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HomeMy WebLinkAboutWQ0006242_Residual Annual Report 2018_20190313INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0006242 SUBMITTAL DATED: 2/26/2019 Project Contact Information Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Lisa Finnerty Email Address* Ifinnerty@synagro.com Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0006242 Permittee * Facility Name * Town of Sparta Town of Sparta Phone Number* 4434899086 r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) Town of Sparta NC 2018 Annual Report.pdf 8.44MB Upload only 1 RDF docurrent. IVliltiple documents must be corrbined into one RDF file. For nein and modif cation permit applications, the paper copy is required to be submitted to the Di, risiom Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follm ging: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extras set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) This shall be mailed to the following address: By US_ Postal Service- Di,vision of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 27699-1617 By Courier, -Special Delivery: Division of Water Resources- Non -Discharge Branch Nathaniel Thornburg- 9th Floor, Office #942M 512 N_ Salisbury St_ Raleigh, NC 27644 For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov. *140 By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/26/2019 435 Williams Court, Suite 100 Baltimore, MD 21220 www.synagro.com FEBRUARY 22, 2019 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 276991617 Re: 2015 Annual Report for Permit No. WQ0006242 Dear NCDEQ: SYNAGRO Synagto is submitting one copy and one electronic copy of the above referenced report on behalf of the Town of Sparta, NC. If you have any questions or need additional information, please do not hesitate to contact Bryan Edwards at (336) 372-4257 or Erik Bruce at (336) 703-8681. Sincerely, Derrick Shivar Environmental Compliance Manager Enclosures cc: Bryan Edwards, Town of Sparta Erik Bruce, Synagro YOUR PARTNER FORA CLEANER, GREENER WORLD TOWN OF SPARTA, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0006242 2018 ANNUAL REPORT Town of Sparta, NC Residuals Land Application Program 2018 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms & Metals Field Loading Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM VQ Permit #: WO0006242 County Alleehany Year 2018 Facility Name (as shown on permit) Town of Sparta W WTP NPDES No. NC0026913 Land Application Operator Smaero Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A,. and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A—Residuals Application Summary: Total number of application fields in the permit: 11 Total number of fields utilized for land application during the year: 3 Total amount of dry tons applied during the year for all application sites: 40_01 Total number of acres utilized for land application during the year: 67.2 Part B —Aanual Comroliance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. I. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendm' year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T. I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15ANCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C —Cert ification: "I cert ify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. ] am aware that thereare significant penalties for submitting false infbrmafion, including the possibility of fines and imprisonment fox knowing violations." Bryan Edwards, Town Manager Permittee Name and Ti1ile typ or int) Signature of Pre} r Date if different from erminee) " gnature of Permittee Date Sign 'e - Date (if different fro ermr ee and P arer) *Preparer is defined in 40 CPR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC SPARTA,NC SPARTA, NC LIME STABILIZED LIQUID DRY METRIC MONTH/YEAR AMOUNT UNIT DRY TONS UNIT TONS April 2018 98,000.00 G 11.56 D 10.49 July 2018 932600.00 G 11.04 D 10.02 October 2018 147,600.00 G 17.41 D 15.80 YEARLY TOTAL 3391200.00 G 40.01 D 36.31 vzzizois SECTION 2 R O tq L C O a) N N m E E N L 0 m N N +L+ N 0 o N N � c C N C � O O C N O N 0 o E Q �N 0Q U N C Y0 E 0 O C N � Y C O N N aE E a Q O m 0 N 0 l d OJ m N a N� N N M O O Z M o ( H F O) d¢� Q 3 �U)Z T 0 L O N Y W N 67 o > E m Q dH d C rn� N � m mA .. ,Oi.. A Q m N y 'o W L � z Z T U) It a1 F E E Un W E E E c o m� a m �o LLN o M E ¢ y -o L 0 �6 o .