Project Number: 106150
Received: 09/26/06 08:50
ANALYTICAL RLPORT
Dilution
Analysis
Analyte
Result
Flag Units
NIRL Factor
Date rime
Method
Batch
Sample ID: NP13179-01 (SWF92506
-Waste Water) Sampled: 09/25/06 14.00
General Chemistry Parameters
BOD - 5 Day
394
mg/L
2.00 1
10/01 /06 23:25
EPA 405A
6094794
Chemical Oxygen Demand
24.5
mg/L
10.0 1
09/27/06 1 L36
EPA 410.4
6094980
Total Suspended Solids
6.00
mg/L
2.00 1
09/26/06 17:44
EPA 160.2
6094803
Total Metals by EPA Method 6010E
Arsenic
ND
mg/L
0.0100 1
09128/0622:03
SW846601OH
6094940
Barium
0.0185
mg/L
0D100 1
09/28/0622:03
SW846601OB
6094940
Cadmium
ND
mgfL
0.00100 1
09/28/0622:03
SW846601OB
6094940
Chromium
0.00760
mg/L
0,00500 1
09128/0622:03
SW846501013
6094940
Lead
ND
mg/L
0.00500 1
09/28/062293
SW846501OB
6094940
Selenium
ND
mg/L
0.0100 1
09/2910622:03
SW846601OB
6094940
Silver
ND
mg/L
0.00500 1
09/28/06 22 03
SW846 501 OB
6094940
Mercury by EPA Methods 7470A/747IA
Mercury
ND
mg/L
0.000200 1
09/29/06 15:08
SW846 7470A
6095002
Purgeable Organic Compounds by EPA Method 624
Acrolcin
ND
ug/L
50.0 1
09/27/06 12:27
EPA 624
6094724
Acrylonitrile
ND
ug/L
10.0 1
09/27/06 12:27
EPA 624
6094724
Benzene
ND
ug/L
1.00 1
09/27/06 I2:27
EPA 624
6094724
Bromodichloromethane
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Bromororm
ND
ug/L
1.00 1
09127/06 12:27
EPA 624
6094724
Bromomethane
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Carbon Tetrachloride
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Chlorobenzene
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Chlorodibromomethane
ND
ug/L
1,00 1
09/27/06 12:27
EPA 624
6094724
Chlemethanc
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Chloroform
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Chloromethane
ND
ug/L
1.00 1
09127/06 12:27
EPA 624
6094724
1,2-Dichlorobenzene
ND
ug/L
1,00 1
09/27/06 12:27
EPA 624
6094724
IA-Dichloroben7ene
ND
ug/L
1.00 1
09127/06 12:27
EPA 624
6094724
1,3-Dichlorobenzene
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Dichlorodiftuoromethane
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
1,2-Dichloroethane
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
1,1- Diehl oroethane
ND
ug/L
1.00 1
09127/06 12:27
EPA 624
6094724
cis-1,2-Dichloroethene
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
trans-1,2-Dichloroethene
ND
ug/L
I.00 1
09127/0612:27
EPA 624
6094724
1,1-Dichloroethene
ND
ug/L
100 1
09/2710612:27
EPA 624
6094724
1,2-Dichloropropene
ND
ug/L
1.00 1
0912710612:27
EPA 624
6094724
cis-1,3-Dichloropropene
ND
ug/L
Loo 1
09/2710612:27
EPA 624
6094724
trans.1,3-Dichloropropene
ND
ug/L
1.00 1
0912710612:27
EPA 624
6094724
Ethylbenzene
ND
ug/L
1.00 1
09/27106IZ27
EPA 624
6094724
Methylene Chloride
ND
ug/L
5.00 1
09/27/06 12:27
EPA 624
6094724
1,1,2,2.Tetrachloroethane
ND
ug/L
1,00 1
09/27/06 12:27
EPA 624
6094724
Tetrachioroethene
ND
ug/L
1.00 1
09/27/06 12:27
EPA 624
6094724
Page 2 of 24

TestAmer ca
ANALYTICAL TESTING CORPORATION
2960 Foster
Creighton Road Nashville,
TN 37204' 800-765-0980' Fax [phone]
Client WRS (3166)
Work Order:
NP13179
221 Hobbs Street, Suite 108
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619
Project Number:
106150
Attn Gary Acquaro
Received:
09/26/06 08:50
ANALYTICAL REPORT
Dilution Analysis
Anallte Result Flag
Units
MRL
Factor Date/Time
Method
Batch
Sample ID: NP13179-01 (SWF92506 - Waste Water) - cont. Sampled:
09/25/06 14:00
Purgeable Organic Compounds by EPA Method 624 - cont.
Toluene ND
uglL
1.00
1 09/27/06 12:27
EPA 624
6094724
1,1,2-Trichloroethane ND
ug/L
Loo
1 09/27/0612:27
EPA 624
6094724
1,1,1-Trichloroethane ND
ug/L
1_00
1 09/27/0612:27
EPA 624
6094724
Trichloroethene ND
ug/L
1.00
1 09/27/06 12:27
EPA 624
6094724
Trichlorolluoromethane ND
ug/L
1.00
t 09/27/06 12:27
EPA 624
6094724
Vinyl chloride ND
ug/L
1.00
1 09/27/06 12:27
EPA 624
6094724
Xylenes, total ND
ug/L
2,00
1 09/27/06 12:27
EPA 624
6094724
Surr: 1,2-Diclrloroethane-d4 (81-126%) 96 %
09127106 12:27
EPA 624
6094724
Surr. Dibromofluoromethane (88-120%) 100 %
09127106 12:27
EPA 624
6094724
Surr: Tohrerre-d8 (85-130%) 115 %
09127106 12:27
EPA 624
6094724
Surr: 4-Bromofluoroben�ene (80-114%) 107 %
09127106 11'27
EPA 624
6094724
Acid and Base/Neutral Extractables by EPA Method 625
Acenaphthene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Acenaplithylene
ND
ug L
10S
1 0912910603:52
FPA 625
6094444
Anthracene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Benzo (a) anthraeene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Benzo (a) pyrene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Benzo (b) ❑uomnthene
ND
ugIL
10.5
1 09/29/06 03:52
EPA 625
6094444
Benzo (g,h,i) perylene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
60944"
Benzo (k) tluoranthene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
4-13romophenyl phenyl ether
N❑
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Butyl benzy] phthalate
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
4-Chloro-3-mcthylphenol
ND
ug/L
t0.5
1 09/2910603:52
EPA 625
6094444
Bis(2-chloroethoxy)methane
ND
ug/L
10.5
1 09/2910603-52
EPA 625
6094444
Bis(2-chloroethyl)ether
ND
ug/l-
10.5
1 09/29/06 03:52
EPA 625
6094444
Bis(2-chloroisopropyl)ether
ND
ug/L
10.5
1 09/29/0603:52
EPA 625
6094444
2-Chloronaphthalene
ND
ug/L
10.5
l 09/29/06 03.52
EPA 625
6094444
2-Chlorophenol
ND
ug/L
10,5
1 09/29/06 03:52
EPA 625
6094444
4-Chlorophenyl phenyl ether
ND
ug/L
10.5
l 09129106 03-52
EPA 625
6094444
Chrysene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Dibenz (a,h) anthracene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Di-n-butyl phthalate
ND
ugll,
10.5
1 09/29/06 03:52
EPA 625
6094444
1,3-Dichlorobenzene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
1,4-1ichlorobenzene
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
1,2-Dichlorobenzene
ND
ug/L
10.5
1 09/29/0603:52
EPA 625
6094444
3,3'-Dichlorobenzidine
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
2,4-Dichlorophenol
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Diethyl phthalate
ND
ug/L
10.5
1 09/29/06 03-52
EPA 625
6094444
2,4-Dimethylplrenol
ND
ug/L
10.5
1 09/29/06 03:52
EPA 625
6094444
Dimethyl phthalate
ND
uglL
10.5
1 09/29/06 03:52
EPA 625
6094444
4,6-Dinitro-2-methylphenol
ND
ug/L
26 3
1 09129/06 03:52
EPA 625
6094444
2,4-Dinitrophenol
ND
ug/L
26,3
l 09/29/06 03:52
EPA 625
6094444
2,6-Dinitrotoluene
ND
ug/L
10.5
l 09/2910603:52
EPA 625
6094444
Page 3 of 24

TestAimerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Gary Acquaro
2WO Foster Creighton Road Nashville, TN 37204 ' 600-765-0980' Fax [phone]
Work Order:
NP13179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Number:
106130
Received:
09/26/06 08:50
ANA1,YT1CAL REPORT
Dilution Analysis
Analytc Result Flag Units INIRI. Factor Datefl'ime Nlethod Batch
........ .... ... ......... ... . .. ... .. ....., ...... . ... ...- ......... -- — . -..... ........... ....-.......
Sample ID: NP13179-01 (SWF92506 - Waste Water) - cont. Sampled: 09/25/06 14:00
Acid and Base/Neutral Extractables by EPA Method 625 - cont.
2,4-Dinitrotoluene
ND
ug/L
10.5
Di-n-octyl phthalate
ND
ug/L
10.5
Bis(2-ethylhexyl)phthalate
ND
ug/L
10.5
Fluoranthene
ND
ug/L
10.5
Fluorene
ND
ug/L
10.5
Hexachlorobenzene
ND
ug/L
10.5
Hexachlorobutadiene
ND
ug/L
10.5
Hexachlorocyclopentadiene
ND
ug/L
10.5
Hexachloroethane
ND
ug/L
10.5
Indeno (1,2,3-cd) pyrene
NI)
ug/L
10.5
Isophorone
ND
ug/L
10.5
Naphthalene
ND
ug/L
10.5
Nitrobenzene
ND
ug/L
10.5
2-Nitrophenol
ND
ug/L
10.5
4-Nilrophenol
ND
ug/L
26.3
N-Nitrosoditnethylamine
ND
ug/L
10.5
N-N itrosod iphenylam ine
ND
ug/L
10.5
N-Nitrosodi-n-propylamine
ND
ug/L
10.5
Pentachloropheno I
ND
ug/L
26.3
Phe nanth rene
ND
ug/L
10.5
Phenol
ND
ug/L
10.3
Pvrene
NI)
ug/L
10.5
1,2,4-Trichlorobenzene
ND
ug/L
10.5
2.4,6-Trichlorophen0l
ND
ug/L
10.5
l,2-Diphenylhydrazine
ND
ug/L
10.5
2-MethyInaphthalene
ND
ug/L
10,5
Sun: Terphenvl-d14 (34-116%)
75 %
Surr: 2,4,6-Tribromophenol (16-130%)
60 %
Surr: PhenoW5 (10-66%)
33 %
Surr: 2-Fluorobiphenyl (32-99%)
73 %
Surr: 2-Fluarophenol (10-81 %)
40 %
Surr: Nitrobenzene-d5 (19-116%)
76 %
1 09/29/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 0929106 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09129/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 0929106 03:52
E PA 625
6094444
1 0929/06 03-52
EPA 625
6094444
1 0929106 03:52
EPA 625
6094444
1 0929/06 0152
EPA 625
6094444
1 0929106 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 0929/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 0929106 03:52
EPA 625
6094444
1 0929/06 03:52
EPA 625
6094444
1 0929/06 03:52
EPA 625
6094444
1 0929/06 03:52
EPA 625
6094444
1 09/29/06 03:52
EPA 625
6094444
1 09f29/06 03:52
EPA 625
6094444
09129106 03:52
EPA 625
6094444
09129106 03:52
EPA 625
6094444
09129/06 03:52
EPA 625
6094444
09129106 03:52
EPA 625
6094444
09129106 03:52
EPA 625
6094444
09129106 03:52
EPA 625
6094444
Page 4 of24

