WQ0000048_Residual Annual Report 2018_20190313

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0000048
SUBMITTAL DATED: 2/26/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Lisa Finnerty
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0000048
Permittee *
Facility Name *
City of Whiteville
City of Whiteville
Phone Number*
4434899086
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
City of Whiteville NC 2018 Annual Report.pdf 3.22MB
upload only 1 R7F docurrent. IVLltiple documents must be cor ined into one R7F file.

For neiv and modif cation permit applications, the paper copy is required to be submitted to the
Di,,isiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ping:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,,ision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942 M
512 N_ Salisbury St_ Raleigh, NC 27604
For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
* I40 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/26/2019

435 NVilliams Court, Suite 100
Baltimore, MD 21220
wwwsynagro.coin
FEBRUARY 22, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2018 Annual Report for Permit No. WQ0000048
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Whiteville, NC.
If you have any questions or comments, please contact Darren Currie at [phone] or Nate
Roth at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Darren Currie — City of Whiteville
Nate Roth - Synagro
YOUR PARTNER FORA CLEANER, GREENER WORLD

CITY OF WHITEVILLE, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000048
2018 ANNUAL REPORT

City of Whiteville, NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses
& SAR Calculation Pages
3. Annual Land Application Field Summary Form
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00000048 County Columbus Year 2018
Facility Name (as shown on permit) City of Whiteville, Whitemarsh WWTP NPDES No. NCO021920
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A —Residuals Application Summa
Total number of application fields in the permit: 35
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 91.77
Total number of acres utilized for land application during the year: 32.80
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
I hint specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T A 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T. I t 11 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
if. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false i 0 oration, including the possibility of fines and imprisonment for
knowing violations."
Darren Currie, City Manager 1— 1
Permittee Name and Title (type or print) Signature o Pe i
Signature Preparer* at S i gn a e of and App1 Date
(if different from Permittee) (if different from 'of
and Preparer)
'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
WHITEVILLE, NC
WHITEVILLE, NC WHITEMARSH AEROB. DIG. LIQUID
MONTHNEAR
May 2018
June 2018
YEARLY TOTAL
AMOUNT UNIT
192,200.00 G
347, 200.00 G
539,400.00 G
DRY TONS UNIT
32.70 D
59.07 D
91.77 D
DRY METRIC
TONS
29.66
53.58
83.24
1/28/2019

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Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2059-01-AEDLIQ-NC WHITEVILLE, NC WHITEMARSH AEROB. 2/15/2018 31112018-1213112018 0.9667
DIG. LIQUID
Na mgll = (Na mglkg x % Solids) � 100 = (2330 x 4.0800) 100 = 95.064
Ca mgll = (Ca mglkg x % Solids) + 100 = (14900 x 4.0800) + 100 = 607.92
Mg mgll = (mg mglkg x % Solids) + 100 = (2040 x 4.0800) + 100 = 83.232
Na meq = Na mg11 + Molec.Wgt.Na = 95.064 + 23 = 4.13322
Ca meq = Ca mgll + Mo[ec.Wgt.Ca = 607.92 + 20 = 30.396
Mg meq = Mg mg/1 + Molec.Wgt.Mg = 83.232 + 12 = 6.936
SAR = Na meq + SgrRoot]0.5 x (Ca meq + Mg meq)] = 4.13322 + SgrRoot[0.5(30.396+6.936)] = 0.956671
Printed: 1/31/2019
Page 1 17:13

SECTION 3

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SECTION 4

Summit Environmental Technologies, Inc.
SUAIMIT 3310 Win St.
FrIVIROMMENTAL TECHNOl-Oams, wry Cuyahoga Falls, Ohio 44223
11rra1ytfPa1 L_at�oralories TEL: [phone] FAX.- [phone]
Website: httn:/Avwyv.settek.com
March 05, 2018
Nate Roth
Synagro
284 Boger Rd.
Mooksville, NC 27028
TEL: [phone]
FAX: (336) 998=8450
RE: Whiteville
Dear Nate Roth: Order No.: 18020863
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/16/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88,0735, California 07256CA, Colorado, Connecticut PH-0l08, Delaware, Flonda NELAC E87688, Georgia E87688, Idaho 01100923, Illinois
200061, lndiaaa C-OU-13, Kansas 1i10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New jersey OH006, New York 11777, North Carolina 39705 mid 631, North Dakota R-201, Oklahoma 9940, Oregon
01-12O0001, Rhode Island LA00031-1, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C991
Page 1 of 31