`3 IF)S o Y E n.LLzo a) 6 ¢ N w a 0 oa LLQUUUJ�z(n N I-I-Qz ^ tD E � a 0 O O UO m O o N r 4 N � N � N U V � C G x N � J m E ry m m � a m o z ° a K m d O O N 9 a E = o m m � Z ?OFm � U c K V 'a Y � N o °u L C a 3g N b W N OJ °J W OJ W n N� N 0 0 � N 0 O O 0 M O o Qj O 0 � N � O U a O N o J � N � J m (O ry m m � a o o z c- m K m d O O a m U E = o m m � Z ?OFm z U K V d Y � N a °u � a 0 0 0 � N 0 O O 0 M O o W O 0 o rn W �F U O N o J N N � J (O ry m oU � a o o z c- m K m d O O m m U m = o m m N N ?OFm U K V d y P N 2 N b W N 0 0 0 � O 0 O O 0 M O o W O 0 o rn W �F O O O N N (O N O V � a o 0 m c- m v m d O O m m U m E C7 U N K � d v a 0 N Y K m wU) Y N m m m 0 0 0 0 0 0 0 0 0 o p o 0 0 0 o rn �F U Z Y a m O m m c- m m m m O O m m U m 7 C7 U o� 2 0 N b W N OJ °J W OJ W CO N� °J °J W 00 W W V N 0 0 N 0 O 0 0 0 0 0 0 0 0 0 O U z 0 V N fOD (OD (00 (00 (00 l00 cOo c00 (00 fOo t00 V N N n N m a V N N O N N O N N N N O O N N N N U Y K m wU) Y N m m m 0 0 0 0 0 0 0 0 0 o p o 0 0 0 o rn Y a m O m m c- m m m m O O m m m m o� o 0 0 b W N OJ °J W OJ W CO N� °J °J W 00 W W 0 0 N 0 0 0 0 0 0 0 0 0 0 0 O 0 0 0 V N N N N N N N N N N N N N N N N V N N O N N O N N N N O O N N N N N V V V 7 J O O O O O O O O O O O O O O O O Y K m wU) Y N m m m 0 0 0 0 0 0 0 0 0 o p o 0 0 0 o rn o O o 0 0 0 0 0 o p o m N M O 0 0 0 O N m m � 0 Z o Z « L y d m 0 E E d E z 'z m in Y o. m m E 'c m `m o� in m m o c E �' a s U) U in Q U F4 ¢ O z N 1O E O O 00 0 �s R M � d0'oC' a o 7 m N m R N � � o m c � c o N U ELL N « 0 ao c t O O a o T K N y a? m a i m 3 � 0 a c m 3 � n U a K Ra' C r 0 ON 0 0 a � N f N N r � a 3� �V v V) N n N 0 o O O 00 0 0 R M � d0'oC' a o 7 m N m R O n IL 0 N J � N U N U (O N m 0 ao U d O � Z o m K .. y a? m a m a E O 0 a � - Z Z Z U N K Ra' r 0 ON 0 0 V N f N N N � a O 0 o O O 00 0 0 R M � d0'oC' ro o 7 0 m m m d0' n U 0 N J N N U N U (O N m 0 0 U d O o Z o m K m d a? m eo m M O 0 a � - N Z m U N K Ra' ON ON V N f N N N N �V v V) N O 0 o O O 00 0 0 N M � d0'oC' ro o 7 0 m m m d0' n U 0 0 o N N U N U (O N O 0 0 d O O 0 o m m m d a? m eo m M 0 a N K Ra' ON ON V N I 0 0 o O o 00 O O N T d0'oC' V 7 m V O d0' n U U U U r U U N U 0 0 0 0 0 0 0 0 o m m m M M m eo m M ON ON V N N N N N N �V V) Q 0 0 o O o 00 O O N T d0'oC' V 7 V V [V d0' n m m m m cn mOf w m 0 0 0 0 0 0 0 0 o m m m M M m eo m M ON ON V N N N N N N �V 0 0 o O o 00 O O O O [V � n m m m m cn mOf w m 0 0 o O o 00 O O O O [V � � m �lJ M 6 � if> N � w oa LLa �En D oa aW w 'f) fr a w L7 2 zP: a NQ N 2 W a z oa z 0 U W J w as ar N UQ Q 0 0 1 u >=c� E/y 0 LU z Z g o I N N u U w oa LLa �En D oa aW w 'f) fr a w L7 2 zP: a NQ N 2 W a z oa z 0 U W J w as ar N UQ Q 0 0 1 W U Z p'� N N •- a 0 C W t a a ¢o W_ OJ Na ag Uy N n a N N a U m c ro E� E N = ttl C o E a= a¢ N C 0 o E t � o U)a L E o c •- m Z � � E -o = O 'U � U m �n � m N = .a a � J N � N O U) cn 0 0 1 U N N •- a -°o >N me Uv 2 a y d1 N W 7 � a 0 w � N cn a N J a a z a a z U U c az 0 0 O z - z O N W (l J a � 3 In Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2040-01-LSLIQ-NC SPARTA, NC LIME STABILIZED LIQUID 4/16/2018 1/1/2018-12/31/2018 0.1065 Na mg/I = (Na mg/kg x %Solids) = 100 = (993 x 2.8300) + 100 = 28.1019 Ca mg/I = (Ca mg/kg x %Solids) = 100 = (162000 x 2.8300) - 100 = 4584.6 Mg mg/I = (mg mg/kg x %Solids) * 100 = (14500 x 2.8300) + 100 = 410.35 Na meq = Na mg/I + Molec. Wgt. Na = 28.1019 + 23 = 1.22182 Ca meq = Ca mg/I + Molec.Wgt.Ca = 4584.6 - 20 = 229.23 Mg meq = Mg mg/I + Molec.Wgt.Mg = 410.35 - 12 = 34.1958 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.22182 + SgrRoot[0.5(229.23+34.1958)] = 0.106462 Printed: 1/23/2019 Page 1 14:18 0 w a 4 a a a o N q a 4 a o N o z z 4 Hew` u u ^� N FL N fG V 00000 0 0 a zzip U r N z o z a H 9 U � y 4 a 4 a a N o z 4 u u ^� N FL N fG V 00000 0 0 a zzip U r N 0 9 U � y 4 b 1y ri N N N N z�z 4 R R 4 q q O = Zv v d"d"v 4 4 40 04 o 0 N N N q = o 0 0 0 0 w H fL . q 9 n.