NCS000528_MONITORING INFO_20180815

-----STORNIWATER-DIVISION-CODING-SHEET -- ---
PERMIT NO.
NLS P0p52$
DOC TYPE
❑FINAL PERMIT
f�.. MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
2018 00 15
YYYYMMDD

W
akW ATERS EDGE ENVIRONMENTAL, LLC
1434 C,HESTER ROAD • RALEIGH, NC 27608 • PHONE [phone]
August 15, 2018
NCDEQ
Division of Water Quality Central Files RECEIVED
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617 AUG 1 Zla�a
CENTRAL FILES
Reference: Year 4- Period 2 Stormwater Monitoring Report DWR SECTION
Premiere Fibers Facility
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge Job No. 119-21
To Whom It May Concern:
We are presenting the stormwater monitoring; report for Year 4- Period 2 in 2018. All results are within
required parameters with the exception of Outfall 003 which had benchmark exceedances for pH (5.5
mg/L versus 6-9 mg/L benchmark). We have performed a Tier II inspection and will resampled that
location on the next representative event. It is felt that with acid rain, the pH across North Carolina and
the remainder of the country is decreasing and is not due to any anthropogenic activities at the site. We
have attached the DMR, SDO, and laboratory analytical results -see Appendix A and B). If you have any
questions, or if we may be of further assistance, please contact me at prahn Rwatersedaeenv.com or
919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
18-065

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 000528 or
Certificate of Coverage Number: NCG
e
SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Premiere Fibers COUNTY Anson
PERSON COLLECTING SAMPLE(S) T. Haynes PHONE NO. 704 826.8321
CERTIFIED LABORATORY(S) Pace Lab # 633 79 O
Lab # (SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate complete to
the best of my knowledge.
Part A: Specific Monitoring Requirements
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfa!!
No -
Date"
Sample
50450;
` °„, , . _:.. Y : h:.<
.. _0055G
00530 ';
004[i0
Total Elow
: Total Ra�nfaU'
` Oiir& Grease t�
Totals
pH`T
New Motor"Oils
,:.
Collected
(if applicatilej:,.
v Suspen„ded
;
r Uisage
r�
ano/dd/yr
MGf
inches.,
mill `mg71
Units
STORM EVENT CHARACTERISTICS -
Date 8.2.18�
Total Event Precipitation (inches): 4rG440A-6 1. 3 s'
Event Duration (hours): N/A (only if applicable — see permit.)
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of lines and imprisonment for knowing violations."
Signs re of Permittee
Date
Form SWU-246-112608
Page 2 of 2

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: httn:Hh2o.enr.state.nc.us/su/Forms Doc uments.htm#miscforms
Permit No.: I N I C I S{ 0; 0 10 15 12 18 1 or Certificate of Coverage No.:
Facility Name: Premiere Fibers
County: Anson
Inspector: Thomas Haynes
Date of inspection: 8.2.18
Time of Inspection: 11:00-12:00/10:30 AM
Total Event Precipitation (inches): 1,38
Phone No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report isaccurateand complete to the best of my knowledge:
. ;Z/
(Signature of Permittee or Designee)
1 Outfall Description:
OutfallNo. 001-005
Structure (pipe, ditch, etc.) Pipe to Ditch
Receiving Stream: Buffalo Creek
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturing
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Page 1 of 2
S WU-242-1 l 2608

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy:
1 O 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no
solids and 5 is the surface covered with floating solids:
1 O 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no
solids and 5 is extremely muddy:
lO 2 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S WU-242-1 12608

C6Analytical s
waw.Pacslabacom
August 15, 2018
Mr. Phil Rahn
Waters Edge Environmental
1434 Chester Road
Raleigh, NC 27606
RE: Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Dear Mr. Rahn:
Pace Analytical Services, LLC
265 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on August 03, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

C8'l k 0121
www.paarlabs.com
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Asheville Certification lDs
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginiaNELAP Certification #: 460222
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738 VrginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

� !a
ceAnalytical
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Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Lab ID Sample ID Matrix Date Collected Date Received
92394362001
Outfaii 001
Water
08/02/18 13:00
08/03/18 13:20
92394362002
Outfall002
Water
08/0211813:15
0810311813:20
92394362003
Outfall003
Water
08102/1813:30
0810311813:20
92394362004
Outfail004
Water
08/0211813:45
08/0311813:24
92394362005
Outfall005
Water
08102/1814:00
08/0311813:20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 15

IeAnalximl e
wwW:psoolwa om
0
SAMPLE ANALYTE COUNT
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92394362001
Outfall 001
SM 2540D-2011
NMH
1
PASI-E
SM 4500-H+B-2011
RAY
1
PASI-E
SM 5220D-2011
GC
1
PASI-A
92394362002
Outfall 002
SM 2WD-2011
NMH
1
PASI-E
SM 4500-H+B-2011
RAY
1
PASI-E
SM 52200-2011
GC
1
PASI-A
92394362003
Outfall 003
SM 254OD-2011
NMH
1
PASI-E
SM 4500-H+B-2011
RAY
1
PASI-E
SM 522OD-2011
GC
1
PASI-A
92394362004
Outfall 004
SM 25400-2011
NMH
1
PASI-E
SM 4500-H+8-2011
RAY
1
PASI-E
SM 5220D-2011
GC
1
PASI-A
92394362006
Outfall 005
SM 2WD-2011
NMH
1
PASI-E
SM 4500-H+8-2011
RAY
1
PASI-E
SM 52200-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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PacoAnalyttcal Services, LLC
aceARalytrcal •
205 East Meadow Road - Suite A
Eden, NC 27288
www.ps awmcom
[phone]
ANALYTICAL RESULTS
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Sample: Outfall 001
Lab ID: 92394362001 Collected: 08/02/18 13:00
Received: 08/03/18 13:20 Matrix: Water
Report
Parameters
Results Units Limit MDL OF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
2.8 mg1L 2.5 2.5 1
08106/18 10:11
4500H+ pH, Electrometric EDN
Analytical Method: SM 4500-H+B-2011
pH at 25 Degrees C
6.0 Std. Units 1.0 0,10 1
08/03/18 1&05 H3,1-16
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 52200-2011
Chemical Oxygen Demand
NO mg1L 25.0 12.5 1
08/06/18 17:00 08/07/18 17:00
Sample: Outfall 002
Lap ID: 92394362002 Collected: OB102118 13:15 Received: 08/03/18 13:20 Matrix: Water
Report
Parameters
Results Units Limit MDL OF Prepared Analyzed CAS No.
Qual
25401) Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
ND mg1L 2.5 2.5 1 08/06/18 10:11
4500H+ pH, Electrometric EDN
Analytical Method: SM 4500-H+B-2011
pH at 25 Degrees C
6.3 Std, Units 1.0 0.10 1 08/03/18 15:11
H3,1-16
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
NO mg1L 25.0 12.5 1 08/06/18 17:00 08/07/18 17:00
Sample: Outfall 003
Lab ID: 92394362003 Collected: 08/02/18 13:30 Received: 08/03/18 13:20 Matrix: Water
Report
Parameters
Results Units Limit MDL OF Prepared Analyzed CAS No.
Qual
2640D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
10.1 mglL 2.5 2.5 1 08/06/18 10:12
4500H+ pH, Electrometric EDN
Analytical Method: SM 4500-H+B-2011
pH at 25 Degrees C
5.5 Std. Units 1.0 0.10 1 08/03/18 15:19
H3,H6
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
NO mg1L 25.0 12.5 1 08/06/18 17:00 08/07/18 17:00
Sample: Outfall 004
Lab iU: 92394362004 Collected: 08102118 13:45 Received: 08103118 13:20 Matrix: Water
Report
Parameters
Results Units Limit MDL OF Prepared Analyzed CAS No.
Qual
2640D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
24.6 mg1L 2.5 2.5 1 08/06/18 10:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08115/2018 01:53 PM
without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

cemalyiiml'
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ANALYTICAL RESULTS
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfall 004 Lab lD: 92394362004 Collected: 08/02/18 13:45 Received: 08/03/18 13:20 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
4500H+ pH, Electrometrlc EDN Analytical Method: SM 4500-H+B-2011
pH at 25 Degrees C 6.3 Std, Units 1.0 0,10 1 08/03/18 15:23 H3,1-16
5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand 37.9 mg1L 25.0 12.5 1 08/06/18 17:00 08/07/18 17:00
Sample: Outfall 005
Parameters
Lab ID: 92394362005 Collected: 08/02/18 14:00
Report
Results Units Limit MDL OF
Received: 08103118 1120 Matrix: Water
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
27.5 mg1L 2.5 2.5 1
08/06/18 14:18
4500H+ pH, Electrometrlc EDN
Analytical Method: SM 4500-H+B-2011
pH at 25 Degrees C
6.3 Std. Units 1.0 0.10 1
08/03/18 15:24 H3,1-16
5220D COD
Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
28.4 mg1L 25.0 12.5 1
08/06118 17:00 08/07/18 17:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/15/2018 01:53 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 15

Pace Analytical Services, LLC
C��aa�i^'� • 205 East Meadow Road - Suite A
G 4LJ Eden, NC 27288
www.pacNabo.com [phone]
QUALITY CONTROL DATA
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
QC Batch: 423246 Analysis Method: SM 254OD-2011
QC Batch Method: SM 254OD-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92394362001, 92394362002, 92394362003, 92394362004
METHOD BLANK: 2341681 Matrix: Water
Associated Lab Samples: 92394362001, 92394362002, 92394362003, 92394362004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 2.5 08/06/18 10:03
LABORATORY CONTROL SAMPLE: 2341682
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg/L 250 264 106 90-110
SAMPLE DUPLICATE: 2341683
92394134001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 49.4 96.0 64 5 D6
SAMPLE DUPLICATE: 2341684
92394134002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L ND ND 5
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalXiml e
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QUALITY CONTROL DATA
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC: Batch: 423304
Analysis Method:
SM 254OD-2011
QC Batch Method: SM 254OD-2011
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92394362005
METHOD BLANK: 2341976
Matrix: Water
Associated Lab Samples: 92394362005
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5 2.5 08/06/18 14:10
LABORATORY CONTROL SAMPLE: 2341977
T
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
%Rec Limits Qualifiers
Total Suspended Solids
mg1L
250 274
110 90-110
SAMPLE DUPLICATE: 2341978
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 2341979
Parameter
Total Suspended Solids
92394043001 Dup Max
Units Result Result RPD RPD Qualifiers
mg1L 104 97,8 6 5 D6
92394043002 Dup
Units Result Result
mg1L ND ND
Max
RPD RPD Qualifiers
5
Results presented on this page are In the units Indicated by the "Units" column except where an attemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08115/2018 01:53 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 15

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aceAnalytica!
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QUALITY CONTROL DATA
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
QC Batch: 422991 Analysis Method: SM 4500-H+B-2011
QC Batch Method: SM 4500-H+B-2011 Analysis Description: 4500H+B PH EDEN
Associated Lab Samples: 92394362001, 92394362002, 92394362003, 92394362004, 92394362005
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE DUPLICATE: 2340568
92394181001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
PH at 25 Degrees C Std. Units 7.9 7.9 0 10 H3,H6
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
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Date: 08/15/2018 01:53 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 15

r
Pace Analytical Services, LLC
CA r� 1, l�n�� 205 East Meadow Road - Suite A
Bem l Vr� Eden, NC 27288
wompnobscara
[phone]
QUALITY CONTROL DATA
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
QC Batch: 423337 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92394362001, 92394362002, 92394362003, 92394362004, 92394362005
METHOD BLANK: 2342126 Matrix: Water
Associated Lab Samples: 92394362001, 92394362002, 92394362003, 92394362004, 92394362005
Blank Reporting
Parameter Units Result Limit MOL Analyzed Qualifiers
Chemical Oxygen Demand mg1L ND 25.0 12.5 08/07/18 16:59
LABORATORY CONTROL SAMPLE: 2342127
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 766 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2342128 2342129
MS MSD
92394225002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L NO 100 100 102 121 100 119 90.110 17 3 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/15/2018 01:53 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

ceAnalytical
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Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyle is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not pe reproduced, except in full,
Date: 08/15/2018 01:53 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 15

a
aceAnalytical'
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Premiere Fibers R9-21
Pace Project No.: 92394362
Lab 1D Sample ID QC Batch Method QC Batch
92394382001
Outfall 001
SM
254OD-2011
423246
92394362002
Outfall 002
SM
254OD-2011
423246
92394362003
Outfall 003
SM
254OD-2011
423246
92394362004
Outfall 004
SM
254OD-2011
423246
92394362005
Outfall 005
SM
254OD-2011
423304
92394362001
Outfall 001
SM
4500-H+B-2011
422991
92394362002
Outfall 002
SM
4500-H+B-2011
422991
92394362003
Outfall 003
SM
4500-H+B-2011
422991
92394362004
Outfall 004
SM
4500-H+B-2011
422991
92394362006
Outfall 005
SM
4500-H+B-2011
422991
92394362001
Outfall 001
SM
5220D-2011
423337
92394362002
Outfall 002
SM
5220D-2011
423337
92394362003
Outfall 003
SM
5220D-2011
423337
92394362004
Outfall 004
SM
5220D-2011
423337
92394362005
Outfall 005
SM
5220D-2011
423337
Date: 08/15/2018 01:53 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent or Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytical
Analytical Method Batch
SM 5220D-2011
SM 5220D-2011
SM 5220D-2011
SM 5220D-2011
SM 5220D-2011
423350
423350
423350
423350
423350
Page 12 of 15

Document Name:
.ond1don 6pon Racal
Document No
5-CAR-CS-033-Rev.06
Laboratory receiving samples:
Asheville ❑ Eden[ Greenwood ❑ Huntersville ❑
Client Name;
t uli � ti Project
- -
Courier: ❑Fed Fat ❑UPS EIUSPsS Clem
❑ Commercial ❑Pace ❑other:
Custody Seal Present? QYes Seats Intact? ❑Yes ONO
Document Revised, February 7, 2019
Page 1 of 2
lssu€ng AuthorNY:
Raleigh❑ Mechanicsville❑
Date/initlals Parson Esamininl contenti:� 0-3-ocd
Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑ Other Blalogical Time Frozen?
Thermometer. �} []Yes []No L;W
❑1R Gun It� 61
type of lcr!;t ❑Blue ❑Nana
Cooler Temp ('C):._ 4. S^ Correction Factor, Add/Subtract ('Cj " b-
(') � Temp should be above freezing to 6'C
Cooler TempCorrected C : Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soll (2"0, water sompie)
Did samples orig€na quarantine zone within the United States: CA, IYY, or 5C (check maps)? Did samoesoriglnate from a foreign source (internatispally,
❑Yes 24o indudiegNawa7 and Puerto Ricol7 []Yes(
CAain or LUStOdy Present?
enYes
N*
N/A
J L
Samples Arrived within Hold TIme7
21 es
❑No
NIA
1 2.
Short NoW Time Analysis (a72 hr.)?
Yes
ON.
N/A
1 3.
Rush Turn Around Time Requested?
Ely.
a C.
N A
4.
Sufficient Volume?
es
ONO
N/A
S.
Correct Containers Used?
-Pace Containers used?
45es
es
❑No
No
QN/A
N/A
6.
Containers Intact?
es
No
NIA
7.
Dissolved analysis: 5arn lesF€eldFiltered?
❑Yes
No
❑N/A
8.
Sample Libels Match COC7
-IncludesDatelrime/ID/Analysis Matrix:
es
Elmo
©N/A
9.
Heads ace in VOA Vials (>5-6mm)?
Yes
No
NJA
10.
Trip Blank Present?
©Yes
❑No
N/A
1!
Trip BlankCuslody Seals Present?
fires
ONo
N/A
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? []Yes []No
Lot ID of Olt containers:
CLIERT NOTIFICA-VON/RESOULInON
Person contacted:
Date/Time:
Project Manager SCURF Review: Data: 0 D
Project Manager SRF Review: f 0ate: �� Page 13 of 15

CHAIN -OF -CUSTODY 1 Analytical Request Document
1!;aceAaalgq!1 The Chain -of -Custody Is a LEGAL DOCUMENT. A9 relevant fields must be concpletedl ccurately.
31
Section A Section a Section C
Pago: of 1
Required Client Inlonnalion: Required Project Information: Invoice Infomtaborr.
pY• Report To: J Aiteni pn:
2178019
`_
/v
AddreSS: VGA
Copy To. I
Company Name:
4EGULATORY AGENCY
(
r NPDES GROUND WATER F INKING WATER
4�" UST (" RCRA F- OTHER
EmitlTo: _f
PurchaseOrderrNo.:
lv
Rorerenc :
Far:
Project Name:
Pr
Site Location
F-I—tedDue DaterrAT:
Project
Pace ROW 9,
Requested
' alysls
Filtered
(YIN)
Section D Matrix Codes
z
Repieed Crerd k0mmnrim MAT'r7[X r eeoE
Drinking Wither OW
M
U
COLLECTED
o
Preservathres
>
Water wr
water 1MVy
m
c rrF
COMPOWE
Este
w
Z
SOWSosd SL
SAMPLE ID aI oL
-
$
�_
er
m
a
q
Wipe WP
(A-Z 0-9 I r) Air AR
p
lu
a
z
H
Sample, Ma MUST BE UNIQUE Tissue TS
O
V
a
12
F
{u
V
Other OT
cr
LU
O
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m
0
m
~
a
a
<L
d
O
N
m
t
p
F
DATE
TIME
f]ATE
TIME
y
_
z
z
o
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race Project koJ Lab I.D.
1
CtLv
D o
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2
3
all
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1
d DOLL3
i
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--
1
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(
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7
I
9
10
1
11
12
ADDITIONAL COMMENTS
RELINOWS ED BY I AFFILIATION
DATE
TIME
ACCEPTED BY i AFFILIATION
DATE
TIME
SAMPLE CONDITIONS ,
l3.2b
y $
13
N
ORIGINAL SAMPLER NAME AND SIGNATURE
PRINT Name of SAMPLER: Sit S
}
SIGNATURE of SAMPLER:DATE Signed
162H
E
w
V u
--
V
m
r
{MMIDD -.
"I'MmUnt NOW By rigWng U" loan you are acMptine Pam's NET 30 day payment terms one *Wft rg to Im aerges of h.s% per month K arry iteroirns not paW wldj days. I/ / F-ALL-"20rev_07. 1 SMay-2007

Document Name:
Document No.:
•Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Emptlam: VOA, Coliform, MC, Oil and Grease, DRO/8015 (water) Doc, LLHg
"Bottom half of box is to fist number of bottle
Revised: February
issuing
Office
m u a v V V A y V Z ¢ tl
►9 QT 18 Ln t9 is a
7 a z 4 Q c S A Z i v Ln
4 a r c QQC
z y� d > d Z 7 7
_u u
u T3 ,"d Z; .A aE aEE gE S 4
a a. a '� ° E d d t,J O O ,'3n
� p. Q J 5 > b y In J E � Q.
E}! N�E C©EJ ;, �yyE� t/E� yEr y °: :: ;; {�E E E Eno " yNEy 4lQE� IfQE� `Q�-' E E
^ N ul M r7 N
3 6 3 z A M w, ur
m m i� m m m m m 3 a' �a a a a o i o >> (A 0 ; a :c a
12
__..... _ _ ___.. _ _ _ ._._ . _.._..__._.._......._._.._....pH Adjustment.Log.for.Preserved.Samples __ . _-_----....._ .__-- •.---,._. _ _..__...._
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
I Time presenndan
adjusted
Amount of Preservative
added
Lot if
Note: wnenever mere is a orscrepancy anecung Nonn uarmma compuance samples, a copy or mis rorm wm oe sent w cne Norm r.arouna ucne,n rerunauon unite p.e.
Out of bold, incorrect greservrt0e, out of temp, In<°mect containers. Page 15 of 16

�TERS EDGE ENVIRONMENTAL, LLC
1434 CHESTER ROAD ► RALEIGH, NC 27608 ► PHONE 919,219.5820
May 3, 2018
NCDEQ
Division of Water Quality
Central Files
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617
Reference: Year 4- Period I Stormwater Monitoring Report
Premiere Fibers Facility
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge Job No. R9-21
To Whom It May Concern:
RECEIVIED
MAY 0 9 2018
CENTRAL F!
DWR SECTION
We are presenting the stormwater monitoring report for Year 4- Period I in 2018. All results are within
required parameters with the exception of Outfall 001 which had benchmark exceedances for TSS (159
mg/L versus 100 mg/L benchmark). We have performed a Tier lI inspection and plan to resampled that
location on April 24, 2018 and results, were ND. We have attached the DMR. SDO, and laboratory
analytical results -see Appendix A and B). If you have any questions, or if we may be of further assistance,
please contact me at prahn a,watersedceenv.com or 919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
18-026

STORMWATER DISCHARGE OUTFALL (SOO)
MONITORING REPORT
Permit Number: NCS 000528 or SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Premiere Fibers COUNTY Anson
PERSON COLLECTING SAMPLE(S) T. Haynes PHONE NO. [phone]
CERTIFIED LABORATORY(S) Pace Lab # 633 7' O
Lab # (SIGNATURE OF PERNIITI'EE OR DESIGNEE)
By this signature, I certify that this report is accurate complete to
the best of my knowledge.
Part A: Specific Monitoring Requirements
.Ou#fall `°D tee ff ^ . '-'7'
iToTtalrg
Total
Collected Rainfall SuspendedSol
Solids (TUSS),S.s . y
Permit Beech NIA I I00 120 6-9
Lzl� mold�lyr'_ aches nigh mgll . ; Units K
1 3.1.18 See Below 159 ND 6.2
2 3.1.18 ND ND 6.3
3 3.1.18 26.8 ND 6.2
4 3.1.18 16.9 88.0 6.9
5 3.1.18 27.9 107 6.5
1 4.24.18 See Below ND
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

Part B: Vehicle Maintenance Activity Monitoring Requirements
outran
No.
Hate
Sample
oo
sso.
ooas3o
ooaoo
Total Flow
Total Rainfall
Qil &Grease
"'Total
pH
New Motor Oil
Collected
(if appllcalile)`
,� _
IF
Suspended
Usage
-
�naolddlyr
MG - '
,inches j.
MgA
mg t
Units
aUcno '
STORM EVENT CHARACTERISTICS:
Date 3.1.1814.24.18
Total Event Precipitation (inches): 0.31 /0.45
Event Duration (hours): N/A (only if applicable — see permit.)
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches):
Event Duration (fours):
(only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly 'responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
a 206
Signabke of Permittee Date
Form SWU-246-112608
Page 2 of 2

4
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: httn:Hh2o.enr,state.ne.us/su/Forms Documents.htm#miscforms
Permit No.: IN i C I S� 0.1 0 j o j 512 � 8 or Certificate of Coverage No.: I I I_ I I 1 i
i
Facility Name: Premiere Fibers
County: Anson Phone No. 704.826.8321
Inspector: Thomas Haynes
Date of inspection: 3.1.18/4.24.18
Time of Inspection: 11:00-12:00/10:30 AM
Total Event Precipitation (inches): 0.31/0.45
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
.;i�
�&_ ;Z/-
(Signature of Permittee or Designee)
1 Outfall Description:
Outfall No. 001-005
Receiving Stream
Buffalo Creek
Structure (pipe, ditch, etc.) Pipe to Ditch
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturi
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Light brown
Page 1 of 2
S WU-242-1 12608

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy:
O[ 2 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no
solids and 5 is the surface covered with floating solids:
1 Q 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no
solids and 5 is extremely muddy:
l (D 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242-1 12608

aceAnalyti{cale
wmpaaelabaoom
March 15, 2018
Mr. Phil Rahn
Waters Edge Environmental
1434 Chester Road
Raleigh, NC 27606
RE: Project: Premiere Fibers
Pace Project No.: 92375307
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on March 01, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

acieAnalximl
WWwpaoelabs,rom
Project: Premiere Fibers
Pace Project No.: 92375307
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28604
Florida/NEIAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certiflcation #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VrginialVELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VrginiaNELAP Certification M 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of pace Analytical Services, LLC. Page 2 of 16

