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HomeMy WebLinkAboutWQ0004825_Residual Annual Report 2018_20190314INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0004825 SUBMITTAL DATED: 2/26/2019 Project Contact Information Hease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Lisa Finnerty Email Address* Ifinnerty@synagro.com Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0004825 Permittee * Facility Name * City of Randleman City of Randleman Phone Number* 4434899086 r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Hans, Specifications, Calculations, Etc.) Randleman NC 2018 Annual Report.pdf 10.66MB l pload only 1 FDF document. ivtaltiple docurrents must be combined into one FDF file. For nein and modif cation permit applications, the paper copy is required to be submitted to the Di, risiom Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follm ging: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extras set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) This shall be mailed to the following address: By US_ Postal Service- Di,vision of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 27699-1617 By Courier, -Special Delivery: Division of Water Resources- Non -Discharge Branch Nathaniel Thornburg- 9th Floor, Office #942M 512 N_ Salisbury St_ Raleigh, NC 27644 For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov. *140 By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/26/2019 435 \Vilhams Court, Suite 100 Bahiinore, NTD 21220 www..synagro.com FEBRUARY 26, 2019 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2018 Annual Report for Permit No. WQ0004825 Dear NCDEQ: SYNAGRO Synagro is submitting one copy and one electronic copy of the above referenced report on behalf of the City of Randleman, NC. If you have any questions or need additional information, please do not hesitate to contact Nick Holcomb at (336) 495-7500 or Nate Roth at (336) 403-4324. Sincerely, r Derrick Shivar Environmental Compliance Manager Enclosures cc: Nick Holcomb, City of Randleman Nate Roth, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD CITY OF RANDLEMAN, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0004825 2018 ANNUAL REPORT City of Randleman, NC Residuals Land Application Program 2018 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms &Metals Field Loading Summary Forms 4. TCLP Analysis 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH &Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM VQ Permit #: WO0004825 County Randolph Year 2018 Facility Name (as shown on permit) City of Randleman W WTP NPDES No. NC0025445 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A—Residuals Application Summary: Total number of application fields in the permit: 16 Total number of fields utilized for land application during the year: 4 Total amount of dry tons applied during the year for all application sites: 136.46 Total number of acres utilized for land application during the year: 74 Part B —Annual Compliance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. I. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality, 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11, Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." //, L� �I� Michael Glass, Plant Superintendent a��"`�r�i /" 2"12 t I Permittee Name and Title (type or print) Signaturetlf PerA11A n _ �Da Signature oPPreparer* Date Signa of Land ApplilU/ Date (if different from Permittee) (ifdifferentftbm ermitteeandPrepazer) *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 02T.1102 (26) DENR FORM ACF (12/2006) 2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC RANDLEMAN,NC RANDLEMAN, NC RANDLEMAN WWTP LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS April 2018 192,200.00 G 36.47 D 33.07 June 2018 266,600.00 G 50.58 D 45.88 August 2018 260,400.00 G 49.41 D 44.81 YEARLY TOTAL 7192200.00 G 136.46 D 123.76 1 /28/2019 SECTION 2 5\ , ` e , , \} } a _ : / \\\_\ ] \ ° # £ / EE kE ) /fes § : }\�\� /��\ LLI +\/\E,�zE \ 0\ !£)�2 -0 $§7 „ &�#4�ff�[; J23Ga <o:00l:2$,eK<z i 19 N z J C� G U) Q 0 U) W J z a �1 a a m in Q 0 Q V V o W n W rn �i � Z K R Q a C O Vl Y •N o Of 7 E O N d C m U) 7 Z R N Q N p a W Z«�4t�� E Eur LL' E E E E•vp?� mLI woc cEN '�E NRa N'=O NdU �EU� d LL Z O d m m m Q 2 m= 0 0 zz , \ Of !§m f {m\ 0 'E0 kj) ( k� \{{\/\)§«£_F_F 0 ) ƒ)2 m 1212 < $ m(§ >/\ §7] 444\Q 0 !§| , IT /® 3 »_ !r! #` #!! ;ef2yF>9W7 \IL °E EBi % ) 0) CA-= iB \\\\4\444\ ) f \Ei ;\\\\\)kk\ % (/ \ % a �j § L6 L6 \ { - L § 0 \\ k o \()§)\) \) \ \ \\ � f \ - > ) / / IEA : k - )\ 2 2 \ « :� �C) . 