HomeMy WebLinkAboutNCS000330_Monitoring Reports_20150719STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
DOC TYPE
❑ FINAL PERMIT
❑ MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ `Z6\
YYYYM M DD
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August 25, 2015
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
RECEIVED
AUG 2 8 2015
CENTRAL FILES
DWR SECTION
TOW
3!�ATI
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Phone: (704) 2894511
Fax: (704)290-5194
Email: Joe.Hinkle@atimetals.com
Attct('1tN(l, ltlotis(-, Cittd stortti\�ial(�r monitoring data for Poniiit No NCS000330. The originals alld
one copy are included. The monitoring data is for the following monitoring schedule:
Monitonng Period
Sample Number
Start
I End
Year 6 — Period 2
12
March 1, 2015
1 August 31, 2015
Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
q{--
(' �/
Jo HGinkle
EHS Manager
Allvac - Monroe Plant
Stonnwater Mo!u �toriay'Reuort
ME --
Sample Time: ,® J15 /'/Y?
T1 Allvac
Storrawater Diggharge Outfall #2
Drainage Area = 272,590sq. ft. = 6.25 acres
% Impervious = 36%
IL
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
0.001
Chromium, total recoverable
1
Lead, total recoverable
AI'D
0.03
Nickel, total recoverable
8.y.-5
0.26
Zinc, total recoverable
90
0.067
Oil and Gwase
(Std units)
30
PH
69 (std units)
Storm Date: Storm Duration: It
A3 - (firs.) Inches of Rainfall:-0-1-0
Duration of time preceding rain event exceeding 0.111: 136 (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x.64) +.9 x inches rain/12inches/ft. x 6.25 x.36)
41 (Total, cfs) 1333 x (Inches of rain) + .168 8 x
(Inches of rain,
6 cfs
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. httl2:/Iportal.ncdenr.org/web/wQ,/ws/su/npdessw#tab-4
Permit No.: N/,
Facility Name:
County: U r
Inspector:
j/o/ or Certificate of Coverage No.:
Phone No.
Date of Inspection: 16 o19-114/S
Time of Inspection: %L1„' 3 '417t g
Total Event Precipitation (inches) b n j/-)
�S I
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
XYes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
..................................................................................
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least'/2 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
...................
...................................... ............... -...... _..... _..........
........................................................................................................._..............................................................._.-----_--_
By this signatuie, I certify that
`this report is accurate and complete to the best of my knowledge:
(Signature of Permitte"r D
Page 1 of 2
SWU-242, Last modified 10/25/2012
1
1. Outfall Description:
Outfall No. /)/) � ZJ6
Receiving Stream:
t
(pipe, ditch, etc.)
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: Chi/V k
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 112,191) 6
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 1 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 6) 4 5
7. Is there any foam in the stormwater discharge? Yes
B. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall?
10. Other Obvious Indicators of Storinwater Pollution:
List and describe /r;�2WZ--
No
Yes No
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
SWU-242, Last modified 10/25/2012
Page 2 of 2
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. http://portal.ncdenr.org/web/wq./ws/su/npdessw#tab-4
Permit No.: N/C/�/Q/�/�//// or Certificate of Coverage No.: N
X
Facility Name:
County: L
Inspector:
Date of Inspection:
Time of Inspection:
Phone No. '1z)if -IZV -ZIS,
Total Event Precipitation (iuclies): � .: ,
ri
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
........... -..................................................................................................................................................................................................................................................................................................................................................................................................................................
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
.........................................................................................................
By this signate, I certify that t�is report is accurate and complete to the best of my knowledge:
(Signature of Pe
Page 1 of 2
SWU-242, Last modified 10/25/2012
1. Outfalt Description:
Outfall No. ,<
Receiving Stream:
Describe the industrial activi
(pipe, ditch, etc.)
that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: mle:7
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 (3� 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 0 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 V 4 5
7. Is there any foam in the stormwater discharge? Yes No
B. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes nNo
10. Other Obvious Indicators of Storinwater Pollution:
List and describe A10AfeE
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
LE-W
w-1fa,�
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: htW://portal.ncdenr.org/web/wq/ws/su.lnl2dessw#tab-4
Permit No.: N/C/,5/6/Q/0
-0/ or Certificate of Coverage No.:
Facility Name: A?% 1 / 1/l� G
County: /I il Lj
Inspector:
Date of Inspection:
Time of Inspection: _//,`0S.bnl
Total Event Precipitation (inches). 3,C,
Phone No.
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
..............................................................................................................................................................
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
...._..