Pace Analytical Services, LLC
aceAnalytical • 205 East Meadow Road - Suite A
Eden, NC 27288
www.pscelehacnrs
[phone]
SAMPLE SUMMARY
Project: Premiere Fibers
Pace Project No.: 92375307
Lab ID Sample ID Matrix Date Collected Date Received
92375307001
OutfallI
Water
03/0111812:00
03/01/1816:45
92375307002
Outfall2
Water
03101/1812:15
03101/1816:45
92375307003
Outfall 3
Water
03/01/18 12:30
03/01/18 M45
92375307004
Outfall4
Water
03/01/1812:45
0310111816:45
92375307005
Outfall5
Water
03/01/1813:00
03/01/1816:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 16

Iac
(
e Analytical'
www.pacwBUCam
SAMPLE ANALYTE COUNT
!.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project:
Premiere Fibers
Pace Project No.:
92375307
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92375307001
Outfall 1
SM 2540D
WCP
1
PAS!-E
SM 4500-H+B
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92375307002
Outfall 2
SM 25400
WCP
1
PASI-E
SM 4500-H+B
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92375307003
Outfall 3
SM 2540D
WCP
1
PASI-E
SM 4500-H+B
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92375307004
Outfall 4
SM 2540D
WCP
1
PASI-E
SM 4500-H+B
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92375307006
Outfall 5
SM 2540D
WCP
1
PASI-E
SM 4500-H+B
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 16

r r
aceAnalytical
www psoewmcam
ANALYTICAL RESULTS
Project: Premiere Fibers
Pace Project No.: 92375307
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfall 1
Lab ID: 92376307001 Collected:
03/01/18 12:00
Received: 03/01/18 16:45 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
159 mg1L 3.4
3.4 1
03/02/18 12:24
4500H+ pH, Electrometric EDN
Analytical Method: SM 4500-1-1+13
pH at 25 Degrees C
6.2 Std. Units 1.0
0.10 1
03102/1810:00 H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg1L 25.0
12.5 1
03/14/18 18:06
Sample: Outfall 2
Lab ID: 92375307002 Collected:
03/01/18 12:15
Received: 03/01/18 16:45 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed CAS No.
Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
NO mg/L 6.2
6.2
1
03/02/18 10:38
4500H+ pH, Electrometric EDN
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.3 Sid. Units 1.0
0.10
1
03/02/18 10:00
H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg1L 25.0
12.5
1
03/14/18 18:06
Sample: Outfall 3
Lab ID: 92375307003 Collected:
03/01/18 12:30
Received: 03/01/18 16:45 Matrix: Water
Report
Parameters
Results Units Limit
MDL
OF
Prepared Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
26.8 mg/L 6.2
6.2
1
03/02/18 12:24
06
4500H+ pH, Electrometric EDN
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.2 Std. Units 1.0
0.10
1
03/02/18 10:00
H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg/L 25.0
12.5
1
03/14/18 18:06
Sample: Outfall4 Lab ID: 92375307004 Collected: 03/01/18 12:45 Received: 03/01/18 16:45 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Quat
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 16.9 mg1L 5.2 5.2 1 03/02/18 12:25
Date: 03/15/2018 04:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 16

IceAnalytical'
www.paoelaftcom
ANALYTICAL RESULTS
Project: Premiere Fibers
Pace Project No.: 92375307
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfall4 Lab ID: 92375307004 Collected: 03/01/18 12:45 Received: 03/01/18 16:45 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
4500H+ pH, Electrometrlc EDN Analytical Method: SM 4500-H+B
pH at 25 Degrees C 6.9 Std. Units 1.0 0.10 1 03/02/18 10:00 H6
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 88.0 mglL 25.0 12.5 1 03/14/18 18:06
Sample: Outfall 5
Lab lD: 92375307005 Collected:
03/01/18 13:00
Received: 03/01/18 16:45 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
27.9 mg/L 8.6
8.6 1
03/05/18 13:38
4500H+ pH, Electrometric EDN
Analytical Method: SM 4500-H+B
pH at 25 Degrees C
6.5 Std. Units 1.0
0.10 1
03/02/18 10:00 H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
107 mg/L 25.0
12.5 1
03/14/18 18:06
Date: 03/1512018 04:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Ul,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 16

aceAnalytical
www.pac labs cunt
Project: Premiere Fibers
Pace Project No.: 92375307
QC Batch: 400423
QC Batch Method: SM 2540D
Associated Lab Samples: 92375307002
METHOD BLANK: 2220595
Associated Lab Samples: 92375307002
Parameter Units
Total Suspended Solids mglL
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit MDL Analyzed
ND 2.5 2.5 0310211810:33
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE: 2220596
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 232 93 90-110
SAMPLE DUPLICATE: 2220597
92376071001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Suspended Solids
mglL
ND
ND
5
SAMPLE DUPLICATE: 2220598
92375307002
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Suspended Solids
mg1L
ND
ND
5
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0311512018 04:34 PM without the written consent of Pare Analytical Services, LLC. Page 7 of 16

ac"Analyiical.
wwwpacebtutoom
QUALITY CONTROL DATA
Project: Premiere Fibers
Pace Project No.: 92375307
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: 400479 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92375307001, 92375307003, 92375307004
METHOD BLANK: 22209V Matrix: Water
Associated Lab Samples: 92375307001, 92375307003, 92375307004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mglL ND 2.5 2.5 03/02118 12:20
LABORATORY CONTROL SAMPLE:
2220918
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2221068
Parameter
Units
Total Suspended Solids
mg1L
SAMPLE DUPLICATE: 2221069
Parameter
Total Suspended Solids
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 232 93 90-110
92375071004 Dup Max
Result Result RPD RPD Qualifiers
ND ND 5
92375307003 Dup Max
Units Result Result RPD RPD Qualifiers
mg/1- 26.8 14.2 61 5 D6
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/1512018 04:34 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

� a
ceAnalytrcal e
wwwpacslabscom
QUALITY CONTROL DATA
Project: Premiere Fibers
Pace Project No.: 92376307
QC Batch: 400672 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92375307005
METHOD BLANK: 2222076
Associated Lab Samples: 92375307005
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE:
Parameter
2222077
Units
Total Suspended Solids
mglL
SAMPLE DUPLICATE: 2222078
Parameter
Units
Total Suspended Solids
mglL
SAMPLE DUPLICATE: 2222079
Parameter
Units
Total Suspended Solids
mglL
Matrix: Water
Blank Reporting
Result Limit
ND 2.5
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
MDL Analyzed Qualifiers
2.5 03/05/18 13:33
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 234 94 90-110
92375211001 Dup Max
Result Result RPD RPD Qualifiers
320 351 9 5 06
92375202001 Dup Max
Result Result RPD RPD Qualifiers
43.7 46.9 7 5 D6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 04:34 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

CeAnalytfcal
www.pscefabaoom
QUALITY CONTROL DATA
Project: Premiere Fibers
Pace Project No.: 92375307
QC Batch: 400451 Analysis Method: SM 4500-H+B
QC Batch Method: SM 4500-H+B Analysis Description: 4500H+B pH EDEN
Associated Lab Samples: 92375307001, 92375307002, 92375307003, 92375307004, 92375307005
SAMPLE DUPLICATE: 2220705
92375307001 Dup Max
Parameter Units Result Resuit RPD RPD
pH at 25 Degrees C Sid. Units 6.2 6.3 1
{
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Qualifiers
10 HIS
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the nght of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 04:34 PM without the written consent of Pace Analytical Services, LI.C.
Page 10 of 16

aceAnalytical
wwwpatxfabscom
QUALITY CONTROL DATA
Project: Premiere Fibers
Pace Project No.: 92375307
QC Batch: 401883 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92375307001, 92375307002, 92375307003, 92375307004, 92375307005
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27286
[phone]
METHOD BLANK: 2229021 Matrix: Water
Associated Lab Samples: 92375307001, 92375307002, 92375307003, 92375307004, 92375307005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand mg1L ND 25.0 12.5 03/14/18 18:06
LABORATORY CONTROL SAMPLE: 2229022
Spike
Parameter Units Cone.
Chemical Oxygen Demand mg1L 750
LCS LCS % Rec
Result % Rec Limits Qualifiers
762 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2229023 2229024
MS MSD
92375897001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L ND 100 100 116 102 107 93 90-110 13 3 R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2229025 2229026
MS MSD
92376112001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L 51.0 100 100 154 154 103 103 90-110 0 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 04:34 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

Pace Analytical Services, LLC
CeAna ical 205 East Meadow
Edenn,, NC 27288
fi � ro*416&=" [phone]
QUALIFIERS
Project: Premiere Fibers
Pace Project No.: 92375307
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
06 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 04:34 PM without the written consent of Pace Analytical Services, LLC, Page 12 of 16

aceAnalytiM/6
www,pwsbba.corn
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Premiere Fibers
Pace Project No.: 92375307
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92375307001
Outfall 1
SM
2540D
400479
92375307002
Outfall 2
SM
2540D
400423
92376307003
Outfall 3
SM
2540D
400479
92376307004
Outfall 4
SM
2540D
400479
92375307006
Outfall 5
SM
25400
400672
92376307001
Outfall 1
SM
4500-H+B
400451
92376307002
Outfall 2
SM
4500-1-1+8
400451
92376307003
Outfall 3
SM
4500-1-1+13
400451
92376307004
Outfall 4
SM
4500-H+B
400451
92376307006
Outfall 5
SM
4500-H+B
400451
92376307001
Outfall 1
SM
5220D
401883
92375307002
Outfall 2
SM
5220D
401883
92375307003
Outfall 3
SM
5220D
401883
92375307004
Ouffall 4
SM
52200
401883
92375307005
Outfall 5
SM
5220D
401883
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 04:34 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

Document Name: Document Revised: February 7, 3
Condition U on Recei t(SCUR) PaLe 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 pace Carolinas Qualfty Office
Laboratory receiving samples:
Asheville ❑ Eden Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[]
aleq Name:
Wf, Project
�YL, L� ✓r r_�_l�
Courier: ❑Fed Ex ❑UPS ' ❑USPS �ZycHent
❑ Commercial ❑Pace Other
Custody Seal Present? ❑Yes t19 . Seals Intact? Dyes ❑No
Packing Material: []Bubble Wrap ❑Bubble Bags ZNone ❑ Other Biological Tissue Frozen? P
Thermometer. ❑Yes ❑No []N/A❑IR Gun fi60001 Type of lce: kTW'et ❑Blue ❑None
Cooler Temp ('C): Correction Factor: Add/Subtract ('C)
Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): ❑Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
rites nNo Indodina Hawaii and Puerto Rkol? rlYes riNo
Comments/Discrepancy:
Chain of Custody Present?
Yes
©No
ONIA
1 1.
Samples Arrived within Hold Time?
Yes
[:]No
ONJA
1 2.
Short Hold Time Analysis M hr.
Yes
Na
N/A
3,
Rush Turn Around Time Requested?
OYes
Na
N/A
4.
Sufficient Volume?
UfYes
ON.
ONJA
S.
Correct Containers Used?
-Pace Containers Used?
es
Yes
ON.
❑No
❑NJA
NJA
6.
Containers Intact?
Yes
[]No
N//A
7,
Dissolved analysis: Samples Field Filtered?
ElVes
Na
N A
8.
Sample Labels Match COC?
-Includes Date/time/ID/Analysis Matrix:
es
ONO
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
Qyes
ONo
A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Oyes
Oyes
ONO
[]No
IA
CJ41A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTTON
Field Data Required? ❑Yes []NO
Person contacted: Date/nme:
Project Manager SCURF Review: V Date: 1 ~(
Project Manager SRF Review: Date: t
_-.. _...- ... _._. _... Page 14 of 16

to
CHAIN -OF -CUSTODY 1 Analytical Request Document
-' The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B section C

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L �
aceAnalytical e
wwwPKetebs.carn
April 27, 2018
Mr. Phil Rahn
Waters Edge Environmental
1434 Chester Road
Raleigh, NC 27606
RE: Project: Premiere Fibers
Pace Project No.: 92382133
Dear Mr. Rahn:
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 11

aceAnalytical"
www.perxr'abcGorn
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Project: Premiere Fibers
Pace Project No.: 92382133
Eden Certlflcatlon IDS
206 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 11

, y
acemaIxical
WmPacakftcom
SAMPLE SUMMARY
Project: I Premiere Fibers
Pace Project No.: 92382133
Lab ID Sample ID Matrix Date Collected Date Received
92382133001 Outliall 001 Water 04/24118 11:30 04/25/18 09:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 11

aceAnalytical
WWW..parblsbacom
SAMPLE ANALYTE COUNT
Project: Premiere Fibers
Pace Project No.: 92382133
P
Pace Analy0cal Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytts
Lab ID Sample ID Method Analysts Reported Laboratory
92382133001 Outfall 001 SM 2540D RAY 1 PASI-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 11
G!

H
aceAnalWale
www.pW84bas0m
ANALYTICAL RESULTS
Project: Premiere Fibers
Pace Project No.: 92382133
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfall 001 Lab lD: 92382133001 Collected: 04/24/18 11:30 Received: 04/25/18 09:25 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg1L 2.5 2.5 1 04/25/18 13:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/27/2018 12:44 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 11

ac"Analytical"
rww.pacatsh, oom
QUALITY CONTROL DATA
Project: Premiere Fibers
Pace Project No.: 92382133
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: 407866 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92382133001
METHOD BLANK: 2263021 Matrix: Water
Associated Lab Samples: 92382133001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 2.5 04/25/18 13:46
LABORATORY CONTROL SAMPLE: 2263022
Parameter Units
Total Suspended Solids mg]L
SAMPLE DUPLICATE: 2263023
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 2263024
Parameter
Total Suspended Solids
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
250 258 103 90-110
92382043002 Dup
Units Result Result
mg1L 157 152
92382019001 Dup
Units Result Result
mg1L 746 437
Max
RPD RPD Qualifiers
3 5
Max
RPD RPD Qualifiers
52 5 D6
Results presented on this page ere In the units Indicated by the -Units" column except where an alternate unit to presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/27/2018 12:44 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 11

ceAnalytical
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: Premiere Fibers
Pace Project No.: 92382133
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute,
LABORATORIES
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shag not be reproduced, except in full,
Date: 04/27/2018 12:44 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 11

ceAnalytric'al
wwrvpecefebs.cam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Premiere Fibers
Pace Project No.: 92382133
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytical
Lab ID Sample 10 QC Batch Method QC Batch Analytical Method Batch
92382133001 Outfall 001 SM 2540D 407866
Date: 04/27/2018 12:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, exoept in fuU,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 11

Document Name:
Document Revised: February 7, 2018
Document NO.:
Laboratory receiving samples:
Asheville ❑ Ede at Greenwood ❑
Issuing Autharlty:
Huntersvllle ❑ Raleigh❑ Mechanicsville[]
Client Name:
Project
Courier: ed Fx UPS USPS Client
Commercial ❑pace [3Other:
Custody Seal Present? []Yes 4N6'.' Seals Intact? []Yes [3No
Packing Material: []Bubble Wrap E]Bubble Sags [3 ane ] Other
Thermometer. s� n (r) rj t lres �+.� urn
❑ A Gun Iad Type ar ice: et QEilue of),.
Cooler Temp (*Q: - ----- �^--i- Correction Factor: Add/Subtract ('Cj
`—"— Temp should be above Freezing to VC
Cooler Temp Corrected ('C): _ Osamples out of temp criteria. Samples on ice, coaling process
has begun
USDA Regulated Soil (❑ N/A, water sample]
Did sa mples oil mate in a quarantine zone within the United States: CA, NY, or SC {check maps)7 old samples originate from a foreign source (internationally,
e7
r IYRS INn 0-1- m. Fi is anA Ouorm Riml? r1Vea r1Nn
Cammersts Diacr nty:
Chain of Cost Present?
es
Na
N/A
L
Sam lee Arrived within Hold Time?
V.
Na
NIA
2.
Shari Hold Time Analis (<72 hr.)?
Yes
No
NIA
3.
Rush Turn Around Time Requested?
Yes
ONIA
4.
Sufficient Volume?
es
No
ON A
S.
Correct Containers Used?
-Pace Containers used?
e'
❑No
ON.
QN/A
N/A
S.
Containers Intact?
res
NoON/1k.
7,
Dissolved anaiysls: Sa imples Field Filtered?
QY.
ON.
N A
S.
Sample Labels Klatch COC?
-Indudes oate/Time/ID/Anafysis Matrix:
Yes
' "'% 4-
ONO
©H/A
9.
Heads ate In VOA Vials O"mm)?
❑Yes
QNa
%
N JN
10.
Trip Stank Present?
Trip Blank Custodt Seals Present?
❑Yes
0Yes
ONO
No
N/A
f
rINIA
11.
COMMENTS/SAMPLE DISCREPANCY / Field Data Required? ❑Yes ONO
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date: ✓
Project Manager SAF Review: Date:
Page 9 of 11

CHAIN -OF -CUSTODY / Analytical Request Document
2ax:if afyAal - The Chain of-Custady is a LEGAL DOCUMENT- All relevant fields must be completed accurately,o
rrw.mntahs.mnt
Section A Suction B 5ettian G
page: o1
Requtred Client Information; Required Project Iniarmatm: IrmoiceWometiom,
CDmP Report To: Attention:
r
2228184
/
Add [aC.
Y TO: r
Comte Nam'
REGULATORY AGENCY
Addrr
( NPDES r GROUND WATER I— DRINKING WATER
`-UST r RCRA j✓r-OTHER
Erroll To: l Purchase
Order ND.: /
/
Pace Ouse
Retcra>ca:
Phone: Fax: lorcied
Name: /
axe PrDjaa
w
Site Location
SMarloTATE:
1
Requested Due DatelfAT: Project
Number: Q
7
Paco Pmfns u:
_itequested
Anaiyisis
Filtered
(YIN)
Section O Matrix COdea
: z
Requir"CfieraW minim MATRD((�OOE
9
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COLLECTED
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START E
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WATERS EDGE ENVIRONMENTAL, LLC
34 CHESTER ROAD • RALEIGH, NC 27608 • PHONE [phone]
November 3, 2017
NCDEQ
Division of Water Quality
Central Files
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617
RFt „1=111F_D
JAN 02 2018
DIN" 3ECTUrl
1i`'r4RIMATIW PRQCESSI`€G MR
Reference: Year 3- Period 2 Stormwater Monitoring Report Addendum
Premiere Fibers Facility
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge Job No. R9-21
To Whom It May Concern:
We are presenting the stormwater monitoring report for Year 3- Period 2 in 2017. All results are within
required parameters with the exception of Outfall 005 which had benchmark exceedances for TSS (115
mg/L versus 100 mg/L benchmark) and COD (176 mg/L versus 120 mg/L benchmark). We have
performed a Tier II inspection and have resampled that location. The TSS results were now below the
100 mg/L benclunark (24,7 mg/L); however, the COD was even more elevated at 310 mg/L versus its
benchmark at 120 mg/L. We believe this is due to construction activities which should considerable
subside during the next sampling period. We have attached the DMR, SDO, and laboratory analytical
results -see Appendix A and B). If you have any questions, or if we may be of further assistance, please
contact me at rahn watersed eenv.com or 919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
17-063

w
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 000528 or SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Premiere Fibers COUNTY Anson
PERSON COLLECTING SAMPLE(S) T. Haynes PHONE NO. [phone]
CERTIFIED LABORATORY(S) Pace Lab # 633
Lab # (SIGNATURE OF PERNIITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate complete to
the best of my knowledge.
Part A: Specific Monitoring Requirements
,Oei#fall
Noyes
-"°•. aar-`3.0
1 :Date _
mple M
.._re'.S^,4,L`�.�
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9.12.17
See Below
39.2
ND
6.5
2
9.12.17
ND
ND
6.6
3
9.12.17
5.3
ND
6.5
4
9.12.17
ND
68.0
7.2
5
9.12.17
115
176
6.8
5
10.23.17
24.7
310
6.8
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month?, yes ✓no (if yes, complete Part B)
Farm SWU-246-112608
Page l of 2
r

Part B: Vehicle Maintenance Activity Monitoring Requirements
:Ontfall�'..
Bate ��-
� • 50o5D -...,t
- _ � � V:,
...� ;00556 �
�`-1105313�
-"' 0o4Ulf �
t.�-�T� �,,:�`-
No
Sample; GTotal>Flow
Total Rainfall
Od& GreaseTo#al;��
pH ` r
New-l4iotor�{?hl'
,Collected -
(if appl�cabie)
;SospeadedUsage+
STORM EVENT CHARACTERISTICS:
Date 9.12.17/10.23.17
Total Event Precipitation (inches): 0.2310.34
Event Duration (hours): NIA (only if applicable — see permit_)
(if more than one storm event was sampled)
Date N/A
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit_)
Mail Original and one copy to:
Division of Water Quality
Attn. Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Sign re of Permittee ate
Form SWU-246-112608
Page 2 of 2
i

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit, http://h2o.enr.state.ne.us/su/Forms Documents.htm#miscforms
Permit No.: � W C S 10 10 1 0� 5 1 2 L or Certificate of Coverage No.: I I ) J I 4 j
Facility Name: Premiere Fibers
County: Anson Phone No. 704.826.8321
Inspector: Thomas Haynes
Date of Inspection: 9.12.17/10.23.17
Time of Inspection: 11:00-12:00
Total Event Precipitation (inches): 0.23/0.34
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check yo ur perm it to verify if Qualitative Monitoring must he performed during a representative storm event
(requirements vary).
A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred.,- A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
V2
(Signature of Permittee or Designee)
1 Outfall Description:
Outfall No. 001-005
Receiving Stream: Buffalo Creek
Structure (pipe, ditch, etc.) Pipe to Ditch
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturing
Z Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Light brown
Pagel of 2
S WU-242-112608

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy:
1 0 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no
solids and 5 is'the surface covered with floating solids:
1 2O 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no
solids and 5 is extremely muddy:
lO 2 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
0
Page 2 of 2
SWU-242-112608

aceAnalytical e
wxm•Aa4vpleds.com
i
September 22, 2017
Mr. Phil Rahn
Waters Edge Environmental
1434 Chester Road
Raleigh, NC 27606
RE: Project: Premiere Fibers
Pace Project No.: 92354922
Dear Mr. Rahn:
Pace Analytical Services, LLG
205 East Meadow Road - Suite A
Enclosed are the analytical results for sample(s) received by the laboratory on September 12, 2017.
The results relate only to the samples included in this report. Results reported h erein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me
Sincerely,
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Eden, NC 27288
[phone]
Page 1 or 15

I
eAnalytical
wwwpacelebs.com
i
Project: Premiere Fibers
Pace Project No.: 92354922
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)62$.8921
Asheville Certification Il]s
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Yrginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Vrginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except In full,
without the wrlden consent of Pace Analytical Services, LLC. Page 2 of 15