0 - �` CO {/\ : \ i � ( E\\) It � § � C)C) < ƒ \ \ a )) / ƒ\] n eeeeee:G/\(\ O w IL y n. �En O 0; Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2027 -01 -LIQ -NC RANDLEMAN, NC RANDLEMAN WWTP 4/13/2018 1/1/2018-12/31/2018 0.2054 LIQUID Na mg/i = (Na mg/kg x %Solids) :100 = (1300 x 4.5500) - 100 = 59.15 Ca mg/I = (Ca mg/kg x %Solids) + 100 = (132000 x 4.5500) + 100 = 6006 Mg mg/I = (mg mg/kg x %Solids) + 100 = (3510 x 4.5500) + 100 = 159.705 Na meq = Na mg/I - Molec.Wgt.Na = 59.15 = 23 = 2.57174 Ca meq = Ca mg/I - MoleaWgt.Ca = 6006 + 20 = 300.3 Mg meq = Mg mg/I - Molec.Wgt.Mg = 159.705 - 12 = 13.3088 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.57174 = SgrRoot[0.5(300.3+13.3088)] = 0.205375 Printed: 2/7/2019 Page 1 11:13 I ej U a R a ¢g 3 W W W N A ej U R a W W W N W W W � � z zU z �i o v a � C W u pT � c a O U U � W � v N � w0 vFi U ej U a W W W N W W W zU z �i o v a � C c u w c U 9 9 � v N � p U za Q a p 9 z Q a a a U a g ro O fi v _� o0 N N N 0.ry P. P. qaA �o� QUA x 9 a C <F U 6 tj n V e h O C �y6 0 � 0 rn N Q a a v, N Ln z �i o x � C c u w c U � v N � p U za Q a p 9 Q U a g ro O fi v Ln o _ � C c u � N � p za Q a p 9 Q ANNUAL METALS FIELD LOADING SUNIMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Randleman, NC Total Dry Tons Applied (Annual): Permit #: W00004825 Cation Exchange Capacity (non 503 only): 49.41 Operator: W. Howard Fields Owner: W. Howard Fields Predominant Soil Series: Coronica Acres Used: 16 Acres Permitted: 16 Site #: NC RD 00018 Field #: RD 00018 0003. 10 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 4/13/18 2 3 4 5 6 7 8 9 10 11 12 %Solids 4.55 8 9 10 11 12 Arsenic 3 Cadmium 2 H Copper 143 Chromi 47 � Lead 15.5 Mercury 0.4 A'+ y Molyb- denum 5 Nickel 12.3 Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 147 0.000 0.000 0.000 0.000 0.000 0.019 Total Phos- horus 6380 0.000 0.000 0.000 0.000 0.000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): TOYal 1 2 3 4 5 6 7 8 9 10 11 12 H DT/AC./ � APP A'+ y Event 3.09 Arsenic 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Cadmimn 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Copper 0.883 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.883 Chromi 0.290 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.290 Lead 0.096 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.096 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 denum Nickel 0.076 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.076 Selenium 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 Zinc 0.908 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.908 Total Phos- 39.403 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 39.403 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that quali£ted personnel properlygathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of £nes and imprisonment for knowing violations". �� ,� 2 �� 9 Signature of Land Applier Date DENR FORM MFLSF (12/2006) I k U a U F N pWp W W W .7 V o E C) °aC' A �3a k U z U F N pWp W W W .7 V o E C) °aC' �3a o � z w � Fw0 a k z F W W W V o E W O � z � a VIM -V CD Q� nn a0 o W z u C) N� 0. z� m V m .N. U C y C k F W W W V W W W z VIM -V CD nn o a U N� 0. z� m V m .N. U C y C b w v a lz Q € i' U a C tj o S' 3 U Ig 73 7 r O r N N VIP inUq C qFa o U � C7 C7 C7 C7 0 0 0 �H � e H NVa s 03 o M m a k F N z O CD nn o a U 0. m V m .N. U C b w v a Q € i' U a tj o S' 3 U k O a U m .a C w a Q € k ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Randleman, NC Total Dry Tons Applied (Annual): W00004825 Cafion Exchange Capacity (non 503 only): Roy Holder Owner: Roy Holder Predominant Soil Series: 28.5 Acres Permitted: 28.5 Site #: NC RD 00019 Field #: RD 00019 0001 36.47 Cecil Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample Or Com- posite Date 1 4/13/18 2 3 4 5 6 7 8 9 10 11 12 %Solids 4,55 8 9 10 11 12 Arsenic 3 Cadmium 2 Copper 143 Chromiu 47 C Lead 15.5 Mercury 0.4 t� Molyb- denum 5 Nickel 12.3 Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 147 0.000 0.000 0.000 0.000 0.000 0.008 Total Phos- horns 6380 0.000 0.000 0.000 0.000 0.000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/AC./ C App. t� Event 1.28 Arsenic 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Cadmium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0:366 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.366 Chromi 0.120 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.120 Lead 0.040 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.040 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 denum Nickel 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 Selenium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Zinc 0.376 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.376 Total Phos- 16.333 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 16:333 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that quahfied personnel properly gathered and evaluated the information snbmitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) :a 3 3 z Q led a a L) .7 w a U U Q E La oo W z W N A w :a 3 3 z Q led z L) .7 w a U U Q Ox La oo W z W N w w w �3a p w' z(j � dO w a 4 wwo :a 3 3 z Q led z L) .7 w U U U N W z W N w w w p z(j � z a 4 w Q 0 p o w � a a n o U a 2 H c4 v a r N Q U 0 w `v n d n :a 3 3 z Q led L) .7 w U U U N W W W N w w w z(j z 4 Q 0 vCY x � a a n U a a v a r N z� 0 `v n d n 2 c w '' U Qw a a n z F U � 7 c c o 0 c6 i - 19 o0 Swa. v�UQ cC v a v � U U c7 c7 C7 �o a w Q� :a 3 3 z Q led w N N z 0 vCY x � a U a a a kn 0 `v U w '' U Qw U � 7 :a 3 3 z Q led vCY � a U a w '' ro Qw ^u ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Randleman, NC W00004825 Rov Holder Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Owner: Roy Holder Predominant Soil Series: 24.70 Appling 11.4 Acres Permitted: 11.4 Site #: NC RD 00019 Field #: RD 00019 0002 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #�: Sample or Com- posite Date 1 4/13/18 2 3 4 5 6 7 8 9 10 11 12 ro solids 