NCS000336_MONITORING INFO_20180731

µ-- STORMWATER-DIVISION-CODING-SHEET-'-T-��
PERMIT NO.
N C S ��
DOC TYPE
❑ FINAL PERMIT
9 MONITORING INFO
❑ APPLICATION
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DOC DATE
❑ 0�0 701 3 j
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sroMMWATCR DOCHARGR OUIFALL (SDO)
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RECEIVED
MAR 2 2 Wa
CENTRAL FILES
DWR SECTION'
Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
February 26, 2018
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000336) for the month of February, 2018 for Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was outside the benchmark value for Zinc. Sample results
will be submitted as a representative rain event occurs for the month of March until three consecutive
below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Zinc Sampling
Lot Number:TB19028
Date Completed:02/2612018
02/28/2018 10:59 AM
Approved and released by:
Project Manager: Kelly M. Nance
� 1 /
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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheelylab.com
Page I of 8

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: TB19028
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Shealy Environmental Services, Inc.
1 OB Vantage Point Drive west Columbia, SC 29172 [phone] Fax [phone] www.shealyleb.com
Page 2 of 8

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: TB19028
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO#2 Shipping/Receiving Aqueous 02/04/2018 0942 02/19/2018
(1 sample)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 8

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Rohm And Haas Company
Lot Number: TB19028
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SDO#2 Shipping/Receiving Aqueous Zinc 200.8 63 ug/L 5
(1 detection)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 8

ICP-MS
Client: Rohm And Haas Company Laboratory ID: TB19028-001
Description: SDO#2 Shipping/Receiving Matrix: Aqueous
Date Sampled:0210412018 0942
Date Received: 0211912018
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 02/22/2018 1945 BNW 02/21/2018 1855 65012
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Zinc 7440-66-6 200.8 63 10 ug/L 1
LOQ - Limit of Quantitation 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOO N - Recovery Is out o! criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W a Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab,com
Page 5 of 8

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,sheelylab.com
Page 6 of 8

s
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CWA ! NPDES
Chain of Custody Record
Shealy EnAronmental Services, Inc.
106 yardage ftini Drive
West Columbia. South Carolina 29172
Telophone No. 8Q3-791-9700 Fax No. 803-791-9111
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Number 46749
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Note: All snnlpWo are retained for tear weeks from Lr6
— rwOlpt unlees other armngwmnts are made. aid
USE ONLY
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SHEALY ENVIRONMENTAL SERVICES, INC.
Slimly Envitttuert -MW 3uraum, In.
D=zuuhd Number: AihXll AC-12
raw Iu(I
1311 -mDisk:Ir:X'AT)IS
Sample receipt Checklist (SRC)
Clicttt: loQgf- 11hu Gaoler lnsimted byAnte: � _i� H ; _-.� - � Lot k: :zil Csaa
Mcuns of mceipt: Pf Sl_S1 . Client C1 UPS 0 Fediix El Other.
_ Y95
To
1. Were cnstrxiy scaly prexcnt an the c:ovlLe
Yesl
7 Nu ',JVAJF
If custad 2 seals were pment, wem they iamm and unbroken?
pIi Strip ID: 17- A .,,-,,,,,,,, Chlurint: Strip W:
Cooler I'D i Original temperature upon recoeipt i Dcrival (C omctcd) wmperauue upon receipt:
I "2. C ?_? °C r 1 -C _i I °C
Mclhucl: G etnperature Blank Lftainut EkAdcs 1R Chun ID: �,_ IR Gun Correction Factor, 0 1C
NMethod of coolant: 0'wat ice C1 too Yt:cl:s 0 D%.Lv 0 Narm
[J Yes
❑ NJ
-
3. If tempemturc of any cooler exceeded 6.0'C, was Project Manager Nt:tificd?
PM was No lifted by: phone i email i taoe-m-face (circle one).
I Ycx
No
A
4. Isthe commemial enuriar's packing slip al(ar:hed ru this funn?
es
I _ N
5. Wcm pro cr custody prourdurna (relinyuialne&receiveed) Wllowed?
at,
G. Wero Rumple TIN lit;ted an the COC?
Yies
771 Na
17. Wem sonpic HN listed all all sample contalttets?
71'y—es
ID tiia
B. WUN collection dub.3k times li-avd on die COC?
Ycs
'_: No
9. Was collection dated; time linted on all %arn le cattlainers7
Pryes
l,_i No
10, Did all container libel information (11), tune, time) ggrcc with the C-0C?
Yes
❑ No
11. Wcre Delta la, im perfurmvd listed on the COC?
Yea
No
12. Did all samples arrive in the proper containers Per each test and?or in goat rendition
(unbroken,lidson,etc,)? , .._.
Yus
Nu
M Was adequate Rumple volume available?
Yes
? 2 No
14. WeYe all samples received uilhin ti the holding lime or d$ ]torus. whichever comes Firs?
VJ Yet
Na
15. Were any samples Wntainu" mixainkVt:X :t5y (circle one) samples Not listed on c.y')0
❑ Ycs
❑ Pep
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16, For VOA and RSK-173 sample ,were laubblas present •�"pea-siu" (Ya''vr 6nun ies ditune:er) lit
any of the V O A vials?
es
No
+ N A
17. Writ all DRO'meraWrtutrient samples tmeivcci al a H nf< 2?
Yos
( Nu
A
18. Were a IJ cyanide sarnplim received at a pl l .- l2 r►rxl aulCdr: sarrtplcs ti i��ccf at a H > 97
❑ Yos
❑ No
T-KA
19 Were a app ice c v Nywi c+p uu r (< . rug+ ) saniple9 teoe of rest ual
ehlurine?
❑ Yac
:
1Vo
A20.WcroclientnrmarkWicqueityiix,
requested dilutions, bt-Sir1SDdesignntinns;etc.•,)
carrwetly htrnwribW Nan Ores COC into ilia continent section in LUMS?
Its
Q1
171, was the Tulle number used taken ftrn the container la11 7
Saruple li'reeervatlon (Muth be completcsd far any samp)c(x) incorrectly prcxervetl ur with headspace)
Sumplu(s) were received incorrectly pree semi and were adjursted accordingly
in Sample Jfteiving Wills (11-2SO , HNO,, HGI, NnOH) using SR A
Time of perservation
Sxtnplc�s) were receiver] with bubbles N6 I= in diameter,
>3arrrplC4(e1) Were received with TRC y 0.5 mel. (1f #19 iv nn) and were
odlLoted accordingly in sample iweiving with sodium 11uosu to (N&'S Qn) With 5hettly ID:
SR. ltart ntie labels spelled by, Date: _
Cmrnenls:
Shealy Environmental Services, Inc.
108 Vantage Point drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 8

RECEIVED
MAR 2 2 20% Rohm and Haas
CENTRAL FILES 6101 Orr Road
DWR SECTION Charlotte, NC 28213
[phone]
March 7, 2018
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000336) for the month of March, 2018 for Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier Il requirements in
permit. The sample result at outfall SDO-002 was outside the benchmark value for Zinc. Sample results
will be submitted as a representative rain event occurs for the month of April until three consecutive
below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely, S—k
U,A,��
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: TC05023
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMPj, standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheelylab.com
Page 1 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: TC05023
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO#2 Shipping/Receiving Aqueous 03/01/2018 0300 03/05/2018
(1 sample)
Shealy Environmental Services, Inc.
106 Vantage Point drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Rohm And Haas Company
Lot Number: TC05023
Sample Sample ID Matrix Parameter Method Result 0 Units Page
001 SDO#2 ShippinglReceiving Aqueous Zinc 200.8 92 ug1L 5
(1 detection)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 7

ICP-MS
Client: Rohm And Haas Company Laboratory ID: TC06023-001
Description: SDO#2 Shipping/Receiving Matrix: Aqueous
Date Sampled:0310112018 0300
)ate Received:03/0612018
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 03/10/2018 0206 BNW 03/06/2018 2002 66184
CAS Analytical
Parameter Humber Method Resuit Q LOQ Units Run
Zinc 7440-68-6 200.8 92 10 uglL 1
LOQ a Limit of Quentitatlon B = Detected In the method blank E = Quentltatlon of compound exceeded the calibration range
ND = Not detected at or above the LOQ N a Recovery is out of criteria P = The RPD between two GC column$ axeeeds 40%
H - Out of holding time W a Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax (B03) 791-9111 www.sheelylob.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive Weat Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 7

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Char of Custody Record
Shealy Environmental Services, Inc.
106 Vantage Point Drive
West CWtunbia, South Carolina 29172
WiaphaneNo.803.791-0700 Faxlfo.803-791-9111
,xq &h9aVah.amr.
Number' 46752
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SHEALY ENVIRONMENTAL SERVICES9 INC.
Shezlr Cnvimnmen1vI Serviom ]na Pup I air t
+ Sample Receipt Checklist (SRC)
Clienl: � ►, i ' [fC q f Cooler inspected Eayidatc: 53L� ' S-1 Iff Lot 4: TC. (i.
q� Yea
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12. Did all aatnpirs arrive in the proper contalnera for each test mmWor in pond condition
(unbroken, lids on, emp —,
Yet
C1 No
13. Was adequate sample valwne available?
Ca nments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyleb.com
Page 7 of 7

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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Monthly Zinc
Lot Number:S1310031
Date Completed:04117/2017
Kelly M. Nance
Project Manager
LABORATORY
� [ I ACCREDITATION
BUREAU
ACCREWE'Oeus,mv
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 4
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: SD10031
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative, The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 4
108 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: SD10031
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO #2 Shipping + Receiving Aqueous 04/03/2017 1930 04/10/2017
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 4
108 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

ICP-MS
Client: Rohm And Haas Company Laboratory ID: SDI 0031-001
Description: SDO 02 Shipping + Receiving Matrix: Aqueous
Date Sampled:04103/20171930
Date Received:0411012017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 04/14/2017 1518 BNW 04/13/2017 0905 39506
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Zinc 7440-66-6 200.8 34 10 ug1L 1
POI. - Practical quantitation limit 8 = Detected In the method blank E = Ouantitalion of compound exceeded the calibration range H = Out of holding time
NO - Not detected at or above the POL J = Estimated result � POL and � MOL P = The RP between two GC columns exceeds 40% N - Recovery is out of criteria
Where applicable, all soli sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 4 of 4
106 Vantage Point Drive West Columbia, SC 29172 [phone] fax [phone] www.shealylab.com

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Ventage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

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SHEALY ENVIRONMENTAL SERVICES INC.
Shtaty Enviremmottel Services, Pit.
Moimcm NvWwr. ME7OINC-0!
N,'*IofI
fiNdive hate; 0397,12017
FApiry rule D3+n700?,'
Sample Receipt Checklist (SRC
Client: ���, Cuolor hispmAcd byMatc: S.X" r f Lot#: Tp 10 OiS
Means ofreeeipl.p
SESI 0 Client Q UPS o FWEx ❑ 011tur '
Yes o
No
1. Meta custody seals present on the cooler?
Yes ©
No o
NA
2. If custody scuts wore present, were thou intact and 'unbrokcr►?
PH strip tD: Cl strip ID,
Cooler ID10riginal Imperature upon receipt Derivcd (corrected) tempera=e upon receipt:
i t-C f 7(' i 1 oC f
Method: Plfemperature ]}tank o Against Ruitles I 0 u n df3:_ _ IP. Gun Correction Factor. D °C
Method of coolant: -Z Wet Ice 0 Blue Ice t7 Dry Ica 0 None
Yes 0
No 0
N?I
3. lftemperature of arty cooler exceeded 6.0'C; ti%w projeen hlanagerNalired?
PM was Notitied b ': horn: ! i=ail f fact; -to -face circle one.
VW 0
Nn 13
NA
4. Is the commercial courler's packing slip attached to this fdrin?
V
No 17
S. Were pmper custody 2rocedures (relin uished?received) followed?
Ym,rf
No 0
6. Wen: surn le 1f.?s listed on IN, COC?
V4:�
Nn n
7. Were shin le Ills Iisred on al qnm le containers?
Yeg .
No ro
X. Was collection dime die. time listed on the COC?
Ya„ef
No n
9. Was collection date & time listed on all sample containersT
Y,
No 17
10. Did all container label information ID, date, time) u ree with the COO
Yee
No 0
11. Were tests to be performed listed on the COC?
Y ,¢f
No
12. Dirt all m nple* arrive in lbu proper wntuincrsforcech last and?or in good condition
unbroken lids an etc.l?
Yes XI
No u
13. Was adequate sample volume available?
Yes n
No)K
1 i. Were All samples received within h the holding time or 48 hours, whichevercomes first?
Yes u
Na
15. Were any samples containers missin 'excess (circle one) samples Not lisped on COC?M�
Yea 0
No u
NA ',
16. Were bubbles present>" ea -size" `/i"or 6mm in diaineteOin an VOA vlaly?
Yesje
No o
NA C
17, Were all DROlmetalslnutrlent sam les received at a PH of < 2?
Yes ❑
No ❑
NW
18, Were all cyanide samples received at a pH > 12 and sulfide samples received at a pH > 97
Yes 13
Na ❑
NA t
19• Were all applicable NI I3/TKN/cyanidlr+phonoVBNA (10;5mam g/L) samples free of residual
chlorine'
Yes C
No 0
NA,4
20. Were collection teem:esatures drraiarnented ov the COC for NC stnrnplcs?
Yes 0
Nu ❑
E�'A�t1
21. Wery client reinarkstrequests (i.e, requested dilutions, i41S IVIS1) designotiotw, ate...)
correctly Iranscribed from the COC into the Corrimcmt scetion in L1MS?
Yes o
Nup
22. Was the quote nuintt)t;r used tukun from the cutituim:r label?
S*m le Fr• wrvintfun (Must be completed for any sample(s) Incorrectly resened orw•itli headspace.)
Sam plt(s) ,vcre received limr=tly preserved and we" axijrrmed a conlingly in
sam le rr:ceivilt with H-,S01 H1r03 HCl Nu0H u3lng SR #
Samples)
were received with bubbles >6 min in diameter.
Samples(s)
adjusted accordiMly
were received with TRC > 0,5 ina,11- (if AN is No) and were
in sample recolvIng with sodium thlosulfata NaISIOa) with Sherd • ID'
SC Drinking Water Prajcct Sanipic(s) pH vcrifled to be -< 2 by Bate:
sample(s) were Not received at A IAI of e 2 aad weft ad usl6d acturdio l ;ush SRO
Sum is labels it lied b Verified by: Date: q-1 &- f7
Comments
i
i
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Monthly Zinc
Lot Number:SD10031
Date Completed:04117/2017
Kelly M. Nance
Project Manager
LABORATORY
ACCREDITATION
BUREAU
r ACCRED1iEDaZemn
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 4
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DREG No: 32010 NELAC No, E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: 5DIO031
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc, ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the DAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, inc. Page: 2 of 4
100 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: SD10031
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO #2 Shipping + Receiving Aqueous 04/03/2017 1930 04/10/2017
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 4
108 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheelylab.com

ICP-MS
Client: Rohm And Haas Company . Laboratory ID: SDI 0031-001
Description: SDO #2 Shipping + Receiving Matrix: Aqueous
Date Sampled:0410312017 1930
Date Received:04/10/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 04/14/2017 1518 BNW 04/13/2017 0905 39506
CAS Analytical
Parameter Number _ Method Result Q PQL Units Run
^ Zinc 7440-66-6 200.8 34 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO - Not detected at or above the PQL J = Estimated result < PQL end? MDL P - The RPD between two GC columns exceeds 40% N - Recovery Is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless nagged with a "W'
Shealy Environmental Services, Inc. Page: 4 of 4
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

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shtnly Givirmtmtatol scrvicky Inc.
mc%imcnt Num?xr. KI WIEC-0Q
Pipo 1 of I
t5 toatiro Dow 03-W-1:017
lxr.i1v nail! 04717021
Srttnple Receipt Checklist (SRC)
Client: S Coular lntipze[ati byldate: ref ? i.at #: 1[] 10 O
Mewsofreceipt.A SESI o Clitm o UPS a FWEx o 01hur__,______�
Yes 13
No
1. Were custodX seals pment. on Ilse cooler?
Ycs ©
No n NA
2. If cuswdy seats wcrt rescm, wcrt they intact and unbrokcn?
PH strip ID: Cl strip ID:
Cooler IDIOrl final temperature upon receipt/Derivod (corrected) temperature upon receipt:,
Method:�yTentperature n1ank n Against Boldes IR (3tin IM. (a 1R Gun Correction Factor: N ac
Method of coolant; z Wet Ice G Blue Ice G Dry Ice © None
Yes 0
No o
N,ti
3. If temperature of any cooler exceeded 6.0'C, vvrss Projec-r Manager Nolifted?
PM was Notitiod b •: 2hong !email I flue -to -face circic one)'
'tr'ea a
No C1
NA_�i
4. Is the commercial courier's Eacking slip attached to this fdrin?
Yat
No tit
S. Wcre Eropcir custody praccdures. (relin uishedr'recelved) followed'
VMdT
No Lr
6. Wens suer le lDs lislixl on the COC?
V-,A
Nn n
7. Were sample IDs lined on all sample containers?
Ves .
No ra
8. W'as collection date & time listed on the COC!
Ves e
No El
9- Was collection date & time listed on all saimp le containers?.
Yma
No zr
10. Did all container label information ID, date, tine) a ree �Nitlt the COO
Yes
Not}
11, Were tests to be peffomed listed on the COC?
ti,p
No
12. aid all samphus +irrivv in the proper r vnwincrs for each test and!or in good condition
(unbrokenlids on etc.)?
YmAd
No to
13, Was ado imte sample volume available'?
Ves n
Nox
14. Wert aril stlmples mc6ved within 'A the holding time or 48 hours, whichever cosmos first?
Yes to
Noid
15. Were any satn les containers missinpjexcess (circle one samples Not listed on COO
- -
Yes D
No ❑
NA
16. Wcre hobbles present?•• a -size" '!a"ar 6MI n in diultteteir in any VOA trials? --
YeSZ
No o
din a
17. Wcre all DROfinetals/mitriettt satrr les received at a pH of <2?
Yes r
No 13
N,
I R. Were all cyanide samples received at a pH > 12 and sulfide samples received at a pH > 97
Yes
No ❑
Np
19, Wert; all applicable N113 TKNfcyanidtiphenoVl3NA (< 0 5mg{L) samples free ot'r'esidual
chlorine?
Yes C
No 13
NA
20. Were collection temperatures documented on the COC for NC sam Ics?
[Y�7=13
NO
,A�
21, Were client remarks'recluests (Le, requested dilutions, M *JMSD designratio n:1, etc...)
correctly transcribed from the COC Into the cornmcnt scrdon'in LIMB?
Nu
22. Wos the quote number used wktm frum the co>Itluincr labci?
Sam le iRmscrvaliun (Must be colrt lctcd for xn sam le(s) incorrectl • preserved or with heads ace.)
Sample(s),
Sample recelvial with
were received incorrectly preserved and wet•e ad weed accordingly in
HiSlDi Hiw03 HCl NaObi uslng Sit 4
tiara 1 sl
were received with bubbles >6 tram In diameter.
Samples(s) were r'vcvived vvi1h TRI' > 0.5 rnyy►- (IF1021 is No) and wore
adlusted accordin l y in sample receiving with sodium thlosulfate . ra=S203 with Sheal • ID.' -
SC Drinking Water Prajcct Samples) PH verifled to be •c 2 by ra(e:
Sam le(s) were Not received at a Al of e 2 and were ad ustW acct)rdin 1 ;u9ir SRN
Sara le l4buls a lied b i
Vurificd by- bate: 14-•1 a-r7
r
Comments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
April 20, 2017
RIFCEIVE
AivN 2 7 2017 �
Sr0RMW T,,, QUAL1
ar�R "ERMIn.NG
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the -month of April, 2017 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was outside the benchmark value for Zinc. Sample results
will be submitted as a representative rain event occurs for the month of May until three consecutive
below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Si cerely,
Aianna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