Pace Analytical Services, LLC
1ceM1alXicalo 2[}5 East Meagow Road -Suite A
Eden, NC 27288
www.paosl ftC0m
{336}623-6921
SAMPLE SUMMARY
Project: Premiere Fibers
Pace Project No.: 92354922
Lab ID Sample ID Matrix Date Collected Date Received
92354922001
Outfall001
Water
09/12/1711:30
09112/1715:30
92364922002
Outfall002
Water
09/1211711:45
09/12/1715:30
92354922003
Outfall003
Water
0911211712:00
0911211715:30
92364922004
Outfall004
Water
09/1211712:15
0911211715:30
92354922006
Outfail005
Water
0911211712:30
0911211715:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, LLC. Page 3 of 15

acMnalytical e
wmpacelabs.mm
i
SAMPLE ANALYTE COUNT
Project: Premiere Fibers
Pace Project No.: 92354922
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Method
Analysts
Analytts
Reported
Laboratory
92364922001
Outfall 001
SM 2540D
CTB
1
PASI-E
EPA 9040
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92364922002
Outfall 002
SM 2540D
CTB
1
PASI-E
EPA 9040
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92354922003
Outfali 003
SM 2540D
CT8
1
PASI-E
EPA 9040
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92364922004
Outfall 004
SM 2540D
CTB
1
PASI-E
EPA 9040
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
92354922005
Outfall 005
SM 2540D
CTB
1
PASI-E
EPA 9040
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Lull,
without the written consent of Pace Analytical Services, LLC. Page 4 of 15

aceAnalytical
e%W-pawaftcom
ANALYTICAL RESULTS
Project: Premiere Fibers
Pace Project No.; 92354922
Pate Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfall 001
Lab ID: 92364922001 Collected: 09/12/17 11:30
Received: 09/12/17 15:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
39.2 mg/L 2.5
2.5 1
09/13/17 15:08
9D40 pH
Analytical Method: EPA 9040
pH
6.6 Std. Units 0.10
0.10 1
09/13/17 13:28 H1,1-16
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg1L 25.0
12.5 1
09/20/17 20:24
Sample: Outfall 00P
Parameters
Lab ID: 92354922002 Collected: 09/12/17 11:45
Report
Results Units Limit MDL DF
Received: 09112/17 15:30 Matrix: Water
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L 2.5
2.5 1
09/13/17 15:08
9040 pH
Analytical Method: EPA 9040
pH
6.6 Std. Units 0.10
0.10 1
09/13/1713:28 H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg1L 25.0
12.5 1
09/20/17 20:24
Sample: Outfall 003
Lab ID: 92364922003 Collected:
09/12117 12:00
Received; 09/12/17 15:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
5.3 mg1L 2.5
2.5 1
09/14/17 12:20
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units 0.10
0.10 1
09/13/17 13:28 H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg/L 25.0
12.5 1
09/20/17 20:24
Sample: Outfall 004 Lab ID: 92364922004 Collected: 09/12/17 12:15 Received: 09/12/17 15:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 2.5 2.5 1 09/14/17 12:21
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 09/22/2017 01:44 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 15

aceAnalytica!'
wwx:psceleba.com
ANALYTICAL RESULTS
Project, Premiere Fibers
Pace Project No.: 92354922
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: Outfall 004
Lab ID: 92354922004 Collected:
09/12/17 12:15
Received: 09/12/17 15:30 Matrix: Water
Report
Parameters
Results Units Limit
MOIL OF
Prepared Analyzed CAS No. Qual
9040 pH
Analytical Method: EPA 9040 '
pH
7.2 Sid. Units 0.10
0.10 1
09/13/17 13:28 1-11,1-16
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
68.0 mg/L 25.0
12.5 1
09/20/17 20:24
Sample: Outfall 005
Lab ID: 92364922005 Collected:
09/12/17 12:30
Received: 09/12/17 15:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
116 mg/L 11.4
11.4
1
09/13/17 15:09
9040 pH
Analytical Method: EPA 9040
pH
6.8 Std, Units 0.10
0.10
1
09/13/17 13:28 H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
176 mg/L 25.0
12.5
1
09/20/17 20:24
Date: 09/22/21317 01:44 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC,
Page 6 of 15

aceAnalytical e
www.pacafapa,00m
i
QUALITY CONTROL DATA
Project: Premiere Fibers
Pace Project No.: 92354922
QC Batch'. 377539 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92354922001, 92354922002, 92354922005
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
(336)e23-8921
METHOD BLANK: 2091869
Matrix: Water
Associated Lab Samples: 92354922001, 92354922002, 92354922005
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5
2.5 09/13/17 15:01
LABORATORY CONTROL SAMPLE:
2091870
Spike
LCS LCS
% Roc
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Suspended Solids
mg1L
250
248 99
90-110
SAMPLE DUPLICATE: 2091872
92354922005
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Suspended Solids
mg1L
115
119
3 5
SAMPLE DUPLICATE: 2094026
92354840001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 360 354 2 5
Results presorted on this page are In the units Indicated by the "Units" column exceptwhere an alternate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 09122/2017 01:44 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 15

aceAnalytical
www.pacelehs.com
Project: Premiere Fibers
Pace Project No.: 92354922
QC Batch: 377697
QC Batch Method: SM 2540D
Associated Lab Samples: 92354922003, 92354922004
METHOD BLANK: 2092616
Associated Lab Samples: 92354922003, 92354922004
Parameter Units
Total Suspended Solids mglL
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result limit MDL Analyzed Qualifiers
ND 2.5 2.5 09/141171216
LABORATORY CONTROL SAMPLE:
2092617
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result %Rec
Limits Qualifiers
Total Suspended Solids
mglL
250 258 103
90-110
SAMPLE DUPLICATE: 2092618
92354978003 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Suspended Solids
mglL
5380 4850
10 5 D6
SAMPLE DUPLICATE: 2092619
92355122001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 343 336 2 5
Results presented on this page are In the units Indicated by he "Units" column except where an alternate unit Is presented to the right of the rosulL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2017 01:44 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 15

/5aceAnalyfical'
j www.Aacela(u,tam
f
QUALITY CONTROL DATA
Project: Premiere Fibers
Paco Project No.: 92354922
QC Batch: 377537 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92354922001, 92354922002, 92354922003, 92354922004, 92354922005
SAMPLE DUPLICATE: 2091860
Parartieter
pH
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
92354922001 Dup Max
Units Result Result RPD RPD Qualifiers
Std, Units 6.5 6.6 1 9 H1,H6
Results presented on this page am In the units indicated by the "Units" column except where an alternate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2017 01:44 AM without the written consent of Pace Analytical Services, I.I.C.
Page 9 of 15

accAnalytical e
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t
QUALITY CONTROL DATA
Project: Premiere Fibers
Pace Project No.: 92354922
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: 378465
Analysis Method: SM 5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92354922001, 92354922002,
92354922003, 92354922004, 92354922005
METHOD BLANK: 2097002
Matrix: Water
Associated Lab Samples: 92354922001, 92354922002,
92354922003, 92354922004, 92354922005
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0 12.5 09/20/17 20:24
LABORATORY CONTROL SAMPLE: 2097003
Spike LCS LCS
% Rec
Parameter Units
Cone. Result % Rec
Limits Qualifiers
Chemical Oxygen Demand mg/L
750 754 101
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2097004 2097005
MS MSD
92354922001
Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Cone. Result Result
% Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L NO
750 750 688 683
90 90 90-110 1 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2097006 2097007
MS MSD
92355015001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L 80.0 750 750 777 768 93 92 90-110 1 3
Results presented on this page are In the units indicated by he "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/22/2017 01:44 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 15

Z
wwwpacelabx=
Pace Analytical Services, LLC
206 East Meadow Road • Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: Premiere Fibers
Pace Project No.: 92354922
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzeno using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethyiv[nyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acroleln and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAS [-A Pace Analytical Services -Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 09/22/2017 01:44 AM without the written consent of Pace Analytical Services, I.I.C. Page 11 of 15

/Ice Analytical e
www.paoslabacoM
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Premiere Fibers
Pace Project No.: 92354922
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID Sample 1D QC Batch Method QC Batch Analytical Method
92354922001
Outfall 001
SM 2540D
377539
92364922002
Outfall 002
SM 2540D
377539
92364922003
Outfall 003
SM 2540D
377697
92354922004
Outfall 004
SM 2540D
377697
92354922005
Outfall 006
SM 2540D
377539
92364922001
Outfall 001
EPA 9040
377537
92364922002
Outfall 002
EPA 9040
377537
92354922003
Outfall 003
EPA 9040
377537
92354922004
Outfall 004
EPA 9040
377537
92364922005
Outfall 005
EPA 9040
377537
92364922001
Outfall 001
SM 5220D
378465
92354922002
Outfall 002
SM 5220D
378465
92364922003
Outfall 003
SM 5220D
378465
92354922004
Outfal1004
SM 5220D
378465
92364922005
Outfall 006
SM 5220D
378465
Date: 09/22/2017 01:44 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 12 of 15

Document Name: Document Revised: August 4, 2017
�acefil1r71�XiCal" Sam le Condition Upon Recel t SCUR Page 1 of 2.
Document No.: Issuing Authority;
F-CAR-CS-633-Rev.04 Pace Quality Office
Laboratory receiving sarnples:
Asheville ❑ Edeng Greenwood ❑ Huntersville
le t Name:
r- Project 0:
Courier: []FedEx ❑UPS USPS Client
❑ Commercial ❑Pace ❑Other:
Custody Seal Preterit? ❑Yes E: N' Seals Intact? Dyes ❑No
Packing Material: ❑Bubble Wrap ❑Bubble Bags 4None
Thermometer: [% IRGun ID: -�b �— Type of Ice: �"re
Correction Factor: Cooler Temp Corrected ('Cl:
Date/initials Person Examining Contents:
❑ Other Biological Tissue Frozen?
❑Blue Done []Yes []NO ❑N/A
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC )check maps)? Did samples originate from a foreign source (internationally,
Mync MAJ. Inrludlnn HA-11 and Puerto Rlenl? I_IYAz I77INn
CommentsJGlsere one :
ChalnofCustod Present?
Yes
QNo
NIA
1.
Samples Arrived within Hold Time?
Yes
ot,.
N A
2.
Short Hold.TimeAnai sIs 1<72 hr.)?
Yes
o
ONIA
3.
Rush Turn Around Time Requested?
Yef
No
N/A
4.
Suffl6ent Volume?
ffies
ONO
N A
S.
Correct Containers Used?
-pace Containers Used?
es
ONO
QNO
❑N/A
N/A
6.
Containers Intact?
Yet
ONO
NIA
7.
g..
Dissolved analysis; Samples Field Filtered? es No A
Sample Labels Match COC?
-includes Date/Time/ID/Analysis Matr{x:
y Yes
!� ✓
(:]No
❑NIA
9.
Heads are in VOA Vials ?S-6mm)?
Yes
ONO
C A
to..
Trip. Blank Present?
Trip Blank Custody Seals present?
[]Yes
❑Yes
❑Na
ONO
❑ JA
N a '
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: Date/Time:
Comments/Sample Discrepancy:
Field Data Required? ❑Yes []NO
Lot ID of split containers; u
Project Manager SCURF Review: Date: / 1 Z 'I l
Project Manager SRF Review-, Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 13 of 15

CHAIN -OF -CUSTODY / Analytical Request Document
- The Chairs -of -Custody is a LEGAL DOCUMENT. Alt relevant fields must be completed accurately.
Section A Section a Section C
Requited Gient Information: Required Project Information: Imam Information: page : T Of T
Company. Waters Edge Environmental Report To: Thomas I Atlentiarc
Address: 4901 Watefs Edge Dr. Copt. To: Cor:pany Name:
Suits 201, R'aWigk NC 27506
Mare=
Email:
Purchase order F.
Pace Quote.
i
Prom: Fax
Pro>eS;t Name= Premiere Fbers
Pace Project Wmuvjor MfiSti.tltr55 lat>s.mrr>,
Requested Due Date:
Pmjed 9. - f
Paco Profire is: -
NC
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COLLECTED
x
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A

aceAnalyrical `
{ www[paoslabscom
October 28, 2017
Mr. Phil Rahn
Waters Edge Environmental
1434 Chester Road
Raleigh, NC 27606
RE: Project: Premiere Fibers R9-21
Pace Project No.: 92360219
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on October 23, 2017.
The results relate only to the samples included in this report. Results reported h erein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

5aceAnaljdical
1�lwsrw.pacelabacam
Project: .,Premiere Fibers R9-21
Pace Project No.: 92360219
Pace Analytical Services, LLC
205 East Meadow Road - Suits A
Eden, NC 27288
[phone]
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #; M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiafVELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification M 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13

aceAnalytical
Iwwwpacelabs.=n
f
Project: Premiere Fibers R9-21
Pace Project No,: 92360219
Lab 11;) Sample 10
SAMPLE SUMMARY
Matrix Date Collected Date Received
92360219001 OUTFALL 006 Water 10/23/17 12:30 10/23/17 16:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.I.C.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 13

aceAnalyircal
/ www.pecelabs.com
{
SAMPLE ANALYTE COUNT
Project: Premiere Fibers R9-21
Pace Project No.: 92360219
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytes
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92360219001 OUTFALL 005 SM 2540D
CTS
1
PASI-E
EPA9040
SAM1
1
PASI-E
SM 5220D
NAL
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the wriHen consent of Pace Analytical Services, LLC, Page 4 of 13

aC`Analytical e
www.pacefehs.mm
ANALYTICAL RESULTS
Project: Premiere Fibers R9-21
Pace Project No.: 92360219
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: OUTFALL 006
Lab lD: 92360219001 Collected:
10/23/17 12:30
Received: 10/23/17 16:30 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. dual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
24.7 mg1L 3.5
3.5 1
10/25/17 13:19
9040 pH
Analytical Method: EPA 9040
pH
6.8 Std. Units 0.10
0.10 1
10/24/17 09:15 Fib
5220D COD
Analytical Method: SM 52200
Chemical Oxygen Demand
310 mg1L 25.0
12.5 1
10/27/17 20:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/28/2017 10:38 AM wrthout the written consent of Pace Analytical Services, LLC.
Page 5 of 13

/5a'ceAnalytical'
waw.patx7aDa.rxwn
QUALITY CONTROL DATA
Project: Premiere Fibers R9-21
Pace Project No.: 92360219
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QC Batch: 383874
Analysis Method: SM 2540D
OC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92360219001
METHOD BLANK: 2127441
Matrix: Water
Associated Lab Samples: 92360219001
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5
2.5 10/25/17 13:13
LABORATORY CONTROL SAMPLE: 2127442
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg1L
250 242 97
90-110
SAMPLE DUPLICATE: 2127443
92360156001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Suspended Solids
mg1L
ND 91.5
5
SAMPLE DUPLICATE: 2127444
92360312001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Suspended Solids
mg1L
604 597
17 5 D6
Results presented on this page are In the units Indicated by the "Units" colurm except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/28/2017 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

1eAnalyficale
—pacalabacdm
Project: Premiere Fibers R9-21
Pace Project No.: 92360219
QC Batch: 383677
QC Batch Method: EPA 9040
Associated Lab Samples: 92360219001
SAMPLE DUPLICATE: 2120260
Parameter Units
PH Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9040
Analysis Description: 9040 pH EDEN
92360219001 Dup
Result Result RPD
6.8 6.9 1
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27268
[phone]
Max
RPD Qualifiers
9 H6
Results presented on this page are In the units Indicated by the "units" column except where an ahamate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shO not be reproduced, except In full,
Date: 10/28/2017 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

aceAnalytical
1 www.pmlabs.com
II
QUALITY CONTROL DATA
Project: Premiere Fibers R9-21
Pace Project No.: ''92360219
QC Batch: 384021 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92360219001
METHOD BLANK: 2128397 Matrix: Water
Associated Lab Samples: 92360219001
Blank Reporting
Pace Analytical Services, I.LC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Parameter
Units
Result
Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand
mg1L
NO 25.0 12.5 10/27/17 20:49
LABORATORY CONTROL SAMPLE:
2128398
Spike
LCS LCS % Rec
Parameter
Units
Cane.
Result % Rec Limits Qualifiers
Chemical Oxygen Demand
mg1L
750
754 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128399 2128400
MS MSD
92359949002 Spike Spike MS MSD MS MSD % Reo Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L ND 750 750 794 792 105 105 90-110 0 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2128401 2128402
MS MSD
92360289001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L 65.0 750 750 866 859 107 106 90-110 1 3
Results presented on this page are In the units Indicated by he "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/28/2017 10:38 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

W aceAnalytical e
www.paaalabs.com
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Project: Premiere Fibers 129-21
Pace Project No.: 92360219
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC institute.
LABORATORIES_,
PASI-A Pace Analytical Services - Asheville
PAST-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/2&2017 10:38 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

Pace Analytical Services, LLC
aceAnalytical a 205 East Meadow Road - Suite A
Eden, NC 27288
wwwpacslabs.oam
[phone]
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Premiere Fibers R9-21
Pace Project No.: �'92360219
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92360219001
OUTFALL 005
SM 2540D
383874
92360219001
OUTFALL 005
EPA 9040
383677
92360219001
OUTFALL 006
SM 5220D
384021
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 10/28/2017 10:38 AM without the written consent of Pace Analytical Services, LLC, Page 10 of 13

aceAnalylrcal
Document Name:
Sample Condition Upon Recei t SCUR
Document Revised: August 4, 2017
Page 1 of 2
Document No.:
F-CAR-CS-033•Rev,04
Issuing Authority:
Pace Q"!q Office
Laboratory receiving samples:
_.. ............ Ashevifltr.❑ _Edeng Greenwood ❑ Huntersville ❑ Raleigh[❑ Mechanicsville❑
Courier:
❑ Commercial
Custody Seal Present?
Packing Material:
Thermometer:
IR Gun ID:
Correction Factor:
Client Name:
Protect
Nfvcifos Uf C.
❑Fed Ex F-]UPV CUSPS Client
❑Pace ❑0lher;
❑Yes eNo Seals intact? ❑Yes ONO
Date/Initials Parton Exam€ningContents:�7/ 7
❑Bubble Wrap ❑Bubble Bags one El other Biological Tissue Frozen?
�� �Type of r wet ❑Blue ❑None ❑Yes ❑Na ❑N/A
I
Cooler Temp Corrected J'CJ; ( Temp should be above freezing to 6T
[]Samples out of tamp criteria, Samples on Ice, cooling process
has begun
USDA Regulated Soil i ❑ NIA, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? aid samples originate from a foreign source {internationally;
Flyes f—INn Includina Haarall and Puerto Rlcol? f-IYes nNo
Comments/Discrepancy;
Chain or Custody Presents
Yes
fING
N/A
1,
Samples Arrived within Hold rime?
Yes
CINO
N A
2.
Short Hold Time Analysis 02 hr.)?
Yes
-ONO
N/A
3.
Rush Turn Around Time Requested?
JJY.
o
N/A
4.
Sufficient Volume?
Aives
[]NO
N A
5.
Correct Containers Used?
-Pace Containers Used?
-fJYes
17yes
❑No
No
❑N1A
N/A
6.
Containers Intact?
QYes
r1N.
N/A
7.
Dissolved analysis: Samples Field Filtered?
OVes
No
ZEJNLA
8.
Sample Labels Match COO
-Includes Date/Time ID Anal sis Matrix:
�©` Yes
1
❑No
❑N/A
9.
Heads ace in VOA Vials P5.6mmJ?
OYeS
ND
A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
0Yes
[]No
0 No
N/A
VfNJA
11.
CLIENT NOTOICATIDN/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Date/Time:
Field Data Required? ❑Yes []NO
Lot ID of split containers:
Project Manager SCURF Revlew: Date: 10 2 �s +
Project Manager SRF Review: v Date: _ I O Z'71% %
Note: whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Cffice (Le.
Out of hold, incorrect pteservative, out of temp, incorrect containers)
Page 11 of 13

0
;ZeLa& icat'
.I mm
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. AN relevant fields must be completed a=rately.
Page.
Section A Section B Section C
a
Required Client Information: - Required Projw lodomoa5on'. .Invoice Information:
Company Report To: f Attention:
%
2177514
t-' titir• / /
ess:
Copy To: 1
Company Name:
REGULATORY AGENCY
Address.
F NPDEs r GROUNDWATER r DRINKING WATER
r UST (RCRA OTHER
Emal To: Z _ % y
PetrrhaSQ Order NO.:
� I
Pam oude
, r �C._(1�jAf
C��
Reform :
Phone:
Fax:
Project Name:
/� y r'.�� tP
Freida
flr
Site Locatlriti
STATE
j r
^
Requested Duo 0atefTAT:
Project mmtn r: �.V ^^t
x
Pxe Prem x
Requested
AnalysisFittered
(YIN)
Section D Matrix Codes
RgWredGkint k>krrnsren MATRoc r CODE
'
COLLECTED
PreservativesDrInb
>`..
ViateIrlg Water OW
Wast WT
U
Y it.JlPl f1
Waste Water WWII
Produa P
m
STYE
UJ
z
1
f
sawso� SL
SAMPLE ID 00
L
�
v
cc
�
Mpe ,
(A-Z. 0-g f :) Air AR
w
o0
-
a
a
Z
as
Fn
o
Sample Ds MUST BE LINIQUE Tissue TS
V
a
�:
i
Other OT
p
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WATERS EDGE ENVIRONMENTAL, LLC
1434 CHESTER ROAD • RALEIGH, NC 27608 • PHONE [phone]
April 21, 2017
NCDEQ
Division of Water Quality
Central Files
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617
RECEIVED
Reference: Year 3- Period I Stormwater Monitoring Report
Premiere Fibers Facility
APR 2 6 2017
Ansonville, North Carolina
Stormwater Permit No. NCS000528
CENTRAL
AL FILES
D1NR SECTION
Waters Edge Job No. R9-21
To Whom It May Concern:
We are presenting the stormwater monitoring report for Year 3- Period 1 in 2017. All results are within
required parameters We have attached the DMR, SDO, and laboratory analytical results -see Appendix A
and B). If you have any questions, or if we may be of further assistance, please contact me at
prahn c�r�,watersedgeenv.com or 919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
- � � 9_j_�e ; � � /_'_ -
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
17-028

I
Permit Number: NCS 000528
Certificate of Coverage Number: NCG
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
or
SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Premiere Fibers
PERSON COLLECTING SAAWLE(S) T. Haynes
CERTIFIED LABORATORY(S) Pace Lab## 633
Lab ##
Part A: Specific Monitoring Requirements
COUNTY Anson
PHONE NO. [phone]
(SIGNATURE OF PERNUTrEE OR DESIGNEE)
By this signature, I certify that this report is accurate complete to
the best of my knowledge.
Outfall
Y s"
Date
�; % sP 4¢
�s de'
' '�p't- I.
•: P €
q I
�`
_ i°S.'.
.
NoR 4
Sample ' :xT01al
Collected:'
:#
Rainfall
Total-
Saspenaed
a
Salads
'160
COD"`6
3
f- � ,124
-`
:.
:#
-
C
�;
,
molddiyr
m
mP�
_ Unfts
o
1
4.6.17
See Below
5.0
N-D
6.4
2
4.6.17
5.5
ND
6.5
3
4.6.17
2.6
ND
5.9
4
4.6.17
23.2
34.0
6.3
5
4.6.17
51.3
63
6.4
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month.? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

Part R: Vehicle Maintenance Activity Monitoring Requirements
%,Outfalt
Date
tC�4
,! 1Ycr
tiSQC1o4�i
SaR�ple
SAT©tai Flow
Total Ra6fall ?4
, Q1 Sc Crease
Total
i 'H
New`t4tator 6i1
Coilectd
(rf applicble) ;
j
: i
Sus eRsfed
P,
i
Usage
z t':.p a E
-
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fir' �
€ II
k €
E
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. -: ¢{g„
4:,:il::.
rtRty/dd
-
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-
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iSl�•_'
- RI
UIiILS _li
9UR10;
I
STORM EVENT CHARACTERISTICS:
Date 4-6-17
Total Event Precipitation (inches): 0.22
Event Duration (hours): N/A (only if applicable — see permit.)
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches).
Event Duration (hours):
(only if applicable — see.permit-)
Mail Original and one copy to:
Division of Water Quality
Attn: Central piles
1617 Mail Service Center
Raleigh, North Carolina 27699-161.7
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signa r of Permittee
� 2r7 t
Date
Form SV U-246-112608
Page 2 of 2

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please visit: htt :1/h2o.enr.state,nc,us/su/Forms DOCuments.htm#miscforms
Permit No.: I N 1C C i S 10 i 0; 0 5 i 2; 8 or Certificate of Coverage No.:
Facility Name: Premiere Fibers
County: Anson
Inspector: Thomas Haynes
Date of Inspection: 4.6.17
Time of Inspection: 11:00-12:00
Total Event Precipitation (inches): 0.22
Phone No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
l Outfall Description:
Outfall No. 001-005
Receiving Stream: Buffalo Creek
Structure (pipe, ditch, etc.) Pipe to Ditch
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturina
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
_Light brown
Page I of 2
S W U-242-112608

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy:
O 2 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no
solids and 5 is the surface covered with floating solids:
O 2 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no
solids and 5 is extremely muddy:
O 2 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242-1 12608

