NCS000330_Monitoring Reports_20110516

STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
O�J�
DOC TYPE
❑ FINAL PERMIT
MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
❑
DOC DATE
YYYY M M D D

Ic
OF
ATI Allvac
2020 Ashcraft Avenue, P.O. Box 5030, Monroe, NC 28110
phone:[phone] fax: [phone]
email: [e-mail]
May 11, 2011
NCDENR - Division of Water Quality
610 East Center Avenue, Suite 301
Mooresville, NC 28115
STORMWATER PERMIT NO. NCS000330 — ZINC MONITORING:
Deal Sainai Bou-Gliazale:
This letter is to notify the DWQ Regional Office that ATI Allvac — Monroe Site has collected the requested
analytical monitoring for zinc from the. galvanized steel structures positioticd in the drainage area for our
representative outfall. As requested, a 4th sampling event was conducted and the laboratory work was split
between Pace Analytical and Prism Laboratories, Inc. Zinc samples 1 — 4 are summarized below:
Anal tical Values
Downspout
Location
1st
sample
2nd
sample
3rd
sam le
4th sample
PACE
4th sample
PRISM
Finishing Bldg
0.294
0.0583
0.299
1.96
0.795
2.0
0.83
UFM Bldg
0.187
0.450
0.235
Press Bldg
0.116
0.383
1 0.553
1.58
1.6
Conditioning Bldg
0.098
0.0769
0.212
1 5.23
4.8
SDO #02(M)
0.392
0.177
0.907 1
0.381
0.4
As we discussed, our facility is unable to identify trends with the sampling value ranges. The analytical
range is likely due to the inconsistent amount of rainfall received during the sampling events, and how fast
that rain fell. The Conditioning Bldg is in the process of installing a new roof, which is likely the reason
the zinc levels for that building have increased.
BMP's ate impletueuted to cottuol I)utctttial Suutces of zinc, such as hydiaulic oil and iLtbber from tire
wear. Our facility roads and parking lots are routinely cleaned and swept by an industrial service provider
Also, routine preventative maintenance schedules aie established fui inobile equipment to reduce oil leaks.
Since there is no zinc in our products as stated previously, ATI Allvac requests NCDENR to revise
Stormwater Permit No. NCS000330 and replace the benchmark value for zinc from 0.067 mg/L to a
"monitor only" condition so the facility can continue to evaluate the effectiveness of our BMP's.
Sincerely,
Preston M. Baucom,
EHS Manager
ATI Allvac - Monroe Site
cc: Ed Stegall, Allvac
Greg Laney, Allvac
Kyle Dunn, Allvac
Tommy Long, Allvac

' '/ ATI AI Ivac ' �' �11� W
2020 Ashcraft Avenue, P.O. Box 5030, Moi���w-�-`
phone:[phone] fax: [phone]
email: [e-mail]
May 11, 2011
NCDENR - Division of Water Quality
610 East Center Avenue, Suite 301
Mooresville, NC 28115
STORMWATER PERMIT NO. NCS000330 — ZINC MONITORING:
Dear Samar Bou-Ghazale:
RECEIVED
DIVISION! OF WATER QUALITY
MAY 16 2011
MOoPEc: ;i..'_�: t-,L-iONAL OFFICE
MAY 3 1 2011
This letter is to notify the DWQ Regional Office that ATI Allvac — Monroe Site has collected the requested
analytical monitoring for zinc from the plvauized steel structures positioned in [lie drainage area for our
representative outf all. As requested, a 4`' sampling event was conducted and the laboratory work was split
between Pace Analytical and Prism Laboratories, Inc. Zinc samples 1 — 4 are summarized below:
Analytical Values
Downspout
Location
1st
sample
2"
sample
3r
sam le
4t sample
PACE
4 thsample
PRISM
Finishing Bldg
GFM Bldg
0.294
0.187
0.0583
0.450
0.299
0.235
1.96
0.795
2.0
0.83
Press Bldg
0.116
0.383
0.553
1.58
1.6
Conditioning Bldg
1 0.098
1 0.0769
1 0.212
1 5.23
1 4.8
SDO #02(M)
1 0.392
1 0.177
1 0.907
1 0.381
1 0.4
As we discussed, our facility is unable to identify trends with the sampling value ranges. The analytical
range is likely due to the inconsistent amount of rainfall received during the sampling events, and how fast
that rain fell. The Conditioning Bldg is in the process of installing a new roof, which is likely the reason
the zinc levels for that building have increased.
BMP's are implemented to control potential sources of zinc, such as hydraulic oil and rubber from tire
wear. Our facility roads and parking lots are routinely cleaned and swept by an industrial service provider.
Also, routine preventative maintenance schedules are established for mobile equipment to reduce oil leaks.
Since there is no zinc in our products as stated previously, ATI Allvac requests NCDENR to revise
Stormwater Permit No. NCS000330 and replace the benchmark value for zinc from 0.067 mg/L to a
"monitor only" condition so the facility can continue to evaluate the effectiveness of our BMP's.
Sincerely,
Preston M. Baucom,
EHS Manager
ATI Allvac - Monroe Site
cc: Ed Stegall, Allvac
Greg Laney, Allvac
Kyle Dunn, Allvac
Tommy Long, Allvac