STORMWATER DISCHARGE OUTFALL
MONITORING REPORT
Permit Number: NCS000389 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
YEAR 7 -- PERIOD 2 January 1, 2017 --- June 30, 2017
FACILITY NAME DAK RESINS LLC
PERSON COLLECTING SAMPLE(S) Sharon Frost
CERTIFIED LABORATORY(S) TBL NC DWQ # 37
ESC Lab Science # 375
AES, Inc.
Part A: Specific Monitoring Requirements
RECEIVED
MAR 2 8 2017
CENTRAL FILES -
DWR SECTION
COUNTY CUMBERLAND
_—P_HONE NO. L910I33-8227
(SIGNATURE OF PERMITTEE' OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Outfall
No.
Date
Sample
Collected
00340
82388
00400
00556
TOTAL
RAINFALL
COD
1,4 DIOXANE.
pH
OIL & GREASE
YEAR 7 PERIOD 2
INCHES
MGIL
MGIL
SU
MG1L
003
No Flow
No Flow
No Flow.
No Flow
F
218/2017
0.3
<30
<.005
7.6
0.76
G
2/8/2017
0.3
41
0.044
7
0.76
H
211512017
0.95
41.5
0.047
7.4
0.85
1
2/8/2017
0.3
<30
0.008
8.2
0.76
J
2/8/2017
0.3
<30
<.005
6.8
1 0.76
004
2/812017
0.3
<30
0.31
6.7
0.76
noes tnis taciury pertorm venue maintenance Activities using more tnan 55 gaiions of new motor oii per month-+ yes A no

STORM EVENT CHARACTERISTICS:
Date
Total Event Precipitation (inches):
Mail Original and one copy to:
Division of Water Quality
2/8/2017 2/15/2017 Attn: Central Files
0.3 0.95 1617 Mail Service Center
Raleigh, North Carolina 27699-1617
" I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
Including the possibility of fines and imprisonment for knowing violations.
(Signature of Permi )
3/22/2017
(Date)

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Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
February 23, 2017
,I
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of February, 2017 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier 11 requirements in
permit. The sample result at outfall SDO-002 was outside the benchmark value for Zinc. Sample results
will be submitted as a representative rain event occurs for the month of March until three consecutive
below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have, any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
RECEIVED
141AR 2 8 2011
DENR-LAND QUALITY
STORMWATER PERMITTING
I
DOW RESTRICTED

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Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Semi Annual Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
March 20, 2017
RECEIVED
MAR 2 3 2017
DENR-LAND QUALITy
STORMWATER PERMITTING
Enclosed are the original and one copy of the Semi -Annual Storm water Discharge Monitoring Report for
the Rohm and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386). The samples were collected on
March 1, 2017. The Semi- annual sample data showed elevated benchmark values at (SDO-002) outfall
for Zinc. Sampling is now being conducted monthly at the Shipping Outfali (SDO-002) for zinc under Tier
Two permit requirements.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

STORMWATER DISCH _ UTFALL (SDO)
MON ORT
Permit Number NCS 000336 0AES COLLECTED DURING CALENDAR YEAR: 0?016-20 7
on
report shall be received by the Division no later than 30 days frnm
N� GPI date the facility receives the sampling results from the laboratory.)
� gE
FACILITY NAME F WR COUNTY Pas uotank
PERSON COLLECTING SAMPLE(S) Adam Fritz PHONE NO. L2 2, 338-2821
CERTIFIED LABORATORY(S) Prein & Newhof Lab #
Lab it
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2,
Part A: Specific Monitoring Requirements
' I11•
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. .-131~. WMITITIMr
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1
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?_ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Mouitorine Reouirements
Outfall
No.
Date
Sample
Collected
500501
00556
O&MO
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appL)
Non -polar
O&GfI?H
(Method 1664
SGT-HEN I), if
&PPL
Total
Suspended
Solids
PH
New Motor
Oil Usage
mo/ddlyr
MG
inches
01101
nun
unit
ma
Form SWU-247, last revised 21212012
Page l of 2

STORM EVENT CHARACTERISTICS:
Date NA
Total Event Precipitation (inches): NA
Event Duration (hours): NA (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches). -
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted Is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility o to and imprisonment for lsnorwing violations."
(Signature of Perm' ee) (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

a
Universal Forest Products, Inc,
May 3, 2017
North Carolina Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Discharge Monitoring Report, Sample Period No. 16
UFP Elizabeth City, LLC
NPDES Permit: NCS000336
Dear Sir or Madam:
Enclosed, please find the storm water report for Sample Period No. 16 (November 1,
2016 through April 30, 2017) at the above -referenced facility.
Please do not hesitate to contact me at [phone] or jmark2nufpi.com if you have
any questions or require additional information on this matter.
Thank you,
Zf 'qw
Joseph Mark, CPG, RG
Regulatory Compliance Administrator
Enclosure
Corporate Headquarters
21101 East,Beltline NE Grand Rapids, M1 49525 Tel; 616,364.6161 Fax: [phone] www.ufpi.cam

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000336 SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days fr
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME UFP Elizabeth City, LLC _ RECEIVED
PERSON COLLECTING SAMPLE(S) Adam
CERTIFIEDLABORATORY(S) Prein&Newhof L bb# JON 7 5 201?
DWR SECTION
Part A: Specific Monitoring Requirement
COUNTY Pasquotank
PHONE NO. (252 ) 338-2821
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Renuirements
Outfall
No.
Date
Sample
Collected
s0050
005%
00530
00400
Total Flow
(if applimble)
Total
Raiafall
Oil & Grease
(if apPL)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), R
L
Total
Suspended
Solids
PH
New Motor
Oil Usage
mol
MG
inches
man
unit
o
Form SWU-247, lust revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date S 5 2017
Total Event Precipitation (inches): 1.0
Event Duration (hours): 3+ (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (incites):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Ann. Central Files
1617 ,Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that q;afdred personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, ;rate, s d complete. Iam aware that there are significant penalties for submitting false information,
including the possibility of t n t for knowing violations."
A , /7
(Signature of Permittee) / (Date)
ij
Form SW-247, last revised 21212012
Page 2 of 2

v
Universal Forest Products, Inc,
June 12, 2017
North Carolina Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE: Discharge Monitoring Report, Sample Period No. 17
UFP Elizabeth City, LLC
NPDES Permit: NCS000336
Dear Sir or Madam:
Enclosed, please find the storm water report for Sample Period No. 17 (May 1, 2017
through October 31, 2017) at the above -referenced facility.
Please do not hesitate to contact me at [phone] orjmark2 a,ufpi.com if you have
any questions or require additional information on this matter.
Thank you,
Joseph Mark, CPG, RG
Regulatory Compliance Administrator
Enclosure
Corporate Headquarters
2801 East Beitline NE Grand Rapids, Mt 49525 Tel: [phone] Fax: [phone] www.ufpi.com

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000336 SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME UFP Elizabeth City, LLC COUNTY Pa4uotank
PERSON COLLECTING SAMPLE(S)
RECEIVED -
Lab
# PHONE NO. L252) 338-2821
CERTIFIED LABORATORY(S) Prein & Newhof Lab #
Nov 10 20, SIGNATURE OF PERMITTEE OR DESIGNEE
REOl1IRED ON PAGE 2.
Part A: Specific Monitoring Requirements CENTRAL FIL
,1 L-GrnoN
1
n
I
1
rr r
D�11
1 1 1 1
[=/��1�
1 I
I �/' •� •
1 1!•iill[�(��IA`[IIIY.I
� t�• • Si
LL�I�C-I��IIUi'i�l'I'
• 1
1 t
r r 1 ►
_1 ' . / ' •
II • 1 1 • - �
4l a - . - •
!i�lkIylll•'�'�ICIi/1l•:.
• • " .. 1 • I
1 ..
��u ;:
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes K no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activitv Monitoring Requirements
�tfv, r;AL I -ILL,.)
DWR SECTION
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appL)
Non -polar
O&G/TPH
(Method 1664
SGT-REM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mold r
MC
inches
myA
m
unitg1VW0
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date NA
Total Event Precipitation (inches): NA
Event Duration (hours): NA (only if applicable— see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-161'7
9 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision is accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and b4cf, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the pussW(!C",
and im onment for knowing violations."
2a r b
(Signature of Permitt ) (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

Universal Forest Products, Inc.
May 11, 2016
North Carolina Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
RE:
RECEIVE®
MAY 16 2016
CENTRAL FILES
DWR SECTION
DischArge Monitoring Report, Sample Period No. 14
UFP Elizabeth City, LLC
NPDES Permit: NCS000336
Dear Sir or Madam:
Enclosed, please find the storm water report for Sample Period No. 14 (November 1,
2015 through April 30, 2016) at the above -referenced facility. -
Please do not hesitate to contact me at [phone] or imark2(Rufpi.com_ if you have
any questions or require additional information on this matter.
Thank you,
�70
Joseph Mark, CPG, RG
Regulatory Compliance Administrator
Enclosure
Corporate Headquarters
2801 East Beltline NE Grand Rapids, MI 49525 Tel: [phone] Fax: [phone] www.ttfpi.com

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000336
FACILITY NAME _ UFP Elizabeth C4, LLC
PERSON COLLECTING SAMPLE(S) Ad M EW7,
CERTIFIED LABORATORY(S) Priers, NewhQ{_Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Pas uotank
PHONE NO. f 2!i2) 338-2821
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
45Us) •• r,
r
r r r
t1
rr WWW rrr;
ur
r �'
i r rrrr rr
�� ► r•�
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes Xno
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitorlux Requirements
Outfall
Na
Date
Sample
ColkctW
50050
00556
005.30
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appL)
Non -polar
O&GITPH
(Method 1664
SGT-HEM), If
a
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/ddlyr
MG
inches
MrA
EVA
unit
saymo
Form SWU-247, last revised 21212012
Page l of 2

+.
STORM EVENT CHARACTERISTICS: Mail Original and one copy to:
April 22, 2016 Division of Water Quality
Date P Attn: Central Files
Total Event Precipitation (inches): 0.1 2 1617 Mail Service Center
Event Duration (hours): 1 (only if applicable — see permit.) Raleigh, North Carolina 27699-1617
(i€ more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (fours): (only if applicable — see permit.)
This DMR is for the period from November 1, 2015 through April 30, 2016.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belie£, true, accurate, and complete. I am aware that there are significant penalties for submitting False information,
including the possibility of fines and imprisonment for knowing violations."
(Signature o ermittee) (Dat
Form 5WU-247, last revised 21212012
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000336 SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITYNAME UFP Elizabeth City, LLC COUNTY Pasauotank
PERSON COLLECTING SAMPLE(S) Adam Fri t z PHONE NO. 1 3 8 - 8 2
CERTUUD LABORATORY(S) P-ri en and Newt of _Lab # C E 1 VE D X COP
_L` ,
ab #E D •i (SIGNATURE OF PERMW E OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Specific Monitoring Requirements CENTRAL FILES
DWR SECTION
Mimi
f f I II
J,
I!_
II �_
11
• •
f • •
, • •i
• • •a
•• • • ••
- •
•- • T.
I
1
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X no
(if yes, complete Part B)
Part B: Vehicee Maintenance Activity Monitorine Requirements
Outiail
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
00 & Grease
(if appL)
Non -polar
O&GI17H
(Method 1"4
SGT-HEM), if
appL
Total
Suspended
Solids
pH
New Motor
011 Usage
ma/d
MG
inches
unit
Raymo
Form SWU-247-062310
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date NA
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
This DMR is for the period from May 1 through October 31, 2015
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and bqK true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possi
"offines and it"risontnent for knowing violations."
Of
(Date}
Form S WU-247-062310
Page 2 of 2

e

STORMWATER DISCHARGE OUTF'ALL (SDO)
MONITORING REPORT
Permit Number NCS 0 0 0 3 3 6
FACILfTY NAME UFP Elizabeth City, LLC
PERSON COLLECTING SAMPLES) Adam Fritz
CERTIFIED LABORATORY(S) P r ipn _ and Ne hQf
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2A 14 - 2 015
(This monitoring report shall be received by the Division no later than 30 cis
the date the facility receives the sampling results from the laboratory.)
COUNTY Pascruotank r�
PHONE N 3 3 8 - 2 8 2 1:•'r'�
RECEIVE '
5IGNATU F PWO-ERMn-ME OR DESIGNEE)
MAY 1$..2 15 compllee�te be t o myr�wledge.this is accurate
CENTRAL FILES r.0
fttinlM QCt` r1^K1
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ^ yes X no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requf vments
Outran
No.
Date
Sample
Collected,
50050
00556
005M
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(d apPL)
Non -polar
O& JTPH
(Method 1"4
SGT-HEM), R
Total
Suspended
Solids
PH
New Motor
011 usage
and
MG
inches
mgunit
Form SWU-247-062310
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date NA
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Matt Original and one copy to:
Division of Water Quality
Attn: Central Fifes
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage systems or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge aiLd true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including and ' rfsonment for knowing violations."
X 4-
(Signature of Per)futtee) (Date)
Form SWU-247-062310
Page 2 of 2

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
April 25, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of April, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was not within the benchmark value for Zinc. Sample
results will be submitted as a representative rain event occurs for the month of May until three
consecutive below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
RECEIVE
APR Z 8 2014
Information Processing Unit
DWQIBOG
DOW RESTRICTED

a
mv
Aw
LLU /I y
ROCS dis&cilityMfQrmVehicle Mahftmnw.Aqdvities"I momthan55gaBomot "moUxroilpermponth?
USM9 Pew yes __w
(ityMcompl&c.P@AB)..
S7.
Nw
FomSW-24&1,12608
Fags 1 Of 2

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name:Stormwater
Lot Number:PDO9048
Date Completed:04/16/2014
Kelly M. Maberry
Project Manager
iq� i¢y At:Cp�ff,
4.f fi
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
• • • • • 0 0 0 •
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] . www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PDO9048
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
It you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com level i Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PD09048
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO#2 Shipping & Receiving Aqueous 04/07/2014 0920 04/09/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealytab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PDO9048
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SDd#2 Shipping & Receiving Aqueous Zinc 200.8 82 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

w1 —19w
Client: Rohm And Haas Company Laboratory ID: PDO9048-001
Description. SDO#2 Shipping & Receiving Matrix: Aqueous
Date 5ampled,04/07/2014 0920
Date Received:04/09/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 04/11/2014 2311 BNW 04/11/2014 1204 44557
CAS Analytical
Parameter Number _Method T Result 0� POL Units Run
Zinc 7440-66-6 200.8 82 10 ug/L 1
POL = Practical quantitation limit H = Detected in the method blank E = Ouantitation Of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PC J = Estimated result c POL and a MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where appllcahlo, all soil sample analysis are reported On a dry weight basis unless flagged with a
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Levef 1 Report v2.1

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�HEALY Chain of Custody Record 106 vaw�!rje Point Olive
vvem columNa, South C:� ro6qa 29172
elephvr* No, (QD3� 791-9700 F.,jx r4f). 791-9111
Number 113052
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SHEALY ENVIRONMENTAL SERVICES9 INC.
shmaly EwiiswuiLatktat ALt Yips, Ina,
Daannicnt Number- F,AD:016
RtNisiaat Nari r. 14
pagt 1 tIa' 1
RtPta::S t?aw(i4 yl;l-1
kfra-aV; Date:OvIrA4
Sample Receipt rhecUA (SRQ
Client: ft"'t_/1 a.uS C:oolerin'spce" by£date:_,U�,,t^,,t t i`>< Lot4- PDf'" '
41!an.s of rect:ipt: SESI ❑ Client ❑UPS [ Fed Ex ❑ Airburnc Fxp ❑ t ith-r
Yee
�+'ci
1. Were c u 5tody seals ;reseiit. oii tht;coolcr?
Y"es
r`tio ❑
'A
7. lfc;ttsirod y seals were )(escot, were t Ivv intact and atnbri)ken '
Cooler ID!UriFirtal tcmperature upon receipL/Dr. ivied (car rectcd) tCrrtpCmtttrt: upon receipt:
Method; E3 Temperatu►e larik ©'Against Battles LR Gun ID: #3 w fR Gard Cormctiun Fact>pr. L?'-t "C
h�ltihoj of coolant.- �i�'ct Ice Blue Ice ❑ i`r ]a ❑ N'One.
yes ❑
No ❑
NA
3. If IcmPcratime. of any cooler exceeded 6.0'C, was Prujtxt Manager notified?
I'M notified by SRC, phone, note (circle: sou:), uihc.r:
(Fur coolers receivW 4in commercial courier, PAJs are to be notified
inirrtrdiatel .)
Yes
ern ❑
tiA 0
4. is the commercial courier's 2acking slip atlached lu this forrn?
Yes
vn D
",i. Were. ro er cuWAY rmicciftirus (relin uishedtrtteived) t'tallowed?
i rs
❑
7-K o C
NA
Sa '4 tm: s les relinquished by client to comwercial cuuricr?
'ir"CS
"Nu
G_ Wele sal[ lc- Ws fisted on the, COC?`
Pass
No ❑
7- Ware sa le 1Ds listed on aril Sur Ic conlainers?
Y.s
o
8. Was collvOiun date & time listed on the COC?
Ye
AU 13
9. Was collection date & titrlr. listed on all sarnt le cutttainurs t
Yes
0
10. Did till container label int'tic-nWtiun (ID, date, thile..),1gree with the COC?
YCs
0
.No 0
11. Were tests to fK erformed listed on the CQC7
Yes
o
1.2, Did all sarn '!les arrive in the proper conlaincrs for each test';"
es
(
Nat ❑
1:3. Did all containers thrive in good condition (unbroken, lids on, ctc.:t?
�'es
o ❑
14. Was adequate sample voluriw avazlahlz?
Yes.
No ❑
15. Werc all samples received within ;� the holdirtg time or 48 hoarr, mobiche-ver
first?
Yes
No i /
_cnrz�.
16. Were on "sent lcs cotttainrrs missing? .,
Yas
� -r }�
1 , . Were there. an excess suer les not listed rill C.
i'es ©NA
�-size"' {rn'ar 6mm�3C'?
18. Were bubbles resent : ` in dinitzrler.) in any VOA vials?
Yea
rNo�
1dA
19. We.rc all metalV0&G(HEh4lnut6eltt tiamplcs received tat a pH of C_'?
`k°ey❑NA
20. Wtrc all cyanide, anti/or stilfY e sane les received at a_pNI� 1 G'
Yes ❑
No ❑
N.A.
21. Were all ,'applicable NMITK.Kicyanide/phenol (<0._rnWL) sumple-s fret. ref
11 residual chlorine"
Vcs E
Na I_I
NA
22. Were collection tern erasures documented on tlic COC for NC: samples?
Yes ❑
No [I
NA
23. �WV r_e client rcnrarkslrt-iltarsts [i.e. requested dilutions, IVISNSD designations,
fetc—)correctly transcrihed from the COC ittlo the commt!nt section in LLVS?
Yes ❑
Nu �
24' Was the quote rrurrtber uu:d taken from the container l;tb::l?
Sample Preservation (Must be completed for any .sawiplt,l ) iiwormctly pceserved or with heads pace.)
Sample(s)._...... ..W, ----- — _ _-._. _+were received incorreccly.prescrved and were: adjusted
accordin l y in sain le jvcciving with _ (H�SO4MNOR.HCI,ir1 K)1i1 using SR #
Satzl l s) _w._..ry Ytx"ere recrAved with huhhh s >6 nun in diameter,
Sam le(;s) tier received A!th'J'KC: >0.2 mgA_ (if #21 is \o)
SC Drinking Water r icet Sample(s) pH verified to be >2 by Dattc.:
tia 1e(s) were not received at u. H ur >2 and were: adjusted accc-ordin Iv us in g Sli#__ _
ti� Ic labels a s lien bv: �'rrzf`tc�3 b Date: t a-
L;umntenrs.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wwwshealylab.com Level 1 Report v2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
16101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name:Stormwater
Lot Number:PD09048
Date Completed:04/16/2014
71W�11
Kelly M. Maberry
Project Manager
�� L4l hCC�R�y
�r g
u N
A
This report shall not be repFoduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyrab.com Level r Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DMEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PDO9048
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report,
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shea)ylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PDO9048
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDQ#2 Shipping & Receiving Aqueous 04/07/2014 0920 04/09/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, $C 29172 �803) 791.9700 Fax [phone] www.shealylab,com Levef 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PDO9048
Sample Sample 10 Matrix Parameter Method Result c Units Page
001 SDO#2 Shipping & Receiving Aqueous Zinc 200.8 82 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Reportv2.1