5ac 16 A na ly fical
www.pacelabs.crom
1
1
April 13, 2017
Mr. Phil Rahn
Waters Edge Environmental
1434 Chester Road
Raleigh, NC 27606
RE: Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on April 06, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
I�'��v/"
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Enclosures
ACC$
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

aceAnalytical
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li
Project: PREMIERE FIBERS 119-21
Pace Project No.: 92336232
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Asheville Certification IDs
2225 Riverside Drive, Asheville, INC 28804
Florida/NELAP Certification #. E87648
Massachusetts Certification* M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification * 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Cerfification #. 99030001
VirginiaNELAP Certification M 460222
North Carolina Wastewater Certification M 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 14

11ceAnalyfical'D
Hwwpacelabs.mm
I
i
SAMPLE SUMMARY
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
Lab ID
Sample Io
Matrix
Date Collected
Date Received
92336232001
OUTFALL 001
Water
04/06/17 11:00
04/06/17 14A0
92336232002
OUTFALL 002
Water
04/06/17 11:15
04/06/17 14:40
92336232003
OUTFALL 003
Water
04/06/17 11:30
04/06/17 14:40
92336232004
OUTFALL 004
Water
04/06/17 11:45
04/06/17 14:40
92336232005
OUTFALL 005
Water
04/06/17 12:00
04/06/17 14:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 14

15a'ce Analytical"
www.pweiabs.com
1
SAMPLE ANALYTE COUNT
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
Pace Analytical Services, LI.0
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Method
Analysts
Anaiytes
Reported
Laboratory
92336232001
OUTFALL 001
SM 2540D
CTB
1
PASI-E
EPA 9040
RAY
1
PASI-E
SM 5220D
MDW
1
PASI-A
92336232002
OUTFALL 002
SM 2540D
CTB
1
PASI-E
EPA 9040
RAY
1
PASI-E
SM 52201D
MDW
1
PASI-A
92336232003
OUTFALL 003
SM 2540D
CTB
1
PASI-E
EPA 9040
RAY
1
PASI-E
SM 5220D
MDW
1
PASI-A
92336232004
OUTFALL 004
SM 2540D
CTB
1
PASI-E
EPA 9040
RAY
1
PASI-E
SM 5220D
MDW
1
PASI-A
92336232005
OUTFALL 006
SM 2540D
CTB
1
PASI-E
EPA 9D40
RAY
1
PASI-E
SM 5220D
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 14

aceAnalytical
""acelabs.com
ANALYTICAL RESULTS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden,NC 27288
[phone]
Sample: OUTFALL 001
Lab ID: 92336232001 Collected:
04/06/17 11:00
Received: 04106M7 14:40 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
5.0 mg1L 2.5
2.5 1
04/11/17 13:37
9040 pH
Analytical Method: EPA 9040
pH
6.4 Sid. Units 0.10
0.10 1
04/07/17 14:55 H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg1L 25.0
12.5 1
04/13/17 22:18
Sample: OUTFALL 002
Parameters
Lab ID: 92336232002 Collected:
Report
Results Units Limit
04106/17 11:15
-
MDL DF
Received: 04/06/17 14:40 Matrix: Water
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
5.5 mg1L 2.5
2.5
1
04/11/17 13:37
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units 0,10
0.10
1
04/07/17 14:55 H1.H6
5220D COD
Analytical Method: SM 52200
Chemical Oxygen Demand
ND mg1L 25.0
12.5
1
04/13/17 22:18
Sample: OUTFALL 003
Lab ID: 92336232003 Collected: 04/06/17 11:30
Received: 04/06/17 14:40 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
2.6 mg1L 2.5
2.5 1
04/11/17 13:37
9040 pH
Analytical Method: EPA 9040
pH
5.9 Sid. Units 0.10
0.10 1
04/0711714:55 1-11,1-16
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg1L 25.0
12.5 1
04/13/17 22:18
Sample: OUTFALL 004 Lab ID: 92336232004 Collected: 04106/17 11:45 Received: 04/06/17 14:40 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 23.2 mg1L 6.2 6.2 1 04111/17 13:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/13/2017 11:08 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 14

2aceAnalyfical'
� www.perelabs.crom
r
ANALYTICAL RESULTS
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
Sample: OUTFALL 004 Lab ID: 92336232004 Collected: 04/06/17 11:45 Received: 04/06/17 14:40 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
9040 pH Analytical Method: EPA 9040
pH 6.3 Sid. Units 0.10 0.10 1 04/0711714:55 H1,1-16
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 34.0 mg/L 25.0 12.5 1 04/13/17 22:18
Sample: OUTFALL 005
Lab ID: 92336232005 Collected:
04/06/17 12:00
Received: 04/06/17 14:40 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
51.3 mg1L 5.9
5.9 1
04111/17 13:39
9040 pH
Analytical Method: EPA 9040
pH
6.4 Sid. Units 0.10
0.10 1
04/07/17 14:55 H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
63.0 mg1L 25.0
12.5 1
04/13/17 22:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/1312017 11:08 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14

aceAnalytical
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1
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
QC Batch: 356168 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92336232001, 92336232002, 92336232003, 92336232004, 92336232005
METHOD BLANK: 1975713 Matrix: Water
Associated Lab Samples: 92336232001, 92336232002, 92336232003, 92336232004, 92336232005
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Total Suspended Solids mg1L ND 2.5 2.5 04/11/17 13:29
LABORATORY CONTROL SAMPLE: 1975714
Spike LCS LCS
Parameter Units Cone. Result % Rec
Total Suspended Solids mg1L 250 240 96
SAMPLE DUPLICATE: 1975715
Parameter
Total Suspended Solids
92336187001 Dup
Units Result Result RPD
mg1L 118 112
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Qualifiers
% Rec
Limits Qualifiers
90-110
Max
RPD Qualifiers
5 5
SAMPLE DUPLICATE: 1975716
92336232005 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 51.3 51.9 1 5
Results presented art this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04113/2017 11:08 PM without the written consent of Pace Analytical Services, LLC,
Page 7 of 14

aXAnalytical
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1
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
QC Batch: 355796 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92336232001, 92336232002, 92336232003, 92336232004, 92336232005
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE DUPLICATE: 1973772
92336158001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH Std. Units 5.9 5.9 0 9 N1,W6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presanted to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
This report shO not be reproduced, except in full,
Date: 04/13/2017 11 i08 PM without the written consent of Pace Analytical Services, LLC, Page 8 of 14

aceAnalytical
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QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
QC Batch: 356633 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 52200 COD
Associated Lab Samples: 92336232001, 92336232002, 92336232003, 92336232004, 92336232005
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
METHOD BLANK: 1978556 Matrix: Water
Associated Lab Samples: 92336232001, 92336232002, 92336232003, 92336232004, 92336232005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 12.5 04/13/17 22:18
LABORATORY CONTROL SAMPLE: 1978557
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 751 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1978568 1978559
MS MSD
92336187001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L 50.0 750 750 831 829 104 104 90-110 0 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1978560 1978561
MS MSD
92336174002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits 'RPD RPD Qual
Chemical Oxygen Demand mg/L ND 750 750 810 795 107 105 90-110 2 3
Results presented on this page are In the units Indicated by the-UrIlts" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/1312017 11:08 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 14

Pace Analytical Services, LLC
® 205 East Meadow Road - Suite A
aceAnalytical Eden, NC 27288
www.pacWabs.com [phone]
QUALIFIERS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte Is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenyiamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute,
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
REPORT OF LABORATORY ANALYSIS
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Dale: 04/13/2017 11:08 PM without the written consent of Pace Analytical Services, I.I.C. Page 10 of 14

aceAnalyticalm
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92336232
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92336232001
OUTFALL 001
SM 25400
356168
92336232002
OUTFALL 002
SM 2540D
356168
92336232003
OUTFALL 003
SM 25400
356168
92336232004
OUTFALL 004
SM 2540D
356168
92336232005
OUTFALL 005
SM 2540D
356168
92336232001
OUTFALL 001
EPA 9040
355796
92336232002
OUTFALL 002
EPA 9040
355796
92336232003
OUTFALL 003
EPA 9040
355796
92336232004
OUTFALL 004
EPA 9040
355796
92336232005
OUTFALL 005
EPA 9040
355796
92336232001
OUTFALL 001
SM 5220D
356633
92336232002
OUTFALL 002
SM 5220D
356633
92336232003
OUTFALL 003
SM 5220D
356633
92336232004
OUTFALL 004
SM 5220D
356633
92336232005
OUTFALL 005
SM 5220D
356633
Date: 04/13/2017 11:08 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 11 of 14

"� Document.M1[art?fl:': Document Revised:4ept,21,2016.
J J SAlhnle fnhF�rflnh ffa:�i,'be,•n:,.frccunl ' .. Paae 1 eE2
F•CAtt 'Pace Qual€ty Office
Laboratory receiving samples: ;. =r' _
Asheville ❑ Eden Greenwood HuntersV1110 Q - ' Rale.l h Mechankstfllle
Client Name: W0 9 6123
.. "t 1hI. II � �3 I hI
Courier: Fe�Ex UPS StS . Client"
❑ commerciai (]Pace . other: 923 Ba32.
Cult*Seal.Ptgtertt? - ..OYes_ ..... Of(lo :..:Sesisintact? [�No _:... " ^
Date/Initials Person Examining Contents., 1
Packing Materlal:: j]BOble Wrap' ' []Bubble Bags ;• atie': `. [�otlmr:
Thermometer, .' Qi 6t : afue ; QNone . - Q5amplesonice;coo€€n$protasshas Wun
OR Gun ID: ��� 7ypeoftces .
CorrectlonFactor; OoaierTempCorrected('CJ; BiofagfcpiTissue.Frozen? []Yes .: CNo. QN/A
Temp should be above (ree;ingto WC .'
USDA Regulated Soil(j] N/A, water Ample)
Did samplei. odehate,In a 4uaran6e zone ivithin the UnitedStates: CA, NY, ar SC (chgck maps)? • Did samptes'ortginate from a forel n sourcetlnternattanalty,
QYe&❑No indudiiiiiHawailand PuertoAfsOl]Yes -- UNti
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Short RhId lime Anal sis
Rush Turn AroOnd Time Re
SuffZdentVolume?
Correct Containers Used?
-Pace t:ontalners Used?'
Container's Intact?
i ;Sam les Field F€ltered?
Yes .: ' No
Yes bNO .' NLA.
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-Includes Date/rfine/ID&a€ sis .Matrix71
€ Heads ace in VOAViafs
Trip Blank Present? ©Yes
Trstody Seals Present? Yea .:QIVo N/a
f CLIENT NOTIFICATIOVOSOLUTION Field tiataRequfred? Yes ONo,
Person Contacted: Date/time:
' -CommentsAample — — — -
3 Discrepancy:
t ,
Project Manager SCURF Review:' ✓ Date: Ll
Project Manager SRFReview, '' . Date.. f
Note: •Whenavertliefe Is a discrepancy affecting North Carofina compliance samples, a cop of this form will h6 sont to the North Carolina D1:RNR Certiflcatlon pf{ke (Le.
Out ofhp1d,Ineorrectpreservative,out oftemp, incormetcdntalners) Pagej 12,of 14

Owl CHAIN -OF -CUSTODY / Analytical Request Document o
:' >aceArralytical The �ln-of-Custody is a LEGAL DOCUMENT. AN relevant fields must be completed accurately.
2,
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Section A ^^_ r T ^x Section B Section C
Page: of ` o_
Required Mont Inforawtion: Required Project Information: Imo;ce Information'.
CampanY' / R"r To: Attention:
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Copy To: r r
ComPa<+Y Nanx':
REGULATORY AGENCY
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SAMPLER NAME AND SIGNATURE
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preseriratian samples, :CHIC Due- nate'6 04/20/1°7 ? :
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--------------
Page 14 of 14
I

s
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 000528 or SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
Certificate of Coverage Number. NCG (This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Premiere Fitters COUNTY Anson
PERSON COLLECTING SAMPLE(S) : T. Haynes PHONE NO. (704)_ 826.8321 .. _
CERTIFIED LABORATORY(S) Pace Lab # 633
Lab # _ (SIGNATURE OF PERNIITTEE OR DESIGNEE)
By this signature, 1 certify that this report is accurate complete to
the best of my knowledge.
Part A: Specific Monitoring Requirements
'
4
d �
i�� V D
OC` 4 4 2.Oi6
DWALFILES
R SECTION
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓no (if yes, complete Part B)
Form SWU-246-112608
Page i of 2

. )
Part B: Ve6. Maintenance Activity Monitoring Requirements
Outfall
Date
5(i458
110556
ai53o
©040(3 ' x
r
No
�- Sample � e ;
Total blow-
nTaial RaEnfalf
01f &�Grease`�;
'fatal �
� �pH��.����
New Motor QilF
-`: 'a"'.-
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inches
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STORM EVENT CHARACTERISTICS:
Date 9.21.16
Total Event Precipitation (inches): . Q.57
Event Duration (hours): NIA (only if applicable — see permit.)
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches):
Event Duration (hours):
(only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
1
Simi_ . re of Permittee
(%AZO/2-04,
Date
Form SWU-246-112608
Page 2 of 2

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit.• httn://h2o.enr.state.ne.us/suUMs Documents.htm#miscfotms
Permit No.: I N I C I S 101010 Lb 121 j or Certificate of Coverage No.: I I� I I I I I I
Facility Name: Premiere Fibers
County: Anson
Inspector: Thomas Haynes
Date of Inspection: 9.21,16
Time of Inspection: 10:00-10:30
Total Event Precipitation (inches): 0.57
Phone No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may_ contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
ES?
(Signature of Permince or Designee)
Outfall Description:
Outfall No. 001-005
Structure (pipe, ditch, etc.) Pipe to Ditch
Receiving Stream: Buffalo Creek
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturing
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Light brown
Page 1 of 2
SWU-242-112608

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3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted `
4 Clarity:
Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy:
1 Q 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no
solids and 5 is the surface covered with floating solids:
1 2O 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no
solids and 5 is extremely muddy:
1 0 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
S Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608

5aceAnalytical
1 '
wwwPacelebs.com
September 27, 2016
Mr. Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 27606
RE: Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
Dear Mr. Rahn:
Pace Analytical Services, Inc.
205 East Meadow Road- Sulte A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 22, 2016.
The results relate only to the samples included in this report. Results reported h erein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shaft not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

/5a'ceAnalytical'
www.p&coabs.cnm
t
I
Project: R0-21 Premiere Fibers
Pace Project No.: 92313257
Pace Analytical Services, Inc.
205 East Meadow Road - 5ulte A
Eden, NC 272a388
[phone]
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87848
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In cull,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 13

aceAnalyilcal
wwwpacslebs.com
SAMPLE SUMMARY
Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92313257001
Outfall 001
Water
09/21/16 12:00
09/22/16 08:53
92313257002
Outfall 002
Water
09/21/16 12:30
09/22/16 08:53
92313257003
Outfall 003
Water
09/21/16 13:00
09/22/16 08:53
92313257004
Outfatl 004
Water
09/21/16 13:30
09/22/16 08:53
92313267006
Outfatl 005
Water
09/21/16 13:45
09/22/16 08:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 13

aceAnalytical
wwwpaeelabs'wm
SAMPLE ANALYTE COUNT
Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
Pace Analytical Sorvlces, Inc.
205 East Meadow Road- Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Method
Analysts
Ana lytes
Reported
Laboratory
92313257001
Outfall 001
SM 2540D
KCE
1
PASI-E
EPA 9040
DWJ
1
PASI-E
SM 5220D
MDW
1
PASI-A
92313257002
Outfall 002
SM 25400
KCE
1
PASI-E
EPA 9040
DWJ
1
PASI-E
SM 5220D
MDW
1
PASI-A
92313257003
Outfall 003
SM 2540D
KCE
1
PASI-E
EPA 9040
DWJ
1
PASI-E
SM 5220D
MDW
1
PASI-A
92313267004
Outfall 004
SM 2540D
KCE
1
PASI-E
EPA 9040
DWJ
1
PASI-E
SM 52200
MDW
1
PASI-A
92313257005
Outfall 005
SM 2540D
KCE
1
PASI-E
EPA 9040
DWJ
1
PASI-E
SM 5220D
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 13

5aceAnalytical1�le
w wpac lift oom
E
i
ANALYTICAL RESULTS
Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A ,
Eden, NC 27288
[phone]
Sample: Outfall 001
Lab ID: 92313257001 Collected: 09/21/16 12:00
Received: 09/22/16 08:53 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
2.9 mg1L 2.5
2.5 1
09/23/16 12:13
9040 pH
Analytical Method: EPA 9040
PH
5.9 Std. Units 0.10
0.10 1
09/22/16 16:00 H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
46.0 mg1L 25.0
12.6 1
09/26/16 22:00
Sample: Outfall 002
Lab ID: 92313267002 Collected: 09/21/16 12:30 Received:
09/22/16 08:53 Matrix: Water
Report
Parameters
Results Units Limit MDL OF Prepared
Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
NO mg1L 2.5 2.5 1
09/23/16 12:13
9040 pH
Analytical Method: EPA 9040
PH
6.6 Std. Units 0.10 0.10 1
09/22/16 16:00
H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg1L 25.0 12.5 1
09/26/16 22:00
Sample: Outfall 003
Lab ID: 92313257003 Collected: 09/21116 13:00 Received:
09/22/16 08:53 Matrix: Water
Report
Parameters
Results Units Limit MDL OF Prepared
Analyzed GAS No.
Qual
2540D Total Suspended Solids
Analytioal Method: SM 2540D
Total Suspended Solids
67.9 mg/L 6.6 6.6 1
09123/16 12:15
D6
9040 pH
Analytical Method: EPA 9040
PH
6.2 Std. Units 0.10 0.10 1
09/22/16 16:00
H1,1-16
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg1L 26.0 12.5 1
09/26116 22:00
Sample: Outfall 004
Lab ID: 92313257004 Collected: 09121/16 13:30 Received:
09/22/16 08:53 Matrix: Water
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
36.2 mg/L 2.8 2.8 1
09/23/16 12:i6
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Date: 09/27/2016 08:24 AM
without the written consent of Pace Analytical Services, Inc..
Page 5 of 13

Paco Analytical Services, Inc.
1acAnaB�ytical a 205 East Meadow Road - Suite A
Eden, NC 27288
11-7mrwpscefabs svm (336j923-8921
1
f
ANALYTICAL RESULTS
Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
Sample: Outfall 004 Lab ID: 92313257004 Collected: 09/21/16 13:30 Received: 09/22/16 08:53 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed CAS No.
Qual
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std. Units 0.10
0.10
1
09/22/16 16:00
H1,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
97.0 mg1L 25.0
12.5
1
09/26/16 22:00
Sample: Outfall 006
Lab ID: '92313257006 Collected:
09/21/16 13:45
Received: 09/22/16 08:53 Matrix: Water
Report
Parameters
Results Units Limit
MDL
OF
Prepared Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
15.9 mg/L 2.8
2.8
1
09/23/16 12:17
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std. Units 0.10
0.10
1
09/22/16 16:00
1-11,146
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
107 mg1L 25.0
12.5
1
09/26/16 22:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 09/27/2016 08:24 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 13

aXAnalytical'
wwwpereleDs.cam
i
QUALITY CONTROL DATA
Project: 119-21 Premiere Fibers
Pace Project No.: 92313257
QC Batch: 330075 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92313257001, 92313257002, 92313257003, 92313257004, 92313257005
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A ,
Eden, NC 27288
[phone]
METHOD BLANK: 1828809
Matrix: Water
Associated Lab Samples: 92313257001, 92313257002. 92313257003, 92313257004, 92313257005
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5
2.5 09/23/16 12:05
LABORATORY CONTROL SAMPLE:
1828810
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg1L
250 266 106
90-110
SAMPLE DUPLICATE: 1828811
92313179001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 132 138 4 5
SAMPLE DUPLICATE: 1828812
92313257003 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 67.9 120 55 5 D6
Results presorted on this page are In the unite Indicated by the "Unite" column exceplwhers an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 09/27/2016 08:24 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 13

iceAnalj6calv
a ww.pscwlaba.cW
I
QUALITY CONTROL DATA
Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
QC Batch: 329920 Analysls Method: EPA 9040
QC Batch Method: EPA 9040 Analysls Description: 9040 pH EDEN
Associated Lab Samples: 92313257001, 92313257002, 92313257003, 92313257004, 92313257005
SAMPLE DUPLICATE: 1828105
92313307001 Dup Max
Parameter Units Result Result RPD RPD
pH Std. Units 4.5 4.5 0
Pace Analytical Services, Inc.
205 East Meadow Road - Sulte A
Eden, NC 27288
[phone]
Qualifiers
9 H6
Results presented on this page am In the units Indicated by the "Units' coluen except where an alternate unit Is presented to the Might at the msuX
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2016 08:24 AM without the written consent of Pace Analytical Services, Inc..
Page 8 of 13

aceAnalytical
www.pacelatia.com
QUALITY CONTROL DATA
Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
QC Batch: 330263 Analysis Method: SM. 52200
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92313257001, 92313257002, 92313257003, 92313257004, 92313257005
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
METHOD BLANK: 1829894 Matrix: Water
Associated Lab Samples: 92313257001, 92313257002, 92313257003, 92313257004, 92313257005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand mglL ND 25.0 12.5 09/26/16 22:00
LABORATORY CONTROL SAMPLE: 1829895
Spike
Parameter Units Cone.
Chemical Oxygen Demand mglL 750
LCS LCS % Rec
Result % Rec Limits Qualifiers
794 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1829896 1829897
MS MSD
92313205002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mglL 348 750 750 1090 1090 98 99 90-110 0 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1829898 1829899
MS MSD
92313487001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand rrtglL 13500 750 750 13200 13200 -45 -45 90-110 0 3 M6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the fight of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/27/2016 08:24 AM without the written consent of Pace Analytical Services, Inc..
Page 9 of 13

Pace Analytical Services, Inc.
15ceAnalXical' 205 East Meadow Road- Suite A
Eden, NC 27288
www.pacefabacnm [phone]
i
I
QUALIFIERS
Project: RS-21 Premiere Fibers
Pace Project No.: 92313257
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit,
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydraz€ne decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values,
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 Is recommended In SW846 Chapter 4 for the analysis of Acroleln and Acrylonitdle by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Dlphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H1 Analysis conducted outside the EPA method holding time.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 09/27/2016 08:24 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13

IooAnalytical e
—psoels"Com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: R9-21 Premiere Fibers
Pace Project No.: 92313257
Lab ID Sample ID QC Batch Method QC Batch
92313257001
Outfall 001
SM 2540D
330075
92313257002
Outfall 002
SM 2540D
330075
92313257003
Outfall 003
SM 2540D
330075
92313257004
Outfall 004
SM 2540D
330075
92313257005
Outfall 006
SM 2540D
330075
92313257001
Outfall 001
EPA 9040
329920
92313267002
Outfall 002
EPA 9040
329920
92313267003
Outfall 003
EPA 9040
329920
92313257004
Outfall 004
EPA 9040
329920
92313257005
Outfall005
EPA 9040
329920
92313257001
Outfall 001
SM 5220D
330263
92313267002
Outfall 002
SM 5220D
330263
92313257003
Outfall 003
SM 52200
330263
92313267004
Outfall 004
SM 5220D
330263
92313267005
Outfall 005
SM 5220D
330263
Date: 09/27/2016 08:24 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytical Method
Analytical
Batch
Page 11 of 13

