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HomeMy WebLinkAboutNCS000330_Monitoring Reports_20150719STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. DOC TYPE ❑ FINAL PERMIT ❑ MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ `Z6\ YYYYM M DD FIL E I y�o wW0 �zw do� r�F wo96u F a ... 0 os� � V oz 0 O O w 0 0 on et q o � b v, O '� � �• q O O W Vq C0 4� TV 0 .r O O q bA ac �- 3 > �c� :; 1 id M P4 N 42 V c o O it O vr' a • ^+ -( PC qi'j ®y it V Qa C �O � v0 iyi = : CCrr .ryy . •�„�y h Cd N h 10, cot 4. o 0 ., 0 0 q e0 q y ' a 4 Cc 4 U a q q o .M y s� o O E� August 25, 2015 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: RECEIVED AUG 2 8 2015 CENTRAL FILES DWR SECTION TOW 3!�ATI P.O. Box 5030 2020 Ashcraft Avenue Monroe, NC 28111-5030 Phone: (704) 2894511 Fax: (704)290-5194 Email: Joe.Hinkle@atimetals.com Attct('1tN(l, ltlotis(-, Cittd stortti\�ial(�r monitoring data for Poniiit No NCS000330. The originals alld one copy are included. The monitoring data is for the following monitoring schedule: Monitonng Period Sample Number Start I End Year 6 — Period 2 12 March 1, 2015 1 August 31, 2015 Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, q{-- (' �/ Jo HGinkle EHS Manager Allvac - Monroe Plant Stonnwater Mo!u �toriay'Reuort ME -- Sample Time: ,® J15 /'/Y? T1 Allvac Storrawater Diggharge Outfall #2 Drainage Area = 272,590sq. ft. = 6.25 acres % Impervious = 36% IL Laboratory Performing Analysis: Analytical Techniques and Methods: Parameter Results (mg/1) Benchmark Values (mg/1) BOD 30 COD 120 TSS 100 Cadmium 0.001 Chromium, total recoverable 1 Lead, total recoverable AI'D 0.03 Nickel, total recoverable 8.y.-5 0.26 Zinc, total recoverable 90 0.067 Oil and Gwase (Std units) 30 PH 69 (std units) Storm Date: Storm Duration: It A3 - (firs.) Inches of Rainfall:-0-1-0 Duration of time preceding rain event exceeding 0.111: 136 (Hrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x.64) +.9 x inches rain/12inches/ft. x 6.25 x.36) 41 (Total, cfs) 1333 x (Inches of rain) + .168 8 x (Inches of rain, 6 cfs NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. httl2:/Iportal.ncdenr.org/web/wQ,/ws/su/npdessw#tab-4 Permit No.: N/, Facility Name: County: U r Inspector: j/o/ or Certificate of Coverage No.: Phone No. Date of Inspection: 16 o19-114/S Time of Inspection: %L1„' 3 '417t g Total Event Precipitation (inches) b n j/-) �S I Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) XYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). .................................................................................. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least'/2 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ................... ...................................... ............... -...... _..... _.......... ........................................................................................................._..............................................................._.-----_--_ By this signatuie, I certify that `this report is accurate and complete to the best of my knowledge: (Signature of Permitte"r D Page 1 of 2 SWU-242, Last modified 10/25/2012 1 1. Outfall Description: Outfall No. /)/) � ZJ6 Receiving Stream: t (pipe, ditch, etc.) Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Chi/V k 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 112,191) 6 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 1 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 6) 4 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? 10. Other Obvious Indicators of Storinwater Pollution: List and describe /r;�2WZ-- No Yes No Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. http://portal.ncdenr.org/web/wq./ws/su/npdessw#tab-4 Permit No.: N/C/�/Q/�/�//// or Certificate of Coverage No.: N X Facility Name: County: L Inspector: Date of Inspection: Time of Inspection: Phone No. '1z)if -IZV -ZIS, Total Event Precipitation (iuclies): � .: , ri Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). ........... -.................................................................................................................................................................................................................................................................................................................................................................................................................................. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ......................................................................................................... By this signate, I certify that t�is report is accurate and complete to the best of my knowledge: (Signature of Pe Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfalt Description: Outfall No. ,< Receiving Stream: Describe the industrial activi (pipe, ditch, etc.) that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: mle:7 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 (3� 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 0 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 V 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes nNo 10. Other Obvious Indicators of Storinwater Pollution: List and describe A10AfeE Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 LE-W w-1fa,� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit: htW://portal.ncdenr.org/web/wq/ws/su.lnl2dessw#tab-4 Permit No.: N/C/,5/6/Q/0 -0/ or Certificate of Coverage No.: Facility Name: A?% 1 / 1/l� G County: /I il Lj Inspector: Date of Inspection: Time of Inspection: _//,`0S.bnl Total Event Precipitation (inches). 3,C, Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). .............................................................................................................................................................. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ...._.. ........................................................................................................................................................................................................._ --- - By this sipature, I certify that this report is accurate and complete to the best of my knowledge: 1/7 (Signature of Peittee or D Page 1 of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. /)MOO-3f` Receiving Stream: Z Describe the industrial activi (pipe, ditch, etc. that occur within the 2. Color: Describe the color of the (light, medium, dark) as descriptors: _ L basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 40 itf- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 9 1 0 3 4 J 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 6D 2 3 4 5 C. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes oNo 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes 1 No 10. Other ObviousIndicators of Storinwaler Pollution: AW List and describe /0AII : Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit, httn://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 Permit No.: N/C/S/L/L/Q/z�/3/6/ or Certificate of Coverage No.: N Facility Name: County: Inspector: Dale of Inspection: Time of Inspection: /,W," / Pm Total Event Precipitation (inches). L3L z Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 9 Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). ...11 ............................... ..... ......... ................................ ............ ......... ... ..................................................... ...................................................... _........................... ................................................ ....................... ...... ....................... ..... .................................... , Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. i A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ................................................................................................ .......... .................. ...: By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of PerrQuee or D Pagel of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No.%' �jt/)y Structure (pipe, ditch, etc.) Receiving Stream: Describe the indust ial activities that occur.witbin the outfall drainage area: 2. Color: Describe the color of thedischarge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: /%d /— k-v cJsL 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): A10' e 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 N clear and 5 is very cloudy: 1 02 3 4 S 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 10 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 20 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No ee 10. Other Obvious Iiadicators of Sturwwater Pollution: List and describe WOMet-E Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 4 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. http://portal.ncdenr.org/web/wq/ws/su/npdessw#tab-4 Permit No.: N/C/,///,�/// or Certificate of Coverage No.: Facility Name: l .L_ %Aldr County- 1. L e Inspector: )f) 6 Date of Inspection: 1 Time of Inspection: Phone No. Total Event Precipitation (inclies): � ,3 0 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). .............................................................................._............................. ................ ................................. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the pernlilled site uulfall. The previous measurable storm event must have been at least 77, hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ............................................................................................._......................................._..................................................._........................