e
Testli nmerlca
ANALYTICAL TESTING CORPORATION 2960 Foster Creighton Roed Nashville, TN 37204 ' 800-765-0980 " Fax [phone]
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Gary Acquaro
Work Order: NP13179
Project Name: Synthron Chemical Fire Site in Morganton, NC
Project Number: 106150
Received: 09/26/06 08:50
ANALI'TICAL REPORT
Dilution
Analysis
Analyte
Result
Flag Units
MRL Factor
Daterrime
Method
Batch
Sample 1D: NP13179-02 (SWNF92506
- Waste Water) Sampled: 09/25/06 14:00
General Chemistry Parameters
BOD - 5 Day
12.0
mg1L
5.00 2.5
10101 /06 23:25
EPA 405.1
6094794
Chemical Oxygen Demand
97.7
mg/L
10.0 1
09/27/06 11:36
EPA 410.4
6094980
Total Suspended Solids
203
mg/L
6,67 1
09/26/06 17:44
EPA 160.2
6094803
Total Metals by EPA Method 6010B
Arsenic
ND
mg/L
0.0100 1
09/28/0622:07
SW8466010B
6094940
Barium
0.0464
mg/L
0.0100 1
09128/0622:07
SW846601OB.
6094940
Cadmium
0.00210
mgJL
0.00100 1
09128/0622:07
SW8466010B
6094940
Chromium
0.0200
mg/L
0.00500 1
09/28/0622:07
SW8466010B
6094940
Lead
0.0122
mg/L
0.00500 1
09128/0622:07
SW8466010B
6094940
Selenium
ND
mg1L
0,0100 1
09/28/0622:07
SW8466010B
6094940
Silver
ND
mg/L
0.00500 1
09/28/0622:07
SW8466010B
6094940
Mercury by EPA Methods 7470A/747IA
Mercury
ND
mg/L
0.000200 1
09/29/06 15:10
SW846 7470A
6095002
Purgeable Organic Compounds by EPA Method 624
Acrolem
ND
ug/L
50.0 1
09/27/06 12:57
EPA 624
6094724
Acrylonitrile
ND
ug/L
10.0 1
09/27/06 12:57
EPA 624
6094724
Benzene
ND
ug/L
1,00 1
09/27/06 12:57
EPA 624
6094724
Bromodichloromethane
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
Elromoform
ND
ug/L
1,00 I
09/27/06 12:57
EPA 624
6094724
Bromomethane
ND
ug/L
I DO 1
09/27/06 12:57
EPA 624
6094724
Carbon Tetrachloride
ND
ug/L
I.00 1
09/27/06 12:57
EPA 624
6094724
Chlorobenzene
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
Chlorodibromomethane
ND
ug/L
100 I
09/27/06 12:57
EPA 624
6094724
Chloroethane
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
Chloroform
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
Chloromethane
ND
ng/L
1.00 1
09/27/06 12:57
EPA 624
6094724
1,2-Dichlorobenzene
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
1,4-Dichloroben7ime
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
1.3-Dichlorobenzene
ND
ug/L
1.00 1
09127/0612;57
EPA 624
6094724
Dichlorodifluoromethatre
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
1,2-Dichloroethene
ND
tig/L
1.00 1
09/27/06 12:57
EPA 624
6094724
1,1-Dichloroethene
ND
uglL
1.00 1
09/27/06 12:57
EPA 624
6094724
cis-1,2-Dichloroethene
ND
ug/L
1.00 1
09/2710612:57
EPA 624
6094724
trans-1,2-Dichloroethene
ND
ug/L
1,00 1
09/27/06 12:57
EPA 624
6094724
l,l-Dichloroethene
ND
ug/L
1.00 1
09127/0612:57
EPA 624
6094724
1-2-Dichloropropane
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
cis-1,3-Dichloropropene
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
trans-i,3-Dichloropropene
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
Ethylbenzene
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
Methylene Chloride
ND
ug/L
5.00 1
09/27/06 12:57
EPA 624
6094724
1,1,2,2-1'ctrachloroethane
ND
ug/L
1.00 1
09/27/06 12:57
EPA 624
6094724
Tetrachloroethene
ND
ugll,
1.00 1
09/27/06 12:57
EPA 624
6094724
Page 5 of 24

s
Testlimerica
ANALYTICAL. TESTING CORPORATION
2960 Faster Creighton Road Nashville,
TN 37204 ' 800-765-0980 ' Fax [phone]
Client WRS (3166)
Work Order:
NP13179
221 1 lobbs Street, Suite 108
Project Name:
Synthron Chemical
Fire Site in Morganton, NC
Tampa, FL 33619
Project Number:
106150
Ann Gary Acquaro
Received:
09/26/06 08:50
ANALYTICAI, REPORT
Dilution
Analysis
Analyte Result Flag
Units
MRL
Factor
Date/Time
Method
Batch
Sample ID: NP13179-02 (SWNF92506 - Waste Water) - cont. Sampled:
09/25/06 14,00
Purgeable Organic Compounds by EPA Method 624 - cont.
Toluene ND
ug1L
1.00
1
09/27/06 12:57
EPA 624
6094724
1,1,2-Trichloroethane ND
ug/L
1.00
1
09/27/06 12:57
EPA 624
6094724
1, 1, 1 -Trichloroethane ND
ug/L
1.00
1
09/27/06 12:57
EPA 624
6094724
'rrichloroethene ND
ug/L
1.00
1
09/27/06 12:57
EPA 624
6094724
Trichlorofluoromethane ND
ug/L
1.00
1
09/27/06 12:57
EPA 624
6094724
Vinyl chloride ND
ug/L
1.00
1
09/27/06 12:57
EPA 624
6094724
Xylenes, total ND
ug/L
2.00
1
09/27/06 12:57
EPA 624
6094724
Surr. 1, 2-Dichloroethane-d4 (81-126%) 97 %
09127106 12:57
EPA 624
6094724
Sorr: DibromoJluoromethane (88-120%) 102 %
09127106 12:57
EPA 624
6094724
5urr. Toluene-cO (85-130%) 113 %
09/27/06 12:57
EPA 624
6094724
Sum 4-BronroJluorobenrene (80-12491-) 105 %
09127106 12:57
EPA 624
6094724
Acid and Base/Neutral Extractables by EPA Method 625
Acenaphthene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Acenaphthvlene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Anthracene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Benzo (a) anthracene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
13enzo (a) pyrene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Benzo (b) tluoranthene
ND
ug11-
10.5
1 09/29/06 04:15
EPA 625
6094444
Benzo (g,h,i) perylene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Benzo (k) fluomnthene
ND
ug/L
10.5
1 09129/06 04:15
EPA 625
6094444
4-Bromophenyl phenyl ether
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Butyl benzyl phthalate
ND
ug/l,
10.5
1 09/29/06 04:15
EPA 625
6094444
4-Chloro-3-methyl phenol
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
E3is(2-chloroethoxy)methane
ND
ug/l,
10.5
1 09/29/06 04:15
EPA 625
6094444
13is(2-chloroethyl)ether
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
E3is(2-chloroisopropyl)ether
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
2-Chloronaphthalenc
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
2-Chlorophenol
ND
ug/L
10.5
1 09/29/0604:15
EPA 625
6094444
4-Chlorophenyl phenyl ether
ND
ug/I,
10.5
1 09/29/06 04:15
EPA 625
6094444
Chrysene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Dibenz (a,h) anthracene
ND
ug/L
105
1 09/29/06 04:15
EPA 625
6094444
1)i-n-butyl phthalate
ND
tig/L
10.5
1 09/29/06 04:15
EPA 625
6094444
1,3-Dichlorobenzene
ND
ug/E,
10.5
1 09/29/06 04:15
EPA 625
6094444
IA-Dichlorobenzene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
1,2-Dichlorobenzene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
3,Y-Dichlorobenzidine
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
2,4-Dichlorophenol
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Diethyl phthalate
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
2,4-Dirnethylphenol
ND
uglL
10.5
1 09/29/06 04:15
EPA 625
6094444
Dimethyl phthalate
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
4,6-Dinitro-2-methyl phenol
ND
ug/L
26.2
1 09/29106 04. 15
EPA 625
6094444
2,4-Dinitrophenol
ND
ug/L
26.2
1 09/29/06 04:15
EPA 625
6094444
2,6-Dinitrotoluene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Page 6 of 24

