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HomeMy WebLinkAboutNCS000330_Monitoring Reports_20140818STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. c-S d 00 -2:>72� � DOC TYPE ❑ FINAL PERMIT MONUUORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ d $ lg YYYYM M DD August 14, 2014 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: RECEIVED Atli 19 Z014 CEI)WOFILES IBOG -*j*-'tAT1 P.O. Box 5030 2020 Asheraft Avenue Monroe, NC 28111-5030 Phone: (704) 289-4511 Fax: (704)290-5194 Email: Joe. Hinkle@atimetals.com Attached, ploase find stonnivater monitoring data for Permit No NCS000330. The originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number Start I End Year 5 — Period 2 10 March 1, 2014 1 August 31, 2014 Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, q— �-L Joe Ilinkle EHS Manager -'�- ATI Allvac Allvac - Monroe Plant Wir Sty Ater Monitoring Report Forin Sample Time: Stormwater Discharge Outfall #2 Drainage Area = 272,590sci. ft. = 6.25 acres % hnpervious = 36% r4alu'lazolla don L i A kca �e :Tr - Parameter Results (mg/1) Benchmark Values (mg/1) BOD 30 COD 120 TSS 100 Cadmium A 0.001 Chromium, total recoverable 6'30 1 Lead, total recoverable . A IYD 0.03 Nickel, total recoverable 0169M 0.26 Zinc, total recoverable 0.067 0-11 and Cifease pH (std units) 30 6,9 (std units) Storm Date: St® Duration: (I-Irs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.1": Estimated Flow Calculation: Q = Cuk Q(Total) = Q(Pervious Area) + Q(hnpervious Area) Q(tot., cfs) = (A x inches rain/1 2 inches/ft. x 6.25 acres x .64) +.9 x inches rain/1 2inches/ft. x 6.25 x .36) f(Total, cfs) 1333 x (Inches of rain) +.1688 x Z 0 4) (Inches ofrain., =S r . D. J�3 7 cfs 0 ,z A isU � oz N 0 H o � 0 PC d Friv� o � �d oo� � in b y � O O oz o q g 4 Ri A � Fa O 'r O O t py o o py o O F � � y a � o 0 A •�•a�w aa� 47 O O � � J Rt aQi /mil a 0 d 40. m Q =� CI y w Mcc a a o eaa ,�•o n p ,Q d 4r ao °7 R• 6 •d d � � a a C �aC ;a Cd C Qualitative Monitoring Report For guidance on filling out this form, please visit_ http://h2c.enr.state.nc.us/su/Forms Documents htm#miseforms Permit No.: Nlv, Ql ✓ ,10101 Facility Name: /% �/i1a e County: Inspecto: Date of I I'iiiie Uf luspeuiun: _ /G�..' l')o Total Event Precipitation (inches): or Certificate of Coverage No.: N/C/GI / l l_l / / Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signatu7 I certify that this eport is accurate and complete to the best of my knowledge: (Signature of Permittee 1. Outfalll Description: OLLtfall NO. ,, S Receiving Stream: Descnbe they ndustrial activities ditch, occur within the uutfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: /, � 1z'f 4? t" 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Page 1 of 2 S,WU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 C) 3 4 5 7. Is there any foam in the stormwater discharge? Yes 6 S. Is there an oil sheen in the stormwater discharge? Yes T�-o 9. Is there evidence of erosion or deposition at the outfall? Yes _ No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 For guidance on filling out this form, please visit_ http:/lh2o.enr.state.ne.us/su/Forms Documents htm#uaiscforms Permit No_: f f / / ! or Certificate of Coverage No.: N/C/G/ Facility Name: % .L % C County: a 17r fD /1 Phone No. _'76?]9 .f - 4S7/ Inspector: _ -Zomin/ Z�2� Date of Inspection: --%� That uI hispeatuu: Total Event Precipitation (inches): 0, 60 Was this a Representative Storm Event? (See information below) 'Yes ❑ No Please check yourpermit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signatureyI certify that this report is accurate and complete to the best of my knowledge: (Signature of 1. Out€allIDescription: outfall No, <_ 60 (2f; truotur (pipe; ditch, etc.) T "� Receiving Stream: / Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (Iight, medium, dark) as, descriptors: fie_ act en l> /ii� V 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /%UPI Page 1 of 2 SWU-242-112608 a 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 Q 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 nq2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 0 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 For guidance on filling out this form, please visit: httlo:/lh2o.enr.state.nc.us/su/Forms Documents htm#tmiseforms Permit No.: N/C./<S/ Facility Name: -- Z County: /, Inspector: Z Date of Inspection: _ Time of Inspection: )/ or ('ertificate of Coverage, No.: N/C/G/ / / /_/ / / Total Event Precipitation (inches): QA 60 f No. Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signatu7, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittr q or 1. Out€a l Desen taon: l / Ouffall Noy c % Stntoture (pipe, ditch, ate.) oVI / c°:�i- Receiving Stream: DesMbe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: �. �h , 3. (odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak - chlorine odor, etc.): /)cg/J Page 1 of 2 SWU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 ?. 0 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 (1 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 @3 4 5 7. Is there any foam in the stormwater discharge? Yes S 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 S)VU-242-112608 ba7' Qualitative Monitoring Report For guidance on filling out this form, please visit: hgp://h2o.enr.state.ne.us/su/Forms Documents.htm#miscforms Permit No : NiC.6/ /C)/c/)/ _S /5/ / or Certificate of Coverage No.: NIC/G/ Facility Name: County: Inspector: Date of Inspection: 'Time of Inspection: Total Event Precipitation (inches): _ CJdCJ ��— No. Was this a Representative Storm Event? (See information below) 'Yes ❑ No Please check yourpermit to veriff if Qualitative Monitoring must be/pe'rformed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. By this signature certify that thiVeport is accurate and complete to the best of my knowledge: (Signature of Permittee 1. Outfall D scrip on: Outfall No. Receiving Stream: Describe the inriustxial activif that uccur %vithin the outfall drainage area: 2. Color: Describe the color of (light, medium, dark) as descriptors: _ 0 I ,jrge using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4C1�'/(f , Page 1 of 2 S,W-242-112608 t 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: - @ 2 3 4 , 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 02 3 4 5 7. Is there any foam in the stormwater discharge? Yes No S. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. SWU-242-112608 Page 2 of 2 dam` rATE r. Qualitative Monitoring Report For guidance on filling out this form, please visit: httio://h2o.enr.state.nc.us/su/Forms Documents htm#miscforms Permit No.: N/Qk, Facility Name: 1 County: Inspector: , le< Date of Inspection: Time of Inspection: Total Event Precipitation (inches): or Certificate of Coverage No.: N/C/G/ / / // / / No. Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has j occurred. A single storm event may contain up to 10 consecutive hours of no nrecinitation_ By this siature, I certify that this report is accurate and complete to the best of my knowledge: 79 A (Signature of Pem ee or 1. Outfall Description: Outfah No. -�� )Sttuctu a (pipe, Glitch, etc:.) r G Reac i vutg Slteam. / W l'.!'1 it f i III r1L l e- t nAet`r;lia f'bi ;—Iiy[.4 nl LLLL,eirl CM 2. Color: Describe the color of the dischajge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: T_A fit; t_j t k-- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ti C-� Page I of 2 S,WU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very, cloudy: 1 `J 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 C2) 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes oNo 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 �,,, 5rA7F s�pur.4fi QualitativeMonitoring Report For guidance on filling out this form, please visit. http:/lh2o.enr.state.nc.us/su/Forms Documents htm#miscforms Permit No.: INt/c4s/0/0/3&t /(D/ or Certificate of Coverage No.: N/C/G/ Facility Name: 1 L. County: -U 11 [r) t Phone No. Inspector: Date of Inspection: __. l'/ Time of Inspection: C L96 f�YYt Total Event Precipitation (inches): Oo 60 " Was this a Representative Storm Event? (See information below) A 'Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has i occurred_ A single storm event may contain up to 10 consecutive hours of no nrecinitation. By this sil�ature, I certify tha� this report is accurate and complete to the best of my knowledge: (Signature of Permit(4 or 1. Outfall Description: Outfall No,, Recei viug S Li=ui. Describe the industaialactivit uctuie Oipe, dttc:11, etu.) i that occur 2. Color: Describe the color of (light, medium, dark) as descriptors: _ (lie iatfall)tlawage area: t (O�Oer� .11. using basic colors (red, brown, blue, etc.) and tint cJr 3. Odor: Describe any distinct