4.ss B 9 10 11 12 Arsenic 3 Cadmium 2 Copper 143 Chromi 47 o Lead 15.5 Mercury 0.4 Molyb- denum 5 Nickel 12.3 Selenium s 0.000 0.000 0.000 0.000 0.000 Zinc I47 0,000 0.000 0.000 0.000 0.000 0.013 Total Phos- horns 6380 0.000 0.000 0.000 0.000 0.000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 B 9 10 11 12 DT/Ac./ o APP Event 2.17 Arsenic 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.013 Cadmium 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Copper 0.620 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.620 Chromi 0.204 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.204 Lead 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 denum Nickel 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Selenium 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Zinc 0.637 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.637 Total Phos- 27.6s1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 27.651 horns "I ceetify, nnder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". %�i 11 /9 Signature of Land Applier Date DENR FORM MFLSF (12/2006) I d W 'a U e 0 w U v O R C v WU Ww G � z Q d W U e 0 w U v O R C v WU Ww G � z �HH �o N a aw. O e 0 w U R C v WU Ww G � z N z v Oq T C x A� E o � w a � N U � z� o ox a � � U < ao 12 N N c o o U au y e w U R C v WU Ww G N z v Oq T C x b E � a � N U z� a a � U < ao 12 N N c o o U au y a ¢z � E e a a a € Q e o w v o� S 49 - � o H � � o Q o � a Q u L a a N r gry x o o � .y o w: z Q o A A vUq O ai a a a � � AEP. u � g a v 3� o U � � 6 qc B U � C7 C7 C7 � � o• W °, a !E3 z x z9 e w R C N G N z v Oq T C x b E a C U a a a � U < ao 12 N N c o U y a � E a € Q e o w v o� S 49 - � o H � � E G N Oq T C b E a C U a � c 3 12 S c o v; y a � E a € Q e E G N Oq T C E a 0.� � c 3 12 c o v; 0 a E � e o w o� S 49 - a a a x o o � .y o w: Q O ai a � � u g 3� o � qc B � � o• W °, a !E3 z x z9 a a . z¢ z, ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Randleman, NC Total Dry Tons Applied (Annual): 25.88 Permit #: W00004825 Cation Exchange Capacity (non 503 only): Operator: Roy Holder Owner: Roy Holder Predominant Soil Series: Cecil Acres Used: 18,1 Acres Permitted: 18.1 Site #: NC RD 00019 Field #: RD 00019 0003 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 4/13/18 2 3 4 5 6 7 8 9 10 11 12 Solids 4.55 8 9 10 11 12 Arsenic 3 Cadmium 2 y Copper 143 Chromi 47 Lead 15.5 Mercury 0.4 w Molyb- denum 5 Nickel 12.3 �� Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 147 0.000 0.000 0.000 0:000 0.000 0.009 Total Phos- horns 6380 0.000 0.000 0.000 0.000 0.000 AnnualHeavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 y DT/Ac./ App. w Event 1.43 �� Arsenic 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.009 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 0.409 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.409 Chromi 0.134 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.134 Lead 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 denum Nickel 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Selenium 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Zinc 0.420 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.420 Total Phos- 18.247 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 18.247 horus "I cerfify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ti�� Signature of Land Applier �� Date DENR FORM MFLSF (12/2006) SECTION 4 TONUMMIT "AYIRONFAENTPL rEC4NOLOGIES, `NC Analytical Laboizionpri February 28, 2018 Clay Fisackerly Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Randleman Dear Clay Fisackerly: Summit Enriromsenta Technologies, lric. 3310 Win St. Cuyahoga Fails, Ohio 44223 TEL (330) 253-8211 FAX. (330) 253-4489 Website: hay.Owwta settek com Order No.: 18011441 Summit Environmental Technologies, Inc. received 1 samples) on 1/30/2018 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative, Quality control data is within laboratory defined ox method specified acceptance. limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, Califomie 07256CA, Colorado, Connecticut PH-OIO$ Delaware, Florida NELAC E87G88, Georgia E87688, Idaho OH00923, Nivois 20006 1, Indiana C -OH -13, Kansas E-10347, Kentucky (Undergromd Stooge Tank) 3, KenNeky 90146, Louisiana 040fi1, Maryland 339, Minnesota 409711, New Hazupshire299G, New ]ersey OH006, New York 11777, North Carolina 39705 aad 631, NoAr Dakota 2-201, Oklahoma 9940, Oregon O112O0001, Rhode Island LA000317, South CzroFna 92016001, Texas T104704466-11-5, Utalr OH009232011-1, Virginia VELAP 9456, Washington C891 Page 1 of 27 S u Alm � e� Sun"'lil Environmental Technologies, Inc. Case Narrative 3310 Win St. rNVIRONMENTA.L 4£CW40i.00125, INC- Cuyahoga Falls, Ohio 44223 WD#: 18011441 Rnefyticn7 Lahoue3ul7e5 TEL: (330) 253-8211 FAX.' (330) 253-4489 W bsite: hila.,/fwww seUekcan Date; 2 /2 812 01 8 CLIENT: Synagro Project: Randleman WorkOrder Narrative: 18011441: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc, or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples This report is believed to meet all of the requirements F4% are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. noted below. Analytical Sequence Sample Notes: 18011441-OOlA SVOC-BNA_TCLP(8270D): Sample exhibited high surrogate recovery, Sample was ND