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NCS000115_HISTORICAL WITH APPLICATION_20181204
STORIVIINATER-DIVISION"CODINGSHEET " PERMIT N0. DOC TYPE 0 FINAL PERMIT ❑ MONITORING INFO 5J,/ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ _ a 0 (g I �(JH YYYYMMDD Date: November 19, 2018 Novozymes, NA Inc. 77 Perry's Chapel Church Rd. Franklinton, N.C. 27525 NCDEQ Division Of Water Quality 1617 Mail Service Center Raleigh, N.C. 27699-1617 Attn: Division Of Water Quality Storm Water Sampling, NPDES Permit No. NCS0001 15 Dear Sir/Madam, novozymev Rethink Tomorrow RECEIVED DEC 0 4 2018 DENR-LAND QUALITY STORMWATER PERMITTING During review of storm water sampling results, it was observed that there was an exceeded benchmark in Biological Oxygen Demand (BOD) from our Outfall 2 location, as well as an exceeded benchmark in pH, (9.5) from Outfall I location. Upon immediate investigation, per Tier One requirements, it was discovered that although during sample event no signs of potential issues were present, the area approximately 20 yards from where samples are collected the combination of filtration systems not properly being maintained/serviced and the off-loading of raw materials are being considered direct causes of the recent exceeding of BOD. Plans are in place to have personnel in area begin with cleaning filtration systems and more caution taken place while material is being handled. Within our Outfall I location upon investigation of exceeded pH benchmark, it was discovered there had been some residual hydrated lime that was left from spillage during off-loading process near a storm drain in production area. The area has been cleaned and no signs remain of hydrated lime that could result in elevated pH readings. Continued monitoring by Environmental Services Department will take place in order to prevent future exceeded benchmarks in Biological Oxygen Demand (BOD) from Outfali 2, and pH from Outfall 1. Kind Regar s, le-w Joe La Environmental Compliance Coordinator Environmental Services STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS NCS000115 FACILITY NAME Novozymes, NA Inc. PERSON COLLECTING SAMPLE(S) Joe Ladd CERTIFIED LABORATORY(S) Enco Labs Lab # Lab # Part A: Specific Monitoring Requirements SAMPLES COLLECTED DURING CALENDAR YEAR: 9i t (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) COUNTY Franklin PHONE NO. 9( 19 ) 494-3000 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. _ £ a _:.' 00 1 • 1 ' 1 Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Oyes e)no (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall -- `Date' r5U054� ' 00556' °���` : `00530� 004U0 ° � ,+ oz�+ 5ampleP f '•c�°k TotallFlow ,Total _ OilBi Grease Nonpolar -To[�al� �` pH�°sr,,;New117otor � ' �' r. Y� Collected .4 - :'�t'�'�' g'. r(dapphcable} ;�" � Rainfall " a�'r w(if appl�s ¢ ; _ 108iGlI PHA '' ti r y (Method,lW4 g is 'Suspended.wb ... i �� ' ' tc �s�; Oil Usage r tom. fUEM),xif 42 moldd/ r'MG ED FROM MlirniiW, �61/mo;A,.„;�..,�,� Form SWU-247, last revised 611212015 Pagel of 2 STORM EVENT CHARACTERISTICS: Date 10/26/18 Total Event Precipitation (inches): 1.25 Event Duration (hours): (only if applicable - see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable - see permit.) Mail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines a34 imprisonment for knowing violations." ( 4 1l/-14-�a�P (Signature of Permittee) (Date) Form SWU-247, last revised 611212015 Page 2 of 2 STORMWATER DISCHARGE OUTFALL (SDO) MONITORING REPORT Permit Number NCS NCS000115 SAMPLES COLLECTED DURING CALENDAR YEAR: :2-o q (This monitoring report shall be received by the Division no later than 30 days from the date the facility receives the sampling results from the laboratory.) FACILITY NAME Novozymes, NA Inc. PERSON COLLECTING SAMPLE(S) Joe Ladd CERTIFIED LABORATORY(S) Enco Labs Lab # Lab # Part A: Specific Monitoring Requirements COUNTY Franklin PHONE NO. 9( 19 ) 494-3000 SIGNATURE OF PERMITTEE OR DESIGNEE REQUIRED ON PAGE 2. • Date Sample Collected I i 1 1 i Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Dyes ono (if yes, complete Part B) Part B: Vehicle Maintenance Activity Monitoring Requirements Outfall No. Date Sample Collected 50050 00556 00530 00400 Total Flow (if applicable) Total Rainfall Oil & Grease (if appl.) Non -polar O&G/TPH (Method 1664 SGT-HEM), if appl. Total Suspended Solids pH New Motor Oil Usage mold r MG inches m WRA unit aUmo Form SWU-247, last revised 611212015 Page I of 2 STORM EVENT CHARACTERISTICS: Date 10/26/18 Total Event Precipitation (inches): 1.25 Event Duration (hours): (only if applicable — see permit.) (if more than one storm event was sampled) Date Total Event Precipitation (inches): Event Duration (hours): (only if applicable — see permit.) Mail Original and one copy to: Division of Energy Mineral and Land Resources Attn: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. i am aware that there are significant penalties for submitting false information, including the possibility of fines and imp*onment for knowing violations." (Signature of Permittee) (Date) Form SWU-247, last revised 611212015 Page 2 of 2 -ENCO Accurate. Timely. Responsive. Innovative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Tuesday, November 6, 2018 Novozymes North America (N0008) Attn: Joe Ladd 77 Perry Chapel Church Road Franldinton, NC 27525 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Stormwater Testing ENCO Workorder(s): C616575 Dear Joe Ladd, S Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, October 26, 2018. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page : of 8 0 www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: Outfell i lab ID: CB16575-01 Sampled: 10/26/18 12:30 Received: 10/26/18 16:25 Parameter Preparation Hold Date/Tlme(sl Preo DatelTlme(sl AnalvsisDate/Time(sl SM 254OD-2011 NO PREP 11/02/18 10/30/16 10:02 10/30/18 10:02 SM 5210 &2011 NO PREP 10/28/18 12:30 10/26/18 16:54 10/26/18 16:54 SM 5220D-2011 Same 11/23/18 10/29/18 12:58 10/29/18 15:35 �ClientI0: Outfall2 LabI0: C616575-02 Sampled: 10/26/18 12:50 Received: 10/26/18 16:25 Parameter Preparation SM 254OD-2011 NO PREP Hold Date/Tlme(s) 11/02/18 Preo Datel7lme(a) 10/30/18 10:02 Analvsls Datel7lme(sl 10/30/18 10:02 SM 5210 8-2011 NO PREP 10/28/18 12:50 10/26/18 15:54 10/26/18 16:54 SM 5220D-2011 Same 11/23/18 10/29/18 12:58 10/29/18 15:35 FINAL This report relates only to the sample as received by the dboratory, and may only be reproduced In full. Page 2 of B www.encolabs.com SAMPLE DETECTION SUMMARY 511ea1t ID: Outfall 1 Lab ID: CB16575-01 Analytm Results flat Va E" Units Metggg Ndu Biochemical Oxygen Demand 10 2.0 2.0 mg/L SM 5210 B-2011 Chemical Oxygen Demand 34 10 10 mg/L SM 5220D-2011 Total Suspended Solids 12 5.0 5.0 mg/L SM 254OD-2011 Cllent ID: Outfall 2 Lab ID: C016575-02 Aaal Result s Elan , Hu E" llnlbli Mgtlls9 �49tC.i Biochemical Oxygen Demand 47 2.0 2.0 mg/L SM 5210 B-2011 Chemical Oxygen Demand 83 10 10 mg/L SM 5220D-2011 Total Suspended Solids 32 6.2 6.2 mg/L SM 2540D-2011 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Page 3 of 8 www.enoolabs.com ANALYTICAL RESULTS Description: Outfall 1 Lab Sample ID: CB16575-01 Received., 10/26/18 16:25 Matrix: Surface Water Sampled:10/26118 12:30 Work Order: CB16575 Project: Stormwater Testing Sampled By:Joe Ladd Chemistry Parameters Analtrte rCAS Numbed Resin B1112 MI]JU PE KU pM Batch Method ABalyged fy Notes Biochemical Oxygen Demand^ 10 mg/L 1 2.0 2.0 8326036 $M 5210 B-2011 10/26/18 16:54 JOC Chemical Oxygen Demand^ 34 mg/L 1 10 10 8129023 SM 5220D-2011 10/29/18 15:35 JOC Total Suspended Sollds^ 12 mg/L 2 5.0 5.0 8130003 $M Z540D-2011 10/30/18 10:02 OMR Description: Outfall 2 Lab Sample ID:CB16575-02 Received: 10/26/18 16:25 Matrix: Surface Water Sampled, 10/26/18 12:50 Work Order: C316575 Project. Stormwater Testing Sampled By:Joe Ladd Chemistry Parameters 13esul On Mnh RE MPS P9L A@Uh Method And Al Notes Biochemical Oxygen Demand- 47 mg/L 1 2.0 2.0 8326036 SM 5210 B-2011 10/26/18 16:54 ]0C Chemical Oxygen Demand^ 83 mg/L 1 10 10 8329023 5M 5220D-2011 10/29/18 15:35 JOC Total Suspended Sollds^ 32 mg/L 2.5 6.2 6.2 8130003 SM 254OD-2011 10/30/18 10:02 OMR FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 of 0 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch W26O36 - NO PREP Blank (8326036-BLK1) Prepared & Analyzed: 10/26/2018 16:54 Spike Source %REC RPD Ana11tt0 Result E1114 FM Unite Level Result %REC Llmlts RPD Lhnit Notes Biochemical Oxygen Demand 2.0 U 2.0 mg/L LCS (8326036-BSI) Prepared & Analyzed: 10/26/2018 16:54 Spike Source %REC RPD Anal a Result Elan FIX UJplts Level Result %REC Limits RPD Llmlt Notes Biochemical Oxygen Demand 180 2.0 mg/L 198 89 85-115 Duplicate (8326036-DUPI) Prepared & Analyzed: 10126/2018 16:54 Source: CB16575-01 Spike Source %REC RPD Anal lda9 Result E1aa e12L 11B1ts Level Resin %REC ljmft RPD Limit Notes Biochemical Oxygen Demand 10 2.0 mg/L 10 3 30 Batch 9729023 - Some Blank (8329023-BLKl) Prepared: 10/29/2018 12:58 Analyzed: 10/29/2018 15:35 Spike Source %REC RPD Anal Yle Result tied em Unite Level Resulj %REC Limps RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (8329023-BSI) Prepared: 10/29/2018 12:58 Analyzed: 10/29/2018 15:35 Spike Source %REC RPD Anal Result Elan M Unfu Level soul! %REC Limns RPD Nmlt Notes Chemical Oxygen Demand 500 10 mg/L 500 99 90-110 Matrix Spike (8329023-MSI) Prepared: 10/29/2018 12:58 Analyzed: 30/29/2018 15:35 Source: CB11866.M Spike Source %REC RPD AnahU Result Flag FM Units Level Resu11; %REC Ljmb RPD LIm11 Notes Chemical Oxygen Demand 530 10 mg/L 526 23 96 90-110 Matrix Spike Dup (8329023-MSD1) Prepared: 10/29/2018 12:58 Analyzed: 10/29/2018 15:35 Source: CBI1866-01 Spike Source %REC RPD Anal vle Result E1a11 M UAlta Level Besult %REC Limits RPD 1llBlt Notes Chemical Oxygen Demand 540 10 mg/L 526 23 98 90-110 2 10 Batch 8.730003 - NO PREP Blank (8330003-BLK1) Prepared & Analyzed: 10/30/2018 10:02 Spike Source %REC RPD Anal Result Elan et2L Units Level Resul$ %REC Limns RPD Limit Notes Total Suspended Solids 2.5 U 2.5 mg/L. LCS (8330003-BS1) Prepared & Analyzed: 10/30/2018 10:02 Spike Source %REC RPD AnaiStte Result flag Ml. UnAs Level Result %REC LIMM RPD Will Notes Total Suspended Solids 92 2.5 mg/L 100 92 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In fut Page 5 of 8 (9 �ea www.encolahs-tom QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Sa[rh &730003 - NO PREP - Continued Duplicate (8130003-DUPi) Prepared & Analyzed: 10/30/2018 10:02 Source: CB15181-01 Spike Source %REC RPD AnaL5t3R Reswt Flea POL Units Level Result %REC Limits RPD Unit Notes Total Suspended Solids 2700 500 mg/L 2200 19 20 Duplicate (8730003-DUP2) Prepared & Analyzed: 10/30/2018 10:02 Source: CB16046-01 Spike Source %REC RPD _Anallde RC3111t Flea PM Rift& Level Result %REC Limits RPD Limit Notes Total Suspended Solids 220 50 mg/L 230 4 20 FINAL This repot relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 6 of 0 CS NS www.enoolabs.com FLAGS/NOTES AND DEFINITIONS 9 The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. RNAL This report relates only to the sample as received by the iaboratory, and may only be reproduced in full. Page 7 of 8 J= L INI C� f•,D775 CentraF POf1 4810 EmQlfin Park COUTI, SLAG 111 102-A WoodvAnds In kz;lr7 l CL Qrterrdo. FL 32824 Jacksormft. FL 3MS-6069 Cary, NC 27511 9 j (407) 826-5314 Fax(407}�6945 (904)296-3007 Faxi9p4►296-6210 (918i467-3090 FRI(919)467a515 Page I of 1 • Sample Ka Prepared Elybatdf'cere Rer>ngwsnsd 8y DataYene -1e1fr A O�7�< — -- . . . . - YM—j4?4--- Camn--fS{p�eaal Rejjp"V Ragrirr}jp'`l-Ift L./[it jJ �a 1 # + J 9- S Reistgrdstled By DOIAW rrre By Dauvrime Received By trale/fene Cocw rs 6 Temps on Raceo D jCwKMicn Ltporr Remo Ildrlx : GW Gmwd-Ww SO—W Dw-Drirdmg water SE-Sednwd SW Swtmw water war-vYastaeraw A -Am comer (dew in co -wft) Prearrath= VIOD n+ICI N+WM 542SO4 NarlaoH o-Mw (eeta3 m canm &Vsj Note: AN samples a MmMed to ENCD tabu are m accwderroe with Ore terms and cwKftonc fisted on the muww o1 dis lam. earkss Prior vnihen aDvements east Energy, Mineral and Land Resources ENVIRONMENTAL OVALITY February 21, 2018 Mr. Randy Green Novozymes North America 77 Perry Chapel Church Road Franklinton, NC 27525 ROY COOPER Governor MICHAEL S. REGAN Secretary WILLIAM E. (TOBY) VINSON, JR. Interim Director Subject: Draft NPDES Stormwater Permit Permit No. NCS000115 Novozymes North America Franklin County Dear Mr. Green: Enclosed with this letter is a copy of the draft stormwater permit for your facility. Please review the draft carefully to ensure thorough understanding of the conditions and requirements it contains. The draft permit contains the following significant changes from the facility's current permit: I. You are required to collect analytical and qualitative monitoring samples during "measurable storm events" as defined in Part II, Section B. This term is different from the "representative storm event" in earlier permits. 2. Requirements for the Stormwater Pollution Plan (SPPP) have been updated in Part II, Section A. I Monitoring requirements in the draft permit have changed slightly. Monitoring is required for BOD, COD, TSS and pH. After review of monitoring data from the past 10 years the results for TKN, NO2/NO3 and TP have remained well below benchmark levels. The draft permit proposes to remove these parameters. Comments from our regional staff or other information may result in maintaining these if it is apparent that your activities in some way have the potential to release these pollutants. Stormwater benchmarks remain in the permit as before. Keep in mind that benchmarks are not permit limits, but rather guidelines for implementing the Stormwater Pollution Prevention Plan (SPPP). A benchmark exceedance is not a permit violation; however, the permittee must respond to exceedances. The draft permit has modified the tiered response process for State of Nash Carolina I Environmental Quality I Energy, Mineral and Land Resources 1612 Mail Service Center 1 512 North Salisbury Street I Raleigh, NC 27699-1612 919 707 9200 T NCS000115 Draft Permit Page 2 benchmark exceedances consistent with other permits in our program. Please become familiar with the tiered process as proper response under the tiers -may be enforceable items under your permit. Response to the tiered process may include review of onsite conditions, installation of BMPs or requirements for more frequent monitoring. 4. Vehicle maintenance (Tables 4 & 5) monitoring parameters have been revised. Non -Polar Oil & Grease [EPA Method 1664 (SGT-HEM)] replaces Oil & Grease/TPH. The benchmark for Non -polar Oil & Grease using this method is 15 mg/L. This requirement appears in all individual stormwater permits; however, it only applies to facilities that perform onsite vehicle maintenance activities. If the facility begins vehicle maintenance during the permit _cycle, the requirements shall apply. Also, pH monitoring is no longer required for discharges only associated with vehicle maintenance activities. 5. Language has been added under Part II Section D to address potential responses to qualitative monitoring issues. 6. A new section on Special Conditions has been added in Part II, Section E to comply with federal regulations requiring electronic submittal of discharge monitoring reports. Our electronic submittal process is not available for use at this time, but we will continue to provide feedback on when this process will be available. 7. Civil and administrative penalty amounts have been updated to reflect current federal law in Part 111, Section A, 2(b) and (g). Please review the draft permit and submit any comments to me no later than 30 days following your receipt of the draft. Comments may be emailed to me at bradley.bennett2ncdenr.gov or mailed to my attention at NC DEMLR, Stormwater Permitting Program, 1612 Mail Service Center, Raleigh, NC 27699-1612. If you have any questions, please email me or call me at (919) 807-6392. Sincerely, Bradley Bennett Stormwater Permitting Program Attachment: Draft Permit NCS000115 cc: Bill Denton, DEMLR Raleigh Regional Office — via email Stormwater Permitting Program Files hb1.1F 1 M' North.Carolina,Department of Natural and Cultural Resources Natural Heritage Program ;Gawernor Roy. Cooper SecretarySusi H- Hamilton March 26, 2018 Bradley Bennett NCDEQ 512 N. Salisbury Street Raleigh, NC 27604 RE: Novozymes North America; NCS000115 Dear Bradley Bennett: NCN H DE-5667 The North Carolina Natural Heritage Program (NCNHP) appreciates the opportunity to provide information about natural heritage resources for the project referenced above. A query of the NCNHP database, based on the project area mapped with your request, indicates that there are no records for rare species, important natural communities, natural areas, or conservation/managed areas within the proposed project boundary. Please note that although there may be no documentation of natural heritage elements within the project boundary, it does not imply or confirm their absence; the area may not have been surveyed. The results of this query should not be substituted for field surveys where suitable habitat exists. In the event that rare species are found within the project area, please contact the NCNHP so that we may update our records. The attached `Potential Occurrences' table summarizes rare species and natural communities that have been documented within a one -mile radius of the property boundary. The proximity of these records suggests that these natural heritage elements may potentially be present in the project area if suitable habitat exists and is included for reference. Tables of natural areas and conservation/managed area within a one -mile radius of the project area, if any, are also included in this report. Please note that natural heritage element data are maintained for the purposes of conservation planning, project review, and scientific research, and are not intended for use as the primary criteria for regulatory decisions. Information provided by the NCNHP database may not be published without prior written notification to the NCNHP, and the NCNHP must be credited as an information source in these publications. Maps of NCNHP data may not be redistributed without permission. The NC Natural Heritage Program may follow this letter with additional correspondence if a Dedicated Nature Preserve (DNP), Registered Heritage Area (RHA), Clean Water Management Trust Fund (CWMTF) easement, or Federally -listed species are documented near the project area. If you have questions regarding the information provided in this letter or need additional assistance, please contact Rodney A. Butler at rod ney.butler ncdcr.aov or 919.707.8603. Sincerely, NC Natural Heritage Program MAILING ADDRESS. Telephone. (919) 707-6107 LOCATION: i651 ml Service Center vvi .ncnhp.org ' 121,West Jones Street U. fgh, NC 27699=1651 Roeigh, NC276Q3 Natural Heritage Element Occurrences, Natural Areas, and Managed Areas Within a One -mile Radius of the Project Area Novozymes North America Project No. NCS000115 March 26, 2018 NCNHDE-5667 Element Occurrences Documented Within a One -mile Radius of the Proiect Area Animal 32239 Waterbird Colony --- 2010-04-19 C 5-Very -- — GNR S3 Assemblage Low Dragonfly or 33749 Somatochlora georgiana Coppery Emerald 2004-Pre H? 5-Very -- Significantly G3G4 S2? Damselfly Low Rare No Natural Areas are Documented Within a One -mile Radius of the Project Area Managed Areas Documented Within a One -mile Radius of the Project Area Tar River Land Conservancy Easement _ Tar River Land Conservancy Private Definitions and an explanation of status designations and codes can be found at httr)s:llncnhde.natureserve.orglcontent/hetn. Data query generated on March 26, 2018; source: NCNHP, 01 January 2018. Please resubmit your information request if more than one year elapses before project initiation as new information is continually added to the NCNHP database. Page 2 of 3 V NCNHDE-5667: Novozymes North America 4 `ems gw rim fi 17 Ar- w � c 5W — - w a 4D4 4 i n �L�1�1MA �' March 21, 2016 Rom (,��,�) Nei-9300 AN (m) 8sf-9400 rococo, MAWOi6uaWu•O m RECE1VEDINCDEQ/[A' R NC Division of Water Resources MAR 2 9 2016 Surface Water Protection Section Water Quality 1617 Mail Service Center Permitting Section Raleigh, NC 27699-1617 RE: Navaxvmes North America Inc. We are the authorized representatives of the referenced company concerning property tax matters In North Carolina. In this capacity, we enclose In duplicate an Application for Tax Certification and Exemption Form TC=WQ. The Application includes a listing of the relevant assets and a sketch of the buildings and equipment. If additional information Is needed, please contact Rich Olofson at 919-494-3235. Thank you In advance for your prompt attention to this matter. Senior Consultant. i ou��Y M TCN: This application is to be used only for waste treatment systems and equipment Rev. 02/20/2014 under the authority of the NC Division of Water Resources (DWR) DIRECTIONS. Complete and and signed copies of the application form and all supporting information to both: 1) the Courrty Tax Admininratgr for the County in which the facility is located (one copy) AND 2) j to the NC Division of Water Resources. Surface Water Protection Section. 1617 Marl Service Center. Raleigh. f4C 27699-1617 (two copies). Type or print in blue or black ink A separate applkabon package II is required for each fn ty where property proposed for tax certificadon is located. THIS APPLICATION WILL NOT BE PROC I=SSED WIT11OUT COMPLETE AND ACCURATE INFORMATION. If you have any questions regarding this application. please call the local tax office or the NC Division of Water Resources at 919=7-MOO or their web sme at hltn:l/Mrta:.nodenr_oral+,Aeblwkrls%alas/nodesRax-certification for more specific contact information. Please Note: ai Tax Certifications wile only be processed for facilities under the authority of the DWR and only if the DWR has found that the described propertT.. 1. Has been or will be oonstr cted or installed; 2- Complies with or Mai plans therefore which have been submitted to the DWR indicate that it will comply with the requirements of the Environmerrtal Management Commission: I i 3. Is being effectively operated or will. when oornpleted. be required to operate in accordance with the flews and conditions of the permit certificate of approval, or other document of approval issued by the DWft and 4. Has or_ when completed, will have as its PRIMARY rather Than incidental purpose the reduction of water pollution: • 5. Is being used exclusively (100%) for waste treatment b) if approved, the Tax Certification issued wrll incorporate all requested assets at the f olity that meet the afteria for Tax Geri fication by DWR. Therefore this application must include any new assets for which Tax Cer'tiffamon is , as well as any ash previvA receiving Tax Certification from DWR for whldh Tax CtsChgtion is still needed. __a 42 icard (Apprcam is the owner oft and taxpayer for, the property described in this appfication for tax oertification. - Name of Applicant Name of Faffrty: = Novozymes North America inc. Franklinton Address of Applicant, if different from faciity where property located: - I Physical Address of Facility where property located (no P.O. Box):- - - P 0 Box 576, Franklinton, NC 27525 1 77 Pem-s Chapel Church Road. Franldinton, X-C 27525 (address) (*l (ZIP) (streetaddress) (dy) (hp) Business Relationship of Applicant to facility where property located: Treasurer located: Franklin Name of Contact Person at FaaTty where property lord: Rich Olofson Does the Applicant hold any NC Division of Wafer Resources Permits? X Yes 1 Ej No I Tide: Director of Corporate Finance Americas Phone Number. 91.9 494 3235 (f yes. please list NCG5001115. NCS000115- WQ0002806. WQ0003487 Perm Na(s): If approved, wiil this be the first Tax Ce licartlon issued for this Facility? if no, attach any previously issued tax X Yes_! _No _ - _ certifications — B. Complete this Section only 1f the 0 eratorNser of the fakir and equipment is different from the Owner of the fa. rl' Ij� 1}1N[;pE( R Name of _ - - - _. Operator/User. OperatotMser Address: _ Water Quality _ (address) (d171 Permitting Section (mi) Operator/User Contact Name: Relationship between OperatodUser of faafity and equipment and µ r CESI, tiL•4r�..ITIA i•v 70 YOUR APPL. f�. N i ^s numberof h ite t.. � 1' rL• { fi . — � V i�T: zew !T7 :?r yr;Ir�s, ��X e.E. _!f..ati0n 15 �ei:1G 'R^. y.ESi E+� fr!s•C`• !'EP CI':f�7R:: r+.n `I;a tt"fa'n a,sr ^` Application Continues on Next Page -> DIVISION OF WATER RESOURCES TAX CERTIFICATION & EXEMPTION APPLICATION PAGE 2 Waste Treatment System &Equipment: waste t vwnem systems if equipment nuM be used e•YUu$iv* tar the abatement of water pollution ar.. ataaoas omC t�T, CMl1+rl 'Vw aSSM MAdd n v c+feK er EWycwc I e+e peme. {temtwi t n Afaet �►�rw � of tw "- 'w' toots:as ^�� cod �Paknon firV I,--.d ; « �_." aaw r i ary car fsh!np �I 1I rN.d.reOYrNo.aae.x>ro�wso. s�iMreAwliPrn9ro� �n.dr� mrA'•Lm`_ „I •T�masy:i �tIa 'xaw l31 e UMU-k ow ny.eor..e.�ar.r:m � �I : ]elm r. +ara�rs urns .. l I I AwrYAil..11l•Ir��^%rhrFl11MrQ1 � Sf Ia''''� -ICS n110! IF I m11G9'S Ci7s W I FOR Y�7gI��M1RSMPITwfSVltW 1 xM I �'IIeTa 1 I 7mrIMwY �I►'[a1TC I -- Y 1 1mw ws�r SP— I i � nswlo+�.�o.re..l,.a.e rc�. � m+c:.a i►�I ary Aeci aeftnq rapm a 1rcl-" �tp4sr • warrrarte.claw�r.I lb., Lrrerr�.+eear t. ar>.r.neeEerwotPrat tern.errr�prcwrryBredreeOtYOpemL�r�peertarsaaacnerotrasa.e.em..ar.erseraerMli7i�rrti�auese+e.a .."b"se IN tyre. rrapgesni.*Mist"c irpae rain orv,..plpslc: rs. retrara+tl� Facill i;e s: To qua* for tax ce wcabm the astir m or section of buafing being applied for. muss be used e=kalrely for water poll uion WvveMlon. A sketch of the fig, square footage all" with detarts as to how the buNltrg Is used for water palAfiort pra,aer 900. Is regtdred. Land: To qualify for raxae VUrian. the land must be used wwkzivdy far water polls M pr mtiom Av&a raft diagram OfMe facffidY detailing V*'land bek4 gPPffi�d foi is `e4utt6tl_' The`ar'roumt of land (acreage) is requwed and hew land is oeirg used to pu'everd water poMftm For v iertreatrnent and hip6m system Est separately ttu acreage used fnr acbm! t eatment from the aceage required by the WWs water quaft permit for btftfers and setbacks. SIGNATURE: I hereby exrtity that the above egwwmi t, b,t fates and/or tarwxare steed for the purpose stated. and that ttx irafomtallon presented ;n this appg,atlon is a=xate. Fu termore. I certify Brat any portable or mobile equrgrment� on ap `` && used etoclusively in true stele of North CarJTma- Signature:r' : i! �/tte. 'c -. Daw fa>R:a4o• -� ROT1Ce The pera tg turret s MammL repras4ufim or cerdficadan - oi: _ .. - hrratn includes imprlsoamem andi or the ammmmRnt of civil urea Mea. tt5efaannpperaala F-W r.w .J m 0 • .j Novozymes North America Inc Franklinton, NC Main number Cost center, Cap. date Name Acq.value 5206 60895-02 10/31/2015 Anaerobic Digester 1C Reactor FEN98CT02 3,719,015 5207 60895-02 10/31/2015 Anaerobic Digester Sulfur Treatment System FEN84A 1,477,412 5209 60895-02 10/31/2015 Anaerobic Digester Recirculation Tank FEN98CT01 261,558 5210 60895-02 10/31/2015 Anaerobic Digester Flare FEN84CS01 155,298 5211 60895-02 10/31/2015 Anaerobic Digester Pre Acidification Tank FEN98ATO 1,104,479 5212 60895-02 10/31//2015 Anaerobic Digester Raw Material System FEN10 104,214 5214 60895-02 10/31/2015 Process Waste Water Clarifier Basin Agitator FC098 95,030 5215 60895-02 10/31/2015 Process Waste Water Pump FC098AP09- 82,753 5216 60895-02 10/31/2015 Process Waste Water Pump FC098AP10 82,753 5217 60895-02 10/31/2015 Process Waste Water Pump FEM98AP04 61,315 5218 60895-02 10/31/2015 Process Waste Water Pump FEM98APOS 61,315 5219 60895-02 10/31/2015 Process Waste Water Primary Clarifier Skimmer FEL9 52,107 .500262 60895-02 12/31/1994 UTILITY BUILDING 241,000 500530 60895-02 10/31/2015 Building FEN 559,901 Grand Total 8,058,149 I'M • • m....Ne.,e. „� .. vat�•--4r.._.._...._.._..�.._.._.._.._.._.._.._.. I� as iee � ; I Comm two � ata aao 10Q —•-.._..�. .._..�._� 1 i j FEN BUILDING 500530 16 { FEN84CS01 ®es� F�Ls I � 1 j i- 10 .Q wwv am � aaa.wrs 5219 I I FEN8413 FEI76P aw j FEN84A a 00t FEM98AP04 (5217) [ fro c 5207 w FEM$8AP05 (5218) rx, r lac j .was UTILffY BUILDING T r 5=62 I ffrwt.w rarw aaw� p� FEN98A 5211 l , FEN98C FEN98C $209 5206 FEN98B r m O l r F � •- ,---- � ----------• , II k a.a I , New zo�is 1= .r, aaa � �TM=_. � � � PFMLEMIMMY aoasatucrweeo,gq�arnwr 9 DevberW I _ L� _ j FCO98AP09 (5215) _ --- FCO98AP10 (5216) --� ac awou FEN98B r.� 5214 `�J w Weaver, Charles From: Weaver, Charles Sent: Wednesday, October 21, 2015 11:48 AM To: 'rwgr@novozymes.com' Cc: 'dasy@novozymes.com'; 'salt@novozymes.com' Subject: renewal of NCG500115 / Novozymes North America Attachments: NCG50 Final 093015.pdf, Technical Bulletin - NCG500000 2015.doc Importance: High Attached you will find the updated version of NPDES General Permit NCG500000, effective 10/1/2015. Discard any previous versions of the General Permit and use this version until further notice. You do not need a reprinted Certificate of Coverage, as the one issued to you in 2012 is still applicable. Thank you for your patience during the longer -than -expected renewal period. If you have any questions about this matter, simply reply to this message. Charles H. Weaver NPDES Unit 1 Weaver, Charles From: RWGR (Randy Green) <RWGR@novozymes.com> To: Weaver, Charles Sent: Wednesday, October 21, 2015 1:25 PM Subject: Read: renewal of NCG500115 / Novozymes North America Your message To: Subject: renewal of NCG500115 / Novozymes North America Sent: Wednesday, October 21, 2015 5:26:22 PM (UTC) Monrovia, Reykjavik was read on Wednesday, October 21, 2015 5:25:13 PM (UTC) Monrovia, Reykjavik. 