Summit Environmental Technologies, Inc. Case Narrative
summly 3310 Win St.
FFviRommrwrALTecompLo3i5.algc= Cuyahoga Falls, Ohio44223 WO#: 18020863
Analytical tabara7arles TEL: [phone] FAX.- [phone]
Website. httn:/hvww.settekcom Date; 3/5/2018
CLIENT: Synagro
Project: Whiteville
WorkOrder Narrative:
18020863: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditationslcertifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Original
v
Page 2 of 31

Summit Environmental Technologies, In Qualifiers and Acronyms
SUMMIT 3310 Win ,�
FWRONME:NTAL WCHHOLOC9t3, Wr, Cuyahoga Falls, Ohio 442� Wo#: 18020863
Analytical t ahoralories TEL: [phone] FAX: [phone]
Website: hitDa/wwiv.settekco Date: 315I2018
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
m Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
BIMB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-1+ The MS or MSD recovery failed low (-) or high (+),
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-l+ The ICV recovery failed low (-) or high (+),
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quamtitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 31

J�� SU I gt M1 Sunmiit Environmental Technologies, Inc.
3310 Win St.
R MIRONME AL UcONo.L ajzs, zNG Cuyahoga Falls, Ohio 44223
Arkveyffcal t abarglodes TEL: [phone] FAX.- [phone]
Website: h9p:/hvww.settekconz
CLIENT: Synagro
Project: Whiteville
Lab SampleID Client Sample ID
18020863-001 Whiteville WWTP
Tag No Date Collected
2/15/2018 10-30'00 AM
Workorder
Sample Summary
WO#: 18020863
05 Mar-18
Date Receivcd Matrix
2/16/2019 10:10:00 AM Solid
Page 4of31

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SUMMINt
Summit Environmental Technologies, Inc.
Analytical Report
3310 Win St.
FKVIRONMENTALTfCONOLOG{ES,
INC
Cuyahoga Falls, Ohio 44223
(base report)
ArzaPyth
,gt LaboratoKest
TEL: [phone] FAX.- [phone]
WO#: 18020863
Website: httg.-Ilwww settekcom
Date Reported: 3/5/2018
CLIENT:
Synagro
Tag Number:
Matrix:
SOLID
Collection Date:
2/15/2018 10:30:00 AM
Lab ID:
18020863-001A
Project:
WhitevilIe
CIient Sample ID WhiteviIle WWTP
Analyses Result
RL Qual
Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW7470A
SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury
ND
0.00200
mg1L
1
2/21/2018 11:06:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
Analyst: KMS
TCLP METALS ANALYSIS (SWI311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L.
1
2/21/2018 7:03:45 PM
TCLP Barium(Ba)
ND
5.00
mglL
1
2/21/2018 7:03:45 PM
TCLP Cadmium(Cd)
ND
0.100
mglL
1
2/21/2018 7:03:45 PM
TCLP Chromium(Cr)
ND
0.200
mglL
1
2/21/2018 7:03:45 PM
TCLP Lead(Pb)
ND
0.500
mg1L
1
2/21/2018 7:03:45 PM
TCLP Selenium(Se)
ND
0.0500
mg1L
1
2/21/2018 7:03:45 PM
TCLP Silver(Ag)
ND
0.500
mg1L
1
2/21/2018 7:03:46 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311I8270)
1,4-Dichlorobenzene
ND
0.0800
mglL
2
2/20/2018 7:32:00 PM
2,4,5-Trichlorophenol
ND
0.200
mglL
2
2/20/2018 7:32:00 PM
2,4,6-Trichlorophenol
ND
0.200
mglL
2
2/20/2018 7:32:00 PM
2,4-Dinitrotoluene
ND
0.0400
mglL
2
2/20/2018 7:32:00 PM
o-Cresol
ND
0.200
mg1L
2
2/20/2018 7:32:00 PM
mlp-Cmsol(s)
ND
0200
mglL
2
2/20/2018 7:32:00 PM
Cresols, Total
ND
4.00
mg1L
2
2/20/2018 7:32:00 PM
Hexachloro-1,3-butadiene
ND
0.0160
mglL
2
2/20/2018 7:32:00 PM
Hexachlorobenzene
ND
0.0400
mg1L
2
D201201 B 7:32:00 PM
Hexachloroethane
ND
0.0800
mglL
2
2/20/2018 7:32:00 PM
Nitrobenzene
ND
0.0800
mglL
2
2/20/2018 7:32:00 PM
Pentachlorophenol
ND
0.200
mg1L
2
2/20/2018 7:32:00 PM
Pyridine
ND
0.200
mg1L
2
2/20/2018 7:32:00 PM
Surr: 2-Fluorophenol
41.2
10 - 109
%Rec
2
2/20/2018 7:32:00 PM
Surr: Phenol-d6
38.4
10 - 109
%Rec
2
2/20/2018 7:32:00 PM
Surr: Nitrobenzene-d5
64.7
19 - 120
%Rec
2
2/20/2018 7:32:00 PM
Surr: 2,4,6-Tribromophenol
37.5
10 - 120
%Rec
2
2/20/2018 7:32:00 PM
Surr. 2-Fluorobiphenyl
66.2
22 - 117
%Rec
2
2/20/2018 7:32:00 PM
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit,
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 6 of 31