s
TestAmerica
ANALYTICAL TESTING CORPORATION 2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax [phone]
Client WRS (3166) Work Order: NP13179
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619 Project Number: 106150
Attn Gary Acquaro Received: 09/26/06 08:50
ANALYTICAL REPORT
Dilution Analysis
AnaNte
Result Flag
Units
MRL
Factor Date/Time
Method
Batch
Sample ID: NP13179-02 (SWNF92506 - Waste Water) - cont. Sampled: 09/25/06 14:00
Acid and 13ase/Neutral Extractables by
EPA Method 625 - cont.
2,4-Dinitrotoluene
ND
uglL
10.5
1 09/29/06 04:15
EPA 625
6094444
Di-n-octyl phthalate
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
F3is(2-ethylhexyl)phthalate
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Fluotanthene
ND
ug/L
10.5
1 09/2910604:15
EPA 625
6094444
Fluorene
ND
ug/I.
10.5
1 09/29/06 04:15
EPA 625
6094444
Hexachlorobenzene
ND
ug/L
10.5
1 09/29/06 04:15
UPA 625
6094444
Hexachlorobutadiene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Hexachlorocyclopentadiene
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Hexachloroethane
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
Indeno (1,2,3-cd) pyrene
ND
ug/l.
10.5
1 09/29/06 04:15
EPA 625
6094444
isophorone
ND
uof
10,5
1 09/29/06 04:15
EPA 625
6094444
Naphthalene
ND
ug/l-
I0,5
1 09/29/06 04:15
EPA 625
6094444
Nitrobenzene
ND
ug/L
10.5
1 09/29/06 04:15
GI'A 625
6094444
2-Nitrophenol
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
4-Nitrophenol
ND
ug/L
26.2
1 09/2910604-15
EPA 625
6094444
N-Nitrosodimethylamine
ND
ug/L
10.5
1 09129/0604:15
EPA 625
6094444
N-Nitrosodiphenylamine
ND
ug/L
10.5
1 09/29/0604.15
EPA 625
6094444
N-Nitrosodi-n-propylamine
ND
ug/1-
10.5
1 09/29/06 04:15
FiPA 625
60944"
Pentachlorophenol
ND
ug/L
26.2
1 09129106 04:15
EPA 625
6094444
Plienanthrene
ND
ug/1-
10.5
1 09/29/06 04:15
EPA 625
6094444
Phenol
ND
ug/L
10.5
1 09/29/06 04: 15
EPA 625
6094444
Pvrene
ND
uF)L
10.5
1 09/29/06 04:15
EPA 625
6094444
1,2,4-Trichlorobenzene
ND
ug1L
10-5
1 09/2910604:15
EPA 625
6094444
2,4,6-Trichlorophenol
ND
ug/L
10.5
1 09/29/06 04:15
EPA 625
6094444
1,2-Dipheny1hydrazine
ND
ug/L
10,5
1 09/29/0604 15
EPA 625
6094444
2-Me1hy1naplithalene
ND
ug/L
10.5
1 09/29/06 04 : 15
IEPA 625
6094444
Starr: Tarphen-vl-d14 (34-116%)
73 %
09129106 04:15
EIIA 625
6094444
Starr: 2,4,6-Tribromophertol (16-130%)
25 %
09129106 04:15
EPA 625
6094444
Surr: Phenol-rI5 (10-66%)
24 %
09129106 04:15
EPA 625
6094444
Surr: 2-Fluorobi1henyl (32-99%)
81 %
09129106 04:15
EPA 625
6094444
Surr: 2-Fluorophenol (10-8I%)
19 %
09129106 04:15
EPA 625
6094444
Srrrr: Arirroben=ene-d5 (19-116%)
81 %
09129106 04:15
EPA 625
6094444
Page 7 of 24

TestAmerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980 • Fax [phone]
Work Order NP13179
Project Name: Synthron Chemical Fire Site in Morganton, NC
Protect Number: 106150
Received: 09/26/06 0&50
SAMPLE EXTRACTION DATA
Wt/Vol
Extraction
Parameter
Batch
Lab Numtx r
Extracted
Extracted Vol
Date
Analyst
Method
Acid and Base/Neutral Extractables by EPA Method 625
E:PA 625
6094444
NP13179.01
950.00
1.00
09/26/06 17:02
KLG
EPA 625
EPA 625
6094444
NP[3179-02
955.00
1.00
09/26/06 17:02
KLG
EPA 625
General Chemistry Parameters
EPA 405.1
6094794
NP13179-01
300.00
300.00
09/27/06 00:20
JTH
BODICBOD
EPA 405.1
6094794
NP13179-02
300.00
300,00
09/27/06 00:20
Ml
BODICBOD
Mercury by EPA Methods 7470A/7471 A
SW846 7470A
6095002
NP13179-01
30.00
30.00
09129/06 10:24
LTB
EPA 7470
SW846 7470A
6095002
14P13179-02
30.00
30.00
09129/06 lU4
LTB
EPA 7470
Total Metals by EPA Method 6010B
NW84660JOB
6094940
NP13179-01
50,00
50.0o
09/27/060830
JMR
EPA3010A
SW846 601OB
6094940
NPt3179-01
50,00
50.00
09/27/06 08:30
JMR
EPA 301OA
SW8466010B
6094940
NP[3179-01
50,00
50.00
09/27/06 08:30
JMR
EPA3010A
SW8466010B
6094940
NP[3179-01
50.00
50.00
09/27/06 08:30
JMR
EPA3010A
SW9466010B
6094940
NP13179-01
50.00
50,00
09127/06 08:30
JMR
EPA3010A
SW84660JOB
6094940
NP133179-01
50.00
50.00
09/27/06 08:30
J\JR
EPA3010A
SW84660JOB
6094940
N1113179-01
50.00
50.00
09/27/06 08:30
JN4R
EPA3010A
SW84660JOB
6094940
NP13179-02
50.00
50.00
09/27/06 08:30
RA
EPA3010A
SW94660JOB
6094940
NP13179-02
50.00
50.00
09/27/06 08:30
JMR
EPA3010A
SW846601OB
6094940
N1113179-02
50.00
50.00
09127/06 08:30
JMR
EPA3010A
SW8466010B
6094940
NP13179-02
50.00
50.00
09/27106 08:30
JMR
EPA3010A
SW8466010B
6094940
NP1317942
50.00
50.00
09121I06 08:30
JMR
EPA 301OA
SW8466010B
6094940
NP13179-02
50.00
50,00
09/27106 08:30
JMR
EPA3010A
S%V8464010B
6094940
NP13179-02
50.00
50.00
09/27/06 08:30
JMR
EPA3010A
Page 8 of24

Test merica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204' 800-705-0960 - Fax [phone]
Client WRS (3166) Work Order: NP13179
22l Hobbs Street, Suite 108 Project Name: Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619 Project Number: 106150
Attn Gary Acquaro Received: 09/26/06 08:50
PROJECT QUALITY CONTROL DATA
Blank
Analvte
Blank Value
Q Units
Q.C. Batch
Lab Number
Analyzed Datcrrime
Ceneral Chemistry Parameters
6094794-BLK1
BOD - 5 Day
<1.00
mglL
6094794
6094794-BLKI
10/01/06 23:25
6094803-BLKI
Total Suspended Solids
<0,500
mglL
6094803
6094803-BLKI
09/26106 17:44
6094980-BLKI
Chemical Oxygen Demand
<5.50
mglL
6094980
6094980-BLKI
09127106 11:36
Total Metals by EPA Method 6010B
6094940-BLK1
Arsenic
<0.00480
mglL
6094940
6094940-BLKI
09128/06 21:32
Barium
<000100
mglL
6094940
6094940-BLKI
09/28106 21132
Cudinium
0.000900
mg1L
6094940
6094940-BLKI
09/29/06 08:49
Chromitun
0.00320
tng1L
6094940
6094940-BLKI
09/28/06 21:32
Lcad
<0.00220
ing/L
6094940
6094940-BLKI
09/28/00 21:32
Selenium
<0,0082o
mglL
6094940
6094940-BLKI
09/28/06 21:32
Silver
0.00350
mgil-
6094940
6094940-BLKI
09/28/06 21:32
Mercury by EPA Methods 7470A17471A
6095002-BLKI
Mercury a 0.000100
Purgeable Organic Compounds by EPA Method 624
6094724-BLKI
Acrolein
<I.18
Acryloninile
<0 520
Bemzene
<0-290
Bromodichlornmethanc
<0, 370
Bromoform
<0.140
Bromomelhane
<0.320
C:ubcn Tutrachimicic
<0. 150
Cldorobenzene
<0.310
Chlorodibromwnethane
<0.130
Chlorocthane
<0.170
Chloroform
<0.130
C hloronlethane
<0.1 10
1,2-Dichlorobenzeae
<0.170
1,4-Dichlorobenzene
<0.310
1,3- Dichlorobe nzene
<0.120
Dichl orodi lluoromethane
<0 470
] 2-Dichloroethane
<0.560
1.1-Dichloroethane
<0-310
ntg1L 6D95002 6095002-13LKI 09/29106 15:03
ug/L
6094724
6094724-BLKI
09/27/06 10:59
ug/L
6094724
6094724-BLKI
09/27/06 10:59
11g1L
6094724
6094724-BLKI
09/27/06 10:59
1g1L
6094724
6094724-BLK1
09/27/06 10:59
ug1L
6094724
6094724-BLKI
09/27/06 W59
ug/L
6094724
6094724-BLKI
09127/06 I0:59
uglL
6094724
6094724-BLKI
09/27/06 IM9
ug/L
6094724
6094724-BLK 1
09127/06 10:59
ug/L
6094724
6094724-BLKI
09/27/06 10:59
ug/L
6094724
6094724-BLKI
09/27/06 10:59
rtglL
6094724
6094724-BLKI
091271D6 10:59
ug/L
6094724
6094724-BLKI
09/27/06 M59
ug/L
6094724
6094724-BLKI
09/27106 1059
ug1L
6094724
6094724-BLKI
09127/06 10:59
ug/L
6094724
6094724-BLKI
09/27/06 10-59
ug1L
6094724
6094724-BLK1
09/27/06 10:59
ug/L
6094724
6094724-BLK1
09/27/06 1059
ug/L
6094724
6094724-BLKI
09/27/06 10.59
Page 9 of 24