for all analytes of interest. Analytical Sequence QC Notes: ccv 40ng S8- svoc-mstr_s(8270): The BNA 8270 CCV (Batch R60867) exhibited high recovery for Pyridine; Associated samples are ND for Pyridine. Original Page 2 of 27 accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 18011441-OOlA SVOC-BNA_TCLP(8270D): Sample exhibited high surrogate recovery, Sample was ND for all analytes of interest. Analytical Sequence QC Notes: ccv 40ng S8- svoc-mstr_s(8270): The BNA 8270 CCV (Batch R60867) exhibited high recovery for Pyridine; Associated samples are ND for Pyridine. Original Page 2 of 27 SUMMIT Sunmilt Environmental Technologies, In Qualifiers and Acronyms RI3310 Win 5 FNVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 442 WO#: 18011441 Analytical Laboralorlas TEL: (330) 253-8211 FAX: (330) 253-446 Website: hero:/hvivw.seuekco Date: 2/28/2018 These commonly used Qualifiers and Acronyms may or may not be present in this report Qualifiers U This list of Qualifiers and Acronyms reflects the most commonly utilized Quali The compound was analyzed for but was not detected. S The reported value is greater than the Method Detection Limit but less than the Reporting Limit. II The hold time for sample preparation and/or analysis was exceeded. D The result is reported from dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. m Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confirmed when GUMS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte.. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+), QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RR Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor fiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Quali£ters or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 27 HISUMIRIT MVIRONMENTAL IECHNOLOGIEs, INC. Anaty ticsl Labors ones CLIENT: Project: Synagro Randleman Summit E n7ironmenta] Technologies, C. 3310 Win St. Cuyahoga Falls, Ohio 44223 TeL: (330) 2,53-8211 FAX: (330) 253-4489 Website: httor/Avivw.senek.corn Workorder Sample Summary WO#: 18011441 28 -Feb -78 Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix 18011441-001 Randleman TCLP 2018 1/29/2018 9:10:00 AM 1/30/2018 11:20:00 AM Sludge Page 4 of 27 U IT samnot EnriromrreMa/Teahnomg es,0W S 3310 Win St.t. Analytical Report rtWIRONh1ENTAL'TECkNODIMEs, 44C Cuyahoga Falls, Ohio 44223 (base report) Analytical LaborBlones TEL: (330) 2538211 FAX: (330) 253-4489 WO#: 18011441 Website: htta.'/Avwry seuek con Date Reported: 2/28/2018 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/29/2018 9:10:00 AM Lab ID: 18011441-OOIA Project: Randleman. Client Sample ID Randleman TCLP 2018 Analyses Result RL Qual Units DP Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: EAM TCLP MERCURY ANALYSIS (SW1311/7470) TCLP Mercury ND 0.00500 mg/L 1 2/12/2018 4:21:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW301OA Analyst: KMS TCLP METALS ANALYSIS (SW1311/6010) TCLP Arsenic(As) ND 0.500 mg/L 1 2/13/2018 8:00:37 PM TCLP Barium(Ba) ND 5.00 mg/L 1 2/13/2018 8:00:37 PM TCLP Cadmium(Cd) ND 0.100 mg/L 1 2/13/2018 8:00:37 PM TCLP Chromium(Cr) ND 0.200 mg/L 1 2/13/2018 8:00:37 PM TCLP Lead(Ple) ND 0.500 mg/L 1 2/13/2018 8:00:37 PM TCLP Selenium(Se) No 0.0500 mg/L 1 2/13/2018 8:00:37 PM TCLP Silver(Ag) ND 0.500 mg/L 1 2/13/2018 8:00:37 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D Analyst: BJH TCLP SEMI -VOLATILES ANALYSIS (SW1311/8270) 1,4 -Dichlorobenzene ND 0.200 mg/L 2 2/15/2018 12:44:00 PM 2,4,5 -Trichlorophenol ND 0.500 mg/L 2 2/15/2018 12:44:00 PM 2,4,6 -Trichlorophenol ND 0.500 mg/L 2 2115/2018 12:44:00 PM 2,4-Dinitrotoluene ND 0.100 mg/L 2 2/15/2018 12:44:00 PM o -Cresol ND 0.500 mg/L 2 2/15/2018 12:44:00 PM m/p-Cresol(s) No 0.500 mg/L 2 2/15/2018 12:44:00 PM Cresols, Total No 10.0 mg/L 2 2/15/2018 12:44:00 PM Hexachloro-1,3-butadiene ND 0.0400 mg/L 2 2/15/2018 12:44:00 PM Hexachlorobenzene No 0.100 mglL 2 2/15/2018 12:44:00 PM Hexachloroethane No 0.200 mg/L 2 2/15/2018 12:44:00 PM Nitrobenzene No 0.200 mg/L 2 2/15/2018 12:44:00 PM Pentachlorophenol No 0.500 mg/L 2 2/15/2018 12:44:00 PM Pyridine ND 0.500 QC+ mg/L 2 2/15/2018 12:44:00 PM Surr: 2-Fluorophenol 1190 10-109 S %Rec 2 2/15/2018 12:44:00 PM Surr: Phenol -d6 584 10-109 S %Rec 2 2/15/2018 12:44:00 PM Surr: Nitrobenzene -d5 1920 19-120 S %Rec 2 2/15/2018 12:44:00 PM Surr 2,4,6-Tribromophenol 1110 10-120 S %Rec 2 2/15/2018 12:44:00 PM Surr. 2-Fluorobiphenyl 1740 22-117 S %Rec 2 2/15/2018 12:44:00 PM Qualifiers: Value exceeds Maximum Contaminant Level. E Valueabove quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected. O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 6 of 27 - sn„nirE",ironmentarTeehbn/10WinS. alytiealReport 3310 es, c. t. FINUMMIT Cuyahoga Pal/s, Ohio 44223 (base repay) Anatytirar taborworlea TEL: (330) 253-8211 PAX., (330) 253-4489 WO#: 18011441 Website: hrta:/hnvmsettek.eom Date Reported: 2/28/2018 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/29/2018 9:10:00 AM Lab ED: 18011441-OOIA Project: Randleman Client Sample ID Randleman TCLP 2018 Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270D Analyst: BJH TCLP SEMI-VOLATILES ANALYSIS (SW131118270) Surr: p-Terphenyl-dl4 2030 34-116 S %Rec 2 2/15/2018 12:44:00 PM NOTES: Sample exhibited high