HomeMy WebLinkAboutNCS000330_Monitoring Reports_20140818STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
c-S d 00 -2:>72� �
DOC TYPE
❑ FINAL PERMIT
MONUUORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ d $ lg
YYYYM M DD
August 14, 2014
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
RECEIVED
Atli 19 Z014
CEI)WOFILES
IBOG
-*j*-'tAT1
P.O. Box 5030
2020 Asheraft Avenue
Monroe, NC 28111-5030
Phone: (704) 289-4511
Fax: (704)290-5194
Email: Joe. Hinkle@atimetals.com
Attached, ploase find stonnivater monitoring data for Permit No NCS000330. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
Start
I End
Year 5 — Period 2
10
March 1, 2014
1 August 31, 2014
Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
q— �-L
Joe Ilinkle
EHS Manager
-'�- ATI Allvac
Allvac - Monroe Plant Wir
Sty Ater Monitoring Report Forin
Sample Time:
Stormwater Discharge Outfall #2
Drainage Area = 272,590sci. ft. = 6.25 acres
% hnpervious = 36%
r4alu'lazolla don L i A kca �e
:Tr -
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
A
0.001
Chromium, total recoverable
6'30
1
Lead, total recoverable
. A
IYD
0.03
Nickel, total recoverable
0169M
0.26
Zinc, total recoverable
0.067
0-11 and Cifease
pH
(std units)
30
6,9 (std units)
Storm Date: St® Duration: (I-Irs.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.1":
Estimated Flow Calculation:
Q = Cuk
Q(Total) = Q(Pervious Area) + Q(hnpervious Area)
Q(tot., cfs) = (A x inches rain/1 2 inches/ft. x 6.25 acres x .64) +.9 x inches rain/1 2inches/ft. x 6.25 x .36)
f(Total, cfs) 1333 x
(Inches of rain) +.1688 x Z 0 4) (Inches ofrain.,
=S r
. D. J�3 7 cfs
0
,z
A isU
�
oz
N
0
H
o �
0
PC
d
Friv�
o
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oz
o
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'r O
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t py o
o
py o
O
F
� � y
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•�•a�w
aa�
47 O
O �
� J Rt aQi
/mil
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C
Qualitative Monitoring Report
For guidance on filling out this form, please visit_ http://h2c.enr.state.nc.us/su/Forms Documents htm#miseforms
Permit No.: Nlv, Ql ✓ ,10101
Facility Name: /% �/i1a e
County:
Inspecto:
Date of I
I'iiiie Uf luspeuiun: _ /G�..' l')o
Total Event Precipitation (inches):
or Certificate of Coverage No.: N/C/GI / l l_l / /
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signatu7 I certify that this
eport is accurate and complete to the best of my knowledge:
(Signature of Permittee
1. Outfalll Description:
OLLtfall NO. ,, S
Receiving Stream:
Descnbe they ndustrial activities
ditch,
occur within the uutfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: /, � 1z'f 4? t"
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
Page 1 of 2
S,WU-242-112608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 C) 3 4 5
7. Is there any foam in the stormwater discharge? Yes 6
S. Is there an oil sheen in the stormwater discharge? Yes T�-o
9. Is there evidence of erosion or deposition at the outfall? Yes _ No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608
For guidance on filling out this form, please visit_ http:/lh2o.enr.state.ne.us/su/Forms Documents htm#uaiscforms
Permit No_: f f / / ! or Certificate of Coverage No.: N/C/G/
Facility Name: % .L % C
County: a 17r fD /1 Phone No. _'76?]9 .f - 4S7/
Inspector: _ -Zomin/ Z�2�
Date of Inspection: --%�
That uI hispeatuu:
Total Event Precipitation (inches): 0, 60
Was this a Representative Storm Event? (See information below) 'Yes ❑ No
Please check yourpermit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signatureyI certify that this report is accurate and complete to the best of my knowledge:
(Signature of
1. Out€allIDescription:
outfall No, <_ 60 (2f; truotur (pipe; ditch, etc.) T "�
Receiving Stream: /
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(Iight, medium, dark) as, descriptors: fie_ act en l> /ii� V
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): /%UPI
Page 1 of 2
SWU-242-112608
a
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 Q 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 nq2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 0 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608
For guidance on filling out this form, please visit: httlo:/lh2o.enr.state.nc.us/su/Forms Documents htm#tmiseforms
Permit No.: N/C./<S/
Facility Name: -- Z
County: /,
Inspector: Z
Date of Inspection: _
Time of Inspection:
)/ or ('ertificate of Coverage, No.: N/C/G/ / / /_/ / /
Total Event Precipitation (inches): QA 60 f
No.