1v1 -1+w
Client: Rohm And Haas Company Laboratory ID: PDO9048-DO1
Description: SDO#2 Shipping & Receiving Matrix: Aqueous
Datp Sampled:04/07/2014 0920
Date Received:04/09/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 04/11/2014 2311 $NW 04/11/2014 1204 44557
GAS Analytical
Parameter Number Method Result Q PQL Units Run
Zinc 7440-66-6 200.8 82 10 uglL 1
l = Practicai quantitaticn limit B = []elected in the method blank E - Quartitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result a POL and a MOIL P = The Rl between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W'
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

l
SHEALY ENVIRONMENTAL SERVICES, INC.
SMALY Chain of Custody Record 106 %fa wge Point 00ve
i Wephune W. (�n.j 7€31-9700 Fax N . sar,3; 741-911 1
Number 113052
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SHEALY ENVIRONMENTAL SERVICES INC.
shzly Gnv'ifeill %r 0=* Itic:
Uxuatt.al Number. 1'•Arl,MA
tt,rvisirirl Number. 14
Page i „t' 1
Rep la::s Lott: agi2fu rf
lrlres::liti'C tl',1[G: C+:vi$?fN�
Sample Receipt Checklist (SRQ
Client: G ro Prat- atCooler inspected by.+elate::. l n _j L-.�--�`� Lot Ogvq
Means of receipt: OSESI ❑ Client ❑ LTS ❑ Fedl x ❑ Airbumc Fxp Othor
Ye:,
No
1. Were custody seals )resuja on the; cooler?
Yes
No
N-A
2. Ifcuslod ' seals were present, were they iniac[ and ulihr++ken?
Cooler 1.1: /O igmal LCMperature, upOn r-ceipUDerived (c.orrecte: J) Ctuiperaturc upon reci:ipt:
Method: ll Temperat ire liink [Tki ainst Bottle% IR [gun Ill. i3 -,, r. Gov CorTCction actor: j QjG
Method of coolant: WC1 1= Blue ice ❑ Rry ice ❑ tiT4Rf~
Yes ❑
No ❑
NA
3. if tcmperatiire of my cooler exceeded COT. was P€ojoct Manager notified?
PM notified by SRC, phone, note (uit, jc. mio), uther:
(Fur coolers received via comnicrcial courir..r, f'NIs .ur, to be notirwd
smmr<liate.l j
Yes
fin ❑
INA
4. 15 clue cammcrcial ennrier's ackina sii atiaclled lu this Corm?
Yes
NOEJ
5, were. ro Gi mandy srrrs ;:iltlres (zti liR uishetltrccti%'ed) followed?
4'c.s
❑ /No
❑
NA
5a Want bwn les relinquished by client to cotmtier6:iid uuuricr'?
Yes
RANo
Nu ❑
6. Were salty lc. Ills listed on the CO[-?
Yns
❑
?. `ti'ere: yarn. IL�s listed un ull sampic containers",
- -- - .. _
Y.a
fa [1
-
8. Was collection date. & time listed on the COC.?
Yes
9. Was collection data & cum listed un all 53n1 A- cunlaincrs?
Ycs
FJYNo
❑
I W. Did all corlttuner label iDfU111 6011 (ID, dam, time) agrec with the C=
yvs
OAOO
11. Were tests to liu ::rf6rit­w_d lived can the COC?
Y�s
ItJD
1.2, .Did all sa )les arrive in the rn er c0ntainors for each test"
"es
Q
'Nsa i]
13. Did all containers arrive in ood condition (unbroken, lids on, arc)'?
Yes
o ❑
14. Was adequate sample voluim available?
Yes
No t -y
i t
1 ! Wm u[I 4trmplE5 received within i ille holding 6mr, or 48 hmis, whiche-vej'
couw..� last?
Yes
Na 1 /
16. Wert an " sacra Ics ennlnifwra missing?
VC5 ❑
No
17. Were theca an ° excess sampics nut, listed on COC?
Yry ❑
u
ILIA
1S. Were bubbles izsunt>" - 7.e"(1/4"ur6mni in diarttcter) in any VOA vWs?
Yes ff
Nei Cl
NA
" 19. i7rr4u -e all metals/O&G/HElvlinuti'iClrt ,;iim lcs received at n pH of <2?
Y
No- ❑
NA In
20. Werc all cyanid acid/or sulfide samples reueivcd at a Il' >12?
Ye; ❑
N`' ❑
NA
21. Were all applicable NH3fI'i4N/cvan idfYphene l (�,0.3mgil..) samples free of
residual chlorine?
Ycs 0
No fj
NA
`22. Wert_ c ollec.lion tern eraturts documented on iho COC for:VC satnplcx"
Yes ❑
No El,
NA
23. WVere elicnt rcmar1:s/teApir.sts (i.e. requested clilulions,MS{M D designatiolis.
etc..,- cu€rf:CLIt .' tranncrihed from the COC itltu thy~ ct)mmanr section in LASS?
Yes ❑
Nu
24, Was the quote nuliiber used taken from the, contaiaei lab,..?
Sample t1reservation Wtistabe CQrnpleted for any StlnllllefS') inct)mctly prekrycd or with headspac ..;l
—__—were mceivcd incorrectly preserved and wery adjusted
amordin ly in sample re�v6vinr, with (H�SC]. HNt?;,HC},Na{)1Il using SR -9
`; _^ _ rt �allt�li,,,v l were recf;t�"ed with }�ohhlr;s �6 ntm i diarnctcr._
Sam Je(s) were received tenth TRC >1,2 mall. (if 021 is No)
SC ]Drinking Water J°rtajrct sample(s) ply veroitWd to lac >2 b _ Dalu:
1;I le(s7 were not received a[ - .H of >2 and wetw adjusted acmudin lv t1`in Slk
tiff lr. labels a tlieil t�v: Verified b Date; + �J
Lomments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 {803) 791-9700 Fax {803) 791-9111 www.shealylab.com Level 1 Report v2.1

a
MO1hiPilBING ..
Pernnit Nhimbarr: NCS . O 0 �3 -or
SAMPLES.CDU.ZCM Dt iUNG EALE� 'YEAR=
Certificate of Coverage Niunber. NCG — fTbi4 mo ari�g report shall be re�eivad.by tic Div % ao late
.. � ' the: date: tLe ta�itl r�xives ttie same: i�salfs tsoim t>� h�or
Fit MatY M h PA&.3 . a,u C
PIMN COLLEMM SAWLE(S} f PH.
'GItBD LABORATORY(S)
j=2- :. - (SIC O& ESICd+i
By thisslguakwei I. cergy09 ibis r*A is a
- cu aipd k to the bed Of arty kPGWledgei
-Part<A: Specific Moulterit Acgdrments
J
l
I�
DOes this facility perfam Yehiale Mahftnanca Mfivitim using mm than 55 pilm of new molar Oil per fit? _Yes __w
- f if yM complete. Part B}. "
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Form SWU-24&1.1260$
Pave t of

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Zinc Testing
Lot Number:PJ15090
Date Completed,.10/17/2014
7144,-M
Kelly M. Maberry
Project Manager
�4C Ltr RCCdRQ,
tic e � rn
KJ
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
• • • a • • • 0 •
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PJ15090
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page,
Shealy Environmental Services, Inc, Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PJ15090
Sample Number Sample ID Matrix Date Sampled Data Received
001 SDO #2 Shipping Receiving Aqueous 10/14/2014 0540 10/15/2014
(1 Sample)
Shealy Environmental Services, Inc. page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary '
Rohm And Haas Company
Lot Number: PJ15090
Sample Sample ID Matrix Parameter Method Result a Units Page
001 SDO #2 Shipping Receiving Aqueous Zinc 2W8 77 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page- 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

ICP-MS
Client: Rohm And Haas Company Laboratory ID: PJ15090-001
Description; SDO #2 Shipping Receiving Matrix: Aqueous
Date Sampled:1011412014 0540
Date Received: 10/1512014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 10/16/2014 2335 CDF 10/16/2014 0913 58450
CAS Analytical
Parameter Number Method Result 0 PQL Units Run
Zinc 7440-66-6 200.8 77 10 ug/L 1
PQL = Practical quanutation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
NO - Not detected at or above the POL J - Estimated result a PQL and a MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless Flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax {803) 791.9111 www.shealylab.com Level 1 Reportv2.1

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Chain of Custody Record
Shealy Environmental Serve, Inc.
106 Vantmge Point thrive
Vilest Columbia, South Carolina 29172
Telephone No- (803) 791.970p Fax No. (80C3) 791-9111
www1-sheebrrt8b =n
Plumber 21477
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3. Received by
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4. Rehnquist" by
Date
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A. Laborakry Received by
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Note: All samples are retained for six weeks front receipt
unless othor au1'altgmenttS are_ Made.
LAB USE ONLY
9aDa�ed cn Ice fChscirj �a n oW 01cePact
ReceiptT* °C
TempAmk Del o N
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SHEALY ENVIRONMENTAL SERVICES INC.
Sb=ly FnvirtMwaaw Servic", Inc. Nag 1 oY 1
rJocumw Nuwber., F-ADA16 Repla= Date 03.1744
Ravisher PAunbcr: 11 Effective Dum 0311114
Sample Receipt Checklist (SRC)
Client: mow, -4ti-C�Cs Cooler Inspected by/date: roc rn_/.iu+v �y Lotit:
Means of receipt: B'SESI ❑ Client ❑ 'UPS ❑ I=edEx ❑ Airborne Up ❑ Other
Yes Na
❑'
1. Wcrc custody seals 2reseni on the Goole&
Yes Nn NA 2. If custad seals were went, were the intent and unbroken?
Cooler ID/Onginal temperature upon rcacirptfDerived (corrected) temperature upon receipt:
/ !l.s 11C 1 i n 1 1 eC+ i �:
Method: 2rTcinperature Blank ❑ Against Battles IR Gun in: #3 IR Gun Correction Factor. a `t °C
Method ofoaalssnt: Wct ice $lue Ica ❑Dry rce ❑Alone
Yes ❑
No [INA
3. If temperature of any cooler exceeded 6.0°C, was Project Manager notified?
PM notified by SRC, phone, note (circle one), other:
[for coolers received via commercial courier, PMs Are to he notified
immedistel
Yes ❑
No ❑
NA P'
4. Is the commercial courier's p2 kin slip attaubrd to 111is farm?
Yes ❑
No
❑
5. Wcwe r_o r r custody roeedures t+elin uishcd/rcc6%vd followed?
Yca ❑
No
I NAO
Sa Were samples rclin uisbed hLclient to commercial courier?
Yes 21
No
]
6„ Wcre sample IDs listed on the COC?
Yes
woo
7,. Were sn ie Ms listed on all sample containers?
Yes
No
❑
8. Was collection date & time listed on the COC7
Yes
No
❑
9. Was collection date & time listed on all sample c titainers?
Ycs
No
❑
10. Did all container label infotmativa III, date time agree with the COC?
Yes
No
11. Were tests to be onmed I i sted on the COC"
Yes
No
12. Did all sam icss arrive in the proper ooatainerx for cacti wsil7
Ycs
No
❑
1:3. Did all containers arrive in good con lition unb lids on etc.)?
Yea
No
14.1Vas adequate supple volume a�^ailable?
Yes
No ❑
15. Wer,c all samples) received within h the holding, timc or 48 hours, whichever
CDmcB fint?
Yes ❑
Na 0—
16. Were any sam Ics containem tni&sin ?
Ycs ❑
No
17. Were there an excess wm les not lisliod on COC7
Yea
No
NA C7"
18. Were bubblest rescue >" -size"'(`4"or 6mm in tU atmwter) in an VOA vials?
Yes
No
NA ❑
19. Were all metalslO&GiHEM. nutrient samples received at a H of <2?
Yes
No
NA
20. Were all c idc andior qulfide samples received at a H >12?
Yes ❑
No ❑
ETA
21. Were all applicable NH3,TK.Nicyanidclphenol (<0.2mg,'L) samples fnec of
residual chlorin?
Y= in
No ❑
NA
22. Wcm oollectiou tem eratvres documented on the COC for AFC sum les?
Yes ❑
No ❑
MA O
23. Were client remarksinqucsts (i,e. requested di)utions, MS/MSD designations,
etr... correct ir.tnschbed dim the COC into the comment section in 1.TNfS?
Yes 01
NO
24. Was the atc number used taken from the cwttainr r label?
Sample Preservation (Must be completed for any sample(s) incorrectly preserved or with headspaee.)
Sample(R) _ wcm rcc6ved incnrnec:tly preserved and were adjusted
accordinglyacwrdingly in sample receiving with 1S0,1O. HCI,NiaO using SRO
Sam le s were recaivcd with bubbles >6 mm in diameter.
Sam 1 s w= received with TXC :1�0,2 m pL (If #21 is Ztio
SC Drinking Water Project Sample(s) pH verified to be > 2 by _ Date:._
Sam i s were not received at a pH of -2 and were adjusted acconlin ly using SRti
Sample labels . lied by: `�[\ Verified b . Date: %0
C6nuncritR:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 {8(13) 791-9700 Fax [phone] www.Shealylab.com Level t Report v2.t

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name. -Zinc Testing
Lot Number:PJ15090
Date Completed:10117/2014
71W�11
Kelly M. Meberry
Project Manager
*4nti �eCogo�
Qw grl t�
L
K �
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Se+vices, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealViab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No:329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PJ15090
This Report of Analysis contains the analytical results) for the sample(s) listed on the Sample Summary following this Case Narrative, The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP. SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PJ15090
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO #2 Shipping Receiving Aqueous 10/14/2014 0540 10/15/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 (B03} 791-9700 Fax [phone] www.shealylab.com level i Report v2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PJ15090
Sample Sample ID Matrix Parameter Method Result 0 Units Page
001 SOO #2 Shipping Receiving Aqueous Zinc 200.8 77 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Report v2.1

ICP-MS
Client:Rohm And Haas Company Laboratory ID: PJ15090.001
Description: SD4 #2 Shipping Receiving Matrix, Aqueous
Date Sampled:10/1412014 0540
Date Received:1011512014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 10/16/2014 2335 1 10/16/2014 0913 58450
CAS Analytical
Parameter Number Method Result 0 PQL Units Run
Zinc 7440-66-6 200.8 77 10 ugi 1
PQL - Practical quantitation limit a - Detected in the method blank E = Quantltation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J . Estimated result < PQL and > IUDL P . The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis uniess flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Reportv2.1

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Shealy Environmental Services, Inc_
106 Vantage €'clini [give
West CO(umbia. South Carolina 29172
Telephone No_ [phone] Fax No. [phone]
W1RrPzhaerylsb3 rn
Plumber 21477
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Fossd*a Hazard Ideati9rslton
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Date
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3. Ratinquirt+er1 by r
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Data
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4. RelhApIsheti 4y
Dabs
T'aire 4.
Laboralrxy Received try
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Note: A samples are reialned for six weeks From receipt
unless other arrangements are made.
LAB USE ONLY
4emimed rn Its rchKk) �a r7 rb ❑Ice PIA
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SHEALY ENVIRONMENTAL SERVICES INC.
Shealy Fminlrftai" Servieas, I= Aege 1 of I
Dacumv* Hwk&er: F-AD•016 Repleem Date: 03.411111114
Revisim t4umbrr. 13 Effe a ive Dare 07115il4
Sample Receipt Checklist (SRC)
C"limt: 'satin w. + �l�a�.S Cooler Inspected by/date: M4+r _flutes `-t Lotit. @ 4\S5 O" M
Means of receipt: O"SESI ❑ Client ❑ UPS ❑ PeIF,x ❑ Airbome Up ❑ Other
Yes No
1. Were custody seals Present on the cooler"?
Yes Na
NA 2. [fcustod scats were PLCScnt, were the intact and unbroken'?
Caroler I1310riginal Ien pasture upon rcmipLID+�etiv�ed (couect4 temperance upon ruccipt:
(c��W
Method: 2rTemperature Blank ❑ Against Dottica IR Gran Tn' 0 IR Gtm Correction l'aCtOT: b "k °C
Method of coolant- Q`Wct kc Blue lea ❑ roe ❑ Notre
Yea ❑
FYea
No El
NA j
3. If temperature of any cooler exceeded 6.0aC, was Project Manager notified?
PM notified by SRC, phone, dole (circle one), other;
(For coolers received via commercial courier, PlU1s are to he notified
immcdiatvl .
❑
No
❑
NA r
4. Its the comtricrcial cuurirn''s packinjg slip attached to Ibis form?
Yes
❑
No
❑1
5. Were proper custody r000dures relin uishcdlreccived followed?
Yes
❑
I
NAO
5a Were sam lcs rclin uislled by client to Commercial cnuricr?
Yes
No
0
6. Wcrc sam le IDs listed on the COC?
Yes
ND
7, Wert sample Ms listed on all mut le containers?
Yes
No
❑
S. Was collection data: & time listed on the COC?
vw
No
❑
y. Was collection date & time listed on all sample containers?
Yes
PlI
No
❑
I
10. Md all container label information ID, bate time agree with the COC?
Yes
Nu
11. Were tests to be performe0sted. on the; COC?
Yes
No
12. Did al I samples arrive in the ra r containers far each test7
Ycs
0
No
❑
11. Did all containers arrive in good condition unbroken lids on, etc,)—?
Yes
No
14. Was adequate sarlaple, volume aNmilable?
Yes
No ❑
15. Were all urnples received within'h the bolding time or 48 hours, whichever
comes first?
_
Yes []
No
16. Were any aam les conUtinem tnissin ?
Ycs
No [
17. Weir, there any excess samples not lislcd on COC?
Yee C1
I Na Q
NA al
18. Were bubbles 2rcm= >` -siW' K"or 6mm in dianicttr inany VUA vials?
Yes
No
NA [J1
19. Were all rneta1s10&GlHl3Mlnutrient snelcs received at a pH of <2?
Yes
Na
NA
20. Were all 'dc andJor rrulfide samples received at a pH>12?
Yes ❑
No ❑
NA
21. Ware all applicable NH3,TKNfcyanidCVphenol (<0.2mg;L) samples free of
residual chloTinc?
Y=
Na ❑
NA
22- W= t:alle ction tern enttlres documented un the COC for NC samples?
Yes ❑
No ❑
MAO
23. Were client rernarkslnaquests (i.e. requested dilutions, MS!MSD designations,
etc...) correctly un scribod from the COC into the Comment section in IJMS?
Yes
I No
24. Was the quote number used taken from the cctntainer label?
Sample Preservation (Must be completed for any sautpl e(s) incorrectly preserved or with headspace,)
Sample(s) _ were received iacormudy preserved and were adjusted
aceordin l y in sanyle receivin with (H2SO4Us HCI,NaO usirl SR #
Sam la s were received with bubbles >6 clam in diameter,
Sam 1 s wc= re=eived with TRC >0.2 m fl If #21 is Eo
SC Drinking Water Project Sample(s) pH vcri tied to be > 2 by Date: .
Sam 1 s) were not received at a pH of <2 and wen adjusted accordingly using SRIi
Sample labels =lied by:__ `-e\ Ve- ificd bY; Date: 10
Conlrgerlt8:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 1803) 791-9700 Fax [phone] www.shealylab.com Level 1 Reportv2,1

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
• [phone]
October 21, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617 js
NOV
CERTIFIED MAIL: 0 6 2014 !
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of October, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was outside the benchmark value for Zinc. Sample results
will be submitted as a representative rain event occurs for the month of November until three
consecutive below benchmark samples are collected.
• Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
i 10-�'
Aianna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
0 DOW RESTRICTED

MRMWATER DIISAMAAGE OiTIFALL (5DO)
MONITORING SPORT
Perna Nmaber NCS 4 0 ()3 3 G -
FACnMNAML UFP Elizabeth City, LLC
PRRSON COLLELTIIt1G SAMPLE(S) jIL?SPj3h T)avi ann
C=TMM LAWRATORY(S) 1 ien and- membnf Lab 0
Lab #- -
Part Al, Speem Mowtaring Regdremeats
SAMPLES COLLECTED DURING CALENDAR YEAR: 2 014
(Thk mmdtorit:$ report dmn be received by the Dtvblom no Iafer Um 30 days b m
the date the fly recelvrca the =MpHag r mWb !roan the laboratory.) •
COUNTY Ratsaujotank
PBONE NO. )338-2821
(SMNAIURE OFISVMtrM OR DlWGNEfi)
By this dpattire, I o wft tbat this report b acia rab
congete to the but of spy imowhdge.
I1
11 •
rl�+
ll��
nJ
11
f 1
1
11
1
L
1 i
i
Does This facility perfotm Vehicle Maintenance Activities using mare that: 55 gallons of new motor oil per mordi? T yes X no
(if yes, oomptete Pats B)
Part B: Vehkle hisfmtmance Aetiviir MonlOrba Reanireti ats
++rr v-U 7 2014
CENTRAL FILES
DWR SECTION
Ott"
No:
Date
S wq&
Corleeted
sow
DVX%
00m
t104QQ
Total Flow
(K,%Mlkabh)
Total
Rainfall
OS & Grcm
OfappL)
Nas-pdar
O&G!rm
(Method l&W
SGT-HEM),.it
a L
Total'
Sbspmded
Solid$
go..
New Mat".
fK1lJaagc
MG
hrebes
UWAtrait
Form 5WU-247-M310
Page 1 of 2