surrogate recovery, Sample was ND for all analytes of interest. TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081 SW351OC Analyst: JBN TCLP PESTICIDES ANALYSIS (SW1311/8081) Chlordane, total ND 0.0200 mg/L 2 2/13/2018 12:16:00 AM Toxaphene ND 0.0400 mg/L 2 2/13/201812:16:00 AM Endrin ND 0.00200 mg/L 2 2/13/201812:16:00 AM gamma-BHC ND 0.00200 mg/L 2 2/13/201812:16:00 AM Heptachlor ND 0.00200 mg/L 2 2/13/2018 12:16:00 AM Heptachlor epoxide ND 0.00200 mg/L 2 2/13/2018 12:16:00 AM Methoxychlor ND 0.00200 mg/L 2 2/13/201812:16:00 AM Surr: TCMX 66.3 10-119 %Rec 2 2/13/2018 12:16:00 AM Surr. DCB 55.4 10-119 %Rec 2 2/13/2018 12:16:00 AM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8151A SW8151A Analyst: JBN TCLP HERBICIDES ANALYSIS (SW131118151) 214-D ND 1.00 mg/L 1 2/23/2018 3:22:00 PM 21475-TP ND 0.500 mg/L 1 2/23/2018 3:22:00 PM Surr: DCAA 101 20-140 %Rec 1 2/23/2018 3:22:00 PM TCLP METALS, VOC; BNA, PEST, HERBKSOLID SW8260B SW1311 M Analyst: MES TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 0.100 mg/L 20 2/13/2018 3:58:00 PM 1,2-Dichloroethane ND 0.100 mg/L 20 2/13/20183:58:00 PM MEK 4.23 0.500 mg/L 20 2/13/2018 3:58:00 PM Benzene ND 0.100 mg/L 20 2/13/2018 3:68:00 PM Carbon tetrachloride ND 0.100 mg/L 20 2/13/2018 3:58:00 PM Chlorobenzene ND 0.100 mg/L 20 2/13/2018 3:58:00 PM Chloroform No 0.100 mg/L 20 2/13/20183:58:00 PM Tetrachloroethene ND 0.100 mg/L 20 2/13/2018 3:58:00 PM Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected 0 RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 7 of 27 SVmml•r SamrmttEm�ir'onrreentalTechnologies, Inc.ffJ 3310 Win St. AllalytlCalRCpOPi UNVIRONI,dENTAL IECHNO LOG i ES, INC Cuyahoga Falls, Ohio 44223 (base report) Arralyf7eaf Lehor'alorles TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18011441 Website: huallanviv.settek.co n Date Reported: 2/28/2018 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/29/2018 9:10:00 AM Lab ID: 18011441-o01A Project: Randleman Client Sample ID Randleman TCLP 2018 Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst: MES TCLP VOLATILES ANALYSIS Trichloroethene ND 0.100 mg/L 20 2/13/20183:58:00 PM Vinyl chloride ND 0.0400 mg/L 20 2/13/2018 3:58:00 PM Surr: 4-Bromofluorobenzene 98.2 70-130 %Rec 20 2/13/2018 3:58:00 PM Surr: Dibromofluoromethane 103 70-130 %Rec 20 2/13/2018 3:58:00 PM Surr: Toluene -d8 98.1 70-130 %Rec 20 2/13/2018 3:58:00 PM RCI -SOLID -W/ IGNITABILITY1030 SW9014 Analyst: MS REACTIVE CYANIDE (901417.3.3.2) -SOLID Cyanide, Reactive ND 0.500 mg/Kg 1 2/7/2018 12:42:00 PM RCI -SOLID -W/ IGNITABILITY1030 SW1030 Analyst: AJT IGNITABILITY OF SOLIDS (SW -846: 1030) Ignitability non-flammable 1 2/9/2018 11:00:00 AM RCI-SOLID-W/IGNITABILITY1030 SW9045D Analyst: DHC PH (SW9045D) pH 6.8 S.u.@19.00 1 2/12/2018 12:03:00 PM RCISOLID-WI IGNITABILITY1030 SW9034 Analyst: MS REACTIVE SULFIDE (9034)17.3.4.2 Sulfide, Reactive 30.0 25.0 mg/Kg 1 2/7/2018 12:42:00 PM QuaOfiers: * Value exceeds Meximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound LiIn ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 8 of 27 U IT SummitEnviromnenla7Technologies,Inc. Accreditation Irrogranl 3310 Win St Analytes Report CNVIRONh1ENTALIECW40LOGIEa,INC Cuyahoga Falls, Ohio 44223 Analytical taborstpNBs TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 18011441 Website: htto: nliviv.senek.com 28 -Feb -18 Client: Synagro State: NW Project: Randleman Program Name: NC—WW—SCM Sample ID Matrix Test Name Analyte Status 18011441-OOIA Sludge Ignitabilityof Solids (SW -9,16:1030) IgnitubilAy A Sludge pit(SW9045D) Hydrogen Ion (pH) A Sludge Reactive Cyanide (9014/7.3.3.2) -Solid Cyanide, Reactive U Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U Sludge TCLP Herbicides Analysis (SW13 1 V8151) 254,5 -TP A Sludge TCLP Herbicides Analysis (SW 1311/8151) 2,4-D A Sludge TCLP Herbicides Analysis(SW1311/8151) DCAA A Sludge TCLP Mercury Analysis(SW1311/7470) Mercury A Sludge TCLP Metals Analysis(SW1311/6010) Arsenic A Sludge TCLP Metals Analysis(SW1311/6010) Barium A Sludge TCLP Metals Analysis (SWI 311/6010) Cadmium A Sludge TCLP Metals Analysis(SW1311/6010) Chromium A Sludge TCLP Metals Analysis(SW1311/6010) Lead A Sludge TCLP Metals Analysis(SW1311/6010) Selenium A Sludge TCLP Metals Analysis (SW 1311/6010) Silver A Sludge TCLP Pesticides Analysis(SW1311/8081) 2,2',3,3',4,4',5,5',6,6'- A Decachlorobiphenyl Sludge TCLP Pesticides Analysis (SWI 311/8081) Chlordane, total A Sludge TCLP Pesticides Analysis (SWI 311/8081) Endrin A Sludge TCLP Pesticides Analysis (SW1311/808 1) gamma -BHC A Sludge TCLP Pesticides Analysis (SW1311/808 1) Heptachlor A Sludge TCLP Pesticides Analysis (SW1311/808 1) Heptachlor epoxide A Sludge TCLP Pesticides Analysis (SWI 311/8081) Methoxychlor A Sludge TCLP Pesticides Analysis (SW 1311/808.1) Tetrachlmo-m-xylene A Sludge TCLP Pesticides Analysis (SWI 311/8081) Toxaphene A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 1,4 -Dichlorobenzene A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,5 -Trichlorophenol A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,6-Tribromopbenol A Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2,4,6-Trichloropbenol A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A Sludge TCLP Semi -Volatiles Analysis (SW 