i
aceAnalj cal
! www.pacelab&c=
May 02, 2011
Mr. Preston Baucom
Allvac
2020 Ashcraft Ave
Monroe, NC 28110
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: ZINC
Pace Project No.: 9293000
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Baucom:
Enclosed are the analytical results for sample(s) received by the laboratory on April 28, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
q/i n M i,)CtJz-�
Erin Waters
[e-mail]
Project Manager
Enclosures
cc: Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[ClGh6—
Page 1 of 12

i
aceAnalXical
w"..pacelabs.c=
1
Project: ZINC
Pace Project No.: 9293000
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Connecticut Certification #: PH-0106
Pennsylvania Certification #: 68-03578
Florida/NELAP Certification #: E87648
South Carolina Bioassay Certification #: 99030002
Massachusetts Certification #: M-NC030
South Carolina Certification #: 99030001
New Jersey Certification #: NC011
Virginia Certification #: 00072
North Carolina Bioassay Certification #: 9
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,n eccaao
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 12

aceAnalj&al
www.pacetab&com
Project: ZINC
Pace Project No.: 9293000
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
9293000001
ROLLING
EPA 200.7
JMW
1
PASI-A
9293000002
CONDITIONING
ErA 200.7
JMW
1
PASI-A
9293000003
PRESS
EPA 200.7
JMW
1
PASI-A
9293000004
GFM
EPA200.7
JMW
1
PASI-A
9293000005
SW02
EPA 200.7
JMW
1
PASI-A
9293000006
IN PROCESS
EPA 200.7
,IMW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
rrie ac=
Page 3 of 12

aceAnalytical
! www.pacelaftcom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC
Pace Project No.: 9293000
Sample: ROLLING Lab ID: 9293000001 Collected: 04/28/11 13:00 Received: 04/28/11 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 1960 ug/L 10.0 1 05/01/11 12:30 05/02/11 03:04 7440-66-6
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
melaci
Page 4 of 12

aceftlytical
( www.pacelabs.com
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC
Pace Project No.: 9293000
Sample: CONDITIONING Lab ID: 9293000002 Collected: 04/28/11 13:10 Received: 04/28/11 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7
Zinc 5230 ug/L 10.0 1 05/01/11 12:30 05/02/11 03:22 7440-66-6
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
,, m
Page 5 of 12

aceAnalytical
www.pacelabs.cm
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC
Pace Project No.: 9293000
Sample: PRESS Lab ID: 9293000003 Collected: 04/28/11 13:15 Received: 04/28/11 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 1580 ug/L 10.0 1 05/01/11 12:30 05/02/11 03:29 7440-66-6
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�nelac .
Page 6 of 12

aceAnalytical
r www.pmWabscom
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC
Pace Project No.: 9293000
Sample: GFM Lab ID: 9293000004 Collected: 04/28/11 13:20 Received: 04/28/11 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7
Zinc 795 ug/L 10.0 1 05/01/11 12:30 05/02/11 03:33 7440-66-6
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 12

aceAnalyticai®
mm..pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC
Pace Project No.: 9293000
Sample: SW02 Lab ID: 9293000005 Collected: 04/28/11 13:25 Received: 04/28/11 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 381 ug/L 10.0 1 05/01/11 12:30 05/02/11 03:36 7440-66-6
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 12