odors that the discharge may have (i.e., smeIls strongly of oil, weak chlorine odor, etc.): � U/1 f Page 1 of 2 5WU-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (D 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 �_:J 3 4 5 7. Is there any foam in the stormwater discharge? Yes DNo 8. Is there an oil sheen in the stormwater discharge? Yes e 9. Is there evidence of erosion or deposition at the outfall? Yes oNo 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence. of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2of2 SWU-242-112608 aceAnalytical www.pacelabs.com July 23, 2014 Mr. Joe Hinkle Allvac RE: Project: Monroe Stormwater Pace Project No.: 92209551 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 16, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted In the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, iA. Laura J Cooper ]aura. cooper c@i pacelabs.curn Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac pCGPF . REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, (,9eO j without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 acmnalytical www.pacelabs.corn i Project: Monroe Stormwater Pace Project No.: 92209551 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certlflcatlon IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #• M-NC030 North Carolina drinking Water Certification * 37712 CERTIFICATIONS Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VFt AP Certification #• 400222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 14 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Project: Monroe Stormwater Pace Project No.: 92209551 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92209551001 MSW02 EPA 1664B CLW 1 PASI-C EPA 200.7 JMW 5 PASI-A SM 2540D TEP 1 PASI-A SM 5210B MAB 1 PASI-A SM 5220D SMW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 Pace Analytical Services, Inc. aceAnalytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92209551 Sample: MSW02 Lab ID: 92209551001 Collected: 07/15/14 19:41 Received: 07/16/14 16:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By TOMMY 1 07/15/14 19:41 LONG, BRANDON LINKER, DAVID POPE JR. Field pH 6.6 Std. Units U. IU I 0//15/14 19:41 Field Temperature 26.3 deg C U.bO 1 07/15/14 19:41 HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 07/18/14 13:01 200.7 MET ICP Analytical Method: EPA200.7 Preparation Method: EPA200.7 Cadmium ND ug/L 1.0 1 07/18/14 12:50 07/22/14 04:11 7440-43-9 Chromium 30.2 ug/L 5.0 1 07/18/14 12:50 07/22/14 04:11 7440-47-3 Lead ND ug/L 5.0 1 07/18/14 12:50 07/22/14 04:11 7439-92-1 Nickel 88.8 ug/L 5.0 1 07/18/14 12:50 07/22/14 04:11 7440-02-0 Zinc 156 ug/L 10.0 1 07/18/14 12:50 07/22/14 04:11 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 21.0 mg/L 3.6 1 07/22/14 03:29 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 11.8 mg/L 2.0 1 07/17/14 06:15 07/22/14 01:45 L1 6220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 39.0 mg/L 25.0 1 07/18/14 23:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 14 ,�aceAnalydcal' www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92209551 QC Batch: GCSV/18268 QC Batch Method: EPA 1664B Associated Lab Samples: 92209551001 METHOD BLANK: 1244684 Associated Lab Samples: 92209551001 Parameter Units Oil and Grease mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 07/18/1413:00 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABOHAiOKY CON I ROL SAMPLE: 1244685 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 37.9 95 78-114 MATRIX SPIKE SAMPLE: 1244686 92209628001 Spike MS MS % Rec Parnmotor Units Rosult Cone ReSUlt % Rec Limits Qualiflei-6 Oil and Grease mg/L ND 40 36.5 91 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14 aceAnalytical wwwpacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92209551 QC Batch: MPRP/16469 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92209551001 METHOD BLANK: 1244788 Matrix: Water Associated Lab Samples: 92209551001 Blank Reporting Parameter Units Result Limit Analyzed Cadmium ug/L ND 1.0 07/22/14 03:47 Chromium ug/L NU 5.0 0'//22/14 03:47 Lead ug/L ND 5.O O7/22/14 03:47 Nickel ug/L ND b.O O1/22/14 03:47 Zinc ug/L ND 10.0 07/22/14 03:47 Qualifiers Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1244789 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug/L 500 487 97 85-1115 Chromium ug/l 500 480 96 85-115 Lead ug/L 500 491 98 85-115 