1311/8270) 2-Pluorobiphenyl A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Fluorophenol A Key Key NC_WW_SCM A Accredited NC—WW—SCM U Unavailable Original #1 Page 9 of 27 U IT Summit Environmental Technologies, Inc. Accreditation Program ffIS3310 Win W23 Analytes Report t-i#VIRONIdEMIi1L 3@CHNULtlaiES, tYC Cuyahoga Falls,Ohio St. y 1' AnafyHcai t-ahnrarurles TEL: (330) 253-8211 FAX.,. (330) 253-4489 WO#: 18011441 website: Into /Avrvw.settek.eom 28-Feb-18 Client: Synagro State: NW Project: Randleman Program Name: NC—WW—SCM (Sample ID Matrix Test Name Analyte Status 18011441-OOIA Sludge TCLPSemi-Volatiles Analysis (SW 1311/8270) 2-Methylpheno1 NC WW SCM A Accredited NC WW SCM U Unavailable Original #1 Page 10 of 27 A Sludge TCLP Semi -Volatiles Analysis (SW 1311/8270) 3,4-Methylphenol A Sludge TCLPSemi-Volatiles Analysis(SW1311/8270) Cresols, Total A Sludge TCLPSemi-VolatilesAnalysis(SW1311/8270) Hexachlorobenzene A Sludge TCLP Serni-Volatiles Analysis(SW1311/8270) Hexachlombutadiene A Sludge TCLPSemi-VolatilesAnalysis(SW1311/8270) Hexachloroethane A Sludge TCLPSemi-VolatilesAnalysis(SW1311/8270) Nitrobenzene A Sludge TCLPSemi-Volatiles Analysis(SW1311/8270) Nitrobenzene-dS A Sludge TCLPSemi-Volatiles Analysis(SW1311/8270) Pentachlorophenol A Sludge TCLPSemi-VolatilesAnalysis(SW1311/8270) Phenol -d6 A Sludge TCLPSenn-VolatilesAnalysis(SW1311/8270) p4erphenyl-d14 A Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Pyridine A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A Sludge TCLP Volatiles Analysis 1,2-Dichloroetbane A Sludge TCLP Volatiles Analysis 2 -Butane A Sludge TCLP Volatiles Analysis 4-Bromofluorobenzene A Sludge TCLP Volatiles Analysis Benzene A Sludge TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volatiles Analysis Chlorobenzene A Sludge TCLP Volatiles Analysis Chlorolcnn A Sludge TCLP Volatiles Analysis Dibromofluoromethane A Sludge TCLP Volatiles Analysis Tetrachloroethene A Sludge TCLP Volatiles Analysis Toluene -d8 A Sludge TCLP Volatiles Analysis Trichloroethene A Sludge TCLP Volatiles Analysis Vinyl chloride A NC WW SCM A Accredited NC WW SCM U Unavailable Original #1 Page 10 of 27 Jn U a R r E E d q � o E U A E E � a E - E a o N � Y a m a on a m c z o N N j N ❑ ❑ E E � E - a N Y a N a on m = N N j N ❑ ❑ n E a - n O Z J ~ U F- ui csN CS � E - N Y a N N m j N n Z ~ a F- U67 � J � a � 2 U 6] a v - J W 0 d E m_TO n U Q n N N C � E o o r a d O� O L p� Y W O `o o O V❑ F Y c n o o m z- t t t _ U) M m U U U F F 1 0 0 a n � � r ❑ m a z o K a E_ N = m ❑ O E a T o J W m E � - � W Y ,y a N � E m j N N o z_ J t= ~ a J o � L M m H t d r fE m m y � a N � W E � m 0 0 0 0 m U L N 0 Y r N W � e a o � q 7 C � � d J � F4 f4 � o a m a", o b z a T a N � v o C o C V 3 a � w .E 09 . 0 >x>� r.. n N N C � E o o r a d O� O L p� Y W O `o o O V❑ F Y c n o o m z- t t t _ U) M m U U U F F 1 0 0 a n � � r ❑ m a z o K a E_ N = m ❑ O E a T o J W m E � - � W Y ,y a N � E m j N N o z_ J t= ~ a J o � L M m H t d r fE m m y � a N � W E � m 0 0 0 0 m U L N 0 Y r N W � e a o � q 7 C � � d J � F4 f4 � o a m a", o b z a T a N � v o C o C V 3 a � w .E 09 . 0 >x>� r.. 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N a N Z o Z Z e N m d K to r d m No rn m m m o m d m r 'o M C3 m n n N K d a � ❑ o � E T N N E N N �- W� M E O J 4! N af N Z o = N m m o ❑ E N U E o c a @ o o m S Q J �❑ U m U E K m ❑ K r d m No rn m m m o m d m r 'o M C3 m n n N E r d m No rn m m m o m d m m C3 m n n r d m No rn m m m � O m C3 �O � N E d _I � ❑ o � E T N N E N N W� r E O � 4! af N Z o N m � O m m �O � N K d ❑ � � o � E m N N E N N y E O 4! N N U O � N U E o c aca ' w o m a _ �❑ J m U E m m ❑ K � U Q � O m m �O � N d N � � o � E m N N E N N y O 4! N N U CY N U E o c m w PC m a _ �❑ m E m m ❑ � U Q � O m m �O � d N '�V N N N N N N N N N N Oro (00 O N O� u0l O N N O O S O N � � %- N� A r m m � d N � � H N N E m N %- O 4! N U E o c w PC m a _ m o O ❑ � T E d — m U Q m PC C N N i '�V N N N N N N N N N N Oro (00 O N O� u0l O N N O O S O N � � %- N� A r m � d � � H N � m m N %- O 4! N U M w m ❑ � T E d — m U Q '�V N N N N N N N N N N Oro (00 O N O� u0l O N N O O S O N � � %- N� A r m N m 0 m OJ T W 00.0000000 00 O N 0 0 0 0 0 0 0 0 r m m� co 0 of r V c v N Sym C � 0 0 0 0 E E 0 o a N E C _ an d -PPL v C D M Lo t o2 t t ❑ow .o `o `o 2 B.�mto r m U 0 U H F � � N � ��%- N %- m N m 0 m OJ T W 00.0000000 00 O N 0 0 0 0 0 0 0 0 r m m� co 0 of r V c v N Sym C � 0 0 0 0 E E 0 o a N E C _ an d -PPL v C D M Lo t o2 t t ❑ow .o `o `o 2 B.�mto r m U 0 U H F 0 r m m� co 0 of r V c v N Sym C � 0 0 0 0 E E 0 o a N E C _ an d -PPL v C D M Lo t o2 t t ❑ow .o `o `o 2 B.�mto r m U 0 U H F w m C � Q a � b C Q � � p 5 t a w �a C a 3 e � d m d � 2 � / )(, ) ) )/ k / )(, ) ) k \\� ()/w �k\ \� \\ /m\ k \ \\)\ : \\ }Cye :!) })}) 00 { )�\\ ) \))\ ) \� \6\` « \32} \\} \\ \ / )(, ) ) k \\� ()/w �k\ \� \\ /m\ \\)\ : \\ }Cye :!) })}) 00 )�\\ \))\ ) \� \6\` / ) ) k \\� ()/w \� \\ \\)\ : \\ }Cye :!) })}) )�\\ \))\ 4/)) \6\` « \32} \\} \\ \ 0 / ) ) k I/ ()/w \\ \\)\ : \\ !!\§ :!) })}) )�\\ \))\ 4/)) \6\` « ) I/ \\ : \\ :!) \} )�\\ 4/)) \6\` \32} \\} #!2: 0 / ) \\� : :!) )�\\ \6\` \\} 0 / ) c-� K Y � � J d v� d . o � � M � V P Y � � J N� v� 00 � � M � m ❑ K a � � a 6 � ❑ m a � m E ro m I N � m N� 0 � W M a. 