P
STORM EVEM (314"CTEBIMCSe
Rate 10/22/2014
Total Event Preelpitallm ( ):. 0.2
Event Duration (hours): (only if applicable —see permit.)
(if more than one storm event was sampled)
Daft
Total Erma Predphadon (lushes):
Dent Duration (homers): (only if applicable — see permit.)
Mail Origlmal and one copy to:
Division of Watsr Quality
Attn: Central Files
1617 Mail Service Center
Raakigb. North Carolina 2709-1617
"I certify, muter penalty of law, that this document and all attachments were prepared under my dlreedon or supervidoo to aeoordaum with a
system designed to assure that quaUded personnel properly gather and evaluate the hdarmation submitted. Bassi on nW k quiry of the person
or persons who manage the syateus r those persons directly respondble for gather ft the information, the information submitted is, to the beat
of my knewhAp and bdief, , a e, and couiplete. I am aware that there are sigoilkamt penalties for subudding false iaforms1lon,
including the for knowing vloladous."
(signature of
Form SWU-247-062310
Page 2 of 2

Universal Forest Products, Inc.
November 3, 2014
North Carolina Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh; North Carolina 27699
RE: Discharge Monitoring Report, Sample No. 11
UFP Elizabeth City, LLC
NPDES Permit: NCS000336
Dear Sir or Madam:
Enclosed please find the storm water report for Sample No. 11 at the above -referenced
facility.
Please do not hesitate to contact me at 616-365-1526 or rdickens(@fpi.com if you have
any questions.
Thank you,
Robert Dickens
Regulatory Compliance Specialist
enclosure
Corporate Headquarters
2801 East 9eltline NE Grand Rapids, Mt 49525 Tel: 616.364,6161 Fax: [phone] www.ufpi.com

19
SI WATI AGE otproA :>f (Soo =
Permit Npmbier. NCS ©03 3 of SAWLFS.Couzctm DUMG CiUggDAR YUIL- ?
C.erW=te of Covwaga Mmbw. NCG f lmrt sTzall be r+ca ed.by! Div�ion iro
. - - . � ' the data Eht fae� regeives tlia Ong: r�lts itoia � faDor
Fi4CUXiY w. A
SON COLLBCTII�IG 5A1HPL r pg 9 a 2
1 '1'IPI6D LABORATORY(S) : ?
# (SIWUTUSB OFF OB DFSM
• - - - - BT this sigt:a� Y. Qerti�j #1�at thie repa�rt is a
compMe to -the best of gry bwwtedge.
: Pwt A: speei&e nfonitariug. -
=,Nlol
1- '
Does this fmlity pufarm Vehicle Nbiatmmw.Activities icing mom dm 55 gaUm of new m kw oil pa Tooth?
Yes �o
otym cowhft.part 13)
P4_rt . VehW* MaWtmwce A lyionito ' is
S�aui�pks W.�.r
.7
Focin.SWU 24-1.12608
Page 1 of 2

"Y defy; MAW penalty otbw, that this document and A aMwhmenb were prepared under my direction or supereiaIon in 4=r&WO with s
system designed to *Mumthat gwMled. personnel properly gather and mhdate the information. submitted. Based qu my inquiry of the person
or persons who managye the systetn, or thampersons directly responslc for gathering the information, the hi[ormatkm submitted is, to the best
PC my. haowledge' and belld, true, aamrate, and conV1tte. -1 am aware that there are but penall ies for sabmitting-be information,
bkhzdhw the _of fines and imprlsa nt for bwwft Yiolagtkx&
- 8 Z7 llq
— csigare. r� Matoi .

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention; Alanna Smith
Project Name:Stormwater
Lot Number:PH15031
Date Completed:08/20/2014
7qu-1v
Kelly M. Maberry
Project Manager
qa'+
u
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmemal Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.Shealy€ab.com level 1 Repon v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC 0HEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PH15031
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (DAMP), standard operating procedures (SOPS), and Shealy
policies, Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
It you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PH15031
Sample Number Sampie ID Matrix Date Sampled Date Received
001 SDO#002 Shipping Receiving Aqueous 08/10/2014 1015 08/15/2014 .
(1 Sample)
dp
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PH15031
Sample Sample 1D Matrix Parameter Method Result Q Units Page
001 S00#002 Shipping Receiving Aqueous Zinc 200.8 32 uglL 5
(1 detection)
:)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www'shealylab.com Level 1 Repogv2,1

ukent: HOnm Ana Kass L;Ompany
Description: S00#002 Shipping Receiving
La4oratory lu: Nniowi-uu1
Matrix: Aqueous
Date Sampled:08/10/20141015
Dat2 Received:08/15/2014
ICP-MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 08/19/20141950 CDF 08/19/20141105 54320
CAS Analytical
Parameter Number Method Result 0 POl- Units Run
Zinc 7440-66-6 200.8 32 10 _ ug/t- 1
POL = Practical quantization limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MOIL P = The RPC between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on ad ry weight basis unless flagged with a'W
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Levels Reportv2 1

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Shealy Environmental Services, Inc.
106 Vantage Point drive
West Cdumbia, South CaroEina 29172
Telephone No. [phone] Fax No. [phone]
nww_dwmlyiab.com
Number 26440
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Sam (P Namsa)
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Tum ArmrdTimD Required (PAeF lab awsmW required la ex*kd TAT)
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Date
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4, ReRnpu
Date
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Mate. AU samples are retained far six weeks rn receipt
unless other arran emsrtts are mane.
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SHEALY ENVIRONMENTAL SERVICESt INC.
Slualy Emircaunmuil Ser+vioes, L1c_ rhwr. l of 1'
Dpcumeot Number. FAD-416 RErbca% 17,yik: 0341?114,
lRevisinn leumttr: 15 EfreLtivu n]unr- 4171M 4 .
Sample Receipt Checklist (SRC)
Cheat. oo;s 57 CLvierInspmied byldate: MLtt>n ?
Means of Tolmipt: SESI ❑ Clicut ❑ UPS ❑ FcdEx ❑ Airborne Exp ❑ (hher
Yes Ej
I No
1, Were CUS194Y seals PnEfit on the cooler?
Yes ❑ i No EU NA 2. if costs+ seals were present were they intact and unbroken'?
Cuuler IDe'1Original tcmperaturc upon receipt-Verived (corrected) temperature upon receipt:
I'L J It �_ -C i Or ZIC1 11 nC
Method. [] Teinperutur` nk Against Bottics IR Gun 1D: #3 TR (run CmTectirm Factnr� \ 4C
Method of c001ant: Wet ]cc ❑ Bluc Ice ❑ Dg Ice Q Nane
Yes ❑
No ❑
NA
i, if temperature cif any cooler exceeded 6.VC, Was Projcct mager notified?
11NI notified by SRC, phone, note (circle one), other,
(For coolers received via mi alemcial cowiet', PNIS are to be notified
iinmediatel .
No ❑
NA
4, Is the commercial courier's packing slip attached to this form?
_yEiL.a
Yes
❑
No ❑
A. Were prciper custody, rncedures (relit uiahedirmeived followed? ..
Yes
No
NA PF
Sa Wcra satnples rc!Lnoishcd by client to commercial courier?
Yes
No
_
❑
6. lrti+= sin le IDs lislcd on the COC?
Yes
No
U
7. Were sample ills listed on all sags containers?
Yes
o
❑
8, Was collection date & time l6ted oto 1ho CM.?
Yes
a
❑
9, Was collection date & time listed on all sam le corltairters?
Vein
o
❑
10. ad all writaincr label information ID, date, time) a *ace with the COC?
Yra
o
11. Were tests to he performed listed on the COC?
Yes
❑
12. Did all rani tiles ;naive in tho rot ur wrilxini rrs for cacti Iriit?
Yes
Eltr
tut 13. Did all containers arrive ingood candiliubrokcn lids art, etc.)?
Yes
lNu
14. Wag ad uate sample -Mums available'?
YGc
n
15. Were all samples received within % the holding Limc ur 48 hours, whichever
comes first?
1 t4. Were any sa lea containo:rs missing?
Yes
Yea I
Na
Ll7- Were there any excess Stan des nw lislad on CDC?
Yes ❑
No ❑
NA
l S. Were bubbltl prestmi >' -size'• ('d: 'or 6mrn in diameler) in an VOA %Jal.s?
Yes R
No ❑
NA. [ ]
L 19, Were ail metals;Q&.G HE1vL1butrient Sam les received at A V14 of •,2?
Yes ❑
Na ❑
NA
20. Were all cyanide andlor sulfide s aril plrs received at a PH > 12?
Yea El
No ❑
NA
21. Were all applicable 1N'H3l"r Nfcysutide+'phenol ({0.2m�'L) samples frc+e of
residual chlorine?
_Y;sr
No 0
NA
22. Were collection temperatures docurnented on the COC for NC sam les?
Yes ❑
No Cl
NA
23. Werc client remaritsirequests (i.e. requested dilutions, MSoIISD drsignatious,
elk; ... ) wn-cctly traru+cribed .f om the MC into the comment section in LIMS?
Y Na 24, Was the quote number used taken fromthe container labcl?
Sample Preservatimr (Must bv completed for any sample(s) incorrectly preservod or with hcadspacc.)
Sa nple(s) wtrrle received i.ncurrectly pr�crvIl and were adjusted
acenrdin I in. sample receirin with �2SO4jtNO3 HC1,Na[] using SR at
Sam 1 s were received with bubbles --6 nun in diarneter.
S le 's wem received with TRC y02 m `I, If #21 is l+la
SC T.h1nklAg Water Project Sample(s) pH vcrilred to bc:- 2 by Date:
le(s Werc nUt ruccived at a EH of t2 and were ad usled accordingly usina SR#
S le labels applied b : M Vcrif`a:cd by: 044 Batt:
agments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Stormwater
Lot Number:PH15031
Date Completed:08/20/2014
71-y"11111
Kelly M. Maberry
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Revel 1 Report v2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NEIAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PH15031
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Raportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PH15031
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO#002 Shipping Receiving Aqueous 08/10/2014 1015 08/15/2014
(1 sample)
Shealy Environmental Services, inc. Page: 3 of 5
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PH15031
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SD0#002 Shipping Receiving Aqueous Zinc 200.8 32 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level s Reportv2.1

uiiem:Honm Ana mass L;ampany
Description: SDO#002 Shipping Receiving
Laooratory lu: NmiSuai-uu,l
Matrix: Aqueous
Date Seim pled:08/10/2014 1015
Date Received : 08/15/2014
ICP-MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 08/19/20141950 CDF 08/19120141105 54320
CAS Analytical
Parameter Number Method Result 0 POL Units Run
Zinc 7440-66-6 200.8 32 10 ug/L 1
POL = Practical quantitation limit B = Defected in the method blank E = Ouan itation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result c POL and > MDL P =7he RPD between two GC columns exceeds 4C% - N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Reportv2.1

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Shealy Environmental Services, Inc.
106 Ventage Point Drive
West Columbia, South Carolina 29172
Telephone No. [phone] Fax No. (803) 791-911 t
WWWA eaiYlaDcam
Number 26440
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PwJacl Name
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Bate
Time
3. Received by
Rste
Time
4. RetheQu
bate
Time
4. l�arff Fred by
l
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Thaw
Note: AU sam-ples are retained for sic weeks rlr C' eipt
ainisas other arran ements are made.
has U&E ONLY
Reodven an lrni>)Is 040 AtoiPatk
RmwiplFcnp 'C
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SHEALY ENVIRONMENTAL SERVICES INC.
5i iraly Eavis mmcxnal Smvires, hie.
Docu=nt Nuu6Fr F-Ar)-t116
fMige 1 of I.'
lRq-4cco nttte: 03417 4 ,
Revising Number. t5 Etixuva hate ii?ri514
Sample Receipt Checklist (SRC)
Client: Iq!� S�. � Cooler IMotrcd by/date: M(Am 0 Or, t`` Lot 0: 0
Means ufnxxipt: SESI ❑ Clicnt ❑ UPS ❑ FcdEx ❑ Airborme Exp ❑ Other-
Ycs Nv 21
1. Were custody seal, resenl on the cooler?
Yes ❑ No ❑ NA 2. If cuRtn seals were Present,, were they intact wid unbrolmn?
Cooler ID/Original tcmperaturc upon reccipb13erived (corrected) temperature upon receipt:
'I MetLud: ❑ T=pereturc nk ErAgaimst Bottles iR Gun iD: #3 TR Gun Cn Twdrm Factor:- \ T
Method of coolnrrt; Wrl Ice ❑ Blur [cc ❑ D Ice None
Yrs ❑
No ❑
NA
3. if terttperawre of any ow1cr oxceedGd 6,0`C, was Project Manager notified?
P-1A notified by SRC, phone, note (circle one), other:
(For coolers roveived via cointu.ercial courier, ?Nis m to be notified
iinmediatei )
Yes
❑
No ❑
NA
4. Is the commercial courier's Packing slip attached to this form?
Yes
❑I
No ❑
VS't:re rn L costa meedures (relit uiRhadlreceived) followed?
Ycs
1,No
NA
5a WCrc samples rc ' ishcd by client to commercial courier? �
Yes
No
6. Were sgVle IDs listed un the COC?
Yes
No
7. Were sample U)s listed on all EM& contta�iium?
Yea
o�
❑
B. Was collection [late & theye listed on ]lie.C?
Yes
u
❑
9. Was collection date fie: time listed on all Sam le containers?
Yes
o
❑
1 U. Did all e,onliaincr label informal ion A7, date, time) a Tee with the [ ClC?
Year
o
11. Were tests; to bt erformed listed on the COC?
Yes
No
❑
12. Did all sari ►left naive in the pircipur vw zjwH ors for cach test?
Yes
t7
❑
13. Did all containers arrive w good couditiurt juabrokcn, lids a ctc.)?
Yes,
15
No
❑
14. Was ad uate sam le volt►rne avai]able?
Yea
loll No (❑
1 S- R'ere all samples. received withik) lea the holding titnc ur 48 hours, w�hichc%rr
comes first?
16. Were any sa led writaincars missin ?
Yea
No
Yea ❑
I No
17. Were there any excess tiara lcs not liswd on CM
Yes ❑
No o
NA
18. R'et'e hubbies VMWnt �` a-si.xe" ('!"nr fimm in diameter in an V(.tA ►vials?
Ymi
Nn ❑
NA. ❑
19. Were all metalsiU&(;iUF.NL'nutricnt samples received at a V14 of <2?
Yes ❑
No ❑
NA
20. Were all c atridc and/or w1fider touTles received at a pH > 12?
Yew ❑
Nn ❑
NA
21, Were all applicable NTHYfKN!cylanide;phenul (=0.2mgiQ sampIcs free of
residual chlorine?
Yes El
No 0
NA
22. W= collection temperatures documented on the LW fbr NC samples?
Ye; ❑
No ❑
NA
23. Wcre client remarks�requesli (i.e. mquesied dilutions. MSr11SD designations,
etc...) ivrr=tly transcribed from the MC into the comment suction in LWS?
Ycs NQ 24. Was the gAote number used taken from Like container label?
Sample Flreservation (Must bc. completed for any sample(s) incorrectly presmed or with hcadspace.)
5a>!nple(t) ' _ _wviued incorrectly preserved and were adjusted
accordingly in xRm le recCivin with g ere mi2 04{ 1OJ HCI,Na0N1 using Sit #
5 le(s) were received with bubbles 7 6 mu in diameter-
5 le s were received with 1RC >0.2 m 7. If 421 is No
SC Drinking Water Project Etztple(s) pH vcriliLd to be > 2 by Date:
S lc(s were not rtccivcd at d pH of <2 and were ad'usted accordingly using SR#f
S2MIelabtft applied b : M Verified Date:
omlqlts:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, 30 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
August 27, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of August, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was within the benchmark value for Zinc. Sample results
will be submitted as a representative rain event occurs for the month of September until three
consecutive below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

w
t
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-
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boas this facility perfarm Vehicle Nlak ten�mcc Agtivities using more than SS gallons of new motor oil per youth? w yes
(iYm cowrete.Part B).
it �
Foci. s W U-2A 6-1.12608
Page 1 of 2

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Semiannual -
Lot Number:P123047
Date Completed:10/02/2014
71i/l_.11ty
Kelly M. Maberry
Project Manager
hC04gfly
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist,
Shealy Environmental Services, Inc. Page: 1 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DM EC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: P123047
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (DAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the,Shealy Project Manager listed on the cover page.
Inorganic Non -Metals
Samples -001 and -002 were received outside of the 48 hour holding time.
The Biochemical Oxygen Demand (BOD) result for samples -001 and -002 has been reported as less than the stated value due to oxygen depletion
of less than 2.0 mgh at each sample dilution. The sample was prepared with a standard series of dilutions based on historical data.
The SCF associated with BOD batch 9370 was 1.26 mg/L (valid range is 0.6 - 1.0 mg/Q. All other OC were within limits and there is no effect on
the SOD result.
Shealy Environmental Services, Inc. Page: 2 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealytab.com bevel t Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: P123047
Sample Number Sample,ld Matrix Date Sampled Date Received
001 SOO-#1 Cove Creek Aqueous 09/16/2014 2156 09/23/2014
002 SD042 Shipping/Receiving Aqueous •09/16/2014 2150 09/23/2014
(2 samples)
Shealy Environmental Services, fnc. Page: 3 of 8
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number., P123047
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
SD041 Cove Creek
Aqueous
BOD, 5 day SM 5210B-
4.0 76
mg/L
5
001
SD041 Cove Creek
Aqueous
TSS SM 2540D-
44
mg/L
5
001
SD041 Cove Creek
Aqueous
Zinc 200.8
63
ug/L
6
002
SD042 Shipping/Receiving
Aqueous
BOD, 5 day SM 5210B-
2.9 76
mg/L
7
002
SD042 Shipping/Receiving
Aqueous
TSS SM 2540D-
28
mg/L
7
002
SD042 Shipping/Receiving
Aqueous
Zinc 200.8
76
ug/L
8
(6 detections)
Shealy Environmental Services, Inc. Page: 4 of B
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slow) yet low l.4L.-,l.4r16wlV
Client:Rohm And Haas Company Laboratory ID:,PI23047-001
Description: SD041 Cove Creek Matrix: Aqueous
Date Sampled:09/16/2014 2156
Date Received:09/23/2014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(BOD, 5 day) SM 521 OB-2011
1 09/29/2014 1030 MEV
09/24/2014 0851
9370
1
(il SM 4500-H B-2011
1 09/24/2014 1606 HMA
56786
1
(TSS) SM 264OD-2011
1 09/23/2014 2141 HMA
56703
CAS Analytical
Parameter
Number Method
Result 0
POL
Units Run
BOD, 5 day
SM 521OB-20
4.0 76
2.0
mglL 1
pH
SM 4500-H B
6.57
su 1
TSS
SM 254OD-20
44
5.0
mglL 1
Footnote(s): 6-D,0. depletion < 2,00 mglL 7-SCF Out of range
POL = Practical quantitation limit B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J - Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is oLt of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] r www.shealylab.com Level 1 Report v2.1