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signatu7, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittr q or
1. Out€a l Desen taon: l /
Ouffall Noy c % Stntoture (pipe, ditch, ate.) oVI / c°:�i-
Receiving Stream:
DesMbe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: �. �h ,
3. (odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak -
chlorine odor, etc.): /)cg/J
Page 1 of 2
SWU-242-112608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 ?. 0 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 (1 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 @3 4 5
7. Is there any foam in the stormwater discharge? Yes S
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S)VU-242-112608
ba7'
Qualitative Monitoring Report
For guidance on filling out this form, please visit: hgp://h2o.enr.state.ne.us/su/Forms Documents.htm#miscforms
Permit No : NiC.6/ /C)/c/)/ _S /5/ / or Certificate of Coverage No.: NIC/G/
Facility Name:
County:
Inspector:
Date of Inspection:
'Time of Inspection:
Total Event Precipitation (inches): _ CJdCJ ��—
No.
Was this a Representative Storm Event? (See information below) 'Yes ❑ No
Please check yourpermit to veriff if Qualitative Monitoring must be/pe'rformed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature certify that thiVeport is accurate and complete to the best of my knowledge:
(Signature of Permittee
1. Outfall D scrip on:
Outfall No.
Receiving Stream:
Describe the inriustxial activif
that uccur %vithin the outfall drainage area:
2. Color: Describe the color of
(light, medium, dark) as descriptors: _
0
I ,jrge using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): 4C1�'/(f ,
Page 1 of 2
S,W-242-112608
t
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
- @ 2 3 4 , 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 02 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
S. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
SWU-242-112608
Page 2 of 2
dam` rATE
r.
Qualitative Monitoring Report
For guidance on filling out this form, please visit: httio://h2o.enr.state.nc.us/su/Forms Documents htm#miscforms
Permit No.: N/Qk,
Facility Name: 1
County:
Inspector: , le<
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches):
or Certificate of Coverage No.: N/C/G/ / / // / /
No.
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
j occurred. A single storm event may contain up to 10 consecutive hours of no nrecinitation_
By this siature, I certify that this report is accurate and complete to the best of my knowledge:
79 A
(Signature of Pem ee or
1. Outfall Description:
Outfah No. -�� )Sttuctu a (pipe, Glitch, etc:.) r G
Reac i vutg Slteam. / W l'.!'1 it f i III r1L l e- t
nAet`r;lia f'bi ;—Iiy[.4 nl
LLLL,eirl CM
2. Color: Describe the color of the dischajge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: T_A fit; t_j t k--
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): ti C-�
Page I of 2
S,WU-242-112608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very, cloudy:
1 `J 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 C2) 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes oNo
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence -of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608
�,,, 5rA7F
s�pur.4fi
QualitativeMonitoring Report
For guidance on filling out this form, please visit. http:/lh2o.enr.state.nc.us/su/Forms Documents htm#miscforms
Permit No.: INt/c4s/0/0/3&t
/(D/ or Certificate of Coverage No.: N/C/G/
Facility Name: 1 L.
County: -U 11 [r) t Phone No.
Inspector:
Date of Inspection: __. l'/
Time of Inspection: C L96 f�YYt
Total Event Precipitation (inches): Oo 60 "
Was this a Representative Storm Event? (See information below) A 'Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
i occurred_ A single storm event may contain up to 10 consecutive hours of no nrecinitation.
By this sil�ature, I certify tha� this report is accurate and complete to the best of my knowledge:
(Signature of Permit(4 or
1. Outfall Description:
Outfall No,,
Recei viug S Li=ui.
Describe the industaialactivit
uctuie Oipe, dttc:11, etu.) i
that occur
2. Color: Describe the color of
(light, medium, dark) as descriptors: _
(lie iatfall)tlawage area: t
(O�Oer� .11.
using basic colors (red, brown, blue, etc.) and tint
cJr
3. Odor: Describe any distinct odors that the discharge may have (i.e., smeIls strongly of oil, weak
chlorine odor, etc.): � U/1 f
Page 1 of 2
5WU-242-112608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 (D 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 �_:J 3 4 5
7. Is there any foam in the stormwater discharge? Yes DNo
8. Is there an oil sheen in the stormwater discharge? Yes e
9. Is there evidence of erosion or deposition at the outfall? Yes oNo
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence. of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2of2
SWU-242-112608
aceAnalytical
www.pacelabs.com
July 23, 2014
Mr. Joe Hinkle
Allvac
RE: Project: Monroe Stormwater
Pace Project No.: 92209551
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on July 16, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted In the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
iA.