0' 0 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NO. NCG500000 TO DISCHARGE NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER BLOWDOWN, CONDENSATE, EXEMPT STORMWATER, COOLING WATERS ASSOCIATED WITH HYDROELECTRIC OPERATIONS, AND SIMILIAR WASTEWATERS UNDER THE ' NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, this permit is hereby issued to all owners or operators, hereafter permittees, which are covered by this permit as evidenced by receipt of a Certificate of Coverage from the Environmental Management Commission to allow the discharge of wastewater in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts 1, H, UI and IN hereof. This permit shall become effective October 1, 2015. This permit shall expire at midnight on July 31, 2020. h0Ct) ()rfen Tyc ;��}a�, _w Lj C�1+r+,,p1•L�nu �V�IkA�I� �h�P 4V" S. Tay Zimmerman Dirce 0 By Authority of the Envi `a at Y., c(c kfi �S��it Scc+ t,*Qc General Permit NCG500000 PART I A (1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FOR NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER BLOWDOWN, AIR COMPRESSOR CONDENSATE AND SIMILAR WASTEWATERS During the period beginning on August 1, 2015 and lasting until expiration, the permittee is authorized to discharge non -contact cooling water, cooling tower and boiler blowdown, air compressor condensate and similar wastewaters from outfalis numbered serially beginning with 001 (specific outfall numbers shall be assigned by the permittee), Such discharges shall be li nited and monitored by the perinittee as specified below: PARAMETER " ` z `' LIMITS 's : . „ , ,;. MONITORING„RE UIRIJIVIENT$:.:> ; s u �� k k a , Monthly `Dail 4 Measuremen �.{FF SamSaple'Location 1 AS of me_:, i, A.vera `"e Maxiiireum., t Fre T ueuc Flow Semi-annuallyEstimate Effluent Effluent, Upstream, Temperature Semi-annually Grab Downstream Total Residual Chlorine' FW 17.0 ug/L Effluent Semi-annually Grab SW 13.0 ug/L Oil and Grease; 15.0 mg/L 20.0 mg/L Semi-annually Grab Effluent H" Semi-annually Grab Effluent Chemical Oxygen Demands Semi-annually Grab Effluent 1. Effluent temperature will be regulated so that the temperature -of the receiving stream does not increase more than: Fresh water classifications 2.8°C above the natural water temperature However, the receiving water temperature in no. case to exceed 29°C at the downstream monitoring location for mountain and upper piedmont waters. However, the receiving water temperature in no case to exceed 32°C at the downstream monitoring location for lower piedmont and coastal plain waters. Trout water classifications 0.5°C above the natural water temperature due to discharge of heated liquids However, the receiving water temperature in no case to exceed 20°C at the downstream monitoring location for trout waters. Salt water classifications 0.8°C above the natural water temperature during the months of June, July and August 2.2°C above the natural water temperature during any other months However, the receiving water temperature in no cases to exceed 320C at the downstream monitoring location for salt waters due to the discharge of heated liquids. The permittee shall demonstrate compliance with the effluent temperature limitations by monitoring the temperature of the receiving stream upstream and downstream of the discharge outfall. The Division should be consulted in selecting a representative upstream/downstrcam site. Upstream and downstream monitoring is not necessary if the discharge is to a receiving stream that does not contain any flowing water at the time of discharge. Page 2 of 20 • General Permit NCG500000 2. Monitoring requirements and limits apply only if chlorine is present in the discharge. Discharges to fresh waters (FW) will be required to meet a daily maximum discharge Iiinitation of 17 �tgl L of Total Residual Chlorine (TRC). Discharges to salt waters (SW) will be required to meet a daily maximum discharge limitation of 13 pgl L of TRC. The Division shall consider all effluent TRC values reported below 50 ggl L to be in compliance with the permit. 3. Monitoring requirement applies only for discharges of air compressor condensate. 4. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units for freshwater classifications The pH shall not be less than 6.8 standard units nor greater than 8.5 standard units for saltwater classifications 5. Mo�nittoorringtregtiiirementrapplie--svo'nly ff w�' atdr ttreatment and/o5i cNe—mica] dditive'� -, ife osiop inlubitorsv c-oxygen-seavengeis,7biocides.oi=oleaning>solvents are'added_to the.-system:V This permit does not authorize the discharge of water treatment or chemical additives (including but not limited to chromium, zinc or copper) other than chlorin_ a and approved de -chlorinating reagents without written approval from the Division. *ThejpermitteetshallrcibwinvapprovalLfromttheaDivisiontpnor toitheiuseioiranytchemical additiv--aii-nitha ep rmitteeiss systems,,co�erediunder3tHis p�"er H.*To obtain approval the permittee shall notify the Director in writing at least ninety (90) days prior to instituting use of any new additive (other than additives previously approved by the Division). Such approval requests shall include a completed Biocide Worksheet Form 101 or equivalent worksheet form approved by the Division, a copy of the Material Data Safety Sheet (MSDS) for the additive, and a map indicating the discharge point and receiving stream. All non -contact cooling water sample locations shall provide representative samples of the discharge and require sampling prior to discharge commingling with any other waters or substances, such as stormwater or surface water to enable characterization of a pollutant of concern. All samples collected should be from a representative discharge event, a measurable discharge event that results in an actual discharge from the permitted discharge outfall. There shall be no discharge of floating solids or visible foam in other than trace amounts. .Submittaboftmonthly Diz_'scharge.Monitoring4Rcportsi(,DMRs)2shaiiinotibeirequiNd;exceptL1ponidemand1by4thelk —DiViffio-rill- This section supersedes the requirement for submitting monthly Discharge Monitoring Reports (DMRs) specified in Part, Section D (2) of this permit. Even though the submittal of the monthly monitoring reports to the Division is suspended, all monitoring requirements remain. The data will be maintained on site for a period of three years. Page 3 of 20 General Permit NCG600000 A (2) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FOR HYDROELECTRIC FACILITIES — ONCE -THROUGH COOLING WATER AND SIMnAR WASTEWATERS During the period beginning on August 1, 2015 and lasting until expiration, the permittee is authorized to discharge once -through cooling waters (including generator cooling water, generator thrust bearing cooling water, turbine guide cooling water & transformer cooling water) and other similar waters associated with hydroelectric facilities from outfalls numbered serially beginning with 001 (specific outfall numbers shall be assigned by the permittee). Such discharges shall be- limited and monitored by the pennittee as specified below; PARAMETER LIMITS MONITORING REQUIREMENTS I A, Y Montlhfy v� Daily 3" Measurement `Sample "�� ` `Sample Location Aveta ,: >SMaiiim Fre a m u,:.. uenc e..Y ?' Flow.. Semi-annually_Estimate Effluent Effluent, Upstream, Temperature Semi-annually Grab Downstream Total Residual Chlorinez FW17.0 ug/L Effluent Semi-annually Grab SW 13.0 ug/L H3 Semi-annually Grab Effluent Chemical Oxygen Demand' Semi-annually Grab Effluent 1. Effluent temperature will be regulated so that the temperature of the receiving stream does not increase more than, Fresh water classifications 2.8°C above the natural water temperature However, the receiving water temperature in no case to exceed 29°C at the downstream monitoring location for mountain and upper piedmont waters. However, the receiving water temperature in no case to exceed 32°C at the downstream monitoring location for lower piedmont and coastal plain waters. Trout water classifications 0.5°C above the natural water temperature due to discharge of heated liquids However, the receiving water temperature in no case to exceed 20°C at the downstream monitoring location for trout waters. "Saltwater classifications 0.8°C above the natural water temperature during the months of June, July and August 2.2°C above the natural water temperature during any other months However, the receiving water temperature in no cases to exceed 32°C at the downstream monitoring location for salt waters due to the discharge of heated liquids. The permittee shall demonstrate compliance with the effluent temperature limitations by monitoring the temperature of the receiving stream upstream and downstream of the discharge outfall. The Division should be consulted in selecting location(s) that provide(s) a representative upstream/downstream site. Upstream and downstream monitoring is not necessary if the discharge is to a receiving stream that does not contain any flowing water at the time of discharge. 2. Monitoring requirements and limits apply only if chlorine is present in the discharge. Discharges to fresh waters (FW will be required to meet a daily maximum discharge limitation of 17 µg/ L of Total Residual Chlorine (TRC). Discharges to salt waters (SW) will be required to meet a daily maximum discharge limitation Page 4 of 20 • • " General Permit NCG500000 of 13 µgl L of TRC. The Division shall consider all effluent TRC values reported below 50 µg/ L to be in compliance with the permit. 3. The pH shall not be less than 6.0 standard units nor greater than 9'.0 standard units for fresh water classifications The pH shall not be less than 6.8 standard units nor greater than 8.5 standard units for saltwater classifications 4. Monitoring requirement applies only if water treatment and/or chemical additives i.e. corrosion inhibitors, oxygen scavengers, biocides or cleaning solvents are added to the system. This permit does not authorize the discharge of water treatment or chemical additives (including but not limited to chromium, zinc or copper) other than chlorine and approved de -chlorinating reagents without written approval from the Division. The permittee shall obtain approval from the Division prior to the use of any chemical additive in the permittec's systems covered under this permit. To obtain approval the permittee shall notify the Director in writing at least ninety (90) days prior to instituting use of any new additive (other than additives previously approved by the Division). Such approval requests shall include a completed Biocide Worksheet Form 101 or equivalent worksheet form approved by the Division, a copy of the MSDS for the additive, and a map indicating the discharge point and receiving stream. All samples collected should be from a representative discharge event, a measurable discharge event that results in an actual discharge from the permitted discharge outfall, All non -contact cooling water sample locations shall provide representative samples of the discharge and require sampling prior to discharge commingling with any other waters or substances, such as stormwater or surface water to enable characterization of a pollutant of concern. There shall be no discharge of floating solids or visible foam (other than trace amounts) in the effluent Submittal of monthly Discharge Monitoring Reports (DMRs) shall not be required except upon demand by the Division. This section supersedes the requirement for submitting monthly Discharge Monitoring Reports (DMRs) specified in Part, Section D (2) of this permit. Even though the submittal of the monthly monitoring reports to the Division is suspended, all monitoring requirements remain. The data will be maintained on site for a period of three years. Page S of 20 General Permit NCO` 500000 A (3) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS FOR HYDROELECTRIC FACILITIES — SUMPS AND DRAINS AND OTHER MISCELLANEOUS WASTEWATERS During the period beginning on August 1, 2015 and lasting until expiration, the permittee is authorized to discharge waters from sumps & drains (including powerhouse sumps & drains, wheel pit drains, head cover drains and gallery sumps & drains) and other miscellaneous wastewaters (fiom sumps & drains associated with hydroelectric facilities) from outfalls numbered serially beginning with 001 (specific outfall numbers shall be assigned by the permittee). Such discharges shall be limited and monitored by the permittee as specified below: PARAMETER x LIMITS w 11ONITORING REQUIREMENTS Monthly 1q Daily F 1 Measurement � yt Sample Sample Locataon ; t Aveira a Mazimurn; ' Fre iienc : Flow Quarterly Estimate Effluent Oil and Grease' 15.0 20.0 mg/L Quarterly Grab Effluent PH guartorly Grab Effluent FW 11.0 ug/L Effluent Total Residual Chlorine' Serni-annually Grab SW 13.0 ug/L Chemical Oxygen Demand Semi-annually Grab Effluent 1. The tailrace shall be visually inspected for oil sheens when a permitted discharge occurs immediately after the lubrication of wicket gates (or other lubrication operations which might result in the discharge of oil and grease) at the hydroelectric facility. 2. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units for fresh water classifications The pH shall not be less than 6.8 standard units nor greater than 8.5 standard units for saltwater classifications Monitoring requirements and limits apply only if chlorine is present in the discharge. Discharges to fresh waters (FW will be required to meet a daily maximum discharge limitation of 17 µg/ L of Total Residual Chlorine (TRC). Discharges to salt waters (SW) will be required to meet a daily maximum discharge limitation of 13 l,tg/ L of TRC. The Division shall consider all effluent TRC values reported below 501tg/ L to be in compliance with the permit. 4. Monitoring requirement applies only if water treatment and/or chemical additives i.e. cotTosion inhibitors, oxygen scavengers, biocides or cleaning solvents are added to the system. Chemical wheel pit cleaning is permitted on a monthly basis. When cleaning of the wheel pits occurs, the tailrace shall be inspected visually for foam and oil. Cleaning shall be conducted only with solvents pre -approved by the Division. The permittee is responsible for retaining documentation of all solvent approvals. Should the permittee wish to change cleaning solvents (other than solvents previously approved) a written request should be made to the Division including the MSDS for the proposed solvent. Mechanical cleaning operations which do not contribute any wastewater to the discharge are not limited by this permit. Non -discharging cleaning operations may be conducted as often as necessary to ensure safety and proper facility operation. Page 6 of 20 • • General Permit NCG500000 This permit does not authorize the discharge of water treatment or chemical additives (including but not limited to chromium, zinc or copper) other than chlorine and approved de -chlorinating reagents without written approval from the Division. The permittee shall obtain approval from the Division prior to the use of any chemical additive in the permittee's systems covered under this permit. To obtain approval the permittee shall notify the Director in writing at least ninety (90) days prior to instituting use of any new additive (other than additives previously approved by the Division), Such approval requests shall include a completed Biocide Worksheet Form 101 or equivalent worksheet form approved by the Division, a copy of the MSDS for the additive, and a map indicating the discharge point and receiving stream. All non -contact cooling water sample Iocations shall provide representative samples of the discharge and require sampling prior to discharge commingling with any other waters or substances, -such as stormwater or surface water to enable characterization of a pollutant of concern. All samples collected should be from a representative discharge event, a measurable discharge event that results in an actual discharge from the permitted discharge outfall. There shall be no discharge of floating solids or visible foam (other than trace amounts) in the effluent. Submittal of monthly Discharge Monitoring Reports (DMRs) shall not be required except upon demand by the Division. This section supersedes the requirement for submitting monthly Discharge Monitoring Reports (DMRs) specified in Part, Section D (2) of this permit. Even though the submittal of the monthly monitoring reports to the Division is suspended, all monitoring requirements remain. The data will be maintained on site for a period of three years. SECTION B. SCHEDULE OF COMPLIANCE 1. The permittee shall comply with Final' Effluent Limitations by the effective date of the Certificate of Coverage. 2. Permittee shall at all times'provide the operation and maintenance necessary to operate the existing facilities in accordance with Standard Conditions for NPDES Permits Section C.2. of this permit. 3. Pertnittee shall operate the existing facilities such that constituents and/or characteristics of the discharge qualify for Certificate of Coverage under the General Permit in accordance with 15A NCAC 02H .0127. In accordance with NPDES regulations at § 122.45, allowing detection of a pollutant: Instances could arise where the combination of process and non -process wastewaters result in dilution of a pollutant of concern such that it would not be detectable using approved analytical methods. Internal monitoring would enable characterization of the pollutant before dilution with other wastewaters. 4. The upstream location for the natural water temperature shall be interpreted as the influent to the penstock or other appropriate location in the impounded waterbody. Effluent is the outflow from the powerhouse. The temperature change between these two values is considered the heat added and judged for compliance with Note 1 of the permit and 15A NCAC 2H.0211 0). Page 7 of 20 General Kermit NCO500000 SECTION C. APPLICABILITY This permit is applicable to the following types of discharges defined below: I . Non -contact cooling water and open recirculation cooling water systems used in industrial processes for the sole purpose of cooling machinery and other equipment. Non -contact cooling water is defined as water used for cooling which does not come into direct contact with any raw material, intermediate product, waste product or finished product. Contact cooling water is defined as cooling water that comes into contact with raw material, intermediate product, .finished product, byproduct or waste product. Open recirculating cooling water systems, continuously reuse the cooling water which passes through the heat transfer equipment. Open recirculating cooling water system discharges to a Water Supply water body may require an individual NPDES permit. Contact cooling water discharges require an individual NPDES permit. 2. Condensate wastewater from atmospheric cooling systems, 3. Blowdown wastewaters. Blowdown is defined as the minimum discharge of recirculating water for the purpose of discharging materials contained in the water, the further buildup of which would cause concentration in amounts exceeding limits established by best engineering practice. 4. Exempt stormwater, which is defined as discharges of stormwater which do not require permits under the state or Federal NPDES programs. Exempt stormwater includes stormwater which accumulates in outdoor basins or ponds designed for cooling water or other waters covered by this permit. 5. Water associated with hydroelectric power facilities, including cooling waters, waters from sumps and drains, dam seepage and exempt stormwater. 6. Other similar wastewaters which may qualify for coverage under this General Permit. SECTION D. N_QTICE_OF INTEND General Permit Expiration General permits will be effective for a term not to exceed five years, at the end of which the Division may renew them after all public notice requirements have been satisfied. If a general permit is renewed, existing permittees do not need to submit a renewal request or pay a renewal fee unless directed by the Division. New applicants seeking coverage under a renewed general permit must submit a Notice of Intent to be covered and obtain a Certificate of Coverage under the renewed general permit [15A NCAC 02H .0127(e)]. A current version of the NOI for this general permit can be obtained by contacting the NPDES Permitting Program at (919) 807-6300 or can be downloaded from the internet at h :/ al.nedenr or web/w /sw 1 s/n des/calendar. NOIs must be signed and submitted to the NPDES Permitting Program 1617 Mail Service Center, Raleigh, NC 27699-1617. Applicants who have submitted a completed NOI are not authorized to discharge until a Certificate of Coverage is issued. In general, the NOI shall include the following information: I . The mailing address and telephone number for the owner and/ or operator 2. The facility name, address and telephone number where the discharge will occur. 3. The permit number of any NPDES permit(s) for any discharge(s) from the site. 4. A description of the discharge, including the number of discharge points, the volume of discharge, the frequency of discharge and any treatment methods applied prior to discharge. 5. The name of the receiving waters and the stream classification (s). 6. An analysis of non -discharge alternatives, including connection to a regional sewer collection system, subsurface disposal and spray irrigation. 7. A 7.5 minute series USGS topographic map with the discharge location clearly indicated. 8, Final plans and specifications for the treatment system and all major components (if applicable), 9. A certification that the information contained in the NOI is true, complete and accurate. 10. A listing of all previously approved water treatment and/or chemical additives i.e. biocides, oxygen scavengers, corrosion inhibitors, and cleaning solvents. Water treatment and chemical additives include any material that is added to water used at the facility or to a wastewater generated by the facility to condition or treat water. Page 8 of 20 • General Permit NCG500000 PART II STANDARD CONDITIONS FOR NPDES PERMITS Section A. Definitions 2/Month Samples are collected twice per month with at least ten calendar days between sampling events. These samples shall be representative of the wastewater discharged during the sample period. 3/Week Samples are collected three times per week on three separate calendar days. These samples shall be representative of the wastewater discharged during the sample period. Act or "the Act" The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33 USC 1251, et. seq. Annual Average The aritlunetic mean of all "daily discharges" of a pollutant measured during the calendar year. In the case of fecal coliform, the geometric mean of such discharges. - Arithmetic Mean The summation of the individual values divided by the number of individual values. Bynass The known diversion of waste streams from any portion of a treatment facility including the collection system, which is not a designed or established or operating mode for the facility. Calendar Day The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any consecutive 24-hour period that reasonably represents the calendar day may be used for sampling. Calendar Week The period from Sunday through the following Saturday. Calendar Ouarter One of the following distinct periods: January through March, April through June, July through September, and October through December. Composite Sample A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 mL in such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The Director may designate the most appropriate method (specific number and size of aliquots necessary, the time interval between grab samples, etc.) on a case -by -case basis. Samples may be collected manually or automatically, Composite samples may be obtained by the following methods: (1), Continuous: a single, continuous sample collected over a 24-hour period proportional to the rate of flow. (2) Constant time/variable volume; a series of grab samples collected at equal time intervals over a 24 hour period of discharge and combined proportional to the rate of flow measured at the time of individual sample collection, or (3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period with the time intervals between samples determined by a preset number of gallons passing the sampling point. Flow measurement between sample intervals shall be determined by use of a flow recorder and totalizer, and the preset gallon interval between sample collection fixed at no greater than 1/24 of the expected total daily flow at the treatment system, or (4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at a constant time interval. Use of this method requires prior approval by the Director. This method may only be used in situations where effluent flow rates vary less than 15 percent. The following restrictions also apply: Page 9 of 20 • 0 General Permit NCG5000'00 D Influent and effluent grab samples shall be of equal size and of no less than 100 milliliters ➢ Influent samples shall not be collected more than once per hour. D Permittees with wastewater treatment systems whose detention time < 24 hours shall collect effluent grab samples at intervals of no greater than 20 minutes apart during any 24-hour period. ➢ Permittees with wastewater treatment systems whose detention time exceeds 24 hours shall collect effluent grab samples at least every six hours; there must be a minimum of four samples during a 24-hour sampling period. Continuous flow measurement Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance activities on the flow device. Daily Discharge The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is calculated as the total mass of the pollutant discharged over the day. For pollutants expressed in other units of measurement, the "daily discharge" is calculated as the average measurement of the pollutant over the day. (40 CFR 122.2; see also "Composite Sample," above,) Daily Maximum The highest "daily discharge" during the calendar month. Daily Sam lin Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the permit. Sampling shall be conducted on weekdays except where holidays or other disruptions of normal operations prevent weekday sampling. If sampling is required for all seven days of the week for any permit parameter(s), that requirement will be so noted on the Effluent Limitations and Monitoring Page(s). DWR or "the Division" The Division of Water Resources, Department of Environment and Natural Resources. Effluent Wastewater discharged following all treatment processes from a water pollution control facility or other point source whether treated or untreated. EMC The North Carolina Environmental Management Commission EPA The United States Environmental Protection Agency Facility Closure Cessation of all activities that require coverage under this NPDES permit. Completion of facility closure will allow this permit to be rescinded. Geometric Mean The Nth root of the product of the individual values where N = the number of individual values. For purposes of calculating the geometric mean, values of "0" (or "< [detection level]") shall be considered W 1. Grab Sample Individual samples of at least 100 mL collected over a period of time not exceeding 15 minutes. Grab samples can be collected manually. Grab samples must be representative of the discharge (or the receiving stream, for instrearn samples). Hazardous Substance Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the CWA. Instantaneous flow measurement _ The flow measured during the minimum time required for the flow measuring device or method to produce a result in that instance. To the extent practical, instantaneous flow measurements coincide with the collection of any grab samples required for the same sampling period so that together the samples and flow are representative of the discharge during that sampling period. Page 10 of 20 r1 • General Permit NCG600000 Monthly Average (concentration.limit) The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of fecal coliform or other bacterial parameters or indicators, the geometric mean of such discharges. Permit Issuing Agihadiy The Director of the Division of Water Quality. Quarterly Average (concentration limit) The arithmetic mean of all samples taken over a calendar quarter. Severe property damage Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable, or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a bypass. Severe property damage excludes economic loss caused by delays in production. Toxic Pollutant: Any pollutant listed as toxic under Section 307(a)(1) of the CWA. Upset An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by operational error, improperly designed treatment facilities, inadequate treatment facilities, lack of preventive maintenance, or careless or improper operation. Weekly Average (concentration limit) The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week, In the case of fecal coliforzn or other bacterial parameters or indicators, the geometric mean of such discharges. Section B. General Conditions I. Duty to Comoly The_ Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation of the CWA and is grounds for enforcement action; for permit termination, revocation and reissuance, or modification; or denial of a permit renewal application [40 CFR 122.411. a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the CWA for toxic pollutants and with standards for sewage sludge use or disposal established under section 405(d) of the CWA within the time provided in the regulations that establish these standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been modified to incorporate the requirement. b. The CWA provides that any person who violates section[s] 301, 302, 306, 307, 308, 318 or 405 of the Act, or any permit condition or limitation implementing any such sections in a permit issued under section 402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402(b)(8) of the Act, is subject to a civil penalty not to exceed $37,500 per day for each violation. [33 USC 1319(d) and 40 CFR 122.41(a)(2)] c. The CWA provides that any person who negligently violates sections 301, 302, 306, 307, 308, 318, or 405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under section 402 of the Act, or any requirement imposed in a pretreatment program approved under section 402(a)(3) or 402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of violation, or by imprisonment of not more than 2 years, or both. [33 USC 1319(c)(1) and 40 CFR 122AI(a)(2)] d. Any person who knowingly violates such sections, or such conditions or limitations is subject to criminal penalties of $5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal penalties of not more than $100,000 per day of violation, or imprisonment of not more than 6 years, or both. [33 USC 1319(c)(2) and 40 CPR 122.41(a)(2)] e. Any person who knowingly violates section 301, 302, 303, 306, 307, 308, 318 or 405 of the Act, or any permit condition or limitation implementing any of such sections in a permit issued under section 402 of the Act, and Page I 1 of 20 0 rI General Permit NCG500000 who knows at that time that he thereby places another person in imminent danger of death or serious bodily injury, shall, upon conviction, be subject to a fine of not more than $250,600 or imprisonment of not more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment violation, a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than 30 years, or both. An organization, as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon conviction of violating the imminent danger provision, be subject to a fine of not more than $1,000,000 and can be fined up to $2,000,000 for second or subsequent convictions. [40 CFR 122.41(a)(2)] f. Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North Carolina General Statutes § 143-215,6A] g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302, 306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such sections in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are not to exceed $16,000 per violation, with the maximum amount of any Class I penalty assessed not to exceed $37,500. Penalties for Class II violations are not to exceed $16,000 per day for each day during which the violation continues, with the maximum amount of any Class II penalty not to exceed $177,500. [33 USC 1319(g)(2) and 40 CFR 122.41(a)(3)] 2. Duty to Mitigate The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in violation of this permit with a reasonable likelihood of adversely affecting human health or the enviromnent [40 CFR 122,41(d)]. 3. Civil and Criminal Liability Except as provided in permit conditions on "Bypassing". (Pail II.C.4), "Upsets" (Part II.C,5) and "Power Failures" (Part II.C.7), nothing in this permit shall be construed to relieve the Permittee from any responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as fish kills, even though the responsibility for effective compliance may be temporarily suspended. 4. Oil and Hazardous Substance Liability Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee from any responsibilities, liabilities, or penalties to which the Permittee is or may be subject to under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for consequential damages, such as fish kills, even though the responsibility for effective compliance may be temporarily suspended. 5. Property Ripbts The issuance of this permit does not convey any property rights in either real or personal property, or any exclusive privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor any infringement of Federal, State or local laws or regulations [40 CFR 122.41(g)]. 6. Onshore or Offshore Construction This permit does not authorize or approve the construction of any onshore or offshore physical structures or facilities or the undertaking of any work in any navigable waters. 7. Severability The provisions of this permit are severable. If any provision of this permit, or the application of any provision of this permit to any circumstances, is held invalid, the application of such provision to other circumstances, and the remainder of this permit, shall not be affected thereby [NCGS 150E-231. 8. Du!y to Provide_ Information The Permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which the Permit Issuing Authority may request to determine whether cause exists for modifying, revoking and reissuing, or terminating this permit or to determine compliance with this permit. The Permittee shall also furnish to the Permit Issuing Authority upon request, copies of records required by this permit [40 CFR 122.41(h)]. 9. Signatory Requirements All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified [40 CFR 122.41(k)]. Page 12 of 20 0 General Permit NCG600000 a. All permit applications shall be signed as follows: (1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in charge of a principal business function, or any other person who performs similar policy or decision making functions for the corporation, or.(b) the manager of one or more manufacturing, production, or operating facilities, provided, the manager is authorized to make management decisions which govern the operation of the regulated facility including having the explicit or implicit duty of making major capital investment recommendations, and initiating and directing other comprehensive measures to assure long term environmental compliance with environmental laws and regulations; the manager can ensure that the necessary systems are established or actions taken to gather complete and accurate information for permit application requirements; and where authority to sign documents has been assigned or delegated to the manager in accordance with corporate procedures . (2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or (3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or ranking elected official (40 CFR 122.221. b. All reports required by the permit and other information requested by the Permit Issuing Authority shall be signed by a person described in paragraph a. above or by a duly authorized representative of that person. A person is a duly authorized representative only if: (1) The authorization is made in writing by a person described above; (2) The authorization specified either an individual or a position having responsibility for the overall operation of the regulated facility or activity, such as the position of plant manager, operator of a well or well field, superintendent, a position of equivalent responsibility, or an individual or position having overall responsibility for environmental matters for the company. (A duly authorized representative may thus be either a named individual or any individual occupying a named position.); and (3) The written authorization is submitted to the Permit Issuing Authority [40 CFR 122.221 c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate because a different individual or position has responsibility for the overall operation of the facility, a new authorization satisfying the requirements' of paragraph (b) of this section must be submitted to the Director prior to or together with any reports, information, or applications to be signed by an authorized representative [40 CFR 122.22] d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the following certification [40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL BE ACCEPTED: 'V certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, trace, accurate, and complete. lam aware that there are significant penalties for submittingfalse information, including the possibility of fines and imprisonment for knowing violations," 10. Permit Actions This permit may be modified, revoked and reissued, or terminated for cause, The filing of a request by the Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned changes or anticipated noncompliance does not stay any permit condition [40 CFR 122.41(f)]. 11. Permit_ Modification, Revocation and Rei_ss_uance, or Termination The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the permit, revoking and reissuing the permit, or terminating the permit as allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina Administrative Code, Subchapter 02H .0100; and North Carolina General Statute 143.215, l et. al. 12. Annual Administering and Compliance Monitoring Fee Requirements The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 02H .0I05(b)(2) may cause this Division to initiate action to revoke the permit, and/or the Certificate of Coverage issued to the permitee under this permit. Page 13 of 20 • • General Permit NCG5000b0 Section C. Operation and Maintenance of Pollution Controls 1. Certified Operator Owners of classified water pollution control systems must designate operators, certified by the Water Pollution Control System Operators Certification Commission (WPCSOCC), of the appropriate type and grade for the system, and, for each classification must [T15A NCAC 08G .0201]: a. designate one Operator In Responsible Charge (ORC) who possesses a valid certificate of the type and grade at least equivalent to the type and grade of the system; b. designate one or more Back-up Operator(s) in Responsible Charge (Back-up ORCs) who possesses a valid certificate of the type of the system and no more than one grade less than the grade of the system, with the exception of no backup operator in responsible charge is required for systems whose minimum visitation requirements are twice per year; and c. submit a signed completed "Water Pollution Control System Operator Designation Form" to the Commission (or to the local health department for owners of subsurface systems) countersigned by the designated certified operators, designating the Operator in Responsible Charge (ORC) and the Back-up Operator in Responsible Charge (Back-up ORC): (1) 50 calendar days prior to wastewater or residuals being introduced into a new system; or (2) within 120 calendar days following: ➢ receiving notification of a change in the classification of the system requiring the designation of a new Operator in Responsible Charge (ORC) and Back-up Operator in Responsible Charge (Back-up ORC) of the proper type and grade; or ➢ a vacancy in the position of Operator in Responsible Charge (ORC) or Back-up Operator in Responsible Charge (Back-up ORC). (3) within seven calendar days of vacancies in both ORC and Back-up ORC positions replacing or designating at least one of the responsibilities. The ORC of each Class I facility (or the Back-up ORC, when acting as surrogate for the ORC) must: ➢ Visit the facility as often as is necessary to insure proper operation of the treatment system; the treatment facility must be visited at least weekly ➢ Comply with all other conditions of 15A NCAC 08G .0204. Note: This requirement does not apply until the permittee receives a letter notifying them of classification of the facility. Currently, facilities are not being classified for this purpose, but may at some time in the future. 2. Proper Operation and Maintenance The Permittee shall at all times properly operate and maintain all facilities and systems of treatment and control (and related appurtenances) which are installed or used by the Permittee to achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate laboratory controls and appropriate quality assurancc procedures. This provision requires the Permittec to install and operate backup or auxiliary facilities only when necessary to achieve compliance with the conditions of the permit [40 CFR 122.41(c)]. NOTE: Properly and officially designated operators are fully responsible for all proper operation and maintenance of the facility, and all documentation required thereof, whether acting as a contract operator [subcontractor] or a member of the Permittee's staff. 3. Need to Halt or Reduce not a Defense It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or reduce the permitted activity in order to maintain compliance with the condition of this permit [40 CFR 122.4l(c)]. Page 14 of 20 General Permit NCG500000 4. Bypassing of Treatment Facilities a. Bypass not exceeding limitations [40 CFR 122.41(m)(2)] The Pen-nittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the provisions of Paragraphs b, and c. of this section. b. Notice [40 CFR 122.41(m)(3)] (1) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior notice, if possible at least ten days before the date of the bypass; including an evaluation of the anticipated quality and effect of the bypass. (2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in Part II.E.6. (24-hour notice). c. Prohibition of Bypass (1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement action against a Permittee for bypass, unless: _ (A) Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; (B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities, retention of untreated wastes or maintenance during normal periods of equipment downtime. This condition is not satisfied if adequate backup equipment should have been installed in the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal periods of equipment downtime or preventive maintenance; and (C) The Pennittee submitted notices as required under Paragraph b. of this section. (2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement action against a Permittee for a bypass as provided in any current or fixture system -wide collection system permit associated with the treatment facility, (3) The Permit Issuing Authority may approve an anticipated bypass, after considering its adverse effects, if the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c. (1) of this section. 5. Upsets a. Effect of an upset [40 CFR 122.41(n)(2)]: An upset constitutes an affirmative defense to an action brought for noncompliance with such technology based permit effluent limitations if the requirements of paragraph b. of this condition are met. No determination made during administrative review of claims that noncompliance was caused by upset, and before an action for noncompliance, is final administrative action subject to judicial review. b. Conditions necessary for a demonstration of upset: Any Permittee who wishes to establish the affirmative defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or other relevant evidence that: (1) An upset occurred and that the Permittee can identify the cause(s) of the upset; (2) The Permittee facility was at the time being properly operated; and (3) The Permittee submitted notice of the upset as required in Part II.E.6 of this permit. (4) The Permittee complied with any remedial measures required under Part LI.B.2. of this permit. c. BLirden of proof [40 CFR 122.41(n)(4)]: The Permittee seeking'to establish the occurrence of an upset has the burden of proof in any enforcement proceeding. 6. ' Removed Substances Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant from such materials from entering waters of the State or navigable waters of the United States except as permitted by the Commission. The Permittee shall comply with all applicable state and Federal regulations governing the disposal of sewage sludge, including 40 CFR 503, Standards for the Use and Disposal of Sewage Sludge; 40 CFR Part 258, Criteria For Municipal Solid Waste Landfills; and 15A NCAC Subchapter 2T, Waste Not Discharged To Surface Waters. The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use or disposal practices. Page 15 of 20 General Permit NCG600000 7. Power Failures The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 02H .0124) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures either by means of alternate power sources, standby generators or retention of inadequately treated effluent. Section D. Monitoring and Records I. Representative Sampling Samples collected and measurements taken, as required herein, shall be representative of the permitted discharge, Samples collected at a frequency less than daily shall be taken on a day and time that is representative of the discharge for the period the sample represents. All samples shall be taken at the monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is diluted by any other wastestream, body of water, or substance. Monitoring points shall not be changed without notification to and the approval of the Permit Issuing Authority [40 CFR 122.41(j)]. 2. Reporting Monitoring results obtained during the previous month(s) shall be suirunarized for each month and reported on a monthly Discharge Monitoring Report (DMR) Form (MR 1, 1.1, 2, 3) or alternative forms approved by the Director, postmarked no later than the last calendar day of the month following the completed reporting period. The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of these, and all other reports required herein, shall be submitted to the following address: NC DENR / Division of Water Resources / Water Quality Permitting Section ATTENTION: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 3. Flow Measurements Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge volumes. Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device. The Director shall approve the flow measurement device and monitoring location prior to installation. Once -through condenser cooling water flow monitored by pump logs, or pump hour meters as specified in Part I of this permit and based on the manufacturer's pump curves shall not be subject to this requirement. 4. Test Procedures Laboratories used for sample analysis must be certified by the Division. Permittees should contact the Division's Laboratory Certification Section (919 733-3908 or http://portal.nedenr.org/web/wq/lab/cert) for information regarding laboratory certifications. Facilities whose personnel are conducting testing of field -certified parameters only must hold the appropriate field parameter laboratory certifications. Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to NCGS 143-215.63 et. seq.), the Water and Air Quality Reporting Acts, and to regulations published pursuant to Section 304(g), 33 USC 1314, of the CWA (as amended), and 40 CFR 136; or in the case of sludge use or disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR 503, unless other test procedures have been specified in this permit [40 CFR 122.41 ]. To meet the intent of the monitoring required by this permit, all test procedures must produce minimum detection and reporting levels that are below the permit discharge requirements and all data generated must be reported down Page 16 of 20 • • General Permit NCG600000 to the minimum detection or lower reporting level of the procedure. If no approved methods are determined capable of achieving minimum detection and reporting levels below permit discharge requirements, then the most sensitive (method with the lowest possible detection and reporting level) approved method must be used. 5. Penalties for Tampering The CWA provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any monitoring device or method required to be maintained under this permit shall, upon conviction, be punished by a fine of not mare than $10,000 per violation, or by imprisonment for not more than two years per violation, or by both. If a conviction of a person is for a violation committed after a first conviction of such person under this paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more than 4 years, or both [40 CFR 122.41]. 6. Records Retention Except for records of monitoring information required by this permit related to the Permittee's sewage sludge use and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40 CFR 503), the Permittee shall retain records of all monitoring information, including; ➢ all calibration and maintenance records ➢ all original strip chart recordings for continuous monitoring instrumentation D copies of all reports required by this permit ➢ copies of all data used to complete the application for this permit These records or copies shall be maintained for a period of at least 3 years from the date of the sample, measurement, report or application. This period may be extended by request of the Director at any time [40 CFR 122.41]. 7. Recording Results For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shall record the following information [40 CFR 122.41]: a. The date, exact place, and time of sampling or measurements; b. The individual(s) who performed the sampling or measurements; c. The date(s) analyses were performed; d. The individual(s) who performed the analyses; e. The analytical techniques or methods used; and f. The results of such analyses. 8. Inspection and Entev The Permittee shall allow the Director, or an authorized representative (including an authorized contractor acting as a representative of the Director), upon the presentation of credentials and other documents as may be required by law, to; a. Enter, at reasonable times, upon the Permittee's premises where a regulated facility or activity is located or conducted, or where records must be kept under the conditions of this permit; b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this permit; c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices, or operations regulated or required under this permit; and d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise authorized by the CWA, any substances or parameters at any location [40 CFR 122.41(i)]. Page 17 of 20 General Permit NCGb00000 Section E Reporting Requirements 1. Chance in Discharge All discharges authorized herein shall be consistent with the terms and conditions of this permit. The discharge of any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall constitute a violation of the permit. 2. Planned Chances The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or additions to the permitted facility [40 CFR 122.41(1)]. Notice is required only when: a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR 122.29(b); or b. The alteration or addition could significantly change the nature or increase the quantity of pollutants discharged. This notification applies to pollutants subject neither to effluent limitations in the permit, nor to notification requirements tinder 40 CFR 122.42(a)(1); or c. The alteration or addition results in a significant change in the Permittee's sludge use or disposal practices, and such alteration, addition or change may justify the application of permit conditions that are different from or absent in the existing permit, including notification of additional use or disposal sites not reported during the permit application process or not reported pursuant to an approved land application plan. 3. Anticipated Noncompliance The Permittee shall give advance notice to the Director of any planned changes to the permitted facility or other activities that might result in noncompliance with the permit [40 CFR 122.41(l)(2)]. 4. Transfers This permit is not transferable to any person without prior written notice to and approval from the Director in accordance with 40 CFR 122.61. The Director may condition approval in accordance with NCGS 143-215. I, in particular NCGS 143-215.1(b)(4)b,2., and may require modification or revocation and reissuance of the permit, or a minor modification, to identify the new permittee and incorporate such other requirements as may be necessary under the CWA [40 CFR 122.41(1)(3), 122.61] or state statute. 5. Monitoring Reports Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.41(l)(4)]. a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II.D.2) or forms provided by the Director for reporting results of monitoring of sludge use or disposal practices. b. If the Permittee monitors any pollutant more frequently than required by this permit using test procedures, approved under 40 CFR Part 136 and at a sampling location specified in this permit or other appropriate instrument governing the discharge, the results of such monitoring shall be included in the calculation and reporting of the data submitted on the DMR. 6. Twenty-four Hour Reporting a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the Permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the Permittee becomes aware of the circumstances. The written submission shall contain a description of the noncompliance, and its cause; the period of noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the noncompliance [40 CFR 122.41(1)(6)]. b. The Director may waive the written report on a case -by -case basis for reports under this section if the oral report has been received within 24 hours. c. Occurrences outside normal business hours may also be reported to the Division's Emergency Response personnel at (800) 662-7956, (800) 858-0368 or (919) 733-3300. 7. Other Noncompliance The Permittee shall report all instances of noncompliance not reported under Part II.E.5 and 6. of this permit at the time monitoring reports are submitted. The reports shall contain the information listed in Part II.E.6. of this permit [40 CFR 122.41(1)(7)]. Page 18 of 20 General Permit NCG500000 8. Other Information Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit such facts or information [40 CFR 122.41(1)(8)]. 9. Noncompliance Notification The Permittee shall report by telephone to either the central office or the appropriate regional office of the Division as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following; a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge digester; the known passage of a slug of hazardous substance through the facility; or any other unusual circumstances. b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate wastewater treatment such as mechanical or electrical failures of pumps, aerators, compressors, etc. c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass without treatment of all or any portion of the influent to such station or facility. Persons reporting such occurrences by telephone shall also file a written report within 5 days following first knowledge of the occurrence. Also see reporting requirements for municipalities in Part IV.C.2.c. of this permit. 10. Availability of Reports Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices of the Division. As required by the Act, effluent data shall not be considered confidential, Knowingly making any false statement on any such report may result in the'imposition of criminal penalties as provided for in NCGS 143- 215. 1 (b)(2) or in Section 309 of the Federal Act. 11. Penalties for Falsification of Reports The CWA provides that any person who knowingly makes any false statement, representation, or certification in any record or other document submitted or required to be maintained under this permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of not more than $25,000 per violation, or by imprisonment for not more than two years per violation, or by both [40 CFR 122.41 ]. PART III OTHER REQUIREMENTS Section A. Construction a. The Permittee shall not commence construction of wastewater treatment facilities, nor add to the plant's treatment capacity, nor change the treatment process(es) utilized at the treatment plant unless (I) the Division has issued an Authorization to Construct (AtC) permit or (2) the Permittee is exempted from such AtC permit requirements under Item b. of this Section. b. In accordance with NCGS 143-2I5.l(a5) [SL 2011-3941, no permit shall be required to enter into a contract for the construction, installation, or alteration of any treatment work or disposal system or to construct, install, or alter any treatment works or disposal system within the State when the system's or work's principle function is to conduct, treat, equalize, neutralize, stabilize, recycle, or dispose of industrial waste or sewage from an industrial facility and the discharge of the industrial waste or sewage is authorized under a permit issued for the discharge of the industrial waste or sewage into the waters of the State. Notwithstanding the above, the permit issued for the discharge may be modified if required by federal regulation. c. Issuance of an AtC will not occur until Final Plans and Specifications for the proposed construction have been submitted by the Permittee and approved by the Division. Page 19 of20 0- 0 General Permit NCO500060 Section B. Groundwater Monitoring The Permittee shall, upon written notice from the Director, conduct groundwater monitoring as may be required to determine the compliance of this NPDES permitted facility with the current groundwater standards. Section C. Changes in Discharges of Toxic Substances The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CFR 122.42): a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent basis, of any toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the following "notification levels"; (1) One hundred micrograms per Iiter (100 µg/L); (2) Two hundred micrograms per liter (200 µg/L) for acrolein and acrylonitrile; five hundred micrograms per liter (500 µg/L) for 2,4-dinitrophenol and for 2-methyl-4,6-dinitrophenol; and one milligram per liter (1 mg/L) for antimony; (3) Five times the maximum concentration value reported for that pollutant in the permit application. b. That any activity has occurred or will occur which would result in any discharge, on a non -routine or infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the following "notification levels"; (1) Five hundred micrograms per liter (500 µg/L); (2) One milligram per liter (I mg/L) for antimony; (3) Ten times the maximum concentration value reported for that pollutant in the permit application. Section D. Facility Closure Requirements The Permittee must notify the Division at least 90 days prior'to the closure of any wastewater treatment system covered by this permit. The Division may require specific measures during deactivation of the system to prevent adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit continue at the permitted facility. Page 20 of 20 Parnell, David From: Ascenzo, Tom Sent: Wednesday, February 22, 2012 1:59 PM To: Smith, Danny; Zhang, Cheng; Mall, Mandy; Witherspoon, Lauren; Landry, Natalie; Herzberg, Barry; Menefee-dunn, Barbara; Wiggins, Mack; Romanski, Autumn; Parnell, David; Zhang, Cheng Subject: Bypass RIMS# 201200336 : 2/20/2012 @ 7:00pm/1:30 am 2/21/2012- Novozymes, 77 Perry Chapel Church Road, Franklinton, NC: Bypass of WW Treatment system resulting from a Palm Oil overflow. The Palm Oil flowed from the overflow and ended up in the collection system, cooled off and hardened as a wax and clogged the collection system. The overflow came out of a manhole located in the street by the Palm Oil loading dock. Flowed down the street and ended up in Buffalo Creek. Approximately 2600 gallons spilled due to overflow. No Palm oil or solids noted in the stream. Site is clean as of 2/22/2012 at 11:55am. Thomas B Ascenzo Environmental Specialist NC Dept. of Environment & Natural Resources Division of Water Quality Raleigh Regional Office 1628 Mail Service Center Raleigh, NC 27609 919-791-4256 FAX: 919-788-7159 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. •a,; � C Romanski, Autumn From: Smith, Danny Sent: Friday, November 04, 2011 5:00 PM To; Romanski, Autumn Subject: FW: NPDES permit feasibility Attachments: Novozymes to Tar River.jpeg Fyi ds From: Belnick, Tom Sent: Friday, November 04, 2011 4:06 PM To: Risgaard, Jon; Montgomery, Lori; Smith, Danny Cc: Poupart, Jeff Subject: FW: NPDES permit feasibility Just had a phone discussion with Novozyzmes, and they are feeling out the possibility of direct discharge to Tar River. I discussed our EAA process, where they would have to demonstrate why their existing land app treatment is not viable for current/future flows. Sounds like they plan to meet with APS next week. Several options that they are considering. Mentioned salt content as potential toxicity issue. -PS- Although they_initially wanted to meet with NPDES next week, they have put that proposed meeting on hold. Tom-, Supervisor, Complex NPDES Permitting Unit NC DENR/Division of Water Quality ti 1617 lylailrviceiCenter, Raleigh, NC 27699-1617 - - - - - -— (919) $390;.fax (919) 807-6495` E-mail c_r-respondence to and from this address is subject to the North Carolina Public Records Law and may=b' =' �iscio`sed to third parties unless the content is exempt by statute or other regulation. - - From: DASY (Dean Sawyer) [mailto:DASY@novozymes.com] Sent, .,Friday, November 04, 2011 12:48 PM .mn To: Sledge,�Bob;-Belnick, Tom Cc SRP=-(Sara Perrin) Subjec�� PDES'permit feasibility Bob and IT. am 'We "would like to meet with you to discuss the feasibility of obtaining an NPDES permit. application permit and small discharge to Franklin County. We currently rely on'a land We are interested in better understanding the potential for us to discharge into the Tar. River (see attached map). -Can you meet Wed., November 9, 2011 at 9:30 AM in your office? �BesY Regards'" =— - Dean Sawyer Sr. Environmental Engineer NoVoiymes-Nardi America Inc. Pb box.576 77 Perrys Chapel Church Road Franklinton NC 27525 United States Phdqe:•+19194943470 Mobile: +1 9195233929 E-mail: dasv@novozvmes.com . Don't print today - contribute to a better environment tomorrow Novozymes North America, Inc. (reg. no.:13-2639630). Registered address: CT Corporation System, 111 8th Avenue, New York, NY 10011, United States of America This a -mail (including any attachments) Is for the Intended addressee(s) only and may contain confidential and/or proprietary Information protected by law. You are hereby notified that any unauthorized reading, disclosure, copying or distribution of this e-mail or use of Information herein is strictly prohibited. If you are not an intehded recipient you should delete this e-mail immediately, Thank you. I 1 2 1. Anaerobic Digester IC Reactor 2. 