1v1 -4f1y
Client: Rohm And Haas Company Laboratory ID: PI23047-001
Description: SD041 Cove Creek Matrix: Aqueous
Date Sampled:09/1612014 2156
Date Received:09/23/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.E 1 09/29/2014 2140 BNW 09/26/2014 1715 56986
CAS Analytical
Parameter Number Method Result 0 POL Units Run
Zinc 7440-66-6 200.8 63 10 ug/L 1
Footnote(s): 6-D.0, depletion < 2.00 mglL 7-SCF Out of range
POL = Practical quantitation limit 8 Detected in the method blank E = Ouantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result < POL and a MOL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Client: Rohm And Haas Company Laboratory ID: P123047-002
Description. SD042 Shipping/Receiving Matrix: Aqueous
Date Sampled:09/16/2014 2150
Date Received:09/23/2014
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst Prep Date
Batch
i (130D, 5 day) SM 521OB-2011
1 09/29/2014 1030
MEV 09/24/2014 0851
9370
1 (pH) SM 4500-H B-2011
1 09/24/2014 1606
HMA
56786
1 (TSS) SM 2540D-2011
1 09/23/2014 2141
HMA
56703
CAS Analytical
Parameter
Number M ethpxL
Result Q POL
Units Run
BOD, 5 day
SM 5210B-20
2.9 76 2.0
mg/L 1
PH
SM 4500-H B
6.9
su 1
TSS
SM 254OD-20
28 2.5
mg/L 1
Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range
POI. = Practical quantitetion limit 9 = detected in the method blank E = Quantitation cf compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result < POL and a MDL P - The RPM between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wwwshealylab.com Level t Reportv2 1

Client: Rohm And Haas Company Laboratory ID: P123047-002
Description: SD042 Shipping/Receiving Matrix: Aqueous
Date Sampled:09/1612014 2150
Date Received:09/23/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Data Batch
1 200.2 200.8 1 09/29/2014 2155 BNW 09/26/2014 1715 56986
CAS Analytical
Parameter Number Method Result 0 POL Units Run
Zinc 7440-66-6 200.8 76 10 ug/L 1
Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range
POL = Practical quantltation limit B = Detected in the method blank E m Quantitation cf compound exceeded the calibraticn range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result < PQL and > I P - The RPO between two GC columns exceeds 40% N = Recovery is out of criteria
Where appikcable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W'
Shealy Environmental Services, Inc. Page: 8 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Shealy Environmental Services, Inc.
106 Vantage Point Drive
West Cciumbia, South Carolina 29172
Telephone No. (803) 751-91DO Fax No_ (BU3) 791-9111
%%ww.ah%alyiabxcm
Number 21478
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Note: All-samifleS are retained For abc weeks from teaelpt
unless other arrapWff!ents are made_ 7i?swirsd
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an 1pp (Chsck) -Al c no a rm f ack IRDm4pi Tamp. -•c
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SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Emvimnmrarat Smirm, rnu. Ngp t L& i
rkt.aimrm NumRxr F•At-qtr, tteplimeq Date: 1`11%5114
RevisianNumhdr. t5 EffbedueDate: 07.+ 914
Sample Receipt Checklist (SRC)
Client: Y-cY't x'�r+ xr 0.� Cooler Inspocled by+date; Srx-VWN ,+ CAVt"'%-� Lot#: I2
Means of receipt: Z-Sksl ❑ Client ❑ UPS ❑ FcdEx ❑ Airborne Exp ❑ Other
Yes
No
1. Were custody seals ppasmt on the cooler'?
Yes 0 No El I NA 2. if custody seals were present, were thEy intact anti unbroken?
Cooler ID/Original temperawre upon receiptiDerived (corrected) tcmperaturc upon receipt:
,rt] 01 "'.. .Q °G f _f aC / + -1C + + °C
Mcibo l: ❑ Temperantre Ftiank Against Bottles iR Gun iD: 43 IR Gun CmTcctitlm Factor: 4 °C
Method of conlani: W'et Ice Blue kc ❑ Dry Ice ❑ None
Yes ❑
No ❑
NA ja`
3. if tempenwre of any Cooler exceeded 6.0l,C, was Project Nlttrtager notified?
PM notified by SRC, pbone, note (circle one), other:
{for coolers received via commemial courier, PMs are to be notified
ininiediatel .
Yes
No
NA L6
4- 'is the commercial onurier's packing F;Iip attached to thie; farm''
Yes
❑
No
5. Were 2wper custnicly prncedures relitl uisheb,'received followed?
Yes
❑
No ❑
NA
Ss Werc sam lcs relinquished by client to commercial ootviu?
Yes
No
❑
b. Were sm lc 1Ds lislt:d on the LYJC?
Yes
NO
❑
7. Were ram le iDs listed an all sample containers'?
Yes
No
g. Was eollecti► n date & time listed uti the COC?
Ycs
2r
No
❑
9. Was collection date & time Iisted on all =Wle containers?
Yes
No
❑
10. Did ull writaina lubr,•1 inlurmutiun QD, date time) agrcc with the COC?
Yes
No
❑
11. Were tests to be gEformed listed on the C OU?
Yes
No
12. Did all a wvi . lea arrive in the proper u�ntainers fur cew-h IcW?
Yes
No
❑
13. Did all oontainers arrive in good condition Luitroken. Lids on, etc.)?
Yr s
No
❑
14. W&% adequate Rain le volume available?
Yes ❑
No 2r
15. ''err all samples reoeived within 14 the Bolding titue or 48.hours, wlticltt:ver
comes first?
Yes
No
16. Wcrc iin • samplos cxtntaincri; minsin .
V05 ❑
No
17. Were tyre wiy excess Satrt lira not. listed on CM?
Yes
Na
IAA
I S. WCre bubblus pius4ml !, ea -size" (1,4'ur 6mm in diamelcr) in am VOA vWg?
Ycs
No ❑
NA ❑
19, W ere all metalsjEJdrt.VlHLM/nutrient samples rftcivcd at a pH of e2?
yes 0
No El
-N--A'7
20. Were all cyan ide and/or sulfide samples received at a pH -r12?
Ycs ❑
No ❑
NA a21.
Were all applicable 1-H3gXK'cyaniderphenol ({0,2n1gIL) satuples free of
residual chlorine?
Yas
No
NA f 3'
22, W= collection tcm cratum documented on the COC for NC: samples!
Yea ❑
No ❑
NA ©'
23. Were client rcmarkairequests (i.e. requested dilutions, M&'1 T.) desigI itions,
ew—) correctly transcri'bcd from the COC into the cclmrmnt wction in LINIS?
Yes hta 24. Was the; quotc number used taken from the Container label?
Sample Prewrvotlon (MiW be completed for any samples) incorrectly preserved or Kith beadspace,)
Samples) were received incrwmtly presm1ed and wcrc: adjusted
accordingly in sam le mceivin with -2SO4 HN0i HC1 Na0 usipA SR #
Samples) ►vcrc recciv A with buhhles _'C, tom in diameter.
sltrra le(s) weft received with TRC >0.2 m L If 921 is No)
.SC Thinking Water Project Sample(s) pH verified to be > 2 by Date:
Sample(tr were Roc received at u PH of <2 and were zi 'uswd accnrdin ly uqing SR#
Sample labels a iod by-- verified h : C' Date; "Z.3
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Leval 1 Reponv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Semiannual
Lot Number:P123047
Date Completed:10/02/2014
7iTk
TVL-C-41
Kelly M. Maberry
Project Manager
t3 �Fl /LCC,j��
4�. {
i 71 r=
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
• • • 0 s • • a
Shealy Environmental Services, Inc. Page: f of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No; 5639
Case Narrative
Rohm And Haas Company
Lot Number: P123047
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (DAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the,Shealy Project Manager listed on the cover page
Inorganic Non -Metals
Samples -001 and -002 were received outside of the 48 hour holding time.
The Biochemical Oxygen Demand (BOO) result for samples -001 and -002 has been reported as less than the stated value due to oxygen depletion
of less than 2.0 mgll at each sample dilution. The sample was prepared with a standard series of dilutions based on historical data.
The SCF associated with BOD batch 9370 was 1.26 mg/L (valid range is 0.6 - 1,0 mg/L). All other QC were within limits and there is no effect on
the BOD result.
Shealy Environmental Services, Inc. Page: 2 of 8
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: P123047
Sample Number Sample.ID Matrix Date Sampled Date Received
001 SD0-#1 Cove Creek Aqueous 09/16/2014 2156 09/23/2014
002 SDO-92 ShippinglRecelving Aqueous 09/16/2014 2150 09/23/2014
(2 samples)
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: P123047
Sample Sample ID
Matrix
Parameter Method
Result O
Units
Page
001
SD0-#1 Cove Creek
Aqueous
BOD, 5 day SM 5210131-
CO 76
mg/L
5
001
SD0-#1 Cove Creek
Aqueous
TSS SM 25400-
44
mg/L
5
001
SDO-#1 Cove Creek
Aqueous
Zinc 200.8
63
ugIL
6
002
SD042 Shipping/Receiving
Aqueous
BOD, 5 day SM 5210B-
2.9 76
mg/L
7
002
SDO-#2 Shipping/Receiving
Aqueous
TSS SM 2540D-
28
mg/L
7
002
SDO-#2 Shipping/Receiving
Aqueous
Zinc 200.8
76
ug1L
8
(6 detections)
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Client: Rohm And Haas Company Laboratory ID: P123047-001
Description: SD041 Cove Creek Matrix: Aqueous
Date Sampled:09/16/2014 2156
Date Received: 0912312014
Run Prep Method Analytical Method
Dilution Analysis Date
Analyst Prep Date
Batch
1 (BOD, 5 day) SM 52108-2011
1 09/29/2014 1030
ME=V 09/24/2014 0851
9370
1 (pH) SM 4500-H B-2011
1 09/24/2014 1606
HMA
56786
1 (TSS) SM 254OD-2011
1 09/23/2014 2141
HMA
56703
CAS Analytical
Parameter _ _ _ _ _
_ Number Method
Result 0 PQL
Units Run
SOD, 5 day
SM 521OB-20
4.0 76 2.0
mg/L 1
PH
SM 4500-H B
6.57
su 1
TSS
SM 254OD-20
44 5.0
mglL 1
Footnote(s): 6-110. depletion < 2.00 mglL 7-SCF Out of range
PQL - Practical quantitaCon Iimit B = Detected in the method bank E = Quantitabon of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a `W"
Shealy Environmental Services, Inc. Page: 5 of 8
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Client: Rohm And Haas Company Laboratory ID: P123047-001
Description: SD041 Cove Creek Matrix: Aqueous
Date Sampled:09/1612014 2156
Date Received:09/23/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200,2 200.8 1 09/29/2014 2140 6NW 09/26/2014 1715 56986
CAS Analytical
Parameter _ Number Method Result Q PQL Units Run
Zinc 7440-66-6 200.8 63 10 ug/L 1
Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF ut o range
PQL = Practical quantitation limit 8 - Detected in the method blank E = Quaniltation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD Oetween two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W'
Shealy Environmental Services, Inc. Page: 6 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com Level 1 Report v2.1

nsVl W"IssV asV@0-11 Gb\QAIV
Client: Rohm And Haas Company Laboratory ID: P123047-002
Description: SDO-#2 Shipping/Receiving Matrix: Aqueous
Date Sampled:09/16/2014 2150
Date Received:09/23/2014
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(BOD, 5 day) SM 521OB-2011
1 09/29/2014 1030 MEV
09/24/2014 0851
9370
1
(pH) SM 4500-H B-2011
1 09/24/2014 1606 HMA
56786
1
(TSS) SM 254OD-2011
1 09/23/2014 2141 HMA
56703
CAS Analytical
Parameter
Number Mgthod
Result 0
POL
Units Run
80D, 5 day
SM 52108-20
2.9 76
2.0
mg/L 1
PH
SM 4500-H 8
6.9
su 1
TSS
SM 2540D-20
28
2.5
mg/L 1
Footnote(s): 6-0.0, depletion < 2.00 mg/L 7-SCF Out of range
POL - Practical quantitation limit e = Detected in the method blank E - Ouamitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J - Estimated result a POL and > MDL P = The RPD between two GC columns exceeds 40% N w Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page. 7 of 8
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4 V 2 -. f l V
Client: Rohm And Haas Company Laboratory ID: PI23047-002
Description: SDO-+<!2 Shipping/Receiving Matrix: Aqueous
Date Sampled:09/1612014 2150
Date Received:09/23/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date . Batch
1 200.2 200.8 1 09/29/2014 2155 BNW 09/26/2014 1715 56986
CAS Analytical
Parameter Number Method Result 0 POL Units Run
Zinc 7440-66-6 200.8 76 10 ug/L 1
Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range
POL = Practical quantitation limit 9 = Detected in the method blank E = Quantization of compound exceeded the calibration range H = Out of holding time
ND - Not detected at or above the POL J = Estimated result -z POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on ad ry weight basis unrass flagged with a "W'
Shealy Environmental Services, Inc. Page: 8 of 8
106 Vantage Point Orive West Columbia, SC 29172 [phone] Fax (803),791.91 11 www,sheatylab.com Level i Report v2.1

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106 Vantage Paint Drive
Was] CotuFn ia, -South Carolfna 29172
7 alephone No. (B03) f91-9MO Fax No. (St}3) 791-9111
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SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Emimnmmtnl Smv:rr_s, Ino.
thwurnrm Nuailt—wr F At?I71h
Ite�ixr�mttlurnh.rr Is
NBC I id' 1
KepbCeg DOW 1113MIA h
Eitective Date: 137! 1914
Simple Receipt Checklist (SRC)
Client: sr NA�� Cwler lnspoeted byldtate: �.� f acts a%. I.ot _;1q'
No ❑
fir. W= � le ms listed am the [RUC?
No ❑
7. Were sam ]t IDs listed on all Sample cmtainers?
qyesNoo
No
A. Was collection date Lime listed cot the COO?
No ❑
_&
9. Was collection date & time listed on all sample containers'?
1 10. Did all wabtain= label inluiinbtiuu 1pdale time) aW= with the COC?
Yes
0 No
11. Were testq to be =formed listed on the COUI
Yea
EF No
12. TNd all tAm fee a M%v in the ro er sxt misters fur chub teal?
No ©
11 Did all oontainers urive in ood oonditiuei unbroke lids on etc. ?
UyCS
No ❑
14. Waa adequate scam le volume available?
Yes ❑
No
15. Wa-e all samples received within ;i the holding time or 46 hours. whivltcver
corns best?
Yea
No
16. W= AnX mWlog umiaintzw nisxin .
vcs ❑
No
17. Were tI.Ift aaX zxce*s s6tu las not listed Ian MCI
Yes ❑
No
NA
18. Were bubbles prc=1 >. 2ua-size:" (1,b"ur 6mm in diametcr) in any VOA vials'?
YcA
No ❑
NA ❑
19, W ere all tnetal00&G114EM/nutrient samples received at a p1l of <2? -
Yea 01
No El
NA
20. Were all c art.ide and/or sulfide sam lea recciv*d at a pH >12?
Ycs C]
No ❑
NA O
21. Were all applicable N-H3fMX`cyaui&pheno1(-t0.2nigCL) samples free: of
residual chlorite?
Yes 0
—NoM
NA 0'
22. Wrsc collection temperatures, docunumded on the COC for NC samples'!
Yes ❑ I
No C]
NA W
23' W err client remarksirequcsts (ix. requested dihrtiong, M&MST) detail;r> lions,
etc...) uuffcctl tiurtxcrilmd frctm the COC into the comment section in LINTS?
Yes
No
24. Was the SHote ntunber used taken from the container label?
ople Prewrvalian (lt. usl br` completod for any Umple(s) incorrectly preserved or with hcsdspeiwe, )
1ple(a;) were received incorrectly preserved and wury adjuster
ordingly in sam le receiving with aSQa Oi HCI Na4 uslia SR A
ttpleis) wcrc ruLciv&A with bubhlm >6 tom in diameter,
n lt:(s were reooivrd with TRC >0,2 rn t If 921 is No)
T)riWdng Water Projoct Sample(s) pH verified to be > 2 by Date:
nple(s) were not Iveeived at a pH of <'2 and wcrc adjusted aocordin lv using SiO
rmle labels axtnlied bye t-^C�y-v-, Veri red bv: ` -C% C X—e,, Dare:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 291172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name:Stormwater
Lot Numbe'r:13130054
Date Completed:10/06/2014
7q11_WEy
Kelly M. Maberry
Project Manager
SEC xµ xCCdgQ,
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
• • • 1 • 0 • • •
Shealy Environmental Services, Inc. Page: i of 5
106 vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: P130054
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the DAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Inorganic Non -Metals
The Biochemical Oxygen Demand (BOD) results for samples -001 and -002 have been reported as less than the stated value due to oxygen
depletion of less than 2.0 mg1l at each sample dilution. The samples were prepared with a standard series of dilutions based on historical data.
Shealy Environmental Services, Inc.. Page: 2 of 5
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: P130054
Sample Number Sample iD Matrix Date Sampled Date Received
001 SDO #1 Cove Creek Aqueous 09/29/2014 1444 09/30/2014
002 SD042 Shipping/Receiving Aqueous 09/29/2014 1443 09/30/2014
(2 samples)
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Client: Rohm And Haas Company Laboratory ID: P130054-001
Description: SDO #1 Cove Creek Matrix; Aqueous
Date Sampled:09129/2014 1444
Date Received:09/30/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (BOO, 5 day) SM 521OB-2011 1 10/06/2014 1055 MEV 10/01/2014 1100 9386
CAS Analytical
Parameter Number Method Result O POL Units Run
BOD, 5 day R SM 521OB-20 _ " ND 6 12 mg/L 1
Footnote(s): 6-D.O. depletion < 2.00 mg/L
PQL = Practical quart Cation limit B = Detected In the method blank E - Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J - Estimated result < PGL and > MDL P = The qPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W'
Shealy Environmental Services, Inc. Page: 4 of 5
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nrvra�,aaruv �w�r—�uvaa+�.y
Ctient:Rohm And Haas Company Laboratory iD: P130054-002
Description: SDO #2 Shipping/Receiving Matrix: Aqueous
Date Sampled:09/29/2014 1443
Date Received:09130/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (BOD, 5 day) SM 521OB-2011 1 10/06/2014 1055 MEV 10/01/2014 1100 9386
CAS Analytical
Parameter Number Method Result 0 POL Units Run
BOD, 5 day SM 5210B-20 2.1 6 2.0 mg/L 1
Footnote(s): it depletion < 2.00 mglL
POL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO - Not detected at or above the POL J = Estimated result c POL and > MDL P = The RPO between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a °W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Coiumbia, SC 29172 [phone] Fax [phone] www.shealylab com Level 1 Report v2.1

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Shealy Environmental Services, Inc.
106 Varfage Point Drive
West Columbia, South Carolina 29172
Telephone Rio. [phone] Fax No. [phone]
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Note: All samples are retained for six weeks from receipt tAB
unless other arras emenft are made.
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I