Laura J Cooper
]aura. cooper c@i pacelabs.curn
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
pCGPF .
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
(,9eO j without the written consent of Pace Analytical Services, Inc.. Page 1 of 14
acmnalytical
www.pacelabs.corn
i
Project: Monroe Stormwater
Pace Project No.: 92209551
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certlflcatlon IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #• M-NC030
North Carolina drinking Water Certification * 37712
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VFt AP Certification #• 400222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Page 2 of 14
aceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: Monroe Stormwater
Pace Project No.: 92209551
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92209551001 MSW02 EPA 1664B
CLW
1
PASI-C
EPA 200.7
JMW
5
PASI-A
SM 2540D
TEP
1
PASI-A
SM 5210B
MAB
1
PASI-A
SM 5220D
SMW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 14
Pace Analytical Services, Inc.
aceAnalytical ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
(704)875-9092
ANALYTICAL RESULTS
Project: Monroe Stormwater
Pace Project No.: 92209551
Sample: MSW02 Lab ID: 92209551001 Collected: 07/15/14 19:41 Received: 07/16/14 16:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
TOMMY
1
07/15/14 19:41
LONG,
BRANDON
LINKER,
DAVID
POPE JR.
Field pH
6.6 Std. Units
U. IU
I
0//15/14 19:41
Field Temperature
26.3 deg C
U.bO
1
07/15/14 19:41
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0
1
07/18/14 13:01
200.7 MET ICP
Analytical Method: EPA200.7 Preparation
Method: EPA200.7
Cadmium
ND ug/L
1.0
1
07/18/14 12:50
07/22/14 04:11
7440-43-9
Chromium
30.2 ug/L
5.0
1
07/18/14 12:50
07/22/14 04:11
7440-47-3
Lead
ND ug/L
5.0
1
07/18/14 12:50
07/22/14 04:11
7439-92-1
Nickel
88.8 ug/L
5.0
1
07/18/14 12:50
07/22/14 04:11
7440-02-0
Zinc
156 ug/L
10.0
1
07/18/14 12:50
07/22/14 04:11
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
21.0 mg/L
3.6
1
07/22/14 03:29
5210B BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
11.8 mg/L
2.0
1
07/17/14 06:15
07/22/14 01:45
L1
6220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
39.0 mg/L
25.0
1
07/18/14 23:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 14
,�aceAnalydcal'
www.pacelabs.com
Project: Monroe Stormwater
Pace Project No.: 92209551
QC Batch: GCSV/18268
QC Batch Method: EPA 1664B
Associated Lab Samples: 92209551001
METHOD BLANK: 1244684
Associated Lab Samples: 92209551001
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 07/18/1413:00
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABOHAiOKY CON I ROL SAMPLE:
1244685
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 37.9
95
78-114
MATRIX SPIKE SAMPLE:
1244686
92209628001 Spike
MS
MS
% Rec
Parnmotor
Units
Rosult Cone
ReSUlt
% Rec
Limits Qualiflei-6
Oil and Grease
mg/L
ND 40
36.5
91
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14
aceAnalytical
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QUALITY CONTROL DATA
Project: Monroe Stormwater
Pace Project No.: 92209551
QC Batch: MPRP/16469
Analysis Method:
EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 92209551001
METHOD BLANK: 1244788
Matrix: Water
Associated Lab Samples: 92209551001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Cadmium
ug/L
ND
1.0
07/22/14 03:47
Chromium
ug/L
NU
5.0
0'//22/14 03:47
Lead
ug/L
ND
5.O
O7/22/14 03:47
Nickel
ug/L
ND
b.O
O1/22/14 03:47
Zinc
ug/L
ND
10.0
07/22/14 03:47
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE:
1244789
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
487
97
85-1115
Chromium
ug/l
500
480
96
85-115
Lead
ug/L
500
491
98
85-115
Nickel
ug/L
500
487
97
85-115
Zinc
ug/L
500
483
97
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1244790
1244791
MS
MSD
92209550002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Cadmium
ug/L
ND
500
500
491
494
98
99
70-130
1
Chromium
ug/L
0,049
500
500
535
535
97
97
70-130
0
mg/L
Lead
ug/L
ND
500
500
477
482
94
95
70-130
1
Nickel
ug/l
0.034
500
600
612
b /
Jb
96
/0-130
1
mg/L
Zinc
ug/l.
