NCS000329_Monitoring Reports_20181212

I A
#; Or AT I
November 28, 2018
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
RECEIVED
DEC 12 2018
CENDAL F11 ES
%:",VVR SECT16;N1 f(AR-0
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Attached, please find stormwater monitoring data for Permit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
I Start
End
Year 9 — Period 2
18
I September 1, 2018
February 28, 2018
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
Sc yan
Environmental Manager

f- A-T-1 AlIvac -A#A
9- a- le Date:
Scruple Loc&flaa:
Perg'Gn c0edring Samples:
MI-vae - Bakers. Plant
stol'alwater Monitoring Re J�Lqrt F (0 1 qI
Storm —water Discharee Outfall #0 1 (Con=* aaled)
Drainage Area. = 1915A70s . ft. = 69 acres
% Impervious = 34%
ME I- �41�
40 CFR Part i 36
Parameter
Results (mg/1)
Benchmm-k Values (fag/l)
BOO
AM
30
COD
I.?. /
120
TSS
16, IV
100
Cadmium
NP
0.001
Chromium, total recoverable
NP
I
Copper, total recoverable
to-oys-
0.007
Nickel, total recoverable
0.00.5-
0.26
Zinc, total recoverable
•
0.067
Oil and Grease
20
Temp (receiving stream)
(deg Q
32 (deg C)
Total Residual Chlorine
0.017
pH
(std units)
6-9 (std units)
Rona Date:. Storms Ba.-F&-tion: -T- I' (ors.) Inches of Rainfrail:
Duration of dmi e preceding r&kp evemt ex:eeedLng 0.111: /U (I-Irs.)
Estimated Flow C&Eculadaa:
Q = CIA
Q(Total) = Q(Perviou-s Area) + Q(Irnperviaus Area),
Q(tot., efs) = (A x inches rdn,/12 inches/ft. x 69, acres x.66) +-9 x inches ran/12inchlesffir. ir 69 x,34)
Q(T otall, cfs) = 1.5180 x /. R (Iin-clues of rafti) + 1.7595 x AS (Lonches of rain-)