98C 5205) Ifur Treatment (FEN84A 5207) I Anaerobic Digester Recirculation Tank a. Small tank is Recirculation Tank (FEN98C 5209) 4. S. Anaerobic Digester Flare (FEN84CS01 5210) EN98A 5211) 6. Anaerobic D FEN10 5212) 7. Process Waste Water Clarifier Basin Agitator (FEN98B 5214) �}S 8. 9. 10, 11. 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March 21, 2011 NOVOZYMES NORTH AMERICA Franklinton NC 27525 -Attn: Joe Jenkins, Randy Green tC: Houston Cash, Jackson Messer Water Treatment Service Report Please find attached the laboratory results from samples collected from the cooling towers that discharge into the receiving stream. We also collected a sample from the city make-up and effluent however we a rain event that may have affected the effluent data slightly. I have tabulated the data that was the cause for collecting these samples, coppe , aluminum and zinc. I have also included conductivity as a reference to determine how the tower can pot tially. cycle con ent ating any 1 al e. 01 P� WS, stem Zinc Co er Aluminum Co_n'ui Make-up 0. < 0. <0.1 ppm 155 mhos FHG 0.5 ppm r �ft2 pprn <0.1 ppm 1005 mhos FEH 0.6 ppm , "<0.1 ppm <0.1 p m 1090 mhos FEG 1.2 ppm 0.3 ppm I <0.1 ppm 996 mhos Effluent 0.5 p m 0.1 ppm 1 0.2 ppm 553 mhos Comments: ✓LU tL �AA.a As you can see as with my on -site testing we have a significant amount of zinc in the make-up water, I assume this is the corrosion inhibitor added by the treatment facility. We have slightly elevated copper in the FEG & FHG towers however it is not observed in the effluent. We do not report any aluminum in any of the towers or make-up, so we should look for other sources of this material. I will investigate in more detail why we are observing copper in the two tower systems, however affective today please reduce the ORP set -point in these two systems by 25mv. We will collect additional samples on my next visit to monitor the changes in copper and zinc and to assist you in your efforts. Jim Sides Sr. Account Manager • ` S►H L OUN 17 Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: City Make-up Sampling Point: City Make-up System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides LWR Number: Project Number: Sample Number: WAL11-614 W-20110309-030 264752 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 32.9 mg/L pH 5.7 ANIONS Chloride (as CI) 16.8 mg/L Sulfate (as SO4) 20.7 mg/L CONDUCTIVITY Conductivity 155.0 PS/cm ACIDIFIED ELEMENTS Iron, (as Fe) < 0.1 mg/L Aluminum, (as AI) < 0.1 mg/L Copper, (as Cu) < 0.1 mg/L Manganese, (as Mn) <10.1 mg/L Zinc, (as Zn) �a� 'i ��, 0.4 iW mg/L 10 !� SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 25.7 mg/L Hardness - Magnesium, Soluble (as CaCO3) 12.8 mg/L Hardness - Total, Soluble (as CaCO3) 38.5 mg/L Silicon, Soluble (as Si02) 10.7 mg/L Sodium, Soluble (as Na) 13.9 mg/L Phosphorus, Soluble (as PO4) 1.8 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 1.7 mg/L Polyphosphate, Soluble (as PO4) < 0.1 mg/L Total Inorganic Phosphorus, Sol (as PO4) 1.7 mg/L Organic Phosphorus, Soluble (as PO4) 0.1 mg/L • tjsH«wv Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: FHG Tower Sampling Point: FHG Tower System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides LWR Number: Project Number: Sample Number: u WALI I-614 W-20110309-030 264753 Customer Information: uate 37t!lLVtt NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type I Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 81.7 mg/L pH 6.4 - ANIONS Chloride (as Cl) 130.0 mg/L Sulfate (as SO4) 156.0 mg/L CONDUCTIVITY Conductivity 1005.0 AS/cm ACIDIFIED ELEMENTS Iron, (as Fe) 1.5 mg/L Aluminum, (as Al) < 0.1 mg/L Copper, (as Cu) 0.2 mg/L Manganese, (as Mn) < 0.1 mg/L Zinc, (as Zn) 0.5 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 223.7 mg/L Hardness - Magnesium, Soluble (as CaCO3) 119.7 mg/L Hardness - Total, Soluble (as CaCO3) 343.4 mg/L Silicon, Soluble (as Si02) 90.2 mg/L Sodium, Soluble (as Na) 116.5 mg/L Phosphorus, Soluble (as PO4) 17.3 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 8.3 mg/L Polyphosphate, Soluble (as PO4) 8.0 mg/L Total Inorganic Phosphorus, Sol (as PO4) 16.3 mg/L Organic Phosphorus, Soluble (as PO4) 1.0 mg/L Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: FEH Tower Sampling Point: FEH Tower System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides L/ale XI I/LUl l LWR Number: WALI I-614 Project Number: W-20110309-030 Sample Number: 264754 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 173.4 mg/L pH 7.1 - ANIONS Chloride (as Cl) 130.0 mg/L Sulfate (as SO4) 180.0 mg/L CONDUCTIVITY Conductivity 1090.0 AS/cm ACIDIFIED ELEMENTS Iron, (as Fe) 0.3 mg/L Aluminum, (as Al) < 0.1 mg/L Copper, (as Cu) < 0.1 mg/L Manganese, (as Mn) <0.1 mg/L Zinc, (as Zn) 0.6 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 215.8 mg/L Hardness - Magnesium, Soluble (as CaCO3) 128.5 mg/L Hardness - Total, Soluble (as CaCO3) 344.3 mg/L Silicon, Soluble (as Si02) 107.2 mg/L Sodium, Soluble (as Na) 127.1 mg/L Phosphorus, Soluble (as PO4) 28.9 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 12.8 mg/L Polyphosphate, Soluble (as PO4) 15.2 mg/L Total Inorganic Phosphorus, Sol (as PO4) 28.0 mg/L Organic Phosphorus, Soluble (as PO4) 0.9 mg/L Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: FEG Tower Sampling Point: FEG Tower System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides 0 Late Jr1 rrLUi1 LWR Number: WAL11-614 Project Number: W-20110309-030 Sample Number: 264755 Customer information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, Pas CaCO3. <0.1 mg/L Alkalinity, Total (as CaCO3) 158.0 mg/L pH 7.1 - ANIONS Chloride (as C1) 116.0 mg/L Sulfate (as SO4) 156.0 mg/L CONDUCTIVITY Conductivity 996.0 µS/cm ACIDIFIED ELEMENTS Iron, (as Fe) 1.0 mg/L Aluminum, (as Al) < 0.1 mg/L Copper, (as Cu) 0.3 mg/L Manganese, (as Mn) < 0.1 mg/L Zinc, (as Zn) 1.2 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 214.5 mg/L Hardness - Magnesium, Soluble (as CaCO3) 116.9 mg/L Hardness - Total, Soluble (as CaCO3) 331.4 mg/L Silicon, Soluble (as SiO2) 89.4 mg/L Sodium, Soluble (as Na) 135.1 mg/L Phosphorus, Soluble (as PO4) 21.8 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 11.6 mg/L Polyphosphate, Soluble (as PO4) 9.1 mg[L Total Inorganic Phosphorus, Sol (as PO4) 20.7 mg/L Organic Phosphorus, Soluble (as PO4) 1.1 mg/L Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: Effluent Discharge Sampling Point: Effluent System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides • vale J11I1LVI1 LWR Number: WALI 1-614 Project Number: W-20110309-030 Sample Number: 264756 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) <0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg1L Alkalinity, Total (as CaCO3) 24.6 mg/L pH 5.7 - ANIONS Chloride (as Cl) 58.6 mg/L Sulfate (as SO4) 123.0 mg/L CONDUCTIVITY Conductivity 533.0 ]AS/cm ACIDIFIED ELEMENTS Iron, (as Fe) 0.8 mg/L Aluminum, (as Al) 0.2 mg/L Copper, (as Cu) < 0.1 mglL Manganese, (as Mn) < 0.1 mg/L Zinc, (as Zn) 0.5 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 120.9 mg/L Hardness - Magnesium, Soluble (as CaCO3) 47.4 mg/L Hardness - Total, Soluble (as CaCO3) 168.3 mg/L Silicon, Soluble (as Si02) 37.1 mg/L Sodium, Soluble (as Na) 67.3 mg/L Phosphorus, Soluble (as PO4) 5.9 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 2.7 mg/L Polyphosphate, Soluble (as PO4) 3.2 mg/L Total Inorganic Phosphorus, Sol (as PO4) 5.9 mg/L Organic Phosphorus, Soluble (as PO4) < 0.1 mg/L Date: April 24, 2014 Novozymes, NA Inc. 77 Perry's Chapel Church Rd. Franklinton, N.C. 27525 RECEIVED MAY 0 2 ZU14 CENTRAL FILES DWQIBOG NCDENR Division Of Water Quality 1617 Mail Service Center Raleigh, N.C. 27699-1617 Attn: Division Of Water Quality Storm Water Sampling, NPDES Pergt No. NCS000115 Dear Sir/Madam novozymes� Rethink Tomorrow During review of storm water sampling results, it was observed that there was an exceeded benchmark in Total Suspended Solids, (TSS) deriving from Outfall 1, Upon immediate investigation, per Tier One requirements, it was concluded that recent construction on site has created much exposed soil in areas in close proximity to storm drains. Works being performed using heavy equipment, dump trucks, and cranes, (tracked vehicles) for example, have resulted in exposed soil in high traffic areas, directly impacting turbidity readings during recent rain events. There have been many projects taking place on site during recent months. It is our belief that the decreasing work over the next couple of weeks, along with updating and replacing current BMP's placed throughout site will result in significantly lowered Total Suspended Solids, (TSS), readings. Continued monitoring by Environmental Services Department will take place in order to prevent future exceeded benchmarks in Total Suspended Solids, (TSS). Kind Regar , Joe Ladd Environme al Compliance Coordinator Environmental Services Cz L" ammi EFFLUENT NPDES PERMIT NO. NCS000115 DISCHARGE NO. 1 MONTH April YEAR 2014 FACILITY NAME NOVOZyIYIBS, NA Inc. CLASS COUNTY: Franklin OPERATOR IN RESPONSIBLE CHARGE (ORC) NIA PHONE (919) 494-3001 CERTIFIED LABORATORIES (1) EnCo 12) CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jos Ladd Mail ORIGINAL and ONE COPY to: ATTN: CENTRAL FILES x NIA DIVISION OF WATER QUALITY (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) 1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS ACCURATE AND COMPLETE TO THE BEST OF MY RALEIGH, NC 27699-1617 KNOWLEDGE. L11 MEMEM Monthly Limit DWQ Form MR- 1(11/04) Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements r (including weekly averages, if applicable) Compliant All monitoring data and sampling frequencies do NOT meet permit requirements Noncompliant The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by Part II.E.6 of the NPDES permit. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Randy Green Permittee (Please print or type) L U t Si re o P ittee*** Date (Required un s submitted electronically) Permittee Address Phone ]Number e-mail address Permit Expiration Date ADDITIONAL CERTIFIED LABORATORIES Certified Laboratory (2) Certification No. Certified Laboratory (3) Certification No. Certified Laboratory (4) Certification No. Certified Laboratory (5) Certification No. PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit at (919) 733-5083 or by visiting the Surface Water Protection Section's web site at h2o.ennstate.nc.us/wK s and linking to the unit's information pages. Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. * No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR for the entire monitoring period. ** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204. *** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). Page 2 EFFLUENT NPDES PERMIT NO. NCS000115 DISCHARGE NO. .FACILIr' NAME NOVOZymeS, NA Inc. CLASS OPERATOR IN RESPONSIBLE CHARGE (ORC) NIA CERTIFIED LABORATORIES (1) Enco (2) CHECK BOX IF ORC HAS CHANGED C::0 PERSON(S) COLLECTING SAMPLES Mail ORIGINAL and ONE COPY to: MONTH April YEAR Joe Ladd COUNTY: Franklin PHONE (919) 494-3001 ATTN: CENTRAL FILES x NIA DIVISION OF WATER QUALITY (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) 1617 MAIL SERVICE CENTER BY THIS SIGNATURE, 1 CERTIFY THAT THIS REPORT IS ACCURATE AND COMPLETE TO THE BEST OF MY RALEIGH, INC 27699-1617 KNOWLEDGE, 2014 DWQ Form MR -I (l 1/04) Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements (including weekly averages, if applicable) Compliant All monitoring data and sampling frequencies do NOT meet permit requirements Noncompliant The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by Part II.E.6 of the NPDES permit. " t certtty, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Randy Green _ Permittee (Please print or type) Si re of ittee*** Date (Required u ess submitted electronically) Permittee Address Phone Number e-mail address Permit Expiration Date Certified Laboratory (2) ADDITIONAL CERTIFIED LABORATORIES Certification No. Certified Laboratory (3) Certification No, Certified Laboratory (4) Certification No. Certified Laboratory (5) PARAMETER CODES Certification No. Parameter Code assistance may be obtained by calling the NPDES Unit at (919) 733-5083 or by visiting the Surface Water Protection Section's web site at h2o.enr.state. nc.uslw s and linking to the unit's information pages. Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. * No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR for the entire monitoring period. ** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204. *** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). Page 2 F�—Id Water Resources ENVIRONMENTAL QUALITY Mr. Rich Olofson Novozymes North America Inc. P.O Box 576 Franklinton, NC 27525 Dear Mr. Olofson: PAT MCCRORY rr,remor DONALD R. VAN DER VAART SvcrMnry S. JAY ZIMMERMAN May 2, 2016 Subject: Tax Certification for Pollution Abatement Equipment Real and Personal Property Tax Certification Number TCS-RH-230 Novozymes North America Inc. Franklin County As per your request, the staff of the Division of Water Resources have completed our review of the Tax Certification Request for real and personal property that we received from your office on March 29, 2016: PIease find attached a copy of Tax Certification Number TCS-RH-230 that has been issued by this office to Novozymes North America for the facility located in Franklin County. Please note that as part of this Tax Certification process the DENR staff did not make any efforts to confirm either the cost of the item(s) certified or the. year of acquisition. If there is a need for any additional information or clarification, please do not hesitate to contact Sonia Gregory at Sonia.gregory4nedenr.gov or 919-807-6333. Attachment Cc: File Copy Since ly, Jahn E. Hennessy,. Su Compliance & Expedited Permitting Unit Dimcror State of North Carolina I Environmental Quality I Water Resources 1617 Mail service Center I Raleigh, North Carolina 27699-1617 919 707 9000 �4 Water Resources ENVIRONMENTAL QUALETY North Carolina Division of Water Resources TAX CERTIFICATION NUMBER TCS-WI-125 In accordance with the provisions of the North Carolina General Statutes G.S.105-275.'(8) this is to certifv that Novozymes North America Inc, located at: 77 Perrys Chapel Church Road Franklin, NC 27525 Franklin County filed a request for tax certification for real and personal property covered under the Division of Water Resources Permit Numbers NCG500115, NCS000115, WQ0002806, and WQ0003487 Staff of the Division of Water Resources inspected these treatment units and/or equipment on February-22, 2016 and found based on the information supplied by the applicant that the facilities and/or equipment listed on the attached application meet the following requirements for Tax Certification: . 1. The property has been, or will be, constructed or installed; 2. The property complies with, or if still under construction will comply with, the requirements of the EMC; 3. The property is being effectively operated, or will when,completed be required to operate, in accordance with the terms and conditions of approvals issued by the EMQ and 4. The property has, or when completed will have, as its primary rather than incidental purpose the reduction of water pollution resulting from the discharge of sewage or waste. Please note that as part of this Tax Certification process the DEQ staff did not make any efforts to confirm either the cost of the items certified or the year of their acquisition. DATE TAX CERTIFICATION -ISSUED: May22016 cc: Tax Administrator, Franklin County Zentral Files Raleigh Office Files. il� E. Hennessy, Supers Aiance & Expedited Tax Certification Insaection Report Determination Facility:.............:...........................NQvozymer North America Inc. (Frankiinton) Tax Certification Number: .......................... TCS-RH-230 Inspection Date: ........................... ,...... Tin cAed o✓+ - (41 /A, oo►�p, ansfleclia,, y-ovl � ALL ITEMS LISTED QUALIFY FOR TAX CERTIFICATION: Yes No ❑ 1. Anaerobic Digester IC Reactor Qualifies? Yes No 2. Anaerobic Digester Sulfur Treatment Qualifies? Ye No Comments: e-N Lc 3. Anaerobic Digester Recirculation Tank Qualifies es) No Comments: a N '7a a rn f� 4. Anaerobic Digester Flare Qualifies? Yes No 5. Anaerobic Digester Pre Acidification Tank Qualifies? Yes No Comments: 6. Anaerobic Digester Raw Material System Qualifies? (Y ) No Comments: 'Fe- w 4d 57Z (?_ 7. Process Waste Water Clarifier Basin Agitator Qualif es? LYes No Comments: q8L SZI Ul File name: check list (00000002) Page No. 1 of 2 `4, Tax Certification Inspection Report Determination Facility:.......................................Novozymer North America Inc. (Franklinton) Tax Certification Number: ........................ TCS-RH-230 Inspection Date: ...................................... Tn c W OA Z-o z- Z 0110,P i 5"b"wedgy 0 ny�nb�t�N►>uc, 4,4r,- $, Process Waste Water, Pump FC098AP09 Qualifies? Yes No Comments: F Lo4O A P6C1 sz� 9. Process Waste Water Pump FC098AP10 Qualifies? No Comments: T C G q pd f)-4,;;- f 10. Process Waste Water Pump FEM98AP04 Qualifies? es Na Comments: Etw I!, A POW -0 Process Waste Water Pump FEM98AP05 Qualifies? Yes No 12. Process Waste Water Primary Clarifier Skimmer Qualifies? es No 13, Utility Building Qualifies? 6DNo -.n nliP/n 16- 14. Building FEN Qualifies? es No File name; check list (OON0002) Page No. 2 of 2 • RECEIVED ASHLAND�F4 1 1.2011 '.SAFETY DATA SHEEODET Raleigh ea anal oft BIOSPERSE® 261T MICROBIOCIDE ,67529 0 Page: 1 Revision Date: 02/21/2007 Print Date: 8/28/2007 MSDS Number: R0196831 Version: 13 I. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND OF THE COMPANY/UNDERTAIUNG,' Ashland Regulatory Information Number 1-800-325-3751 P.O. Box 2219 Telephone 614-790-3333 Columbus, OR 43216 Emergency telephone number 1-800-ASHLAND { 1-800-274-5263) Product name BIOSPERSE® 261T MICROBIOCIDE Product code 67529 Product Use Description No data 2. HAZARDS IDENTIFICATION Emergency Overview Appearance: solid, slight!chlorine, white Corrosive to skin, Corrosive to eyes. Potential Health Effectg Routes of exposure Inhalation, Skin contact, Bye Contact Eye.contact Can cause permanent eye:injury. Symptoms include stinging, tearing,. redness, and swelling of eyes. Can injure the cornea and cause blindness. Contact with dilute solutions (0.1 % or less) is not irritating to the eyes. Skin contact' Can cause permanent skin damage. Symptoms may include redness, burning, and swelling of skin, burns, and other. skin damage. Contact with dilute solutions (0.1% or -less) is=not irritating,.to the skin. Iagestlon. Swallowing this material may be harmful or fatal. Inhalation This material is a dust or may,produce dust. Breathing small amounts of this material during normal handling is not likely to cause harmful effects. Breathing large amounts maybe harmful. Prolonged or repeated breathing of dust may result in Page l 19 'Ar,DE K 6 aatei�l� 0(51a� ASHLAND SAFETY'DATA-SHEET BIOSPERSE_ ® 26IT MICROBIOCIDE 67529 Page: 2 Revision Date: 02/21/2007 Print Date: 8/28/2007 MSDS Number: R0196831 Version: 1.3 progressive and permanent lung disease {fibrosis) which may cause death from respiratory and/or heart failure. Symptoms include coughing and difficult breathing which -becomes worse with physical activity. Aggravated MedicaLCondition Preexisting disorders of the following organs (or organ systems) maybe aggravated.bj exposure to,this material:, skin, lung (for example, asthma-like�cnnditions) Symptoms Signs and symptoms of exposure to this material through breathing, swallowing, andlor passage of the material through. the skin may include:,, stomach or intestinal upset (nausea, vomiting, diarrhea), irritation (nose, throat, airways), lung irritation, respiratory depression (sIowing'of the breathing rate), damage to the mouth, throat, and/or airways, shock, convulsions, coma, and death Target Organs No data Carcinogenicity This material is not listed as a carcinogen.by the International Agency for Research on Cancer (IARC), the National Toxicology Program (NTP), or the Occupational Safety'and Health Aftinistration (OSHA). Reproductiveatazard. There are no data available_ for assessing risk to the fetus from maternal exposure to this material. Other information No data 3. COMPOSITIONANFORMATION ON INGREDIENTS Components CAS -No. Concentration 2,4-54IDAZOLIDINEDIONE, 1-BROMO-3- 16079-88-2. >=90-<-I00% CHLORO-5,5-MlETHYL- WATER 7732-18-5 >=2-<=6% 4. FIRST AID MEASURES. Eyes Paget/9 *tovv FSB1 ATV • ASHLAND SAFETY'DATA SHEET BIOSPERSE® 261T MICROBIOCIDE, 67529 Page: 3. Revision Datc: 02/21/2407 Print Date: 8/28/200.7 MSDS Number: R0196831 Version: 1:3 If material gets into the .eyes, immediately flush- eyes gently with water for at'least` 15. minutes.while holding;eyelids apart. If symptoms develop as a result�of vapor exposure, immediately move individual away from exposure and into fresh air before flushing as recommended above. Seek immediate medical attention. Skin Immediately flush skin.with water for at.least 15 minutes while removing contaminated clothing andshoes: Seek immediate medical attention. Wash.clothing before reuse and. discard contaminated`shoes. Ingestion Seek. immediate medical attention. Do not induce vomiting. Vomiting will cause further damage to the mouth and throat. If individual is conscious and alert, immediately rinse -mouth with water and give milk or water to drink. If possible, do not leave individual unattended. Inhalation If symptoms develop, immediately move individual away from exposure and into fresh air. Seek immediate. medical attention, keep person warm and quiet. If person is not'breathing,.begin. artificial "respiration. If breathing is difficult, administer oxygen. Notes to physician. Hazards: No'information available. Treatment: Probable mucosal damage•may contraindicate the use of gastric lavage. Measures against, circulatory shock, respiratory depression and convulsions may be needed. 5. FIRE -FIGHTING MEASURES Suitable extinguishing media water spray Hazardous combustion products May form:, bromine, chlorine, hydrogen bromide, hydrogen chloride Precautions for fire -fighting Substance is'an oxidizer that will cause moderate increase in the burning rate of combustible materials with which it comes into contact.Wearfull firefighting turn -out gear (fall Bunker gear)i and respiratory protection (SCBA).. Page 319- 0 �1►5HL AND SAFETY DATA SHEET BIOSPERSES 261T MICROBIOCIDE 67529 b. -ACCIDENTAL RELEASE `MEASURES Personal precautions No data Environmental precautions No data 0 Page: 4 Revision Date: 02/21/2007 Print,Date: 8/28/2007 MSDSNumber: R0196831 Version: 1.3 Methods W cleaning up Persons not wearing protective equipment should be excluded from area of spill' until clean-up'has been completed. Shovel material into containers. Thoroughly sweep area'of spill to clean up -any residual material. 7. HANDLING AND STORAGE Handling Containers of this material may be hazardous when emptied. Since emptied containers retain product residues (vapor, liquid, and/or solid), all hazard precautions given in the data sheet must be observed. Strong oxidizing agent. Mix only with water. Use cleani.dry utensils and,equipment. Do not.add this product to any dispensing. device containing remnants of any other product. Such use may cause a violent reaction leading to fire and explosion. Contamination with other, chemicals may start, a chemical reaction with generation of heat, hazardous gases and possible fire and explosion. In case of contamination or.decomposition,,do nct,reseal.,container. If possible, isolate container in open. air orwell-ventilated area. If.necessary, flood, with large volumes of water. Avoid creating and breathing dust. Use'dustless systems for handling, storage, and clean up so that airborne dust does not exceed the PEL. Use adequate, ventilation and dust collection. Practice good housekeeping. Do not permit dust to collection walls; floors; sills, ledges, machinery, . or• equipment. Storage Do. not allow moisture or water contamination of product. Do not store in temperatures above' 120 degrees F. Store in closed containers in a dry, well -ventilated area. S. EXPOSURE CONTROLS / PERSONAL PROTECTION Exposure Guidelines General advice Page 4 / 9 REGENtu FEB 1 1911 t4G DER Ra1e10 Re41011a1 flffi" 0 ASH«IVD.- SAFETY DATA SHEET BIOSPERSE®261T MICROBIOCIDE 61529 Page: 5 Revision Date: 02/21/2007 Print Date: 8/28/2007 MSDS Number: R0196831 Version: 1.3 These recommendations provide general guidance for handling.tiiis product. Personal protective equipment should be selected=for individual applications and should consider factors'which affect exposure potential, such as handling practices, chemical concentrations and ventilation. It�is.ultimately the responsibility of the employer to follow regulatoiy guidelines established'hy Incal authorities. Exposure controls Provide sufficient mechanical (general arid/of local exhaust) ventilation,to maintain exposure below TLV(s). Eye protection Chemical 'splash'rgoggles and face shield (8"',min.) in compliance with OSHA regulations are advised; however, OSHA regulations also permit other•type safety glasses. (Consult your industrial hygienist.) Skin and body protection To prevent skin contact, wear impervious clothing and boots:Wear resistant -gloves such as: Respiratory protection, If overexposure, has-been determined or documented, a NIOSH-approved air supplied respirator is advised in absence of proper environmental control. OSHA regulations also permit other NIOSH respirators under specified conditions. (See your safety equipment supplier.) Engineering or administrative controls should be implemented to reduce bkposute.. 