11.1
500
500
11500
11400
78
68
70-130
0 M1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1244792
1244793
MS
MSD
92209482001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium ug/L 0.26 500
500
742
741
96
96
70-130 0
mg/L
Chromium ug/L 0.67 500
500
1130
1060
93
78
70-130 7
mg/L
Lead ug/L 20.4 500
500
21100
20600
130
40
70-130 2 M6
mg/L
Results presented on this page are in the units indicated by the
"Units" column except where an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc..
Page 6 of 14
aceAnalytical
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QUALITY CONTROL DATA
Project: Monroe Stormwater
Pace Project No.: 92209551
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1244792
1244793
MS
MSD
92209482001 Spike
Spike
MS
MSD
Parameter Units
Result Conc.
Conc.
Result
Result
Nickel ug/L
1.8 500
500
2220
2140
mg/L
Zinc ug/L
50.8 500
500
60800
60600
mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
MS MSD % Rec
% Rec % Rec Limits RPD Qua]
89 74 70-130 3
-20 -60 70-130 0 MG
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc..
Page 7 of 14
4
aceAnalytica(
www.pacelabs.com
Project: Monroe Stormwater
Pace Project No.: 92209551
QC Batch: WET/32201
QC Batch Method: SM 2540D
Associated Lab Samples: 92209551001
METHOD BLANK. 1246458
Associated Lab Samples: 92209551001
Parameter Units
Total Suspended Solids mg/L
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 07/22/14 03:24
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE:
1246459
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250
226 90
80-120
SAMPLE DUPLICATE: 1246460
92209869001
Dup
Parameter
Units
Result
Result RPD
Qualifiers
Total Suspended Solids
mg/L
273
292
7
SAMPLE DUPLICATE: 1246461
92209553001
Dup
Parameter
Units
Result
Result RPD
Qualifiers
Total Suspended Solids
mg/L
255
244
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 14
�acmnalj6cal"
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QUALITY CONTROL DATA
Project: Monroe Stormwater
Pace Project No.: 92209551
QC Batch: WET/32129 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92209551001
METHOD BLANK: '1243591
Associated Lab Samples: 92209551001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 1243592
Parameter Units
BOD, 5 day mg/L
SAMPLE DUPLICATE: 1243593
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/22/14 01:45
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 256 129 84.5-115.4 L0,L1
92209401001 Dup
Result Result RPt1 Cualifiers
12.2 12.2 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 14
aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Monroe Stormwater
Pace Project No.: 92209551
QC Batch: WETA/19630
Analysis Method: SM
5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92209551001
METI IOD BLANK: 1245549
Matrix:
Water
Associated Lab Samples: 92209551001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed
Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
07/18/14 23:00
LABORATORY CONTROL SAMPLE: 1245550
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits
Qualifiers
Chemical Oxygen Demand mg/L
750
776
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1245551
1245552
MS
MSD
92208517002
Spike
Spike MS
MSD MS
MS1)
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 351
750
750 776
769 57
56
75-125
1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1245553
1245554
MS
MSD
92209553001
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec
% Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 133
750
750 549
556 55
56
75-125
1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc..
Page 10 of 14
�acmnalyficalo
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QUALIFIERS
Project: Monroe Stormwater
Pace Project No.: 92209551
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S Surrogate
1,2-Dlphenylhydrazlne (82/0listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
11 Analyte recovery In the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MF Matrix splko and Matrix erliko dupllcato recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14
aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
Pace Project No.:
Monroe Stormwater
92209551
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92209551001
MSW02
FLD/
92209551001
MSW02
EPA 1004E
GCSV/18268
92209551001
MSW02
EPA 200.7
MPRP/16469 EPA 200.7
ICP/14873
92209551001
MSW02
SM 2540D
WET/32201
92209551001
MSW02
SM 5210B
WET/32129 SM 5210B
WET/32132
92209561001
MSW02
SM 5220U
WE IA/19630
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2014 09:27 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 14
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