WQ0006984_Residual Annual Report 2018_20190315

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0006984
SUBMITTAL DATED: 2/28/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Lisa Finnerty
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0006984
Permittee * South Fork Industries
Facility Name * South Fork Industries
Phone Number*
4434899086
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2018 Annual Report for South Fork Industries
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
South Fork NC 2018 Annual Report.pdf 7.52MB
upload only 1 RDF docurrent. NLltiple documents must be corrbined into one RDF file.

For nein and modif cation permit applications, the paper copy is required to be submitted to the
Di, risiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ging:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,vision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942M
512 N_ Salisbury St_ Raleigh, NC 27644
For questions or problems contact Tessa Monday at: 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
*140 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/28/2019

435 Williams Court, Suite 100
Baitinorc, 1VID 21220
Nv ww synagrn. com
FEBRUARY 27, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2018 Annual Report for Permit No. WQ0006984
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of South Fork Industries, NC.
If you have any questions or comments, please contact Everette Owens at 828-428-9921 or Erik
Bruce at [phone].
Sincerely,
7
Derrick Shivar
Environinental Compliance Manager
Enclosures
cc: Everette Owens, South Fork Industries
Erik Bruce, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

SOUTH FORK INDUSTRIES, INC., NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006984
2018 ANNUAL REPORT

South Fork Industries, Inc., NC
Residuals Land Application Program
201E Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen Reduction/Vector Attraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: W00006984 County Catawba Year 2018
Facility Name (as shown on permit) South Fork Industries NPDES No. NC0006190
Land Application Operator Svnawo Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Application Summary:
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 123.12
Total number of acres utilized for land application during the year: 49_70
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil PIT of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T. I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
IL Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No ranoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Everette Owens, Plant Manager G��Gif' Z� !
Permittee Name and Title (type or print) Sr�'gnatwe ofPe i D
Signature ofPreparer* Date Signatt of Land AppliV Date
if different from Permittee) (if different from Perruittee and Preparer)
*Prepazer is defined in 40 CFR Part
503.9(r) and ISA NCAC 02T ,1102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
SOUTH FORK INDUSTRIES, INC., NC
SOUTH FORK INDUSTRIES, INC., NC MAIDEN PLANT TEXTILE RESID. LIQUID
DRY METRIC
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT TONS
September 2018 1,004,400.00 G 123.12 D 111.68
YEARLY TOTAL 110047400.00 G 123.12 D 111.68
1 /28/2019

SECTION 2

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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2105-01-TXLIQ-NC
SOUTH FORK INDUSTRIES, INC.,
MAIDEN PLANT TEXTILE RESID,
NC
LIQUID
1/12/2018
1/112018-12/3112018
4.6597
Na mg/I = (Na mg/kg x %Solids) + 100 = (7410 x 2.9400) :100 = 217.854
Ca mg/I = (Ca mg/kg x %Solids) + 100 = (4240 x 2.9400) - 100 = 124.656
Mg mg/I = (mg mg/kg x %Solids) + 100 = (829 x 2.9400) = 100 = 24.3726
Na meq = Na mg/I + Molec.Wgt.Na = 217.854 + 23 = 9.47191
Ca meq = Ca mg/I + Molec.Wgt.Ca = 124.656 + 20 = 6.2328
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 24.3726 + 12 = 2.03105
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 9.47191 + SgrRoot[0.5(6.2328+2.03105)] = 4.65974
Printed: 2/11/2019
Page 1 09:06

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SUAINKIT
"AfIRON MENTAL rECHNOLOGIE5, INC
ldnaf yA+ca! Labarelot'7r.G
February O15 2018
Erik Bruce
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
SunanifiTint7romnental Technologies, Inc.
3310 Win St.
Cayahoga Falls, Ohio 44223
TeL: [phone] FAX: [phone]
Website: haw/huwm settekcom
RE: South Fork Industries
Dear Erik Bruce: Order No.: 18010751
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/17/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you haveany questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Proj eat Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, Californ
ia 07256CA, Colorado, Colmccficut PH -0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, lllinois
200061, Ivdiana C -OH -l3, Kaysas E-10347, Kentucky (Uvdergrowrd Storage Tauk) 3, KenNcky 90146, Louisia,ra 04061, Maryland 339, Mivvesota
409711, New Aampsldre 2996, Naw Jersey OH006, New Ydrk l 1777, NoM Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH200001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OB009232011-1, Virghua VLLAP 9456, Washington
C891
Page 1 of 26