summilt
Summit Environmental Technologies, Inc.
3310 Win St.
Analytical Report
r-WIRONMENTAL TECHNOLOGIE5, WC
Cuyahoga Falls, Ohio 44223
(base report)
Ar"tytlzal tabcraiariex TEL: [phone] FAX [phone]
WO#: 18020863
Website: htW.11www.se1tek.coin
Date Reported: 3/5/2018
CLIENT:
Synagro
Tag Number:
Matrix:
SOLID
Collection Date:
2/15/2018 10:30:00 AM
Lab ID:
18020863-001A
Project:
Whiteville
Client Sample ID Whiteville WWTP
Analyses
Result RL Qual Units
DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270D
SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Surr; p-Terphenyl-d14 88.2
34 - 116
%Rec
2
2/20/2018 7:32:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
Analyst: JBN
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total ND
0.0200
mglL
2
2/26/2018 3:02:00 PM
Toxaphene ND
0.0400
mglL
2
2/26/2018 3:02:00 PM
Endrin ND
0.00200
mglL
2
2/26/2018 3:02:00 PM
gamma-BHC ND
0.00200
mg1L
2
2/26/2018 3:02:00 PM
Heptachlor ND
0.00200
mg1L
2
2/26/201 B 3:02:00 PM
Heptachlor epoxide ND
0.00200
mg/L
2
2/26/2018 3:02:00 PM
Methoxychlor ND
0.00200
mg/L
2
2/26/2018 3:02:00 PM
Surr: TCMX 35.1
10 - 119
%Rec
2
2/26/2018 3:02:00 PM
Surr: DCB 36.4
10 - 119
%Rec
2
2/26/2018 3:02:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8151A
SW8151A Analyst: JBN
TCLP HERBICIDES ANALYSIS (SW131118151)
2,4-D ND
1.00
mg/L
1
2/28/2018 6:33:00 PM
2,4,5-TP ND
0.500
d mg/L
1
2/28/2018 6:33:00 PM
Surr: DCAA 84.0
20 - 140
%Rec
1
2/28/2018 6:33:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
SW82608 SW1311 M Analyst: MES
0.100
mg1L
20
2/21/201 B 5:09:00 PM
0.100
mg1L
20
2/21/2018 5:09:00 PM
0.500
mg/L
20
2/21/2018 5:09:00 PM
0.100
mg/L
20
2/21/2018 5:09:00 PM
0.100
mg/L
20
2/21/2018 5:09:00 PM
0.100
mg/L
20
2/21/2018 5:09:00 PM
0.100
mg/L
20
2/21/2018 6:09:00 PM
0.100
mglL
20
2/21/2018 5:09:00 PM
0.100
mg/L
20
2/21/2018 5:09:00 PM
0.0400
mg1L
20
2/21/2018 5:09:00 PM
Queliriers: *
Value exceeds Maximum Contaminant Level,
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 7of31