........................................................................................................................................................................................................._ --- -
By this sipature, I certify that this report is accurate and complete to the best of my knowledge:
1/7
(Signature of Peittee or D
Page 1 of 2
SWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No. /)MOO-3f`
Receiving Stream: Z
Describe the industrial activi
(pipe, ditch, etc.
that occur within the
2. Color: Describe the color of the
(light, medium, dark) as descriptors: _
L
basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 40 itf-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy: 9
1 0 3 4 J
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
6D 2 3 4 5
C. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes oNo
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes 1 No
10. Other ObviousIndicators of Storinwaler Pollution:
AW
List and describe /0AII :
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit, httn://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
Permit No.: N/C/S/L/L/Q/z�/3/6/ or Certificate of Coverage No.: N
Facility Name:
County:
Inspector:
Dale of Inspection:
Time of Inspection: /,W," / Pm
Total Event Precipitation (inches). L3L z
Phone No.
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
9 Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
...11 ............................... ..... ......... ................................ ............ ......... ... ..................................................... ...................................................... _........................... ................................................ ....................... ...... ....................... ..... ....................................
,
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
i
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
................................................................................................ .......... .................. ...:
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of PerrQuee or D
Pagel of 2
SWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No.%' �jt/)y Structure (pipe, ditch, etc.)
Receiving Stream:
Describe the indust ial activities that occur.witbin the outfall drainage area:
2. Color: Describe the color of thedischarge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: /%d /— k-v cJsL
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): A10' e
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 N
clear and 5 is very cloudy:
1 02 3 4 S
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
10 2 3 4 5
G. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 20 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
ee
10. Other Obvious Iiadicators of Sturwwater Pollution:
List and describe WOMet-E
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
4
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4
Permit No.: N/C/,///,�/// or Certificate of Coverage No.:
Facility Name: l .L_ %Aldr
County- 1. L e
Inspector: )f) 6
Date of Inspection: 1
Time of Inspection:
Phone No.
Total Event Precipitation (inclies): � ,3 0
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
.............................................................................._.............................
................
.................................
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
pernlilled site uulfall. The previous measurable storm event must have been at least 77, hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
............................................................................................._......................................._..................................................._........................---
By this signare, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permit* or De
Pagel of 2
SWU-242, Last modified 10/25/2012
1. Outfall Description:
Outfall No. / ,l J Stru
Receiving Stream: —
Des�ribe the industrial activities
(pipe, ditch, etc.)iC fL
2. Color: Describe the color of the
(light, medium, dark) as descriptors: /
within the outfall drainage area:
basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): ��A1G
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
G. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe A/0AleG_
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
��A
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. httl2:llportal.ncdenr.org/web/wqZws/su./npdessw#tab-4
Permit No.: N/C/k
Facility Name:
County: -/I/) /�Q ,
Inspector:
Date of Inspection:
0 or Certificate of Coverage No.:
Phone No.
Time of Inspection: 4K
PF
Total Event Precipitation (inches): .�z��
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Quulitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
..................................................................
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
pernlit.t.ed site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains . approval from the local DWQ Regional Office.
... ......................................................................................................................................................................... _................................................... ... ......................._........................................................ _
By this si nature, I certify t
(Signature of PernAtee or
this report is accurate and complete to the best of my knowledge:
e)
SWU-242, Last modified 10/25/2012
Pagel of 2
1. Outf 11 Description:
Outfall No. St
Receiving Stream: A ILAZ
(pipe, ditch, etc.) -:1'r-
2. Color: Describe the color of the disc�}ay using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: xel b lOr').i
3. Odor: Describe any di
weak chlorine odor, etc.): i
�odors that the discharge may have (i.e., smells strongly of oil,
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
`�/ 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 `._./ 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Al0 AILS
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
leAnalytical
WWW.Faceiab9.cm
July 27, 2015
Mr. Joe Hinkle
Allvac
RF• Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on July 20, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
rriost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew.brainard@pacelabs.com
pacelabs.corn
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 18
,�aeAnalytical
wwwpacelabs.com
CERTIFICATIONS
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Caroline Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712
Viroinia/VFL AP Certification #- 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 18
aceAnalytkal
www.paoelabs.com
SAMPLE ANALYTE COUNT
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersvilie, NC 28078
(704)875-9092
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92259465001
MONROE SW02
SM 5220D
MAB
1
PASI-A
92259465002
MONROE SW02
EPA 1664B
JMS
1
PASI-C
92259465003
MONROE SW02
SM 2540D
MDW
1
PASI-A
92259465004
MONROE SW02
SM 5210B
MLS
1
PASI-A
92259465005
MONROE SW02
EPA 200.7
JMW
5
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 18
,�acmnalydcal
www.pacelabs.com
ANALYTICAL RESULTS
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MONROE SW02 Lab ID: 92259465001 Collected: 07/19/15 17:45 Received: 07/20/15 13:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 48.0 mg/L 25.0 1 07/22/15 09:55
Date: 07/27/2015 09:02 AM
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, Inc.