SUMMIT
Summit Environmental Techno,ogres, Inc.ffl Case Narrative
3310 Win St.
rNVIRONMENTAL MCHNOLOGIES, INC- Ciryahoga Falls, Ohio 44223 w0#: 18010751
Anaty6'oaf Lahoosiorles TEL: [phone] FAX: [phone]
Website: htto:/Amviy.settekcom Date: 2/1/2018
CLIENT: Synagro
Project: South Fork Industries
WorkOrder Narrative:
18010751: This report in its entirety consists of the following docmnents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc, and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples
are reported
on an
"as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry"
designation
on the
reporting units.
This report is
believed
to meet all of the requirements of the
accrediting agency,
where applicable: Any
comments or
problems
with the analytical events associated
with this report are
noted below.
Analytical Sequence QC Notes:
18010751-OOlAMS SVOC-BNA_TCLP(8270): MS exhibited low recovery for Pyridine. Pyridine is a
known poor performer.
18010751-001AMSD SVOC-BNA_TCLP(8270): MSD exhibited low recovery for Pyridine. Pyridine is
a known poor performer.
Original
Page 2 of 26

U INt Sunimil.Environmental Technologies, In Qualifiers and Acronyms
3310 Win 8
FUVIRONMENTdL IECm10LO0IE5, MC. - Cuyahoga Falls, Ohio 4422 WO#: 18010751
Analgfi^al L$Fron, lodes TEL: [phone] FAX. [phone]
Website: han.lApnrvserrekco Date: 2/1/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U
The compound was analyzed for but was not detected.
J
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
I
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution.
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m
Manual integration was used to determine the area response.
d
Manual integration in which peak was deleted
N
The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GC/MS.
X
The result was not confirmed when GC/MS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCB contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low (-) or high (+).
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Pleaserefer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method. Detection Limit
MB
Method Blank LOD Level of Detection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Lfinit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD
Relative Percent Different M MCL Minimum Compound Limit
ICV
Initial Calibration Verification RA Reanalysis
ICB
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCR
Continuing Calibration Blank RT Retention Time
RLC
Reporting Limit Check CF Calibration Factor
DF
Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in tltis
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 26

ffISUMM101
Summit Enviromnentol Technologies, Inc. WOrkorder
3370 Win St.
FNVIRONNIENTAL IECHNOLOGIES, 1NG Cuyahoga Falls, Ohio 44223 Sample Summary
A.nalyfFcal taboratorles TEL: [phone] FAX. [phone] WO#: 180107.51
Website.: ht1v7111ovtvseaek.com 01-Feb-18
CLIENT: Synagro
Project: South Fork Industries
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
18010751-001 South Fork Industries 1/12/2018 11:00:00 AM 1/17/2018 2:00:00 PM Sludge
Page 4 of 26

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NyMMIT Summit Environmental Technologies, Inc.ffIAna lytlCalRepOrt
3310 Win St.
rNVIRONMIENTA.L IECW40LOcoE8, INC. Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laharalorms TEL: [phone] FAX: [phone] WO#: 18010751
Website: h1W_1Avunn.settek.eom Date Reported: 2/1/2018
CLIENTS
Synagro
Matrix:
SLUDGE
Lab ID:
18010751-OOIA
Project:
South Fork Industries
Client Sample
ID South Fork Industries
Tag Number:
Collection Date: 1/12/2018 11:00:00 AM
Analyses
Result
RI. Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA,
PEST, HERB -SOLID
SW7470A
SW7470A Analyst:
EAM
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND
0.00200
nI
1
1/23120182:17:00
PM
TCLP METALS, VOC, BNA,
PEST, HERB -SOLID
SW6010D
SW301OA Analyst:
KMS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsentc(As)
ND
0.500
mg/L
1
1/23/2018 8:36:26
PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
1/23/2018 8:36:26
PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
1/23/2018 8:36:26
PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
1/23/2018 8:36:26
PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
1/23/2018 8:36:26
PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
1/23/2018 8:36:26
PM
TCLP Silver(Ag)
ND
0.500
mg1L
1
1/23/2018 8:36:26
PM
TCLP METALS, VOC, BNA,
PEST, HERB -SOLID
SW8270D
SW361OC Analyst:
BJH
TCLP SEMI -VOLATILES ANALYSIS (SW131118270)
1,4 -Dichlorobenzene
ND
0.0800
mg/L
2
1/24/2018 6:58:00
PM
2,4,5 -Trichlorophenol
ND
0.200
mg/L
2
1/24/2018 6:58:00
PM
2,4,6 -Trichlorophenol
ND
0.200
mg1L
2
1/24/20186:58:00
PM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2
1/24/2018 6:58:00
PM
o -Cresol
ND
0.200
mg/L
2
1/24/2018 6:58:00
PM
m/p-Cresol(s)
ND
0.200
mg/L
2
1/24/2018 6:58:00
PM
Cresols, Total
ND
4.00
nI
2
1/24/2018 6:58:00
PM
Hexachloro-1,3-butadiene
ND
0.0160
mg/L
2
1/24/2018 6:58:00
PM
Hexachlorobenzene
ND
0.0400
mg/L.
2
1/24120186:58:00
PM
Hexachloroethane
ND
0.0800
mg/L
2
1/24/2018 6:58:00
PM
Nitrobenzene
ND
0.0800
mg/L
2
1/24/2018 6:58:00
PM
Pentachlorophenol
ND
0.200
mg/L
2
1/24/2018 6:58:00
PM
Pyridine
ND
0.200
mg/L
2
1/24/2018 6:58:00
PM
Surr: 2-Fluorophenol
41.5
10-109
%Rec
2
1/24/2018 6:58:00
PM
Surr: Phenol -d6
20.4
10-109
%Rec
2
1/24/2018 6:58:00
PM
Surr: Nitrobenzene -d5
78.6
19-120
%Rec
2
1/24/2018 6:58:00
PM
Surr: 2,4,6-Tribromophenol
52.3
10-120
%Rec
2
1/2412018 6:58:00
PM
Surr 2-Fluorobiphenyl
71.5
22-117
%Rec
2
1/24/2018 6:58:00
PM
Qualifiers: ' Value exceeds Maximum Contaminant Level.
H
E Value above quantitationrange
Holding times for preparation or analysis exceeded M Manual Integration d to determine
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
usearea response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL permit Limit Original
RL Reporting Detection Limit
Page 6 of 26