/aXAnalj&ale
( www.pacelabscom
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: ZINC
Pace Project No.: 9293000
Sample: IN PROCESS Lab ID: 9293000006 Collected: 04/28/11 13:30 Received: 04/28/11 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Zinc 713 ug/L 10.0 1 05/01/11 12:30 05/02/11 03:39 7440-66-6
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
lea
Page 9 of 12

® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
acemalXical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www.pacelabscom Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
l [phone] [phone] [phone]
QUALITY CONTROL DATA
Project: ZINC
Pace Project No.: 9293000
QC Batch: MPRP/8280
Analysis Method:
EPA200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 9293000001, 9293000002, 9293000003, 9293000004, 9293000005, 9293000006
METHOD BLANK: 598445
Matrix: Water
Associated Lab Samples: 9293000001,
9293000002,
9293000003, 9293000004, 9293000005, 9293000006
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Zinc
ug/L
ND 10.0
05/02/1102:04
LABORATORY CONTROL SAMPLE:
598446
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Zinc
ug/L
500 487
97 85-115
MATRIX SPIKE SAMPLE:
598447
9292978002 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Zinc
ug/L
13.8 500
488 95
70-130
MATRIX SPIKE SAMPLE:
598449
9293000001 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Zinc
ug/L
1960 500
2510 111
70-130
SAMPLE DUPLICATE: 598448
9292744005 Dup
Parameter
Units
Result Result
RPD Qualifiers
Zlnc
ug/L
29.4 28.1
5
SAMPLE DUPLICATE: 598450
9293000002 Dup
Parameter
Units
Result Result
RPD Qualifiers
Zinc
ug/L
5230 5380 3
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
�fielac
Page 10 of 12

Air I
aceAnalytical
www.pacelabs.c=
Project: ZINC
Pace Project No.: 9293000
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values
l CS(D) - t aboratory Control Sample (Duplicate)
MS(D) Matrix £pilco (Duplicoto)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
Date: 05/02/2011 04:09 PM REPORT OF LABORATORY ANALYSIS Page 11 of 12
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
rt�,N ACC 9
,,inelac

aceAnalytical
wvnvpacelaps.can
Project: ZINC
Pace Project No.: 9293000
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
9293000001
ROLLING
EPA200.7
MPRP/8280
EPA200.7
ICP/7656
9293000002
CONDITIONING
EPA 200.7
MPRP/8280
EPA 200.7
ICP/7656
9293000003
PRESS
EPA 200.7
MPRP/8280
EPA 200. /
ICP/7656
9293000004
GFM
EPA 200.7
MPRP/8280
EPA 200.7
ICP/7656
9293000005
SW02
EPA200.7
MPRP/8280
EPA200.7
ICP/7650
9293000006
IN PROCESS
EPA200.7
MPRP/8280
EPA200.7
ICP/7656
Date: 05/02/2011 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
r eJa6-
Page 12 of 12

a
o
so
00
.t
QI
N
A
5a
N
ITEM #
m
o
3
a
o m m
m
3 .o .p.
a
vc .�»
3
o
t
•,mac
nD
g
CD
o
h
No
v
t
z
NK
rD
C1
_
S
m� m '
\
m
O>
C
C
3
`
C
z
m
,i
41
O =1P Ornv ego
j. N •� _ O p y m �.
CDC N � [1 N tD F
NK
O m D
^
'V
m
'O
n
•o
n
0
o
C
m
COX--p
TJ 70 (n
m ID A
V .n.
A. C'C
z
Cs
r0r�:E
a
m
@
R
a s
m'
3
o
3
D
O
m
- W
"a
�f�S
MATRIX CODE (see valid codes to left)
V.
r
TYPE (G=GRAB C=COMP)
cSAMPLE
N
°
o
3
j
o'
o
�`
�
3
^C
0
0
Ap
a
m
,
m
(b
m
O
N
O
z
z
z
n
• V
Z
l�j
tH
nl
h
a
m n
m
3
D\
m
zo
c o
m
m
!
in
o
va
''Z
a
W
ti
b'
o
C
m
�
F
w
1
�,
SAMPLE TEMP AT COLLECTION
m
`o m tD
1
V
# OF CONTAINERS
oKv�.o
g
g
$
a
0
m
a
^.
Unpreserved
H,SO4
m
Z
d
o 0
HNO3
y
3,
o.
h
X
HCI
C
NaOH
v
0
Na2S203
CDS
m
Methanol
Other;
v
Q,
jAnalysis Test 1
Xi N j
_
A
yl
m
m
Zu
CO
M
rn
o
."'
z
z;
C
z
m
m
Temp in °C
CA
0
Residual Chlorine (Y/N)
D
F"
Received on
Ice (YIN)
D
y
-
C
p p
C)Sealed
Custody
Cooler
O
o
m
0
(Y/N)
,w,
�
o
G)
- P
Cn
r
Samples Intact
a CD—
—DI
rn
(Y/N)