E]bt umeet Namei!'
Document Revised: May 24, 2016
•
20'6k�'Cal
Sim le°Colittitlon 6 ott Recei t SCUR t
Pe e l of.2,
;-5 •
DocumerttNo '.
isiuingAuthority.
F4DNb03=Rev:14' •
Pace Eden 0.uoli Olfice
2 of 2for Internal Use ONLY
I Client Name:
project
li
a ecl
S
i
�d �1
Courier. Fed Ex UPS I USPS CiEeett � � � E l (l, I;-€„ 511 r -1
Cl Commercial ❑Pace I Othe r ' �' " f, ❑ r. $ 1 2l
_ 7,
Custody Seal Present? ❑Yes �fo 5oalslntact? Yes ❑No
-�
Date/Initials Person Examining Co tentsL
Packing Material: []Bubble Wrap ❑(ubble' Bags ❑None' Bother.'
Thermometer. E0007 Type of ice Rwwet:. ❑Blue [)None []Samples on Ice, cooling process has begun
Correction factor: 0.0'C Cooler Temp Corrected ('Cji Hlaloglcal Tissue Frozen? []Yes. []No []N/A
Temp should be above freezing to VC
USDA Reguiatttd Soil (❑ N/A; water semple)
Did samples originate In a quarantine zone within the UnitedStates: CA, NY, oi.$C(check maps)? Did samples originato from a foreign source (internationally,
Myes FINo indudlnQ Unwalr and Ruerts R.eol? rives I-'•INo
Comments Discrepancy.*
Chain of Custody Present?
Yes''
No
N A'
• 1.
Sam les Arrived within Hold Time?
Yes.:
No
QLA
,:2.
Short Hold Time Analysis <72 hr.)?
byes
No
N A..
r3.
Rush Turn Around Time Reg uasted?
OYes
a
, A
.4.
Sufficient
Yes
• No
M NA
FS.
Correct Containers Used?
Yes
❑No
'f
QN/A
6.
.Pace Containers Used?
Yds
ONo
N A
Containers intact?
Yes
- No
ONYA,
7.
Samples Field Filtered?
Yes
No
A
:8.
Note If sediment is visible in the dissolved container.
Sample Labels Match CDC? , I_
,:
Yes
❑No
O A
9.
..
:...,. ; ....._.. , ... r,....
VVTInclude
s Date im ID Ana sis. Matd:
.. „
...>
,.
r... .... .. . . . __ ,....... :...-......,.
All contelners needing acid/base preservation have been
10. H„asHn
checked?. -
Pals
❑No
❑N/A
All'tontalners needing preservation are found to be in
Haan:
compliance with EPA recommendation?
HeroiPHa
(HNOa, HISOs, HCIc2; NoOH >9 Sulfide, NoOH>12 Cyanide)
Ves
❑No
❑N/A
a;oHProu
Exceptions: VOA, Coliform, TOC, Oil and Grease,
.DRO 8015 water DOC,LLH
Yet
No
136'
Sam lei checked for dechlorinatlon?
Ya,.
No
NIA-
'11.
Heads ace In VOA Vials >5.6mm ?
Ekes
No
I
Trip Blank Present?
[]Yes
❑No
IIIA
13:
Trip Blank Custody Seals Present?
❑Yes.
❑No
.t2NN/A
Pace Trip Blank Lot#(ifpurchased):
i
CLIENT NOTIFICATION/RESOLUTION Flald Data Required? []Yes []No
Person Contacted: Date/Tlme:
Comments/Sample
Discrepancy:
Project Manager SCURF Revlew: q 0=4 Date:
Project Manager SRF Review: Date:
Note:; Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy,of this form will be sent to the Mart rollna li�A-14R Certificatlon OHiee (i.e.
Out of hold, Incorrect preservative, out ottemp, Incorrect containers)
Page 12 of 13

')12.... aoca
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT- All feWvarrt fields must be awn~ accurately.
Section A Section B Section CPaw
°t /
Required Client tnformaaon: Roquimd ProjecL.Uftma5an:. Mvoice tdormalim
-
CanvaaY C /3L G�J F4VartTa: /d
216.8
2a0
7�r
Address:
OPYo:
CaPayNam:
REGJf.bk(AGENCY '` -
r NPDES GROUNDWATER F DRINKING WATER
j` UST !- RCRA OTHER
EMM TO:
Purchase Order Na.
Quaee
! !�
-
Phone:
Fax
?reject Name: -
PNiea
SrLe L.oraliOri
--
Requested Due DaU iAT:. .
Proiw NumDer.-
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Requested:Analyses-FittterNd
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Sectwa D Codas
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SAMPLER NANE AND SIGNATURE
PRINT Name of UMPLER: S
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SIGNATURE of SAtIPLER DATE SWml
'"Vwtam Norc By at➢urig rM re rn you am aocepwg Pace & NET M d y PWMere terms and 9 ro 1= ciWM C9 I,5% car Moran for." rnvekes!+a dm. / F-ALL-Q-020rev o7. 15-K a 200T

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Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http://h2o.enr.state.nc.us/su/Forms Doc uments.htm#miscforms
Permit No.: 1 N 1 C� Si 0 10 1 0[ 5 12 1 8! or Certificate of Coverage No.:
Facility Name: Premiere Fibers
County: Anson
Inspector: Thomas Haynes
Date of Inspection: 5.5.16
Time of Inspection: 11-00-11.30
Total Event Precipitation (inches): 0.16
Phone No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
Outfall Description:
Outfall No. 001-005
Structure (pipe, ditch, etc.) Pipe to Ditch
Receiving Stream: Buffalo Creek
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturina
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Medium brown
Page I of 2
SWU-242-I 12608

1
1
f
1
1
1
1
1
1
1
s Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy:
1 O 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no
solids and 5 is the surface covered with floating solids:
Q 2 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no
solids and 5 is extremely muddy:
l Q 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 is there an oil sheen in the stormwater discharge? Yes No
9 is there evidence of erosion or deposition at the outfail? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S WU-242- l i 2608

Pace Analytical Services, Inc.
aceAnalytJcal • 205 East Meadow Road - Suite A
Eden, NC 27288
www-pac wacom [phone]
May 19, 2016
Mr. Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 27606
RE: Project: PREMIERE FIBERS R9-21
Pace Project No.: 92296545
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on May 05, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
'8&tag. &4m
-
Brittany Gibson
[e-mail]
Project Coordinator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„
Page 1 of 13

'
Pace Analytical Services, Inc.
aceArralytrcal •
205 East Meadow Road - Suite A
Eden, NC 27288
'
www•pacelabs com
[phone]
CERTIFICATIONS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92296545
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification M 40
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Wastewater Certification M 633
North Carolina Drinking Water Certification #: 37738
VrginiaNELAP Certification #: 460025
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REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 13
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SAMPLE SUMMARY
rtuyecc rr«mir-rtr- rmr-mo rra-n
Pace Project No.: 92296545
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92296545001
OUTFALL 001
Water
05/05/16 10:45
05/05/16 15:20
92296646002
OUTFALL 002
Water
05/05116 11:00
05/05/16 15:20
92296546003
OUTFALL 003
Water
05/05116 11:30
05/05/16 15:20
92296545004
OUTFALL 004
Water
05/05/16 12:00
05/05/16 15:20
92296646006
OUTFALL 005
Water
05/05/16 12:15
05/05/16 15:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 13
1

to
a ce Analytical
www.paca'abs.caM
1
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Project:
PREMIERE FIBERS R9-21
Pace Project No.:
92296545
'
Analytes
Lab ID
Sample ID
Method
Analysts
Repotted
Laboratory
'
92296545001
OUTFALL 001
SM 2540D
KCE
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
i
92296546002
OUTFALL 002
SM 2540D
KCE
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
'
92296545003
OUTFALL 003
SM 2540D
KCE
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
92296646004
OUTFALL 004
SM 2540D
KCE
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
'
92296645005
OUTFALL 005
SM 2540D
KCE
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
1
1
1
1
1
1
1
i
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 13

Pace Analytical Services, Inc.
accAnalytrcal •
205 East Meadow Road - Suite A
Eden, NC 27288
WWWP&CN&bswm
[phone]
'
ANALYTICAL
RESULTS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92296545
1
Sample: OUTFALL 001
Lab ID: 92296645001 Collected:
05/05/16 10:45
Received: 05/05/16 15:20 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed CAS No. Qual
'
Analytical Method: SM 2540D
2640D Total Suspended Solids
Total Suspended Solids
57.0 mg1L 2.5
2.5
1
05/10/16 13:07
1
9040 pH
Analytical Method: EPA 9040
pH
6.3 Std. Units 0.10
0.10
1
05/06/16 09:30 H6
5220D COD
Analytical Method: SM 52200
Chemical Oxygen Demand
ND mg/L 25.0
12.5
1
05/18/16 20:00
Sample: OUTFALL 002
Lab ID: 92296646002 Collected:
05/05/16 11:00
Received: 05/05/16 15:20 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed CAS No. Qual
'
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND mg/L 2.6
2.6
1
05/10/16 13:08
9040 pH
Analytical Method: EPA9040
PH
6.3 Std. Units 0,10
0.10
1
05106/16 09:30 H6
1
5220D COD
Chemical Oxygen Demand
Analytical Method: SM 5220D
ND mg/L 25.0
12.5
1
05/18/16 20:00
Sample: OUTFALL 003
Lab ID: 92296646003 Collected:
05/05/16 11:30
Received: 05/05/16 15:20 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
12.3 mg/L 2.6
2.5 1
05/10/16 13:08
9040 pH
Analytical Method: EPA 9040
pH
6.0 Std. Units 0.10
0.10 1
05/06/16 09:30 H6
5220D COD
Analytical Method: SM 52200
Chemical Oxygen Demand
ND mg/L 25.0
12.5 1
05/18/16 20:00
Sample: OUTFALL 004
Parameters
25400 Total Suspended Solids
Total Suspended Solids
Date: 05/191201611:24 AM
1
Lab iD: 92296545004 Collected: 05/05/16 12:00 Received: 05/05/16 15:20 Matrix: Water
Report
Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 2540D
54.8 mg1L 3.3 3.3 1 0511011613:09
REPORT OF LABORATORY ANALYSIS
This report shall not t>e reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 13

leAnalytical
' wwwpeteiabs_com
1
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92296545
Sample: OUTFALL004
Lab ID: 92296545004 Collected:
05105/161Z00
Received: 05105116 1520 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
t9040
Analytical Method: EPA 9040
pH
pH
6.8 Sid. Units 0.10
0.10 1
05/06/16 09:30 H6
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
".0 mglL 25.0
12.5 1
05/18/16 20:00
Sample: OUTFALL 005 Lab ID: 92296646006 Collected: 05/05/16 12:16 Received: 05/05/16 15:20 Matrix: Water
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No. Qual
'
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
33.0 mg1L 2.5 2.5 1
05/10/16 13:09
'
9040 pH
Analytical Method: EPA 9040
pH
7.1 Sid. Units 0A 0 0,10 1
05/06/16 09:30 H6
t
5220D COD
Analytical Method: SM 52200
Chemical Oxygen Demand
97.0 mg1L 25.0 12.5 1
05/18/16 20:00
'
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 05/19/2016 11:24 AM
without the written consent of Pace Analytical Services, Inc..
Page 6 of 13
1

' Pace Analytical Services, Inc.
® 205 East Meadow Road - Suite A
aceAnalytical Eden. NC 27288
' wwwpacelabe awrr
[phone]
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
. Pace Project No.: 92296545
QC Batch: EDEN122755 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
. Associated Lab Samples: 92296545001, 92296545002, 92296545003, 92296545004, 92296545005
METHOD BLANK: 1729704 Matrix: Water
Associated Lab Samples: 92296545001, 92296545002, 92296545003, 92296545004, 92296545005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 2.5 05/10/16 13:06
.
LABORATORY CONTROL SAMPLE:
1729705
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 238 95
90-110
SAMPLE DUPLICATE: 1731808
92296922001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Suspended Solids
mg/L
17.4 79A 128
5 D6
SAMPLE DUPLICATE: 1731821
92296874001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Suspended Solids
mg/L
141 161 14
5 D6
Results presented on this
page are in the
units indicated by the "Units" column except where an alternate unit
Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2016 11:24 AM
without the written consent of Pace Analytical Services, Inc..
Page 7 of 13

aceAnalytrcal
' www.pacsla"Oom
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
iPace Project No.: 92296545 QC Batch: EDEN122737 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
' Associated Lab Samples: 92296545001, 92296545002, 92296545003, 92296545004, 92296545005
SAMPLE DUPLICATE: 1727808
92296545005 Dup
Parameter Units Result Result RPD
�m
1
1
1
1
1
1
1
1
1
Std. Units 7.1 7A
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Max
RPD Qualifiers
0 9 H6
Results prevented on this page are in the units Indicated by the "Units" column except where an a8emate unh Is presented to the right of the result.
Date: 0511912016 11:24 AM
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 13

'
Pace Analytical Services, Inc.
�rQ���_ ire®
Vi J1 /`� r
205 East Meadow Road - Suite A
Eden, NC 27288
'
w".paosulcom
[phone]
'
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92296545
'
QC Batch: WETA127648 Analysis Method: SM 5220D
OC Balch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92296545001, 92296545002, 92296545003, 92296545004, 92296545005
'
METHOD BLANK: 1736167 Matrix: Water
Associated Lab Samples: 92296545001, 92296545002, 92296545003, 92296545004, 92296545005
Blank Reporting
'
Parameter Units Result Limit MDL
Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 12.5
05/18/16 20:00
'
LABORATORY CONTROL SAMPLE: 1736168
Spike LCS LCS
% Rec
Parameter Units Conc. Result % Rec
Limits Qualifiers
'
Chemical Oxygen Demand mg/L 750 750 100
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1736169 1736170
'
MS MSD
92296421009 Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
'
Chemical Oxygen Demand mg1L ND 750 750 725 725
97 97 90-110 0 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1736171 1736172
MS MSD
92296603001 Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
'
Chemical Oxygen Demand mg1L 209 750 750 911 911
94 94 90-110 0 3
t
1
'
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/19/2016 11:24 AM without the written consent of Pace Analytical Services, Inc..
Page 9 of 13

1
1
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acoAnalytt+cal
QUALIFIERS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92296545
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27298
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines. unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited anelytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
lib Analysis initiated outside of the 15 minute EPA required holding time.
IaF3ia[i>ryf E•IP�r);[."tiflF�l1►1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc -
Page 10 of 13

acemalxical
www.pKwbs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
'
Project:
Pace Project No.:
QUALITY CONTROL DATA CROSS REFERENCE TABLE
PREMIERE FIBERS R9-21
92296545
Analytical
Lab ID
Sample la
QC Batch Method
QC Batch Analytical Method Batch
92296645001
OUTFALL 001
SM 2540D
EDENI22755
'
92296645002
OUTFALL 002
SM 2540D
EDENI22755
92296WO03
OUTFALL 003
SM 2540D
EDENI22755
92296545004
OUTFALL 004
SM 2540D
EDENI22755
92296645005
OUTFALL 005
SM 2540D
EDEN122755
t
92296545001
OUTFALL 001
EPA 9040
EDENI22737
92296545002
OUTFALL 002
EPA 9040
EDEN122737
'
92296545003
92296545004
OUTFALL 003
OUTFALL 004
EPA 9040
EPA 9040
EDENI22737
EDEN122737
92296646005
OUTFALL 005
EPA 9040
EDENI22737
92296545001
OUTFALL 001
SM 5220D
WETA127648
92296645002
OUTFALL 002
SM 5220D
WETA127648
92296646003
OUTFALL 003
SM 52200
WETA127648
92296545004
OUTFALL 004
SM 5220D
WETAl27648
92296545005
OUTFALL 005
SM 5220D
WETAl27648
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/1912016 11:24 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 13
1

ae�Analytical'
,.R ,
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed 20rUrat*.
-
Section A Section B Section C
Page: at f d
Required Client Irdamadan: Required Project Information: Invoice Infptmation: -
Company. Report TO: tle
N ntion:
-
2038611
Address: Copy
To:
Company Name:
R_ EGULATORY AGEH.CY
rew
f NPOES r . GROUNDWATER DRINKING WATER_
r UST f RCFW OTHER
Fanal To: PyrT/te5e
Order NO.: rj /
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Phone: Fax: Project
Name:
Prajetl
SkeLoe8ltdn
/e, ! .S
S7ATF:
-
5
Requested Due DatprrAT: Project
Number: /
Profile A[
Requestsd
Anatysis
Fiita'eif;{Y1N)
'
Section D Matrix Codes
Raclrrt aaCfient inrarrr,etton MATRlx r CODE
9
COLLECTED
Preservatives
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Ddradnp water Ow
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waste water WW
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DATE
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=9:
10
12
- ADDITIONAL COMMENTS , - -
RELINQUISHED BY./ AFFILIATION
DATE - ,
- �.TmE
ACCEPTED BY 1 AFFILIATION -
_ DATE . '
. -- TIME
SAMPLE CONDITIONS
l 3261
SAMPLER NAME AND SIGNATURE _
v
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ORIGINAL
s
8 8
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PRINT flame of SAMPLER:
m
" SIGNATURE of SAMPLER: �/} DATE Signed
v N
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J
'Important Note, By sWhV tNs tarns you we aompting Parana NET 30 day payment terms and agreemg to late Charges d 1.5% per uOrM for any krd0i;es not 30 days. F-ALL-0-020rev.07, 15-May-2007

1
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s
Doc(tmf I�[arre:
; 5 le<;Cond(tton; 90_016co!ptfscug .
Document Revised, 26FEB2016
Page. I of 2
', Docur7i4ntN6.:,.
•IssufngAu�hority:`•.
cgnaica!•.
FER1yI-05=Q0jli a 13.
Pace Eden Qua Office
RBceiiH -
outer: e ULIPS BUSPS ',jCffe
❑ Commercial Pace]Other
CustodySeal Present? Yes jto Seals Intact? : , . ElYes ❑fVo
Date/initials Peraan Examining CanDe� 1? 11 4P
Packing Material: j]Bubble Wrap . []Bubble Bagsipna �Oxher; ►�
Theirttome4er.' [j IR Gun E.DOD7. Type of I .�": ' et ❑8fue.,; None [�$ampieson fc `cgoling process has beg
Correction Factor. 0.0'C .. Cooler Temp Corrected ('Cj. / `.. Biological Tissue Froren?.: ,Yes ❑No,' . ❑N/A .: »l
Temp should be above freexfng to VC
USDA Regulated Soi! ([f N/A, ,hater sample}
Did samples originate In a quaMntlne zone within the United States CA, NY, or SC (check maps}? Dfd samples originate from a foreign source {fntematlonaliy,
.. _
' .IriYax No � .: ...... . :. .. inciudine itawall and Diierto Ricoi&:. Yes No,
CGMMFM[S:
Chain of Cuskil y Present?
Yes
Na N A
1
Chain of Cusco Filled Out?
Yes
. NN
o A'
.2.
Chaln.of CustodyRelln wished?
Yes'EINO.
ONIA
3
Sam Ier.EVama`an orSl ature.onCDC?
es
No NA
4,
-'Sam IesAMvedwithIn Hold•Tlme? •
.,•..,
Yes...
. No,: A:
,S:.:: : .
-Short 101d -nme Ana[ s A2 hr ?.:
hush 7urridroundTtnie R" "ue+`tcd? .:.: :
:Yes' ' o= N
Sufticlentvolume? t:
es
No 0 N A
8.
Correct Coiztalners Used?
as
©No... ©NIA
9. ,
-Pace Containers Used?
Cho N A
Containers Intact?
Yes
No
Filtered volume.Recelved for Dissolved Tests?
Yes
QNo A
11 Note If sediment is visible In the dissolved container'. .
Sample Labels Match CDC? Yes" j F o r f 110k,.
in, -
..
::-Includes Aate/11rn D/Ana . fs.. Matrix: :VIA
Al containers needing;add/base preservation have been
chgckea? .
pYes
�No ©NIA
'
Ali containers needing preservation ere found to be in
compllanoewfth EPA recomrnendation?,,
'ONO
(HNOs, 1`12SOy HCId, NaOH>9 Sulfide, NaOHn12 Cyanide)
jes
©WA
Fxceptlons: VOA, Coliforr irTOC,'DII and.Grease,
E
DRO/8015 water DOC,LLH
13Yes
No N A
Sam les shedted for dechlorination
Yes
No : NIA :
14
Hea dspace in .V•f}A Vlais
Trip Blarik Preseint7
©V s J []No N
16.
Pace Trl Blank Lut# (ff urohased
r
�
,
Trip 81ankCustody$,ealsPresent?
GdENf NOTlf117T014JRESDLUTION:,
. FieldRequlred?
s 1
Person Contacted,
L Date/lime:
1 I
°?• �
Comments/Resolution:
.
Project Manager SCURF Review:
Date:.
i
Project Manager SRO Review:
Date:
}
Note: Whenever there is a discrepancy affecting North Carolina tompliance samples; a copy of this form will be sent to the North Carolina DEHNR Certificationf.13 of'13 .
Out of hold, incorrect preservative, out ofternp, Incorrect contelners)

1
1
1
1
1
1
1
i
1
M4WZAT E R E ENVIRONMENTAL, LLC
401 WATERS EDGE DRIVE, SUITE 201 a RALEIGH, NC 27606 • PHONE [phone] • FAx [phone]
November 18, 2015 A
NCDEQ
Division of Water Quality
Central Files
1617 Mail Service Branch 00*b
RECEIVED
Raleigh, North Carolina 27699-1617
4;40 MAY S 1 2016
Reference: Year I - Period 2 Stormwater Monitoring Report
Premiere Fibers Facility CENTRAL FILES
DWR SECTION
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge Job No. 119-21
To Whom It May Concern:
We are presenting the stormwater monitoring report for Year I- Period 2 in . All results are
within required parameters We have attached the DMR, SDO, and laboratory analytical results -see
Appendix A and B). If you have any questions, or if we may be of further assistance, please contact me
at [e-mail] or 919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
15-090

rs am 111111110 ILIUM r WON r MW r am r 11110r � 11111101 ■r- ■r 111110M ■ter
Permit Number: NCS 000528
Certificate of Coverage Number: NCG
FACILITY NAME Premiere Fibers
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
or
SAMPLES COLLECTED DURING CALENDAR YEAR: 2016
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
PERSON COLLECTING SAMPLE(S) T. Haynes
CERTIFIED LARORATORY(S) Pace Lab # 633
Lab #
Part A: Specific Monitoring Requirements
COUNTY Anson
PHONE NO. [phone]
;
(SIGNATURE OF PERMITI'EE OR DESIGNEE)
By this signature, I certify that this report is accurate complete to
the best of my knowledge.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

� NMI M r N.M � � zlw r .ter .�■� .� �■�.
Part B: Vehicle Maintenance Activity Monitoring Requirements
STORM EVENT CHARACTERISTICS:
Date 5.5.16
Total Event Precipitation (inches): 0.16
Event Duration (hours): NIA (only if applicable — see permit.)
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches):
Event Duration (hours):
(only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the 'information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
a��-
V-S—iiwture of Permittee
Zv Zc7l (V
Date
Form SWU-246-112608
Page 2 of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 000528
Certificate of Coverage Number: NCG
FACILITY NAME Premiere Fibers
PERSON COLLECTING SAMPLES) T. Haynes T
or SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
CERTIFIED LABORATORY(S) Pace Lab # 633
E❑
zPb #
CENTRAL_ ALES
Part A: Specific Monitoring Requirements DINR SECTION
COUNTY Anson
PHONE NO. [phone] 0.
-3
(SIGNATURE OF PERNIITTEE OR DESIGNEE�-"
By this signature, I certify that this report is accurate comillete
the best of my knowledge.
,;Outfall_
No.,:---
._.Date
Sample
e
Collectd.
,Total
Ratnfall�
r Total,.
Suspended
ti _
CODP
-
_
_.
w --
-0
'�_- _
�� mo/d�f�r�-
=' inches—".�
'--• mg/l :
1
11.3.15
See Below
5.5
ND
6.7
2
11.3.15
38.2
ND
6.5
3
11.3.15
15.1
ND
6.0
4
11.3.15
6.5
ND
6.3
5
11.3.15
5.9
ND
6.3
_
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

Part B: Vehicle Maintenance Activity Monitoring Requirements
a=0utfa[I�
1Vo�'��_
WN
mute
�S$inp��
s„mColieCted _
a
�vfsFlow
p`i5nspen
" TotalRainfall
Oilrfi. Gr a
m Total ��
ieu
_
n
pH
N w Mnto Oif
rn,0-
Units
il/i�a
STORM EVENT CHARACTERISTICS:
Date 11.3.15
Total Event Precipitation (inches): 0.14
Event Duration (hours): NIA (only if applicable — see permit.)
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable -- see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Si tore of Permittee
1r 19 Z�15
Date
Form SWU-246-112608
Page 2 of 2