9:'PHYSICAL AND CHEMICAL PROPERTIES Physical state Form Colour Odour Boiling, pointlrange pH Flash 09hat Evaporation rate Explosion limits Vapour pressure Vapour density Density Page 5/9 solid. tablet, White slight chlorine No data 3.5 No data < 1 N-Butyl.Acetate No data No data No data No data ASHLANI] SAFETY DATA SHEET BIOSPERSEO 261T MICROBIOCIDE 67529 :Solubility negligible in.water Partition coefficient {n= No data octanol/water) Autoignition,temperature No data 10. STABILITY AND REACTIVITY Stability Stable. Conditions to avoid None known. Page: 6 Revision Date: 02/21/2007 Print Date: 8/28/2007 MSDS Number: R0.196831 Version: 1.3 Incompatible products Avoid contact with:, ammonia, calcium hypochlorite, organic materials; reducing agents, strong alkalis, urea Hazardous decomposition products May,form:, bromine; chlorine, hydrogen bromide, hydrogen chloride Hazardous'reactions Product will not undergo hazardous polymerization. Thermal decomposition No data 11. TOXICOLOGICAL INFORMATION Acute oral toxicity 2,44MMAZOLIDINEDIONE, 1- LV50 Rat: 578 mg/kg SROMO-3-CHt.ORO,-5,5-DIMETHYL- Acute inhalation toxicity 2,44MIDAZOLIDINEDIONE, I- 9ROMO-3-CHLORO-5,5-DIMETHYL- Acute dermal toxicity 2,4-IMIDAZOLIDINEDIONE, I- $ROMO-3-CHLORO-5;5-DIMETHYL- P.age.6 / 9 •LC.50 Itat: 1.11 mg/I, 4 h LD 50 Rabbit: 2 g/kg ASHL.ANU Page: 7 SAFETY DATA SHEET Revision Date: 02/21/2007 Print Date: 8/28/2007 MSDS Number: R0196831 BIOSPERSE® 26IT MICROMOCIDE Version: 1.3 '67529 12. ECOLOGICAL INFORMATION Aquatic toxicity Acute and Prolonged Toxicity to Fish 96 h LC 50 Oricorhynchus. rityldss (iainbow trout), static test: 0.87 mg/1 96 h LC 50 Pimephales promelas (fathead minnow), static test: 2.25 mg/1 Acute Toxicity to Aquatic Invertebrates 48.h LC 50 DapMia magna (Water flea), static test: 0.48 mgn .Envirarimental fate and pathways No data 13. DISPOSAL CONSIDERATIONS Wastedisposal methods Dispose of in.dccordance with- all applicable local, state -and -fcdcral regulations. Do not discharge effluent:`containing this product into 1&6s,,streams,-ponds or estuaries,. oceans, or. other waters unless in . accordance with the requirements of a National PollutantDischarge- Elimination System' (NPDES) permit, and the permitting authority has heen•nntified in writing prior to discharge: Do not.discharge effluent.containing this. product to sewer systems without previously notifying the local sewage treatment plant authority. For guidance., contact your State Water -Board or Regional Office of the EPA. Improper:disposal of excess pesticide,; spray mixture, or rinsate is a violation of Feddral La*.' If "these wastes cannot be dispnsecl of by use according to label instructions, contact your State Pesticide:or Environmental. Control Agency or the Hazardous, Waste Representative at the nearest EPA Regional Office�fnr guidance. Do not contaminate water, food, or feed, by storage ordisposal or cleaning. of equipment. Do' not put product, spilledproduct; or filled'orpartially filled containers into, the trash or waste compactor. Contact with incompatible materials:codld cause a,reaction or fire. Do not reuse container. Rinse thoroughly before discarding in trash. For'assistance with your waste management needs - including disposal, recycling and waste stream reduction, contact Page 7 19 ASHLAND Page: 8 SAFETY DATA SHEET Revision Date: 02/21/2007 Print Date: 8/28/2007 MSDS Number: R0196831 BIOSPERSE® 26IT MICROBIOME Version: 1.3 67529 Ashland Distribution Company, IC&S Environmental Services Group at 800=637-7922. 14. TRANSPORT INFORMATION IMD.G: UN1479,. OXIDIZING SOLID, N.O.S. (BROMO CHLORO, DIMETHYLHYDANTOIN,.) 5.1, I1 IATA_P: UN1479; Oxidizing solid, n.o.s.(BROMO:CHLORO.DIMETHYLHYDANTOIN, IATA. C: UN1479, Oxidizing solid,-n.o.s_ (BROMO CHLORO DIMETHYLHYDANTOIN, ) 5.1, II CFR_ROAD: UN1479; Oxidizing solid, n.o.s. (BROMO CHLORO DIMETHYLHYDANTOIN, ) 5.1,11 CFR RAIL: UN1479, Oxidizing solid, n.o.s. (BROMO CHLORO DIMETHYLHYDANTOIN, ) 5.1,.11 CFR INWTR: UN1479, Oxidizing solid, n.o.s. (BROMO CHLORO DIMETHYLHYDANTOIN, ) 5.1, 11 Dangerous `goods descriptions may not reflect package_size, quantity, end -use or region - specific exceptions. that can be,applied.to shipments. Consult, shipping documents for material -specific descriptions. 15. REGULATORY INFORMATION California P "rap: 65 WARNING! This product'contai`ns a chemical known in.the State, of California. to cause cancer. BROMOFORM SARA Hazard Classification Acute Health Hazard SARA 313 Components) OSHA Hazards Page-8./ 9 Corrosive to skin 11P ASHLAND Page 9 SAFETY DATA SKEET Revision Date: 02/21/2007 Print Date: V28/2007 MSDS Numbcr: R0196831 BIOSPERSEO 261 T MICROBIOCIDE Version: 1:3 67529 Corrosive to "eyes Health Flammability Reactivity Other HMIS No data NFPA No data 6.OTHER INFORMATION The information, accumulated herein is -believed to be accurate but is not warranted to, be whether originating with the,company or.not. Recipients are advised to confirm in advance of need that the information is current, applicable, and suitable to their circumstances. This MSDS has been prepared by Ashland's Environmental Health and Safety Department (1-800-325-3751). lop eon°na Page 919 tavoon 2— Metals: Results in maR 2010 Cd cu Pb Ni Zn CI TDS March <.0036 <.015 <.019 <.018 1 0.168 170 2200 July <0.0036 <0.016 <0.019 <0.01 a 0.0959 300 2000 tlovember <0.0036 0.017 <0.019 <0.018 0.13 260 • e aan 2 Metals : Resuits in ma/i 2010 Cd Cu Pb Ni Zn cl TDS March <.0036 <.015 <.019 <.018 0.166 170 2200 .July <0.0036 <0.016 <0.019 <0.018 0.0959 300 2000 November <0.0036 0.017 K0.019 40:018 0.13 260 RECEIVED FEB 1 I IV NO DENR Saleigh90111,al(nee "„ -wiper Diagram, Stiff Diagram, D-;ov Plot and Other Water Chemistry Diagram Types in ... Page 2 of 3 http://www.rockware.com/product/gallery.php?id=150 3/31 /2011 -Piper Diagram, Stiff Diagram, D4v Plot and Other Water Chemistry Diwrn Types in ... Page 3 of 3 � f IT Durov Diagram Schoeller diagram Click on image to enlarge Click on image to enlarge i � I j g Series Plot Time Series Plot Click on image to enlarge Click on image to enlarge 1 Pie Chart Ion Balance Diagram Click on image to enlarge Click on image to enlarge y I r Radial Plot Click on image to enlarge p 2004 - 2011 RockWare, Inc, ESRI and ArcView are registered trademarks provided under license From Environmental Systems Research Institute, Inc. http,Hwww.rockware.com/product/gailery.php?id=l 50 3/31/2011 •Piper Diagram, Stiff Diagram, Dwv Plot and Other Water Chemistry Dram Types in... Page l of 3 v v 0 0 0 0 0 0 0 0 i 0 0 F 0 n Indus ■ Civil ■ Environmental ■ eote hnigal ■ Mining ■ Petroleum r CAD ■ Contouring ■ Educationa__l r GIS ■ ra hing/Plottin ■ Groundwater -Model ■ Maps/Topos ■ Math/ t ti gics Discipline r Geoloeical ■ Ge physics ■ Hydrology ■ Mfi rapes ■ Structural �T http://www.rockware.com/product/gallery.php?id=150 3/31/2011 Schoeller Plot 100.0 10.0 Cr N E p 1.0 , 0 U 0.1 - ------ 0.0 Ca Mg Na CI SO4 K Parameters DESCRIPTION: + Company PROJECT: PROJECT NO: y Logo CLIENT: DATE: Ternary Diagram Na do 80 ------------------------- ao 60------------------------- ---, ---------------------- �C�t�tf��PMl 10 40 ---------- ----- - 20 ;q Y ------•----•------- i60n K to �'o po 0 Ca DESCRIPTION: + Company PROJECT: PROJECT NO: ♦ Logo CLIENT: DATE: Ternary Diagram Mg ryo 80--------------------------- ao 60------------------------------------------- --- 40 --------------------- 20 r=-------------------------=� ��Vl0 1-- �o r479�G K `�o `'o Ca DESCRIPTION: + Company PROJECT: PROJECT NO: ♦ Logo CLIENT: DATE: Ternary Diagram mg/l 20 Cl DESCRIPTION: MCompany E Logo PO4 80 --------------------------ryo - 60 --------------------------- ------------- ------------- o 40 -------------------------- 'x., ------------------------------------------------------ Lagoon 2 DEC' +ag'olon 2 NOY L ---------- ---------- ------- ---------------------- -------------- own do' 00 �O vo� 1 -0 '4 0 WJ09111*0111003 CLIENT: I DATE: SO4 (.Sample Summary Site CT blowdown Location Geology Watertype Na-SO4-CI Temperature (°C) pH 5.7 Sum of Anions (meg11) 187.5 Sum of Cations (megll) 767.3 Balance 19.5 Total dissolved solids Total hardness 0.0 mgll CaCO3 Alkalinity 0.0 mgll CaCO3 Major ion composition mgll mmolll megll Na 67.3 2.93 2.93 K Ca Mg CI 58.6 1.65 1.65 SO4 123 1.28 2.56 NO3 HCO3 Ratios Comparision to seawater mgll mmolll mgll mmolll Ca/Mg 0.319 0.194 Ca1SO4 0.152 0.364 Na/Cl 1.15 1.77 0.556 0.858 Cl/Br 287 648 SI Calcite u DESCRIPTION: + Company PROJECT: PROJECT NO: ~ Logo CLIENT: DATE: Sample Summary Site CT blowdown Location Geology Watertype Na-Ca-SO4-CI Temperature (°C) pH Sum of Anions (meq/1) 249.2 Sum of Cations (meg/1) 343.7 Balance -31.5 Total dissolved solids 730 Total hardness 2.7 mg/I CaCO3 Alkalinity 0.0 mg/I CaCO3 Major ion composition mg/I mmol/I meq/1 Na 132 5.74 5.74 K 29.3 0.749 0.749 Ca 73.5 1.83 3.67 Mg 20.3 0.84 1.67 CI 100 2.82 2.82 SO4 140 1.46 2.92 NO3 HCO3 Ratios Comparision to seawater mg/1 mmol/I mg/I mmol/I Ca/Mg 3.62 2.20 0.319 0.194 Ca/SO4 0.53 1.26 0.152 0.364 Na/CI 1.32 2.04 0.556 0.858 Cl/Br 287 648 SI Calcite DESCRIPTION: + Company PROJECT: PROJECT NO: ♦ Logo CLIENT: DATE: Sample Summary Site outfall Location Geology Watertype Na-Ca-SO4-CI Temperature (°C) pH 1 Sum of Anions (meq/1) 211.1 Sum of Cations (meq/1) 1343.5 Balance -28.1 Total dissolved solids 600 Total hardness 2.1 mg/l CaCO3 Alkalinity 0.0 mg/1 CaCO3 Major ion composition mg/I mmol/I meq/1 Na 101 4.39 4.39 K 24.9 0.637 0.637 Ca 57.4 1.43 2.86 Mg 15.4 0.63 1.27 Cl 84 2.37 2.37 SO4 120 1.25 2.50 NO3 HCO3 Ratios Comparision to seawater mg/I mmolll mg/I mmolll Ca/Mg 3.73 2.26 0.319 0.194 Ca/SO4 0.48 1.15 0.152 0.364 Na/CI 1.20 1.85 0.556 0.858 Cl/Br 287 648 SI Calcite DESCRIPTION: + Company PROJECT: PROJECT NO: '� Logo CLIENT: DATE: Sample Summary Site lagoon 2 Location Geology Watertype K-Na-HCO3-CI-PO4 Temperature (°C) pH Sum of Anions (megll) 459.5 Sum of Cations (meq/1) 871.4 Balance -2.7 Total dissolved solids 2100 Total hardness 0.4 mg/l CaCO3 Alkalinity 3.8 mg/I CaCO3 Major ion composition mg/I mmolll meq/1 Na 60.5 2.63 2.63 K 282 7.213 7.213 Ca 13.35 0.33 0.67 Mg 1.23 0.05 0.10 CI 100 2.82 2.82 SO4 60 0.63 1.25 NO3 HCO3 230 3.77 3.77 Ratios Comparision to seawater mg/I mmolll mg/l mmol/i Ca/Mg 10.85 6.58 0.319 0.194 Ca/SO4 0.22 0.53 0.152 0.364 Na/Cl 0.61 0.93 0.556 0.858 Cl/Br 287 648 SI Calcite DESCRIPTION: + Company PROJECT: PROJECT NO: Logo CLIENT: DATE: Sample Summary Site Location Geology Watertype Temperature (°C) pH Sum of Anions (megll) Sum of Cations (megll) Balance lagoon 2 K-HCO3-CI 736.6 741.8 9.8 Total dissolved solids 2100 Total hardness 0.4 mg/l CaCO3 Alkalinity 7.7 mgll CaCO3 Major ion composition mg/1 mmolll megll Na 60 2.61 2.61 K 362.5 9.272 9.272 Ca 11.85 0.30 0.59 Mg 1.36 0.06 0.11 Cl 130 3.67 3.67 SO4 75 0.78 1.56 NO3 HCO3 450 7.37 7.37 Ratios Comparision to seawater mgll mmolll mgll mmolll Ca/Mg 8.71 5.28 0.319 0.194 Ca1SO4 0.16 0.38 0.152 0.364 Na/Cl 0.46 0.71 0.556 0.858 Cl/Br 287 648 SI Calcite DESCRIPTION: + Company PROJECT: PROJECT NO: '� Logo CLIENT: DATE: -Sample Summary Site Location Geology Watertype Temperature (°C) pH Sum of Anions (meq/1) Sum of Cations (meq/1) Balance Total dissolved solids Total hardness Alkalinity Major ion composition Na K Ca Mg Cl SO4 NO3 HCO3 Ratios Ca/Mg Ca/SO4 Na/CI Cl/Br SI Calcite lagoon 2 K-HCO3-CI 904.1 665.8 16.1 2100 0.4 mg/1 CaCO3 10.4 mg/I CaCO3 mg/I mmol/I meq/1 73 3.18 3.18 373 9.540 9.540 13.3 0.33 0.66 1.16 0.05 0.10 170 4.80 4.80 75 0.78 1.56 570 9.34 9.34 Comparision to seawater mg/l mmol/i mg/I mmolll 11.47 6.95 0.319 0.194 0.18 0.42 0.152 0.364 0.43 0.66 0.556 0.858 287 648 DESCRIPTION: + Company PROJECT: PROJECT NO: Logo CLIENT: DATE: • Sample Summary Site Location Geology Watertype Temperature (°C) pH Sum of Anions (megll) Sum of Cations (meqll) Balance Total dissolved solids Total hardness Alkalinity Major ion composition Na K Ca Mg Cl SO4 NO3 HCO3 Ratios Ca/Mg Ca/SO4 Na/Cl Cl/Br SI Calcite lagoon 2 K-Na-CI-HCO3 1058.7 1125.4 -18.4 0.8 mgll CaCO3 9.6 mg/I CaCO3 mgll mmolll megll 153 6.66 6.66 945 24.170 24.170 22.8 0.57 1.14 4.6 0.19 0.38 330 9.31 9.31 160 1.67 3.33 550 9.01 9.01 Comparision to seawater mgll mmolll mg/I mmolll 4.96 3.01 0.319 0.194 0.14 0.34 0.152 0.364 0.46 0.71 0.556 0.858 287 648 DESCRIPTION: + Company PROJECT: PROJECT NO: Logo CLIENT: DATE: Romanski, Autumn E t( -h From: Guyer, Shawn Sent: Friday, May 20, 2011 2:18 PM To: Romanski, Autumn Subject: Novozymes Autumn, You can access all of the information I just relayed over the phone through our database UI, Drinking Water Watch (DWW). As I mentioned, Franklin County Water and Sewer (FCWS), the supplier of water, purchases water from three surface water systems: Henderson -Kerr Lake Regional Water System, the Town of Franklinton, and the Town of Louisburg. The area of the County where Novozymes (Novo) is located is predominantly served by Franklinton and Louisburg. Currently, FCWS is in some kind of contractual dispute with the Town of Franklinton and is not actively purchasing water from them. Louisburg is likely the predominant source of water for Novo at this time. You can access Louisburg's monitoring data via DWW above. I) Click on the link to DWW. 2) Search for "Louisburg" or the PWSID: 0235015. 3) In the results list, select the link to the left of the name NCO235015. 4) Amidst the links at the top of the screen, 3rd column t the right, 2ad link from bottom, click on Other Chemical Results by AnaI,L. 5) Select the number to the left of the analyte of your choice. 6) The next screen should show all recorded samples, select the date of choice and view results. Call if you have any more questions or would like contact info for FCWS. Shawn Shawn F. Guyer, P.E. Environmental Engineer Raleigh Regional Office Public Water Supply Section Division of Environmental Health NC Department of Environment and Natural Resources www.deh.enr.state.nc.us/pw 919.791.4299 (direct) 919.605.6016 (mobile) 919.788.5349 (fax) Shawn.Guyer@ncdenr.gov E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be disclosed to third parties. Romanski, Autumn From: Zhang, Cheng Sent: Thursday, January 13, 2011 11:09 AM To: Romanski, Autumn Subject: FW: Novozyme FYI From: Wrenne Kapornyai[mailto:wkapornyai@franklincountync.us] Sent: Thursday, January 13, 2011 11:07 AM To: Zhang, Cheng Subject: RE: Novozyme No they have not resumed discharging and will not until their permit has been modified. Wrenne From: Zhang, Cheng [mailto:cheng.zhang@ncdenr.gov] Sent: Thursday, January 13, 2011 10:40 AM To: Wrenne Kapornyai Subject: Novozyme Wrenne, A quick question: Has Novozyme resumed discharging wastewater to Franklin County WWTP? If yes, when? Thanks, Cheng Zhang Environmental Specialist NCDENR- Raleigh Regional Office Surface Water Protection 1628 Mail Service Center Raleigh, NC 27699-1628 Office (919) 791-4259 Fax (919) 788-7159 E-mail correspondence to and from this address may be subject to the North Carolina Public Records Caw and may be disclosed to third parties. NC Division of Energy, Mineral and band Resources NPDES Stormwater Permit Contacts Summary ISV I)F INI I,R has the foliois in a contact information in our Permi Datahare forvogr permit as of 2I1312f118. Permit Number: NCSOD0115 Permit Type: Stornnvater Discharoc.Jgivldu.I facility Name: N...sLv44=0911hArmrka Facility Addressl: %Lftiy bAkQl Q=LU Facility Address2: City, State & Zip: Eranklint4Ll Z►C 27525-0576 Owner Name: NOvti. Me514=b America Inc Owner Type: h!Qn-Government Owner Type Group. fZrganizatlnn Owner Affiliation: jam Manme Title: E _-fA Addressl: 77 PrrryDaoel Church Rd Address2: City, State & Zip: Frankiinton. NC 275X5--Q5-7h Work Phone: 9�- # V"' Fax: 919 a94 345D Email Address; Billing Month: August +uwsar? tmr��m�mtisr�ssmmam:�r�� r�r " { �' � @ � � �#"' �Y E Owner,,Contact;t?ersolw{s1` ' � $1 3 �`;�Fti>;:'MU€ai1IR ,1`i.3 € PIRI s ��i�eli73` i�:i6; s4:!d1,01,I<; I :a.,� #tliil;;33 €��Iffii�;1i1;; Contact Name rft Address. p g EON f1Illj rM ✓ Address Phone E" Randy Green Ln,y�isn sw}sF �O{So77 perryChapel Church Rd, PO Box 576, 919-494-3001 919.494-3458 rwgr@novozymes.co Franklinwn NC 27525-0576 m Joe Ladd 77 Perry Chapel Rd, Franklinton, NC-,G9,..a3d 2fi1]L. ,/ r"n %! a CeVV71;#44 # e I,7Z© rrVA..4e,77J675-0576 4 i9 - kg V —3117 6 _ -_- -,x„ .J L b C1 l0 h1Quo?-i P,errn�t,Contact�Person(s . �r �� t ' �" Contact Name rft Addres Ehon1 Email ve A EI%%f•+f6A „'�ti��1 PO Sox 576, Frankllnton, NC 27525-0576 919 494 3�00 / J �1 Con Sta elman a '3t�0 is —� trzs/a.DzB �Jf„ PO 80V pj.c�vr S3 - e jFta''� a� 9 Page 1 NC Division of Energy, Mineral and Land Resources NPDES Stormwater Permit Contacts Summary NC 1}i•:N11.R has the fallorrina Contact informaliun_in our Permit Dutahase_for --our permit as of 2/1312018. Permit Billing Contact '; !r, ;: � ::- ,. • . ' ,� „ .6 Contact Name title Adores£ Phone FBA Email Randy Green EnI . R t*+Qasd" PO Box 576, Fro nklintcn, NC 27525-0576 3G, o TI?O toIqV` 3 u' �3� lqq .2 Nova-ayrus TS iv Arl 4j .41V cl� 4 (.A� Ler(-e� -ew-4 t 4 N, J C4\A !L-- Lp C�d cov lo ccefi m 14 S� C4to ID gum 0-,d 06 3 --o as Suva v, Tm r6l 0,30070101 W _T _ a,r 0 Sp )ilt,,c 814�� Crtek is' LyKo&jrj 'bv'v4 Far- Pam 14 a(V 7 -S IA bGd i 11 ol -0 3 - 0 1 f! C-ACJVI� )I,% -rC4'f- Pa4V) MAW � J-e IN tutu 4 pqs-;4') 046t doikU sjot.�r, M*-Ai JV6 X6 (,4 1 4v j t v; CAJOIg CitiA yj J 3 J lda�ls S" 03 yz Lie lv� A SE' r t S. tpe eZ. d�4-4 a 4&,J rs o are A 5171-4d. - lqqq Lim t-,z 3 t; kz, kl'-- VI J wv� N L 14 r;$ample Qate .; Outfall # -= Parameters:Sampled ; . _ = ` ==--Lab;Results ... _- = W Storm Event Qata 11T1/2012 ' #1 - BOD; COD, TSS, TKN, NO2/NO3, SOD: 79.0, COD: 250.00, TSS: 75.01 Sample Time: 1450, pH: 7.8, Rainfall Total Phosphorus" TKN:`J9, N021NO3: 0.53, Total P:'0.330_ Total@.Time of-Sampling:.3" . . 1/11/2012 1 #2 BOD, COD, TSS, TKN, N021NO3, BOD: 13.00, COD: 110.00, TSS:-'kb, Sample Time: 1520, pH: 7.4, Rainfall Total Phosphorus TKN: 1., N021NO3: 0.39, Total P:.330 Total@ Time of Sampling:.3" 12/26/2012 #1 BOD, COD, TSS, TKN, NO2/NO3, BOD: 5.3, COD: 59.00, TSS: 19.0, TKN: Sample Time: 1705, pH: 6.2, Rainfall Total Phosphorus .95, N021NO3: 0-25, Total P: 0.83 Total@ Time of Sampling: 0.3" 12/26/2012 #2 BOD, COD, TSS, TKN, NO2/NO3, BOD: 2.50, COD:-46.00, TSS: 74.00, Sample Time: 1720, pH: 6.1, Rainfall Total Phosphorus TKN: 0.99, N021NO3: 0.44, Total P:.30 Total@ Time of Sampling: 0.3" 2/26/2013 #1 _ -BOD COD, TSS, TKN N021NO3,:. BOQ; 3 00'; COQ 43:OQ, TSS 45 Q; TKN: SampleTtme 350, pH 7 2 _Rainfall w :; Total Phosphorus ''` 0.89;�N021NO3. 0.02, Total P..0 320 - Total Time of-Samplinga0 75'. _ W ,v >2126/2013 -.' _ _#2 B0D,_COD, TSS, TKN; NO2lNO3 BOD:3 70;_-COD 60 00, TSS &00 Sample Time: -.A 300 pH 7 8; _Rainfall: - _ = TotalPhosphorus - x'`= TKN:O.7fi N021NO3:€0.02, TotalP:-.097 - Total Time of Sam9: plin Q75" - 11/26/2013 #1 } BOD ,COD;_TSS TKN NO2/NO3 : BOD -4 2, -COD 57;0, TSS:-74 0, TKN Sample Time 1500, pH 6'6 Rainfall. - Total=Phosphorus _ �_._ 1.20"N021NO3. 1.1VTotal P_..250 r� .° Total Time of.Sampling. U 5" g ` - BOD -COD, TSS TKN :NO2/NO3 BOD:=S 10,' COD 36:0; TS5:.9 6 _-TTKN: mm Sample'Ttme 1520; pH 6 6 Rainfall:— 11/26/2013 _ Total Phosphorus •--: D.56;,N021NO3. 0.15,TotaGP .0:240 T6619 Time+of:Sam lin90!5'' - P � 4/7/2014 #1 BOD, COD, TSS, TKN, NO2/NO3, BOD: 6.1, COD: 45.00, TSS: 14.0, TKN: Sample Time: 0850, pH: 7.6, Rainfall Total Phosphorus 1.1, N021NO3: 0.61, Total P: 0.280 Total@ Time of Sampling: 1.0" 4/7/2014 #2 BOD, COD, TSS, TKN, NO2/NO3, BOD: 12_00, COD: 55.00, TSS: 39.0, Sample Time: 0920, pH: 6.0, Rainfall Total Phosphorus TKN: 1.6, N021NO3: 0.52, Total P:.280 Total@ Time of Sampling: 1.0" 12/9/2014 #1 BOD, COD, TSS, TKN, N021NO3, BOD: 3.5, COD: 54.00, TSS: 120.0, TKN: Sample Time: 1545, pH: 8.9, Rainfall Total Phosphorus 1.00, N021NO3: 0.41, Total P: 0.300 Total@ Time of Sampling: 0,25" 12/9/2014 #2 SOD, COD, TSS, TKN, NO2/NO3, BOD: 2.00, COD: 12.00, TSS: 1.00, TKN: Sample Time: 1300, pH: 7.8, Rainfall Total Phosphorus 0.30, N021NO3: 0.08, Total P:.250 Total@ Time of Sampling: 0.75" _312712015 .__ #1 :.--BOD _COD;:TSS TKN; N021NO3 _; 60D:=15 00; COp :44.00; TSS 38:0 _ -.. Sample Time -.1150, pH 8 O'Rainfall - - 4 _- - _ _ _ = Total PH63phorus - - TKN. 1' 80; N021NO3: 4 5; Total P: 0A80 Total Thi ew Sampling. 0:3' - *51112D15 .:. _. #1 .. ,: TSS TSS: =. Sample Time: 0900 - -*71312015 #1 TSS'= - TSS: 14 = Sample Time: 1150 " #1 BOD COD, TSS, TKN, NO2/NO3, SOD: 2.8: COD: 25,00, TSS: 39:0, TKN: Sample Tie: 0940, H: 8.4 Rainfall p p .811/2015 _ - TotaE Phosphorus = 84, NO2IN03.87, Total P: 0.40 Total@ Time of'Sam ling:A." BOD, COD, TSS, TKN, NO2/NO3, . SOD: 5.3,. COD: 49.00, TSS: 93.00, TKN: Sample Time: 0920, pH: 8.9, Rainfall 8/1/2015 92 :-Total Phosphorus .72, NO2►NO3:.41, Total P: 0.20 Total@ Time of Sampling: V' 4/12/2016 #1 BOD, COD, TSS, TKN, N021NO3, BOD: 3.6, COD: 14.00, TSS: 15.0, TKN: Sample Time: 0900, pH: 8.2, Rainfall Total Phosphorus 1.0, N021NO3; 0.90, Total P: 18.0 TotaQ Time of Sampling:.5" BOD, COD, TSS, TKN, NO2/NO3, BOD: 73.00, COD: 190.00, TSS: 17.0, Sample Time: 0935, pH: 7.9, Rainfall 4/12/2016 #2 Total Phosphorus TKN: 6.7, NO2/NO3: 0.11, Total P:.16 Total@ Time of Sampling:.5" 12/6/2016 #1 BOD, COD, TSS, TKN, NO2/NO3, SOD: 3.0, COD: 30.00, TSS: 30.0, TKN: Sample Time: 1330, pH: 8.3, Rainfall Total Phosphorus .59, N021NO3- 0.2, Total P: 0.500 Total@ Time of Sampling: 0.5" 12/6/2016 #2 BOD, COD, TSS, TKN; NO2/NO3, BOD: 33.00, COD: 130-00, TSS: 13.00, Sample Time: 1440, pH: 7.5, Rainfall Total Phosphorus TKN: 2.2, NO2/NO3: 0.19, Total P:.100 Total@ Time of Sampling: 0.5" 3/14/2017 =.. #1 BOD, COD, TSS, TKN, NO2/NO3, SOD: 2.90, COD: 30.00, TSS: 11.0, TKN: Sample Time: 1100, pH: 6.6, Rainfall Total Phosphorus 1.0, N021NO3: 1.10, Total P: 0.20 Total@ Time of Sampling: 1 "5" .3/14/2017'_ #2 BOD COD, TSS, TKN, NO2/NO3, SOD: 1S.00; COD: 4100, TSS:`2.5, TKN: Sample Time: 1000, pH: 6.8,`Rainfall - Total Phosphorus 0.6, NO2/NO3: 0.16, Total P:.025 ' Total 'Time of Sampling: 1.5" *4/2312017 #2 BOD, COD BOD: 3.3, COD: 28.0 Sample Time: 1500 '5/23/2017 #2 BOD, COD BOD: 5.40, COD: 58.0 Sample Time: 1430 01612017 #1 BOD, COD, TSS, TKN, NO2/NO3, SOD: 5.0, COD: 27.00, TSS: 32 0 TKN: Sample _Time: a1300, pH:_7.2,.Rainfall :1;., a=tlTotal Phosphorus 1.1, N021NO3:.09, Total P: 0.40 Total@ Time of Sampling:.5" BOD, COD, TSS, TKN, N021NO3, BOD: 49.00, COD: 96.00, TSS.`25:0,. Sample Time:°1230; pH 6.9, Rainfa[I" W 10/6/2017m,_ -. #2 " Total Phosphorus _ _ TKN: 2.0, NO21NO3: 0.81, Total P:.40 d _ . Total Time of Sampling... " ,.-Due to exceeded Benchmark in TS, —(2015 sample collection), and BOD and COD, (2017 collection) samples were collected on consecutive months for a Wat �tr, .?x� - SJ YkWff sMV�j bN Fitt- 0`'7 -AW! 11r hod i Col L-1 -10 IG. -701'1 da , - l 0 a�leeJan�rS... d� . c�ak �n4 itia ./ D L I f 5 �.s �j�l Go Ntrr tad � � wri- 3 • • • D "`i NC Division of Energy, Mineral and Land Resources Review of Permit Renewal — NCS000115 Novozymes North America SIC 2869 — Industrial Inorganic Chemicals - Enzymes Monitoring — The facility has been monitoring for BOD, COD, TSS, TKN, NO2/NO3, TP and pH. Previous permit did have tier system (2 tiers) o Since 2012 the facility has had three exceedances of BOD and COD and one TSS exceedance. Had exceedances at each of their two outfalls, but not at the same event. BOD and COD exceedances in consecutive events in 2016. Fallowing increased monitoring below benchmark. o Other parameters — no benchmark exceedances. o Maintain BOD, COD, TSS and pH in this permit. o Tier structure adjusted to have the three levels in current permits. o VM monitoring changed to be consistent with current permits. o Parameter codes added to permit. Buffalo Creels 28-22 in the Tar -Pamlico River Basin. 2014 Assessment Report shows no listing for this stream segment other than the statewide Hg listing and this facility has no indication of Hg source. Basin is NSW, but facility monitored for nutrient parameters since 2008 with no benchmark exceedances. NSW TMDL does not set any specific requirements for these facilities outside of new construction needing stormwater control through the local government and protection of any onsite stream buffers. NC National Heritage review — no record of any species or communities of concern within a one mile radius. See attached letter. RRO —Thad Valentine inspected the site on 3/8/2018. Based on their review no concerns were indicated for issuance. Thad did raise the question of whether vehicle maintenance applied if equipment maintenance was done outside. Provided response to Thad on this question. Facility also asked about discharge to impaired waters. It is in Tar -Pam NSW so no additional restrictions at this pointgigiven the measures already in place. Oq WATF, Permit Coverage g Renewal application Form i National Pollutant Discharge Elimination System Permit Number Stormwater Discharge Permit NCS000115 The following is the information currently in our database for your facility. Please review this information carefully and make all corrections/additions as necessary in the space provided to the right of the current information. Owner Affiliation Information *Reissued Permit will be mailed to the owner address Owner / Organization Name: Novozymes North America Owner Contact: Randy Green Mailing Address: PO Box 576 Franklinton, NC 27525 Phone Number: 9l,4l L494 -30c Fax Number: ' E-mail address: 9W6KQ novaZgMeS •CM AQuozypAe-<..c�om Facility/Permit_ Contact Information Facility Name: Novozymes North America Facility Physical Address: 77 Perry Chapel Church Franklinton NC, 27525 Facility Contact: tt xreen E Mailing Address: i� PCr 1�uPe f Chct,+C �0� . j ss Phone Number: 91Q yqCJ -3GG j Fax Number: } E-mail address: Discharge Information Receiving Stream Buffalo Creek (South Side Tar River) Stream Class: WS-IV; NSW Basin: Tar -Pamlico River Basin Sub -Basin: 03-Q3-01 Number of Outfalls: Co lj Impaired Waters/TMDL Does this facility discharge to waters listed as impaired or waters with a finalized TMDL? ❑ Yes VNo ❑ Don't Know ( for information on these waters refer to http://h2o.enr.state.nc.usIsulImpaired WatersTMDL1 ) bcof(Palo Grcek- 15 /161 hskd 61 SOR Impa"tcd Wa4r : 15ala(6 6-eek, o(l saa-4na 40'U'e- -far 1 ucr-, ic) )s hs)d Q,E a _D/ra4 2d/Z Ivaf,-cGi Wal r 0ed reY,43 )e )4e �JC ltMpairyj tja)itS � TIn DL Ap Q cees-<eot o-i. Jurie a ), 201;2- CERTIFICATION I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief such information is true, complete and accurate. Signature Print or type name of person signing above Please return this completed renewal application form to: Date A, t, Title Stormwater Permitting Unit Attn: Brian Lowther 1617 Mail Service Center Raleigh, North Carolina 27699-1 �WR D AUG-T2012 a DENR - WATER QUALITY "ands 8 5tor, nwrto= a. SUPPLEMENTAL INFORMATION REQUIRED FOR RENEWAL OF INDIVIDUAL NPDES STORMWATER PERMIT Two copies of each of the following shall accompany this submittal in order for the application to be considered complete: Initials (Do not submit the site Stornwater Pollution Prevention Plan) 1. A current Site Map from the Stormwater Pollution Prevention Plan. The location of industrial activities (including storage of materials, disposal areas, process areas and loading and unloading areas), drainage structures, drainage areas for each outfall, building locations and impervious surfaces should be clearly noted. 2. A summary of Analytical Monitoring results during the term of the existing permit (if your permit required analytical sampling). Do not submit individual lab reports. The summary can consist of a table including such items as outfall number, parameters sampled, lab results, date sampled, and storm event data. H 3. A summary of the Visual Monitoring results. Do not submit individual monitoring reports. The summary can consist of a table including such items as outfall number, parameters surveyed, observations, and date monitoring conducted. 4. A summary of the Best Management Practices utilized at the permitted facility. Summary should consist of a short narrative description of each BMP's in place at the facility. If the implementation of any BMP's is planned, please include information on these BMP's. 5. A short narrative describing any significant changes in industrial activities at the permitted facility. Significant changes could include the addition or deletion of work processes, changes in material handling practices, changes in material storage practices, and/or changes in the raw materials used by the facility. 6. Certification of the development and implementation of a Stormwater Pollution Prevention Plan for the permitted facility (Sign and return attached form). If the final year analytical monitoring of the existing permit term has not been completed prior to filing the renewal submittal, then the last years monitoring results should be submitted within 30 days of receipt of the laboratory reports. (i.e. do not withhold renewal submittal waiting on lab results) ,�&s ' STORM�V�AT=ER P®LYLUTIO�N PtREV�ENTION PLAN DEI�ELOPM°ENTA'1DA IlVIPrLEMENTATION_ �. .0 a . 4 { j n xl1 [6 ns r u i aa+ .. rE'I'IC�ION a : North Carolina Division of Water Quality - Stormwater Permitting Unit Facility Name: Novozymes North America Permit Number: NCS0001 i 5 Location Address: 77 Perry Chapel Church Franklinton NC, 27525 County: Franklin "I certify, under penalty of law, that the Stormwater Pollution Prevention Plan (SPPP) document and all attachments were developed and implemented under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information required by the SPPP. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information gathered is, to the best of my knowledge and belief, true, accurate and complete." And "I certify that the SPPP has been developed, signed and retained at the named facility location, and the SPPP has been fully implemented at this facility location in accordance, with the terms and conditions of the stormwater discharge permit." And "I am aware that there are significant penalties for falsifying information, including the possibility of fines and imprisonment for knowing violations." j'1L'�iMi1;!1T!1!j.!�i "III �',Inl :II hi . ,: dlll' :III 1"hIII .. "ia'I n . ,.II'!Ili i:ll! it l' 9 h1'1'.. ''1,.i. III "d Ali Il i,i� _" .ul l h :'l!I l 11 Ili r 'll Sign (according to permit_signatory requirements) and return this Certification. DO NOT SEND STORMW,'ATERIiPOLL::.UTION,,P:. R,EVENTION..P,L..AN�WITH THISI,AT,ION Signature or type name of person signing above Date /,0 Title SPPP Certification 5/09 l �1 e� WA L"RSi _u L.AY2,T LC- GATION IMPEF\IOJS AREA T07 AL_AREA F.AT10 AREA 1 7.003 i6e.li3 04, AREA Z 7.1u0 11C,0'30 .059 A F e A _ 33.17o 47,795 on5 AREA 4 52",53C 1,000,c?% AREA 5 246,780 524.70D .470 TOTAL J 815,553_ _- 1,858,478 .438 LEGF D: AREA 1 3 AREA 4 AREA 5 GAJCs F 9 194' 24p' 39[7' t"=199' t-1':-M PFi �» Fl<NSED L� FlElFi L'C41MEI.lS 1�1 S.i FCp W� PiF.v:T NZNA FAA r� SITE MAP FOR STORM WATER PERM![ DRANACE AREAS AND IMPERVIOUS SERFACES °'" FAA30806 c c a � � 0 j CS 2S OD i y!