--- By this signare, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permit* or De Pagel of 2 SWU-242, Last modified 10/25/2012 1. Outfall Description: Outfall No. / ,l J Stru Receiving Stream: — Des�ribe the industrial activities (pipe, ditch, etc.)iC fL 2. Color: Describe the color of the (light, medium, dark) as descriptors: / within the outfall drainage area: basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ��A1G 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 G. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe A/0AleG_ Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 ��A NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. httl2:llportal.ncdenr.org/web/wqZws/su./npdessw#tab-4 Permit No.: N/C/k Facility Name: County: -/I/) /�Q , Inspector: Date of Inspection: 0 or Certificate of Coverage No.: Phone No. Time of Inspection: 4K PF Total Event Precipitation (inches): .�z�� Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Quulitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). .................................................................. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the pernlit.t.ed site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains . approval from the local DWQ Regional Office. ... ......................................................................................................................................................................... _................................................... ... ......................._........................................................ _ By this si nature, I certify t (Signature of PernAtee or this report is accurate and complete to the best of my knowledge: e) SWU-242, Last modified 10/25/2012 Pagel of 2 1. Outf 11 Description: Outfall No. St Receiving Stream: A ILAZ (pipe, ditch, etc.) -:1'r- 2. Color: Describe the color of the disc�}ay using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: xel b lOr').i 3. Odor: Describe any di weak chlorine odor, etc.): i �odors that the discharge may have (i.e., smells strongly of oil, 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: `�/ 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 `._./ 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Al0 AILS Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 leAnalytical WWW.Faceiab9.cm July 27, 2015 Mr. Joe Hinkle Allvac RF• Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 20, 2015. The results relate only to the samples included in this report. Results reported herein conform to the rriost current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com pacelabs.corn Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 18 ,�aeAnalytical wwwpacelabs.com CERTIFICATIONS Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Caroline Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 Viroinia/VFL AP Certification #- 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 18 aceAnalytkal www.paoelabs.com SAMPLE ANALYTE COUNT Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersvilie, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92259465001 MONROE SW02 SM 5220D MAB 1 PASI-A 92259465002 MONROE SW02 EPA 1664B JMS 1 PASI-C 92259465003 MONROE SW02 SM 2540D MDW 1 PASI-A 92259465004 MONROE SW02 SM 5210B MLS 1 PASI-A 92259465005 MONROE SW02 EPA 200.7 JMW 5 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 18 ,�acmnalydcal www.pacelabs.com ANALYTICAL RESULTS Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MONROE SW02 Lab ID: 92259465001 Collected: 07/19/15 17:45 Received: 07/20/15 13:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 48.0 mg/L 25.0 1 07/22/15 09:55 Date: 07/27/2015 09:02 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 18 Pace Analytical Services, Inc. ,�www.pacelabs.comeAnalytical ® 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MONROE SW02 Pace Project No.: 92259465 Sample: MONROE SW02 Lab ID: 92259465002 Collected: 07/19/15 17:47 Received: 07/20/15 13:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Oil and Grease Analytical Method: EPA 1664B ND mg/L 5.0 1 REPORT OF LABORATORY ANALYSIS 07/24/15 10:37 This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 18 �acmnalytical www.pacelabs.com ANALYTICAL RESULTS Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MONROE SW02 Lab ID: 92259465003 Collected: 07/19/15 17:49 Received: 07/20/15 13:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 8.3 mg/L 2.5 1 07/22/15 16:00 Date: 07/27/2015 09:02 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc... Pogo 6 of 18 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MONROE SW02 Lab ID: 92259465004 Collected: 07/19/15 17:51 Received: 07/20/15 13:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5210E BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 8.0 mg/L 2.0 1 07/21/15 17:07 07/26/15 16:00 Date: 07/27/2015 09:02 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 18 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersviile, NC 28078 (704)875-9092 Sample: MONROE SW02 Parameters Lab ID: 92259465005 Results Units Collected: 07/19/15 17:53 Report Limit DF Received: 07/20/15 13:50 Matrix: Water Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 07121/1519:00 07/23/1510:08 7440-43-9 Chromium 13.7 ug/L 5.0 1 07/21/1519:00 07/2311510:08 7440-47-3 Lead ND ug/L 5.0 1 07/21/1519:00 07123/1510:08 7439-92-1 Nickel 89.5 ug/L 5.0 1 07/21/1519:00 07/23/1510:08 7440-02-0 Zinc 138 ug/L 10.0 1 07/21/1519:00 07/23/1510:08 7440-66-6 Date: 07/27/2015 09:02 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pago 8 of 18 �acmnalj&alo www.pacelabs.com QUALITY CONTROL DATA Project: MONROE SW02 Pace Project No.: 92259465 QC Batch: GCSV/22060 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92259465002 METHOD BLANK. 1:517635 Associated Lab Samples: 92259465002 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 1517636 Parameter Units Oil and Grease mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 07/2411510:26 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 36.6 92 78-114 MATRIX SPIKE SAMPLE: 1517637 92258814004 Spike MS MS % Rec Parameter Units Result Conc Result % Rec t imits Qualifiers Oil and Grease mg/L ND 40 39.3 97 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 18 aceAnalXical www.paoelabs.00m QUALITY CONTROL DATA Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: MPRP/19052 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92259465005 METHOD BLANK: 1614673 Matrix: Water Associated Lab Samples: 92259465005 Blank Repnrling Parameter Units Result Limit Analyzed Qualifiers Cadmium ug/L ND 1.0 07/23/15 08:22 Chromium ug/L NU b.0 01/23/ Ib 08:22 Lead ug/L NU b.0 01123/1b 08:22 Nickel ug/L ND b.0 U//23/1b 08:22 Zinc ug/L ND 10.0 07/23/15 08:22 LABORATORY CONTROL SAMPLE: 1514574 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug/L 500 452 90 85-115 Chromium ug/L 500 470 94 85-115 Lead ug/L 500 450 90 85-115 Nickel ug/L 500 454 91 85-115 Zinc ug/L 500 457 91 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1514576 MS 92259467003 Spike Parameter Units Result Cult(,. Cadmium ug/L ND 500 Chromium ug/L 0.023 500 mg/L Lead ug/L ND 500 NI(.k(;l ug/t 0.012 !QUO mg/L Zinc ug/L 0.0033J 500 mg/L 1514577 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 452 440 90 88 70-130 3 500 493 481 94 92 70-130 2 500 445 436 89 87 70-130 2 500 461 450 90 88 14 130 7 500 456 446 91 88 70-130 2 Qual MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1514578 1514579 MS MSD 92259470001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Cadmium ug/L ND 500 500 447 405 89 81 70-130 10 Chromium ug/L ND 500 500 454 413 90 82 70-130 10 Lead ug/L 0.0038J 500 500 428 390 85 77 70-130 9 mg/L Nickel ug/L 0.041 500 500 466 425 85 77 70-130 9 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 18 acmnalytical www.pacelabs.com QUALITY CONTROL DATA Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1514578 1514579 MS MSD 92259470001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Zinc ug/L 0.024 500 500 454 413 86 /8 10-130 10 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 18 ��aceAnalytica( www.pacelabs.com QUALITY CONTROL DATA Project: MONROE SW02 Pace Project No.: 92259465 QC Batch: WET/39016 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92259465003 METHOD BLANK: 1515746 Associated Lab Samples: 92259465003 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1515747 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1515748 Parameter Total Suspended Solids SAMPLE DUPLICATE: 1515749 Parameter Total Suspended Solids Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)876 9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07/22/1516:00 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 262 105 90-110 92259467003 Dup Units Result Result RPD Qualifiers mg/L 48.2 69.8 - 37 D6 92259553001 Dup Units Result Result RPD Qualifiers mg/L 51.4 52.0 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 18 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: MONROE SW02 Pace Project No.: 92259465 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: WET/38980 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92259465004 METHOD BLANK: 1514697 Matrix: Water Associated Lab Samples: 92259465004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 07/26/15 16:00 LABORATORY CONTROL SAMPLE: 1514698 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 181 91 84.6-115.4 SAMPLE DUPLICATE: 1514699 92259476001 Dup Parameter Units Result Result RPD Qualifiers BUU, 5 day mg/L 338 314 