WATERS EDGE ENVIRONMENTAL., LLC
4901 WATERS EDGE DRIVE, SUITE 201 • RAI.EIGH, NC 27606 • PHONE [phone]$7 9 FAx [phone]=
November 18, 2015
NCDEQ
Division of Water Quality
Central Files
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617
Reference: Year 1- Period 2 Stormwater Monitoring Report
Premiere Fibers Facility
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge Job No. 119-21
To Whom It May Concern:
RECEIVED
NOV 2 3 2015
CENTRAL FILES
DWR SECTION
We are presenting the stormwater monitoring report for Year 1- Period 2 in 2014-2015. All,results are
within required parameters We have attached the DMR, SDO, and laboratory analytical results -see
Appendix A and B). If you have any questions, or if we may be of further assistance, please contact me
at prahnnwatersedReenv.com or 919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
15-090

4�•�l
Stormwater Discharge Outfall (SD4)
Qualitative Monitoring Report
Forguidance onflling out Loris form, please visit: htta:/1h2o.enr.state. nc.us&Oorms Documents.hu0misdorms
Permit No.: I NJ C1 S1 0 10 10 15 12 8 or Certificate of Coverage No.:
Facility Name: Premiere Fibers
County: Anson Phone No. 704.826.8321
Inspector: Thomas Haynes
Date of inspection: 11.3.15
Time of Inspection: 10:30-11:30
Total Event Precipitation (inches): 0.14
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please checkyour permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that -
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has;,
occurred. A single storm event ma contain gp to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
UZ
(Signature of Permittee or Designee)
outfali Description:
Qutfall No. 001-005
Receiving Stream: Buffalo Creek
Structure (pipe, ditch, etc.) Pipe to Ditch
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturing
2 Color.
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Medium brown
Pagel of 2
SWU-242-112608

L .,. ,ter: :i I al s ��.. :,� .I f..�i � �� � i _ r �r. .,. ii i. � �1
r i, . ,
r•

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy:
O 2 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no
solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no
solids and 5 is extremely muddy:
1 O 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608

/55'ceAnalytical"
rwww.pawlabs.com
I
November 12, 2015
Mr, Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 27606
RE: Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on November 04, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sam ple anaiyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
"au*N- cal . AJ d�YU
Brittany Gibson
[e-mail]
Project Coordinator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc,.
Page 1 of 15

a xftlytical �
www.pscefaOs.00m
E
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #; E87648
Massachusetts Certification #: M•NCO30
North Carolina Drinking Water Certification #: 37712
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shaft not be reproduced, except In full,
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aceAnalytical
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SAMPLE SUMMARY
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Pace Analytical Services, Inc.
205 East Meadaw Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Recelved
92274714001
OUTFALL 001
Water
11/03/15 12:00
11/04/15 16:15
92274714002
OUTFALL 002
Water
11/03/15 12:15
11/04/15 16:15
92274714003
OUTFALL 003
Water
11/03/15 12:30
11/04/15 16:15
92274714004
OUTFALL004
Water
11/0311612:45
11104/1616:15
92274714005
OUTFALL 005
Water
11/03/15 13:00
11/04/15 16:15
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Pate Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytts
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92274714001
OUTFALL D01
SM 2540D
DWJ
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
92274714002
OUTFALL 002
SM 2540D
DWJ
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 52201)
WRC
1
PASI-A
92274714003
OUTFALL 003
SM 2540D
DWJ
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
92274714004
OUTFALL 004
SM 2540D
DWJ
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
92274714005
OUTFALL 005
SM 2540D
DWJ
1
PASI-E
EPA 9040
KCE
1
PASI-E
SM 5220D
WRC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27280
[phone]
Sample: OUTFALL 001
Lab ID: 92274714001 Collected:
11/03/15 12:00
Received: 11/04/15 16:15 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.6 MOIL 2.5
2.5 1
11/05/15 10:25
9040 pH
Analytical Method: EPA 9040
pH
6.7 Std. Units 0.10
0.10 1
11/05/15 10:35 H3,H6
6220D COD
Analytical Method: SM 62200
Chemical Oxygen Demand
ND mg/L 25.0
12.5 1
11/09/15 13:40
Sample: OUTFALL 002
Lab ID: 92274714002 Collected:
11103/15 12:15
Received:
11/04/15 16:15 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared
Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
38.2 MOIL 2.5
2.5
1
11/06/15 10:25
9040 pH
Analytical Method: EPA 9040
pH
6.5 Std. Units 0.10
0.10
1
11/05/15 10:35
1-13,146
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg/L 25.0
12.5
1
11/09/15 13:40
Sample: OUTFALL 003
Lab ID: 92274714003 Collected:
11/03/15 12:30
Received:
11/04/15 16:15 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared
Analyzed CAS No.
Quaff
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
16.1 mg1L 2.5
2.5
1
11/05/15 10:26
9040 pH
Analytical Method: EPA 9040
pH
6.0 Std. Units 0.10
0.10
1
11/05/15 10:35
H3,1-16
6220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg/L 25.0
12.5
1
11/09/15 13:40
Sample: OUTFALL 004 Lab ID: 92274714004 Collected: 11 /03115 12:45 Received: 11/04/15 16:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 6.6 mg/L 2.5 2.5 1 11/05/15 10:26
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: OUTFALL 004
Lab ID: 92274714004 Collected:
11/03/15 12:45
Received: 11/04/15 16:15 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No, Qual
9040 pH
Analytical Method: EPA 9040
PH
6.3 Std. Units 0.10
0.10 1
11/05/15 10:35 1-13,1-16
6220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg1L 25.0
12.5 1
11/09/15 13:40
Sample: OUTFALL 006
Lab ID: 92274714005 Collected:
11/03/15 13:00
Received: 11/04/15 16:15 Matrix: Water
Report
Parameters
Results Units Limit
MIX DF
Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.9 mg1L 2.5
2.5 1
11/05/15 10:26
9040 pH
Analytical Method: EPA 9040
PH
6.3 Std. Units 0.10
0.10 1
11/05/15 10:35 H3,H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg1L 25.0
12.5 1
11/11/15 18:00
REPORT OF LABORATORY ANALYSIS
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Date'. 11112/2015 08'.07 AM without the written consent of Pace Analytical Services, tne.. Page 6 of 15

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QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
OC Batch: EDEN120636
Analysis Method: SM 2540D
OC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended
Solids
Associated Lab Samples: 92274714001, 92274714002, 92274714003, 92274714004, 92274714005
METHOD BLANK: 1599405
Matrix: Water
Associated Lab Samples: 92274714001, 92274714002, 92274714003, 92274714004, 92274714005
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed Qualifiers
Total Suspended Solids
mg1L
ND 2.5
2.5 11/05/15 10:19
LABORATORY CONTROL SAMPLE:
1599406
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result %Rec
Limits Qualifiers
Total Suspended Solids
mg1L
250 258 103
90-110
SAMPLE DUPLICATE: 1599407
92274792001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 114 121 6 5 D6
SAMPLE DUPLICATE: 1599408
92274797001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg1L 106 124 16 5 D6
Results presaged on this page are In the units Indlcsted by fie "Units" column except where an alternate unit Is presented to the right of the resulL
REPORT OF LABORATORY ANALYSIS
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Date: 11/12/2015 08:07 AM without the written consent of Pace Analytical Services, Inc..
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QUALITY CONTROL DATA
Project: PREMIERE FIBERS 139-21
Pace Project No.: 92274714
QC Batch: EDEN120639 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92274714001, 92274714002, 92274714003, 92274714004, 92274714005
SAMPLE DUPLICATE: 1699660
92274714005 Dup
Parameter Units Result Result
PH Sid. Units 6.3 6.3
Pace Analytical Services, Inc,
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Max
RPD RPD Qualifiers
0 9 H3,H6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit In presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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ZAnalj cal o
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f
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
QC Batch: WETN25312 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92274714001, 92274714002, 92274714003, 92274714004
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
METHOD BLANK: 1602017 Matrix: Water
Associated Lab Samples: 92274714001, 92274714002, 92274714003, 92274714004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand mg1L ND 25.0 12.5 11/09/15 13:40
LABORATORY CONTROL SAMPLE: 1602018
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 742 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1602019 1602020
MS MSD
92274934001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone, Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L 1740 3000 3000 4350 4350 67 87 90-110 0 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1602021 1602022
MS MSD
92274982001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc, Cone. Result Result %Rec %Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L 40.0 750 750 729 729 92 92 90-110 0 3
Results presented on this page are in the units Indicated by he "Units" colunm except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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/55'ceAna1jNca19
! www.pacelab3.com
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
OC Batch: WETA125361 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92274714005
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
METHOD BLANK: 1604129 Matrix: Water
Associated Lab Samples: 92274714005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chemical Oxygen Demand mg1L ND 25.0 12.5 11/11/15 18:00
LABORATORY CONTROL SAMPLE: 1604130
Spike LCS LCS % Rec
Parameter Units Cone, Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 771 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1604131 1604132
MS MSD
92275179002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Oual
Chemical Oxygen Demand mg/L 8350 15000 15000 23900 23900 104 104 90-110 0 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1604133 1604134
MS MSD
92275004001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L 5660 30000 30000 36600 36600 103 103 90-110 0 3
Results presented on this page are In the units indicated by the "Units" column except where an altemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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11ce Analytical
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QUALIFIERS
Project: PREMIERE FIBERS R9-21
Pace Project No,: 92274714
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
Pace Analytical services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
S - Surrogate
1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270, The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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)
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92274714
Lab ID Sample ID QC Batch Method
92274714001
OUTFALL 001
SM 2540D
92274714002
OUTFALL 002
SM 2540D
92274714003
OUTFALL 003
SM 2540D
92274714004
OUTFALL 004
SM 2540D
92274714005
OUTFALL 006
SM 2540D
92274714001
OUTFALL 001
EPA 9040
92274714002
OUTFALL 002
EPA 9040
92274714003
OUTFALL 003
EPA 9040
92274714004
OUTFALL 004
EPA 9040
92274714006
OUTFALL 005
EPA 9040
92274714001
OUTFALL 001
SM 5220D
92274714002
OUTFALL 002
SM 5220D
92274714003
OUTFALL 003
SM 5220D
92274714004
OUTFALL 004
SM 5220D
92274714005 OUTFALL 006 SM 5220D
QC Batch
EDEN/20636
EDEN/20636
EDEN/20636
EDEN/20636
EDEN120636
EDEN/20639
EDEN/20639
EDEN/20639
EDEN120639
EDEN/20639
WETA/25312
WETA125312
WETA/25312
WETA125312
WETA/25361
Pate Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytical Method
Analytical
Batch
REPORT OF LABORATORY ANALYSIS
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%, r a.a.

CHAIN -OF -CUSTODY I Am"cal Request Document

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Permit Number: NCS 000528
Certificate of Coverage Number: NCG
FACILITY NAME Premiere Fibers
PERSON COLLECTING SAMPLE(S) T. H
CERTIFIED LABORATORY(S) Pace
Part A: Specific Monitoring Requirements
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
or
SAMPLES COLLECTED DURING CALENDAR YEAR: 2015
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Anson
PHONE NO. [phone]
Lab # 633
Lab # (SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, l certify that this report is accurate=*plete to
the best of my knowledge.
Outfall
Date
No.
Sample
Collected
Total
Rainfall
Total
Suspended
Solids (TSS)
COD
pH
Permit Bench
NIA
100
.120
6-9
mo/dd/yr
inches
mg/I
mg/l
units
1
5.1.15
See Below
ND
NA
6.5
=7
■W
--gel
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

Part _B.- Vehicle Maintenance Activity Monitoring Requirements
i
-
-
Total F[ow
4S1 Rsiiia.;
.:.Q�1&:Greaser :
- Toiai
pH
=11FeiT plQtor O'::
:... .:....:.....:...
1lected : •
--a tiealife�
�l
-
tt�p
y:S nded`
-
gsllio:
STORM EVENT CHARACTERISTICS:
Date 5.1,15
Total Event Precipitation (inches):
Event Duration (hours): NIA
0.12
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches):
Event Duration (hours):
(only if applicable — see permit.)
(only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Sign re of Permittee
i Z/b
Date
Form SWU-246-112608
Page 2 of 2

d4WATERS EDGEENVIRONMENTAL, LLC
4901 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 • PHONE [phone] • FAx [phone]
May 14, 2015
NCDENR
Division of Water Quality RECEIVED
Central Niles
May 2 r 2015
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617 CEN-rPAL FILES
DWR SECTIQN
Reference: Year 1- Period 1 Stormwater Monitoring Report
Premiere Fibers Facility
Ansonville, North Carolina
Stormwater Permit No. NCS000529
Waters Edge Job No. R9-21
To Whom It May Concern:
We had originally reported the stormwater monitoring; report for Year 1- Period 1 in 2014-2015. All
results are within required parameters with the exception of a TSS exceedances for Outfall #1 (TSS
detected at 231 mg/L versus a 100 mglL benchmark) and a pH exceedance at Outfall #1 pH detected at
4.0 versus a benchmark at 6-9). However, we conducted a Tier 1 inspection on March 3, 2015 and had a
crew clean out trash that had accumulated in the Outfall. Subsequent to this cleanup, a 6.0 pH was
detected using Litmus paper. On May 1, 2015, we remobilized and resampled Outfall #1 for TSS and
pH. Both parameters were below benchmark levels (DMR, SDO, and laboratory analytical results -see
Appendix A and B). If you have any questions, or if we may be of further assistance, please contact me
at [e-mail] or 919.859.9987,
Sincerely,
Waters Edge Environmental, LLC
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
15-050

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out thisform, please visit: ligp://li2o.enr.state.nc.us/su/Forms Documents.htm#miscforms
Permit No.: LN J C! S 1 0 10 10 15 12 18 or Certificate of Coverage No.: _
Facility Name: Premiere Fibers
County: Anson
Inspector: Thomas Haynes
Date of Inspection: 5.1.15
Time of Inspection: 10:3D-11:30
Total Event Precipitation (inches): 0.12
Phonc No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0. l inches has
occurred_ A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permitter or Designee)
1 Outfall Description:
Outfall No. 001-005 Structure (pipe, ditch, etc.) Pipe to Ditch
Receiving Stream: Buffalo Creek
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturina
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Medium brown
T%___ 1 _rn

1 1
3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy:
1 0 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no
solids and 5 is the surface covered with floating solids:
1 O 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no
solids and 5 is extremely muddy:
O 2 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608

r
ceAnalyical
May 08, 2015
Mr. Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 27606
RE: Project: PREMIER FIBERS
Pace Project IVo.: 92248039
Dear Mr. Rahn:
Pace Analytical Services, Inc.
205 East Meadow Road • Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 04, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
terri.page spacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 12

eeAnalytr'eal
wxw.paoalabs:com
Project: PREMIER FIBERS
Pace Project No.: 92248039
Pace Ana VicaI Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Eden Certification IDS
205 East Meadow Road Sufte A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification X: 633
Virgin"ELAP Certification 4: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of PamAnaMical ServbM Inc, Page 2 of 12

eeAnalylical
www.patxNde.ram
Project: PREMIER FIBERS
Pace Project No.: 92248039
Lab ID Sample 10
92248039001 Ot.1TFALL 001
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 05/0111612,00 05/04/1511:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
wMuxd the written content of Pere Analytical Services, Inc.,
pace Analytical Services, Inc.
205 East Meadow Road - 50e A
Eden, NC 27288
J336)623-N21
Page 3 of 12

ceAnaVical
wrvw.paoelels.can
SAMPLE ANALYTE COUNT
Project, PREMIER FIBERS
Pace Project No.: 92248039
Pace Anayttcat Services, Inc:
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analyses
Lab tD Sample ID Method Analysts Reported Laboratory
92240039001 OUTFALL 001 SM 2540D JTF 1 PASI-E
EPA9040 DWJ 1 PASI-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In Tull,
without the written consent of Pace Analytical ServloM Inc,.
Page 4 of 12

aceAnalytrcal
wnryaceleLtcom
ANALYTICAL RESULTS
Project: PREMIER FIBERS
Pace Project No.: 92248039
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623489z1
Sample: OUTFALL 001 Lab lD: 92248039001 Collected; 05101115 12:00 Received: OS10411511:45 Matrix: Alater
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
25 0D Total Suspended Solids Anatylical Method: SM 2540D
Total Suspended Solids ND mg1L 2.5 2.5 1 05/05115 09:34
9040 pH Analytical Method: EPA9040
PH 6.6 Sid, Units 0.10 0.10 1 0510411514AS 1-13,1-16
Date: 05108►2015 04:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyhcal Services, Inc,
Pags5of12

wAnaly ical'
www.pxalebe.com
QUALITY CONTROL DATA
Project: PREMIER FIBERS
Pace Project No.: 92248039
QC Batch: EDEN118370 Analysis Method: SfM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92248039001
METHOD BLANK: 1449910 Matrix: Water
Associated Lab Samples: 92248039001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L NO 2.5 05105/15 09:27
Pace Ana tytical Services, Inc:
205 East Meadow Read - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1449911
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Suspended Solids mglL 250 224 90 90-110
SAMPLE DUPLICATE: 1449912
92247745M Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Total Suspended Solids mg/L 32.6 28.2 15 5 D6
Results presented on this page are in the unRs hrdlcated by the "Unks" column except where an akemMe unR Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0510812015 04:02 PM witt*ut the written consent of Pace Analytical Services, Ina.
Page 6 of 12

IeArralytical
twnxpt owshtwn
14111141fatial011 Mal 49L-iEl
Project: PREMIER FIBERS
Pace Project No.: 92245039
QC Batch: EDENl18361 Analysis Method: EPA9040
QC Batch Method: EPA9040 Analysis Descriptlon: 9040 pH EDEN
Associated Lab Samples: 92248039001
SAMPLE DUPLICATE: 1449559
Parameter
PH
Pace Analytical Services, Inc.
205 East Meadow Road - 8Oe A
Eden, NC 27288
[phone]
92248039001 Dup Max
Units Result Result RPD RPD Qualifiers
Std, Units 6.5 6.6 0 9 H3,H6
Results presented on thfa papa an to the unite fndkatsd by the " 11nlh" catumn except when an alternate unit Is presented to thedpht of theresult.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except fn full,
Date: 05108=15 04:02 PM wfthout the wr ten consent of Pace Analytical Services, Inc .
Page 7 of 12

I f
Pace Analytical Services, Inc:
e/'!nalytka'e 205 East MeadowEden, NC 27288
rKva' mn (335)623Z921
QUALIFIERS
Project: PREMIER FIBERS
Pace Project No.: 92248039
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection Iimit and below the adjusted reporting limit,
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantftatfon Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenythydrazine decomposes to and cannot be separated from Azobonzone using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guldelines, unrounded data are displayed and have been used to calculate % recovery and RPD values,
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD- Relative Percent Difference
NO - Not Calculable.
SG - Silica t,yel- Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethytvinyt ether, Styrene, and Vinyl chloride,
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acro lain and Acrylonitr€le by EPA
Method 8260.
N-Nitrosodlphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Inst€t w.
LABORATORIES
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
DO The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits,
M3 Sample was received or analysis requested beyond the recognized method holding time.
H6 Analysts initiated outside of the IS minute EPA recommended holding time.
Data: 0510812015 04:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of pace AnalyN l Servicea, Inc.
Page 8 of 12

i
P9ce Analytical Services, Inc.
�t __ f, 1f,,,, f 205 East Meadow Road -Sulfa A
Ce�f�jl�/�0 VEdon, NC 27288
www.P9Wbba0om
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: PREMIER FIBERS
Pace Project No.: 92248039
Analytical
Lab tD Sample ID QC Batch Method QC Batch Analytical Method Batch
92248039001 OUTFALL 001 SM 2540D EDEN/18370
92249039001 Ot1TFALL 001 EPA 9040 EDENl18381
Data: OW81201 S O4:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 9 0112

• . .
,CE�;/lai}ItICc�
b�� etie
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain-of-GRrAndy Is a LEGAL DOCUMENT. M mleveMSelds must be completed a=rately.
Seetbat A section a Section G
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CHAIN -OF -CUSTODY 1-Analytical Ret�uest'Wcument
ace 1�,� r.. The Ctwk.os.cusMdr o a LEGAL DOCUM84T. an relevant dales Muir be, a=UtafetY
Ssotlorl A SacLion B Sestlon C. .
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ge 12 of 12

WATERS EDGE ENVIRONMENTAL. LLC
901 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 • PHONE [phone] • FAX [phone]
MEMORANDUM
Date February 3, 2015
To Mr. Dewey Fulton and Ted Kalamatas - Premiere Fibers
From Mr. Phil Rahn - Waters Edge
Subject April -September 2014 Stormwater Sampling Problems
Premiere Fibers
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge performs the Stormwater sampling for the Premiere Fibers facility located in
Ansonville, North Carolina (Stormwater Permit No. NCS000528). We conducted the Year
5- Period 2 sampling on March 18, 2014 and had several exceedances of benchmark
standards. Based on the permit, a Tier I inspection was conducted and then an additional
sampling round was conducted on April 15, 2014. Since the permit had expired, our
sampler believed that the sampling conducted on April 15, 2014 would suffice for the April -
September 2014 period of the new permit which we had not received. Based on additional
conversations with Premiere, it is our understanding that NCDENR disagrees that this April
2014 sampling would suffice since it was for a subset of the required analytical parameters.
This was an error by our sampler and we regret the oversight.
We are being forwarded a copy of the new permit and will comply with the sampling
requirements for October 2014-March 2015 time period. If there are any questions, please
contact me at [e-mail] or 919.219.5820.