Testl�,merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Ant Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204 . 800-765-0980 • Fax [phone]
Work Order:
NP13179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Number:
106150
Received:
09/26/06 08:50
PROJECT QUALITY CONTROL DATA
Blank - Cont.
Analyte
Blank: Value Q
Units
Q.C. Batch
Lab Number
Analyzed Daielrime
Purgcable Organic Compounds by EPA Method 624
6094724-BLKI
cis-1,2-Dlchloroethene
<0.130
ug/L
6094724
6094724-BLKI
09/27/06 10:59
trans-1,2-Dichloroethene
<0A30
ug/L
6094724
6094724-BLKI
09127/06 10:59
1,1-Dichlomethene
<0.100
ug/L
6094724
6094724-13LKI
09/27/06 10:59
1,2-Dichloroprapane
<0, 150
ug1L
6094724
6094724-BLKI
09/27106 10:59
cis-1.3-Dichloropropene
<0.250
ultfh
6094724
6094724-BLKI
09127/06 t0:59
trans-1,3-Dichloropropene
<0.100
ug1L
6094724
6094724-BLKI
09127/06 t0:59
Ethylbenzcnc
<0.230
ug/L
6094724
6094724-BLKI
09/27/06 10:59
Methylene Chloride
0.970
uglL
6094724
6094724-BLK1
09/27/06 10:59
1.1,42-Tetmchloroethme
<0.[30
ug/L
6094724
6094724-BLKI
09/27/06 10:59
Teirachloructhene
<0.I10
ug/L
6094724
6094724-BLK1
09/27/06 10:59
Toluene
<0.280
ug/L
6094724
6094724-BLK1
09/27/06 10:59
1,1,2-Trichloroethane
<0.240
ue/L
6094724
6094724-BLKI
09/27/06 10:59
1,1,1-Trichloroethane
<0.110
ug/L
6094724
6094724-BLKI
09/27/06 10:59
Triehloroethene
<0.100
ug/L
6094724
6094724-BLKI
09127/06 10:59
Trichlorofluor0methane
<0.120
ug/L
6094724
6094724-BLKI
09/27106 10:59
Vinyl chloride
<0.370
ug/L
6094724
6094724-BLKI
09/27/06 10:59
Xylenes, total
<0.680
ug/L
6094724
6094724-BLKI
09/27/06 10:59
Surrngate: 1,2-Drch1nrae1hanr-d4
95%
6094724
6094724-BLKI
09/27/06 10:59
Surrogate: DibrorrroJluornruerhune
100%
6094724
6094724-BLKI
09/27/06 10:59
SurrqE�ate: Taluene-d8
113%
6094724
6094724-BLKI
09/27106 10:59
Surrugalc: a-Rroniglluarobenzene
108%
6094724
6094724-BLKI
09/27/06 10:59
Acid and Base/Neutral Extractables by EPA llethod 625
6094444-BLKI
Acenapbthene
<2,90
Acenaphthylene
<3V0
Anthraceae
<2.80
BcnZD (a) anthracene
<2.60
Benzo (a) Pyrrne
<2. 80
Bcnzo (b) Iluoranthene
<3.00
Bcnzo (g,h.i) perylene
<2.90
Benzo (k) Fluorantltene
<3,70
4-Brontophenyl phenyl ether
<2,20
Butyl bcnzyk phthalate
<2.70
4-Chloro-3-methylphenol
<2.40
Bis(2-chloroctboxy)methane
<3.40
Bis(2-chloractltyl )cther
< 1.90
Bis(2-ehloroisopropyl)ether
<4.50
2-Chloronaphthalene
<3.00
2-Chloropltenol
<2.00
4-Chlon>phenyl phenyl cuter
<2.50
ug/L
6094444
6094444-BLK1
09/29106 00:28
ug/L
6094444
6094444-131-KI
09129/06 00:28
ug/L
6094444
6094444-BLKI
09129106 0018
ug/L
6094444
6094444-BLKI
09/29/06 00:28
ug/L
6094444
6094444-BLKI
09/29/06 00:28
uglL
6094444
6094444-BLK1
09/29/06 00:28
ug/L
6094444
6094444-BLKI
09/29/06 00:28
ug&
6094444
6094444-BLK 1
09/29/06 00:28
ug/L
6094444
6094444-BLK 1
09/29/06 00:28
ug/L
6094444
6094444-BLK 1
09/29/06 00:29
ug11'
6094444
6094444-BLK I
09/29/06 00:28
ug/L
6094444
6094444-BLK 1
09/29/06 00:28
ug/L
6094444
6094444-BLKI
09/29/06 00:28
ug/L
6094444
6094444-BLK 1
09129/06 00:28
uglL
6094444
6094444-BLK 1
09/29/06 00:28
ug1L
6094444
6094444-BLKI
09/29106 00:28
u(Jl.
6094444
6094444-BLKI
09129106 00:28
Page 10 of24

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 • 800-765-0980' Fax [phone]
Client WRS (3166) Work Order: NPI3179
221 Hobbs Street, Suite 108 Project Name- Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619 Project Number: 106150
AM Gary Acquaro Received: 09/26/06 09:50
PROJECT- QUALITY CONTROL DATA
Blank -Cont.
Analvie Wank Value Q Units Q.C. Batch lab Number Analyzed ➢aterrime
Acid and Base/Neutral Extractables by EPA Method 625
6094444-BLKI
Chrysene
<2.40
"fill.
6094444
6094444-BLKI
09/29/06 00:28
Dibenz(a,h)anthracene
<2,90
ug/L
6094444
6094444-BLKI
09/29/06 00:28
Di-n-butyl phthalate
<2.60
ug/L
6094444
6094444-BLKI
09/29/06 00:28
1,3-Dichlorobenzene
Q,50
ug/L
6094444
6094444-BLKI
09129106 0028
1,4-Diehlorobenzene
<1.70
ug/L
6094444
6094444-BLKI
09129106 M28
1,2-Dichlorobenzene
<1.70
u£JL
6094444
6094444-BLKI
09129/06 00:28
33-Dichlorobenzidine
<2.70
ug1L
6094444
6094444-BLKI
09129/06 W28
2A-Dichlorophenol
<3.10
ug1L
6094444
6094444-BLKI
09129/06 00:28
Diethyl phthalate
<2.60
uglL
6094444
6094444-BLKI
09129106 00:28
2,4-Dimethylphenol
<5.20
ugn,
6094444
6094444-BLKI
09129/06 00:28
Dirnethylphthnlate
<2.40
ugJL
6094444
6094444-BLKI
09/29/06 00:28
4,6-Dinitro-2-medrylphenol
<3.30
teili,
6094444
6094444-BLKI
09/29/06 00:28
2,4-Dinitrophenol
<2.90
ug/L
6094444
6094444-BLKI
09/29/06 00:28
2,6-Dinitmtoluene
<2.80
ug1L
6094444
6094444-BLKI
09/29106 00:29
2,4-Dinitrotoluene
<2.50
ug/L
6094444
6094444-BLKL
09129106 00:28
Di-n-oetyl phthalate
<2.80
ug/L
6094444
6094444-BLKI
09/29/06 00:28
Bis(2-ethylhexyl)phthalate
<3.50
ug/1,
6094444
6094444-BLK1
09/29/06 0028
Fluoranthene
<2.50
ug/L
6094444
6094444-BLKI
09/29/06 00:28
Fluorene
<2.70
ug/l,
6094444
6094444-BLKI
09/29/06 00:28
Hexachlorobenzene
<2.40
1111,
6094444
6094444-BLKI
09/29/06 00:28
Hcxachlorobutadiene
G.20
ug1L
6094444
6094444-BLKI
09129/06 00:28
Hexachlorocyclopentadiene
<5.50
ug1L
6094444
6094444-BLKI
09/29106 00:28
Hexachlorocthane
<1.80
ug/L
6094444
6094444-BI,K1
09129106 00:28
Lndeno(1,2,3-cd)pyrene
<2.90
ug/L
6094444
6094444-BLKI
09/29106 00:28
lsophorone
<2.40
ug/L
6094444
6094444-BLKI
09129106 00:28
Naphthalene
<2.90
ug1L
6094444
6094444-BLKI
09/29/06 00:28
Nitrobenzene
<4.50
ug/L
6094444
6094444-BLK1
09129106 00:28
2-Nitrophenol
<2.50
ug1L
6094444
6094444-BLKI
09129106 00-28
4-Nitrapltenol
<4.50
ug1L
6094444
6094444-BLK1
09/29/06 00:28
N-Nitrosudintethylaptine
<3.70
ug/L
6094444
6094444-BLKI
09129106 00:28
N-Nitrnsodiphenylamine
<3.80
ug/L
6094444
6094444-BLKI
09129/06 00:28
N-Nitrosodi-n-propylatnine
<2.00
ug/L
6094444
6094444-BLKI
09/29/06 00:28
Pentachlorophenol
<:,00
ug/L
6094444
6094444-BLKI
09/29106 00:28
Phcnanihrene
<2.40
ug/L
6094444
6094444-BLKI
09/29/06 0028
Phenol
<4.60
11g/L
6094444
6094444-BLKI
09/29/06 00.28
Pyrene
<2.70
ug/L
6094444
6094444-BLK1
o9129106 0028
1,2,4-Trichlarobenzene
<2.70
ug/L
6094444
6094444-BLK1
09/29/06 00:28
2.4.6-Trichlorophenol
<2.90
ug/L
6094444
6094444-BLKI
09/29/06 00:28
Benziditte
<34.0
ug/L
6094444
6094444-BLKI
09/29/06 00:28
1,2-Diphenylhydrazine
<2.90
ug/L
6094444
6094444-BLKI
09/29/06 00:28
2-Methylnaphthalene
<1.50
ug/L
6094444
6094444-BLK1
09/29/06 00:28
.Srrrru, ale: Tcrphct1yl-d14
88%n
6094444
6094444-BLKI
09/29/06 00:28
Page l 1 of 24

•
TestAmerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 l lobbs Street, Suite 109
'Tampa, FL 33619
Attn Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204 • 800-765-0980 - Fax [phone]D4
Work Order:
NPI3179
Project Name;
Synthron Chemical Fire Site in Morganton, NC
Project Number:
106150
Received:
09/26/06 08:50
PROJF,CT QUALITY CON FROL DATA
Blank - Cant.
Analyze
i3lank Value Q
Units Q.C. Balch
Lab Number
Analyzed DaMrrime
Acid and 13as&Neutral Extractables by EVA Method 625
6094444-BLK1
Surmgule: Z4.6-Trihrotnophennl
81%
6094444
6094444-BLKI
091291D6 00.28
Surmgme: Phenol-d5
32%
6094444
6094444-BLKI
09129106 0028
Surrnguie: 2-Nuumhiphenvl
72%
6094444
6094444-BLK I
09129106 00:28
Surrogate: 2-1,7uoruphenol
42%
6D94444
6094444-BLK 1
09129106 00:28
Surrogate: Mimben_ene-d5
75%
6094444
6094444-BLKI
09/29/06 00:28
Page 12 of 24

0
TestAimerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attu Gary Acquaro
2960 Foster Creighton Road NashAlle, TN 37204 ' 900-765-0980' Fax [phone]
Work Order: NP13179
Project Name: Synthron Chemical Fire Site in Morganton, NC
Project Number- 106150
Received: 09/26/06 08:50
PROJEC"I' QUALITY CONTROL DATA
Duplicate
Sample
Analyzed
Analyse
Orig. Val.
Duplicate Q
Units
RPD
Litnit
Batch
Duplicated
Date/Time
General Chemistry Parameters
6094794-DUP1
BOD - 5 Day
4.99
6.16 R2
rng/L
21
20
6094794
NP13121-05
10/01/06 23:25
6094794-DUP2
BOD - 5 Day
23.1
2.74 R2
mg/L
158
20
6094794
NP13121-06
10/01/06 23:25
6094803-DU P1
Total Suspended Solids
11000
10300
ntgll,
7
20
6094803
NP12997-02
09/26/06 17:44
6094980-DUP1
Chemical Oxygen Demand
131
131
ntg/l,
0
10
6094980
NP13282-02
09/27106 1 1:36
Page 13 of24