aceAnalytical
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November 14, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
AC�O
REPORT OF LABORATORY ANALYSIS
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Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification lDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification lDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #• 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNFL AP Certification #• 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SW OUTFALL 901(B)
92405880
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92406880001
BSW01
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
92405880002
BSW01
EPA 1664B
JMS
1
PASI-C
92405880003
BSW01
SM 5220D-2011
GC
1
PASI-A
92405880004
BSW01
SM 521OB-2011
SMK
1
PASI-A
92406880005
BSW01
SM 2540D-2011
CEH
1
PASI-A
92405880006
BSW01
SM 4500-01 G-2011
MDW
1
PASI-A
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Sample: BSW01 Lab ID: 92405880001 Collected: 11/05/18 06:21 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND
ug/L
1.0
1
11/06/18 05:44
11/08/18 23:46
7440-43-9
Chromium
ND
ug/L
5.0
1
11/06/18 05:44
11/08/18 23:46
7440-47-3
Copper
45.2
ug/L
5.0
1
11/06/18 05:44
11/08/18 23:46
7440-50-8
Nickel
6.1
ug/L
5.0
1
11/06/1805:44
11/08/18 23:46
7440-02-0
Zinc
12.7
ug/L
10.0
1
11/06/1805:44
11/08/18 23:46
7440-66-6
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW01 Lab ID: 92405880002 Collected: 11/05/18 06:19 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
Field Data
Collected By
Collected Date
Collected Time
pH
Temperature
I IEM, UII and Grease
Oil and Grease
Date: 11/14/2018 04:06 PM
Analytical Method:
DPJ
11/05/18
06:14
6.8 Std. Units
16.1 deg C
Analytical Method. E11A 1664B
ND mg/L
1
11/05/18 06:21
1
11/05/18 06:21
1
11/05/18 06:21
0.10 1
11/05/18 06:21
0.50 1
11/05/18 06:21
4.8 1
11/14/18 06:03
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Sample: BSW01 Lab ID: 92406880003 Collected: 11/05/18 06:18 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand 33.1 mg/L 25.0 1 11/08/18 19:11 11/09/18 00:07
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Sample: BSW01 Lab ID: 92405880004 Collected: 11/05/18 06:17 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210E BOD, 5 day Analytical Method: SM 521 OB-2011
BOD, 5 day ND mg/L 2.0 1 11/06/18 19:07 11/11/18 13:37 133
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Sample: BSW01 Lab ID: 92405880005 Collected: 11/05/18 06:15 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D-2011
Total Suspended Solids 16.4 mg/L 5.0 1 11/08/18 00:47 D6
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ANALYTICAL RESULTS
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW01 Lab ID: 92405880006 Collected: 11/05/18 06:22 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.045 mg/L 0.024 1 11/07/18 18:21 7782-50-5 H3
Date: 11/14/2018 04:06 PM
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
QC Batch: 442144 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92405880002
METHOD BLANK: 2427246
Associated Lab Samples: 92405880002
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE. 2427247
Parameter Units
Oil and Grease mg/L
MATRIX SPIKE SAMPLE:
Parameter
2427248
Units
Oil and Grease
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 4.8 11/14/18 04:51
Spike LCS
Conc. Result
38.5 36.8
92405492004 Spike
Result Conc.
ND 38.5
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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LCS
% Rec
% Rec
Limits
Qualifiers
96
78-114
MS
MS
% Rec
Result
% Rec
Limits Qualifiers
39.0
101
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
QC Batch: 440463 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92405880001
METHOD BLANK: 2419374
Matrix: Water
Associated Lab Samples: 92405880001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
11/08/18 23:12
Rhromium
up/L
ND
F 0
11/08/18 23.12
Copper
ug/L
ND
5.0
11/08/18 23.12
Nickel
ug/L
ND
5.0
11/08/18 23:12
Zinc
ug/L
ND
10.0
11/08/18 23:12
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2419375
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
480
96
85-115
Chromium
ug/L
500
484
97
85-115
Copper
ug/L
500
499
100
85-115
Nickel
ug/L
500
478
96
85-115
Zinc
ug/L
500
467
93
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2419376
2419377
MS
MSD
92405896001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
503
500
101
100
70-130
1
Chromium
ug/L
ND
500
500
506
504
101
100
70-130
0
Copper
ug/L
0.0053
500
500
521
519
103
103
70-130
0
mg/L
Nickel
ug/L
ND
500
500
493
490
98
97
70-130
1
Zinc
ug/L
0.011
500
500
502
499
98
98
70-130
1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2419378
2419379
MS
MSD
92405904001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD
Qua[
Cadmium
ug/L
ND
500
500
498
501
100
100
70-130
1
Chromium
ug/L
ND
500
500
503
504
101
101
70-130
0
Copper
ug/L
ND
500
500
510
514
102
103
70-130
1
Nickel
ug/L
ND
500
500
490
494
98
98
70-130
1
Zinc
ug/L
0.014
500
500
497
499
97
97
70-130
0
mg/L
Results presented on this page are in
the units indicated by the
'Units" column except where an alternate unit is presented
to the right
of the result
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
QC Batch: 440996 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92405880005
METHOD BLANK: 2421944
Associated Lab Samples: 92405880005
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE:
Parameter
2421945
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2421946
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2421947
Parameter
Units
Total Suspended Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 11/08/18 00:38
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 244 98 90-110
92405900003 Dup
Result Result RPD Qualifiers
27.8 31.0 11 D6
92405880005 Dup
Result Result RPD Qualifiers
16.4 18.2 10 D6
Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the right of the result
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QUALITY CONTROL DATA
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
QC Batch: 440961 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92405880006
METHOD BLANK: 2421856
Associated Lab Samples: 92405880006
Parameter Units
Chlorine, Total Residual mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 11/07/1818:16
SAMPLE DUPLICATE: 2421857
92405880006 Dup
Parameter Units Result Result
Chlorine, Total Residual mg/L 0.045 0.041
RPD Qualifiers
9 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SWOUTFALL#01(B)
Pace Project No.: 92405880
QC Batch: 440600
Analysis Method:
SM 521 OB-2011
QC Batch Method: SM 521 OB-2011
Analysis Description:
5210E BOD, 5 day
Associated Lab Samples: 92405880004
METHOD BLANK: 2420066
Matrix: Water
Associated Lab Samples: 92405880004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mg/L
ND
2.0 11/11/18 13:26 63
LABORATORY CONTROL SAMPLE: 2420067
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 192
97 84.6-115 B3
SAMPLE DUPLICATE: 2420068
92405881001 Dup
Parameter
Units
Result Result
RPD Qualifiers
BOD, 5 day
mg/L
ND
ND B3
Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result
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QUALITY CONTROL DATA
Project: SW OUTFALL#01(B)
Pace Project No.: 92405880
QC Batch: 441148 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92405880003
METHOD BLANK: 2422559
Associated Lab Samples: 92405880003
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Uuallflers
ND 25.0 11/09/18 00:04
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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LABORATORY CONTROL SAMPLE: 2422560
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 757 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422561 2422562
MS MSD
92406236003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 107 100 100 216 216 109 109 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422563 2422564
MS MSD
92405876001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 100 100 130 133 113 116 90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SW OUTFALL #01(B)
Pace Project No.: 92405880
Lab ID
92405880002
92405880002
92405880001
92405880006
92405880006
92405880004
92405880003
Sample ID
BSW01
BSW01
BSW01
BSW01
BSW01
BSW01
BSW01
Date: 11/14/2018 04:06 PM
Pace Analytical Services, LLC
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Analytical
QC Batch Method QC Batch Analytical Method Batch
EPA1664B 442144
EPA 200.7 Rev 4.4 1994 440463
SM 254OD-2011 440996
SM 4500-CI G-2011 440961
SM 5210F1 2011 440600
SM 5220D-2011 441148
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 200.7 Rev 4.4 1994 440492
SM 621OR 2011 440712
SM 5220D-2011 441293
Page 17 of 20