�o C L C C F F G F F G F r i A i i A Z d i A A # A %% i i i% f i i 1 i d 1■ O N a A A A A g�&a>aaa>a>aa�>a>a$�a�>aaa>aaa&a>>a''°aaa>aaa>�aa$aa�aa�aayaayaay&aaaaaaaaaaaa>a>aayaa;g 3333i333�3a)j>aja�aT��T ;�ij> �ygy��; ��y�T�T;a�>la;�jaa;�a?{t3t��ti!t' •�. 3;3> >) 3 3 �.>f. . i;I i 4 ; > >3;> �r33L L(LLrL �. 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BRIG '-slap, w_ mr r�s{ 1I I IEr 51 rs, A Rs-n was DIIAE/16 [ = f1rRP.OI 7ryN 53125.W —51 w �� r..R m ' m-4 I� -6 13 n. I P 47 � w � os-44 f ' F I I O 2 os I -A - Ps-_ 5¢ tRA I �n wR�e—f I _ C I �❑ �.u.� 7 -�„ I-T--_T x F� H I J a N s? L N s - j a 1 STORM SEWER SYSTEM OVERALL SITE PLAN 0 100' 2D0' 3OW iiiiiii I100'-D- ++c-.+ ro ERs7. E>f...Rl . sz7,ano: ..ivnaoox NNTES: i. PERMIT NO. NCS000115 2. SEE DRAVANG FAA33406 FOR STORM DRAINAGE DETAILS. REFERENCE DRAWINGS: FAA32031 FAA32032 FAA32033 FAA32034 FAA32035 MK32005 b TAI RAWIN S: FAA32067 - SITE DETAILS FAA32068 - MISCELLANEOUS DETAILS FAA32071 - DRIVEWAY DETAILS FAA32072 - TYPICAL DETAILS SHEET 1 FAA32073 - TYPICAL DETAILS SHEET 2 FAAM74 - TYPICAL DETAILS SHEET 3 FAA32075 - TYPICAL DETAILS SHEET 4 LEGEND I 512.5 SPOT ELEVATION 512.60 TP TOP OF PAVEMENT ELEVATION 512.50 TC ' TOP OF CURB ELEVATION STANDARD CURB AND GUTTER DRAINAGE INLET AND PIPING STORM DRAINAGE YATH FLARED END SECTION GS65 DRAINAGE STRUCTURE IDENTIFIER DRAINAGE STRUCTURE LOCATION P.T, I FLARED END SECTION W4TH R1P-RAP - - - DIRECTION FLOW FOR SWALE —CL— CLEARING LIMITS QUAD A WAD $ FAA33402 FAA33403 .QUAD C 141UAD D FAA33404 FAA33405 KEY PLAN 9 L- s-11 P E RIIC 4 m m F! W006]!4 B 6-2rw 4M YYHp REWn PVt WO •EMT ! SODOR304 7 6-2--0= PIPE .Iwo A4RIO,m rwm 'rW RaR Tw GEIAw Tra[ Px0¢r IGI Y]r I2 TIE Rr REv® PER w 5=oeg2 • ]pp=DlS Rw R... Wt.: or9 R.N_. — - — sow. Pm. ,m, _ - s7. — _ - - r. W.) -_ E.c 4REr 7/2E/E6 NZNA FAA w STORM SEWER SYSTEM rs .uan OVERALL SITE PLAN EMR.P nR: Via. _ FAA334Q1_ FAA334Q1 Analytical Monitoring Results Summary Sample Date Outfall # Parameters Sampled Lab Results (MG/0 Storm Event Data BOD, COD, TSS, TKN, NO2/NO3, B0D:3.5 COD:20 TSS:50.0 Sample Time: 1800 pH: 6.5 Rainfall Total @Time of 5/18/2008 #1 Total Phosphorus, TKN:0.71 NO2/NO3:0.49 Total Sampling: 0.3" P:0.46 BOD, COD, TSS, TKN, NO2/NO3, 80D:5.1 C00:13 TSS:7,2 5/18/2008 #2 TKN:0.78 NO2/NO3:0.33 Total Sample Time: 1810 pH: 6.8 Total Rainfall: 1.2" Total Phosphorus P:0.33 80D, COD, T55, TKN, NO2/NO3, BOD:5.2 COD:78 TSS:75 Sample T}me: 0900 pH: 8.3, Rainfall Total @Time of 1/6/2009 #1 Total Phosphorus, TKN:1.1 NO2/NO3:0.31 Total Sampling: 0.3" Total Rainfall:0.5" P:0.52 BOD:2.7 COD:41 TSS:51 1/29/2009 #2 BOD, COD, T55, TKN, NO2/NO3, TKN:1.2 NO2/14103:0.23 Total Sample Time: 1600 pH: 8.2 , Rainfall Total @Time of Total Phosphorus, P:0 05 Sampling: 0.2" Total Rainfall: 1.1" BOD, COD, T55, TKN, NO2/NO3, BOD:4.7 COD:41 TSS:14.0 Sample Time: 2150 pH: 6.3 Rainfall Total @Time of 5/5/2009 #1 Total Phosphorus, TKN:1.2 NO2/NO3:0.97 Total Sampling: 0.2" PA18 BOD, COD, T55, TKN, NO2/NO3, BOD:6.6 COD:55 TSS:13.0 5/5/2009 92 TKN:1.2 NO2/NO3:0.16 Total Sample Time: 2140 pH:7.9 Total Rainfall: 1.3" Total Phosphorus, P:0.17 BOD, COD, TSS, TKN, NO2/NO3, BOD:2.0 CM31 TSS:17 Sample Time: 1330 pH: 5.8 Rainfall Total @Time of 12/2/2009 #1 Total Phosphorus, TKN:0.18 NO2/NO3:.051 Total Sampling: 0.15" P:.032 BOD:3.8 COD:35 TSS:82 12/2/2009 #2 BOD, COD, TSS, TKN, NO2/NO3, TKN:.78 NO2/NO3%31 Total Sample Time: 1346 pH:6.4 Total Rainfall: 1.0" Total Phosphorus, P: 32 BOD, COD, TSS, TKN, NO2/NO3, BOD:16 COD:51 TSS:61 Sample Time: 2010 pH: 8.8, Rainfall Total @Time of 5/22/2010 #1 Total Phosphorus, TKN:1.9 NO2/NO3:.47 Total Sampling: 0.2" P:.62 BOD, COD, T55, TKN, NO2/NO3, BOD:4.9 CODA4 *TSS:120 5/22/2010 #2 TKN:0.99 NO2/NO3:.28 Total Sample Time: 2020 pH: 6,7 Total Rainfall: 1.2" Total Phosphorus, P:.25 BOD, COD, T55, TKN, NO2/NO3, BOD:27 COD:72 TSS:14 Sample Time: 1150 pH: 7.1 Rainfall Total @Time 12/12/2010 #1 Total Phosphorus, TKN:2.2 NO2/NO3:0.46 Total of Sampling- 0.5" P:0.37 B013:5.1 COD:87 `TSS:170 12/12/2010 42 BOD, COD, TSS, TKN, NO2/NC3, TKN:1.0 NO2/NO3:0.38 Total Sample Time: 1215 pH: 6.8 Total Rainfall: 1.0" Total Phosphorus, P:0.51 '3/6/2011 #2 T55 TSS: 15 SampleTime:1310 pH: n/a Rainfall Total @Time of Sampling: 0.3" Total Rainfall: 1.0" Sample Time: 1000 pH:n/a Rainfall Total *4/5/2011 #2 T55 TSS: 5.0 @Time of Sampling: 0.5 " Total Rainfall: 1.0" BOD, COD, T55, TKN, NO2/NO3, BOD:24 COD:100 TSS:55.0 Sample Time: 1610 pH: 7.2, Rainfall Total @Time 5/27/2011 #1 TKN:4.3 NO2/NO3:0.57 Total Total Phosphorus, of Sampling: 0.5" P; 0.88 BOD, COD, TSS, TKN, NO2/NC3, BOD:7.7 COD:70 TSS:5,0 5/27/2011 #2 TKN:1.3 NO2/NO3:00.07 Total Sample Time: 1640 pH: 6.9 Total Rainfall: 1.0" Total Phosphorus, P:0.04 80D, COD, T55, TKN, NO2/NO3, BOD:3.5 CM20 TW50.0 Sample Time: 11:10 pH: 8.2, Rainfall Total @Time of 11/16/2011 #1 Total Phosphorus, TKN:0.71 NO2/NO3:0.49 Total Sampling: 0.6" P;0,46 BOD:3.5 COD:20 TSS:50.0 11/16/2011 #2 BOD, COD, TSS, TKN, NO2/NO3, TKN:0.71 NO2/NO3:0.49 Total / Sample Time: 11:30 pH: 7.9 Total Rainfall: 0.8" Total Phosphorus, P:0.46 BOD, COO, T55, TKN, NO2/NO3, BOD:79.0 COD:250.0 TSS:75.0 Sample Time: 1450 pH: 7.8, Rainfall Total @Time of 1/11/2012 #1 Total Phosphorus, TKN:0.79 NO2/NO3:0.53 Total Sampling: 0.3" P:0,33 BOD:13.00 COD:110 TSS:99.0 1/11/2012 #2 BOD, COD, T55, TKN, NO2/NO3, TKN:1.00 NO2/NO3:0.39 Sample Time: 1520 pH: 7.4 Total Rainfall: 0.7" Total Phosphorus, Total P:0.33 ' Due to exceeded Benchmark in TSS samples were collected on consecutive months for analysis of TS5 only. Visual Monitoring Results Facility Name: Novozymes, N.A. Facility Permit No: NCS000115 Parameters Monitored & Observations Date Monitoring Conducted Outfall Number Total Precipitation During Monitoring Event Color Odor Present Clarity Floating Solids Suspended Solids Foam ISheen Oil Signs of Pollution * 5/18/2008 #1 1.2" Clear None Good None None None None No " #2 It Clear None Good None None None None No * 1/6/2009 #1 .73" Clear None Great None None None None No " #2 Clear None Great None None None None No 6/5/2009 #1 1.3" Clear None Good Alum. Cans None None None No " #2 It Clear None Good None None None None No 12/2/2009 #1 1.0" Clear None Good None None None None No " #2 " Clear None Good None None None None No 5/22/2010 #1 1.2" Clear None Great None None None None No " #2 " Clear None Good None None None None No 12/12/2010 #1 1.0" Clear None Avg. None minimal None None No " #2 " Clear None Good None None None None No 5/27/2011 #1 1.0" Clear None Good paper cups None None None No " #2 " Clear None Good min. trash None None None No 11/16/2011 #1 0.8" Clear None very good leaves None None None No " #2 Clear None Good leaves None None None No 1/26/2012 #1 0.7" Clear None Good paper and plastic cups None None None No #2 Clear None Great None None None None No Best Management Practices (BMP's) BMP's are currently being utilized to minimize discharge of potential pollutants in storm water from the Novozymes, N.A. facility. Preventative measures are a key BMP component utilized in the minimization of storm water discharges. Listed below are the preventative measures in place at the facility. Non-structural BMP's • ISO-14001 Environmental Management System and corrective/preventative action request system • Maintenance of vegetation and proper erosion control practices • Color coding of drain inlets • Education of onsite employees for environmental awareness • Annual training of employees on how specific job duties could impact storm water quality • Inspection and monitoring in accordance with all of NZNA's environmental permit requirements • Good housekeeping and equipment maintenance • Off site maintenance of company vehicles • Proper labeling and readily -available MSDS' for all materials used on site • Proper disposal of generated waste materials Structural BMP's • Storm water diversion to process wastewater system • Two (2) onsite mobile spill vacuum units • Five "Spill Cabinets" containing spill control supplies and clean-up materials • Secondary containment of above -ground storage tanks • Recently modified/upgraded Emergency storm water retention system, (Storm Water Valve) • Storm water conveyance systems • Properly covered storage of raw and processed materials • Vapor and dust control devices to minimize releases of airborne contaminants • Bioretention for roof top runoff Novozymes, N.A. Inc. Permit Number: NCS000115 June 4 2012 This is to verify, that there have not been any significant changes in industrial activities, such as material handling practices, storage areas, or work practices, or raw materials being utilized at the permitted facility, except as noted below. The fuel oil and used oil storage along with the loading/unloading areas have been relocated within the existing site as reflected in the current Site Map. The oil storage capacity was reduced and permanent secondary containment added for the unloading area. These changes represent improvements in storm water pollution prevention at the facility. Joe dd Environmental Compliance Coordinator Rcleigh, NC Greenviil?, NC C'hattcnoogo, TN A`irtnta, C;;A C� L� H Pl ota,enHendev ENGINEERS. AItCFIIi'EC'IC; AND SURVEYORS C� 420 P iW AV-mue Post Office E1ox 171) Green nlle, SG 23�502 Lv.J TeJ 803/242--1717 Fax 943/?35-9062 POH DRAWING NUMBF ......... — .......... -_..... ........ -- ........ — .. ----- 3 I ��' P.1PE _ RFViSE:D FER FIFLp COfuIMENTS __...._ SN J(, IHC THE WCICFN CO DPAWIN[, AND CONTRACTORS RED LtJE j 6---15--99 D._C MEPA ADDRD FFI PROCESS SEINER PIPING _ - ���8 ? I _g GG FJPE REVISED & REDRAWN PER FIELD CCMMEH C'S--- F'.ev. Rev fate, Doan I F.evisions. --- novozymes1 Aiovo7:Ym es ;to-th Arr)&tf,a �tate Fnad 106.3 P.D €9o;a !,76 F,a.Hinton, N L- 27S."', USA Iel (919) 494- 3CIOP E-st WNA FAA PFC}''�;E`>> '- E1NF R ' )VEF,ALL `'SITE F'IL/\N Pay �n. FAA '. 0 1 0 -------- ................................ .... ---- ...... ....... ............ ter O poleiyh, NC Greenville, NC Chattonooga, TN A°!onta, GA lied MIC ►en HE nsliey ENGINEERS, ARCHITECTS AND SURVEYORS 420 P�u-k Avenue Post Office Box 1717 GreE,nville, SC 29»(7:'' Tel. 803/242-17T7 Fox: 803/235-9062 POH DRAWING NUMBER --------- ....... PJ6 REVISED & REDP,ArNN PER FIEhCr ENTS 3 1 _0Z 5iJ Mi.PA REV'ISEb Si f?EDFtA`1VT1 PEA FlEI-D C OyIMENT 99 J,[NC THE WrOTEN "'0 DRAWING 7T1D C9NTF'Fl(7TOf,S RP, 9/" 0 98 G7� PJPE f3EV15Ef? �& f?EDRA'NN PEP, E[EI_D CU=UMEN1�. Rev.: Rev, date: EEv Revisions-- dk novaWe , Ncvo�ymes North An-er3co State Pcan TOUT, PO 60S76 14G riJ._J -J5A 'el (Eli 3} 494-3000 Est. ;late: -' 23/')8 '1ZNA FAA — DPsi =>TOPr) 'FWEI' ':�'t `.:7 T P i scale. AS N0-_-ED _ -'IVEF,ALL SITE PLAN t rou no,. ............... W,,'' TERSHFF LA YCIU T ,A T t ;;� lM[DF 1 l%J� REA. 1 ,.I. -PA.. AfRF a. AREA I AREA 2 .1 OD I ,>r),0ii0 AREA 3 � 4.7 19 4i AFEA 4 AF�EA 5 _4T I04 LAGOON #2 LA6 C411LER UTILITIES • PECFIN,i:�c BUILUNC, GRANULATION PLANT Pl f N r: (Fl-K) NEW FERMENTATION PLAN] PLOT I 7 PL J, (FGF A&. FIB PI 0YFf SERVICES At PRODI ICTION BUILDING BUSINESS OPERATION" BUILDINo' BLJILCIW� (FHI<) Ailk d fir' LA8 N. IFFIK PARKIN(" (FHI) C-) NO LEGEND DE'S-CR IFI ON T -- - -- - --- -- ---- - - - - -- -- ---------- _j�,jl SODIUM ALUMINAITE TAW/ FORMIC ACID TANK 4 PERLIR_ TANK AGING TANK ,AGING TAN14, r AiJNG TANK ANG TANK GLUCOSE TANK 10 STANDARDIZATION TANK 1 1 IL Z_ PIRCCE`7 TANK T280 FEWENTER '1, F E _'V E N TE R 14 FE7'MENTER MIXING TAN,` 16 FERMENTER 17 FERIVIENTER 18 FERIVIENTER 19 S1.0- CC)RN STARCH /GRITS/SOYNAEAL 20 SILO '2 1 SI L(D SLO 23 SBM HOLDING TANK — T,407A 2) 4 B SBM HOLDING TANK - T407 45 SBM BUFFER TANK -- 1408 26 LIME SILO) 27 DIESEL FUEL TANKS FOR BOILERS 28 ANHYDROUS AIVIVIONlA 21 9 USED OIL TANK - 500 GAI 30 L)IE.-SEL FUEL TANK -- 5)00 GAL IT, OLD WASTEWATER SUPGE TANK 32 SL)uR0!:lF SOLUlI('_)N 33 C.(--lRN STEEP LIQUOR 34 EXHAUST GAS-'S EPARATCR 15 ENZYME DUST COLLECTION '56 GLYCOL- TANK 37 SODIUM ALUMINATE 4i MCD[WR North Carolina Department of Environment and Natural Resources Division of Water (duality Beverly Eaves Perdue Charles Wakild, P.E. Dee Freeman Governor Director Secretary October 15, 2012 Mr. Randy Green Novozymes North America PO Box 576 Franklinton, NC 27525 Subject: NPDES Permit Renewal Application Novozymes North America Permit Number NCS000115 Individual Stormwater Permit Franklin County Dear Mr. Green: The Division of Water Quality's Stormwater Permitting Unit (SPU) acknowledges receipt of your renewal application for coverage under NPDES Permit Number NCSOOO115 on August 1, 2012. We currently have a backlog of individual permit renewals in-house and are working to get to these as quickly as we can. Please continue to comply with all conditions and monitoring requirements in your current or expired NPDES stormwater permit. As long as you have submitted a complete renewal request package and maintain compliance with those permit conditions, stormwater discharges from this facility are authorized by that permit until the Division issues a renewal permit or notifies you of an alternative action. No additional information is required at this time, but we may contact you in the future. Please notify us if any significant changes have taken place at this facility since you submitted the renewal package. If you have any questions about this matter, please contact me at (919) 807-6378, bradley.bennett@ncdenr.gov. cc: Stormwater Permitting Unit Files Central Files Wetlands and Stormwater Branch 1617 Mail Service Center, Raleigh, North Carolina 27699.1617 Location: 512 N. Salisbury St. RateigIh, North Carolina 27604 Phone: 919-807-63001 FAX: 91 H07-6494 Internet: www.xwaterquality.org An Fmiol rinnnrinaity 4 Af nrnaCva Antinn Fmnlnvor Sincerely, MIM% r VA Bradley Bennett Stormwater Permitting Unit One No Carolina atura!!b North Carolina Beverly Eaves Perdue Governor • • A7iA. NCDENR Department of Environment and Natural CERTIFIED MAIL RETURN RECEIPT REQUESTED RECEIPT # 7008 1300 0000 1133 3895 Mark Paige Vice President of Technical Operations Novozymes North America Inc, 77 Perry Chapel Church Road Franklinton, NC 27525 Subject: Notice of Violation NOV-2011-PC-0135 Permit No. WQ0002806 Dear Mr. Paige, Division of Water Quality Coleen H. Sullins Director February 23, 2011 Novozymes North America, Inc. Franklin County Resources Dee Freeman Secretary As reported to our office on February 14, 2011, Novozymes .had a release of process wastewater (Incident # 201100342) that discharged an estimated 2,000 gallons to surface water in the Cedar Creek fZoodplain in Franklin County; Farm 3 Field G2, with a BOD concentration of 12 mg/l and an Ammonia concentration of 0.09 mg/l. The discharge mixed and pooled with ephemeral surface water, none of which reached Cedar Creek, which is located approximately 500-600 feet to the East. The Division received an email February 18, 2011 pertaining to the hydrant failure and corresponding release to the surface water. On February 16, 2011, and prior to receipt of the email, the Division conducted a site inspection of the hydrant failure. The following was noted at the time of the inspection: 1. The hydrant that failed was installed and operating within the approved design range. However, it appears that the air release valve contributed to the failure by allowing air to accumulate in the line. 2. The process water released was treated in an activated sludge system prior to storage in lagoon three, where there is a (MCRT) mean cell residence time of 50 days and additional polishing from surface aerators. 3. No apparent indication of environmental impact was observed during the site inspection of the process wastewater release area. 4. A new hydrant has been installed with ductile iron and a Valmatic air/vacuum relief valve replacing the previous ball valve configuration. Aqu'sl'er Pruleclion Section 1628 Mail Service Center, Raleigh, North Carolina 27699-1628 OneLocation: 3800 Barren Dr., Raleigh, North Carolina 27609 NOI"CilCiilGlI17a Phone: 919-791-42001 FAX: 919-571-47181 Customer Service: 1.877-623-6748 Internet: www.newaterauality.org A&A111Y An Equal Opportunity) Aftirmative Action Employer • Novozymes North America Inc. Permit # WQ0002806 NOV-201 1-PC-0135 February 23, 2011 Page 2 of 2 The following specifies permit conditions and limitations that were in violation as a result of the discharge on February 14, 2011 to the unnamed ephemeral surface water. OPERATION AND MAINTENANCE REQUIREMENTS 1. Condition I11.1, which states, the facilities shall be properly operated and maintained at all times. The facilities shall be effectively maintained and operated as a non -discharge system to prevent the discharge of any wastewater resulting from the operation of this facility. The Permittee shall maintain an Operation and Maintenance Plan pursuant to 15A NCAC 02T .0507 including operational functions, maintenance schedules, safety measures, and spill response plan. You are required: to take any necessary action to correct the above violations and to provide a written response to this Notice by March 25, 2011. Please include in your response all corrective actions already taken and a schedule for completion of any corrective actions not addressed. Please note that assessment of civil penalties may have already been recommended for violations described within this Notice of Violation. Failure to comply with the State's rules, in the manner and time specified, may result in the assessment of additional civil penalties and/or the use of other enforcement mechanisms available to the State. Failure to comply with conditions in a permit may result in a recommendation of enforcement action, to the Director of the Division of Water Quality who may issue a civil penalty assessment of not more that twenty-five thousand ($25,000) dollars against any "person" who violates or fails to act in accordance with the terms, conditions, or requirements of a permit under authority of G.S. 143-215.6A. If you have any questions concerning this Notice, please contact Steve Kaltenbach or me at (919) 791-4200. Sincerely, 4ay L.G. Environmental Program Supervisor cc: Danny Smith, Surface Water Protection Section Franklin County Environmental Health Department RRO-APS Files Aquifer Protection Section Central Files • ASHk,A' ND. Ashland Hercules Water Technologies Division of Ashland Inc, 3930 Glenwood Drive Charlotte,NC 28208 Tel: 704 391-5932 www.ashland.com March 21, 2011 NOVOZYMES NORTH AMERICA Franklinton NC 27525 Attn: Joe Jenkins, Randy Green CC: Houston Cash, Jackson Messer Water Treatment Service Report Please find attached the laboratory results from samples collected from the cooling towers that discharge into the receiving stream. We also collected a sample from the city make-up and effluent however we a rain event that may have affected the effluent data slightly. I have tabulated the data that was the cause for collecting these samples, copper, aluminum and zinc. I have also included conductivity as a reference to help determine how the tower can potentially cycle concentrating any value. S s em Make-up Zinc Co er Alumiirsum <0.1 ppm Conductiui 155 mhos 0.4'ppm < 0.1 ppm FHG 0.5 ppm 0.2 ppm <0.1 ppm 1005 mhos FEH 0.6 ppm <0.1 ppm <0.1 Penn 1090 mhos FEG 1.2 ppm 0.3 ppm <0.1 ppm 996 mhos Effluent 0.5 ppm 1 0.1 ppm 0.2 ppm 553 mhos Comments: As you can see as with my on -site testing we have a significant amount of zinc in the make-up water, I assume this is the corrosion inhibitor added by the treatment facility. We have slightly elevated copper in the FEG & FHG towers however it is not observed in the effluent. We do not report any aluminum in any of the towers or make-up, so we should look for other sources of this material. I will investigate in more detail why we are observing copper in the two tower systems, however affective today please reduce the ORP set -point in these two systems by 25mv. We will collect additional samples on my next visit to monitor the changes in copper and zinc and to assist you in your efforts. Jim Sides Sr. Account Manager • SH LIV C7 Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: City Make-up Sampling Point: City Make-up System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides 10 vate Sri 11AU11 LWR Number: WAL11-614 Project Number: W-20110309-030 Sample Number: 264752 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 32.9 mg/L pH 5.7 - ANIONS Chloride (as Cl) 16.8 mg/L Sulfate (as SO4) 20.7 mg/L CONDUCTIVITY Conductivity 155.0 0/cm ACIDIFIED ELEMENTS Iron, (as Fe) < 0.1 mg/L Aluminum, (as Al) < 0.1 mg/L, Copper, (as Cu) < 0.1 mg/L Manganese, (as Mn) < 0.1 mg/L Zinc, (as Zn) 0.4 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 25.7 mg/L Hardness - Magnesium, Soluble (as CaCO3) 12.8 mg/L Hardness - Total, Soluble (as CaCO3) 38.5 mg/L Silicon, Soluble (as Si02) 10.7 mg/L, Sodium, Soluble (as Na) 13.9 mg/L Phosphorus, Soluble (as PO4) 1.8 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 1.7 mg/L Polyphosphate, Soluble (as PO4) < 0.1 mg/L Total Inorganic Phosphorus, Sol (as PO4) 1.7 mg/L Organic Phosphorus, Soluble (as PO4) 0.1 mg/L .ASH l.�lV Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: FHG Tower Sampling Point: FHG Tower System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides . unte J1111LV11 LWR Number: WALI 1-614 Project Number: W-20110309-030 Sample Number: 264753 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 81.7 mg/L pH 6.4 - ANIONS Chloride (as Cl) 130.0 mg/L Sulfate (as SO4) 156.0 mg/L CONDUCTIVITY Conductivity 1005.0 0/cm ACIDIFIED ELEMENTS Iron, (as Fe) 1.5 mg/L Aluminum, (as Al) < 0.1 mg/L Copper, (as Cu) 0.2 mg/L Manganese, (as Mn) < 0.1 mg/L Zinc, (as Zn) 0.5 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 223.7 mg/L Hardness - Magnesium, Soluble (as CaCO3) 119.7 mg/L Hardness - Total, Soluble (as CaCO3) 343.4 mg/L Silicon, Soluble (as Si02) 90.2 mg/L Sodium, Soluble (as Na) 116.5 mg/L Phosphorus, Soluble (as PO4) 17.3 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 8.3 mg/L Polyphosphate, Soluble (as PO4) 8.0 mg/L Total Inorganic Phosphorus, Sol (as PO4) 16.3 mg/L Organic Phosphorus, Soluble (as PO4) 1.0 mg/L 9A' .y_�,.y�'.. r ,X lHLAIN n Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: FEH Tower Sampling Point: FEH Tower System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides ivate Sri rr1.ui i LWR Number: WAL11-614 Project Number: W-20110309-030 Sample Number: 264754 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 173.4 mg/L pH 7.1 - ANIONS Chloride (as Cl) 130.0 mg/L Sulfate (as SO4) 180.0 mg/L CONDUCTIVITY Conductivity 1090.0 0/cm ACIDIFIED ELEMENTS Iron, (as Fe) 0.3 mg/L Aluminum, (as Al) < 0.1 mg/L Copper, (as Cu) < 0.1 mg/L Manganese, (as Mn) <0.1 mg/L Zinc, (as Zn) 0.6 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 215.8 mg/L Hardness - Magnesium, Soluble (as CaCO3) 128.5 mg/L Hardness - Total, Soluble (as CaCO3) 344.3 mg/L Silicon, Soluble (as SiO2) 107.2 mg/L Sodium, Soluble (as Na) 127.1 mg/L Phosphorus, Soluble (as PO4) 28.9 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 12.8 mg/L Polyphosphate, Soluble (as PO4) 15.2 mg/L Total Inorganic Phosphorus, Sol (as PO4) 28.0 mg/L Organic Phosphorus, Soluble (as PO4) 0.9 mg/L Ashland Hercules Water Technologies Sample Type: WATER Sample Identification: FEG Tower Sampling Point: FEG Tower System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides 0 Late J! 1 111W 1 1 LWR Number: WALI1-614 Project Number: W-20110309-030 Sample Number: 264755 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 158.0 mg/L PH 7.1 - ANIONS Chloride (as Cl) 116.0 mg/L Sulfate (as SO4) 156.0 mg/L CONDUCTIVITY Conductivity 996.0 PS/cm ACIDIFIED ELEMENTS Iron, (as Fe) 1.0 mg/L Aluminum, (as Al) < 0.1 mg/L Copper, (as Cu) 0.3 mg1L Manganese, (as Mn) < 0.1 mg/L Zinc, (as Zn) 1.2 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 214.5 mg1L Hardness - Magnesium, Soluble (as CaCO3) 116,9 mg1L Hardness - Total, Soluble (as CaCO3) 331.4 mg1L Silicon, Soluble (as Si02) 89.4 mg/L Sodium, Soluble (as Na) 135.1 mg/L Phosphorus, Soluble (as PO4) 21.8 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 11.6 mg/L Polyphosphate, Soluble (as PO4) 9.1 mg/L Total Inorganic Phosphorus, Sol (as PO4) 20.7 mg/L Organic Phosphorus, Soluble (as PO4) 1.1 mg/L Ashland Hercules Water Technologies Sample Type: WATER Sample identification: Effluent Discharge Sampling Point: Effluent System ID: COOLING Sample Date: 03/07/2011 Customer Number: 0000329682 Sales Rep: James Sides 0 "lite Jll IllulI LWR Number: WALE 1-614 Project Number: W-20110309-030 Sample Number: 264756 Customer Information: NOVOZYMES NORTH AMERICA INC 77 PERRY CHAPEL CHURCH RD FRANKLINTON NC 27525 Analysis Type Description Result Units ALKALINITY Alkalinity, Hydroxide (as CaCO3) < 0.1 mg/L Alkalinity, P as CaCO3. < 0.1 mg/L Alkalinity, Total (as CaCO3) 24.6 mg/L pH 5.7 - ANIONS Chloride (as Cl) 58.6 mg/L Sulfate (as SO4) 123.0 mg/L CONDUCTIVITY Conductivity 533.0 0/cm ACIDIFIED ELEMENTS Iron, (as Fe) 0.8 mg/L Aluminum, (as Al) 0.2 mg/L Copper, (as Cu) < 0.1 mg/L Manganese, (as Mn) < 0.1 mg/L Zinc, (as Zn) 0.5 mg/L SOLUBLE ELEMENTS Hardness - Calcium, Soluble (as CaCO3) 120.9 mg/L Hardness - Magnesium, Soluble (as CaCO3) 47.4 mg/L Hardness - Total, Soluble (as CaCO3) 168.3 mg/L Silicon, Soluble (as Si02) 37.1 mg/L Sodium, Soluble (as Na) 67.3 mg/L Phosphorus, Soluble (as PO4) 5.9 mg/L PHOSPHORUS Orthophosphate, Soluble (as PO4) 2.7 mg/L Polyphosphate, Soluble (as PO4) 3.2 mg/L Total Inorganic Phosphorus, Sol (as PO4) 5.9 mg/L Organic Phosphorus, Soluble (as PO4) < 0.1 mg/L NCDENR North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor July 23, 2007 Randy Ward Green Novozymes North America, Inc. 77 Perry Chapel Church Road Franklinton, NC 27525 William G. Floss, Jr., Secretary Coleen H. Sullins, Director Subject: Renewal of coverage / General Permit NCG500000 Novozymes North America Certificate of Coverage NCG500115 Franklin County Dear Permittee: In accordance with your renewal application [received on January 26, 20071, the Division is renewing Certificate of Coverage (CoC) NCG500115 to discharge under NCG500000. This CoC is issued pursuant to the requirements of North Carolina General Statue 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated May 9, 1994 [or as subsequently amended]. If any parts, measurement frequencies or sampling requirements contained in this General Permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, the certificate of coverage shall be final and binding. Please take notice that this Certificate of Coverage is not transferable except after notice to the Division. The Division may require modification or revocation and reissuance of the certificate of coverage. Contact the Raleigh -Regional Office prior to any sale or transfer of the permitted facility. Regional Office staff will assist you in documenting the transfer of this CoC. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning the requirements of the General Permit, please contact Jim McKay [919 733-5083, extension 595 or james.mckay@ncmail.net]. Sincerely, z-. -A 4�" for Coleen H. Sullins cc: Central Files Raleigh Regional Office / Surface Water Protection NPDES file 1617 Mail Service Center, Raleigh, North Carolina 27699.1617 One 512 North Salisbury Street, Raleigh, North Carolina 27604 N&fficarohna Phone: 919 733.6083 / FAX 919 733-07191 Internet: www.ncwaterquality.org An Equal Opportunity/Affirmative Action Empfoyer — 50% Recycled110% Post Consumer Paper ;Vaturallff STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY GENERAL PERMIT NCG500000 CERTIFICATE OF COVERAGE NCG500115 TO DISCHARGE NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER BLOWDOWN, CONDENSATE AND SIMILAR WASTEWATERS UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Novozymes North America, Inc. is hereby authorized to discharge Cooling Tower Blowdown & Condensate from a facility located at Novozymes North America 77 Perry Chapel Church Road Franklinton Franklin County to receiving waters designated as an unnamed tributary to Buffalo Creek in subbasin 30301 of the Tar -Pamlico River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV hereof. This certificate of coverage shall become effective August 1, 2007. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day July 23, 2007. /..