� a5w W N ¢�z � N N iV -N h FiN V o 0 0 0 �rrrr 3 Q 'a�va, b� vi vai a a a a a °i v4, va,ti� a � .Q tl a o O i5 O o O m M N N N e m N N 41 F \ a 4 a a N o z ^� N o V a U r N 0 9 U � y 4 p q O = ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Sparta, NC Total Dry Tons Applied (Annual): Permit #: W00006242 Cation Exchange Capacity (non 503 only): Operator: Greg Wagoner Owner: Greg Wagoner Predominant Soil Series: Acres Used: 29.6 Acres Permitted: 29.6 Site #: NC AG 00005 Field #: 17.42 Chester AG 00005 0001 Residual Analysis Data (Heave Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date � 4/16/18 � 3 b 5 6 7 8 9 10 11 12 Solids 2.83 8 9 10 11 12 Arsenic 3 Cadmium 2 H Copper 459 Chromi 20.5 ° Lead 14.2 Mercury 0.4 m Molyb- denum 0.59 5 Nickel 17.6 .. Arsenic Selenimn 5 0.000 0.000 0.000 0.000 0.000 0.000 Zinc 430 0.000 0.000 0.000 0.000 0.004 Cadmium Total Phos- horus 9900 0.000 0.000 0.000 0.000 0.000 0.000 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total � 2 3 4 5 6 7 8 9 10 11 12 H DT/Ac./ ° APP m Event 0.59 .. Arsenic 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.540 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.540 Chromiu 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 Lead 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 denum Nickel 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Selenium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Zinc 0.506 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.506 Total Phos- 11.642 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 11.642 horus "I certify, under penalty of ►ave, that this document was prepared under my directton or superv�ston m accuruance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1� Signature of La d Applier �°l P �I � i � � Date DENR FORM MFLSF (12/2006) I N m a a d Q A N m a z w w Wa Ww x V w w w P � U Cli ry zU U N 0. U Q a a n n p 0 z�z q� 6 U nnna pA z aaa� a a N N N N m m m m O N � o yP4 o oo SOY,, Q v � d N [V N cV 6 N �aax 3 r s r y Q Q '� v vai vai vai ro ti 0 0. h va W ti Z o w ii F W Q 0 0 0 y U e O N d o ^' ^ M u y W 00 H 03 O NQ1QQ Q� N m a z x V M P � U Cli ry U N U p 0 o q� 6 U N m ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this farm to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Sparta, NC Total Dry Tons Applied (Annual): 11.05 4 Permit #: W00006242 Cation Exchange Capacity (non 503 only): 7 Operator: Ronny Edwards Owner: Ronny Edwards Predominant Soil Series: Hayesville 12 Acres Used: 25.7 Acres Permitted: 25.7 Site #: NC AG 00008 Field #: AG 00008 0001 9 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample Or Com- posite Date � 4/16/18 � 3 4 5 6 7 8 9 10 11 12 Solids 2.83 8 9 10 11 12 Arsenic 3 Cadmium 2 y Copper 459 Chromim 20.5 �°+ Lead 14.2 Mercury 0.4 w Molyb- denum 5 Nickel 17.6 .. Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 430 0.000 0.000 0.000 0.000 0.000 0.003 Total Phos- horus 9900 0.000 0.000 0.000 0.000 0.000 Annual Heavy Metal Field Loadines (Calculated in lbs/acre): Total � 2 3 4 5 6 7 8 9 10 11 12 y DT/Aa/ �°+ APP w Event 0.43 .. Arsenic 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.395 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.395 Chromiw 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Lead 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.Ol2 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 denum Nickel 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 Selenium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Zinc 0.370 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.370 Total Phos- 8.514 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.514 horus "I certify, under penalty of law, that this document was prepared under my direction or superv�ston m accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". � / l Signature of Land er � 'nate DENR FORM MFLSF (12/2006) F Y N �d C� a N a x d U U U 0 Q T W vi Q F Y N �d C� N x U U U 0 Q N W vi W W oo,C) cj w w 3 z o O Q Ey w 7dy E W w a O F Y N �d N U U U 0 � O W W W cj w w w V 7dy E 0...i ti .. vC5 6 S N b U .z a#a N N N � o d V [V N N �w`Rx