w
Testl�-merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204 • 800-765-0980' Fax [phone]
Work Order: NP13179
Project Name: Synthron Chemical Fire Site in Morganton, NC
Project Number: 106150
Received: 09/26/06 08:50
PROJI:C'I' QUALITY CONTROL DATA
LCS
Target
Analyzed
Analyze
.. ........ ..............................
Known Val.
Analyzed Val
......... ....
Q Units
-- .......... ...
% Rec.
. --................
Range
Batch
..... ...
Dateffime
.... ..---
General Chemistry Parameters
6094794-BSI
ROD - 5 Day
198
220
ugtmL
1 11 %
85 - 115
6094794
10/01106 23:25
6094803-BSI
Total Suspended Solids
100
96.0
mg/L.
96%
90 - I l0
609,1803
09/26/06 17:44
6094980-BS1
Chemical Oxygen Demand
20.0
20.7
uglmL
$04%
90- 1 to
6094980
09/27/06 11:36
Total ,,\letals by 1,PA Method 6010B
6094940-BS1
Arsenic
0.0500
OA554
mg1L
l 1 1 %
80 - t 20
6094940
09/28/06 21:36
Barium
2.00
2-13
mg/L
106%
SO- 120
6094940
0912 M 21:36
Cadmium
0.0500
0.0543
mg/L
109%
SO- 120
6044940
09/28106 21:36
Chromium
0.200
0.207
mg1L
104%
80. 120
6094940
09/28/06 21:36
Lead
0.05D0
010485
tng/L
97%
go- 120
6094940
09/28/06 21:36
Selenium
0 W00
0.D557
rnglt.
111%
80. 120
6094940
09/28/06 21:36
Silver
0.0500
0.0547
utg1L
109%
80 - 120
6094940
09/28/06 21:36
,Nlereury by EPA Methods 7470AI7471A
6095002-BS1
hlcrcun
0.00100
0.000933
Ing1L
93%
78 - 124
6095002
09129/06 15:05
Purgeable Organic Compounds by EPA Method 624
6094724-BSI
Acrolein
250
523
L ug/L
209%
19. 196
6094724
09/27/06 10:00
Acrylonitrile
250
207
ug/L
83%
73 - 132
6094724
09/27/06 10:00
Benzene
50.0
45.8
ug/L
92 %
37 - 15l
6094724
09/27/06 10:00
Bromodichloromethatse
50.0
48.2
ugll-
96%
35 - 155
6094724
09/27/06 10:00
Bromoform
50.0
56.2
ug/L
I 12 %
45 - I69
6D94724
09/27/06 10:00
Bromomethane
50.0
52.1
ug1L
104%
1 - 242
6094724
09/27/06 10:00
Carbon Tetrachloride
50.0
46-5
ug1L
93 %
70 -140
6094724
09/27/06 10:00
Clrlorobenzene
50,0
53.5
ug/L
107%
37.16D
6094724
09/27/06 10:00
Cldorodibromomethane
500
66.3
ug/L
133 %
53 - 149
6094724
09/27/06 10:00
Chloroediane
50,0
49D
ug/L
98%
14 - 230
6094724
09/27/06 I0t00
Chlorof)mt
50.0
45.5
ug/L
91%
51- 138
6094724
09127/06 10:00
Chloromethanc
50.0
43.9
%10,
98%
1- 273
6094724
09127/06 10:00
1,2-Dichlorobenzene
50.0
57-t
ug/L
114%
18-190
6094724
09127/06 10-00
1,4-Dichlorobenz-ene
50-0
53.3
uy/L
107%
18 - 190
6094724
09/27/06 10:0e
1,3-Dichlorobenzene
50.0
55.6
ug/L
111 %
59 - l56
6094724
09127/06 10:00
I7ichl0r0dillu0r0methane
50-0
35.3
ug/1-
71%
33 - 142
6094724
09127/06 10:00
1,2-Dichloroethane
50.0
44A
ug1L
88%
49- 155
6094724
09/27/06 10:00
1,1-Dich1oroethane
50-0
45.6
ug/L
91%
59- 153
6094724
09/27/06 10:00
Page 14 of 24

Testl�-merica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 ' 6DO-765-0980' Fax [phone]
Client WRS (3166) Work Order: NP13179
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical fire Site in Morganton, NC
Tampa, Fl. 33619 Project Number: 106150
Attn Gary Acquaro Received: 09/26/06 08:50
PROJECT QUAIATY CONTROL DATA
1.C5 - Cont.
Target
Analyzed
Analyte
Known Val.
Analyzed Val
Q Units
% Rec,
Range
Batch
DaWTirne
Purgeable Organic Compounds by
EPA Method 624
6094724-BS1
cis-1,2-Dichlorcethene
50,0
440
ugn-
88%
54-156
6094724
09/27/06 10:00
trans-l.2-Dichloroethene
50.0
45.2
ug/L
90%
54-156
6094724
09/27/06 10:00
1,1-Dichloroethene
50.0
46.2
ug/L
92 %
1- 234
6094724
09/27/06 10:00
1,2-Dichtoropropane
50.0
43.2
uglL
86%
1 - 210
6094724
09/27/06 t0;00
cis-1.3-D-echloropropene
50.0
55.3
ug/L
111 %
1 - 227
6094724
09127/06 10:00
trans-1,3-Diehloropropene
50.0
57.7
uglL
115 %
17- 183
6094724
09/27/06 [0:00
Bthylbenzene
50.0
52.6
ug/L
105%
37- 162
6094724
09/27/06 10:00
Methylene Chloride
50.0
41.4
ugll-
83 %
1 - 221
6094724
09/27/06 10:00
1,1,2,2-Tetrachlorocthane
50.0
46.0
uglL
92%
46- 157
6094724
09/27/06 10:00
Tetrachluroethene
50.0
52.6
uffL
105%
64- 148
6094724
09/27/06 10:00
Toluene
50.0
52.0
ug/L
104%
47 - 150
6094724
09/27/06 10:00
1,1,2-Triehloroethane
50.0
53.9
ug/L
108%
52- 150
6094724
09/27/06 10:00
1,1,1=1-richlarocthanc
50.0
45.6
ug/L
91%
52 - [62
6094724
09/27106 10:00
Trichloroethene
50.0
52,5
ug/L
105%
71- l57
6094724
09127106 10:00
Trichloroftuarornctlranc
50.0
37.9
ug1L
76%
17-181
6094724
09127/06 10:00
\'invl chloride
50.0
473
ug/L
95%
1- 251
6094724
09/27106 10:00
Xylencs, total
L 50
159
uglL
106 %
SO- 125
6094724
09127106 10;00
Surrogate: 1.2-Dichlormfhaac-d4
30.0
28.6
95%
8 t - 126
6094724
09127/06 10:00
Surrogate: Drbramoflucimmerhane
30.0
30.9
103%
88 - 120
6094724
09/27/06 10:00
Surrogive: Dduene-dR
30.0
3 3.9
113 %
85 - 130
6094724
09/27/06 10:00
Surrogure; 4-13romty1rurrnbenzene
30.0
31.4
105%
80- 124
6094724
09/27/06 ]D;00
Acid and Base/Neutral Estractables by EPA Method 625
6094444-BS1
Acenaphthene
50.0
3T7
ug/L
75 %
47 - 145
6094444
09129/06 00:51
Acenaphthylene
50.0
39.2
ug/L
78%
33- 145
6094444
09129/06 M51
Antlrracene
50,0
45.6
ug/L
91%
27- 133
6D94444
09I291D6 W51
Benzo (a) anthracene
5D.0
45.3
uglL
91%
33, 143
6094444
09129106 00:51
Benzo (a) pyrene
50.0
48.2
ug/L
96 %
17 - 163
6094444
09/29/06 00:51
Benzo (h) fluormthene
50.0
46.5
u61L
93%
24 - 159
6094444
09/29106 00:51
Benzo (g•h,i) perylenc
500
43.0
uglL
86 %
I - 219
6094444
09129/06 00:51
Benzo (k) fluoranthene
50.0
44-2
ug/L
88 %
I I - 162
6094444
09/29106 00:51
4-Bromophenyl phenyl ether
50.0
3U
ugIL
78%
53 - 127
6094444
09129/06 00;51
Butyl henzyl phthalate
50.0
45.6
ug1l.
91 %
1- 152
6094444
09/29/06 00:51
4-Chloro-3-methylphenol
50.0
34.4
ug/L
69%
22-147
6094444
0912910600:51
Bis(2-ehloroethoxy)tnethane
50.0
38.1
ug/L
76%
33 - 184
6094444
09/29/06 00:51
Bis(2-chloi oethyl)ether
50.0
40.4
ug/L
81 %
12 - 158
6094444
09/29/06 00:51
Bis(2-chloroisopropyl)cthcr
50.0
38.1
ug/L
70%
36- 166
6094444
09/29/06 00:51
2-Chloronaphthalene
50,0
34.4
uglL
690/0
60 - 118
6094444
09/29106 00:51
2-Chlomphenol
50,0
34.2
uglL
69%
23 - 134
6094444
09129/06 00:51
4-Chlorophcnyl phenyl ether
50.0
40.2
ugll.
80%
25 - 158
6094444
09/29/06 00:51
Page 15 of24