-, -A �_� for Coleen H. Sullins, Director Division of Water Quality By Authority of the Environmental Management Commission 1� Z O W Z O Vcr— d CD ,C i r c>� r COUNTY/FIZEMISE NUMBER- FACErITY: CITY: PEILN= NUMBER COUNTY: w Permit Information that Nerds to be Incorporated into Future Permit Revisions: DATE' COAU. MNTS NA ff NCDENR f rP z ° Zo1z ' SL. North Carolina Department of Environment and Natural Resources—, Division of Water Quality—�' 'fire Beverly Eaves Perdue Charles Wakild, P.E. Dee'Freeman Governor Director Secretary ' August 3, 2012 Mr. Randy Ward Green Novozymes North America, Inc. 77 Perry Chapel Church Road Franklinton, NC 27525 Subject: Renewal of coverage 1 General Permit NCG500000 Novozymes North America Certificate of Coverage NCG500115 Franklin County Dear Permittee: The Division is renewing Certificate of Coverage (CoC) NCG500115 to discharge under NPDES General Permit NCG500000. This CoC is issued pursuant to the requirements of North Carolina General Statue 143-215.1 and the Memorandum of Agreement between North Carolina and the US Environmental Protection agency dated October 15, 2007 [or as subsequently amended]. If any parts, measurement frequencies or sampling requirements contained in this General Permit are unacceptable to you, you have the right to request an individual permit by submitting an individual permit application. Unless such demand is made, the certificate of coverage shall be final and binding. Please take notice that this Certificate of Coverage is not transferable except after notice to the Division. The Division may require modification or revocation and reissuance of the certificate of coverage. Contact the Raleigh Regional Office prior to any sale or transfer of the permitted -facility. Regional Office staff will assist you in documenting the transfer of this CoC. This permit does not affect the legal requirements to obtain other permits which may be required by the Division of Water Quality or permits required by the Division of Land Resources, Coastal Area Management Act or any other Federal or Local governmental permit that may be required. If you have any questions concerning the requirements of the General Permit, please contact John Hennessy [919 807-6377 or john.hennessy@ncdenr.gov]. Sincerely, Original signed by John Hennessy for Charles Wakild, P.E. cc: Raleigh-Regional•Office i-Surface Water.Pro_ tection NPDES file 1617 Mail Service Center, Raleigh, North Carolina 27699-W7 512 North Salisbury Street, Raleigh, North Carolina 27604 Phone: 919 807-63001 FAX 919 807-6489 / Internet: www.ncwaterquality.org An Equal Opportunity/Affirmative Action Employer - 50% Recycled110% Post Consumer Paper One No Carolina Naturally STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES DIVISION OF WATER QUALITY i i GENERAL PERMIT NCG500000 CERTIFICATE OF COVERAGE NCG500115 TO DISCHARGE NON -CONTACT COOLING WATER, COOLING TOWER AND BOILER BLOWDOWN, CONDENSATE AND SIMILAR WASTEWATERS UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM In compliance with the provision of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, Novozymes North America, Inc. is hereby authorized to discharge Cooling Tower Blowdown & Condensate from a facility located at Novozymes North America 77 Perry Chapel Church Road Franklinton Franklin County to receiving waters designated as an unnamed tributary to Buffalo Creek in subbasin 03- 03-01 of the Tar -Pamlico River Basin in accordance with the effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV hereof. This Certificate of Coverage shall become effective August 3, 2012. This Certificate of Coverage shall remain in effect for the duration of the General Permit. Signed this day August 3, 2012 Original signed by John Hennessy for Charles Wakild, Director Division of Water Quality By Authority of the Environmental Management Commission State of North Carolina Department of Environment and Natural Resources Division of Water Quality Water Quality Section, Stormwater & General Permits Unit 512 North Salisbury Street Raleigh, NC 27604-1143 FAX# (919) 733-9919 PHONE# (919) 733-5083 TELECOPY TO: Steve Stadelman FAX NUMBER: 919-494-3463 FROM: Darren England PHONE: (919) 733-5083 Ext. 545 3 pages, including cover sheet COMMENTS: I circled the storage area in question. If that material storage area is in drainage area 5, you will need to start monitoring or request representative outfall status for that outfall. The permit does not specify each outfall, so this will not hold up the renewal process. You should revise the SPPP to explain why the site map indicate 5 outfalls, but you only sample 2, if it does not already include this information. -dme Regional Offices Asheville Fayetteville Mooresville Raleigh Washington Wilmington Winston-Salem 704-251-6208 910-486-1451 704-663-1699 919-571-4700 252-946-6481 910-395-3900 336-771-4600 P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-3083 Fax 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper I PP PER LVE / ltl '. 1 \ I 5 —' — — — — LAGOON 12 LAGOON fl 1 �1 tt '1 v.st.tAvvk 1 ! I I I N(F k I ON 4 — l. [ FFF t I�-i ' r"1 � I � K} -lKoc 1f.I _� I r _I i I�PLIN ;► I I I I_ I I _ BUSNE55-OKI — �FHK1- 1 ` r 1+ 11 1 � VAKKM rj • �I xf •I •I � r 'I ^I •I .'� i Ii �-�_'v_� •l T':' i�� ,�- �) � "i /``ate\ �� P � � � I� _YC,C-"!IN " E}I _ �,PLAHI [N7RaNCE R 1 .� • SG•Hn!U j _ 0°09 O D �� _ CIO 6 � - I x - �pAn _ I I a-b rF�ss S7 I i I - � •vs;nty I•li I �' I II i- gig U I � I I i I,i ,-y,�sa moo 1 �i . uaam — I /~-•. •, i s .slaw_ G III, _I • �,r ',i ,��-•' , ARKI NPDES FACILITY AND PERMIT DATA 09/19/99 15:33:59 UPDATE OPTION TRXID 5NU KEY NCS000115 PERSONAL DATA FACILITY APPLYING FOR PERMIT REGION FACILITY NAME>.NOVO NORDISK BIOCHEM INC COUNTY> FRANKLIN 05 ADDRESS: MAILING (REQUIRED) LOCATION (REQUIRED) STREET: 77 PERRY CHAPEL CHURCH ROAD STREET: 77 PERRY CHAPEL CHURCH ROAD CITY: FRANKLINTON ST NC ZIP 27525 CITY: FRANKLINTON ST NC ZIP 27525 TELEPHONE 919 494 3390 DATE FEE PAID: 10/09/92 AMOUNT: 400.00 STATE CONTACT> ENGLAND PERSON IN CHARGE STEVE STADELMAN 1=PROPOSED,2=EXIST,3=CLOSED 2 1=MAJOR,2=MINOR 2 I=MUN,2=NON-MUN 2 LAT: 3607390 LONG: 07827330 N=NEW,M=MODIFICATION,R=REISSUE> R DATE APP RCVD 04/13/99 WASTELOAD REQS DATE STAFF REP REQS / / WASTELOAD RCVD DATE STAFF REP RCVD / / SCH TO ISSUE DATE TO P NOTICE / / DATE DRAFT PREPARED 05/10/99 DATE OT AG COM REQS / / DATE DENIED DATE OT AG COM RCVD / / DATE RETURNED DATE TO EPA / / DATE ISSUED / / ASSIGN/CHANGE PERMIT HATE FROM EPA / / EXPIRATION DATE FEE CODE ( 4 ) 1=(>1DMGD),2=(>1MGD),3=(>D.1MGD),4=(<D.1MGD),5=SF,6=(GP25,64,79), 7=(GP49,73)8=(GP76)9=(GP13,34,30,52)0=(NOFEE) DIS/C 73 CONBILL ( ) COMMENTS: MESSAGE: ***,ENTER DATA FOR UPDATE *** State of North Carolina Department of Environment and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary A. Preston Howard, Jr., P.E., Director February 19, 1999 LEE YARBROUGH NOVO NORDISK BIOCHEM STATE ROAD 1003 PO BOX 576 FRANKLINTON, NC 27525 1•WA ANN% 000%WWW" NCDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES Subject: NPDES Stormwater Permit Renewal Novo Nordisk Biochem Permit Number NCS000115 Franklin County Dear Permittee: Your facility is currently covered for stormwater discharge under NPDES Permit NCS000115. This permit expires on August 31, 1999. In order to assure your continued coverage under your permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit. To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed you will find an individual permit renewal application form, supplemental information request, and Stormwater Pollution Prevention Plan certification. Filing the application form along with the requested supplimental information will constitute your application for renewal of your permit. The application form must be completed and returned along with all requested information within thirty days of receipt of this letter in order to constitute a timely renewal filing. Recent legislation modified the fee structure for DWQ permits. Renewal fees have been eliminated and annual fees have been changed. The new annual fee for your permit is now $715.00 (you will be invoiced later this year for your annual fee.)"A copy of the new fee schedule is enclosed in this package. Failure to request renewal within the time period indicated may result in a civil assessment of at least $250.00. Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility without coverage under a valid stormwater NPDES permit would constitute a violation ofNCGS 143-215.1 and could result in assessments of civil penalties of up to $10,000 per day. If you have any questions regarding the permit renewal procedures please contact Darren England of the Stormwater and General Permits Unit at (919) 733-5083, ext. 545. Sincerely, Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Raleigh Regional Office P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper State of North Carolina Department of Environment and Natural Resources Division of Water Quality James B. Hunt, Jr., Governor Wayne McDevitt, Secretary Kerr T. Stevens, Director April 19, 1999 Mr. Steve Stadelman Novo Nordisk Biochem 77 Perry Chapel Church Road Box 576 Franklinton, North Carolina 27525 NCDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES Subject: NPDES Permit Renewal Application Permit Number NCS000115 Individual Stormwater Permit Franklin County Dear Mr. Stadelman: The Division of Water Quality's Stormwater and General Permits Unit hereby acknowledges receipt of your renewal application for coverage under NPDES Permit Number NCS000115 on April 13, 1999. The submitted renewal package contained the following items: ➢ Signed application ➢ Site map ➢ Analytical monitoring results summary ➢ Visual monitoring results summary ➢ Best Management Practices summary Narrative describing significant changes at the permitted facility ➢ Signed Stormwater Pollution Prevention Plan certification A preliminary review of the submitted renewal application package has been conducted and it appears to be complete. No further information is required at this time. If you have any questions about the renewal process or would like to discuss this letter, please contact me at (919) 733-5083, extension 545. Sincerely, Darren M. England Environmental Engineer cc: Raleigh Regional Office Stormwater and General Permits Unit Central Files S W U-238.032499 P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper - -04 . RE: NCS 000115, Novozymes Subject: RE: NCS 000115, Novozymes From: "Ron Boone" <ron. boone@ncmail. net> Date: Mon, 3 Dec 2007 12:41:18 -0500 To: "Kelly Johnson" <kelly.p.johnson@ncmaiI.net> CC: <jennifer.jones@ncmail.net> Kelly, Don't have any concerns right now. I've never been to the facility yet but have been planning to do an inspection sometime in the near future. I'll try to investigate the BOD5 issue while there. Go ahead and issue the permit for now. Thanks for the information on it. Ron -----Original Message ----- From: Kelly Johnson [mailto:kelly_p:johnson@ncmail.net] Sent: Friday, November 30, 2007 2:19 PM To: Ron Boone Cc: jennifer.jones@ncinail.net Subject: NCS 000115, Novozymes Ron, I have attached a staff report and a draft permit for this facility in Franklin County. We are working through a substantial backlog of individual permits, and this one is among the oldest on file. They applied in 2004. This facility manufactures enzymes. Most of the analytical data was alright, but they have consistently high BOD5 at Outfall 2. And, we typically expect to see a relationship between BOD5 and COD such that COD is -4X BOD5. BOD5 has a hold time requirement, so I am not sure if this discrepancy is due to not meeting hold time requirements at the lab or if this is some sort of other anomaly. But, we can mention in the cover letter of their permit that this should be something that they talk to their lab about. Chad Coburn and Aisha Lau did a site visit last August, and did not find anything of concern. ,Aisha actually said that they were very organized and knowledgeable. We have changed some things with the individual permits (as you may have heard). The staff report summarizes the issues that have changed for all permits (see "Revised Permit Recommendation: Analytical Monitoring", #2-6, and "Other Proposed Changes to the Permit", #1-5.) The most significant,of which is number 4 in the first grouping. Permittees are now required to take action based on their analytical testing. If it is too high once, then they essentially have to inspect their own facility and try to fix the problem. If it is high again, they move to monthly monitoring. There is also some language that allows DWQ to get involved if they don't make any improvements. Does the Raleigh Regional Office have any concerns about issuing this permit? If not, we will issue it in 30'days. I will send you a hard copy of the staff report through inter -office mail along with a site map. You can keep the site map if you like (I have a duplicate), but please return the signed staff report to our office. I will be going on maternity leave within the month, and Jennifer Jones will be the contact for this permit while I am out. Kelly Kelly Johnson Environmental Engineer N.C. Division of Water Quality 1 of 2 12/3/2007 3:01 PM --------------- RE: NCS 000115, Novozymes Stormwater Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Phone: (919) 733-5083 ext. 376 Fax: (919) 733-9612 2 of 2 12/3/2007 3:01 PM RE: NC Stormwater Permit, NCS000115 Subject: RE: NC Stormwater Permit, NCS000115 From: "RWGR (Randy Green)" <RWGR@novozymes.com> Date: Tue, 27 Nov 2007 11:41:10 -0500 To: "Kelly Johnson" <kelly.p Johnson@ncmail.net> CC: <jennifer.jones@ncmail.net> Kelly Johnson & Jennifer Jones Answers to questions: l.Correct 2.Correct 3.No 4.Area #3 drains to the second outfall. right corner of area #3 at the culvert. street side ditch from "F" block to "M" UNT then to Buffalo creek. 5.919-494-3001, Randy Green Best Regards Randy Green Phone: +1 9194943001 E-mail: rwgr@novozymes.com The outfall is at the bottom The outfall flow goes along a block then under the road to a Novozymes North America, Inc. (reg. no.: 13-2639630) PO BOX 576 77 Perry Chapel Church Road Franklinton, NC 27525, United States This e-mail (including any attachments) is for the intended addressee(s) only and may contain confidential and/or proprietary information protected by law. You are hereby notified that any unauthorized reading, disclosure, copying or distribution of this e-mail or use of information herein is strictly prohibited. If you are not an intended recipient you should delete this e-mail immediately. Thank you. -----Original Message ----- From: SAST (Steve Stadelman) Sent: Tuesday, November 27, 2007 10:50 AM To: Kelly Johnson; RWGR (Randy Green) Cc: jennifer.jones@ncmail.net Subject: RE: NC Stormwater Permit, NCS000115 Hi Kelly, I am forwarding this to Randy Green, who has responsibility for the Stormwater Permit. Best Regards Steve Stadelman Phone: +l 9194943390 E-mail: sast@novozymes.com Novozymes North America, Inc. (reg. no.: 13-2639630) PO BOX 576 77'Perry Chapel Church Road Franklinton, NC 27525, United States This e-mail (including any attachments) is for the intended addressee(s) only and may contain confidential and/or proprietary information protected by law. You are hereby notified that any unauthorized reading, disclosure, copying or distribution of this e-mail or use of information herein is strictly prohibited. If you are not an intended recipient you 1 of 2 11/27/2007 3:18 PM RE: NC Stormwater Permit, NCS000115 should delete this e-mail immediately. Thank you. -----Original Message-7--- From: Kelly Johnson [mailto:kelly .p.johnson@ncmail.net] Sent: Tuesday, November 27, 2007 8:51 AM To: SAST (Steve Stadelman) Cc: jennifer.jones@ncmail.net Subject: NC Stormwater Permit, NCS000115 Steve, The Division of Water Quality conducted a site visit of your facility in August.of 2006. Unfortunately, there has been a considerable lag time since then and we are just now processing your permit application. The two DWQ staff that conducted the visit have since changed jobs, and I have now been assigned to your permit. I will be working with another engineer -in our group, Jennifer ,Tones, to finalize this process. The phone number that I have for you on file is not working. So, I thought I would email you a few questions that we have about your permit application and then we can either discuss it over email or you can give me a call, whichever you prefer. -I have on file that you are the facility contact for this permit. If that is no longer the case, would you please forward this to the appropriate person? 1.) We have that the legal owner of your facility is "Novozymes North America Inc". Is that still correct? 2.) We have that the legal name of your facility is "Novozymes North America Incorporated". Is that still correct? 3.) Has the facility undergone any major changes in the past few years? For instance, are you still making the same types of products or have you had any considerable expansions? 4.) Your site plan has five drainage areas, and all of them appear to drain into one another and leave the site through a single ditch near the lagoons. The analytical data from your previous permitting cycle has two outfalls. Are there two outfalls both along the ditch near the lagoons? If so, where is each one along that ditch. Or, if the second outfall is not along that ditch, where is it? 5.) What is the phone number where you (or the appropriate contact person) can be reached? I have drafted your new permit, and will update it discussing these questions,with you. Then, I will regional office to get their input, and also send Your permit should be issued in approximately the year. I will be your contact person•ifor the next be going on maternity leave soon. Jennifer, who i will be your contact while;I am out. Thanks, Kelly Kelly Johnson Environmental Engineer N.C. Division of Water Quality Stormwater Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Phone: (919) 733-5083 ext. 376 Fax: (919) 733-9612 if necessary after work with our it to public notice. first quarter of next month or so, but will s cc1d on this email, 2 of 2 11/27/2007 3:18 PM Re: [Fwd: Re. NCS000115, Novozymes] Subject: Re: [Fwd: Re: NCS000115, Novozymes] From: Kelly Johnson <kelly.p Johnson@ncmail.net> Date: Mon, 26 Nov 2007 15:08:34 -0500 To: Aisha Lau <Aisha.Lau@ncmail.net> Thanks, Aisha? Aisha Lau wrote: Howdy Kelly, Before I left I just gave a quick comment about the site visit in the comments section of the draft applications BIMS screen. .What I remember from the site visit was that they had all of their is dotted and is crossed at least a couple of times. They had documentation to show that all of their personnel had been trained annually, their SPPP was up to date, and above and beyond that, all of their drainage areas were labeled with color coded drains at the plant indicating which drains went to sanitary sewer and which went to the storm sewer. They are also one of 6 environmental stewards participating in Pollution Prevention's ESI program. Here's a link to their case study. http://www.122pays.org/ref/41/40979.pdf I don't recall any areas that I was concerned about for potential stormwater pollution points. If you have any other specific questions I'd be happy to help as best I can. Take care, Aisha Kelly Johnson wrote: Mitch, Are you now the contact for Franklin County? inspection notes from a site visit from last visit, but they are both now in Wilmington. send them my way? I am trying to track down some year. Chad and Aisha did the site If you can find those, will you Also, I copied a new engineer in our group, Jennifer Jones. She will take over this permit when I go on maternity leave in a few weeks. Thanks, Kelly Subject: Re: NCS000115, Novozymes From: Chad Coburn <chad.coburn@ncmail.net> Date: Wed, 21 Nov 2007 13:24:56 -0500 To:' Kelly Johnson <kelly.p.johnson@ncmail.net>, Aisha Lau <Aisha.Lau@ncmail.net> To: Kelly Johnson <kell .johnson@ncmail.net>, Aisha Lau <Aisha.Lau@ncmail.net> Kelly, I am no longer the contact for this one. Aisha and I are both down in the Wilmington Regional office now as luck would have it. If I had to guess who �2 11/26/2007 3:08 PM Re: [Fwd: Re: NCS000115, Novozymes] has this permit now, I'd say Mitch Hayes in the Raleigh Regional Office. 919-791-4200. My inspection letter should be in the file folder stared at the RRO. I may have a copy of it here in my electronic records that I brought with me when I moved my office. I'll speak with Aisha and see.if she remembers the specifics of this inspection because I can't right off hand. Chad Kelly Johnson wrote: Chad & Aisha, I have started the staff report & permit drafting for this facility. I saw in RIMS that you did an inspection on 8/2/06. 1 don't see any inspection notes on file. Do either of you have additional notes? Specifically, this facility is monitoring only 2 outfalls, but they have five. Do you remember if you discussed representative outfall status with them? Also, there is an old (-2004) note on file questioning part of one of the drainage areas. There is also a note on one of the drawings that Bill Mills talked to someone at the facility & it had been addressed, but I wanted to see if you had discussed it further with them to see if the "fix" was a permanent one. Also, the qualitative data show that there is some "strapping" (presumably packing material) that made its way to the stream. That is a pretty easy housekeeping fix, but I didn't know if they had addressed it already. Finally, did you discuss any analytical parameters that needed to be added to the permit? Based on their past data, I don't think we'll remove any, but I didn't know if you saw something that needed to be added. I know it has been a while, but I thought I would ask in case you remembered... Also, Chad, are you still the contact for this permit in Franklin County? will be drafting up the initial parts of this and a new engineer in our group, Jennifer Jones, will take over when I go on maternity leave next month. Thanks, Kelly Kelly Johnson Environmental Engineer N.C. Division of Water Quality Stormwater Permitting unit 1617 Mail Service Center Raleigh, NC 27699-1617 Phone: (919) 733-5083 ext. 376 Fax: (919) 733-9612 2of2 11/26/2007 3:08'�J r �1 .INC Stormwater Permit, NCS000115 V— . '"r: Subject: Re: NC Stormwater Permit, NCS000115 From: Kelly Johnson <kel ly.p.j ohnson@ncmail. net> Date: Wed, 12 Dec 2007 09:15:39 -0500 To: "RWGR (Randy Green)" <RWGR@novozymes.com> CC: jennifcr.jones@ncmail.net Thanks, Randy. We will make a note of that in the file. Kelly RWGR (Randy Green) wrote: Kelly FYI We have a "Letter of Approval" for a Erosion and Sedimentation Plan dated 10/30/07. This is for a expansion for out the BOB building. 3,600 ft2 on the south side 5,380 ft2 on the north side There will also be about 500 - 800 ft2 of concrete walk ways added Best Regards Randy Green Phone: +1 9194943001 E-mail: rwgr@novozymes.com Novozymes North America, Inc. (reg. no.: 13-2639630) PO BOX 576 77 Perry Chapel Church Road Franklinton, NC 27525, United States This e-mail (including any attachments) is for the intended addressee(s) only and may contain confidential and/or proprietary information protected by law. You are hereby notified that any unauthorized reading, disclosure, copying or distribution of this e-mail or use of information herein is strictly prohibited. If you are not an intended recipient you should delete this e-mail immediately. Thank you. -----Original Message ----- From: Kelly Johnson [mailto:kelly.p.johnson@ncmail.net] Sent: Tuesday, November 27, 2007 3:24 PM To: RWGR (Randy Green) Cc: jennifer.jones@ncmail.net Subject: Re: NC Stormwater Permit, NCS000115 Thanks, Randy. We'll be back in touch soon. Kelly RWGR (Randy Green) wrote: Kelly Johnson & Jennifer Jones Answers to questions: 1.Correct 2.Correct 3.No 4.Area 43 drains to the second outfall. The outfall is at the bottom right corner of area #3 at the culvert. The outfall flow goes along a street side ditch from "F" block to "M" block then under the road to a 1 of 4 12/14/2007 1:56 PM LVNC Stormwater Permit, NCS000115 UNT then to Buffalo creek'. 5.919-494-3001, Randy Green Best Regards Randy Green Phone: +1 9194943001 E-mail: rw r@novoz.ymes.com Novozymes North America, Inc. (reg. no.: 13-2639630) PO BOX 576 77 Perry Chapel Church Road Franklinton, NC 27525,'United States This e-mail (including.any attachments) is for the intended addressee(s) only and may contain confidential and/or proprietary information protected by law. You are hereby notified that any unauthorized reading, disclosure, copying or distribution of this e-mail or use of information herein is strictly prohibited. If you are Inot an intended recipient you should delete this e-mail immediately. Thank you. -----Original Message ----- From: SAST (Steve Stadelman) Sent: Tuesday, November 27, 2007 10:50 AM To: Kelly Johnson; RWGR (Randy Green) Cc: jennifer_.-'ones@ncmail.net Subject: RE: NC Stormwater Permit, NCS000115 Hi Kelly, I am forwarding this to Randy Green, who has responsibility for the Stormwater Permit. Best Regards Steve Stadelman Phone: +1 9194943390 E-mail: sast@novozvmes.com Novozymes North America, Inc. (reg. no.: 13-2639630) PO BOX 576 77 Perry Chapel Church Road Franklinton, NC 27525, United States This e-mail (including any attachments) is for the intended addressee(s) only and may contain confidential and/or proprietary information protected by law. You are hereby notified that any unauthorized reading, disclosure, copying or distribution of this e-mail or use of information herein is strictly prohibited. If you are Inot an intended recipient you should delete this e-mail immediately. I Thank you. -----Original Message ----- From: Kelly Johnson[mailto:kelly.p.johnson@ncmail.net) Sent: Tuesday, November 27, 2007 8:51 AM T To: SAST (Steve Stadelman). Cc: jennifer.jones@ncmail.net 2 of4 12/14/2007 1:56 PM i NC Stormwater Permit, NCS000115 Subject: NC Stormwater Permit, NCS000115 Steve, The Division of Water Quality conducted a site visit of your facility in August of 2D06. Unfortunately, there has been a considerable lag time since then and we are just now processing your permit application. The two DWQ staff that conducted the visit have since changed jobs, and I have now been assigned to your permit. I will be working with another.engineer in our group, Jennifer Jones, to finalize this process. The phone number that I have for you on file is not working. So, I thought I would email you a few questions that we have about your permit application and then we can either discuss it over email or you can give me a call, whichever you prefer. I have on file that you are the facility contact for this permit. If that is I no longer the case, would you please forward this to the appropriate person? 1.) We have that the legal owner of your Inc". Is that still correct? 2.) We have that the legal name of your Incorporated". Is that still correct? 3.) Has the facility undergone any major years? facility is "Novozymes North America facility is "Novozymes North America changes in the past few For instance, are you still,making the same types of products or have you had any considerable expansions? 4.) Your site plan has five drainage areas, and all of them appear to drain into one another and leave the site through a single ditch near the lagoons. The analytical data from your previous permitting cycle has two outfalls. Are there two outfalls both along the ditch near the lagoons? If so, where is each one along that ditch. Or, if the second outfall is not along that ditch, where is it? 5.) What is the phone number where you (or the appropriate contact person) can be reached? I have drafted your new permit, and will update it if necessary after discussing these questions with you. Then, I will work with our regional office to get their input, and also send it to public notice. Your permit should be issued in approximately the first quarter of next year. I will be your contact person for the next month or so, but will be going on maternity leave soon. Jennifer, who is cc'd on this email, will be your contact while I am out. Thanks, Kelly Kelly Johnson Environmental Engineer N.C. Division of Water Quality Stormwater Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Phone: (919) 733-5083 ext. 376 Fax: (919) 733-9612 3 of 4 12/14/2007 1:56 PM ,RI�-NC Stormwater Permit, NCS000115 Kelly Johnson Environmental Engineer N.C. Division of Water Quality Stormwater Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Phone: (919) 733-5083 ext. 376 Fax: (919) 733-9612 Kelly Johnson Environmental Engineer N.C. Division of Water Quality Stormwater Permitting Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Phone: (919) 733-5083 ext. 376 Fax: (919) 733-9612 4 of 4 12/ I4/2007 1:56 PM Re: NC Stormwater Permit, NCS000115 Subject: Re: NC Stormwater Permit, NCS000115 From: Jennifer Jones <Jennifer.Jones@ncmail.net> Date: Wed, 02 Jan 2008 11:10:39 -0500 To: "RWGR (Randy Green)" <RWGR@novozymes.com>, Kelly Johnson <kell y.p, j ohnson@ncmai l.net> Hi Randy, Here are the links to the Surface Waters and Wetlands Standards (the 15A NCAC 2B .0200 <../admin/rules/documents/rb080104.pdf> file). http://h2o.enr.state.nc.us/su/Neuse SWProgram Documents.htm http://h2o.en.r.state.nc.us/admin/ru.l.es/documents/rbO80104.pdf On your draft permit on the front page it shows the receiving water is listed as a class C, NSW water. In the table of contents there is a link to the Fresh Water Quality Standards for Class C waters - if you click on the page number it will take you there and gives a list of all the standards for Class C. There is also a list of standards for the Tar -Pam River basin. The Tar -Pam is nutrient sensitive for Nitrogen and Phosphorus so that was a factor in keeping those parameters in your monitoring. If you�have any further questions or need further explanation on this please let me know. Thank you, Jennifer Jones Jennifer Jones Environmental Engineer NCDENR I DWQ I Stormwater Permitting Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 512 N. Salisbury St, Raleigh, NC 27604 Phone: (919) 733-5063 ext. 591 Fax: (919) 733-9612 Email: jenn,fer.jones@ncmai.l.net Website: http://h2o.enr.state.nc.us/su/stormwater.htmi RWGR (Randy Green) wrote:. Kelly Johnson & Jennifer Jones Answers to questions: 1.Correct 2.Correct 3.No 4.Area 43 drains to the second outfall. right corner of area #3 at the culvert. street side ditch from "F" block to "M" UNT then to Buffalo creek. 5.919-494-3001, Randy Green Randy Green Phone: +1 9194943001 E-mail:•rwgr@novozymes.com The outfall is at the bottom The outfall flow goes along a block then under the road to a Best Regards I of3 1/2/2008 11:12 AM Novozymes, Inc. Phone correspondence with Randy Greene: January 2, 2008 919-494-3001 Randy Greene wanted to know: l . What is a benchmark? a. A: a guideline for the permit. Told him to see permit and see tiered structure if these guidelines were exceeded. 2. Were these benchmarks specific or general? a. A: These guidelines are general for all permits [see guidance document]. Difficult to know — would need to measure each stream in many storm events. Based on the stream etc. 3. Are these benchmarks flexible? a. A: not really 4. Where are the regulatory limits listed? a. A: See redbook — standards for class C. Sent an email to document. LAGOON #2 l..AfiG��J �1 i IILER f31JILiJI G U 111J IILQ BUILDING 11PPIN J fiLt;F'VIIV AL BIIILDIPIC 4 - REi;OVERY , CRAHUI...ATIM PLANTAL PLs4CJT. - " FCMEPJTAIII]N r PLAN f e I I PLAA T ' -mill A�ii is is; „ 2i a. _� --� -': s PF,DDUCI It)N .. SPACE J... IaLIIL.DING � • �11tiINlE_';5 011CRATIf)fJ6 • BIJILDIV', f TNI) I JILDINC 1 (riv) ..... - LAB a : r 2 _ YHGE BUILDING PARKING(Flit) M m 13 LL- cn i5 r LEGEND nlrr 1 DE= lr,h! F IN11SH PR(?['7LJC 1 TANKS 2 ALUMINATE TANK I 3 -SCDIUV _ --- FORMIC ACID TANK 4 PERLITE TANK C 5 AC1NC7 TANK - ----- -..._ F. A C•I N G TANK-----.