Summit Environmental Technologies, Inc. Analytical Report
summilu 3310 Win St.
F'NV1FtONMENTALTfCHNOLDGIES,ING Cuyahoga Falls, Ohio44223 (base report)
Art-41ybcaf CaborOooes TEL [phone] FAX.- [phone] WO#: 18020863
Website: hgq.-1Avww.seitek.com Date Reported: 3/5/2018
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 2/15/2018 10:30:00 AM
Lab ID: 18020863-001A
Project: WhitevilIe
Client Sample ID Whitewille W WTP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB
-SOLID
SW8260B
SW1311M
Analyst: MES
TCLP VOLATILES ANALYSIS
Surr: 4-13romofluorobenzene
93.9
70 - 130
%Rec
20
2/21/2018 5:09:00 PM
Surr: Dibromofluoromethane
99A
70 - 130
%Rec
20
2/21/2018 5:09:00 PM
Surr. Toluene-d8
99.1
70 - 130
%Rec
20
2/21/2016 5:09:00 PM
RCI-SOLID-WI IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (901417.3.3.2)-SOLID
Cyanide, Reactive ND 0.500
mg/Kg 1
2/22/2018 4:49:00 PM
RCI-SOLID-Wl IGNITABILITY1030
SWI030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
1
2/21/2018 10:30:00 AM
RCI-SOLID-WIIGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH 6.8
s.u.@19.1C 1
3/1/2018 11:17:00 AM
RCI-SOLID-W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive 30.0 25.0
mg/Kg 1
2/22/2018 4:49:00 PM
*
Qualifiers:
Value exceeds Maximum Contaminant Level.
H
Bolding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 31

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
Accreditation Program
Anal tes Report
y ll
FFiV1R0fJME:NTALTFCHN0L0Cjr!s,wo
Cuyahoga Falls, Ohio44223
Arralyffcal Leghoraforiva TEL: [phone] FAX: [phone]
WO#: 18020863
Website: htt ://iviviv.settekcom
05 Mar-18
CIient:
Synagro
State: NW
Project:
Whiteville
Program Name: NC WW_SCM
Sample ID Matrix
Test Name
AnaIyte Status
18020863-00 lA Solid
lgnitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7 3 3 2)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7 3.4.2
Sulfide, Reactive
U
Solid
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Solid
TCLP Herbicides Analysis (SW13I1/8151)
2,4-D
A
Solid
TCLP Herbicides Analysis (SWI 311/815 1)
DCAA
A
Solid
TCLP Mercury Analysis (SW131 in470)
Mercury
A
Solid
TCLP Metals Analysis (SW131116010)
Arsenic
A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW13I 1/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW13I1/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW 1311/8081)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Solid
TCLP Pesticides Analysis (SW131118081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW13111808I)
Endrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gar mna-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW 131118081)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis(SW131119081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Tetrachlora-m-xylene
A
Solid
TCLP Pesticides Analysis (SW1311/8091)
Toxaphene
A
Solid
TCLP Semi-Volatiles Analysis (SWI311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SWi311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW13IV8270)
2,4,6-Tribromophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW 1311 /8270)
2,4,6-Trichlomphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2-Fluorobiphenyl
A
Solid
TCLP Setni-Volatiles Analysis (SW1311/8270)
2-Flumophenol
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Original #I
Page 9 of 31