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 • BOo-765-0980 • Fax [phone]
Client WRS (3166) Work Order: NP13179
221 1lobbs Street, Suite 108 Project Name: Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619 Project Number: 106150
Alto Gary Acquaro Received: 09l26/0608:50
PRO•IF,CT QUALITY CONTROL DATA
LCS - cont.
Target
Analyzed
Analyte
Known Val.
Analyzed Val
Q Units
% Rea
Range
Batch
DatvTime
Acid and Base/Neutral F.xtractables by FPA Method 625
6094444-BS1
Chrysene
SOA
44.1
ug/L
88%
17 - 168
6094444
09/29106 00:51
Dibenz (a,h) anshraeene
50,0
43-4
uglL
87%
l - 227
6094444
09/29/06 00:51
Di-n-6utyl phthalate
50.0
46.4
ug/L
93%
1 - 118
6094444
09/29/06 00:51
1.3-Dic}tlorobenzene
50.0
28.2
u&/L
56%
1- 172
6094444
09/29/06 00:51
1,4-Dichlorobenzene
50.0
27.6
ug/L
55%
20 - 124
6094444
09/29/06 00:51
1,2-Dichlorobenzene
50.5
29.6
ug/L
501.
32. 129
6094444
09/29/06 00:51
3,3'-Dichlorobenzidine
5o,o
44.2
uglL
88%
1 - 262
6094444
09129106 00:51
2,4-Dichlorophenol
50.0
35A
ug1L
71°/a
39-135
6094444
09129106 00:51
Diethyl phthalate
50,0
37,7
uglL
75%
1- 114
6094444
09/29/06 00;51
2,4-Dimethylphenol
50,0
16,0
ug1L
32%
32 - 119
6094444
09/29/06 00:51
Dimethyl phthalate
50,0
26,4
ug/L
53%
1- 1l2
6094444
09/29/06 W51
4,6-Dinino-2-methvlphenol
50.0
47.5
uglL
95%
1- 181
6094444
09/29/06 00:51
2,4-Dinitrophenol
50.0
46.0
ug/L
92%
1- 191
6094444
09/29/06 00:51
2,6-Dinitrololuene
50.0
47.5
ug1L
95%
50- L58
6094444
09129/06 00:51
2,4-Dinilrololuene
50.0
47.6
ug/L
95%
39- 139
6094444
09/29/06 00:51
Di-n-octyl phthalate
50.0
50.6
ug11'
I01 %
4. 146
6094444
09/29/06 00:51
Bis(2-ethylltexyl)phthalate
50.0
45.1
ug/L
90%
8 - 158
6094444
09/29/06 00:51
Fluoranthene
50.0
45.3
ug/L
91 %
26 - 137
6094444
09/29/06 00:51
Fluorene
50.0
40,7
ug/L
81%
59- 121
6094444
09t29106 00:51
tlexachlorobenzene
50.0
44.2
ug/L
88%
1- 152
6094444
09/29/06 00:51
Hexachlorobutadiene
50.0
29.0
ug1L
58%
24- 116
6094444
09/29/06 00:51
Hceachlorocyclopentadiene
50.0
32.4
uglL
65 %
23 - 86
6094444
09/29/06 00:51
Hexachlorocthane
50.0
28.9
ug/L
58%
40 - 113
6094444
09/29/06 00:51
Indeno (1,2,3 -cd) pyrene
50.0
42.6
ug/L
85%
1- 171
6094444
09/29/06 00:51
Isophorone
50.0
40.8
ug/L
829/6
21 - 196
6094444
09/29/06 00:51
Naphthalene
50.0
28-6
ug/L
57%
21 - 133
6094444
09/29/06 00:51
Nitrobenzene
50.0
35.2
ug/L
70%
35 - 180
6094444
09/29/06 00:51
2-Niirophenol
50.0
37.6
ug/L
75%
29. 182
6094444
09/29/06 00:51
4-Nitrophenol
50.0
16-0
uglL
32%
1- 132
6094444
09129/06 00:51
N-Nitrosodimethylamine
50,0
21.0
ug/L
42%
23-69
6094444
09/29/06 00:51
N-Nitrosodiphenylamine
50.0
58-9
L ug/L
118%
42 - 111
6094444
09129ID6 00:51
N-Nitrosodi-n-propylmninc
50.0
42.9
ug/L
86%
1 - 230
6094444
09129/06 W51
Pentachlorophenol
50.0
52.6
ug/L
l05%
14 -176
6094444
09/29106 00:51
Phcnanthrenc
50,0
42.9
ug/L
86%
54 - 120
6094444
09/29/06 00:51
Phenol
50,0
16.3
ug/L
33%
5 - 112
6094444
09/29/06 00:51
Pvrene
50.0
47.0
ug/L
94%
52- 115
6094444
09/29/06 00;51
1,2,4-Trichlombenzcne
50,0
27.0
u f-/L
54%
44 - 142
6094444
09/29/06 00:51
2,4,6=Criclilorophcnol
50.0
42.7
ug/L
85%
37- 144
6094444
09/29/06 00:51
Benzidine
50,0
39.1
ug/L
78%
1- 122
6094444
09/29/06 00:51
1,2-Diphcnylhydrazine
50.0
41.7
ug1L
83 %
47 - 117
6094444
09129106 00:51
2-Methylnaphrhalene
50.0
29.6
ug1L
591/
34 - 110
6094444
0912%06 00:51
Page 16 of 24

Testl�merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
'Pampa, FL 33619
Attn Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204 • 800-765-0980 • Fax [phone]
Work Order;
NP13179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Number:
106150
Received:
09/26/06 08:50
PRO.IEC-1' QUAIATY CONTROL DATA
LCS - Cont.
Target
Analyzed
Analvte
Known Val,
Analyzed Val
Q Units %Rec.
Range
patch
Dateiiime
Acid and Base/Neutral Fxtractables
by EPA Method 625
6094444-BSI
SurroSnre''1'erphem•l-dl4
50.2
43.7
87%
34-116
6W)4444
09/29/06 00;51
.Swrogare:2.4,h-Trihramophennl
50.2
42.6
85%
16-130
6094444
09/29/06 00:51
Surmt!ure: Phenol-0
50.2
14,2
28%
10-66
6094444
09/29106 00:51
.Surmgufe. 2-1-lunmbiphenyl
50.2
38.6
771/6
32 - 99
6094444
09/29/06 00:51
.Surrogare: 2-1.71uomph nol
50.2
19.4
391%
10 - 81
6094444
09/29/06 00:51
.Surmgure: Nlrrohen_ene-di
50.2
363
72%
19 - I t6
6094444
09129106 00:51
Page 17 of 24

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 ' ODO-765-0980' Fax [phone]
Client WRS (3166) Work Order: NP13179
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619 Project Number: 106150
Attit Gary Acquaro Received: 09/26/06 08:50
PROJECT QUALITY CONTROL DATA
LCS Dup
Spike Target Sample Analyzed
Analyze Orig. Val. Duplicate Q Units Cone % Ree. Range RPD Limit Batch Duplicated Daterrime
General Chemistry Parameters
6094803-BSD1
Total Suspended Solids
Total Metals by EPA Method 601013
6094940-BSD1
Arsenic
Raritan
Cadmium
Chromium
Lead
Selenium
Silver
97.0 mglL I DD 97°% W - I ID 1 20 6094803 09/26106 17:44
0,0501
mglL
0-0500
1W10
80 - 120
10
20
6094940
09/28/06 21:41
2.05
mglL
2.00
102%
80-120
4
20
6094940
09l281o6
21-41
0,0521
mg]L
0.0500
104%
go- 120
4
20
6094940
09/28/06
21:41
0.199
mg/L
0 2D0
99%
SO • 120
4
20
6094940
0912SM
21:41
0.0465
mg1L
0,05DO
93 %
SO- 120
4
20
6094940
09/28/06
21 Al
0.0543
mc/L
0.05D0
109%
SO- 120
3
20
6094940
09/28106
21:41
0.0511
ingll.
0.05D0
102 %
SO- 120
7
20
6094940
09/28/06
21:41
Acid and Base/Neutral Extractables by EPA Method 625
6094444-BSDI
Acenaphthenc
5.96
Acenaphthylene
6.03
Anthracene
7.12
Benzo (a) anthmcene
6,56
Benzo (a) pyrcnc
6,82
Benzo (b) fluoranthene
6,87
Renzo (g,hJ) perylene
6,08
Benzo (k) fluoranthene
693
4-13tomophenyl phenyl ether
5,98
Bulyl beazyl phthalatc
698
4-Chloro-3-methylphenot-
6.00
Bis(2-chloroe1hoxy)methane
7.77
Bis(2-chtoroethyl)ether
7.19
B is(2 -ch1 oroisopropyl)eth er
6.39
2-Chlornnaplrthalcne
5.42
2-Chlorophenol
5.67
4-Chlorophenyl phenyl ether
6.53
Chrysene
6.99
Dibenz (n,h) anthracene
6.20
Di-n-butyl phthalatc
7,08
1,3-Dichlorobenzene
3.68
1,4-Dichlumben T.cae
3.72
1,2-Dichlorobenzene
4.24
3,3'-Dichloroben7idine
6.69
2,4-Dichlorophenol
5.89
Diethyl phthalatc
6.41
2,4-Dimethylphenel
ND
L2, R2
ug/L
Soo
12%
47 - 145
145
41
6094444
09/29/06 Ot:13
L2, R2
upJL
50.0
12%
33- l45
147
33
6094444
09/29/06 01:13
L2, R2
ugrL
100
l4%
27 - 133
146
38
6094444
09/29/06 01:13
L2, R2
ug/L
50.0
13%
33- 143
149
35
6094444
091291D6 01:13
L2, R2
uglL
50,0
14°%
17 - 163
150
37
6094444
09129/06 01:13
L2, R2
ug/L
500
14%
24 - 159
149
37
6094444
09/29/06 01:13
L2, R2
uLlL
50.0
12°0
1 - 219
150
36
6094444
09/29/06 01:13
L2, R2
ug/L
50.0
14%
I l - 162
146
40
6094444
09129106 01 -l3
L2, R2
uglL
50-0
12%
53 - 127
147
35
6094444
09/29/06 01:13
L2. R2
ue![,
50.0
14%
1- 152
147
37 ,
6094444
09/29/06 01:13
L2, R2
urJL
50,0
)2%
22 - 147
141
38
6094444
09/29/06 01:13
L2, R2
ug/L,
50,0
16%
33 - 184
132
34
6094444
09/29/06 01:13
L2, R2
ug/L
50,o
14%
12 - 158
140
44
6094444
09129/06 01:13
1,2, R2
ugJL
50.0
13%
36 - 166
l43
40
6094444
09l29% 01:13
L2, R2
ug/L
50.0
ll%
60- 118
146
41
6094444
09/79/06 01:13
L2, R2
ug/L
50.0
l I%
23 - 134
143
59
6094444
09/29/06 01:13
t,2, R2
ug1L
50 0
13%
25 - 158
144
38
6094444
09/29/06 01:13
L2, R2
ug1L
50.0
14%
17 - 168
145
35
6094444
09/29106 01:13
1-2, R2
ug/L
50-0
12%
1 - 227
150
41
6094444
09/29/06 01:13
L2, R2
ugll.
500
14%
l - 118
147
M
6094444
09/291D6 01:13
42, R2
ug/L
50.0
7°%
l - 172
154
55
0094444
09/29/06 01:13
L2- R2
ug/1,
50.0
7 %
20- 124
152
57
6094444
09/29/06 0113
L2, R2
ug/L
50.5
8%
32 - 129
150
55
6094444
09129106 OL 13
L2, R2
ug/L
50.0
G %
1 - 262
147
44
6094444
09/29/06 01:l3
L2,R2
ug1L
500
12%
39-135
143
57
6094444
09/29/06 01-.13
L2, R2
ueJL
50.0
13%
I - 114
142
38
6094444
09129fo6 01:13
L2
ug/L
50.0
0 %
32 - 111.)
73
6094444
09/29/06 01:13
Page 18 of24