a ay d n 'L` o " •�• o ren Qt�wd � M 43 N C7 a G �= t? 0 0 F oao a3 �o mm F Y N �d N 0 � O 0 V 0 0 vC5 6 U ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Sparta, NC Total Dry Tons Applied (Annual): 11.57 Permit #: WQ0006242 Cation Exchange Capacity (non 503 only): Operator: Ronny Edwards Owner: Ronny Edwards Predominant Soil Series: Hayesville Acres Used: 11.9 Acres Permitted: 11.9 Site #: NC AG 00008 Field #: AG 00008 0002 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Data 1 4/16/18 2 3j 4 5 6j 7 8 _Wj 10 1_L1_j 12 % Solids 2.83 8 9 10 11 12 Arsenic 3 Cadmiuml 2 H Copper 459 Chromium 20.5 Lead 14.2 Mercury 0.4 y Molyb- denum 5 Nickel 17.6 Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 430 0.000 0.000 0.000 0.000 0.000 0.006 Total Phos- horus 9900 0.000 0.000 0.000 0.000 0.000 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 H DT/Ac,/ App, y Event 0.97 Arsenic 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.892 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.892 Chromirml 0.040 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.040 Lead 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 denum Nickel 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Selenium 0.010 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 1 0.000 0.000 0.010 Zinc 1 0.836 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.836 Total Phos- 19.246 0.000 0.000 0.0000.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 19.246 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of LLan pplier Date SECTION 4 Tyoummil ENVIRONMENTAL TECNNOLO"S'"r 1NC AnxtyWat Laboratories March 06, 2018 Erik Bruce Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336)998-7150 FAX: (336) 998-8450 RE: Yadkinville WWTP Dear Erik Bruce: S Mout Envu onnienlal Tra nologies, Inc. 3310 Win Sl. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489 Websit : hhiho v n senekconn Order No.: 18010570 Smnmit Environmental Technologies, Inc, received 1 samples) on 1/12/2018 fox the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel fr ee to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 07256CA, Colorado, Cormecticu[PH-0108, Delaware, Florida NELAC E87G88, GeorLna E87688, Idaho OH00923, Illino's 20006 1, Indimra C -0H-13, Kansas E-10347, Kentucky (Underground StomeeTank) 3, Kentucky 90146, Lowsiane 04061, Maryland 339, Minnesota r A0971 I, New Hampshae 2996, New Jersey OHOOG New York 11777, North Caro]ina 39705 and 631, Noah Dakota R-201, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA00037 7, South Carolina 92016001, Texas 7104704466-11-5, Utah OH009232011-I, Virginia VELAP 9456, Washington C891 Page 1 of 13 SUMMIT summit Environmental Techno,ogies, Inc.ffl 3310 Win St. Case Narrative rNVIRONRIENTALTECNNOLOGIES,+NC. Cuyahoga Falls, Ohio 44223 WO#; 18010570 AnaYyOral Laborafuries - TEL: (330) 253-8211 FAX: (330) 253-4489 Website: hatto //wwivsettek com Date: 3/6/2018 CLIENT: Synagro Project: Yadkinville WWTP WorkOrder Narrative: 18010570: This report in its entirety consists ofthe following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report; Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on Lite reporting units. This report is believed to meet all of the. requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 18010570-001 a tclp-svoc-cpest tclp(8081): The Pesticide MS and MSD pair exhibited high RPDs for all analytes of interest; Recoveries were within acceptance limits for all analytes individually in both the MS and the MSD. Analytical Sequence QC Notes: 18010570-OOlams tclp-svoc-cpest tclp(8081): The Pesticide MS and MSD pair exhibited high RPDs for all analytes of interest; Recoveries were within acceptance limits for all analytes individually in both the MS and the MSD. 18010570-001amsd tclp-svoc-cpest_telp(8081): The Pesticide MS and MSD pair exhibited high BPDs Original Page 2 of 13 91 SU IT SummaEnvonm ,arT hnooge,Tc. Case Narrative 3310 Win St. MVIRONMENTAL IECONOLGGIES, iNC- Cuyahoga Falls, Ohio 44223 WOE: 18010570 Apitytcal Laborainrles TEL: (330) 253-8211 FAX: (330) 253-4489 Date: 3/6/2018 Website:M lAviv,vsette&com