,�www.pacelabs.comeAnalytical ® 9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: MONROE SW02
Pace Project No.: 92259465
Sample: MONROE SW02 Lab ID: 92259465002 Collected: 07/19/15 17:47 Received: 07/20/15 13:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Oil and Grease
Analytical Method: EPA 1664B
ND mg/L 5.0 1
REPORT OF LABORATORY ANALYSIS
07/24/15 10:37
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Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 18
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ANALYTICAL RESULTS
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MONROE SW02 Lab ID: 92259465003 Collected: 07/19/15 17:49 Received: 07/20/15 13:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 8.3 mg/L 2.5 1 07/22/15 16:00
Date: 07/27/2015 09:02 AM
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MONROE SW02 Lab ID: 92259465004 Collected: 07/19/15 17:51 Received: 07/20/15 13:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210E BOD, 5 day Analytical Method: SM 5210B
BOD, 5 day 8.0 mg/L 2.0 1 07/21/15 17:07 07/26/15 16:00
Date: 07/27/2015 09:02 AM
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersviile, NC 28078
(704)875-9092
Sample: MONROE SW02
Parameters
Lab ID: 92259465005
Results Units
Collected: 07/19/15 17:53
Report Limit DF
Received: 07/20/15 13:50 Matrix: Water
Prepared Analyzed CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug/L
1.0 1
07121/1519:00
07/23/1510:08
7440-43-9
Chromium
13.7
ug/L
5.0 1
07/21/1519:00
07/2311510:08
7440-47-3
Lead
ND
ug/L
5.0 1
07/21/1519:00
07123/1510:08
7439-92-1
Nickel
89.5
ug/L
5.0 1
07/21/1519:00
07/23/1510:08
7440-02-0
Zinc
138
ug/L
10.0 1
07/21/1519:00
07/23/1510:08
7440-66-6
Date: 07/27/2015 09:02 AM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: MONROE SW02
Pace Project No.: 92259465
QC Batch: GCSV/22060 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92259465002
METHOD BLANK. 1:517635
Associated Lab Samples: 92259465002
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 1517636
Parameter Units
Oil and Grease mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 07/2411510:26
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 36.6 92 78-114
MATRIX SPIKE SAMPLE: 1517637
92258814004 Spike MS MS % Rec
Parameter Units Result Conc Result % Rec t imits Qualifiers
Oil and Grease mg/L ND 40 39.3 97 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
QC Batch: MPRP/19052
Analysis Method:
EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description:
200.7 MET
Associated Lab Samples: 92259465005
METHOD BLANK: 1614673
Matrix: Water
Associated Lab Samples: 92259465005
Blank Repnrling
Parameter
Units
Result Limit
Analyzed
Qualifiers
Cadmium
ug/L
ND
1.0 07/23/15 08:22
Chromium
ug/L
NU
b.0 01/23/ Ib 08:22
Lead
ug/L
NU
b.0 01123/1b 08:22
Nickel
ug/L
ND
b.0 U//23/1b 08:22
Zinc
ug/L
ND
10.0 07/23/15 08:22
LABORATORY CONTROL SAMPLE: 1514574
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Cadmium
ug/L
500 452
90
85-115
Chromium
ug/L
500 470
94
85-115
Lead
ug/L
500 450
90
85-115
Nickel
ug/L
500 454
91
85-115
Zinc
ug/L
500 457
91
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1514576
MS
92259467003
Spike
Parameter
Units
Result
Cult(,.
Cadmium
ug/L
ND
500
Chromium
ug/L
0.023
500
mg/L
Lead
ug/L
ND
500
NI(.k(;l
ug/t
0.012
!QUO
mg/L
Zinc
ug/L
0.0033J
500
mg/L
1514577
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
452
440
90
88
70-130
3
500
493
481
94
92
70-130
2
500
445
436
89
87
70-130
2
500
461
450
90
88
14 130
7
500 456 446 91 88 70-130 2
Qual
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1514578
1514579
MS
MSD
92259470001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qua[
Cadmium
ug/L
ND
500
500
447
405
89
81
70-130
10
Chromium
ug/L
ND
500
500
454
413
90
82
70-130
10
Lead
ug/L
0.0038J
500
500
428
390
85
77
70-130
9
mg/L
Nickel
ug/L
0.041
500
500
466
425
85
77
70-130
9
mg/L
Results presented on this page are in
the units indicated by the
"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc..