-.AkeAnalytical' Client Name: J\\�cC Project # � 3(Doo
Where Received: ER'*�Huntersville ❑ Asheville ❑ Eden
—
Courier: ❑ Fed Ex El UPS [IUSPS El Client ❑ U Commercial race Other
Custody Seal on Cooler/Box Present: ❑ ygs []'no Seals intact: ❑ yes ❑ no proj%Due Date
Packing Material: ❑ Bubble Wrap ❑Bubble Bags None ❑Other
Thermometer Used: IR Gun: T1101 Type of Ice: et Blue None ErSamples on ice, cooling process has begun
Temp Correction Factor: Add / Subtract 0 °C
Corrected Cooler Temp.:C
Biological Tissue is Frozen: Yes No
Date and Initials of person examining
contents:' -NM ?N !A —CM— `k
Temp should be above freezing to 6°C
Comments:
Chain of Ctrstndy Present-
G? es ❑No
❑N/A
1 _
Chain of Custody Filled Out:
PP<—
❑No
❑N/A
2.
Chain of Gusted Relinr�tlishecl:
9Yes
❑No
❑N/A
3,
Sampler Name & Signature on COO:
Lms
L1No
LJN/A
4.
Samples Arrived within Hold Time:
2<
ON.
❑N/A
5.
Short Hold Time Analysis (<72hr):
❑Yes
9110
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
Leo
❑N/A
7.
Sufficient Volume:
E]Yes
ON.
❑N/A
8,
Correct Containers Used:
El No
❑NIA
9.
-race Containers Used:
��s
LAY®s
❑No
❑N/A
Containers Intact:
E Yes
❑No
❑N/A
10.
Filtered volume received for Dissolved tests
❑Yes
❑No
L1l/A
11.
Sample Labels match COC:
2Yes
❑No
❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
❑No
❑N/A
13.
All containers needing preservation are found to be in
Sores
❑No
❑N/A
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
❑Yes
El No
Initial when completed
Samples checked for dechlodnation:
LJYes
LJNo
[Ai
•14.
Headspace in VOA Vials ( >6mm):
FYes
QNo
PrK/A
15.
Trip Bitanl( Present:
❑Yes
❑Novi///A
16.
Trip Blank Custody Seals Present
❑Yes
❑No
C27N/A
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
Field Data Required?
Y / N
SCURF Review: Date: SRF Review: Date: 4
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers)
F-C H R-CS-003-rev.0313Apr2011

PRISM
LABORATORIES, INC.
ATI Allvac
Preston Baucom
P. O. Box 5030
Monroe, NC 28110
NC Certification No. 402
SC Certification No. 99012
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions
Project: Stormwater Split
Lab Submittal Date: 04/28/2011
Prism Work Order: 1040646
Case Narrative
05/06/2011
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data quallflers are flagged Indlvldually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Project Manager
Data Qualifiers Key Reference:
Reviewed By
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 10