�---- 7 ACING TANK— f3 ACING TANK 9 GLUCOSE TANK ._; i AND'AR D1GA Ti ON TAkiK 1 �-- PP Or -' F SS TANK -80 - 12 F F �' M E N TL R_- -' FERMENTER --- —_- 14 FERMENIER — TANK`— 16 _ FERMENTER 'I FERMENTED, 18 FERMFNTER 19 SILO CORN STARCH/GRI1S/SOY1vIEAL 20 SILT) SILO _-?3.__. '-�I3M HOLDING TANK T407A --- S(3M HC)LDING TANK - 7-407B �� SCPrI BLIEFFI� TAN}< T4t08: - - f �'6 LIME SILO 7 T ' � I E � U E I- '__ � TANKS TOR C OM ERS 28 ANHYDROUS AMMONIA 29 USED OIL TANK - 500 GAL ---`-- 30 DIFTSEL GAL :12 �341 5 _ ^FUEI__TANK --JO._) _._... OLD WASTEWATER R SURGE TANK SUCROSE ;SOLUTION CCIRNu "TTEEF UOIJOR LXHAUST GAS `-IEPARATOR __- ENZYME DUST COLLECTION 37 SOD) UM ACUMINATE 38 CALCIUV CHLORIDE TANK 3 9 _. M p, G N A FLOC------- ----- ---- 40 FERMEr1TATION BROTH TANKS 41 I�FERMENTATION 13ROTH TANKS-_�- - 42 �PERL i TE HOL.DIN(:1 TANK 1_5 - L I ME S ILO 4._..__SEM HUFFEF' TANK 5- 1 MIXING TANK 46 PROCESS FII_TRATE 1-ANKS �4,7 PROCE13S FILTRATE 'ANK`~ 48 PROCESS FILTRATE�TANK< - --- 49 PROCESS FILTRATE TANK` 50 CONCEf-J (RATED CAUSTIC (KOI I) ,.I CONCENTRATED NITRIC ACID �2 FINISH PR0rC7UCT 1 53I HJISH PRODUCT �'>4-----FINISH PRC?DUOi__�_� ...__-...._.-� 55 FINISH PRODL)CT 56 FINISH PRODUCT 5 7 F-IN I S H P RODU C T 58 PINISH PRODUCT 59 FINISH PRODUCI 60 FINISH PRODUCT 61 FINISH PRODUCT _6.—�_ ✓=ORMIG ACID TANK �-------._.._-- 6;; PHOSPHORIC ACID TANK 641 FI._OCUL.ATIONTANK NC T-ES: - AU'FA GRAPHIC SCALL 0 '100' 200' 300, 1„ W 100, 3-23-99 PJPe RWGR AS-BIJILT 6 96 PJPe PJPE I I"1EVISED LFOCND _ 1 __91, C.I6 SASt FIRST ISSUE FOR STORM PEPUT -- - - , novazymes� , rJ w.,yme.s North Awerlca 'Stot,e Read 7p0:3 P_0Box 576 Frorikiintan, NC 275:a USA Tel {91�J) 41D4-,TOO CM. Ijte: 6-ta---- :Js--- NZNA FAA SITE MAP FOR S-ORM De2L2,] i`'_ 1'Zg WAIFR PERMIT- LOCATION WDU'S'-1R1AL. Sale: AS -NOTED _ ACTIVITI!_ S� LOAEAGANILOADING AR�:AS L.rotJp . E ?.: 4 ......_..,_—. - -. . ..._ .... __.......... —................ _. .... J... t-� OF WAT Michael F. Easley, Governor O� QG State of North Carolina � _ William G. Ross, Jr., Secretary Department of Environment and Natural Resources 0 Coleen H Sullins, Director Division ofWaterQuality December 4, 2007 Mr. Steve Stadelman Novozymes North America 77 Perry Chapel Church Rd Franklinton, North Carolina 27525 Subject: Draft NPDES Stormwater Permit Permit No. NCS000115 Novozymes North America Franklin County Dear Mr. Stadelman: Enclosed with this letter is a copy of the draft stormwater permit for your facility. Please review the draft very carefully to ensure thorough understanding of the conditions and requirements it contains. The draft permit contains the following significant changes from this facility's current permit: Analytical monitoring changes: 1. All monitoring parameters have been continued since the previous permit. 2. pH has been added to the analytical monitoring requirements. 3. All analytical monitoring has been set to semi-annually during a representative storm event as defined in Part lI Section B. The permittee must also document the total precipitation for each event. If no discharge occurs during the sampling period, the permittee must submit a monitoring report indicating "No Flow" within 30 days of the end of the six-month sampling period. Additionally, samples must be taken a minimum of 60 days apart, as specified in Table 2. 4. Benchmarks for analytical monitoring have been added to this draft permit. Exceedances of benchmark values require the permittee to increase monitoring, increase management actions, increase record keeping, and/or install stormwater Best Management Practices (BMPs) in a tiered program. If the sampling results are above a benchmark value, or outside of the benchmark range, for any parameter at any outfall then the facility shall follow the Tier 1 guidelines which require a facility inspection within two weeks and implementation of a mitigation plan within . two months. If during the term of this permit, the sampling results are above the benchmark values, or outside of the benchmark range, for any specific parameter at a specific discharge outfall two times in a' row (consecutive), then the facility shall follow the Tier 2 guidelines which' require a repetition of the steps listed for Tier 1 and also immediately institute monthly monitoring for all parameters at every outfall where a sampling result exceeded the benchmark value for two consecutive samples. 5. You are required to collect all of the analytical and qualitative monitoring samples during representative storm events as defined in Part II Section B. Qualitative monitoring is required regardless of representative outfall status. 6. You are responsible for all monitoring until the renewal permit is issued. See Footnote 1.of Tables 1, 4, and 5. . 7. The flow reporting requirement has been removed per DWQ revised strategy. (The total rainfall and event duration parameters are in this permit, however.) 8.. Vehicle maintenance monitoring has been revised to semi-annually in order to coincide with analytical and qualitative monitoring. This requirement appears in all Individual Stormwater permits, however it only applies to facilities that do vehicle maintenance. If the facility begins vehicle maintenance during the permitted timeframe then the requirements shall app] North Carolina Division of Water Quality (919) 733-7015 1617 Mail Service Center FAX (919) 733-0719 Raleigh, North Carolina-. 27699-1617 On the Internet at http://h2o.enr.state.nc.us/ Mr. Steve Stadelman Novozymes North America, Inc. Permit No. NCS000115 Page 2 Other permit changes: 1. Additional guidance is provided about the Site Plan requirements. The site map must now identify if the receiving stream is impaired and if it has a TMDL established. It must also describe potential pollutants in each outfali. The map requirements are stated more explicitly. And, the site plan must contain a list of significant spills that have occurred in the past three years and also must certify that the outfalls have been inspected to ensure that they do not contain non-stormwater discharges. Additional information is provided in Part II Section A. 2. Additional requirements for the Stormwater Management Plan have been specified in Part II Section A. More details regarding secondary containment are provided. 3. Additional requirements for the Stormwater Pollution Prevention Plan have been specified in Part lI Section A. The plan must also be updated annually to include a list of significant spills and to certify that the outfalls do not contain non-stormwater discharges. 4. The facility must now implement a semi-annual Facility Inspection Program of the site's stormwater management controls as specified in Part 11 Section A. 5. Information regarding the No Exposure Exclusion has been added to this draft permit. If industrial materials and activities are not exposed to precipitation or runoff as described in 40 CFR §122.26(g), the facility may qualify for a No Exposure Exclusion from NPDES stormwater discharge permit requirements. Additional information is provided in Part I Section A. Please submit any comments to me no later than thirty (30) days following your receipt of the draft. Comments should_ be sent to the address listed at the bottom of this page. If no adverse comments are received from the public or from you, this permit will likely be issued in about two months. If you have any questions or comments concerning this draft permit, contact Jennifer Jones at (919) 733- 5083 x 591 or jennifer.jones®ncmail.net Sincerely, Alyy on Environmental Engineer Stormwater Permitting Unit cc: Raleigh Regional Office, Ron Boone (w/attachment) Stormwater Permitting Unit Attachments 2 Michael F. Easley, Governor William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E. Director Division of Water Quality May 3, 2007 Mr. Steve Stadelman Novozymes North America, Inc. 77 Perry Chapel Church Road Franklinton, North Carolina 27525 Subject: NPDES Permit Renewal Application Permit Number NCS000115 Individual Stormwater Permit Franklin County Dear Steve, The Division of Water Quality's Stormwater and General Permits Unit hereby acknowledges in writing the receipt of your renewal application for coverage under NPDES Permit Number NCSOOOI 15on April 4, 2004. The submitted renewal package contained the following items: ➢ Signed application ➢ Site map ➢ Analytical monitoring results summary ➢ Visual monitoring results summary ➢ Best Management Practices summary ➢ Narrative describing significant changes at the permitted facility ➢ Signed Stormwater Pollution Prevention Plan certification I apologize for the long delay in preparing your permit renewal. When we met during a site visit last August I had anticipated having your permit reissued by now. At this time I have scheduled a time to draft your permit during the week ending May 18, 2007, so you can anticipate receiving a draft for your review by the end of .tune. A preliminary review of the submitted renewal application package has been conducted and it appears to be complete. No further information is required at this time. If you have any questions about the renewal process or would like to discuss this letter, please contact me at (919) 733-5083, extension 578. S'. cerel , Atsha Lau Environmental Engineer cc: Raleigh Regional Office Stormwater and General Permits Unit Central Files SWU-238-090199 tCarolina UNIly North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Phone (919) 733-7015 Customer Service Internet: h2o,enr.state.nc.us 512 N. Salisbury St. Raleigh, NC 27604 FAX (919) 733-2496 1-877-623-6748 An Equal OpportunitylAffirmative Action Employer— 50% Recycledl10% Post Consumer Paper August 11, 2006 Mr. Thomas Nagy, President Novozymes North America, Inc. P.O. Box 576 Franklinton, NC 27525 Compliance Evaluation Inspection NPDES Permit No. NCG500115 & NCS000115 Franklin County Dear Ms Rodgers, Michael F. Easley, Governor William G. Ross, Jr., Secretary North Carolina Department of Environment and Natural Resources Alan W. Klimek, P.E., Director Division of Water Quality Mr. Chad Coburn and Mrs. Aisha Lau of the Division of Water Quality, conducted an compliance evaluation inspection of Novozymes North America, Inc. for coverage under the NPDES permits NCG500115 and NCS000115 on August 10, 2006. Mr. Jack Blackmer and Mr. Randy Green represented Novozymes North America, Inc. during the inspection and their assistance was greatly appreciated. Findings during the inspection are as follows: 1) The Stormwater Pollution Prevention Plan (SPPP) and all documentation required were reviewed and no discrepancies or deficiencies were noted. All internal training is done on a yearly basis and is in compliance with permit requirements. Certification that stormwater has been evaluated for the presence of process water was on file as well. 2) The permit, certificate of coverage (COC), and proper up to date analytical and qualitative monitoring documentation were available on site during the inspection. 3) No vehicle maintenance activities occur onsite. 4) Best Management Practices (BMP's) were reviewed and observed. The facility stormwater is kept separate from the process water and conveyances are marked by either blue or red piping respectively. If you have any questions concerning the inspection, please call Mr. Chad Coburn (9I9) 791-4200 or you can email at chad.coburn(cDncmail.net. Sincerely, Chad Coburn Environmental Technician Cc: Central Files RROISWP files Jack Blackmer, same address Randy Green, same address None Caro tua Aduralilb, North Carolina Division of Water Quality Raleigh Regional Office Surface Water Protection Phone (919) 7914200 Customer Service Intemel: h2o.enr.state,no.us 1628 Mail Service Center Raleigh, NC 27699-1628 FAX (919) 571-4718 1-877-623-6748 State of North Carolina Department of Environment and Natural Resources Division of Water Quality Michael F. Easley, Governor William G. Ross Jr., Secretary Alan W. Klimek, P.E., Director March 10, 2004 NOVOZYMES NORTH AMERICA INCORPORATED ATTN: STEVE STADELMAN, OR SUCCESSOR PO BOX 576 FRANKLINTON, NC 27525 Dear Permittee: A F15WA 0-ft NCDENR NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES Subject: NPDES Stormwater Permit Renewal Novozymes North America Incorporated Permit Number NCS000115 Franklin County Your facility is currently covered for stormwater discharge under NPDES Permit NCS000115. This permit expires on September 30, 2004. North Carolina Administrative Code (15A NCAC 2H.0105(e)) requires that an application for permit renewal be filed at least 180 days prior to expiration of the current permit. In order to assure your continued coverage under your permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit. To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed you will find an individual permit renewal application form, supplemental information request, and Stormwater Pollution Prevention Plan certification. Filing the application form along with the requested supplimental information will constitute your application for renewal of your permit. As stated above, the application form must be completed and returned along with all requested information by April 3, 2004 in order for the permit to be renewed by September 30, 2004. Failure to request renewal by April 3, 2004 may result in a civil assessment of at least $500.00. Larger penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility without coverage under a valid stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and could result in assessments of civil penalties of up to $25,000 per day. If you have any questions regarding the permit renewal procedures please contact Bill Mills of the Stormwater and General Permits Unit at (919) 733-5083, ext. 548. Sincerely, Bradley Bennett, Supervisor Stormwater and General Permits Unit cc: Central Files Stormwater and General Permits Unit Files Raleigh Regional Office 1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone 919-733-5083 Fax 919-733-9919 An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper n� in�� imc*V ovozymes APR 1 2004 March 30, 2004 Bill Mills Stormwater and General Permits Unit 1617 Mail Service Center Raleigh, NC 27699-1617 RE: NPDES Stormwater Permit Renewal for Novozymes North America, Inc., Franklin County. Permit # NCS000115 Dear Mr. Mills: Please find attached the renewal application and supplemental information for renewal of permit # NCS000115 for storm`vater discharge at the Novozymes facility in Franklin County. We have made several improvements in our stormwater management program in the past 5 years. The most significant improvements include conversion of several storm drains to process wastewater drains in areas of raw material unloading and certification of our facility to the ISO 14001 environmental management system standard in 2000. During review of data for this permit renewal, we have realized that only one of the four required sampling events was conducted according to the schedule in the permit. We will be conducting 3 additional sampling events for each of the 2 outfalls in 2004 according to the following schedule: Sample interval March - April 2004 May - June 2004 July - August 2004 IPQL� .ulorlc novozyme�� We will forward results of sampling to you as they become available. I apologize for the inconvenience that this may pose. Please contact me at (919) 494-3390 at your convenience if you have any questions or require additional information. Sincerely, Steve A. 14elman Manager of Environmental Operations, NZNA cc: Lee Yarbrough, President, NZNA Paul Rehder, Director of Engineering Services, NZNA SUPPLEMENTAL INFORMATION REQUIRED FOR RENEWAL OF INDIVIDUAL NPDES STORMWATER PERMIT Two copies of each of the following shall accompany this submittal in order for the application to be considered complete: (Do not submit the site Stormwater Pollution Prevention Plan) Initialss 1. A current Site Map from the Stormwater Pollution Prevention Plan. The location of industrial activities (including storage of materials,disposal areas, process areas and loading and unloading areas), drainage structures, drainage areas for each outfall, building locations and impervious surfaces should be clearly noted. 2. A summary of Analytical Monitoring results during the term of the existing permit (if your permit required analytical sampling). Do not submit individual lab reports. The summary can consist of a table including such items as outfall number, parameters sampled, lab results, date sampled, and storm event data. * 3. A summary of the Visual Monitoring results. Do not submit individual monitoring reports. The summary can consist of a table including such items as outfall number, parameters surveyed, observations, and date monitoring conducted. 4. A summary of the Best Management Practices utilized at the permitted facility. Summary should consist of a short narrative description of each BMP's in place at the facility. If the implementation of any BMP's is planned, please include information on these BMP's. _ Z S. A short narrative describing any significant changes in industrial activities at the permitted facility. Significant changes could include the addition or deletion of work processes, changes in material handling practices, changes in material storage practices, and/or changes in the raw materials used by the facility. ✓ 6. Certification of the development and implementation of a Stormwater Pollution Prevention Plan for the permitted facility (Sign and return attached form). * If the final year analytical monitoring of the existing permit term has not been completed prior to filing the renewal submittal, then the last years monitoring results should be submitted within 30 days of receipt of the laboratory reports. (i.e. do not withhold renewal submittal waiting on lab results) Representative storm sampling may now be conducted anytime during the year (the April to November window has been eliminated) and the representative rainfall event is now defined as a storm event that measures greater than 0.1 inches and is preceded by at least 72 hours in which no storm event measuring greater than 0.1 inches has occurred. PERMIT COVERAGE RENEWAL APPLICATION FORM Permit Number National Pollutant Discharge Elimination System NCS000115 Stormwater Discharge Permit THIS APPLICATION MUST BE SIGNED AND RETURNED ALONG WITH TILE REQUESTED SUPPLEMENTAL INFORMATION TO THE DIV. OF WATER QUALITY IN ORDER FOR YOUR FACILITY TO QUALIFY FOR RENEWAL OF YOUR STORMWATER PERMIT NCS000115 The following is the information currently in our database for your facility. Please review this information carefully and make all corrections as necessary in the space provided to the right of the current information. OWNER INFORMATION Owner/Org. Name: NOVOZYMES NORTH AMERICA INC Owner Contact: Mailing Address: Phone Number: Fax Number E-mail address: FACILITY INFORMATION Facility Name: NOVOZYMES NORTH AMERICA INCORPORATED Facility Contact: Facility Address: 77 PERRY CHAPEL CHURCH RD FRANKLINTON, NC 27525 Phone Number: Fax Number E-mail address: PERMIT INFORMATION Permit Contact: STEVE STADELMAN Mailing Address: PO BOX 576 FRANKLINTON, NC 27525 Phone Number: 9194943000 Fax Number: / V E-mail address: ovo 7_ rues C01-►' DISCHARGE INFORMATION Discharge Receiving Water: UT BUFFALO CREEK Stream Class: WSIV NSW Basin: TAR - PAMLICO Sub -Basin #: 03030E Number of outfalls: CERTIFICATION I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief such information is true, complete and accurate. Signature _`6 Date �+_ �� d`�/ lv� Q�� �G�H tl ej" p. �Vr 7^ort ►ri. r�4>� Print or type name of person signing above Title �- arr r Please return this completed renewal application form to: Individual Permit Renewal Attn: Bill Mills Stormwater and General Permits Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 (�L�ii h� ert CG Novozymes North America, Inc. 77 Perrys Chapel Church Road Franklinton, NC 27525 Permit # NCS000115 1. Current Site Maps from the Stormwater Pollution Prevention Plan *See attached maps 2. Summary of Analytical Monitorin results Discharge Characteristics Units Date: 9/4/03 Outfall # # 1 #2 41 #2 # 1 #2 # 1 #2 BOD5 m Il 22 35 COD mg/1 75 48 TSS mg/1 11.3 24 TKN m /l 0.95 1.34 NO2+NO3-N m /l 0.79 1.33 Total - P mg/1 0.35 0.40 Event Duration minutes 90 , 90 Total Flow MG 0.04 0.92 Only the 3Q 2003 sampling event was conducted. Additional sampling will be conducted and reported in 2004. 3. Summary of the Visual Monitoringresults esults *See attached tables: Table -3a Stormwater outfall inspections Table -3b Stormwater conveyance system 4. Summary of the Best Management Practices utilized at Novozymes NA, Inc. BMP Education of employees for environmental awareness ISO 14001 Environmental Management System and corrective / preventative action request system Proper labelin and readily - available MSDS sheets for all materials Covered storage of raw and process materials Secondary containment of above round storage tanks Vapor and dust control devices to minimize the release of air -born contaminants Good housekeeping and equipment maintenance Off site maintenance of company vehicles Proper disposal of generated waste products Maintenance of vegetation and proper erosion control practices Color coding and labeling stormwater drains to increase employee and driver awareness Converting stormwater drains to process drains in high risks ill areas 7 converted, 2 planned in 04) Placement of spill control materials in key areas through out the site 3 permanent and one mobile units Novozymes North America, Inc. 77 Perrys Chapel Church Road Franklinton, NC 27525 Permit # NCS0001 15 5. Significant changes in the industrial activities at the permitted facility The following changes have taken place: Reduced raw material storage on site Finished product customization area that consist of tanks and concrete containment that drains to the process waste water system 6. Stormwater Pollution Prevention Plan Certification *See attached Novozymes North America, Inc. 77 Perrys Chapel Church Road Franklinton, NC 27525 Permit # NCSOOO 115 Table # 3a - NZNA 00-04 Stormwater outfall inspections Date Outfalls Color Odor Clarity Floating Solids Suspended Solids Foam Oil Sheen NoteslOther 311812004 Outfall#1 Clear None Good None None Nano None Outfall # 2 Clear None Good None None Mona None 211912004 Outfall #1 Clear Nana Good None None None None Outfall# 2 Clear None Good More None None None 1114/2004 Outfall #1 Clear None Good More None None None Outfall# 2 Clear None Good None None None None 12/1112003 Outfall #1 Clear None Good None None None None Outfall # 2 Clear None Good None None None None 1111B12003 Outfall#1 Clear None Good None None Nona None Outfall # 2 Clear None Good Nona None None None ' 1012412003 Outfall #1 Clear More Good None None Nona None Outfall # 2 Clear None Good Nona None None None Plastic Strapping in Rocks 9117/2003 Outfall #1 Clear Nona Good Mona None None None Outfall # 2 Clear None Good None Nona None None 8/2112003 Outfall #1 Clear None Good None None None Nona Outfall # 2 Clear None Good None None None None 7/1712003 Outfall #1 Clear None Good None None Nana None Outfall # 2 Clear None Good None None None None 6/2412003 OuNall#1 Clear None Good None None Nana None Outfall # 2 Clear None Good None None None None 512012003 Outfall #1 Clear None Good None None None None Outfall # 2 Clear None Good None None None None 411512003 Outfall #1 Clear I None Good Nana None None None Outfa9 # 2 Clear None Goad None None None None 3/312003 Outfal1 #1 Clear None Goad None None None None OutfalI# 2 Clear None Good None None None None 2114120f13 Outfall #1 Clear None Good None None Nona None Outfall # 2 Clear None Good None None None Nona 11812003 Outfall #1 Clear None Good None None None Nana Outfall # 2 Clear None Good None None None None 12111/2002 Outfall#1 Clear None Good None None None None Outfall # 2 Clear None Good None More None None 11/2&2D02 Outfall #1 Clear None Good None None None None Outfall # 2 Clear None Good None None None None 1011612002 Outfall #1 Clear None Good None None None None Outfall # 2 Clear Nana Good None None None None Plastic strapping in rocks 91512002 Outfall #1 Clear None Good Nona <Nona None Nona Outfali # 2 Clear None Good None None None None 811312002 Outfall #1 Clear None Good None None Nona None Outfall # 2 Clear None Good None None None None 7/1M002 Outfall #1 Clear None Good None None None None 0 tfoll # 2 Clear None Good None None None None 616/2002 Outfall 11 Clear None Goad Nona None None None Outfall # 2 Clear None Good None None None None Novozymes North America, Inc. 77 Perrys Chapel Church Road Franklinton, NC 27525 Permit # NC5000115 5/23/2002 I Oulfall #t Clear None Good None None None Nona Outfall # 2 Clear None Good None None None Nana 4/102002 Outfall #1 Clear None Good YES None None , Nona Grass & Bark in water Outfall # 2 Clear None Good None None None None 3/21/2002 Oulfall#1 Clear None Good None None None None. putfall # 2 Clear None Good None None None None 2/14/2002 Outfall #1 Clear None Good None None Nona None Outfall # 2 Clear None Good None None None None V612002 Outfall #1 Clear None Good None None None None outfall # 2 Clear None Good None None None None 12/6/2001 Outfall #1 Clear None Good None None Nana None Outfall # 2 Clear None Good None None Nona None 1111232001 Outfall #1 Clear None Good None None None None Outfall # 2 Clear None I Good None None None None 10119/2001 Outfall #1 Clear None Good YES None Nona None Pine Bark in water Outfall # 2 Clear Nona Good None None None None 9117/2001 outfall #1 Clear None Good None None None None Outfall # 2 Clear None Good None None None None Plastic Straping in Rocks 81412001 Ouffall #1 Clear None Good None None None None Outfall # 2 Clear None Good None None None Nona 7/17/2001 Outfall 91 Clear None Good YES None None None Grass & Bark in water Outfall # 2 Clear None Good None None None None 61112001 Outfall #1 Clear Nona Good None None None None Outfall # 2 Clear None Good None None Nona None 51412001 Outfall 01 Clear None Good YES None None None Grass & Bark in water Outfall # 2 Clear None Good None None None None 31912001 Outfall #1 Clear None Good None None None None OutfalI # 2 Clear None Goad None None None None lf712000 Outtaff #1 Clear None Good YES None None None Grass & Bark rn water outfall # 2 Clear None Good None None None None 2123/2000 Outfall #1 Clear Nana Good YES None None None Grass & Berk in water Outfall # 2 Clear None Good None None None None 302000 Outfall #1 Clear None Good YES None None None Grass & Bark, in water Outfall # 2 Clear None Good None None None None 411312000 Outfall #1 Clear Nona Good YES None None None Grass & Berk in water Outfall # 2 Clear None Good Nona None None Nona 519/2000 OuMall #1 Clear None Good YES None None None Bark in water Oulfall # 2 Clear None Good None None None None 6/1512000 Outfall #t Clear None Goad YES None None None Mulch & Plastic Boltles in water Outfall # 2 Clear None Good None None None None 7/1212000 Outfall #1 Clear None Goad YES None None None Trash & Mulch in water Outfall # 2 Clear None Good None None Nona I None 8716/2000 Outfall #f Clear None Good None None None None Small amount of trash around outfall Outfall # 2 Clear None Good None None None Nano Small amount of trash around outfall 911212000 Outfall #1 Clear None Good YES None None None Bark in water Outfall # 2 Clear Nano Good None None None Nona 101912000 outfall #1 Clear None Good YES None None Nona Bark in water Outfall # 2 Clear None Good None None None None 1111512000. Outfall #1 Clear Norte Good None None None Nona Outfall # 2 Clear Nana Good None Name None Nana Novozymes North America, Inc. 77 Perrys Chapel Church Road Franklinton, NC 27525 Permit # NCSOOO 115 Table 3b - Stormwater Conveyance System Date Area Erosion Nonstorm water discharge Conveyance system operating as designed Nate 2/6/2004 1 No No Yes 2 No No Yes 3 No No Yes 4 No No Yes 12/11/2003 1 No No Yes 2 No No Yes 3' No No Yes 4 No No Yes 9/17/2003 1 No No Yes 2 No No Yes 3 No No Yes 4 No No Yes 6/19/2003 1 Yes No Yes Erosion - small amount coming of dirt road 2 No No Yes 3 No No Yes 4 No No Yes 2/14/2003 1 Yes No Yes Erosion - smalll amount coming of dirt road 2 No No Yes 3 No No Yes 4 No No Yes 9/5/2002 1 Yes No Yes Erosion - small amount coming of dirt road 2 No No Yes 3 No No Yes 4 No No Yes 6/6/2002 1 Yes No Yes Erosion - small amount coming of dirt road 2 No No. Yes 3 No No Yes 4 No No Yes 11/15/2001 1 Yes No Yes Erosion - small amount coming of dirt road 2 No No Yes 3 No No Yes 4 No No Yes 6/21/2001 1 Yes No Yes Erosion - small amount coming of dirt road 2 No No Yes 3 No No Yes 4 No No Yes 1019/2000 1 Yes No Yes Erosion - small amount coming of dirt road 2 No No Yes 3 No No Yes 4 No No Yes Trailer area, erosion from under steps STORMWATER POLLUTION PREVENTION PLAN DEVELOPMENT AND IMPLEMENTATION CERTIFICATION N.C. Division of Water Quality, Stormwater and General Permits Unit Facility Name: NOVOZYMES NORTH AMERICA INCORPORATED Permit Number: NCSOOOt t5 Location Address: 77 PERRY CHAPEL CHURCH RD FRANKLINTON, NC 27525 County: FRANKLIN "I certify, under penalty of law, that the Stormwater Pollution Prevention Plan (SPPP) document and all attachments were developed and implemented under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information required by the SPPP. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information gathered is, to the best of my knowledge and belief, true, accurate, and complete" "I certify that the SPPP has been developed, signed and retained at the facility location and the SPPP has been fully implemented at the named facility location in accordance with the terms and conditions of the stormwater general permit." "I am aware that there are significant penalties for falsifying information, including the possibility of fines and imprisonment for knowing violations" Sign (according to permit signatory requirements) and return this Certification. DO NOT SEND THE STORMWATER POLLUTION PREVENTION PLAN WITH THE CERTIFICATION. Signature 7 Print or type name of person signing above Date 3 .?Z5 0 Q4�,lr Title Q �J Pi✓a-i7 Urti-s SPPPCenificaiion 2/99