Summit Environmental Technologies, Inc. Accreditation Program
suramilt 3310 Win St. Anal tes Report
1 MV111044MENTALTEC14NO1-004fe9, INC; Cuyahoga Falls, Ohio 44223 Y P
Analytical L,abors00605 TEL: [phone] FAX.- [phone] wok 18020863
Website: h1tp.11www.settekcom
05 Mar-18
Client: Synagro
State: NW
Project: Whiteville
Program Name: NC WW_SCM
Sample ID
Matrix
Test Name
Analyte
Status
18020863-001A
Solid
TCLP Semi-Volatiles Analysis (SW131118270)
2-Metliylpbenol
A
Solid
TCLP Semi-Volatiles Analysis (SW 131118270)
3,4-Methylphenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/9270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW131118270)
Nitrobenzene-d5
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentaeblorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW131118270)
Phenol-d6
A
Solid
TCLP Semi-Volatiles Analysis (SW131118270)
p-TerphenyW14
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Solid
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroetbane
A
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Solid
TCLP Volatiles Analysis
Key
NC WW SCM A Accredited
NC WW SCM
U Unavailable
2-Butanone
4-Bromofluorobenzene
Benzene
Carbon tetrachloride
Chlorobenzene
Chloroform
Dibromofluoromethane
Tetrachloroetheno
Toluene-d8
Triehloroethene
Vinyl ebloride
A
A
A
A
A
A
A
A
A
A
A
Original #1
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Summit Environmental Technologies, Inc.
SUMMIlu 3310 Win St.
RNViRONMEMTALTECANOLOdiFS,mr, Cuyahoga Falls, Ohio44223 Sample Log -in Check List
Anolytrcal Lafaoraiories TEL: [phone] FAX: [phone]
Websile. hW--11www.settek,cow
Client Name: SYN-NC-27028 Work Order Number: 18020863 RcDtNo: 1
Logged by: Christopher Livengood
Completed By: Antonio Setscakos
Reviewed By: Jennifer Woolf
Chain of Custody
1. Were seals intact?
2. Is Chain of Custody complete?
3. How was the sample delivered?
Log In
4. Coolers are present?
5_ Was an attempt made to coal the samples?
211612018 1010:00 AM
211612018 314:33 PM
/r�
211912018 4:11:00 PM 0f %►�
Yes 0 No ❑ Not Present ❑
Yes 0 No ❑ Not Present ❑
FedEx
Yes 0 No ❑ NA ❑
Yes 0 No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C
7. Sample(s) in proper container(s)?
$. Sufficient sample volume for indicated tost(s)?
g. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 114 inch or. 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15, is it clear what analyses were requested?
16, Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handlino (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
Nol
NA ❑
Yes
❑
No ❑
yes
❑
No ❑
Yes
0
No ❑
Yes
❑
No ❑
NA ❑�
NA
Yes
❑
No ❑
No VOA Vials W1
Yes
❑
No -❑d
Yes
d❑
No ❑
Yes
W
No ❑
Yes
❑
No ❑
Yes
�/❑
No ❑
Yes ❑ No ❑ NA W
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No 1. Temp °C 1. Condition Seal Intact I Seal No I Seal hate Signed B
9 _ 4.1 � Good Not Present 1 _ ,T _
- — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — —
Page 1 of 1
Page 31 of 31

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Whiteville WQ Permit Number: W0000048
WWTP Name: Whiteville WWTP NPDES Number: NCO021920
Monitoring Period: From
01/01/2018 To 12/31/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if nnnlirahla fa alfarnnfivp nerfnrmed (Cinss S nr Class R) rmmnlefe fhe fnllnwinu mnnifnrina data --
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
24400
24800
25300
CFU/g
0
Once a
grab
9222D
CFU
year
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Newlvn McCullen Wastewater Treatment Plant Suuervisor
Preparer Name and Title (type or print)
Signature o reparer* �Dl
a
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date

Cameron Testing Services, inc. Laboratory Report
NC DFHNK#654
NC PH1H5 037799
US EPA #NC01918
}� I
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Whiteville WVYTP
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Yes
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Sample Information
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unfirrr[ C 733t} �cliresfi`kaiurontaling.vira

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Date
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Time
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SECTION 6

Agricultural Lime Application Log
2018
Project: Whiteville
Field
(state -county -site -field)
Grower
Moil
Lime Requirement
(from soil analysis) 11
Tons/Acre
Applied
Date
JApplied
NC-CO-108-1
Woodus Hayes
6.5
O.OTIAC
0.0
NIA
NC-CO-108-4
Woodus Hayes
6.7
O.OTIAC
0.0
NIA
NC-CO-110-1
Larry Mercer
6.0
O.OTIAC
0.6
NIA
* lime has been ordered but not spread

SECTION 7

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