,� I `- n %� Full -Service Analytical &
J' V' Environmental Solutions
"'A LABORATORIES, INC
Sample Receipt Summary
05/06/2011
Prism Work Order: 1040646
Client Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
Rolling
1040646-01
Water
04/28/11
04/28/11
Conditioning
1040646-02
Water
04/28/11
04/28/11
Press
1040646-03
Water
04/28/11
04/28/11
GFM
1040646-04
Water
04/28/11
04/28/11
SW02
1040646-05
Water
04/28/11
04/28/11
In Process
1040646-06
Water
04/28/11
04/28/11
Samploc rocoivod in good oondition at 0.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 10

/RRISM Full -Service Analytical
Environmental Solutions
.:A IA RRTORIE$ INC.
ATI Allvac
Attn: Preston Baucom
P. O. Box 5030
Monroe, NC 28110
Project: Stormwater Split
Sample Matrix: Water
Laboratory Report
05/06/2011
Client Sample ID: Rolling
Prism Sample ID: 1040646-01
Prism Work Order: 1040646
Time Collected: 04/28/11 01:00
Time Submitted: 04/28/11 16:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Zinc 2.0 mg/L 0.030 0.0022 1 *200.7 513/11 21:31 DWR P1E0005
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] [_Page 3 0f 10

�, J I ` Service Analytical Environmental
rx J Environmental Solutions
:,�.. LABORATORIES, INC.
ATI Allvac
Attn: Preston Baucom
P. O. Box 5030
Monroe, NC 28110
Project: Stormwater Split
Sample Matrix: Water
Laboratory Report
05/06/2011
Client Sample ID: Conditioning
Prism Sample ID: 1040646-02
Prism Work Order: 1040646
Time Collected: 04/28/11 01:10
Time Submitted: 04/28/11 16:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Zinc 4.8 mg/L 0.030 0.0022 1 *200.7 5/3111 21:38 DWR PIE0005
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 10

Laboratory Report
P R I `- n A I
Full -Service Analytical &
r J' V'
Environmental
Environmental Solutions
05/06/2011
a.. , .... LABORATORIES ING
ATI Allvac
Project: Stormwater Split
Client Sample ID: Press
Attn: Preston Baucom
Prism Sample ID: 1040646-03
P. O. Box 5030
Prism Work Order: 1040646
Monroe, NC 28110
Sample Matrix: Water
Time Collected: 04/28/11 01:15
Time Submitted: 04/28/11 16:50
Parameter
Result Units Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Total Metals
Zinc
1.6 mg/L 0.030
0.0022 1 *200.7 5/3/11 21:46 DWR PlE0005
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 10

PRISM
R I S Environmental
Service Analytical &
Ar Environmental Solutions
ll 27"i V,90MTO m ma
ATI Allvac
Attn: Preston Baucom
P. O. Box 5030
Monroe, NC 28110
Project: Stormwater Split
Sample Matrix: Water
Laboratory Report
05/06/2011
Client Sample ID: GFM
Prism Sample ID: 1040646-04
Prism Work Order: 1040646
Time Collected: 04/28/11 01:20
Time Submitted: 04/28/11 16:50
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Zinc 0.83 mg/L 0.030 0.0022 1 *200.7 5/3/11 21:53 DWR PIE0005
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 r
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 10

Laboratory Report
R I S M
Full-Service &
.P
Environmental
Environmental Solutions
al Solutions
05/06/2011
..,:. LABORATORIES, ING
AT[ Allvac
Project: Stormwater Split
Client Sample ID: SW02
Attn: Preston Baucom
Prism Sample ID: 1040646-05
P. O. Box 5030
Prism Work Order: 1040646
Monroe, NC 28110
Sample Matrix: Water
Time Collected: 04/28/11 01:25
Time Submitted: 04/28/11 16:50
Parameter
Result Units Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Total Metals
Zinc
0.40 mg/L 0.030
0.0022 1 *200.7 5/3111 21:58 DWR P1E0005
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 10

Laboratory Report
RI S M
-Service Analytical&
:Full
Environmental Solutions
05/06/2011
LABORATORIES. I —
AT[ Allvac
Project: Stormwater Split
Client Sample ID: In Process
Attn: Preston Baucom
Prism Sample ID: 1040646-06
P. O. Box 5030
Prism Work Order: 1040646
Monroe, NC 28110
Sample Matrix: Water
Time Collected: 04/28/11 01:30
Time Submitted: 04/28/11 16:50
Parameter
Result Units Report
MDL Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Total Metals
Zinc
0.76 mg/L 0.030
0.0022 1 *200.7 513/11 22:05 DWR PlE0005
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 10