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Erivironmesual Sertixs, Inc- I'ap 1 of I
Ex"arp,T1 NtJM1Kr. F-A"16 tiel.+IWes Date: 0300A4
Kevision Numbei: 15 Effecti ve Pate: 07 1 S' A
Sample Receipt Checklist (SRC)
Client; �r re, ,F-„ „ Owler frispm,e d hy'rinte: r cat U-4 P:
Means of receipt ZSESI ❑ Client ❑ UPS ❑ FedEx ❑ Airborne Exp _ ❑ Other
Yes
No l _ Were custody seals Eesent on the cooler?
Yes LJ
I No NA 2. If uustody sE ils wen prosMil., wcru Ih�2 inimul and unbroken?
doter ID10riei.nal t"Verattlre upon rL°oeipl/Derived (calrectetl) tempernture upon receipt;
j IDISC , °C I I nC / f 111C if l °C
Method: ❑ TcmpmaturG lank Agtlitlst Holtks IR Gun IA: #3 IR Gun CcirrtmiOn. Ffictor: G.`',"C
Method of coolant: [TWct Icc ❑ Bitic [cc ❑ Pry Ice ❑Neon
Ycs ❑
No ❑
NA
3. If temperature: of any viler exceeded G.0°C, was Project Manager notified?
PM noliflud by SRC, pllolle, note (circle oue), other:
(For coolers received via commercial courier, P'.1'Js are to be notified
iminediately.)
Yes
❑
No
(]
NA, Ol
4. Is the wmmtmr ial wvnyr'a"king iiho m"hO to this femn?
Ycs
Nu
❑
5. Were proper custody procedures re1u uished'received followed:'
Y&A
❑ I
No
❑
NA
5a Wem earn les rolinquishcd bK client to commercial courier?
Yes
Nu
6. Were sample IDs listed on the COC?
Yes
9
No
❑
7., Were sample IDs listed on all smnplc containers?
Yes
NoU
S. Was c ollwion date & time listed on the COC7
Yes
Non
9. Was collection date & time listed on 131.1 salsa le contalinera'?
lvn
❑
10. Did all oontuinar label ittforntarinfl TD, date, lime) a3 nee with the COC?
Nu
❑
11. Were tests to bee erformed listed on the COC?
Ics
No
❑
12, Did all a Irs arrive in the rcaprr ctmlainer's for each kst?
No
❑
13. Did allcontainers arrive in ood condition unbroken, lids on etc. ?
No
❑
14. Was ad to sample volume available?
Yes le
No ❑
15. Were all samples received within',i the holding Iimc or 48 hours, whiuhcwr
comes Frrst?
V-e ❑
No
_
16. Were any sam lcs containers n ia3in
Yes
No
17. Were there an excess sa lea not listed on CrUC:?
Yes ❑
No ❑
NA
I R. Wem bubblerti lwvsent "aea-sin" ':"ar fnnm in diameter) in imy VOA vials?
Ycs
NA 2r
19, Were al.l metaWO&GdHIE.M+nutrient s ]cs receiived of a pli of 1.2?
_Eq.Q.
Yet, ❑
No ❑
NA ff
20. Were alla: anidc andrur salfldr stunples reqeived at a H >12?
�,cb El
No ❑
NA
21. Were all applicable N113i l'lCNlcyanidelphenol (��Uwp l) samples free of
residual chlorine?
Yes ❑
No ❑
ILIA ff
22. Were collcctinn telluperaturcs documented on the COG for NC samples?
Yes ❑
No ❑
NA 0'
23. Were client remarks1requests (i.e. requested dilutions, IvIS�11 U) designations,
etc.. conwAly transcribed from the COC- into the comment section in .LIMS?
Yes
Na
2 ,Was the quote number uxod taken from the; c ontaincr label?
Sample Preservation (Must be completed for any sample(%) incarrectly pre=r ed or with headspace)
samplu(ti) were received incorrectly preserved and were adjusted
w*ardjnj& in sam le receiving with H2SO4Os HGI„YaIOH usin SIt #
SawleLsl were rcccivcd with bubbles 36 nmt in diamcwr.
sample(s) wem received with TRC -0.2 m L, If #21 is N2
SC Drinking Water Project Sample(s) pH verified to be } 2 by Bate:
Sa lo(r;} werc not received at a pll of <2 and were ad usted accordingly using SRN
Sam le labels appliEd b : Verified b . Date;
Comma:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheafylab.com Levet 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Stormwater
Lot Number:P130054
Date Completed:10/06/2014
71W.Tyby
Kelly M. Maberry
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: P130054
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Inorganic Non -Metals
The Biochemical Oxygen Demand (BOD) results for samples -001 and -002 have been reported as less than the stated value due to oxygen
depletion of less than 2.0 mgll at each sample dilution. The samples were prepared with a standard series of dilutions based on historical data.
Shealy Environmental Services, Inc. Page: 2 of 5
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: P130054
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO #1 Cove Creek Aqueous 09/29/2014 1444 09/30/2014
002 SDO #2 Shipping/Receiving Aqueous 09/29/2014 1443 09/30/2014
(2 samples)
Shealy Environmental Services, Inc. Page: 3 of 5
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Client: Rohm And Haas Company Laboratory ID: P130054-001
Description: SDO #1 Cove Creek Matrix: Aqueous
Date Sampled:09/29/2014 1444
Date Received:09/30/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (BOD, 5 day) SM 521OB-2011 1 10/06/2014 1055 MEV 10/01/2014 1100 9386
CAS Analytical
Parameter Number Method Result 0 POL Units Run
BOD, 5 day SM 52106-20 ND 6 12 mg/L i
Footnote(s): 6-D.O. depletion < 2.00 mg/L
POL - Practical quantitation Ilmit B = Detected in the method blank E = Ouantitaticn of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result < POL and > MDL P - The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W'
Shealy Environmental Services, Inc. Page: 4 of 5
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n rveyuruv rrvr rrrra.aury
CI'ient:Rohm And Haas Company laboratory ID: PI30054-002
Description: SDO #2 Shipping/Receiving Matrix: Aqueous
Date Sampled:09/29/2014 1443
Date Received:09/30/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (60D, 5 day) SM 521OB-2011 1 10/06/2014 1055 MEV 10/01/2014 1100 9386
CAS Analytical
Parameter Number Method Result 0 POL Units Run
BOD, 5 day SM 521OB-20 2.1 6 _ 2.0 mg/L 1
Footnote(s), 6-D.0. depletion < 2.00 mg/L
POL = Practical quanlitatlon limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated resull c PQLand > MDL P = The RPD between twc GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless Bagged with a 'W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 (e03) 791.9700 Fax [phone] www.sheafylab.com Levef 1 Report v2 1

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Chain of Custody Record
Shealy Environmental Services, Inc.
1DO Vardage Poird Drive
West Columbia, South Carolina 29172
Telephone Into. 1803) 791-9700 Fax No. [phone]
www.showoo 'U"
Dumber 2 6 5 9 0
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OC Ftogriraments (sprtidryl
Pamble Hazard Identtfi zWn
t!arard :3FWrmmbM 1396t irtt'rl UPctOM oUnirrraan
1. €i I e(i by i &ampler
Date
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1. Received r
Date
9T 304Y'
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4. FteliMisW by
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Note: All s8inptes are Malned for Six weeks froth receipt
unless otter arrangements are made.
iLAS USE ONLY
Fl"-BW on ke Pa* 17Yea o Mo u In Padr
Re* l emp •SZ "C
Temp. BW* 0 Y ! B*Fi
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0

SHEALY ENVIRONMENTAL SERVICES INC.
Shealy envinmmenUl Scrvia a, he. Page 1 o81
AoewsuM Number F ALW 16 Replaces Umcr 03et)'V14
Revision Nu[abcr. 15 EfTtrtive rjow 0?11S'Ldl
Sample Receipt Checklist (SRC)
Client: '--4'yyc' 4 , _ Cooler Inspected byo'date:Mc,rn i !: �UA 9: Q\
Means of receipt. ZSL'Sl ❑ Client ❑ UPS ❑ FedEx ❑ Airborne 1=acp ^ � ❑ Other
Yes 17
1 No Lgff
I
1. Were Gusto seals esettt on the cooler?
Yes
No Ll
I NAB
2. If uustudy 3Cahi wcrea pruseni, wcru 1buy lrllacl "d ttnbraktat?
Cooler ID!Original temperature upon reoeipt/Derived (corrected) tern-perature upon receipt:
i D-\ to .S °C I ,, eC f f 'C f f 0C
Method: ❑ TLmWeraturc plank Agttiwo Ek)ltles IR Gtin ID] 43 III. Caen Curm-ciiion F11c:lor: G •'-%,°C
Method of coolant: /[ Wet Ice ❑ Blue Ii:c ❑ Dry Ice ❑ Nuno
Yos ❑
No ©
NA
1 if temperature of any woler exceeded 6.00(; was Project Manager notified?
PM ljudEud by SRC, plione, tote (circle one). other:
(For coolers received via commercial courier, PNIs are to be notified
immediately.)
Ye ❑
No
�--^�
Q
N.A
4is the [:ornwurt.iM wur'icr'a pnking kill ill:t4010 Ira thin Forte!?
YCS
No
❑
_
5. Were proper custody�tocedures refin rtishedlreceived Followed'!
Yes ❑
No
❑
NA
5a Wem saris les r0inquished b client to commcrcial courier?
Yes
No
6. Were sample IDs listed on the COC?
Yes
No
❑
?. Were sample: DDls listed on all sam lc containers?
Yes
No
8. Was wllcction elate & time listed on the COC?
Yes
No
9, Was collection date &time listed on all sample containers?
Y
Na
❑
10, Nd all containerlabel infortnation i10, date, tiene) agree with the COC?
Yea
Nu
❑
11. Were tests to be performed listed on the COC?
YeR
No
❑
12, Did all sENlys arrive; in lhr propr cunlai.tters lur each trnt7
Yes
No
❑
13. Did all containers arrive in good condition Junbroken, lids on etc.)?
Ycs
No
❑
14. Was a to sample voltune available?
Yes
No ❑
15, Were all samples received within 1/i the holding time etir 48 hum, whichever
comes first?
Yes ❑
No
16. Were any slam Ics containers missin
Yes
No
17. Were there my excess sa des not listed on C (X; ,'
Yes ❑
No ❑
NA
I R, Wcr+e bubbles 1xvsent ?" -size°' ?."or 6mm in diameter) in auy VOA vials?
Ycs
No
NA O'
1.9, Were ail metaWO&.G'HEMlnutrient samples rec6ved al a pH of --2?
Yefi ❑
No ❑
NA
20. Werc all cyanide andlor sulfide sump Les Yeceived at a 1-1 > 12?
Ycs ❑
No ❑
NA
21. Were all applicable NIIJ KNieyartidelphenol (<0,2mg+'L) samples free of
residual chlorine'?
Yes 0
No ❑
NA 9
22. Were collection tem ratures docurncnLed on the COC for NC stunples?
Yes ❑
No ❑
NA
23. Were client remarks/requests (i.e. requested dilutions, NISiMS1) designations,
etc_.. Correctly transcribed from the CCIC into the oalnment section in L MS?
Yes
No
24. W as the quote number used taken fum the container label? _
Sample Preservatlon (Must be oornpteted fnr any sample(q) incorrectly preserved or withheadspaee.)
satnplc(li were wtived incorrectly preserved acid were adjusted
acccardin in sate le receiving with WiSO4JJN0j I1CI,Na01.1) using, sit is
sample(s) were received with bubbles >6 mm in diamnt.cr.
Sa le s u," received xZth TRC -0.2 m 'L Qf#21 is No
SC Drinking Waier Project Sarnple(s) pH verified to be > 2 by _ Bate:
sa lr~(n) were not received at a PI of <2 and were adjusted accordingly using SR#
Sam le labels appliod b G•�Vyj Verified by. M6 I= Date:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 {803) 791-9700 Fax [phone] www.shealylab.com Lovell Reportv2,1

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
October 12, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Semi Annual Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Semi -Annual Storm water Discharge Monitoring Report for
the Rohm and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386). The samples were collected on
09/16/2014 & 09/29/2014. The Semi- annual sample data for the month of September showed elevated
benchmark values at the (SDO-002) outfall for Zinc. Sampling is now being conducted monthly at the
Shipping Outfall (SDO-002) for zinc under Tier Two permit requirements. All other results were within
the limits of our permit.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
V rlr�/u' •�
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

mN
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Permit ft�. G mp�gftrWg reportshA be rcc&pd.lby,ffie vhwou . no 30 days-kom -
Cgrar=f& of Coverage NW33ber. NC
the 4W* ft faeMq r0ches the =Vft r=Wb boin'theta l
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For 06 SWU-246-1,1260.9
Page I of 2
L�

SHEALY ENVIRONMENTAL SERVICES, INC.
f
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Lot Number:PG14036
Date Completed:07/17/2014
7ajw_wt'(
Kelly M. Maberry
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated, documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist,
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Polnt Drlve West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2 1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PG14036
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PG14036
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO-02 Shipping & Recieving Aqueous 07/03/2014 2050 07/14/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PG14436
Sample Sample ID Matrix - Parameter Method Result Q Units Page
001 SDO-02 Shipping & Aqueous Zinc 200.8 110 ug/L 5
0 detection)
Shealy Environmental Services, Inc. Page. 4 of 5
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I V I -IfI V
Client:Rohm And Haas Company Laboratory ID: PG14036-001
Description•, SDO-02 Shipping a Recieving Matrix: Aqueous
Date Sampled:07/03/2014 2050
Date Received:07/14/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
r 1 200.2 200.8 1 07/17/2014 0348 BNW 07/16/2014 1625 51530
CAS Analytical
Parameter Number Method Result 0 POL Units Run
Zinc 7440-66-6 200.8 110 10 ug/L 1
POL= Practical quantization limit e = Detected in the method blank E = Quantltation of compound exceeded the calibration range H - Out of holding time
ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC Columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive west Columbia, SC 29172 [phone] Fax [phone] it www.shealylab.com Level 1 Report v2.1

N
A
CWA ! WDES
19 Chain of Custody Record
Sheaty Environmental Services, Im-
106 Vantage Paint Oreve
West Columbla. South Carolina 29172
Telephone No. [phone] Fax No. [phone]
w+xnr.st*"sb.wrn
Number 21479
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Andy Baruaduc+eml,i setviom trx. PAD 1 or 1
DDOW tl Wumbrs ww-016 Acphm Date.- OVM 3
Revtaioe plumber. 14 Efftfvt Dau. t13MY14
S le Receipt Checklist (SRC)
Client:. EG i��� er �pdcted by/date:-tJ'.tfq.Lot #: p-am pbu
Meam of mccipt 0SIES1 [] Client ❑ UPS ❑ FeclFat ❑ Airborne Ertp ❑ Othcr
Yes
0 1No
1, Were custody seals preumt on the cooler?
Yea
No
NA
2. If ctilstod seals wem were *y .intact and imbroken?
Cooler mvoriginal temperature upon receipuVedved (correcMd) temgrerauturae upon tewipt:
1 y 1 _c /- I- -°C l I °C
°C __
lwiethod: ❑ TemperatweBlank Against bottles IR Gun ID: 03 IR Gun Correction Factor. f-7•I'C
_
Method of coolant et Ice Blue TCe �] 1]t'V Icr None
Yes ❑ .
No ❑
NA
3. If terAvA tone of tiny cooler ersaendod 6.O°C, was Praj=t Manz a nod
PM notified by SRC. phone, hate (circle one), other:
(R-W coolers received via commercial courier, PMs are to be notified
imnwAatel )
Yes
UNo
NA 0
4. Is the commercial courkr's sr attached to dhis form?
Yes
No
S. Were proUr custad oczdures tell uisbedheceiveti followed?
Yes
❑tie
❑
bTA
5a Were samples relinquished client to commercial courier?
Yes
6. W= wnple Ma listed on the COC?
Yes
7. Wem MMIe ID9 listed on all saTple containers?
Yes
C34X0
S. Was collection date & tints listed on the COC?
Yes
0
LNO
❑
9. Was collection date & tim listed on all contaiam?
Yes
No
11
Cl
la. Did all conttdner Iabei inforrratian (ID, data, time) !M with the OOC?
Yes
al
No
11. Were tests to be otmed listed on the COC?
Yes
LXJqo
❑
12. Did all san4&s arrive in the er containers for each test?
Ycs
u
11
13. Did all contamcn arrive in good.condition. (unLr2kM lids on ctc. 7
Yes
Na
❑
14. Was ate sample volume available?
No
�,�.t�
15. Were all samples received within y4 the holding tithe or 48 bouts. whichever
rorttea first?
Yes
No
16. Werc an s lcs containers rnissin ?
'Yes
No
7. Were there au eacoess les not listed on COC?
Yes
n ❑
NA
18. Were bubbles resent >" ea -size" 'A"or 6mrn in diarneter) in any VOA vials?
YGs
No
NA
19. Were all tnetalFJ0&G/EIEM/nlstl:ient satn leg received at tt H of Q?
Yes
No
NA
20. Were all cyanide and/or sulfide les received at a H >12?
Yes ❑
No [I
NA
1. Wcre all applicable NN3frKAVcyattide/phenol (<D.2'mg/L) samples free of
residual chlorine?
Yes ❑
Na
NA
22. Were collection to res documented on the COC for NC sam lcs7
Yes []
No
NA
23. IWcrc client r xegtlests (i.e. rerque cl dilutions. MSIMSD designations,
etc... carrr�cll transcribed from the COC into the D ntlmenl section in LEAS?
Yes ❑
N
2d, Was the quote number used taken from the container label?
Sample Prem vation (Must be corTleted for any sample(s) incorrectly preserved nr with hearist ace.)
sample(s) were r+et:cived incorrectly preserved and wem adjusted
accordingly in L&Mle receiving with (H2804.HNO3.HCI.Na0H) using SR #
Sa le(s) were tt ecived with bubbles >6 mm in diumter.
S l s were received %ith TRC >01 #21 is No
SC Drinidag Wawr Project Sarrrple(s) pH verified to be >2 by pate:
S lG s were not received at a H of >2 and were ad'uAcd accardin us`5RIt
5 le labels gpeed b Verified b : Date:
Cp►nments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Reportv2.1

•
Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
July 25, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr. Road (Permit #NCS 000386) for the month of July, 2014 Zinc sampling.
Sampling is now being conducted monthly at Outfall SDO-002, per Tier 11 requirements in permit. The
sample result at outfall SDO-002 was not within the benchmark value for Zinc. Sample results will be
submitted as a representative rain event occurs for the month of July until three consecutive below
benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

i
a
�,.
}
.: ��:
Fr
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01
Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
November 25, 2014
RECEIVED
DEC 17 2014
CENTR,gL FILES
DWI? SECTION
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of November, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 were within the benchmark value for Zinc. Sample results
will be submitted as a representative rain event occurs for the month of December until three
consecutive below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sin erely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Naas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Stormwater
Lot Number:PK18059
Date Completed:11/23/2014
Kelly M. Maberry
Project Manager
'S
4
This report shalt not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] t www.shealylab.com Level 1 Report v2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PK18059
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SQPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP. SOPS or policies are qualified on the results page or discussed below.
if you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Poim Drive West Columbia, SC 29172 [phone] Fax (B03) 791.9111 www.shealylab.com Level 1 Report v2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PK18059
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SOO Ill Shipping/Receiving Aqueous Zinc 200.8 65 ug/L 5
(t detection)
Shealy Environmental Services, Inc, Page: 4 of 5
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] www.Shealylab.com Level 1 Aeponv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PK18059
Sample Number Sample ID Matrix Bate Sampled Date Received
001 SRO #2 Shipping/Receiving Storm Water Sample Aqueous 11/17/2014 0429 11/18/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab,com Level Reportv2A

ICP-MS
Client:Rohm And Haas Company Laboratory ID: PKi8059-001
Description: SDO rig Shipping/Receiving Storm Water Sample Matrix: Aqueous
Date Sampied:11/17/2014 0429
Date Fie ceived:11/1812014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 1 1 /21 /2014 2109 B N W 11 /20/2014 0734 61303
CAS Analytical
Parameter Number Molhad Result Q PQI_ Units Run
Zinc 7440-66-6 200.8 65 10 ug/L 1
POL - Pracucal puantitation limit B - Detected in the method blank E = Ouantitation of compound exceeded the cisi bratlon range H • Out of holding time
ND - Not defected at or above the PQL J = Estimated result < PDL and > MDL P - The RPD between two GC columns exceeds 40% N . Recovery is out of crnar4
Where applicable, all spkl sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Report v2.1

Sheaty Envimnmenlaf Services, Inc.
f9 101i Vantage Point Drive
Chain of Custody Record West Colurnble. South Carolna 29172 Number 26445
Telephone No. (803) 791-97W Fax Na. [phone]
wWw.st>wyLitr Dorn
Client
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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Stormwater
Lot Number:PK18059
Date Completed:11/23/2014
7, r
�w
Kelly M. Maberry
Project Manager
AH A C C<)Ra'
y
fJ �
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Reportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 .
Case Narrative
Rohm And Haas Company
Lot Number: PK18059
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (DAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the DAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax {803) 791-9111 www.shealylab.com Level 1 Aeportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PK18059
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO #2 Shipping/Receiving Storm Water Sample Aqueous 11/17/2014 0429 11/18/2014
0 sample)
Shealy Environmental Services, Inc. Page- 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,sheelylab.com Level 1 Reportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PK18059
Sample Sample ID Matrix Parameter Method Result o Units Page
001 SOO #2 Shipping/Receiving Aqueous Zinc 200.8 65 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

ICP-MS
Client: Rohm And Haas Company Laboratory ID, PK18059-001
Description: SDO lit Shipping/Receiving Storm Water Sample Matrix: Aqueous
Date Sampled:ll/17/2014 0429
Date Received:11/18/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 11/21/2014 2109 BNW 11/20/2014 0734 61303
GAS Analytical
Parameter _ Number Method Result 0 T POL Units Run
Zinc 7440-66-6 200.8 65 10 ug/L 1
POL = Practical quanlilation limit 6 Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J . Estimated result < POL and a MDL P = The RPD between two OC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all Boll sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab.com Level i Report v2.1