Page 10 of 18
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QUALITY CONTROL DATA
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1514578 1514579
MS MSD
92259470001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Zinc ug/L 0.024 500 500 454 413 86 /8 10-130 10
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: MONROE SW02
Pace Project No.: 92259465
QC Batch: WET/39016 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92259465003
METHOD BLANK: 1515746
Associated Lab Samples: 92259465003
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 1515747
Parameter Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 1515748
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1515749
Parameter
Total Suspended Solids
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)876 9092
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 07/22/1516:00
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 262 105 90-110
92259467003 Dup
Units Result Result RPD Qualifiers
mg/L 48.2 69.8 - 37 D6
92259553001 Dup
Units Result Result RPD Qualifiers
mg/L 51.4 52.0 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: MONROE SW02
Pace Project No.: 92259465
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QC Batch: WET/38980
Analysis Method:
SM 5210B
QC Batch Method: SM 5210B
Analysis Description:
5210E BOD, 5 day
Associated Lab Samples: 92259465004
METHOD BLANK: 1514697
Matrix: Water
Associated Lab Samples: 92259465004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND
2.0 07/26/15 16:00
LABORATORY CONTROL SAMPLE: 1514698
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 181
91 84.6-115.4
SAMPLE DUPLICATE: 1514699
92259476001 Dup
Parameter
Units
Result Result
RPD Qualifiers
BUU, 5 day
mg/L
338
314 7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: MONROE SW02
Pace Project No.: 92259465
uc Batch: WETA/23796 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92259465001
METHOD BLANK: 1514120 Matrix: Water
Associated Lab Samples: 92259465001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 07/22/15 09:55
LABORATORY CONTROL SAMPLE: 1514121
Spike LCS LCS
Parameter Units Cone. Result % Rec
Chemical Oxygen Demand mg/L 750 752 100
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
% Rec
Limits Qualifiers
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1514122 1514123
MS MSD
92259092002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits KF'U Uual
Chemical Oxygen Demand mg/L 270 1500 1500 1380 1380 74 74 90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: MONROE SW02
Pace Project No.: 92259465
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a oornbined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Sorvi000 Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M 1 Matrix spike recovery exceeded QG lirnils. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 18
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
MONROE SW02
Pace Project No.:
92259465
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92259465002
MONROE SW02
EPA 1664B
GCSV/22060
92259465005
MONROE SW02
EPA200.7
MPRP/19052 EPA200.7
ICP/17120
92259465003
MONROE SW02
SM 2540D
WET/39016
92259465004
MONROE SW02
SM 5210B
WET/38980 SM 5210B
WET/38985
92259465001
MONROE SW02
SM 5220D
WETA/23796
Date: 07/27/2015 09:02 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 18
uwtunCm rvdnrrr: uocufnern rtavrseu. roray ro, LU 1V
. aceak�lytica!` Sample Condition Upon Receipt SCUR Page 1 of 2*
Document Number: Issuing Authority:
F-CHR-CS-003-rev.16 Pace Huntersville Qualitv Office
Client Name' t7 EC j 4 * Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Clien Commercial❑ Pace Other # t.
Custody Seal on Cooler/Box Present: yes ❑ no Seals intact: yes ❑ no
Packing Material: ❑ Bubble 1/Dp ❑ Bubble Bags ❑ None Other
Thermometer Used: IR Gun T1401 Type of Ice- Wet Blue None ❑ Samples on ice, cooling process has begun
Temp Correction Factor T1401 No Correction
Corrected Cooler Temp.:` �6 •C Biological Tissue is Frozen: Yes No N/A Date and inttiais of person examining
contents:_ `r' , ).
Temp should be above freezing to R°t: n,,..,...-__a_.
Chai'n'of Custod Present:
Yes ONo
ON/A
1.
Chain of Custody Filled Out
� fLI ON.
ON/A
2.
Chain of Custody Relinquished:
Yes ONo
❑NIA
3.
Sampler Name & %Qature on COC:
Yes ONo
ON/A
4.
5.
6.
Samples Arrived within Hold l ime: es ONo
ON/A
Short Hold Time Analysis (<72hr): Dyes fano N/A
Rush Turn Around Time Requested:
Dyes- o
❑NIA
7.
Sufficient Volume:
Yes ONo
❑NIA
8.
Correct Containers Used:
Yes ONo
ON/A
9.
-Pace Containers Used:
Yes ONo
❑NIA
Containers Intact:
fires 0No
❑NIA
10.
Filtered volume received for Dissolved tests
Yes ONo
ON/A
11.
Sample Labels match COC:
.-ages ONo
ON/A
12.
-Includes date/time/ID/Analysis Matrix:
k)
All containers needing preservation have been checked.
es ONo
ON/A
13.
All containers needing preservation are found to be in"
compliance with EPA recommendation,
'21ONo
i-IN/A
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
❑Yes o
mples-eheeked4er-deehlor4natio-n, --E
*e —QN
t
®a pe _sc® in VOA Vials (>6m �
. m . A_
❑Yes ONo
N/l
Trip Blank Present:
❑Yes ONO
N/A
to.
Trip Blank Custody Seals Present
OYes ONu /A
Pace Trip Blank Lot # if purchased): --
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:
SRF Review: iDate: IIf-wrg
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
Place label here
it
1111111111111111111111
9225946S
Page 17 of 18
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