Nickel ug/L 500 487 97 85-115 Zinc ug/L 500 483 97 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1244790 1244791 MS MSD 92209550002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[ Cadmium ug/L ND 500 500 491 494 98 99 70-130 1 Chromium ug/L 0,049 500 500 535 535 97 97 70-130 0 mg/L Lead ug/L ND 500 500 477 482 94 95 70-130 1 Nickel ug/l 0.034 500 600 612 b / Jb 96 /0-130 1 mg/L Zinc ug/l. 11.1 500 500 11500 11400 78 68 70-130 0 M1 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1244792 1244793 MS MSD 92209482001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L 0.26 500 500 742 741 96 96 70-130 0 mg/L Chromium ug/L 0.67 500 500 1130 1060 93 78 70-130 7 mg/L Lead ug/L 20.4 500 500 21100 20600 130 40 70-130 2 M6 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92209551 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1244792 1244793 MS MSD 92209482001 Spike Spike MS MSD Parameter Units Result Conc. Conc. Result Result Nickel ug/L 1.8 500 500 2220 2140 mg/L Zinc ug/L 50.8 500 500 60800 60600 mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MS MSD % Rec % Rec % Rec Limits RPD Qua] 89 74 70-130 3 -20 -60 70-130 0 MG Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 14 4 aceAnalytica( www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92209551 QC Batch: WET/32201 QC Batch Method: SM 2540D Associated Lab Samples: 92209551001 METHOD BLANK. 1246458 Associated Lab Samples: 92209551001 Parameter Units Total Suspended Solids mg/L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07/22/14 03:24 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1246459 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 226 90 80-120 SAMPLE DUPLICATE: 1246460 92209869001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 273 292 7 SAMPLE DUPLICATE: 1246461 92209553001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 255 244 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14 �acmnalj6cal" www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92209551 QC Batch: WET/32129 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92209551001 METHOD BLANK: '1243591 Associated Lab Samples: 92209551001 Parameter Units BOD, 5 day mg/L LABORATORY CONTROL SAMPLE: 1243592 Parameter Units BOD, 5 day mg/L SAMPLE DUPLICATE: 1243593 Parameter Units BOD, 5 day mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 07/22/14 01:45 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 256 129 84.5-115.4 L0,L1 92209401001 Dup Result Result RPt1 Cualifiers 12.2 12.2 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14 aceAnalytical www.pacelabs.corn QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Monroe Stormwater Pace Project No.: 92209551 QC Batch: WETA/19630 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92209551001 METI IOD BLANK: 1245549 Matrix: Water Associated Lab Samples: 92209551001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 07/18/14 23:00 LABORATORY CONTROL SAMPLE: 1245550 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 776 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1245551 1245552 MS MSD 92208517002 Spike Spike MS MSD MS MS1) % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 351 750 750 776 769 57 56 75-125 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1245553 1245554 MS MSD 92209553001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 133 750 750 549 556 55 56 75-125 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 14 �acmnalyficalo www.pwelabs.c= QUALIFIERS Project: Monroe Stormwater Pace Project No.: 92209551 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S Surrogate 1,2-Dlphenylhydrazlne (82/0listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. 11 Analyte recovery In the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. MF Matrix splko and Matrix erliko dupllcato recovery not evaluated against control limits due to sample dilution. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: Monroe Stormwater 92209551 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92209551001 MSW02 FLD/ 92209551001 MSW02 EPA 1004E GCSV/18268 92209551001 MSW02 EPA 200.7 MPRP/16469 EPA 200.7 ICP/14873 92209551001 MSW02 SM 2540D WET/32201 92209551001 MSW02 SM 5210B WET/32129 SM 5210B WET/32132 92209561001 MSW02 SM 5220U WE IA/19630 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. 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