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 18 ��acieAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: MONROE SW02 Pace Project No.: 92259465 uc Batch: WETA/23796 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92259465001 METHOD BLANK: 1514120 Matrix: Water Associated Lab Samples: 92259465001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygen Demand mg/L ND 25.0 07/22/15 09:55 LABORATORY CONTROL SAMPLE: 1514121 Spike LCS LCS Parameter Units Cone. Result % Rec Chemical Oxygen Demand mg/L 750 752 100 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 % Rec Limits Qualifiers 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1514122 1514123 MS MSD 92259092002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits KF'U Uual Chemical Oxygen Demand mg/L 270 1500 1500 1380 1380 74 74 90-110 0 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 18 aceAnaljftal www.pacelabs.com QUALIFIERS Project: MONROE SW02 Pace Project No.: 92259465 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a oornbined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenyla mine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Sorvi000 Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M 1 Matrix spike recovery exceeded QG lirnils. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2015 09:02 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 18 ��acmnalyfical www.pacelabsxom QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MONROE SW02 Pace Project No.: 92259465 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92259465002 MONROE SW02 EPA 1664B GCSV/22060 92259465005 MONROE SW02 EPA200.7 MPRP/19052 EPA200.7 ICP/17120 92259465003 MONROE SW02 SM 2540D WET/39016 92259465004 MONROE SW02 SM 5210B WET/38980 SM 5210B WET/38985 92259465001 MONROE SW02 SM 5220D WETA/23796 Date: 07/27/2015 09:02 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 16 of 18 uwtunCm rvdnrrr: uocufnern rtavrseu. roray ro, LU 1V . aceak�lytica!` Sample Condition Upon Receipt SCUR Page 1 of 2* Document Number: Issuing Authority: F-CHR-CS-003-rev.16 Pace Huntersville Qualitv Office Client Name' t7 EC j 4 * Page 2 of 2 is for Internal Use Only Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Clien Commercial❑ Pace Other # t. Custody Seal on Cooler/Box Present: yes ❑ no Seals intact: yes ❑ no Packing Material: ❑ Bubble 1/Dp ❑ Bubble Bags ❑ None Other Thermometer Used: IR Gun T1401 Type of Ice- Wet Blue None ❑ Samples on ice, cooling process has begun Temp Correction Factor T1401 No Correction Corrected Cooler Temp.:` �6 •C Biological Tissue is Frozen: Yes No N/A Date and inttiais of person examining contents:_ `r' , ). Temp should be above freezing to R°t: n,,..,...-__a_. Chai'n'of Custod Present: Yes ONo ON/A 1. Chain of Custody Filled Out � fLI ON. ON/A 2. Chain of Custody Relinquished: Yes ONo ❑NIA 3. Sampler Name & %Qature on COC: Yes ONo ON/A 4. 5. 6. Samples Arrived within Hold l ime: es ONo ON/A Short Hold Time Analysis (<72hr): Dyes fano N/A Rush Turn Around Time Requested: Dyes- o ❑NIA 7. Sufficient Volume: Yes ONo ❑NIA 8. Correct Containers Used: Yes ONo ON/A 9. -Pace Containers Used: Yes ONo ❑NIA Containers Intact: fires 0No ❑NIA 10. Filtered volume received for Dissolved tests Yes ONo ON/A 11. Sample Labels match COC: .-ages ONo ON/A 12. -Includes date/time/ID/Analysis Matrix: k) All containers needing preservation have been checked. es ONo ON/A 13. All containers needing preservation are found to be in" compliance with EPA recommendation, '21ONo i-IN/A exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) ❑Yes o mples-eheeked4er-deehlor4natio-n, --E *e —QN t ®a pe _sc® in VOA Vials (>6m � . m . A_ ❑Yes ONo N/l Trip Blank Present: ❑Yes ONO N/A to. Trip Blank Custody Seals Present OYes ONu /A Pace Trip Blank Lot # if purchased): -- Client Notification/ Resolution: Field Data Required? Y / N Person Contacted: Date/Time: Comments/ Resolution: SCURF Review: SRF Review: iDate: IIf-wrg Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold, incorrect preservative, out of temp, incorrect containers) Place label here it 1111111111111111111111 9225946S Page 17 of 18 'b � � g o 2. O o ® \ Z Y m m v, z D Z 3 4 z m z d m A 0 V) V) N 0 v v D im z A m T D Temp in °C r p NReceived on Ice (YIN) VCustody cn Sealed Cooler K (YIN) w 0 0 Samples Intact (YIN) r; C z c m m O m A 3 m 0 O z 0 0 z 0 ITEM # �® 3 a; N oc D 3 IV c N{ r mIYI s ; c Z fJ m °00. o m � a N �N''0'D�r�� MATRIX GODC {see vend a des to isn} SAMPLE TYPE (G=GRAB C=COMP) 0 m n m ° D V AO -f N m 0 r r 0 Dml p C) �N m 1 m m SAMPLE TEMP AT COLLECTION # OF CONTAINERS HNO3 HCl NaOH t Na2SZ03 y Methanol Other Analysis Test YI Residual Chlorine n ®� 0 a0 1 m e� .n N m 0 0 m n K n N _ C 1D m g A , 60 o h' 0 m z D SU � � n w N r{ \ a r m (D fit 01 f3 I1G) M•nD rn Z <J I aIt GO 60 D m m 1z 18 of 18