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108 Vantage Point Drive
West Columbla, South Carolina 29172 Number 26445
Telephone No. (803) 79i I700 Fax Flo. [phone]
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sncaly MVtrof=cWfl1 ScrYieca, tne. Page 1 of 1
W-vumCrtt Ntmbcr. F-AL141 G ttaptwes Dow 31A Sr 14
Revision N'auutW47 14 rffWtive rjpw r U07"14
Sample Receipt Checklist (SRQ
Client: stir--� �U�c,cs Cooler Inspected byidate:l ]lam 1 L\`1 Loth.
Means of receipt: f atESI ❑ Client ❑ UPS D FodEy ❑ Airborne. Exp ❑ Other
Yes
_
Na
1. Were cuslod seals resent on the, cooler?
Yes
No--
INAff
12.lfrustod4scalfjwcruErcsoul,werr.:IhLyiritnitindimbrokcn7
Cooler ID/Original temperature upon reoeipt0erived (corrected) temperature upon receipt:
/"L u{ °C ! 1 °C ! I 11C ! °C
Method: . empuntlurt� 131auir ❑ Agnirut R011leu IP. Gull TD:, 4 IR C'run C orrecNnn Fuctor; Q • f'
Method Urvoolanr et Ice ❑ Blue Ice Diry Ice ❑ None
Yes ❑
No ❑
Moe
3. If temperature of any txioler exceeded 6.0°C, was Project Manager notified?
PM notified by SRC, phone, note (circle one), other:
(For coolers received via commercial courier, Phis are to be notified
immediately.)
Yes
❑
No 0
NA-0
4. Is the comrnnrcial cutuicr's packing s4ap twuhcd to 1hib form?
Ycs
No C1
L5. Wcm Fupercusiod procedures rrl uishetllrrceived followed?
Yes
No ❑
NA
Sa Were sam les relinquished by client to commercial courier?
o
6. Were sate le Ins listed on the COC?
o ❑�
7. Were sa,17 le IDS listed on all sample. containers?
4YesN,
o
B. Was W11f cation elate & Iirn.e lisped on the C QC'J'
❑
9. Was collection date & time listed on all sample containers'?
Ycs
RrNa-D
10. Did all container label inforrim lon TT), date, titne) a gee with the CW
Yes
RTNa
11. Were tests to be perfornied listed on the COC?
Yes
RT
No ❑
12. Did all sam les arrive in the comtainers t(rr each test?
Yes
PY
No 13
13. Did all containers arrive in good condition (uqbmkLc% lids on etc.)?
Yes
No ❑
14. Was a alc sample volvmc availmblc?
Yes
o ❑
15. Wcrc all samples rrt.rivcd within ! the holdi.ug time or 48 hours, whichever
comes first?
Yes
No
16, Were an • samp ter, containers; missin ►?
YCS D
Na
Na ❑
17. Were there any excess samples riot listed on COG?
Yes
NA
18. W=bubbles resent }" na-seize" '1X"or 6rnmi in diameter in an VOA vials?
Yes
No
NA ❑
19. Wczc all metals/OcYeWHEMinutrient samples received at a pH of f2?
Yes
No
NA
20. Were all cyanide and or sulfide sa lcs rcccived at a pH > 127
Yes ❑
No ❑
NA
21, Were all applicable NH3?TKNlcyanide/phenol (<O.2mgil.) samples free of
residual chlorine?
Yes
No ❑
NA
22• Were collection temperatures docunwated on the COC for NC. samples?
EE
Yes ❑ f
I
No ❑
NA
23, Were client rtmhL arksgtu:sts (i.e. requested dilutions, MS.74fSD &Esignations,
etc...) correctly transcribed from the 00C into the comment section in_LIMS?
Y" ❑
Nrr
24. Was the quotc number used taken .fCcan the conminer label?
Sample Proserwation (Must be completed fbr any samples) incorrectly preserveA or with head%tace.)
Samples) mere received incorrectly preserved and were adjusted
accordin Iv in sera le rzcei ' with i,SO`,HNO./,HCI.NsOH) using SR 4
Sample(s) were rectdved with bubbles>6 mm in diameter-
Sa1n Ie(s were mcejwvd with TRC >0.2 ma,'I- (if #21 is Vol
SC Drinking Water Project Sampl4s) pH vcriliod to bt~> 2 by Date:
Sam lr(s) were not received at a p1l of <2 and were adjusted accordingly usine SRN
Sara 1e labcls a lied b : Verified i*r~ Date:
Cammentsl:
Shealy Environmental Services, Inc.
106 Ventage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.t

Permit Number NCS 0 0 0 3 3 6
1 \EG&W DI5CHARGB OUTFALL (SDO)
RING REPORT
MAY 272014
CENTRAL ALES
DWQIBOG
FACILITY NAME UFP Elizabeth City, LLC
PERSON COLLECTING SAMPLE(S) tnsgp= h navi sane
CERTIFIED LABORATORY(S) Pri-Pn and Mp whnf _Lab ti
Lab 6
Part A: Specific Monitoring Rapireneents
Scanned
SAMPLES COLLECTED DURING CALENDAR YEAR: 2 014
('ILis monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Pasauotank _
PHONE.XO (2 5 2 13 3 8- 2 8 21
(SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes X po
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitories Requirements
OettaB
No.
Date
Sample
Collected
ism
00556
00530
00400
Total Flow
(if applicable)
Total
RabdM
Oil & Grease
(lf appl.)
Nan -polar
O&GIPPH
(Method 16"
SGT HRM), if
Total
Suspended
So"
pH
New Motor
011 Usage
and
MG
hsches
nWA
malt
Form SWU-247-062310
Page h of 2
—X.

STORM EVENT CAARACTERI[STiCS:
Date 3/17/2014
Total Event Precipitation (Inches): 0.5 (on 3 / 17) and 1.0 (on 3 / 18 )
Event Duration (hours): (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attu: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certlfy, under penalty of law, that this docent and all attachments were prepared under my direction or supervision In accordance with a
system designed to assure that qualified persound properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted h, to the best
of my knowledge and beliet, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
includim the posslILIft oMses and imptisotmgM for knowing violations."
(Signature of
5-
(Date)
Form SWU-247-062310
Page 2 of 2

Universal Forest Products
May 22, 2014
North Carolina Division of Water Quality
Surface Water Protection Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699
RE: Discharge Monitoring Report, Sample No. 10
UFP Elizabeth City; LLC
NPDES Permit: NCS000336
Dear Sir or Madam:
Enclosed please find the stormwater report for sample No. 10 at the above -referenced
facility.
Please do not hesitate to contact me at 616-365-1526 or rdickensaWbi.com if you have
any questions.
Thank you,
Robert Dickens
Regulatory Compliance Specialist
enclosure
2801 East Beltline NE Grand Rapids, Ml 49523 Tel: [phone] Fax: [phone] www.ufpi.com

a
16� 14-1.
REM
D= dib fadfity pafozm VeWqle Nfibftwmcc Ap"ties USM9 more than 55 g"ons of MOW mo= oil per "nth? yes --Ao
fym
")Mpkft.p@xt B)..
rw-cis:-venmDaa teu=CeAcoviumonitor!mRomurements
For; SWU-24&-1.12608
Page 1 of 2

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
June 20, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of June, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was not within the benchmark value for Zinc. Sample
results will be submitted as a representative rain event occurs for the month of July until three
consecutive below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOw RESTRICTED

• SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Lot Number:PF13052
Date Completed:06/20/2014
Kelly M. Maberry
Project Manager
�;gyp Lp� �,C�pR�4y
u rfl�
K
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report, Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Repon v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Fieid Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PF13052
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

• SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PF13052
Sample Number Sample ID Matrix Date Sampled Date Received
001 Zinc (#5D0-2) Storm Water Aqueous 06/08/2014 1356 06/13/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PP13052
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 Zinc (#i5DQ-2) Storm Water Aqueous Zinc 200.8 140 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point 0rive West Columbia, SC 29172 [phone] Fax [phone] www,sheaiylab.com Level 1 Report v2.1

we -IFiV
+ CtientRohm And Haas Company Laboratory ID'. PF13052-001
Description: Zinc (#5D0-2) Storm Water Matrix: Aqueous
Date Sarnpled.06/08/2014 1356
Date Received:06/13/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200,2 200.8 1 06/18/2014 0314 CDF 06/17/2014 1102 49184
CAS Analytical
Parameter - - _Number Method Result 0 _ POL Units Run
Zinc 7440-66-6 200.8 140 10 ug/L 1
POL = Practical quantltaticn limit B = Detected in the method blank E - Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimatad result < PQL and > MDL P = The RPD between two GC cciumns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level t Report v2.1

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SHEALY ENVIRONMENTAL SERVICES9 INC.
.Shealy lntirt�nmcrnnt ,Snrvi „rt, 4 �e.
De .,umew Somber- f-XD-0 16
Rmsian ir'umbm-, t=
Page t of.1
Ei1et6ve t?dte:03rti7,rtd
Sample Receipt Checklist (SRC}
Client. .. r `t l`1')I d' Cnc)ler lnspc: tcd byldate: r" J ib-! v, Lot#: J—y /?C _
Mewls of receipt: F1 SESI Cl Client ❑ UPS ❑ 1=edNx ❑ Airburne Exp ❑ t-ther
yes No 1. Wrrc cttstnrt vials present oil tilt! t:t.,0c.0
Yes 'Vra NAP 2. If custod.y seals wvw. resent, were 04t ' intact and tinhmkerl?
CoolerlD/OflginAl winporttiureup0iimcc.iPUDcriverl (.corrr..ctcd) tettlperatuie upon n:ccipt:
p ° F ot" r e `'C`:
Tw�erltc►t1: ❑ '1`etrt .:rtuurt, flan..,.,._. -� C .�.,...�..,,.�..._..
r � :'�� _ `�C I
kainst: I�r�ttli.5 IFt Gun T} iR Gun C"€rlcctiort F tkct �r:
Method of ecoolmoll: r7l"'Oget lee FI R111e lust M Dry Ice F-1 None
Vr-5 ❑
tiC, ❑
NA QQ
I. if temperature of any cuulcr excee led 6.U'C. was Project lanugC.r nntifiPd'�
YM notified by SRC, phone,, note. (Circle erne), (rtlu.r:
(For coolers rcceived Via Cornnlercial Cf)Ul lCI', P.NC ;Ara to be notified
.� iintiiediiilcl ',.)
N" ❑
1A ®
-1. Is the conunerr:ial cotlriet''S packing slip attuchcd tU this forme
YL,�
-Nr, F1
- Were prnp�-r custody pract:Jurus (rclin uishedlrecei%vd) followed,
7eR ❑
11Z ❑
'q
y,
Se, Were samples Tt lin(I"1shed I?y client to C(7k11nlelcttll L(rktri:a:r?
"es
3a, ❑
G. Vi" out.:almple 10s listed can the C'C?r;. t
N'C8 Vca
11140
7. Were -yarn 1c Ms listed on all 5att1 le containers?
Yes
An ❑
8, Was collcctian date & drix: listed on the C OC':'
Yes:
El9.
Was collection date & time listed tot all sam le containers"!
Yesa
10. Did all container label infornlatiCul (113, date, time agree v,tith the CO Y
ye:
O
v ❑
f
I I. Were tests to be Purformcd li:rted on the COC?
Yrs
{Q
Xj ❑
1
12, lair) all sairt le.s arrive in the tear containers for each test 1
Yes
O,Nn.cl
1�. Did all containem arfive, in gwd condition (unhrok-en, lies~ on, rtc•..)'.1
Yes
No L1
�
14, Was a dv(piate Sampleyoluaw availahli ?
�
Ye"s
n
15, Were all SUMPICK, 1"L'Ce1l' d within 16 the hoidlllg t1mc or-18 hours, Lwhic- ]ever
colnes first?
Yes ❑
1 16. WLra any samples containers trlistiivg?
Yes I
Na
A7. Were there an • ex( rss samples not listed on MC"
Yes C
No [I
NAErl
18. Were btlbbles resent ]" ca-size" i l.a"nr 6nun in diameter) in tin • %tQA vials-'1
Yes C
No ❑
NA ❑
,19- Wete all metalgO&.(iil-IEVLrnutrie.ni slain lt,s re:e.ived ai as pH of C77
Yes [j
No ©
NA2{l.
Were 111 Cyanide nndJt.trsullyde satt:lples rccci%cd at a �1 27
iG3 ❑
ltiat ®
21.. Wrrr, ;All applicabit: NH 17KXN cy:1C idelphenol r<(J.?t11jK%I) saryiptCR free of
residtial chlorine"
Yes ❑
Ttic:t ❑
?2. Wete ctallcctinn tenlarMti;Cs docuniewud ern thw• C� for.NC; Sam .les?1`e5
�]
e�\Ct ❑
'23. Were client relnarkSltecliwAs {i_e. requestcd dilutions h'1VNfSD t1CSio atiQ11S,
correctly transel ibcd farm the. COC: into dw comment section in LI 1S:'
yc:s ❑
Ni
24. Was the quote nuinber used taken from the container label?
Sample Preservation fMiigt he completed for any sample(s) incorrectly preserved or with haadspacc, i
Samples) _ :"ere receivud incnrrt�:tly flrescrved and wefe a(dju,ted
at cvrdin ,] itt Stitm�l.e receivitt with — Naral-l) using SR if
Samp Q( _ where receiver) ~Milli bubbles ; n'i 6 n in diameter.
M.
Sant I.eis1 were rrceiresi with TRG r(1.2 m (If #21-is Nir
E,151C.Dlinkang Water Projecr Saniple(s) pH veriliud to he >2 by_ Cute,ets.?were not receivt tl at n Hof :2 and "ere ad'usted ak:curdint;l iisitl SRCc. labels a Iia d b.r: tz 14, Vcritied bv:— -- Date: L2
Cv l cots:
Shealy Environmental Services, tnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyiab.com Levef 1 Report v2.1

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CENTRAL FILET DWOIBOG

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
May 30, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of May, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was not within the benchmark value for Zinc. Sample
results will be submitted as a representative rain event occurs for the month of June until three
consecutive below benchmark samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name:Stormwater
Lot Number:PE19022
Date Completed:05/23/2014
7q
Kelly M. Maberry
Project Manager
s, .t�ni. der
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Crain of Custody Record and Sample Receipt Checklist,
Shealy Environmental Services, Inc. Page: 1 of a
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 INC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PE19022
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the DAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 4
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Repon v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PE19022
Sample Number Sample ID _ Matrix Date Sampled Date Received
001 S130-2 Shipp ing/Fieceiving Aqueous 05/15/2014 0825 05/19/2014^
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 4
106 Vantage Point Drive West Columbia, $C 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

1v1 -nw
Client: Rohm And Haas Company Laboratory ID: PE19022-001
Description: SDO-2 Shipping/Receiving Matrix: Aqueous
Date Sampled:05/15/2014 0825
Date Received:05/19/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 05/22/2014 0959 CDF 05/21/2014 1414 47185
CAS Analytical
Parameter Number Method Result 0 POL Units Run
Zinc 7440-66-6 200.8 71 10 ug/L 1
POL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the POL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a'W'
Shealy Environmental Services, Inc. Page: 4 of 4
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Report v2.1

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.N1irtuy rA1YrfAfnlYhlal Nt3v CLi, hf"..
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Page t of 3
R.-.p1arxs Auto: 09 2lVi !
F11Mtivt Date: 0SAMU
Sample Receipt Checklist (tSVil
) _
cnolex inspected b;adaie; � Lot #-. t d J -'
Mrs of receipt: ❑1ES1 Client ❑ UPS [I FedEx ❑ Airborne Bxp [] C1tber
Ycs
No
!. Werw ta cossealsrCscnt an the cooler?
Yes
Nay
NA 2. If custody seals were )reseed, wcrz they intact and unbroken?
4
Cooler ID!Originat temperature upon recciptlDlerived (ctmocted) temperature upon receipt,
Method: ❑ "remperarltre Blank EjAgainsl Battles TR Chin LL): #3 TR Gun C'L,rmct.ictn Facter:Lo.t'C
Nfr,thnd of coolant: Wex ice ElBlue Ice El Dry Tee 0 None
Ycs ❑
No ❑
-Nix 0
3. if ternperature r+f any cooler exceeded 6.0"C, was Project Manager notified?
PM notified by SRC, phone, not- (circle one), other:_,.
(Forc.00lers received Via commrrclal courier, Ms are to ix: notified
imrnediatelv)
Yr, ❑
No.
—NA_
4, is the commcmial courites p;wking sH2 attaLhLd to this fora!?
Yes
®
Na ❑ F
Were proper custody rncedttres re-hn uishediree6vcdl followal?
No ❑
NA 0
5a Were s!m les relinquished h I elirnt to commercial courier?
.Yes
Yes
-*
No ❑ #
6. Werc saris rle TC)s listrd on the COC:!
Ycs
Na
?. Were son !e 1Ds listed on all sam It containers?
Yes.
No ❑
8. Was collection slate & time. listed un the COC?
Yes
.
No ❑
9. Was collection date & time listod on all sample. containers?
Y"
No ❑
10, Utd all container label information ID. date, Lurie) aEM with the CDC?
1'es
l,To
] 1. Wtrc tests to bepct,•funncd listed on the COC.?
Ycs
E3
xu ❑
12. Did all sam les arrive in the m) nr containm for each test?
'4'cs
vt ❑
13. Did all ctxntainers arrive in goW ccmdititm unbroken, lids on, etc. !
Yes
r
din []
ld. Was adc4uatc s le volume available.? .
`fa•s ❑
'rYtf ❑"
lS. Were all samples receivt;d within Fh the hnlfling time or 48 hours, %1iiclicvcr
cntrts first?
} es
yr, ET
IG. Wert ansam lcs containers Mti i.ng? i
Yes ❑
A1. Were there any axces � Lns not listed on COO .
Yes U
No
NA
18. Were biftles .sent >" -size" 'A"ur 6mm in diemetex iln 3nv SiOA vials? ;
yes
o ©
XTA ❑
19. Wets all mrtals/0&011'!.1'.Mutrieni sam les rweivui at a pH off?
Ycs
Na ii
NA
10. Were all c •anide andlor sulfide sam les received at a pH >121
Y t; ❑
Nisi
NAresidual
21. +ere all applica c NH3lTiCN�ayanidcJphectol (<(},2tttglh} satuplu FTu of
chlorine?
Yr ❑
Na ❑
VA
23. Were collrcticm to tares d.nctamentcd on. the COC for INC sartl lcs?
Yes ❑
No ❑
NA
3. Were client rctnarkshroquerts (i-e. requested dilutions, MSMISD desigmtttinnn,
ccotTmily transcribed from the COC into the coltutl at svcdon in LTMlS?
Lei
Ne
A. Was the quote nur bry used taken from the contaitnet label?
Sample Preservation (Must be complctcd far any samples) incorrectly presenetl or with hm&vpace.)
Samples) wort: mcciveti incorrectly preserved and were adjusted
ueccrdin •l y in ,am le vecei! in with I12SU4iN(h,HCI,NaO using SR #
Sa le(s) were received with bubbles >b mm in diameter.
Sam lc(s) Wert received with TRC >t1.2 (lf #21 is No)
SC Drinking Water Project Sample(s) pU verifird to be >2 by �,. _ _-- Due,
Sam lC(5) were not reccived at a pIT of>2 and were. ad'us'Ir d accurdin minSRO
Sam le labels a lied bv; Verified — _M .Date:
mments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

9
MOAMRINg REPORr
SjWW.COI,3[,XCTJiII NUING C-&L]W"- YHAM'
permit Numbw. Nd%�_� or
zy �a be =rcceft�e�d...by -the D10-012 no b- W than 30 days buin
the '116:t
Cerffmft of Coverage Nwaber.
es the
]ft ig=14 ftvfn the lab6ial aiy.)
/ZC k�Vj 306_�/ C&
FACUM MW _A v, e a L CGUNff
PERSON COLLECrING SAMPLEo). cl, irr%,. Y-" 12.4 o I
CEI VrUMW LABORATORY(S) ,S
(MR&TURs orOR biwGN
.By this dguftwvi I pK.gMrTE9 dy imt ft'repol is a
w=pIde wtbe bed of n knowbfte.
t Monw1bg-
"age.
Tom
Mr. - Ta sum
f, r-JIMMI
Vt.
0TRWIM
Does this facility ;=fmmVehicle Mdwmao=A4"dcs.-i more 'waWo'iIper "th?_yes __W,
using V9W
(if.yes. complete Put B),
oil
I I SAW
IM
mom
IVMM
Fo4nSWU-24&1126Q , 8
Page 1 of 2