r11rqAU!:!hstAmerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Ann Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204 • 800-765-0980' Fax [phone]D4
Work Order:
NP13179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Number:
IU6150
Received:
09/26/06 08:50
PROJECT QUALITY CONTROL, DATA
LCS Dup - Cont,
Spike Target Sample Analyzed
Analyze Orig. Val. Duplicate Q Units Conc % Rec, Range RPD Limit Batch Duplicated Date/Tirne
Acid and Base/Neutral Estractables by EPA Method 625
6094444-BSDI
Dimethyl phthalate
4.65
4,6-Di nitro-2-methylphenol
4.37
2,4-Dinitrophenol
3.86
? 6-DiniWoluene
7.03
2,4-Dinitmtoluene
7.22
Di-n-octyl phthalale
6.85
Bis(2-ethvlhexyl)phthala1e
7.24
Finertmthene
6.78
Fluorene
7.11
Hesachlorohenzene
6.52
Hesachlorobutadiene
4.68
Hexachlorocyclapentadiene
ND
Heaachloroethane
4,32
]ndeno (1,2,3-cd) pyrene
6,22
Isophorone
8,37
Naphthalene
4.56
Nitrobenzene
7.01
2-Nitrophenol
5,97
4-Nitrophenol
ND
N-Nitrosodimeftlatuine
4.08
N-Nitrosodiphenylamine
IIA
N-Nilrosodi-n-propyl nmi nc
8.85
Pentachlorophenol
SA6
Phenmrthrette
6, 83
phenol
ND
pwene
7.19
1,2.4-Trichlorobenzene
4.26
2,4,6= rrichlorophenol
6.36
Beaaidine
ND
1,2-Diphenylhydrazine
7.65
2-Mctltyluaphthalene
5,29
Surrogate. Terpheoyl-d14
6.82
.5'0rrnl;are: 2,4,6-Tribromophenol
5,76
sur"' a w Phen"1,15
2.38
Surrapale: 2-Muorahiphertyl
6.19
,Surrogate: 2-Fluoralthenal
314
Surmgale: Nirrohcwene,15
7.26
1.2, R2
ug/L
Soo
9%
1 - 112
140
36
6094444
09/29106 01:13
1.2, R2
ug/L
50.0
9%
1- 181
166
59
6094444
09/29/06 01:13
L2, R2
ug/L
50.0
8%
1- 191
169
35
0094444
09/29/06 01:13
L2, R2
uglL
50.0
14%
50- 158
148
40
6094444
09/29/06 01:13
L2, R2
ugJL
50.0
14%
39 - 139
147
36
6094444
09/29/06 01:13
L2, R2
ug/L
50.0
14%
4 - 146
152
44
6094444
09/29/06 0113
L2, R2
ug/L
500
14%
8 - 158
145
37
6094444
09129/06 01:13
1,2, R2
ug/L
500
14%
26 - 137
148
34
6094444
09129/06 01:13
L2, R2
ug/L
Soo
14%
59- 121
141
36
6D94444
09129/06 01:13
1.2, R2
ug/L
500
13%
1- 152
149
34
6094444
09129/06 01:13
L2. R2
uglL
500
9%
24 - 116
144
55
6094444
09/29/06 01-13
L2
ug/L
50.0
0%
23 - 86
55
6094444
09/29106 01:13
1.2, R2
ug/L
50.0
9%
40 - 113
148
59
6094444
09/29/06 0 L l3
L2, R2
ug/L
50.0
12%
1- 171
149
41
6094444
09/29/06 01:13
1.2, R2
uglL
50.0
17%
21 - 196
132
33
6094444
09/29106 01A3
L2, R2
uglL
500
9a/
21 - 133
145
44
6094444
09/29/06 01:13
L2. R2
ug/L
50.0
14%
35- 180
134
35
6094444
09129/06 01a3
[.2, R2
ug1L
500
12%
29 - 182
145
55
6094444
09/29106 01:13
L2
ug/L
Soo
0%
1- 132
48
6094444
09/29106 01-13
I.2, R2
ug/L
5D.O
8 %
23 - 69
135
51
6094444
09/29106 01:13
L2, R2
ug/L
50.0
22%
42 - ] I]
137
32
6094444
09/29/06 01:13
TA, R2
ug/L
50,0
18%
l - 230
131
47
6094444
09/29/06 01-13
L2, R2
ug/L
500
11%
14 - 176
162
47
6094444
09/29/06 01:13
L2. R2
ug/L
50.0
14%
54 - 120
145
39
6094444
09/29/06 01:13
L2
ug/L
50.0
0%
5 - 112
54
6094444
09/29/06 01:13
L2, R2
ug l-
50.0
14%
52 - 115
147
35
6094444
09/29/06 01:13
t-2, R2
11g1l.
50,0
9%
44- 142
145
50
6094444
09/29/06 01-13
L2, R2
ug/L
50.0
13%
37 - 144
] 48
62
6094444
09/29/06 01.13
L2
ug1L
SOn
0%
1- 122
85
6094444
o9129106 DI:13
1-2. R2
ug1L
50.0
15%
47- 117
139
36
6094444
09129106 OP13
I.2, R2
ug/L
500
11%
34- 110
139
41
6094444
09/29106 0L13
Z6
ug/L
50.2
14%
34 - 116
6094444
09/29/06 01:13
Z6
ug/L
502
11%
16 - 130
6094444
09/29106 01:13
Z6
ug/L
50.2
5%
10 - 66
6094444
09129/06 01: I3
Z6
ug/L
50.2
12%
32 - 99
6094444
09129/06 01:13
Z6
ug/L
50.2
6 %
10 - 81
6094444
09129106 01:13
Z6
ug/L
50.2
14%
l9- 116
6094444
09129/06 01:13
Page 19 of 24

Testl�merica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Attn Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980 *Fax [phone]
Work Order:
NP13179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Number-
106150
Received:
09/26/06 08:50
PROJECTQUALITY CONTROL DATA
Matrix Spike
Target Sample Analyzed
Analyle Orig. Val. MS Val Q Units Spike Cone %Rcc. Range Batch Spiked Date/Time
......................................................... ... .....................-'--'-'--'----..--.-.------------ -------•----------'-
General Chemistry Parameter
6094980-MS1
Chemical Oxygen Demand 4,10 53.1 ughnf. 50.0 99% 90 - 110 6094980 N1113072-01 09/27/06 11:36
Total Metals by EPA Method 6010E
6094940-MS1
Arsenic
ND
0.0502
mglL
0.0500
1DO%
75 - 125
6094940
NP13129.14
09/28106 21:50
Barium
0.0522
2,10
mg1L
2.00
102%
75- 125
6094940
NP13129-14
09/28/06 21:50
Cadmium
0.00140
0.0519
mglL
0.0500
101 %
75 - 125
6094940
NP13129-14
09/28/06 21:50
Chromium
0.00580
0.199
mg1L
0.200
97%
75- 125
6094940 .
NP13129-14
09/28/06 21750
Lead
ND
0.0471
mg1L
0.0500
94%
75- 125
6094940
NP13129-14
091281D6 21:50
Selenium
ND
0.0510
mg/L
00500
102%
75. 125
6094940
NP13129-14
09128106 2L50
Silver
D.0052D
0,0543
mg1L
0.0500
98%
75- 125
6094940
N1113129.14
09/28/06 21:50
Mercury by EPA INIclhods 7470A/7471A
6095002-MS1
Mcrcury ND
Purgeable Organic Compounds by EPA Nlelhod 624
6094724-M S 1
Acrolein
ND
Acrylonitrile
ND
Benzene
ND
Bromodichloromethane
ND
BrOmutarnt
ND
Bromomethane
ND
Carbon Tetrachloride
ND
Chlorobenzcne
ND
Chlorodibromomethane
N D
Chloroethane
ND
Chlorot'01111
ND
Chloromethane
ND
1,2-I)ichlombenzene
ND
t.4-Dichlorohenzene
ND
1,3-DichlaroN-,nzenc
ND
Dicltl orodi Il unrornellime
ND
1,2-Dichloroethane
N D
1 J-Dichlomethanc
ND
cis- 1,2-Dichloroethcne
0.670
trans- l,2-Dichloroethene
ND
0.00103 mg1L oMl00 103% 63 - 138 6095002 NP13571-04 09/29/06 16:08
193
ug1L
250
73%
19- 196
6094724
NP13162-02
09127/06 20:17
207
ug/L
250
83 %
73 - 132
6094724
NP13162-02
09/27/06 20:17
46.0
ug/L
50.0
92%
37 - 151
6094724
NP13162-02
09/27/06 20:17
48.4
ug/L
50.0
97%
35 - 155
6094724
NP13162-02
09/27/06 20:17
52.6
ug/L
50.0
105%
45 - 169
0094724
NP13162-02
09/27/06 20:17
53.4
ug/L
50.0
107%
1 - 242
6094724
NP13162-02
09/27/06 20:17
50-2
ug/L
50.0
100%
70-140
6094724
NP13162-D2
0912710620:17
53.3
uglL
50.0
107 %
37 - 160
6094724
Nil] 3162-02
09/27/06 20:17
W6
ugJL
SRO
121 %
53 - 149
6094724
NP13162-02
09/27106 20:17
52.2
ug/L
50.0
104 %
14 - 230
6094724
NP13162-02
09127/06 20:17
45.6
ug/L
50.0
91 %
51 - 138
6094724
NPI3162-02
09/27/06 20; l7
510
ug/L
50.0
102%
1 - 273
6094724
NP13162-02
09127106 20717
55.1
ug/L
50.0
110%
18. 190
6094724
NP13162-02
09/27/06 20:17
52.3
ug/L
50,0
105%
IS- I
6094724
NP13162-02
09/27/06 20:17
54.7
ug/L
50.0
109%
59- 156
6094724
NP13162-02
09/27/06 20:17
47.5
ug/L
500
95 %
33 - 142
6094724
NP13162-02
09/27/06 20:17
43.2
uvJL
50.0
86%
49-155
6094724
NP13162-02
09/27106 20:17
45.7
ugJL
50.0
911/a
59-155
6094724
NP13t62-02
09/27/06 20:17
45.8
ug/L
50.0
90%
54 - l56
6094724
NP13162-D2
09127l06 20:17
46.6
ug/L
50.0
93%
54-156
6094724
NP13162-02
09127106 20:t7
Page 20 of 24