MWAT,�ERS EDGE ENVIRONMENTAL, LLC
4901 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 •PHONE [phone] • FAx [phone]
April 28, 2014
NCDENR
Division of Water Quality
Central Files
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617
Reference: Year 5- Period 2 Stormwater Monitoring Report
Premiere Fibers Facility
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge Job No. R9-21
To Whom It May Concern:
We have previously submitted a stormwater monitoring report for Year 5- Period 2 in 2013-2014. All
results were within required benchmark parameters with the exception of a TSS exceedances for Outfall
#1 (TSS detected at 366 mg/L versus a 100 mg/L benchmark) and several pH exceedances (Outfall #1 at
5.9, Outfall #2 at 5.9, Outfall #3 at 5.8, and Outfall 44 at 2.8.. It was concluded that the TSS
exceedances was due to significant construction activities associated with a building expansion in that
area of the site. Most of the pH exceedances were near the lower 6.0 lower benchmark and could be due
to causes that are beyond the control of the facility (e.g. acid rain). However, the 2.8 reading at Outfall
#4 was considered to be anomalously low. During the sampling, we saw no unusual characteristics
(color, turbidity, etc.) that would indicate anything out of the ordinary. However, we conducted a Tier 1
inspection on April 9, 2014 and there wasn't anything unusual noted at the Outfall.
On April 15, 2014, we returned to the facility and resampied Outfall 41 (TSS) as well as Outfall #144
(pH) and all parameters were within the benchmark parameters (SDO, DMR, and analytical results
contained in Appendix A and B). This was conducted subsequent to the expiration of the stated permit
on March 31, 2014. We have applied for a permit renewal. We will record the Tier One response in the
Stormwater Pollution Prevention Plan (SPPP). If you have any questions, or if we may be of further
assistance, please contact me at prahnnwatersedgeenv.com or 919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
-;;� 4
74,o�e,
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
14-037A

Permit Number: NCS 000528
Certificate of Coverage Number: NCG
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
SAMPLES COLLECTED DURING CALENDAR YEAR: 2014
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME Premiere Fibers COUNTY Anson
PERSON COLLECTING SAMPLE(S) T. Haynes PHONE NO. 704 826.8321
CERTIFIED LABORATORY(S) Pace Lab # 633
Part A: Specific Monitoring Requirements
or
Lab # (SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate complete to
the best of my knowledge.
Outfall
�1Vo
Date
Sample
Collected
'
;
Total z 's
Rautfall
dotal -
Sus endues
:COD
pII="
F
h
Permit Bench-
_-
`-N/A
-,AJ _;
. � i20 -41
014 `
11 1..
. _�
mo/ddtyr ::.
finches;
. u m
64 imo: i. 9
W
1
3.18.14
0.28
366
ND
5.9
2
3.18.14
0.28
37.6
ND
5.9
3
3.18.14-
0.28
5.8
26.0
5.8
4
3.18.14
0.28
47.0
42
2.8
5
3.18.14
0.28
14.5
ND
6.2
1
4.15.14
0.34
66.9
NA
6.2
2
4.15.14
0.34
NA
NA
6.4
3
4.15.14
0.34
NA
NA
6.3
4
4.15.14
0.34
NA
NA
6.5
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No
: • . Date
"Sample
_ 5005©.
00556 .
-00530
00400 a
Tafal F[ow
Total Rawfal!
O�i &,Grease,-
Total
pH
r:New Motor 0�l .:
Colletteds
(if appl cable)
;,
k
5uspend'ed :
,
Usage
MG-"
inches;`
Uiaolddvr ui-
oMe
STORM EVENT CHARACTERISTICS:
Date 3.18.14
Total Event Precipitation (inches):
Event Duration (hours): NIA
0.28 (March)10.34
(April)
(only if applicable — see permit.)
(if more than one storm event was sampled)
Date 3.18.14/4.15.14
Total Event Precipitation (inches): 0.28/0.34
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Date
Form S W U-246-112608
Page 2 of 2

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: httt)://h2o.enr.state.nc.tislsip/Forms_ Documents.hini4miscforms
Permit No.: 31 N C I S `:. 0 0 10 r 5 2 18 or Certificate of Coverage No.:
Facility Name: Premiere Fibers
County: Anson
inspector: Thomas Haynes
Date of Inspection: 3.18.14
Time of Inspection: 10:00-1100
Total Event Precipitation (inches): 0.28
Phone No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to_10 consecutive hours of no precipitation.
-----
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
— — z
;�K/_
(Signature of Permittee or Designee)
1 Outfall Description:
Outfall No. on1-nn5
Structure (pipe, ditch, etc.) . Pipe to Ditch
Receiving Stream: Buffalo Creek
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturina
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Medium brown
Page 1 of 2
S WU-242- l 12608

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy:
1 O2 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no
solids and 5 is the surface covered with floating solids:
Q 2 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no
solids and 5 is extremely muddy:
1 Q 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608

0
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http://h2o.enr.state.nc.us/sit/Fonns Docunients.htm#niisefonns
Permit No.: i N' C i S' 0 10 i 0 i 5: 2# 8 j or Certificate of Coverage No.: { j
Facility Name: Premiere Fibers
County: Anson
Inspector: Thomas Haynes
Date of inspection: 4.15.14
Time of Inspection: 10:15-11:00
Total Event Precipitation (inches): 0.34
Phone No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no�recipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
- � xt,/_
(Signature of Permittee or Designee)
l Outfall Description:
Outfall No. 001-005
Receiving Stream: Buffalo Creek
Structure (pipe, ditch, etc.) Pipe to Ditch
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturinq
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Medium brown
Page I of 2
S W U-242-112608

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy:
1 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no
solids and 5 is the surface covered with floating solids:
l (2 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no
solids and 5 is extremely muddy:
I Q 3 4 5
7 Is there any foam in the stormwater discharge? Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
IU Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242-112608

aceftlydml
w+►w.psoe(a6s.can
April 01, 2014
Mr. Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 27606
RE: Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
Dear Mr. Rahn:
Pace Analytical Services, Inc.
265 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 18, 2014, The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Ino..
Page 1 of 14

_ 2ce Analytical`
www.pacelahs.own
I
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden. NC 27288
[phone]
CERTIFICATIONS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massa chusetts'Certifrcation #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certiflcation #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 14

aceAnalytical
wxwpecelaba.cam
i
SAMPLE SUMMARY
Project: PREMIERE FIBERS 139-21
Pace Project No.: 92193713
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Matrix Date Collected Date Received
92193713001
OUTFALL 001
Water 03/18/14 11:00 03/18/14 15:05
92193713002
OUTFALL 002
Water 03/18/14 11:15 03/18/14 15:05
92193713003
OUTFALL 003
Water 03/18/14 11:30 03/18/14 15:05
92193713004
OUTFALL 004
Water 03/18/14 11:45 03/18/14 15:05
92193713005
OUTFALL 005
Water 03/18/14 12:00 03/18/14 15:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 14

ace ldmlytrcal'
I` wwxpacelabs.com
f
SAMPLE ANALYTE COUNT
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
Pace Analyticat Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92193713001
OUTFALL 001
EPA 9040
JTF
1
PASI-E
SM 2540D
MAB
1
PASI-A
SM 5220D
EWS
1
PASI-A
92193713002
OUTFALL 002
EPA 9040
JTF
1
PASI-E
SM 25400
MAB
1
PASI-A
SM 5220D
EWS
1
PASI-A
92193713003
OUTFALL 003
EPA 9040
JTF
1
PASI-E
SM 2540D
MAB
1
PASI-A
SM 5220D
EWS
1
PASI-A
92193713004
OUTFALL 004
EPA 9040
JTF
1
PASI-E
SM 2540D
MAB
1
PASI-A
SM 5220D
EWS
1
PASI-A
92193713005
OUTFALL 005
EPA 9040
JTF
1
PASI-E
SM 2540D
MAB
1
PASI-A
SM 5220D
EWS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shatl not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 14

Pace Analytical Services, Inc.
;aceAnalytical* 205 East Meadow Road -Suite A
Eden, NC 27288
' wwwcpsc&bd.eorn [phone]
ANALYTICAL RESULTS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
Sample: OUTFALL 001 Lab ID: 92193713001 Collected: 03/18/14 11:00 Received: 03/18/14 15:05 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF
Prepared Analyzed CAS No. Qual
9040 pH
Analytical Method: EPA 9040
pH
5.9 Std. Units 0.10
0.10 1
03/19/14 09:36 H6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
366 mg/L 25.0
25.0 1
03/25/14 07:17
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg/L 25.0
25.0 1
03/24/14 17;00
Sample: OUTFALL 002
Lab ID: 92193713002 Collected:
03/18/14 11:15
Received:
03/18/14 15:05 Matrix: Water
Report
Parameters
Results Units Limit
MDL
OF
Prepared
Analyzed CAS No.
Qual
9040 pH
Analytical Method: EPA 9040
pH
6.9 Std. Units 0.10
0.10
1
03/19/14 09:36
H6
25400 Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
37.6 mg1L 5.0
5.0
1
03/25/14 07:17
D6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg1L 25.0
25.0
1
03/31/14 14:41
Sample: OUTFALL 003
Lab ID: 92193713003 Collected:
03/18/14 11:30
Received:
03/18/14 15:05 Matrix; Water
Report
Parameters
Results Units Limit
MDL
OF
Prepared
Analyzed CAS No.
Qual
9040 pH
Analytical Method: EPA 9040
pH
5.8 Std. Units 0.10
0.10
1
03/19/14 09736
H6
2540D Total Suspended Solids
Analytical Method; SM 2540D
Total Suspended Solids
5.8 mg1L 2.9
2.9
1
03/25/14 07:17
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
26.0 mg/L 25.0
25.0
1
03/31/14 14741
Sample: OUTFALL 004
Lab ID: 9219371300.4 Collected:
03/18/14 11:45
Received:
03/18114 15:05 Matrix: Water
Report
Parameters
Results Units Limit
MDL
OF
Prepared
Analyzed CAS No.
Qual
9040 pH
Analytical Method: EPA 9040
pH
2.8 Std. Units 0.10
0.10
1
03/19/14 09:36
H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01/2014 05:17 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 14

aceAnalyfrcal`
' WWW.paCef9hacorrr
1
ANALYTICAL RESULTS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)623-B921
Sample: OUTFALL 004
Lab ID: 92193713004 Collected:
03/18/14 11:45
Received: 03/18/14 15:05 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
47.0 mg/L 2.8
2.8 1
03/25/14 07:18
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
42.0 mg/L 25.0
25.0 1
03/31/14 14:41
Sample: OUTFALL 005
Parameters
Lab ID: 92193713005 Collected:
Report
Results Units Limit
03/18/14 12:00
MDL DF
Received: 03/18/14 16'05 Matrix: Water
Prepared Analyzed CAS No. Qual
9040 pH
Analytical Method: EPA 9040
pH
6.2 Sid, Units 0.10
0.10 1
03/19/14 09:36 H6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
14.5 mg1L 2.6
2.6 1
03/25/14 07:18
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
ND mg/L 25.0
25.0 1
03/31/14 14:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01/2014 05:17 PM without the wntten consent of Pace Analytical Services, Inc.. Page 6 of 14

aceAnalytical
' www.pacalabscom
I
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
QC Batch: EDEN114014 Analysis Method: EPA9040
QC Batch Method: EPA9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92193713001, 92193713002, 92193713003, 92193713004, 92193713005
SAMPLE DUPLICATE: 1159991
Parameter
pH
Date: 04/01/2014 05:17 PM
92193713001 Dup
Units Result Result
Std. Units 5.9 5.8
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Max
RPD RPD Qualifiers
1 20 H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 14

aceAnalytical
www pecefahs.cam
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
QC Batch: WET130154
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92193713001, 92193713002, 92193713003, 92193713004, 92193713005
METHOD BLANK: 1163771
Matrix: Water
Associated Lab Samples: 92193713001, 92193713002,
92193713003, 92193713004, 92193713005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L
NO 2.5 03/25/14 07:14
LABORATORY CONTROL SAMPLE: 1163772
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mglL
250 254 102 80-120
SAMPLE DUPLICATE: 1163773
92193672006 Dup Max
Parameter Units
Result Result RFD RPD Qualifiers
Total Suspended Solids mg/L
NO NO 10
SAMPLE DUPLICATE: 1163774
92193713002 Dup Max
Parameter Units
Result Result RPD RPD Qualifiers
Total Suspended Solids mglL
37.6 47.8 24 10 D6
Date: 04/01/2014 05�17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, inc..
Page 8 of 14

ace Ana,(Xical o
www.peoelebs.wm
Project: PREMIERE FIBERS R9.21
Pace Project No.: 92193713
QC Batch: WETA118458
QC Batch Method: SM 5220D
Associated Lab Samples: 92193713001
METHOD BLANK: 1163154
Associated Lab Samples: 92193713001
Parameter Units
Chemical Oxygen Demand mg1L
QUALITY CONTROL DATA
Analysis Method: SM 52201)
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 03/24/1417:00
Pace Anatytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1163155
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg1L 750 776 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1163156 1163157
MS MSD
92193424001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L 4220 7500 7500 11200 11200 93 93 75-125 0 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1163158 1163159
MS MSD
92193441003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L 7830 7500 7500 15000 14800 95 93 75-125 1 20
Date: 04/01/2014 05:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 14

Pace Analytical Services, Inc.
m 205 East Meadow Road - Suite A
aceAnalytrcal Eden, NC 27288
r www.peWabscom [phone]
I
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
QC Batch: WETA/18509 Analysis Method: SM 52201D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92193713002, 92193713003, 92193713004, 92193713005
METHOD BLANK: 1166807 Matrix: Water
Associated Lab Samples: 92193713002, 92193713003, 92193713004, 92193713005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 03/31/14 14:41
LABORATORY CONTROL SAMPLE: 1166808
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 743 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1166809 1166810
MS MSD
92194855001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L 477 750 750 1210 1210 97 98 75-125 0 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1166811 1166812
MS MSD
92194629001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg/L 2640 15000 15000 16800 16900 95 95 75-125 0 20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01/2014 05A7 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 14

/ice Analytical
1 www.pacefabs.mm
QUALIFIERS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(0) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01/2014 05A 7 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 14

aceAnalytical
f %Wpecela5aoom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92193713
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92193713001
OUTFALL 001
EPA 9040
EDEN/14014
92193713002
OUTFALL 002
EPA 9040
EDEN/14014
92193713003
OUTFALL 003
EPA 9040
EDEN/14014
92193713004
OUTFALL 004
EPA 9040
EDEN/14014
92193713005
OUTFALL 005
EPA 9040
EDEN/14014
92193713001
OUTFALL 001
SM 2540D
WET130154
92193713002
OUTFALL 002
SM 2540D
WET/30154
92193713003
OUTFALL 003
SM 2540D
WET/30154
92193713004
OUTFALL 004
SM 2540D
WET130154
92193713005
OUTFALL 005
SM 2540D
WET/30154
92193713001
OUTFALL 001
SM 5220D
WETA/18458
92193713002
OUTFALL 002
SM 5220D
WETA/18509
92193713003
OUTFALL 003
SM 5220D
WETA/18509
92193713004
OUTFALL 004
SM 5220D
WETA/18509
92193713005
OUTFALL 005
SM 5220D
WETA/18509
Date: 04/01/2014 05:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc„
Page 12 of 14

I
CHAIN -OF -CUSTODY 1 Analytical Request Document
L�liU I'V IUJ✓ � '�y� • i The Chain -of -Custody Is a LEGAL DOCUMENT. NI relevant fields must be completed accurately.
ww.paeslaks.aom
Section A Section 8 Section C Page: % of I
Required Client Information: Required Project Information: I Invoice Information: 1712796
Compan : YUZ-�� / Report To: Attention: .L 712 7 9 6
Address: �^J�f �/ Copy To: T Company Name: - I -. Fi ui ATOCX -:
Address. r NPDES - r GROUNDWATER r DRINKING WATER
Email To: �Fa
Purchase Order No.: Para QuoinPhone: ( Reference:
�'" UST RCRA OTHER ProjectNarrre: PnxPrged Sitel.ocatiori
Requested Due DatdTAT: Project Nu Pem gPro{b ft y
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Section D MaMi odes g - - -
Req¢IrWCI{entlydonnsllon nrArRlx ClCODE § o 'COLLECTED Preservatives >- _
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Drinking weir DW g
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Waste Water WW cc wpcd3m
Product P �rcT ENDOW u� ,
SoillSoid SL U ��
SAMPLE ID Oil
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Sample IDs MUST BE UNIQUE Tissue TS O a m : R' P �{
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p to Q df
f Co nA ONE DATE TIME # � _ Z.
C71 z z z 2 O ;,� 11 Pace Project NoJ Lab I.U.
.5
B -
-z, I
a _
g.
�11 -
12
-ADDfTIDNAI: COMMENTSRk_LINQUISwr:n Y! AFFILJATION QATE/7�1M`E - - 'ACCEPTEQ BY! AFFtLFATIQN-.aQATE . TIME SAMPLE CONDITIONS
I
3AMPLEi #FAME A_ND SIGNATURE � *
w ORIGINAL PRINT Name .ofSAMPLER-
. J
a _m
E U — E
SIGNATURE of SAMPLrR: DATE Signed rK Co
—
A 'Im Note: B nI this farm are mce Hn Pace's NET 30 and agreebw to late charges of 1.5% per month for any invam" not paid 3o days. F-ALL-Q. 420rev.07, i 5-M 2007
P Y �6 n9 Y� P g day Pa!' ay-

f7 RVG/"U1a1Y111.PQl •wr...., vvw♦
Document No::
rEUV i VIA
issuing AuthMties
F->ADN7-CS-003-rev,09
Pace Eden Wit•Office
G11ent Name:: .�;. ...
.
Where.Recelved: ❑ Huhtersville " ❑ Asheville Edon ❑
Raleigh
Courier (circle): ' Fed Ex :UPS . USPS lie Commercial Pace Other
Custody Seal on Cooierlt3ox Present: DyesPIrKo Seals Intact: ❑ yes
❑ no r
.l,
Packing Materlal: [3ubble Wrap "❑Bubble Bags ane ❑. Cther
i
Thermometer Used: IR Gun ED007 'j`ype of ice; a Blue None
Ales on toe, pooling procBss has bsgun ', -...
Temp Correction Factor0AMA ) Subttac# _C
r
carrected cooler Terizp.: C $lolpgirsal•Tfssue Is Frozen: Yes Na :NIA'
pate and in , s of person nine .
:"
contents:
Tempshould be above frgez€ng to siG _ .Coninfents:, .'....
. .
Chain of OustPresent: , .... Yea ONO ". ]WA 1.
Chafe of Cuk�Flfied Out:. .Urea, QNo . ONA
Chain ofCustb Relin bished:. ...'.. Yea: ONa, ON/A 3.
Sampler Nama & SI nature on COC: " , .. Yes. ONo, ❑WA, 4.
Samples Antved.wlthin.Hold Time; ..: : " .: ea ❑No OWA.
Short Hold Time Analysts ra72hr :. Yes .LINO
Rush:TuM Around.Tlme Re nested: " ". ". ©Yee, I]Nq. R<A 7..,.
Sufficient Volume: - .:• o... jatres ❑N ©WA 8.
CorrectContalrim' 'Used: .fires. OIYo ,.F"1N1A 9.
-Pace Contalners Used: 2ea ONo,. ©NA::.
Containers Intake , ....... :" TYes dNo. 13WA 10.:....
Filtered volume reoelved.for Dissolved tests 'C1Yes ONO Lko 11.
Sample Labels match COC: sea ©No I NrA 12,
-Includes datehlmeAgL) nal sR Matltic
All oontalners needing preeervallon have bean oheoked:
No bWA
r"
�•
All oontoom needing preservation are found to be In ONO ❑ WA
oompllance With EPA recommendation.
"
lens: 1'bA, oolltorm roc k)&Q, Wf {iR0 wets I]Yes. 13 No Initial when dom mad.
Samples chocked f6r'doohlorination: es ❑No ..DWA 14.
Headsoe In VOA Vlals Amm :. ❑veo : C1No �WA
16.
Trap Blank Present:: Oyes ONO MA 16..
Ttfp.Blank Custody Seals Present . ©Yes ❑No.. A
Pace Trlp Blank Lot # if urchasa
Client Notification/ Resolution:
Field Data Required? Y" I N
Person Contacted: DateMme:
Comments/ Resolution;
SCURF Review: Dater
dDate.-`
Place label here
SRF Review:
x1namplianoe
OR
Note: Whenever there is a disomwoy affecting North Ca
samples; a copy of this form will be sent to the North Carolina DEHNR
Handwrite project number
n w jectavainumber
Cenlfloatlon Offloe ( Le out of bald, incorrect preservattvs, out of temp,
label
incorrect oontalners)
Page 14 of 14

_ 2ce Analytical
� www.pecelebs.cam
i
I
April 23, 2014
Mr. Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 2760E
RE: Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on April 15, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, .
without the written consent of Pace Analytical Services, Inc..
Page 1 of 12

Pace Analytical Services, Inc.
aceAllalytrca! b 205 East Meadow Road - Suite A
Eden, NC 27288
wxwpeoeleba.com [phone]
CERTIFICATIONS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certification #: 37738 VrginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 12

0kialytrcal
www.Paaelabs.cam
)
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
Lab ID Sample ID Matrix Date Collected Date Received
92197489001
OUTFALL 001
Water
04/15/14 12:15
04115/14 15:25
92197489002
OUTFALL 002
Water
04115/14 12:00
04/15/14 15:25
92197489003
OUTFALL 003
Water
04/15/14 11:45
04/15/14 15:25
92197489004
OUTFALL 004
Water
04/15/14 12:15
04/15/14 15:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 12

aceAnalyt#ical
� www.paoefaes.ean
I
SAMPLE ANALYTE COUNT
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID -
Sample ID
Method
Analysts
Analytts
Reported
Laboratory
92197489001
OUTFALL 001
SM 2540D
JTF
1
PASI-E
EPA 9040
JTF
1
PASI-E
92197489002
OUTFALL 002
EPA 9040
JTF
1
PASI-E
92197489003
OUTFALL 003
EPA 9040
JTF
1
PASI-E
92197489004
OUTFALL 004
EPA 9040
JTF
1
PASi-E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 12

aceAnalyifical
I - trwwpaceiabacom
f
i
ANALYTICAL RESULTS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 272BB
[phone]
Sample: OUTFALL 001
Lab ID: 92197489001 Collected:
04/15/14 12:15
Received: 04/15/14 15:25 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF
Prepared Analyzed CAS No, Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
66.9 mg/L 2.8
2.8 1
04/18114 08:36
9040 pH
Analytical Method: EPA 9040
pH
6.2 Std. Units 0.10
0.10 1
04/16/14 12:20 H3,H6
Sample: OUTFALL 002
Lab ID: 92197489002 Collected:
04/15/14 12:00
Received:
04/15/14 15:25 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF
Prepared
Analyzed CAS No.
Qual
9040 pH
Analytical Method: EPA 9040
pH
6.4 Std. Units 0.10
0,10 1
04/16/14 12:20
H3,H6
Sample: OUTFALL 003
Lab ID: 92197489003 Collected:
04/15/14 11:45
Received:
04115/14 15:25 Matrix: Water
Report
Parameters
Results Units Limit
MDL OF
Prepared
Analyzed CAS No.
Qual
9040 pH
Analytical Method: EPA 9040
pH
6.3 Std. Units 0.10
0.10 1
04/16/14 12:20
H3,1-16
Sample: OUTFALL 004 Lab ID: 92197489004 Collected: 04/15/14 12:15 Received: 04/15/14 15:25 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
9040 pH Analytical Method: EPA 9040
pH 6.5 Std. Units 0.10 0.10 1 04/16/14 12:20 H3,H6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/23/2014 11:21 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12

aceAnalytical
wxw.pacetaes.cam
r
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
QC Batch: EDEN114351
QC Batch Method: SM 2540D
Associated Lab Samples: 92197489001
METHOD BLANK: 1181046
Associated Lab Samples: 92197489001
Parameter Units
Total Suspended Solids mglL
LABORATORY CONTROL SAMPLE: 1181047
Parameter Units
Total Suspended Solids mg1L
SAMPLE DUPLICATE: 1181046
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1181049
Parameter
Total Suspended Solids
Date: 04/23/2014 11:21 AM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 04/18/14 08:34
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
250 236 94 80-120
92197629001 Dup
Units Result Result
mg/L 97.7 78.0
92197707002 Dup
Units Result Result
mg1L 7520 6780
Max
RPD RPD Qualifiers
22 10 R1
Max
RPD RPD Qualifiers
10 10
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 12

11eAnalyticale
www.pacefeea.own
QUALITY CONTROL DATA
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
QC Batch: EDEN114321 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92197489001, 92197489002, 92197489003, 92197489004
SAMPLE DUPLICATE: 1179574
92197489001 Dup
Parameter Units Result Result RPO
pH Std. Units 6.2 6.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/23/2014 11:21 AM without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Max
RPD Qualifiers
1 20 H3,H6
Page 7 of 12

aceAnalytrcal
www.pecefehs.wm
QUALIFIERS
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
DF : Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPO values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/23/2014 11:21 AM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12

lice Analyfica I
' www.pec"s.mm
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: PREMIERE FIBERS R9-21
Pace Project No.: 92197489
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92197489001
OUTFALL 001
SM 2540D
EDEN/14351
92197489001
OUTFALL 001
EPA 9040
EDEN114321 <
92197489002
OUTFALL002
EPA9040
EDEN114321
92197489003
OUTFALL003
EPA9040
EDEN114321
92197489004
OUTFALL004
EPA9040
EDEN114321
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0412312014 11:21 AM without the written consent of Pace Analytical Services, Inc.. Page 9 of 12