J
Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
March 20, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of March, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfail SDO-002, per Tier 11 requirements in
permit. The sample result at outfall SDO-002 was within the benchmark value for Zinc. There has now
been two consecutive below benchmark results for Zinc @ SDO-002.Sample results will be submitted as
a representative rain event occurs for the month of April until three consecutive below benchmark
samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
-No-� � ' —`
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

SHEALY ENVIRONMENTAL SERVICES, INC.
I
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Stormwater
Lot Number:PC12065
Date Completed:03/14/2014
R
Kelly M. Maberry
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
0 • • • • • • s
Shealy Environmental Services, Inc. Page: t of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Report v2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PC12065
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc, ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Repartv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PC12065
Sample Number Sample ID Matrix Date Sampled bate Received
001 SD0.2 Shipping/Recieving Aqueous 03/06/2014 2042 03/12/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Repertv2,1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PC12065
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SDO-2 Shipping/Recieving Aqueous Zinc 200.8 23 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.t

1V1 -'WNW
Client:Rohm And Haas Company Laboratory 10: PC12065-001
Description: SDO-2 Shipping/Recieving Matrix: Aqueous
Date tampled:03/0612014 2042
Date Received:03/12/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 03/14/2014 0327 CDI= 03/13/2014 1920 42224
CAS Analytical
Parameter Number Method Result 0 PDL Units Run
Zinc 7440-66-6 _ 200.8 23 - 10 ug/L 1
PQL _ Practical quantitatior limlt 8 = Detected in the method blank E = Quantitation of compound exceeded the csllbratior range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result r POL and > MDL P = The RPQ between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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SHEALY ENVIRONMENTAL SERVICES INC.
r
Stw.:rt Fsvviro inicnml SC V.; m,1as:, f°aid 3 ,rf i
Il;rr:wnr:rt- F-Ar) Nt' lice :.a L�at_. tits'*a'13
F e.'i atrn �rirrihrr' 14 l lfcctivC Ult'::'��'fl s I�
firmple Rcr.:opt Checklist ($RC)
:Imcn; h»rr1Cailr Inspect:d �y+dato: i6,
l.nl 9::
w1cu.11ti a#' r ^eeiht: ❑'"SES] ❑ clit7w ❑ 1 ll's F] Fe::iiF.x j Fl Air
orae I xll__._...� C itlier
Yes I
No E] I • 1, W�nc cti%lody walls present oil lhv «4.olr-r:'
r�
El
I No ❑-i \A [jf 2. ll' kai iwdy seals were )resent. wl:-rr, ihiA, iwact ;i
Ild irnhroken" �+
C'onle.r 1010rigin [l wilil'ict'.itt.11V UP011 ti;'L'4'lpt/Ded ved (Carrectc-d) 1[',r tpi:1 .rimit . 1iji
lllethc,rii: ❑ T.ntpmatWr1nitl,.'ainrtEiutllc's LR Gulp117: N1 A 1Ft Clue
Nk,thod ,,,f coirllaqu aril Ice BILK 1CVi, r !
n rcccipt:
Cclrrc't:6or1
411e
(9jt' l Manager n41t1t eJ9
:_
'ere, to lie note; ied
Yr..L ❑
No ❑
y�
KA t❑✓
r3 if icuiperawN lrr ally cuoi.n ox,:eeded 601-L'. '.w:iti
I'M nnuf cd h\ SRC, phoac. twit; (circle cane.), othc
0--or coolers nczivod vin c ollirlittfes r1 ecrurier. Pats
ia]tile diatell'.)
Yths i
..:v) (..] NA ❑
4. r.5_the, commercial. courier's pt�kilrg sir ,attached t
} this L' mli!
Ycs i
Nt,
5. wti'`:iv pii vi-custody eiwt7lums
)'cc ❑
No ❑
i NA-'-_
Sa Were sam lc s nrlimpti.Aied by client t6 cclnum
°iam4 cornier' M
'4o C
6, ww'Wre s;tm le 11.)s listed on the CVC?
Yrs ❑"
.fir, ❑
�. Were. svTT !,s If7S li.;lril ,�n all sample CutmluillulS"
Yo [
,tic. El
8, w' us collccti,;ln elate S time listiod on lhr_.--
l'r5 iti'� ❑
9. was, cAlectitm bLe & tirn.: lisIcfl tlei 111 Sim lle co
Ilainurs";'
Yi<z � ; i ,�rL�I
I 11, 1]iii all E�nnrainct' labk I inftlrno�:dis n I' [L), of tic., t€rn_`�
it �rar,: wil_h the MCI
1 do ❑
_.__,._.
_1 1.Were tests to be perfortiled Listed nn the COCk '
{
Yrs ❑I
'No []
12, Did ' l! S,illn ICS arriV,: in tine 2101)CL conMioers i-nr
each le'ST'•'
Ell
tie ❑
13, Did all �_rrntrliners arrive in good condition (unbrokcn.
lids eltl,
l77
S•L'T
vs
��1
"h4 ❑
�14. ` ai ade tlatl Sample volililtr,;1V;I;1al)k'?
15. were, .ill xampk* rccci4'c witlriu I.,':s the hoidina 0t,
or �4S hnurs, whiuh4•,tcr
16. wt'crc art r samrt ley ctowainers mis;rint:'r'"�-
4'r- ❑
c> [
-17, W.—,rG llirrr. arty' e tiCesi ti311k lei not listedjori i 04-
18. Were, hobbles prr.se.tit :-"Ela-R17e" ('»"br'NmiL i11
iamelert in my 1 ()A
yei ❑
,No ❑
_NA ❑
"tis
No ❑
NA ❑1'
19. Were all ttu tul5'C)[ G+'1IPIwflllutritrnt sctrri Ic:s rrc
itieci at a H tlf { '�
N 1 ❑
7
,� �j
2(), W rc all c�,l.ni�le. xnd/ae sulfide sartr{rIc s ttit:e-iscCl
a pH :�12''
El
No ❑
�, ❑
l w�'crc- dl appli4;ihlr NI l'�il'k.Nkyanrdelphenl_11 l_�".
residual chlorine:?
).''rT�pr1L; camp](* I'll.-C.l If
Y� ❑
No (❑
l;A Q
11 Were entlection tern .l•.rtrlumts do unle.w6d on the
: (")(.' 4'nr NC sane .lrs?
YI-c ElN,1
r❑
'
nA
??.W'ere client remirksercqucsts fi.es. reque.sied cliluli
' I
tslC....1 cnrrcetlt� transcrib,:d ITorn the C OC. into the: t!,'j
1n,4, MSIMSD desicntltiQ11S,
Ierlwiit section in LINTS'.'
i'es ❑
�Swiiilel(-
No
'23, W'as the quote nunihtar u.5M inken from the corilainuo
.la)el'?
Preservalic)n il,Musl be et)mpletcd fortiny smti t:l") incrirrectly presea
-ed or With hcatlq%ICe:.)
san7plcf.5) ......,_..__._ „ .»« were: received iT0irrr.GlI
ac-zordi;gzlx m �,nmple re"ccivinp vrit4l f H:5(=t;,H CIi.ElC1,_Nat)t 1)
Sane lqy) _ wcrc rcce ivct] 1A itlr l�tlb
' pvcC zrx-cd and were im(tjtltiTed
using SR 4
Iz; >6 lnrn in dianrter.
---were raceitied titiith'1
k(: '(l.' mg1L + if )421 is \u)
S{_' L)rinkinl*,W.mtcr PrujW Slltlrtllell�6 pH verified to be 2 to-t'
ve rlut t,;,;6 `ed ,it a pH of x2 and wt-. ' nditived ac
orclirigly using, SR r
'.11 t11Ie Iaht_,1s arpliviI br: . j�t ):p Verified by:
t,:t-rmill -niti:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Project Name: Stormwater
Lot Number: PC12065
Date Completed:0311412014
i
Kelly M. Maberry
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29472 [phone] Fax [phone] www.shealylab.com Level 1 peport v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No; E87653 NC DENR No; 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PC12065
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project.Manager listed on the cover page.
Shealy Environmental Services, inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealytab.com Level 1 Flepart v2.i

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PC12065
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO-2 Shipping/Recieving Aqueous 03/06/2014 2042 03/12/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sh ealyl ab corn Level 1 Reportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PC12065
Sample Sample ID Matrix Parameter Method Result a Units Page
001 SOO-2 Shipping/Recieving Aqueous Zinc 200.8 23 ug/L 5
(1 detection)
Shealy Environmental Services, Inc, Page- 4 of 5
106 Vanlage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com Level 1 Repon v2.1

Client:Rohm And Haas Company Laboratory ID: PC12065-001
Description: SDO-2 Shipping/Recieving Matrix', Aqueous
Date Sartipled:03106/2014 2042
Date Received: 0311212014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 03114/2014 0327 CDF 03/13/2014 1920 42224
CAS Analytical
Parameter Number MethodResult 0 POL Units Run
Zinc 7440-66-6 200.8 23 10 ug/L 1
POL = Practical quantitation limit B = Detected in the method blank E . Ouantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result < POL and > VOL P - The RPD between two GC columns exceeds 40% N . Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
3hoaly Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sif
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Shealy Environmental Services, lnc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab,com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Eln;ylli':W "k, Ill fill,
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CiIlilllwllls:
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheaiylab.com Level 1 Report Q 1

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
March 20, 2014
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of March, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier II requirements in
permit. The sample result at outfall SDO-002 was within the benchmark value for Zinc. There has now
been two consecutive below benchmark results for Zinc @ SDO-002.Sample results will be submitted as
a representative rain event occurs for the month of April until three consecutive below benchmark
samples are collected.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any additional
information.
Sincerely,
Alanna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DQw RESTRICTED

Rohm and Haas
6101 Orr Road
Charlotte, NC 28213
[phone]
Division of Water Quality
Surface Water Protection Section
ATTN: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
CERTIFIED MAIL:
Re: Storm water Discharge Monitoring Report
Rohm and Haas Chemicals LLC
Permit No. NCS000386
RECEIVED
FEB 2 7 2014
CENTRAL FILES
DWQIBOG
February 20, 2014
Enclosed are the original and one copy of the Storm water Discharge Monitoring Report for the Rohm
and Haas Chemicals LLC, 6101 Orr Road (Permit #NCS 000386) for the month of February, 2014 Zinc
sampling. Sampling is now being conducted monthly at Outfall SDO-002, per Tier 11 requirements in
permit. The sample at outfall SDO-002 was within the benchmark value for Zinc. Sample results will be
submitted as a representative rain event occurs for the month of March until three consecutive below
benchmark samples are collected.
Also enclosed you will find a Delegation of Authority for MR. Matthew Church. Matthew is our new site
leader and will need to be added as a company official. Mr. nick Gipson will need to deleted.
Please feel free to contact me at [phone] x 3069 if you have any questions or need any
additional information.
Sincerely,
A anna Smith
Environmental Health & Safety/Health Services
cc: Matthew Church
Jamie Watts
DOW RESTRICTED

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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Lot Number:PB07059
Date Completed:02/17/2014
11*'P�)w
Kelly M. Maberry
Project Manager
��9 tih� ACCpa�*
� f
!:d x
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PB07059
This Report of Analysis contains the analytical results) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyleb.com Level 1 Reportv2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PB07059
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO.2 Shipping/Receiving Aqueous 02/04/2014 2125 02/07/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC. "
Executive Summary
Rohm And Haas Company
Lot Number: PB07059
Sample Sample ID Matrix Parameter Method Result 0 Units Page
001 SDO-2 Shipping/Receiving Aqueous Zinc 200.8 42 uglL 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax (B03) 791-9111 www.shealylab.com Level 1 Report v2.1

11.01 -IRV
Client:Rohm And Haas Company Laboratory ID: PB07059-001
Description: SDO-2 Shipping/Receiving Matrix: Aqueous
Date Sampled:02/04/2014 2125
Dale Received:02/07/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200,2 200.8 1 02/15/2014 0318 CDF 02/10/2014 2130 40159
CAS Analytical
Parameter _ Number Method Result Q POL Units Run
Zinc 7440-66-6 200.8 42 10 uglL 1
POL = Practical quantn1ion limit B = Detected in the method blank E = Quantltation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the POL J = Estimated result < POL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where appficable, all soil sample analysis are reported on a dry weight basis unless flagged with a 'W'
Shealy Environmental Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealyiab.com Leval 1 Reportv2.1

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Note: All samp[�s are retained for six weeks (Film receipt
ofilwis other armigements are mado_ -r I
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SHEALY ENVIRONMENTAL SERVICES INC.
i InouanwulNumt;,a; F-+,D i;19f
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Sample Reuelpt Chock[i5t (SR '') .
. t c,lrr Ins e.cd,.d hVdate. �:� � /� Lot #:--•.�:.-- i, a '_x
Felca ni of receipt: h T ,.IlllT Client J CJF'S ❑ FcF F,� Q Airl>ur;re !xp C71 (?fl]:C
, t: l i.l -
I. ';X ej C ruuytt) Rea1s present Lin the ruolC11
Yes 2. IT l::LL t� dy scab ������t, ��rU (h !W� �l and uabrokca ?
Cooler M."' 3rlipipal Irltiper.1tor'e t1pon r�"ccipllDrrltcd {c-orrccie4)) trmpei.lure upon receipt:
141 titRa�i: L P �'rf,,tperxur a l�lrs"irk ro c+inst7�l�]o ties Ili %jtttt ID- -? ��_ !R C�urr Cr�rr�►ti�rt I'a� lnr} Ci 1.�^�:
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--- lc'l h�,ai t.11 CC11iLl : '1S'Gt lct'J ❑ LF� llC Ice i� Lf [[4" - Nonr
If rrspalnse t,; No (+'1t Vm fir 14, 15, lC)asn nxplanatranJtc s,,lulicn must he providcd.
3, ff tcmpe.rattrrc of any cocirr exce.cded 6.13T, wmq Proied,Mailagcr t10 ified?
Yes No r�
1..,! NAO' ltM untlfrr~cl by ill(:, phone, rroIC ('Circle 41t'1r'), other: —. ihur
s arr In be trnmrdiarely.
�]
No
\MittrcTeorxtyT,r
al crruri� s ft cicis� stir attached to h s flied
5. Were)rnperctrsrodYprot;ed.urcc(ml.ingtrislrt~11r' -ceived)follr.►a.c3
Yes
s
Yes
iti,ta 1`73
VA
a Werp. rx,lincluished by u4ciat 16 colnrncrc,al u.ouricr?
'C4
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ti e rnplC iTJB 119t{1 �T�—� Y
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Yr3
Yes
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No 1.,.,}
I:)td �11 ram, le` a 7
`t.��la e , arrive in the prul,a r container& fc,r each 11 jt'. _
10. DI'd all container label informatiun (T1'), date, tuna ape wiLh C OCr!
11. in dition
NO
-- M„
Did all entiminers ar6vc good co (trnbpLC cn lids on Ott .)?
Y x [ }
NO �
12, 'Was adtnwalc sarttpic v(Jurrrc at:iilable? -
Were all samplt;.s rcccived wit] iin ,,i the hn1dit►g Iir it: ur 18 Hours, wTj7rhr 11_l
yCS
No13.
i
Ct3rLC5 {]rSt?
No d
14. Were ai1T y swj )Jes cunt7in&rs M Ssip1 e
I :i, Weic tllrre any exctrss &-ilapics not listed Ion CC :!
V'cs
_
16- Were hublslcs present -`pca-sizc" { /4-'t)r 6nnn in diamet: r) ill any VOA
L'1i'tls:
Ycs�
ca ._ i
NA
11, WQrc. al! mVtalsrV&-fit` -U7' lfntrttierrt samples rrceivrc3 at�f �;
1'os
W
18_ Weee *iH cyanide andior sulfide samples ieerivod at a fi -3 2° _
�1'cre
aff aprplicahlc. N113/ 'KN cv} inidciplicuu1 f.,11 4mpt) ,4amplos fi-ec L)f
�'es �] ; o 0 NA.�9. VAresidual
djirurinc'
Y i 1� NGtµ I�1:AT .0. Wei e t.ullecki[ant trues dtictirta.trticd a?n tkrc Z:()t' for Nt sartrpies'?
21. Were cheol tk*narks:'regirests (i.e. rr.quested dilutit,us: M tMSD rl signaticns,
�PCS U U '�'e� _
ciC,,,.) cfiji't'1.:11L'trausCTll?Cd I.rer1[ I. LG C�l.�[ ilrt(i F.l]C :.E?ir'litsevl serlion llt 1..1-i1�]S
' Saituplc l't esrrvation. (M. urr he-, coniple€tcd frnr any salsrple[s) inctfrr MTly pre,rrvcd or with hcatispaice.) -
s were. rnwciivcd itwul-FCctly prc vfvcd and�wc c ldjusii:l
acc.cxrc,ingly -m sam.plc re.ce.it7ing ilat.h — (ill SO4,111' 03'Hi.'!,NtrOlI with tl:1e SR 4 (nunibcT)
ere rzccive4 with hubbies tr in ciial,mmer.
Ull;_..[zlct.s,l _ ...w__-_..... .....,. ...�........ _,..... _.wtire received with `l.p.0 4.2 rn�,I� fret N133!
,
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t R: fv LV'kti1 C�[.,,t lllr £.'r14`ll
It: Iabtds 4cTift,.d h}" f3at� :
Ma
C'nrrectl�•e- Artiun ta.lrrn if r�ecr,cssarw;
'Alas client untilicd: Yes Mj No [
SCSI eniployce:
Did clicrtt m,5pot4d- lie:, [] Nu
Hate OfreSponsc:
Shealy Environmental Services, Inc. Level 1 Report v2.1
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheafylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Rohm And Haas Company
6101 Orr Road
Charlotte, NC 28213
Attention: Alanna Smith
Lot Number:PB07059
Date Completed:02/17/2014
7w"q-y
Kelly M. Maberry
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealytab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Rohm And Haas Company
Lot Number: PB07059
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Shealy Environmental Services, Inc. Page: 2 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 4 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Rohm And Haas Company
Lot Number: PB07059
Sample Number Sample ID Matrix Date Sampled Date Received
001 SDO-2 Shipping/Receiving Aqueous 02/04/2014 2125 02/07/2014
(1 sample)
Shealy Environmental Services, Inc. Page: 3 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatylab.com Lovell Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Rohm And Haas Company
Lot Number: PB07059
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 S130-2 Shipping/Receiving Aqueous Zinc 200.8 42 ug/L 5
(1 detection)
Shealy Environmental Services, Inc. Page: 4 of 5
106 Vantage Point Drive West Columbia SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Reportv2.1

Client: Rohm And Haas Company Laboratory ID: PB07059-001
Description: SDO-2 Shipp!ng/Receiving Matrix: Aqueous
Date Sampled :02/04/2014 2125
Date Received; 02/07/2014
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 02/15/2014 0318 CDF 02/10/2014 2130 40159
CAS Analytical
Parameter Number Method Result 0 PQL Units Run
Zinc 7440-66-6 200.8 42 10 ug/L 1
PQL = Practica4 quamitation limit B = Detected in the method blank E = Quamitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result a PQI. and > MDL P = The RPD between two GC columns exceeds 40% N a Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmenlal Services, Inc. Page: 5 of 5
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Urfleus Fatter ikr, ill jE'rT[ti1tt5 8tt' iziciili�. - _.,- »r :,, p lr�,i it i': m �. p.,;i, ii a iju. 'C 7;:, h:.Pit:
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SHEALY ENVIRONMENTAL SERVICES9 INC.
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Yes NU I
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Yes
No F
1 NA J�r
I'M notified by SRC, phone, nolic (circle ortr), other;
6wCre Sample IDS listed?
17
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Were N::CjVeLj In(,
112
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Did 6<zntn�5pou� Yes [l No -1
Date of rtspowu�
Shealy Environmental Services, m«. c uo�ru ro��rou uw�nx m1-u11 www.shealylab.com �" `n�« ,u`