Sample Extraction Data
Prep Method:200.7
Lab Number
Batch
Initial
Final
Date
1040646-01
P1 E0005
50
mL
50 mL
05/02/11
1040646-02
P1 E0005
50
mL
50 mL
05/02/11
1040646-03
P1 E0005
50
mL
50 mL
05/02/11
1040646-04
P1 E0005
50
mL
50 mL
05/02/11
1040646-05
P1 E0005
50
mL
50 mL
05/02/11
1040646-06
P1 E0005
50
mL
50 mL
05/02/11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 Of 10

0 4)
E
>
LL LU
C4
z
E z
i5
001
ZO
A
Oull
0
CL
,11
ello
.8!e
u,"r
0
E 0
�s
0
4)
t
cn
.0
c 0
4-01--
2 CL
0)
0 cc
z ',
X
13
LLI
EGi
ul E
6 U.
OR, 00
_j
r
0
0. LU w co
Jk
cc
LU
N
V7
Ill
LU
. I
CL
2
<
-
LU 0
IL -i
--
J 0
0 L'u
rL
ii
C)

❑ ❑ cw
Woo
Z
C
O
n
i
�;\
C�
<
'�
to
a
tnCDMM
,-. O
~'� 0 m
LZ,
c zco
� �� U?
tnm.
o a p
�"t7
�OOc v t m inky
0zi
3 Z
s.0
� m
z
no fn m
co Nn
o
} _
N
I
iv
en,
"�•
Q.Ct
r D
�'`'ry`� fD
Z m O.
� o
y
I
a
C �
O
e o o y
(
ey
C a
o
�_
C) -4
°� A
- 1 o
�- z .�S m :•fie
`
c-Im
m
(1 m �
m 4 m
is
c� z . o @ M cn
I
g
n coil m-+, a
a 1 x �. � C).o W
( P
X
M
It��
W8
my pN
❑p co <� `" \..���'a
�"'
�I
D
xTn o m
°m.o'o G Q.I
ID
z cp
Orm
z{- m 0
r m- oo
�M
x� \-Q
I.
`z
m
o O
mm� H.m .
WmN� �'°
I
I
Dec o
a ms
O
I�
p
Z
`
gs.m OZ
❑ ❑
m N �: � ' � w
3 i a cn `
5,
oy
Z
m
i Z 2 07�
�
f�f
w
$
'?,_
v
-1 O N N fD
D' -4 an d
mzi,� m
y
W �{{ tDs
00
C� .'
r
b
1m
rnm
mo 3 y
cDa n m
t caom
n0 a = m
� y
�
as
�'
}e`
v4
\!'
iii <
- o�
`
p a �.o
(A ti� D
d �.D A
m�N��O
t,3
n fD >
v -.
-:
q-•
G NKD3' N
m� �oO
DO
Z a b ,C o
z O
—cA♦ m m n
LD
o 0�0
cL
sn
� �
a
m
m
z 5q m
Cl)` N
D
�\
�. •f1
I
m
r
ow ID c rm-
y
�m.cc
�
� 3
N•;
Q
0. Q N M z.
ci
W
o m O 0
3
n
h h m
0
3 x z
�.
m
zm.c -�
p 7i7 .n N
�,
N
y
Ik r-
m.
CD'
m. m D':`
Q ? .Zt 0
0
-I
D r m
I ao
I
CD ID
CD
co
'0 JJ M 0
�' •.,v tD ID10,
.
m ,moo
tD y
a
� a a. -tx
t;a o:ry Noy
43
N A z 0�
c z g . t: O
r�l * *
K �°'• � -� Un N n
y 1✓ °"� g c
n < -
C m o�
t A W
z
� n
N C .�•,
N =
o 0 to
•� y �, � to
N C 7 b Z 0.
U) C N
0 � � I�
3 z
g oN.N O O
m
Eq. s O
=tm N m
d N m
CD fi
a � i
•'O D C - r
n Z
r m c�
mC
m
Cl
So �