RISUMMIT
Summit Environmental Technologies,. Analytical Report
33/00Win in StSt.
FMVIRONMENTAL IRCHNOLOCIes, 1NC Cuyahoga Falls, Ohio 44223 (basereport)
Analytical tahnratonee TEL: [phone] FAY [phone] WO#: 18010751
Website: hoo 11 nuiv seltekeom Date Reported: 2/1/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/12/201811:00:00 AM
Lab ID: 18010751-OOIA
Project: South Fork Industries
Client Sample ID South Fork Industries
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270D SW351OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
Surr: p-Terphenyl-114 80.3 34-116 %Rec 2 1/24/2018 6:58:00 PM
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081 Analyst: JBN
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND 0.0100 mg/L 1 1/26/2018 3:44:00 PM
Toxaphene ND 0.0200 mg/L 1 1/26/2018 3:44:00 PM
Endrin ND 0.00100 mg1L 1 1/26/2018 3:44:00 PM
gamma-BHC ND 0.00100 mg/L 1 1/26/2018 3:44:00 PM
Heptachlor ND 0.00100 d mg/L 1 1/26/2018 3:44:00 PM
Heptachlor epoxide ND 0.00100 mg/L 1 1/26/20183:44:00 PM
Methoxychlor ND 0.00100 mg/L 1 1/26/2018 3:44:00 PM
Surr. TCMX 72.9 10-119 %Rec 1 1/26/2018 3:44:00 PM
Surr: DCB 73.3 10-119 %Rec 1 1/26/2018 3:44:00 PM
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8151A SW8151A Analyst: JBN
TCLP HERBICIDES ANALYSIS (SW131118151)
214-D ND 1.00 mg/L 1 1/26/2018 11:43:00 PM
2,4,5-TP ND 0.500 d mg/L 1 1/26/2018 11:43:00 PM
Surr: DCAA 77.1 20-140 %Rec 1 1/26/2018 11:43:00 PM
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8260B SW1311 M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.0500 mg/L 10 1/24/2018 6:57:00 PM
1,2-Dichloroethane ND 0.0500 mg/L 10 1/24/2018 6:57:00 PM
MEK ND 0.250 mg/L 10 1/24/20186:57:00 PM
Benzene ND 0.0500 mg/L 10 1/24/20186:57:00 PM
Carbon tetrachloride ND 0.0500 mg/L 10 1/24/2018 6:57:00 PM
Chlorobenzene ND 0.0500 mg/L 10 1/24/2018 6:57:00 PM
Chloroform ND 0.0500 mg/L 10 1/24/2018 6:57:00 PM
Tetrachloroethene ND 0.0500 mg/L 10 1/24/2018 6:57:00 PM
Trichloroethene ND 0.0500 mg/L 10 1/24/20186:57:00 PM
Vinyl chloride ND 0.0200 mg/L 10 1/24/2018 6:57:00 PM
Qualifiers: * E Value above quantitation range
Value exceeds Maximum Contaminant Level.
H
Holding times £or prepazation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Liini[.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
N Tentatively pounds
O RSD is greater than RSDlimit
pL permit L nut Original
RL Reporting Detection Limit
Page 7 of 26