CLIENT: Synagro Project: Yadkinville WWTP for all analytes of interest, Recoveries were within acceptance limits for all analytes individually in both the MS and the MSD. Original Page 3 of 13 u ill Summit Environmental Technologies, In Qualifiers and Acronyms prS33/0 Win FrWINONiAENTALI£CANOLOGIES, INC Cuyahoga Falls, Ohio 44Z WO#: 18010570 ArrafyHaal Laboratories TEL: (330) 253-8211 FLY: (330) 253-445 Date: 3/6/2018 Website.' It lip LAviru1 settekco These commonly used Qualifiers aad Acronyms may or may not lie present in thisaeport Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. I The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the Inxear range of the calibration or is estimated due to interference, MC The result is below the Minimum Compound Limit. s The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confirmed when GC/MS Analysis was performed. BIMB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CC V recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+), QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample. LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MhaCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in th.e Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding theuse of these Qualifiers on reported data. Original Page 4 of 13 SUMMIT UIT Summit Enriranmental Technologies, St. yr Oil�Oi�UCT 331010 Win St. MVIRONMENTAL 7 ECHNOLOGIrS, n1c Cuyahoga Falls, Ohio 44223 Sample Summary Anaipfical Laboratories TEL: (330) 253-8211 FAX,' (330) 253-4489 WO#: 18010570 Webslle: ham./hvivw settekconi 06-Mar-18 CLIENT:. Synagro Project: YadkinvilleWWTP Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 18010570-001 Sparta W WTP 1/10/2018 9:00:00 AM 1/12/2018 12:20:00 PM Solid Page 5 of 13 s '.l summit Ehvironmen[al Techfio%Win St. Analytical Report 33100 Win St. ffl £PlvIRONMEMTAL 7£CNNOL0C31E5, iPtL Cuyahoga Falls, Ohio 44223 (base report) Anafyflraf LaborsaMes TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18010570 Webmre: htto'//vi [[ek eom Date Report ed: 3/6/2018 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 1/10/2018 9:00:00 AM Lab ED: 18010570-001A Project: YadkinvilleWWTP Client Sample ID Sparta W WTP Analyses Qualifiers: Result RL Qual Unite DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: EAM TCLP MERCURY ANALYSIS (SW131117470) TCLP Mercury NO 0.00200 mg/L 1 1/18/201811:10:00 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: KMS TCLP METALS ANALYSIS (SW131116010) TCLP Arsenic(As) ND 0.500 mg/L 1 1/17/20181:19:00 PM TCLP Barium(Ba). ND 5.00 mg/L 1 1/17/2018 1:19:00 PM TCLP Cadmium(Cd) NO 0.100 mg/L 1 1/17/2018 1:19:00 PM TCLP Chromium(Cr) NO 0.200 mg/L 1 1/17/2018 1:19:00 PM TCLP Lead(Pb) NO 0.500 mg/L 1 1/17/2018 1:19:00 PM TCLP Selenium(Se) NO 0.0500 mg/L 1 1/17/2018 1:19:00 PM TCLP Silver(Ag) NO 0.500 mg1L 1 1/17/2018 1:19:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW3510C Analyst: BJH TCLP SEMI -VOLATILES ANALYSIS (SW131118270) 1,4 -Dichlorobenzene NO 0.200 mg/L 2 1/18/201811:19:00 AM 2,4,5 -Trichlorophenol NO 0.500 mg/L 2 1/18/2018 11:19:00 AM 2,4,6 -Trichlorophenol NO 0.500 mg/L 2 1118/201811:19:00 AM 2,4-Dinitrotoluene NO 0.100 mg1L 2 1/181201811:19:00 AM o -Cresol ND 0.500 mg/L 2 1/18/2018 11:19:00 AM m/p-Cresol(s) NO 0.500 mg/L 2 1/18/2018 11:19:00 AM Cresols, Total NO 10.0 mg/L 2 1/18/201811:19:00 AM Hexachloro-1,3-butadiene NO 0.0400 mg1L 2 1/181201811:19:00 AM Hexachlorobenzene ND 0.100 mg/L 2 1/18/2018 11:19:00 AM Hexachloroethane ND 0.200 mg/L 2 1/18/201811:19:00 AM Nitrobenzene NO 0.200 mg/L 2 1/181201811:19:00 AM Pentachlorophenol NO 0.500 mg/L 2 1/18/2018 11:19:00 AM Pyridine ND 0.500 mg/L 2 1/18/201811:19:00 AM Surr: 2-Fluorophenol 29.4 10-109 %Rec 2 1/18/2018 11:19:00 AM Surr: Phenol -d6 14.1 10-109 %Rec 2 1/18/2018 11:19:00 AM Surr: Nitrobenzene -d5 52.0 19- 120 %Rec 2 1/18/2018 11:19:00 AM Surr: 2,4,6-Tribromophenol 34.9 10-120 %Rec 2 1/18/2018 11:19:00 AM Surr: 2-Fluorobiphenyl 54.8 22-117 %Rec 2 1/18/2018 11:19:00 AM * Value exceeds Maximum Contaminant Levet. H E Value above quantitation range Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits N Tentatively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 7 of 13 NV AMM1 � son,miLEnvhornnenralTechno33/100Win SStl. l. Analytical Report fNVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report) Arralyfical Laboreiories TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 18010570 Website: him lhvw,v setrek.cam Date Reported: 3/6/2018 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 1/10/2018 9:00:00 AM Lab ED: 18010570-OOIA Project: Yadkinville WWTP Client Sample ID Sparta W WTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270D SW3510C Analyst: BJH TCLP SEMI-VOLATILES ANALYSIS (SW131118270) Surr: p-Terphenyl-dl4 55.0 34-116 %Rec 2 1/18/2018 11:19:00 AM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: JBN TCLP PESTICIDES ANALYSIS (SWI311/8081) Chlordane, total ND 0.0100 mg/L 1 1/17/2018 5:58:00 PM Toxaphene ND 0.0200 mg/L 1 1/17/2018 5:58:00 PM Endrin ND 0.00100 mg/L 1 1/17/2018 5:58:00 PM gamma-BHC ND 0.00100 mg/L 1 1/17/20185:58:00 PM Heptachlor ND 0.001.00 mg/L 1 1/17/2018 5:58:00 PM Heptachlor epoxide ND 0.00100 mg/L 1 1/17/2018 5:58:00 PM Methoxychlor ND 0.00100 mg/L 1 1/17/2018 5:58:00 PM Sun': TCMX 55.2 10-119 % Rec 1 1/17/2018 5:58:00 PM Sun': DCB 39.0 10-119 % Rec 1 1/17/2018 5:58:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8151A SW8161A Analyst: JBN TCLP HERBICIDES ANALYSIS (SW131118151) 254-D ND 1.01) mg/L 1 1/23/2018 5:55:00 PM 2,415-TP ND 0,500 mg/L 1 1123/20185:55:00 PM Surr: DCAA 111 20-140 % Rec 1 1/23/2018 5:55:00 PM NOTES: Sample's Prep Method hold time was exceeded by 2 days. TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8260B SW1311M Analyst: CTB TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 0.0500 mg/L 10 1/17/2018 4:38:00 PM 1,2-Dichieroethane ND 0.0500 mg/L 10 1/17/2018 4:38:00 PM MEK ND 0.250 mg/L 10 1/17120184:38:00 PM Benzene ND 0.0500 mg/L 10 1/17/2018 4:38:00 PM Carbon tetrachloride ND 0.0500 mg/L 10 1/17/2018 4:38:00 PM Chlorobenzene ND 0.0500 mg/L 10 1/17/20184:38:00 PM Chloroform ND 0.0500 mg/L 10 1/17120184:38:00 PM Tetrachlomethene ND 0.0500 mg/L 10 1/17/2018 4:38:00 PM QAAltfiars: 4 Value exceeds above quantitation range Maximum Contaminant Leval. H Holding times Por preparation or analysis exceeded MG Value is below Minimum Compound Limit ND Nat Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value M Manual Integration used to determine area response N Tentatively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 8 of 13 u int Summit En,hronnenra/Technor10Wi S1. Ana lyticalReport 3310 Win 23 rNVIROMMENTAL I ECHNO LOG I E5, SNC Cuyahoga Falls, Ohio 44223 (base report) AnalpHcal LabarnforW.t+ TEL: (330) 253-6211 FAX., (330) 253-4489 WO#: 18010570 Webote: htm llawipserrekcc Date Reported: 3/6/2018 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 1/10/2018 9:00:00 AM Lab ID: 18010570-OOIA Project: Yadkinville WWTP Client Sample ID Sparta WWTP Analyses Result TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP VOLATILES ANALYSIS Trichloroethene ND Vinyl chloride ND Surr: 4-8romofluorobenzene 96.4 Surr: Dibromofluoromethane 109 Surr: Toluene -d8 105 RCI -SOLID -W/ IGNITABILITY7 030 REACTIVE CYANIDE (901417,3.3.2) -SOLID Cyanide, Reactive ND RL Qual Units DF Date Analyzed SW8260B SW1311M Analyst: CTB 0.0500 mg/L 10 1/17/20184:38:00 PM 0.0200 mg/L 10 1/17/20184:38:00 PM 70 -130 % Rea 10 1/17/2018 4:38:00 PM 70 -130 %Rea 10 1117/2018 4:38:00 PM 70 - 130 %Rec 10 1/17/2018 4:38:00 PM SW9014 Analyst: MS 0.500 mg/Kg 1 1/19/20184:48:00 PM RCI -SOLID -WI IGNITABILITY1030 SW1030 Analyst: AJT IGNITABILITY OF SOLIDS (SW -846: 1030) Ignitability non-flammable 1 1/25/2018 1:00:00 PM RCI -SOLID -WI IGNITABILITY1030 SW9045D Analyst: DHC PH (SW9045D) pry 7.4 s.u.@18.6C 1 1/17/201811:56:00 AM RCI -SOLID -W/ IGNITABILITY1030 SW9034 Analyst: MS REACTIVE SULFIDE (9034)17.3.42 Sulfide., Reactive ND 25.0 mg/Kg 1 1/19/20184:48:00 PM QnaliOers: � Value exceeds.Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compowrd Linrit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area response N Tentatively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 9 of 13 3 u sa am tEavr onn e, a Technologies, Inc. Accreditation Program 3310 Winst. Analytes Y Report rNVIRONWEN'rdL IECHNOL=E5, INC Cuyahoga Falls, Ohio 44223 Analyfirat Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18010570 Website: htm./Avroiv seltelr. coni 06 -Mar -18 Client: Synagro State: NW Project: YadkinvilleWWTP Program Name: NC—WW—SCM Sample ID Matrix Tes[ Name Analy[e Status Key Key 18010570-OOIA Solid Ignitability of Solids (SW -846:1030) Ignitabihty A Solid PH (SW9045D) Hydrogen Ion (plf) A Solid Reactive Cyanide (901417.3.3.2) -Solid Cyanide, Reactive U Solid Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U Solid TCLP Herbicides Analysis (SWI 311/8151) 23425 -TP A Solid TCLP Herbicides Analysis (SW1311/8151) 2,4-13 A Solid TCLP Herbicides Analysis (SW1311/8 15 1) DCAA A Solid TCLP Mercury Analysis(SW1311/7470) Mercury A Solid TCLP Metals Analysis (SW 1311/6010) Arsenic A Solid TCLP Metals Analysis(SW1311/6010) Barium A Solid TCLP Metals Analysis(SW1311/6010) Cadmium A Solid TCLP Metals Analysis (SW 1311/6010) Chromium A Solid TCLP Metals Analysis(SW1311/6010) Lead A Solid TCLP Metals Analysis(SW1311/6010) Selenium A Solid TCLP Metals Analysis(SW1311/6010) Silver A Solid TCLP Pesticides Analysis (SW1311/808 1) 2,2',3,3',4,4',5,5',6,6'- A Key Key Decachlorobiphenyl Solid TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A Solid TCLP Pesticides Analysis (SW1311/8081) Endrin A Solid TCLP Pesticides Analysis (SW 1311/8081) gamma -BHC A Selid TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Solid TCLP Pesticides Analysis(SW1311/808.1) Heptachlor epoxide A Solid TCLP Pesticides Analysis (SW1311/808 1) Methoxychlor A Solid TCLP Pesticides Analysis (SWI 311/8081) Tetrachloro-m-xylene A Solid TCLP Pesticides Analysis (SW1311/808 1) Toxaphene A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) 1,4 -Dichlorobenzene A .Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,5 -Trichlorophenol A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,6-Tribromophenol A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) 2,4,6 -Trichlorophenol A Solid TCLP Semi -Volatiles Analysis (SW 1311/8270) 2,4-13initiotoluene A 6olid TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Fluorohiphenyl A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Fluorophenol A Original #1 Page 10 of 13 NC WW SCM A Accredited NG WW SCM U Unavailable Original #1 Page 10 of 13 SUMMIT Suamnt En,aronmental TechnologtesJnc. Accreditation Program 3310 Win St. Analytes Report mi CNVIHONhIENTAL TECHNOLOGIES, INC Cuyahoga Falls,. Ohio 44223 Y 11 AresIyMcal Laboratories TEL: (330) 2534211 FAX (330) 253-4489 WO#: 18010570 Website: hap'Anvm.setrekcom O&Mar48 Client: Synagro State: NW Project: YadkinvilleWWTP Program Name: NC_WW_SCM Sample ID Matrix Test Name Analyte Status 18010570-OOIA Solid TCLP Semi -Volatiles Analysis (SW1311/8270) 2-Methylphenol A Solid TCLP Semi -Volatiles Analysis(SWl 3l 1/8270) 3,4-Methylphenol A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Cresols, Total A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobenzene A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachloroethane A Solid TCLP Semi -Volatiles Analysis (SWI311/8270) Nitrobenzene A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Nitrobenzene -d5 A -Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Pentachlorophenol A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Phenol -d6 A Solid TCLP Semi -Volatiles Analysis (SW 1311/8770) p-Terphenyl-d14 A Solid TCLP Semi -Volatiles Analysis (SW 1311/8270) Pyridine A Solid. TCLP Volatiles Analysis 1„ 1-Dichloroethene A Solid TCLP Volatiles Analysis 1,2-Dichloroethane A Solid TCLP Volatiles Analysis 2-Butanone A Solid TCLP Volatiles Analysis 4-Bromofluorobemmne A Solid TCLP Volatiles Analysis Benzene A Solid TCLP Volatiles Analysis Carbon tetrachloride A Solid TCLP Volatiles Analysis Chlorobenzene A Solid TCLP Volatiles Analysis Chloroform A Solid TCLP Volatiles Analysis Dibromofluoromethane A Solid TCLP Volatiles Analysis Tetracbloroethene A Solid TCLP Volatiles Analysis Toluene -d8 A Solid TCLP Volatiles Analysis Trichloroethene A Solid TCLP Volatiles Analysis Vinyl chloride A NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Original #1 Page 11 of 13 M O N SUMMIT UMMI Summit Environmental Technologies, W Inc. 3310 Win St. rNVIRONMENTAL1aCHNOLOGISS,vNC- Cuyahoga Falls, Ohio 44223 Sample Log -In Check List Analytical Laboratories TEL: (330) 253-8211 FAX (330) 253-4489 Website: Nita /Avivmsettekcom Client Name: SYN -NC -27028 Work Order Number: 18010570 RcptNo: 1 Logged by: Antonio Betscakos 1/12/2018 12:20:00 PM 4� �"- `. Completed By: Antonio Betscakos 1/15/2018 2:33:08 PM.