TestAmerica
ANALYTICAL TESTING CORPORATION
Client WRS (3166)
221 l lobbs Street, Suite 109
Tampa, FL 33619
Ann Gary Acquar0
2960 Foster Creighton Road Nashville, TN 37204' 800-765-0980' Fax [phone]D4
Work- Order:
NPI3179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Number:
106150
Received:
09/26/06 08:50
PRO.IF,CT QUALITY CONTROL DATA
Matrix Spike - Conti.
TargetSample
Analyzed
Analyte
Orig. Val.
NIS Val Q
Units
Spike Cone
%Ree.
Range
Batch
Spiked
Dwerimc
Purgeable Organic Compounds by EPA Xlethod 624
6094724-MS1
I,1-Dichloroethene
ND
50,9
ug/L
50.0
102%
]- 234
6094724
NPI3162-02
09/27106 20:17
1,2-Dichloropropane
ND
44.7
ug/L
50.0
89%
1 - 210
6094724
NP13162-02
09/27/06 20:17
cis- 1,3 -Dichloropropene -
ND
54.0
ug1L
50.0
108%
1- 227
6094724
NP13162-02
09/27/06 20:17
trans-1,3-Diehloropropc-
ND
56.4
ug/L
Sob
113%
17- 183
609.1724
NPI3162-02
09/27/06 20:17
Ethy[henzene
ND
52.3
ug/L
50.0
105%
37 - 162
6094724
NP13162-02
09/27/06 20:17
Methylene Chloride
ND
41.3
ug/L
50.0
83%
1 - 221
6094724
NPI3162-02
09/27/06 20:17
1,1.2,2-Tcnachloroethane
ND
50.5
ug/L
50.0
101%
46. 157
6094724
NP13162-02
09/27/06 20:17
Tetrachlomethene
ND
54.8
ug/L
50.0
1 10%
64 - 148
6094724
NI113162-02
09127l06 20:17
Toluene
0.0800
51.2
uy)L
50.0
102%
47- 150
6094724
NP13162-02
09127/06 20:17
1.1,2-Trichlorocthane
ND
51.1J
ug/L
50.0
102%
52- 150
6094724
NPI3162-02
09127/06 20:17
I,t,l-Trichlomethane
ND
48.3
ug/L
50.0
97%
52-162
6094724
NP13162-02
09127/06 20:17
Trichloroethene
ND
49.5
ug11.
50.0
990/
71 - 157
6094724
NP13162-02
09127106 20A7
Trichlorofluoromethanc
ND
49.4
ug/L
50.0
991/
17- 181
6094724
N110162-02
09/27/06 20:17
Vinyl chloride
ND
53.9
ugfL
50.0
108%
1 - 251
6094724
NP[3162-02
09/27/06 20:17
Xylenes, total
ND
160
ug/L
150
107%
80 - 125
6094724
NPU 162-02
09/27/06 20:17
,Surragzrw. 1,3-1J±eh1oroethanc-d4
289
ug/L
30.0
96%
81 - 126
6094724
NP13162-02
09/27/06 20:17
Surmgase: Dibrnm<Jruornmedbane
3 L5
ug/L
30.0
105%
88 - 120
6094724
NPI3162-02
09/27/06 20:17
6'urmgatc: Toluene-dS
33.4
ug/L
30.0
111
85 - 130
6094724
NPI3 162-02
09/27/06 20:17
.15rrrc��uti•: 4-HromgJ1uorobenzene
30.0
ug/L
30,0
100%
SO- 124
6094724
NP13 162-02
09/27/06 20:17
Page 21 of 24

r
Testl�-merica
ANALYT1CAL TESTING CORPORATION
Client WRS (3166)
221 Hobbs Street, Suite 108
Tampa, FL 33619
Ann Gary Acquaro
2960 Foster Creighton Road Nashville, TN 37204 • 800-765-0980 • Fax [phone]
Work Order;
NP13179
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Project Number:
106150
Received:
09/26/06 08:50
PROJECT QUALI.1-Y CONTROL DATA
Malrix Spike Dup
Spike Target Sample Analyzed
Analyte Orig Val. Duplicate Q Uvits Cone %Rec, Range RPD Limit Batch Duplicated Dalerrirne
General Chemistry Parameters
6094980-MSD1
Chemical Oxygen Demand 4.1D 52.5 uglmL 50.0 97% 90- 110 1 10 6094980 NP13072-01 09/27/06 11:36
Total Metals by EPA ,Method 6010B
6094940-MSD1
Arsenic
ND
0.0543
mg1L
0.0500
109%
75-125
8
20
6094940
NP13129.14
09/28106 21:54
Barium
0.0522
207
mglL
2.00
101%
75-125
1
20
6094940
NP13129-14
09/28/06 21:54
Cadmium
0.00140
0.0517
mg1L
00500
l0l%
75 - 125
0.4
20
6094940
NP33129-14
09/28/06 21:54
Chromium
0,00580
0,199
mg/L.
0.200
96%
75-125
0.5
20
609494D
NP13129-14
09128106 21:54
Lead
ND
0.0450
mglL
00500
90%
75-125
5
20
6094940
NP13129-14
09/28/06 21:54
Selenium
ND
0.0510
mg1L
0.0500
102%
75 - 125
0
20
6094940
NP13t29.14
09/28l06 21:54
Silver
0.00520
0.0543
mglL
0,0100
99%
75 - 125
0
20
6094940
NN3129-14
09/28106 21:54
Mercury by EPA Methods 7470A/7471A
6095002-MSDI
Mercury ND 0.00107 mg/L 0.DO100 107% 63 - 138 4 22 6095002 NP13571-04 09/29/06 1616
Page 22 of 24

Testl�.merica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204' 600-765-0980' Fax [phone]
Client WRS (3166)
Work Order:
NP13179
221 I lobbs Street, Suite
108
Project Name:
Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619
Project Number
106150
Attn Gary Acquaro
Received:
09/26/0608.50
Cl,RTIhICATION SUMMARN'
TestAmerica - Nashville, TN
Method
Matrix
A114A
Nelac
North Carolina
EPA 160.2
..
Water
NIA
X
X
EPA 405.1
Water
NIA
X
X
EPA 410A
Water
NIA
X
X
EPA 624
Water
N/A
X
X
EPA 625
Water
NIA
X
X
SW8466010B
Water
NIA
X
X
SW846 7470A
Water
NIA
X
X
Page 23 of 24

TestAimerica
ANALYTICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville, TN 37204 • 800-765.0980' Fax [phone]
Client WRS (3166) Work Order: NP13179
221 Hobbs Street, Suite 108 Project Name: Synthron Chemical Fire Site in Morganton, NC
Tampa, FL 33619 Project Number: 106150
Arm Gary Acquaro Received: 09/26/06 09:50
DATA QUALIFIERS AND DEFINITIONS
11 Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the acceptance limits. Analyte not
detected, data not impacted.
1,2 Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery vvas below acceptance limits.
R2 The RPD exceeded the acceptance limit.
Z6 Surrogate recovery was below acceptance limits.
METHOD MODIFICATIONNOTES
COD 410.4 M - M = COD method modified for use of Hach method 8000.
Page 24 of 24

• 10/09/06 23:59 10/09/06 2159
TestAmer�l�a 1
ANALYflCAI TE5TING CORPORATlOM
Nashvillee-Diyision
COOLER RECEIPT FORM BC#
NP13179
Cooler Received/Opened On 09/26/06 0850 /1c�
I. Indicate the Alrblll Tracking Number (last 4 digits for Fedes only) and Name of Courier below:_ 7
ed-Ex UPS Velocfty DHL Route Off-street Misc.
r-
2. Temp erature epresentativesample ortemperature blank when opened: DQgCQQS CQ�51[1S
(indicate IR Gun ID#) .
NA A00466 A00750' A01124 100190 101282 Rsynger SI
3. Were custody scale on outside of cooler?......
a. If yes, how many and where:_ _ L � -
4. Were the seals intact. signed, and dated correctly? ................................................. :........... YES... . NA
S. Were custody papers inside cooler7....... '.................................. .............................. ....... .. 0S.... NO A
I certify that�ened the cooler and as awered questions 1-5 (intlal) ...............................................6. Were custody seals on containers: YES 9 and Intact YES NO
were these signed, end dated -correctly? ....... ............ ................................... YES ... NO...�
-7. What kind of packing material used? B brews - Peanuts Vermiculite Foam Insert
Plastic bag Paper Other None
8. Cooling process: Ice -pack Ice (direct contact) Dry ice Other None
9. Did ail containers arrive'In good condition (unbroken)?............................................................. ... NO ... NA
10. Were all container labels complete (#, date, signed, pres., etc)? ............................................ (7)S... NO ... NA
11. Did all container labels and tags agree with custody papers? ................................................ �... NO...NA
12, a. Were VOA vials received?...................................................................................... 1 ...NO...NA
b: Was there any observable head space present in any VOA vial? ................................. ............. YES......NA
I cer-f!a that I unload cd the cooler and answered questions 6-12(intial)................... I .......
...........
13. a: On preserved bottles did the plI test strips suggest that preservation reached the correct pH level? NO ... NA
b. Did the bottle labels indicate that the correct preservatives were used ...................... �.NO... NA
If preservation in-house was needed, record standard ID of preservative used here
14, Was residual chlorine present?............................................................................. ... YES ... 610... NA
I certify that I checked far chlorine and pH as per SOP and answered questions 13--JA (intlal)......
15. Were custody papers properly tilled out (ink, signed, etc)? .................................................
ff5.... NO ... NA
16. Did you sign the custody papers in the appropriate place? .................................................
YV ....NO ... NA
17. Were correct containers used for the analysis requested? ....................... I...........................
...NO...NA
18, .Was sulllcient amount of sample sent In each container? ....................................... :.............
f�s... NO ... NA
I ceMfy that I entered this protect into LIMS and answered questions 15-18 (lntial) ............... _Mai
I -certify that I attached a label with the unique LINTS number to each container (ink ...................
Ohl
19. Were there Non -Conformance issues at login YES Jeri) Was a PIPE generated YES NO #
BIS - Broken in shipment ��//
Cooler Receipt Form LF-I Revised 319/06
End of Form

TesUAmerica
ANALYTICAL TESTING CORPORATION
Client Neme W R5 Client#: 3 6 C
Address: ZZ It Hc66 &1 . Sc„f e. !a _
C41Slat&Zp Code: q rntp q_ . �L 3 3!r J 4
Project Manager: <37-Mb gart`, g6 r7
Telephone Number: $Z GI Y&P c/&gg- Fax:
To esslst us In using the propel analytical methods,
is this work being conducted for Regulatory, purposes?
Compliance Monitoring A/r~ ssi-*rjL
Project Name: 0S 15r,4- fit? to I -
Project#: 10616-a
Site/Location ID: %?ergo» State: Al L-
Report To: S Sec. &--1 cd
Sampler Name: (Print Name) GA C4 or AiZO Invoice To: W R S
Sampler Signature: Quote M PO#: 7 S 44� ?, S'
I Matrix Presarvadon & # of C taineral
a Analyze For:
TAT
Standard
>a 12
3 -6 s
n s
Lead row PA eotoi None
k Rush (surcharges may apply)
r
y H Se/eR/urn rora) Mercury Level 2
Fp4
Q 0 ,-rA L
fR
€
` 6 SilVer r� (Batch QC)
Data Needed: is. -GC
a �'
V. 4 ° m f" hip13 q Level
a) T
s
N F — Level 4
Fax Results: Y
c
Q y r7
T N Other:
v�
rn
E.2
ffi
SAMPLE ID
p
z
1
N
S REMARKS
sWF RzSaC.
14.znr
1 oo
Q
wLo
f
.3
11
1
131
Vfi
31 A-r
SWAJF- S zSo
CL •zs
)
Spacial instructions: �Mes: �1 2S4tfy .�/e7 Y
�q��4gRctC wrsie.cor�
LABORATORY COMMENTS:
Init Lab Temp:
ck> 7- L
Rec Lab Temp:
t,,yaG
Reli ulshed�!
Date:
Time.
Received
Date:
Time:
Custody Seals: Y N N/A
Bottles Supplied by Test America: Y N
Method of Shipment:
Red ulshed
Date:
Time;
Received
Date:
Time:
Relinquished By:
Date:
Time:
(, o
R -! ZC G 9=L�e;
Time;