summiliff Summit Environmental Tehno/WinSInc. Analytical Report
33/010Win St:
rNVIRONMEWAL 1EC8t10L0GrES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical LabaratoYJes TEL: [phone]// FAX: [phone] w0#: 18010751
Website: htto://unvw.settek.c°m Date Reported: 2/1/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/12/2018 11:00:00 AM
Lab ID: 18010751-OOIA
Project: South Fork Industries
Client Sample ID South Fork Industries
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
Not Detected
SW8260B
SW1311M
Analyst: CTB
TCLP VOLATILES ANALYSIS
Surr: 4-Bromofluorobenzene
92.7
70-130
%Rec
10
1/24/2018 6:57:00 PM
Surr: Dibromofluoromethane
107
70-130
%Rec
10
1/24/20186:57:00 PM
Surr: Toluene -d8
94.5
70-130
% Rec
10
1/24/2018 6:57:00 PM
RCI -SOLID -W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2) -SOLID
Cyanide, Reactive
ND
0.500
mg/Kg
1
1/24/2018 11:28:00 AM
RCI -SOLID -W/ IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW -846:1030)
Ignitability
non-flammable
1
1/25/2018 1:00:00 PM
RCI -SOLID -W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH
7.4
s.u.@20.4C
1
1/23/2018 1:53:00 PM
RCI-SOLID-Wl IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive
30.0
25.0
mg/Kg
1
1/24/2018 11:28:00 AM
Qualifiers: °
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentadvely identifietl compounds
O RSD is greater than RSDlimit
PL
permit Limit Original
RL Reporting Detection Limit
Page 8 of 26

s V i� SummitEnvionmentalTechnologies, Inc. Aeereditatilon Program
ffl 3310 Win St. Analytes Report
r,f4VIRONh9ENTAL TECHNOLOGIES, We Cayohoga Falls, Ohio 44223 y p
Arralyticat Laboratories TEL: [phone] FLY: [phone] WO#: 18010751
Website: hay:/Arww.settekco»a 01-Feh-18
Client: Synagro State: NW
Project: South Fork Industries Program Name: NC—WW—SCM
Sample ID Matrix
Test Name
Analyte
Status
18010751-OOIA Sludge
Ignitability of Solids (SW -846: 1030)
ignitability
A
Sludge
PH(SW9045D)
Hydrogen Ion(pH)
A
Sludge
Reactive Cyanide (9014/7.33.2) -Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis(SW1311/8151)
2,435 -TP
A
Sludge
TCLP Herbicides Analysis(SW1311/8151)
2,4-D
A
Sludge
TCLP Herbicides Analysis(SW1311/8151)
DCAA
A
Sludge
TCLP Mercury Analysis(SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SWI
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW131 1/8081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SWI 311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SWI 311/8081)
gamma -BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Tetrachloro-m-xylene.
A
Sludge
TCLP Pesticides Analysis (SWI 31 l/8081)
Toxaphene
A
Sludge
TCLP Semi -Volatiles Analysis (SW1311/8270)
1,4 -Dichlorobenzene
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,5 -'Trichlorophenol
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,6-Tribronophenol
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,6 -Trichlorophenol
A
Sludge
TCLP Semi -Volatiles Analysis(SWI 311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2-Fluorobiphenyl
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2-Fluorophenol
A
Key
Key
NC WW SCM A Accredited
NC WW SCM U Unavailable
Original #I
Page 9 of 26

U IT summit Environmental Technologies, Inc. Accreditation Program
3310 Win St: Analytes Report
rNVIRONh1ENTAL 12CHNOLOCIES, INC Cuyahoga Falls, Ohio 44223 Y C
Anafyticsl Gshw'stuYtes TEL: [phone] FAX: [phone] WO#: 18010751
Website: hay.1Aww.settek.corn 01 -Feb -18
Client: Synagro State: NW
Project: South Fork Industries Program Name: NC—WW—SCM
Sample ID Matrix Test Name Analyte Status
18010751-OOIA Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2-Methylphenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 3,4-Methylphenol A
Sludge TCLP SemiNolatiles Analysis (SW1311/8270) Cresols, Total A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi -Volatiles Analysis (SW1 311/8270) Hexachlorobutadiene A
Sludge TCLP SemiNolatiles Analysis (SW1311/8270) Hexachloroethane A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Nitrobenzene A
Sludge TCLPSemi-VolatilesAnalysis(SW1311/8270) Nitrobenzene -d5 A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Phenol -d6 A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) p-Terphenyl-dl4 A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Diehloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis 4-Bromofluorobenzene A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Dibromofluoromethane A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis ToluesI A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
NC_WW_8CM A Accredited NC_WW_SCM U Unavailable
Original #I
Page 10 of 26