�- r i� Reviewed By: Chain of Custody 1. Is Chain of Custody complete? Yes ❑ No ❑ Not Present ❑ 2. How was the sample delivered? FedEx Loa In 3, Coolers are present? Yes J❑ No ❑ NA ❑ 4, Shipping container/cooler in good condition? Yes No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present fv� No, Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes © No ❑ NA ❑ 6. Were all samples received at a temperature of >0° C to 6.0°C Yes � No ❑ NA ❑ 7, Samples) in proper container(s)? Yes 0 No ❑ g, Sufficient sample volume for indicated test(s)? Yes 0 No ❑ g. Are samples (except VOA and ONG) properly preserved? Yes No ❑ 1 D. Was preservative added to bottles? Yes ❑ No ❑ NA NA 11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials 0. 12. Were any sample containers received broken? Yes ❑ No V] 13. Does paperwork match bottle labels? Yes No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes No ❑ 15. Is it clear what analyses were requested? Yes No ❑ 16. Were all holding times able to be met? Yes No ❑ (If no, notify customer for authorization.) Special Handling (if applicable) 17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA W Person Notified: ��i Date li By Whom: Via: ❑ eMail ❑Phone [] Fax ❑ In Person Regarding: Client Instructions: 18, Additional remarks: Cooler Information ECoolerNo Temp °C Condition Seal Intact Seal No Seal Date Signed By 1 4.5 Good Not Present Page 13 of 13 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Sparta WQ Permit Number: WQ 0006242 WWTP Name: Town of Sparta WWTP NPDES Number: NC 0026913 Monitoring Period: From 01/01/18 To 12/31/2018 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray _ Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens x If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting _ Aerobic Digestion Anaerobic Digestion If applicable to alternative erformed Class A or Class B complete the immwm monitoring cars: Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 OptiowAlt.3 Option/Alt.4 (V S reduction) (40 -day bench) (30 -day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt 8 (14 -Day Aerobic) (Alk Stabilization) x (Drying—Stable) (Drying—Unstable) Option/Alt 9 Option/Alt. 10 (Injection) (Incorporation) _ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/ISANCAC 02T.1107 have been met" "I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector athaction reduction requirement in 40 CFR 503.33/15ANCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. 1 am aware that there are significant penalties for false certification including fine and imprisonment" Todd Lar son, O erations Dir for Preparer N Yi ipe L 11 Signature of Preer* atc( D Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15ANCAC 2T.1102 (26) Date Frequenof cy Sample Type Analytical Technique Parameter Allowable Level in Sludge Pathogen Density ExceNo. e- Minimum Geo. Mean Maximum Units dentes Analysis Fecal 2x10 tothe 6a MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 OptiowAlt.3 Option/Alt.4 (V S reduction) (40 -day bench) (30 -day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt 8 (14 -Day Aerobic) (Alk Stabilization) x (Drying—Stable) (Drying—Unstable) Option/Alt 9 Option/Alt. 10 (Injection) (Incorporation) _ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/ISANCAC 02T.1107 have been met" "I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector athaction reduction requirement in 40 CFR 503.33/15ANCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) 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