72ce Ana ical'
' rrrw.pace-Isps,com
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Sectian B Section C
Page_ ! of
Required Client Information: Required Project Information: Invoice information;
Company: To: Attention:
0 O
/'
fAy.Report
..L
Address:
Copy To: ff
Company Name:
- -
REGULAT0RY AGENCY c
r NPDES r GROUND WATER r DRINKING WATER
r UST r RCRA OTHER'
Email To:
Purchase Order No.:
�e emote
Reference:
Phone:
Fax:
Project Name:
7 �r� b
Pace Prole -A
Hammer
°
S[te Location
-
_
-
Requested Due Date/TAT:
Project Number: � _
Pate Profile#:
Requested
--
Ailialysili`Filtered'{Y1N)
_
- _ -
- j
Section D Matrtx Codes
z
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RegrdredCKerdlnfwnra0on LdET31x1cCZpE
COLLECTED
Pneservaums
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Drinking water Dw
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WIT
Waste Water WW
c�
COsr��
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Product P
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SAMPLE ID pa wP
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(A-Z. D-9l:) Air AR
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Sample ]Ds MUST BE UNIQUE Tissue VS
O
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Other OT
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DATE
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#
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2
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PBCB Project T10J Lab I.D.
--
3
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16
11
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- -:' AODFTIONAL COMLEENTS _ ` -i
'-RELINQUISHED BY IAFFILWTIO#f
-OATEN_
-; TIME
I - ACCEPTED BY IAFFRIATION
DATE--'
TIME -.%
SAMPLE CONDITIONS
SAMPLER NAME AND SIGIEATIIRE _ t :_
U
`a
6
9
c
o ORlGINA1 PRINT Name wsAMPLt=R
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� �_
_
DATE Signed
8
sICNATURs of SAMPLER: qr�{MMlDD0 ry
~
n
,1.. rtm Now, ay sW&V cos Term you me amapWnq Pace's NET 30 day paymoM terms and apreeMp m 181a rhaTM of 1.5% PM month oF�r eny invoices ra I g rr sa days. f / r F-Ai.i.41020ray.07, 15-May-2(l07

`. aceAnal ical e.
: - www.;tacalabs.com
Section A :
Section 8 .
Required GfeM Information:.
Required Project
['-amPaR9""
Re •Tn-
Address: /
Copy To: ,
J
r
Ernad To: _ / /
Purchase Odder I1
CHAIN -OF -CUSTODY
The Chain-oi-Custody Is a LEGAL 0
-
-- SectionC
umation:
Invoice inf,Dm
.
-
Anartdon! -
�!
Company Nar
- - ...
Address:
P*wQw a
Reference:
'hone:
Fax:
Project Name:
Para
taquestad Due DatdTAT. - -
Project Number.
Pau
-
Section D _ Matrix Codas
Rogvbvd Gent k4o"adon MATRIX r CODE
—°o'
g
COLLECTED' -
: Drirddng Water DW
U
zz
:
-
'
Water -'. WT
U
' Waste Water WW
a
Do�E
coMPosrcP
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Product P -
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WrAW �
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SAMPLE ID Oil
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Sample IDs MUST BE UNIQUE -'. Tmaue - TS
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DATE
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V-
ADDITIORAL COMMENTS
.1 Analytical Request Document
OCUMENT. AN retevam fields must he completed accurately.
s'
M®�
W■■■■■■■■■■
■■■■O■■■■■■■■■
SAMPLER NAME AND SIGNATURE
U o
m
.
- _ PRINT Name of SAMPLER: � �5 - �� -- - - -
- -
' Q � t, .
$ S Z_ •
z
- b - - - - DATE Signed
m `—m'
U
E `
- ry SIGNATURE of SAMPLER: (MMloD!'rY):
-
rn
100
N
•tmpwt&m Nate: By signing d83 f&m you are acceom Pace's NET,3U day payment temre and agreeing to late charges or 1.5% per month any 17nVDi= not pal n 3p days. -
F-ALL-Q-020rev.07,, 45-May-2007

Document Name., Sample Condition Upon
Document Revised: March l3, 2013
i�ARG31"
`�-
Recel t (SCUR)
Page 1 of 2.
Document No.:'
issuing Authorities:
F-EDN-CS-003-rev.09
Pace Eden Quail Office —
ClientName:
Where Received: ❑ Huntersville ❑ Asheville 2rEden ❑ Ralelgh
Cauriar (circle): Fed Ex _ UPS , .LISPS Ilent Commercla! !�
eusio eaI on-0oaledBox
Pacirin .. Mate�lal: alibis W----Bub61eOther
-- _ .......
9 mP ❑ cgs Nona ❑ OtherThermometer Used: IR Gun ED007 Typo of ice: a Blue None - plas on ioe, cooling prooesa has begun
Temp Correction Factor Ad ! Subtract�C -
Corrected CoolerTem.: C
Temp should be above freezing to 600
8biogica! Tissu® is Frozen: Yes Na NIA
Comments: '
Date and Initials of person examining
contents:
Chain of Custody Present:
Oyes ONO
EINIA
f.
Chain of Custody Fllled Out:
JffYes ❑No
0NVA
2,
Chain of Custody Relinquished:
ea ❑No.
❑WA
3.
Sampler Name & Signature on COC:
PYes. 014o
❑N/A
4.
Samples Arrived within Hold Time:
es ONO
❑NIA
5.
Short Hold Time Analysis <72hr :
ee ONO
❑WA
6.
Rush Turn Around Time Requested:
❑Yes ONO
❑ A
7. .
Sufficient Volume:
❑ ee ❑No
❑NIA
9:
Correct Containers Used:
Pace Containers Used:
0se ONO
Yes ONO
❑N1A
❑NIA
9.
Containers Intact:
es ONO
❑wA
10,
Filtered volume received for Dissolved tests
OYea ONO
AVA
11.
Sample Labels match COC:
AYes ONO
❑NIA
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be In
compliance with EPA recommendation,
&M Clans: VO collform, TOO, o&Q, WE qR0 (wake
ONO.
,3�'s ©Na
�- �"
❑Yea ❑No
❑NIA
❑NlA
13.
Initial when ocm sled
�Js--
Samples checked for dechlorinatlori:
es ONO
❑NIA
14.
Heads ace In VOA Vials >6mm :
❑Yea .,❑No ../IA
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trig Blank Lot # if urchase
❑Yes ❑Nc
❑vas ❑No
0ydA
iI_1 A
16,
Client Notification/ Resolution: Field Data Required? Y / N.
Person Contacted: DateMme:
Comments/ Resolution:
SCURF Review: L Data: Place label here
SRF Review: Date:
Note: Whenever tftere is a dis panty affecting North C I a mp lance OR
samples, a copy of this form will be sent to the North Carolina DEHNR. Handwrite project number
Gerll"catlon Office (1.9 out of hold, Incorrect preservative, out of temp,
incorrect containers) (if no label available)
Page 12 of 12

,4 `WA"I"ER5 EDGE EN VERON,bfE�]TAL. LLC
4901 WATERS EDGE DRIVE, SUITE 201 • RALEIGH, NC 27606 • PHONE [phone] • FAx [phone]
August 1, 2013
NCDENR
Division of Water Quality
Central Files
1617 Mail Service Branch
Raleigh, North Carolina 27699-1617
Reference: Year 5- Period 1 Stormwater Monitoring Report (Fall 2013)
Premiere Fibers Facility
Ansonville, North Carolina
Stormwater Permit No. NCS000528
Waters Edge Job No. 119-21
To Whom It May Concern:
Please find enclosed the stormwater monitoring report for Year 5- Period I in 2013-2014. All results are
within required parameters (DMR, SDO, and laboratory analytical results -see Appendix A and B). If
you have any questions, or if we may be of further assistance, please contact me at
prahn c watersedgeenv.com or 919.859.9987.
Sincerely,
Waters Edge Environmental, LLC
Phillip L. Rahn
President
cc: Mr. Dewey Fulton and Mr. Kevin Bowers- Premier Fibers
13-108

Permit Number: NCS 000528
Certificate of Coverage Number: NCG
FACILITY NAME Premiere Fibers
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
or
SAMPLES COLLECTED DURING CALENDAR YEAR: .2013
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
PERSON COLLECTING SAMPLE(S) T. Haynes
CERTIFIED LABORATORY(S) Pace Lab # 633
Part A: Specific Monitoring Requirements
COUNTY Anson
PHONE NO. [phone]
Lab # (SIGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, 1 certify that this report is accurate complete to
the best of my knowledge.
* Outfall
No
.
f Ua
' Sample
-Y.Collecte�d _
Totals'
Rm a%tl
d
Total
Suspended
*lms'(T s
COD
H
;� _ _
-
OermAi W nch ,
« ql
l W
Z6
;�
A':
mo/dd/yr ,,
,.
r
� mg/1� �
_ .. Umts
l
T2.13
See Below
32.5
37
7.1
2
7.2.13
See Below
10.7
79
7.2
3
T2.13
See Below
4.0
35
6.8
4
7.2.13
See Below
15.8
35
7.4
5
7.2.13
See Below
13
79
7.4
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _ yes ✓ no (if yes, complete Part B)
Form SWU-246-112608
Page 1 of 2

Part B. Vehicle Maintenance Activity Monitoring Requirements
�Outfsll
No ,..
Date ,
Sample
- S00SQ
00556.
„g 00530
: ; 00400
' Total+Flower
Total Rainfall°
O &�`Gr ae se'
YTota , `
pN
IVew M©tor Oil
Collected
(ef applicable} M
ry
Suspended
Usage
Shcids`
moldd/yr
MG
inches 'a ff
mom
.. ...._
mal/mo 1
STORM EVENT CHARACTERISTICS:
Date 7.2.13
Total Event Precipitation (inches): (0.9)
Event Duration (hours): NIA (only if applicable — see permit.)
(if more than one storm event was sampled)
Date NIA
Total Event Precipitation (inches):
Event Duration (hours):
(only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Date
Form SW U-246-112608
Page 2 of 2

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance onfilling out thisform, please visit: htt ://h2o.enr.state.nc.uslsu/Forms Docunients.htm#miseforms
Permit No.: 11 N! C i S 0 i 0 1 0 i 5 12 18 i or Certificate of Coverage No.:
Facility Name: Premiere Fibers
County: Anson
Inspector: Thomas Haynes
Date of Inspection: 7.2.13
Time of Inspection: 13:00-14:00
Total Event Precipitation (inches): 0.9
Phone No. 704.826.8321
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please checkyourpermit to verify if Qualitative Monitoring must be performed during a representative storm event
(requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
�,�D,� 7 �/
(Signature of Permittee or Designee)
1 Outfall Description:
Outfal I No. 001-005
Structure (pipe, ditch, etc.) Pipe to Ditch
Receiving Stream: Buffalo Creek
Describe the industrial activities that occur within the outfall drainage area:
Textile Manufacturinq
2 Color:
Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as
descriptors:
Medium brown
Page l of 2
SWU-242-112608

3 Odor:
Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):
No odor noted
4 Clarity:
Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy:
]O 2 3 4 5
5 Floating Solids:
Choose the number which best describes the amount of floating solids in the stormwater discharge, where I is no
solids and 5 is the surface covered with floating solids:
1 a2 3 4 5
6 Suspended Solids:
Choose the number which best describes the amount of suspended solids in the stormwater discharge, where I is no
solids and 5 is extremely muddy:
1 O 3 4 5
7 Is there any foam in the stormwater discharge? •Yes No
8 Is there an oil sheen in the stormwater discharge? Yes No
9 Is there evidence of erosion or deposition at the outfall? Yes No
10 Other Obvious Indicators of Stormwater Pollution:
List and describe
None
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of
pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242-11260 &

aca m ytical
' www.paoalobs.corn
July 22, 2013
Mr. Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 27606
Pace Analytical Services; Inc.
205 East Meadow Road - Suite A
Eden. NC 27288
RE: Project: Premiere Fibers
Pace Project No.: 92163878
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on July 03, 2013. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNl standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
\-JX6
Terri'Page
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

aceAnalytical
j wwwpecerehs.cnm
Project: Premiere Fibers
Pace Project No.: 92163878
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
CERTIFICATIONS
[phone]
Asheville Certification Ibs
2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
FloridalNELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification* 356
North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9600 Kincey Ave. Suite 100
Huntersville, NC 2BO78
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 13

r aceAnalyfical
WW pscelafla coal
I
Project: Premiere Fibers
Pace Project No.: 92163878
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92163878001
Outfall001
Water
07102113 13:00
0710311315:35
92163878002
Outfall002
Water
07/02/1313:15
0710311315:35
92163878003
Outfall003
Water
07102/1313:30
0710311315:35
92163878004
Outfall004
Water
07102/1313:45
07/0311315:35
92163878005
Outfall005
Water
0710211314:00
0710311315:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc -
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 13

aceAnalytical
wrrwpecelahacom
1
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc,
2225 Riverside Or,
Asheville, NC 28804
(B28)254-7176
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Premiere Fibers
Pace Project No.:
92163878
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92163878001
Outfall 001
SM 25401)
CHM
1
PASI-E
EPA9040
CHM
1
PASI-E
SM 5220D
EWS
1
PASI-A
92163878002
Outfall 002
SM 2540D
CHM
1
PASI-E
EPA9040
CHM
1
PASI-E
SM 5220D
EWS
1
PASI-A
92163878003
Outfall 003
SM 2540D
CHM
1
PASI-E
EPA 9040
CHM
1
PASI-E
SM 5220D
EWS
1
PASI-A
92163878004
Outfall 004
SM 2540D
CHM
1
PASI-E
EPA9040
CHM
1
PASI-E
SM 5220D
EWS
1
PASI-A
92163878006
Outfall 005
SM 2540D
CHM
1
PASI-E
EPA9.040
CHM
1
PASI-E
SM 5220D
EWS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 13

aceAnalytkal®
www.parxlehsoom
1
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Premiere Fibers
Pace Project No.: 92163878
Sample: Outtall 001
Lab ID: 92163878001 Collected:
07/02/13 13:00
Received: 07/03/13 15:35 Matrix: Water
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed CAS No. Quai
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
32.5 mg1L 2.7
2.7 1
07/08/13 14:25
9040 pH
Analytical Method: EPA 9040
pH
7.1 Std. Units 0.10
0.10 1
07/08113 07:50 H6
6220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
37.0 mglL 25.0
25.0 1
07/18/13 16:00
Sample: Outfall 002
Lab ID: 92163878002 Collected:
07/02/13 13:15
Received:
07/03/13 15:35 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared
Analyzed CAS No.
Qual
2640D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
10.7 mg/L 2.5
2.5
1
07/08/13 14:27
9040 pH
Analytical Method: EPA 9040
pH
7.2 Std. Units 0.10
0.10
1
07/08/13 07:50
H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
79.0 mg/L 25.0
25.0
1
07/18/13 16:00
Sample: Outfall 003
Lab ID: 92163878D03 Collected:
07/02/13
13:30
Received:
07/03/13 15:35 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared
Analyzed CAS No.
Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
4.0 mg1L 2.6
2.6
1
07/08/13 14:34
9040 pH
Analytical Method: EPA 9040
pH
6.8 Sid. Units 0.10
0.10
1
07/08/13 07:50
H6
52200 COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
35.0 mg1L 25.0
25.0
1
07/18/13 16:00
Sample: Outfall 004 Lab ID: 92163878004 Collected: 07/02/13 13:45 Received: 07/03/13 15:35 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 15.8 mg/L 2.5 2.5 1 07/08/13 14:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in NO,
Date: 07/22/2013 11:45 AM without the written consent of Pace Analytical Services, Inc..
Page 5 of 13

Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
acek alytical
205 East Meadow Road - Suite A
2226 Riverside Dr.
9800 Kincey Ave, Suite 100
- wwwpecamb3.0"
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
1
[phone]
[phone]
[phone]
ANALYTICAL RESULTS
Project: Premiere Fibers
Pace Project No.: 92163878
Sample: Outfall 004
Lab ID: 92163878004 Collected:
07102/13 13:45
Received: 07/03/13 15:35 Matrix: Water
Report
Parameters
Results Units Limit
MOIL OF
Prepared Analyzed CAS No. Qual -
9040 pH
Analytical Method: EPA 9040
pH
7.4 Std. Units 0.10
0.10 1
07/08113 07:50 H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
35.0 mg1L 25.0
25.0 1
07/18/13 16:00
Sample: Outfall 005
Parameters
Lab ID: 92163878005 Collected:
Report
Results Units Limit
07/02/13 14:00
MDL OF
Received: 07/03/13 15:35 Matrix: Water
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
13.0 mglL 2.5
2.5 1
07/08/13 14:44
9040 pH
Analytical Method: EPA 9040
pH
7.4 Std. Units 0.10
0.10 1
07/08/13 07:50 H6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
79.0 mg/L 25.0
25.0 1
07/18/13 16:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 0712212013 11 A5 AM without the written consent of Pace Analytical Services, Inc- Page 6 of 13

ZaceAnalytical
www.Pecatab.com
J
Project: Premiere Fibers
Pace Project No.: 92163878
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: EDEN111978 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92163878001, 92163878002, 92163878003, 92163878004, 92163878005
METHOD BLANK: 1005927 Matrix: Water
Associated Lab Samples: 92163878001, 92163878002, 92163878003, 92163878004, 92163878005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 07/08/13 14:22
LABORATORY CONTROL SAMPLE: 1005928
Parameter Units
Total Suspended Solids mg1L
Date: 07122/2013 11:45 AM
Spike LCS
Conc. Result
250 258
Pace Analytical Services, Inc.
9800 Kincey Ave. Su4e 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
103 80-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page 7 of 13

aceAnalytical`
www.pawws.com
f
i
Project: Premiere Fibers
Pace Project No.: 92163878
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr,
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: EDEN/11973 Analysis Method: EPA 9040
QC Batch Method: EPA 9040 Analysis Description: 9040 pH EDEN
Associated Lab Samples: 92163878001, 92163878002, 92163878003, 92163878004, 92163878005
SAMPLE DUPLICATE: 1005705
92163670001 Dup
Parameter Units Result Result RPD
pH Std. Units 7.7 7.5 2
Date: 07/22/2013 11:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Max
RPD Qualifiers
20 H6
Page 8 of 13

aceAnalytrcal
w►vw.pacefahs.aom
Project: Premiere Fibers
Pace Project No.: 92163878
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr. .
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: WETA116847 Analysis Method: SM 5220D
QC Batch Method: SM 52200 Analysis Description: 5220D COD
Associated Lab Samples: 92163878001, 92163878002, 92163878003, 92163878004, 92163878005
METHOD BLANK: 1010609 Matrix: Water
Associated Lab Samples: 92163878001, 92163878002, 92163878003, 92163878004, 92163878005
Blank Reporting
Parameter Units Result Limit Analyzed
Chemical Oxygen Demand mg/L ND 25.0 07/18/13 16:00
Qualifiers
Paco Analytical Services, Inc.
980D KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1010610
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 762 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1010611 1010612
MS MSD
92163700001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mgtL 65.0 750 750 806 801 99 98 75-126 1 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1010613 1010614
MS MSD
92163878004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD RPD Qual
Chemical Oxygen Demand mg1L 35.0 750 750 773 776 98 99 75-125 0 20
Date: 07/22/2013 11:45 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
Page 9 of 13

e
aceARalytical
' www.pac&bd.com
I
Project: Premiere Fibers
Pace Project No.: 92163878
DEFINITIONS
Pace Analytical Servicee, Inc.
205 East Meadow Road - Su�te A
Eden. NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenythydrazine (8270 listed anaiyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nilrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
H6 Analysis initiated outside of the 15 minute EPA recommended holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/22/2013 11:45 AM without the written consent of Pace Analytical Services, inc.. Page 10 of 13

llceAnalyfical'
www.pacelehaeem
j
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Premiere Fibers
Pace Project No.: 92163878
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92163878001
Outfall 001
SM 2540D
EDEN111978
92163878002
Outfall 002
SM 2540D
EDEN111978
92163878003
Outfall 003
SM 2540D
EDEN111978
92163878004
Outfall 004
SM 2540D
EDENI11978
92163878005
Outfall 005
SM 2540D
EDEN111978
92163878001
Outfa11001
EPA 9040
EDEN/11973
92163878002
Outfall 002
EPA 9040
EDEN111973
92163878003
Outfall 003
EPA 9040
EDEN111973
92163878004
Outfall 004
EPA 9040
FDEN111973
92163878005
Outfall 005
EPA 9040
EDEN111973
92163878001
Outfall 001
I�
! SM 5220D
WETA115847
92163878002
Outfall 002
SM 5220D
WETA115847
92163878003
Outfall 003
SM 5220D
WETA115847
92163878004
Outfall 004
SM 5220D
WETA115847
92163878005
Outfall 005
SM 5220D
WETA115847
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/22/2013 11:45 AM without the written consent of Pace Analytical Services, Inc..
Page 11 of 13

aceAnal'�}ical'
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Pape of
Section A
Section B
Section C
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Rogrdred Cllent Information:
Required Project Intwmetion:
Invulce Imo:
Report To:
%7 _�
Attendon:
1629790
Address:
CapyTo:
Company Name:Addrew
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-hWwtam Nate: By *Fitt Cie loan you ate a M*V Pne's NET 30 dry PeY+we hrve wW aWveep Eo Ift o rg m or 1.5% per mood or cry hrvalm Doi t v OM d.,L / / F-ALL-Q-020rev.07, 15-May2007

pocument Name: Sample Condition Upon
lieael t SCIlR
Documenf Revlsed: March 13, 2013
P e 1 eta
Document No.:' . ; .
F-EDN-CS-003-rev.09
issuing Athbri�as:
race Eden Quality Office
Client Name: W4.
Where Roc6Wd: j] HuntersAlle ❑ Asheville den 0. ❑ Raleigh
Courier (circle): Fed Esc LIPS LISPS Ilent Commorolal Pace Other......
Custody Seal on Cooler/Box Present: .❑yes ❑' no Seals intact: ❑ yes ❑ no
Packing Material: 034bble Wrap ❑Bubble Bsas ❑ Nona Other
Thermometer Used; IR faun ED007 Type of ice: et Sloe Nona , mples on Ice, 000iing process has begun
Temo Correction Vactors. Addy Subtract 'hPek 0—A C
Corrected CoolorTempr C
Temp should be above freezing to B°C
Biological Tissue Is Frozen: Yes No NIA
Comments:
Data and Initi. trip,
Chain of Custod Present
es ©No
ClW'A 1,
Chain of Cust6dy Filled Out:
- es ❑No
QwA 2,
Chain of Custb& Relinquished.
.0& QNo
Elf iA 3.
Sampler Name & Si nature on COO:
05m Elmo
QWIA 4,
Samples Arrived within Mold Time: '
-an's m.
DNA 6.
Short Hold Time Analysis 2hr :
❑Yes vo
DWA 6.
Rush Turn Around Tfine Re nested:
bYea jb
El N/A 7,
Sufficient Volume.
Rfe QNo
DWA 18.
Correct Containers Used:
-Pace Containers Used:
des QNo
'Dws ©No
©NIA 9.
DWA
Containers Intact:
]:]�No
VWA 10.
Filtered volume received for pissofved tests
CIYes ❑No
a1VA 11.
Sample Labels match COO:
-Includes date/timelID/Analyals Matrbc
Yes ©No QwA 12.
N oontalners needing preservation have been oheciced.
If oontainers needing preservaflon are found to be In
compliance with EPA recommendaWn.
w000ns: VOA, oollfamm TOG, 640, WI-0RO �r
�v es ❑No
-- .lam pNo
©Yes ❑No
faNIA 13.
OWA
Inifiei whw oDm feted .
$am fes checked for dechiorination:
pies Oleo
IINIA 14.
Pleads cs In VOA Vfais >Smm :..
DYes ❑No
016 16.
Trip Flank Present:
Trip Blank Custody Seals Present
-Peas TO Blank Lot #f iY purchased),
©Yea 12No
Dyes DNo
18.
E I m
Client Notlflaation! Resolution: Fleld•Data Required?
Person Contacted: batelTime: .
Commentsf Resolutlon:--
SCURF ReVIeW: �q Date: ' Place label here
SRF Review: Date: % 3 OR
Not% Whensver the VWOU86rropanoy affecting forth CaWr4fni oo pffanoe
samples, a copy this form will be sent to the Norlh CaroMa DEHNR number
num project Handwrite proj
Certiffoaifon Offloe (I.e out of hold, Incorrect preservaft out of tomp, Han
Inoorreot oontalners) _ — - ( no label ect num
_ )
Y 1 N
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