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SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: South Fork Industries WQ Permit Number: WQ 00006984
WWTP Name: South Fork Industries NPDES Number: NC0006190
Monitoring Period: From 01/01/2018 To 12/31/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Vector Attraction Reduction
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
MPN
<557
<716
<885
MPN/g
0
Annual
Grab
Sm9221C
Coliform
power per gram
E
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
(40 CFR 503.33/15A NCAC 021.1107) -Please Indicate option/alternative performed:
Option/Alt. 1 Opfion/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40 -day bench) (30 -day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
CERTIFICATION STATEMENT (please check the appropriate statemenk)
Option/AIL. 7 Option/Alt. 8
No vector attraction reduction alternatives were performed X
"I certify, under penalty of law, that the pathogenic uirements in 40 CFR 503.32/ISA NCAC 021.1106 and She vector athaction
X reduction requirement in 40 CFR 503.33/15A NCAC 02`C.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 021.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have
been met. I am awaze that there are significant penalties for false certification including fine and imprisonment:"
Everette Owens, Plant Man
ager
Pre ser Name and TjY e (type or print)
C 2.zz-t9
Land Applies Name and Title (if applicable) (type or print)
Signature reparer* Date
nature
of Land Applies (if applicable)
*Prepares is defined in 40 CFR Fait 503.9(r) and 15A NCAC 21.1102 (26)
Date

Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 02/06/2018
Reported: 02/08/2018
For: South Fork Ind
Comments: Geometric Mean <716 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
180206-28-01
Fecal Coliforms
SH
<735
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-01
Percent Solids
SF1
2.72
%
SM25408-1997
02/06/2018
WC
180206-28-02
Fecal Coliforms
SF2
<885
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-02
Percent Solids
SF2
2.26
%
SM25406-1997
02/06/2018
WC
180206-28-03
Fecal Coliforms
SF3
<557
MPN/g
sM9221cE-2aoe
02/07/2018
WC
180206-28-03
Percent Solids
SF3
3.59
/
SM2540e-1997
02/06/2018
WC
180206-28-D4
Fecal Coliforms
SF4
<660
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-04
Percent Solids
SF4
3.03
%
SM25406-1997
02/06/2018
WC
180206.28-05
Fecal Coliforms
SF5
<851
MPN/g
SMS2210E-2006
02/07/2018
WC
180206-28-05
Percent Solids
SF5
2.35
/
SM25406-1997
02/06/2018
WC
180206-28-06
Fecal Coliforms
SF6
<676
MPN/g
SM92210E-2006
02/07/2018
WC
180206-28-06
Percent Solids
SF6
2.96
/
SM254 B-1997
02/06/2018
WC
180206-28-07
Fecal Coliforms
SF7
<704
MPN/g
SM9221GE-2006
02/07/2018
WC
180206-28-07
Percent Solids
SF7
2.84
/
SM25406-1997
02106/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 •Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-02 Temp on Arrival: 5.4
Parameter Schedule: Percent Sotids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 18020
6-28-03 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Cpliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-04 Temp on
Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-05 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 •Statesville, NC 28687 • 704/872/4697
Page 2 of 4
Condition
of
Receipt
Sample Number 180206-28-01
Temp on Arrival:
5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-02 Temp on Arrival: 5.4
Parameter Schedule: Percent Sotids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 18020
6-28-03 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Cpliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-04 Temp on
Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-05 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 •Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-06 Temp on Arrival: 5.4
Parameter Schedule: PercenfSolids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180206-28-07 Temp on Arrival: 5.4
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 •Statesville, NC 28687 • 704j872J4697
Page 3 of 4

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SECTION 6

Agricultural Lime Application Log
Year: 2018
Project: South Fork Industries
Field
(state -county -site -field)
Soil
pH
(from
Lime Requirement
soil analysis)
TonslAcre
Applied(CCE Eq.)
Date Applied
CA -06-01
7.3
O.OT/Ac.
CA -06-02
5.6
1.OT/Ac.
CA -06-03
5.7
1.OT/Ac,
O.OT/Ac.
O.OT/Ac.
*Lime will be applied when conditions improve.

SECTION 7

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