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J N K a � U U J J ❑ � a � o m m E m m N 0 O LO m N � d) P4 o m a ti a k4 Y1 > w o x N p N� m W M a, n N K 0 U U J J ❑ � o m E m m a�0 N 0 O LO m N � d) P4 o m a ti a k4 Y1 > w o x N p N� N W M a, M K 0 a � U � � o E m m a�0 N QN p U � o c V U U N a N E 00 ❑ m w E m m P fn U Q E � m n U Q N 0 O LO m N � d) P4 o m a ti a k4 Y1 > w o x N p N � M a, 0 U � m � .N a�0 QN p U � o c V Q U N N E 00 ❑ w E m m P fn U Q N 0 O LO m N � d) P4 o m a ti a k4 Y1 > w o x a k4 Y1 > w o x a .N a�0 � o c V � U E � o A N 3 C p a a X ❑ E ¢a�za a .N a�0 � o c V � U E a k m P fA a .N a�0 � o c V � U E a k m P x � w w a § \ / ) \ � )! \ / ) \ � \) \\(e \) \\\\ \\ a ±3 E, ; !7 §� ;):@ \\)) _P� ) \) \\(e \) \\ a )) ; !7 §� ){\! \\)) \\\\ !xe! ®(\ \\(e a )) ; §� ){\! \\\\ LQ\ ) � �k\ (®2� \ \\� _ \\ ))/) \() \\ I \\ \_ /) )L) \\ \\; )�\\ )�} �{\ »);2 c! \\ \{)) ]&24 {\ { ! > f} �( ;r ca &3` )4 «� < (\ 12!; �\\ o o kk\ 6;: // \,aG C3 q LQ\ ) � �k\ (®2� \ \\� _ \\ ))/) \() \\ I \\ /) )L) \\ \\; )�\\ )�} �{\ »);2 c! \\ \{)) ]&24 {\ { ! > f} �( ;r ca &3` )4 «� < LQ\ ) � �k\ (®2� \ \\� _ \\ ))/) \() \\ I \\ /) )L) \\ LQ\ ) � �k\ (®2� \\� \\ ))/) \() \\ I \\ /) )L) \\ \\; )�\\ )�} �{\ »);2 \\ \{)) ]&24 LQ\ ) � �k\ (®2� \\� \\ ))/) \\ I \\ /) )L) \\ )�\\ )�} »);2 � ) � }$ (®2� \\� \\ ))/) \\ \\ )L) \\ )�\\ »);2 \\ \{)) ]&24 {\ { ! > � i ) � }$ (®2� \\ ))/) \\ E2!§ \\ )�\\ »);2 \{)) i }$ \\ \\ \\ \{)) ]&24 % \ 2 ) u (� ) f) k 7! 00 ) ) k 7! 00 _( ) ) k 00 _( \ Id / / \\ fE ))\j \\ \ *j!{ \\ \ £E#§ \\ ):E« R: \/ \\\} \C6 \})_ 7#2/ {� =,y: ) ) k 00 _( \ Id / / \\ fE ))\j \\ \ *j!{ \\ \ £E#§ \\ ) ) k 00 _( \ Id / / \\ ) ) k 00 _( \ Id / / \\ ))\j \\ \ *j!{ ) ) k 00 _( \ / / \\ ) ) k 00 \ / / ) ) k )) {}$i \\ ))\j *j!{ £E#§ \\ ):E« \\\} ) )) \\ \\ \\\} \})_ 7#2/ =,y: § 3 )Z ] ) \ \\ \ \\� !}r )Z � ) \ } \ \\� !}r 46 ° / \ ; \� Ofaf \� \ \\ =»f! Cl \ � ) � ) \ } \ \\� !}r 46 ° / f \� \� \ \\ =»f! Cl \ � ) j)\! \\ :* \\ \` ]j5) � ) / ) \ } \ \\� !}r 46 ° / f \� \� \\ =»f! Cl \ � ) j)\! \\ :* \\ \` ]j5) 7\ \\ } \f/) { F0 ])2� Df ) / ) \ } \ \\� !}r 46 )) \� \� \\ =»f! Cl \ � ) j)\! \\ :* ]j5) 7\ \\ } \f/) { ) / ) \ } \ !}r 46 )) )i:� \� \\ =»f! Cl \ � ) j)\! ) / ) \ \ !}r 46 )) )i:� \� \\ =»f! \ � ) j)\! :* ]j5) 7\ \f/) { ])2� Df \\ \\ t = e 77 /2 ) / ) \ \ !}r )) )i:� \� \\ =»f! \� j)\! :* ]j5) 7\ \f/) { ])2� Df \\ \\ ) / ■ % \ 2 ) \ \ !}r )) )i:� )j){ \\ =»f! \` j)\! :* ■ % \ 2 ) )) () \\ \` ]j5) \f/) ])2� ■ % \ 2 � � wo ) � CY )Z � � wo ) � CY } (}\{ \ k| ! _ cl !k� ( £ \\ { \\ \ei / f2!) � � wo ) � } } (}\{ k| _ cl !k� ( £ \\ { \\ \ei / f2!) \ } ) � � wo ) � CY } (}\{ k| _ cl !k� \ \\ { \\ \ei / f2!) � � ) � } (}\{ k| _ cl \� \ \\ { \\ \ei / f2!) \ } \\\\ � � ] / ) � } (}\{ k| _ cl \� \\ \ \\ \ei / f2!) \\\\ ! ))2/ _ 2 \0 k 00 cy ] / ) � } (}\{ k| cl \� \\ \ \\ \ei ] / ) � } (}\{ \§ {))3 \� ] / ) � } (}\{ \§ {))3 \\ \ei ] / \ 2 ) � } (}\{ {))3 f2!) \ 2 ) )) \\ /\ \\\\ ))2/ =-2e \ 2 � � till � � ) % )/ §§! ) % \) §§! \ ;§! 3 / \) \\� \\){ : \{ \\ /!°° E®;! }2 2U E« )§ ;]2/ »»mm ))2! _- \\ 7)/) \\ \\j) \\ \ -=y® \\ ) % \) §§! \ 0 3 / \) \\� \\){ : \{ \\ /!°° E®;! }2 E« )§ ;]2/ »»mm ))2! _- 7)/) \\ \\j) -=y® \\ } \ ) % \) \,\ \ 0 3 / ) \) \,\ \j)( \) \\� \\){ : \{ /!°° E®;! }2 E« ;]2/ »»mm ))2! _- ) \) \) \\� : \{ /!°° ±\\) )[{g ))2! 7)/) \\� : /!°° ±\\) )[{g 7)/) \\j) -=y® \ |� Pei ca I ) ) ) � ƒ §)) ())\ \ — \ � , )® \\\ ( \\ ) \\)\ \� \ {/ { ) \\ Pei ca I ) ) ) � ƒ §)) ())\ /\ — \ — , )® \\\ ( \\ ) \\)\ \� \ {/ { ) \\ ! /a!$ & !3 \ )�)) ) ca »)»m. » { \)}` ) Pei ca I ) ) ) � ƒ §)) ())\ /\ — \ — , )® \\\ \\ \\)\ \� \ {/ { ) \\ ! /a!$ & !3 )�)) Pei I ) ) ) � ƒ §)) ())\ /\ — — )® \\\ \\ \\)\ \� \ {/ { ) \\ ! /a!$ & !3 )�)) »)»m. » { \)}` ) \\\\ \\}j ))/_ � \ 0 I ) ) ) � ƒ §)) ())\ /\ — — )® \\\ \\ \\)\ \� {/ { \\ ! /a!$ & !3 )�)) »)»m. » \)}` \\\\ \\}j ))/_ \\\ \(\` CY Lo 0 L6 \ 0 I ) ) � \\ §)) ())\ /\ )® \\\ \\ \ 0 I ) ) \§ §)) ())\ /\ \\\ \\ \ 0 I ) ) §)) ())\ /\ \\ \\)\ \� {/ { \\ \ 0 I ) ) ())\ /\ \\ \\)\ {/ { \\ ! /a!$ & \ 0 ) ) ) ())\ \\ \\)\ \\ /a!$ !3 )�)) »)»m. » ) \} \\ \\ !3 )�)) \)}` \\\\ \\}j ))/_ % § \ \\), )\/) )�)) \)}` \\}j % § \ \ TO ) � )! §)k \ TO ) � 46 §)k (®$) \ cl \ � \� \\j{ B}} \) /\ \ ) Eƒi§ k \ of \ (0 Ey \\ FT a \ ) � 46 §)k (®$) \ \ � \� \\j{ B}} \) /\ \ ) Eƒi§ k \ CO \ (0 Ey \\ FT a o \ f3 \ { /\ ) \/ \ \ ) � §)k (®$) \ \ � \� \\j{ B}} \) /\ \ ) Eƒi§ CO \ (0 Ey \\ FT a \ \ ) � §)k (®$) \ \ � \� \\j{ B}} \) /\ \ ) \ ) � (®$) \ \ � \\j{ B}} \) /\ \ ) Eƒi§ \ (0 Ey \\ \ \ \ 3 ) � (®$) \ \ � \\j{ B}} \) /\ \ ) Eƒi§ 3a Ey \\ \ \ 3 ) � (®$) \ \\j{ \\ \) /\ \ ) Eƒi§ 3a Ey \\ \ f3 \ /\ \ \ 3 ) � (®$) \ \\j{ \\ \) /\ \ Eƒi§ 3a Ey \\ \ \ 3 ) � (®$) \\j{ \\ \) Eƒi§ 3a Ey \\ f3 /\ \/ \ \\\\ \ \ 3 ) ) � (®$) \\j{ \) Eƒi§ 3a Ey \\ f3 ) )) \) \\ f3 \\\\ � § � _ ) / , ) (� � ƒ) )! CY _ ) / ) � )! CY _ ) / ) � CY \\� {$$} \ m ))\3 \� \\ ) \ \«)84 ,El= \\}\ _ ) / ) � \\� {$$} ))\3 \� \\ ) \ \«)84 ,El= \\}\ \/ CY ))/( ~/! „ :a \\3\ \{/! \ U) ) \/\\ 46 cl 00 _ ) / ) � \\� {$$} ))\3 \� \\ \«)84 ,El= \\}\ \/ CY ))/( „ :a \\3\ \{/! \ U) _ ) / i ) � !] {$$} ))\3 \\ \«)84 ,El= \\}\ \/ ))/( „ :a i !] \\ )\ \/ \\3\ \{/! \/\\ \ & 2 v o E m - ro o w LO ro N v'i c4 v N m - d o w LO ro N U W v N m - N o w LO ro N c a c � o a U � a J � bq m uE@i v N 0 - w LO ro N c a c � o a U U J J � bq G � oa o k (n U Q N m - w LO ro N c a c � o a d � bq G � oa o k E m 0 0 �r U a V 3 Q °' oo � 3 F w U c4 d m a�a�za x � a COza fn U Q N O w LO ro N c � C � o a w a bq G �� o k 0 0 �r U � V 3 °' oo � 3 F w o c4 w G �� o k 0 0 U � V 3 � 3 F a�a�za x � a COza G �� o k 0 0 U � V 6 � 3 F x � a a a iia m 0 Uc w o� �o U � F ro C Q M�V J� •CA a �1 MMSUMMIT Sunmti(Environmental Technologies, Inc. 3310 Win Sr. rNVIRONNIENTAL IECHNOLOc1ES, INC- Cuyahoga Falls, Ohio 44223 Sample Log -In Check List Analytical Le4oretorles TEL: (330) 253-8211 FAX (330) 253-4489 Website: h ty.,11 imv.settek.com Client Name: SYN -NC -27028 Work Order Number: 18011441 Logged by: Lori Douglas Completed By: Christopher Livengood Reviewed By: Jennifer Woolf 1/30/2018 11:20:00 AM 1/30/2018 2:47:22 PM 1131/2018 11:33:06 AM RcptNo: 1 Chain of Custody 1, Is Chain of Custody complete? Yes No ❑ 2. How was the sample delivered? Fed6c Lo In Samples) in proper container(s)? Yes 0 No 3, Coolers are present? Yes 0 No ❑ 4, Shipping container/cooler in good condition? Yes 91 No ❑ ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ ❑ No. Seal Date: Signed By: Yes ❑ 5. Was an attempt made to cool the samples? Yes V No ❑ 6. Were all samples received at a temperature of >00 C to 6.0°C Yes 91 No ❑ 7_ Samples) in proper container(s)? Yes 0 No ❑ 8, Sufficient sample volume for indicated test(s)? Yes V No ❑ 9, Are samples (except VOA and ONG) properly preserved? Yes 0 No ❑ 10. Was preservative added to bottles? Yes ❑ No ❑ 11. Is the headspace in the VOA vials less than 114 inch orb mm? Yes ❑ No ❑ 12, Were any sample containers received broken? Yes ❑ No W 13. Does paperwork match bottle labels? Yes 0 No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes 0 No ❑ 15, Is it clear what analyses were requested? Yes W No ❑ 16. Were all holding times able to be met? Yes ❑e No ❑ (If no, notify customer for authorization.) Special Handling (if applicable) 17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ Not Present ❑ NA 1:1Not Present S6 NA LlNA ❑ NA o NA No VOA Vials 91 NA � Person Notified: Date By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 1$, Additional remarks: Cooler Information Cooler No Temp °C Condition Seal Intact Seal No Seal Date Signed B 1 3.6 Good Not Present Page 27 of 27 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Randleman W WTP WQ Permit Number: W1 P Name: Town of Randleman W WTP NPDES Number: _ Monitoring Period: From 01/01/18 To 12/31/2018 WQ 0004825 NC 0025445 Pathogen Reduction (40 CFR 503.32/15A NCAC U2T.1106) -Please indicate level achieved and alternafive performed: Class A: Alt. 1/A (time/temp) Alt 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PERP) If applicable to alternafive performed (Class A only) " indicate Process to Further " Reduce Pathogens: Compost Heat Drying Heat Treatment Thermophilic Beta Ray _ Gannon Ray Pasteurization of Class B: Ah. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion .. __________ ________"_.___-.�_.__�...,___ • __�,_.._ns ..,......:..... .r...ear,....:..,, ,..,...:«..,.:.... a,.,. Parameter Allowable Level in Sludge Vector Attraction Reduction (40 CPR 503.33/15A NCAC 02T1107) -Please indicate opti Option/AIC. 2 Pathogen Density No. of Frequency Sample Analytical (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Excce- of Type Technique (Drying — Stable) (Drying — Unstable) Minimum Geo. Mean Maximum Units dences Analysis (Injection) Fecal 2x10 to the 6°i MPN CERTIFICATION STATEMENT (please check the appropriate statement) MPN/g Coliform power per gram of total solids CFU/g CFU m 1000 MPN per graof MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) on/alternative performed Option/ALC. 1 attractionX "q certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." Option/AIC. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40 -day bench) (30 -day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14 -Day Aerobic) (Alk Stabilization) X (Drying — Stable) (Drying — Unstable) Option/Alt.9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements,) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met I am aware that there are significant penalties for false certification me acting fine and imprisonment." Michael Glass Plant Superintendent Prep Or r N me apd Title (type or print) Signature ofPreparcr* Date Land Applies Name and Title (if applicable) (type or print) Signature of Land Applies (if applicable) Date *Prepares is defined in 40 CFR Part 503.9(1) and 15A NCAC 2T.1 102 126) 4 a t W Q ;~ R Sampler & pH f �. analystinitials k ci F G1 i+a �q T t p Sampletime/ �n N M e pHtest time cn m "A M £ Aafe of 24 hour:eat sample &pHtest p \ \ U� U °v c 41 all s N r N N E � �, t N Sampler&pH J •�' analystinitialsNN r Sample fime7 .= >+l PH test time N u\ �. o hl �Go Rtj l( �i Sampler & PH nalystinitlals �� %a) Sample time/ PH testfima N M Date of Initial & 2 hr: �� � N1 d sample e&pHtest J 4 x s 4 a SECTION 6 1 /28/2019 Soil Reports 2018 - Dropbox Agricultural Lime Application Log 131 Year:. 2018 Project: Randleman Field state -count -site-field code Soil pH Lime Requirement from soil anal sis Tons/Acre Applied Date Applied NC -RD -19-01 7.1 0.0 tons/ac. NC -RD -19-02 6.9 0.0 tons/ac. 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