Ana�Y+l�,t al
Document Name:
Sample Condition Upon Receipt(SOUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev,06
issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
_� •" Client Name:
i
Courier: [—]Fed Ex ❑UPS ❑USPS
❑ Commercial ❑Pace ❑Other:
Custody Seal Present? ❑Yes Flo seals intact? ❑Yes
Huntersville [J/ Raleigh[] Mechanicsville❑
Project A W V V 0
tQNo ti � i #"
Date/initials Person Examining Contents:` . ) I 1
i
r
Packing Material: []Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑No
[](R Gun ID:
92T045 Type of Ice: ❑wet MBiue None
Cooler lernp ('Ll. Currtttion fatter: Add/Sul b ma (°C) -(), I Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): ` (' []samples out of temp criteria. Samples on ice, cooling process
hasbegun
USDA Regulated Soll (❑' N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
,­i..dr„s u.—ii and 0—rrn Rirn17 rlyrs 1 INo
Comments/discrepancy:
Chain of Custody Present?
r
Ejves
[]No
[]N/A
1.
Samples Arrived within Hold Time?
fes
❑No
©N/A
2.
Short Hold Time Analysis (e72 hr,)?
. Yes
ONo
❑N/A
3.
Rush Turn Around Time Requested?
)]yes
ONo
[]N/A
4.
Sufficient Volume?
33 es
❑No
i]N/A
S.
Correct Containers Used?
E]Yes
❑No
[3N/A
6.
-Pace Containers Used?
[fYes
[IN.
pN/A
Containers intact?
' yes
(]No
(]N/A
7.
Dissolved analysis: Samples Field Filtered?
Des
❑No
�N/A
8.
Sample Labels Match COC?
QYEs
[]No
❑N/A
9.
f
-includes Date/Time/[D/Analysis Matriu:
10.
s
Headspace in VOA Vials (>5-6mm)? []Yes ONo N/A
Trip Blank Present?
❑Yes
❑No
( IG//A
11,
Trip Blank Custody Seals Present?
[]Yes
❑No
E]N/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: Date/Time: _
Project Manager SCURF Review:
Project Manager SRF Review:
Date: _ t �1 a
Date: (l t 11 fir
Page 18 of 20

Document Name:
Document Revised: February 7, 2018
ri aceAnalyticale
Sample Condition upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR•CS-033•Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or deehiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
Bottom half of box is to list num er of mot a ----
Project# WO#:92405880,
12M: MWB Due Date: 11/14/18
CLIENT: 92-Allvac NC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office p.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 19 of 20

tormwater Monitoring
Chain of Custody Record
Project Number/Name: SW Outfall #al(B)
Project Location: ATI SM - Bakers
Sam ler's
Si nature:
' Date:
z
> U
Requested Test Parameters
�a
+� 6
H U a
G G /(D HNO3 Y Total Recoverable: Chromium, Nickel, Copper, Zinc
G
G /(D
HNO3
Y
Cadmium A
19�..
G
eG ! I'
HCL
Y
Oil & Grease
G
G /69
H2SO4
Y
COD S
G
G /®
None
Y
BOD Q tj
./
G
G /a
None
Y
TSS try
G G /(D None Y
Residual Chlorine
Onsite Field pH Analysis
Onsite Field Temperature Analysis
pH: j -� (s.u.) Sample Time: ,/yam,
Temp: _ _(0C) Sample Time: /a
Analysis Time: f •�I�
Analysis Time:
Meter Calibrated: YeS
Thermometer Calibrated: / N
Sampling and field an„ lysis completed by:
r
Relinquished By:
Received y7.
Date: I`"'
Time:"
Date:
Time:,
Relinquished By:
Received By:
Date:
Time:
Date:
Time:
EHS-SW-Chain of Costody Outfall 01-Rev 001 Page 20 of 20

-%#Af ATIF I A111vac
Allvat - Bakers Plant
Stommater �ort F�
Sample Date: Sample Time:
Sqmple Location: Sty water an-C2mmin gled
Drainage Area = 212.952sa. ft. = 4.9 acres
% lmpervious = 12%
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOO
1VL)
30
COD
SO-S
120
TSB
09
100
Cadmium
ND
0.001
Chromium, total recoverable
Copper, total recoverable
0.007
Nickel, total recoverable
/V10
0.26
Zinc, total recoverable
6AIR
0.067
pH
14.9 (std units)
6®g (std units)
Storm Buramon: -T.s- (Hrs.) Inches ®f Rainfall:
DuystiOn ®f time preceding raia event exceeding 0.111:
Estimated Flow C&1cuj&dojm:
Q = CIA
Q(Total) = Q(Pervious Area) + qhnpervious Area)
Q(tot., efs) = (A x inches rain/1 2 inches/ft. x 4.9 acres x .88) + .9 x inches rain/1 2inches/R. x 4.9 x. 12)
Q(Total, cfs) = 0.1437 x &4 (inches ®f rain) + 0.0441 x (Inches of rain)
= — CA

/7, laceAnalytical"
wwwpacetabs.com
November 12, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
Q.PCCRFp,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13

a'ceAnalXica
vnnrpacelabs.com
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification M 37712
•
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNFL AP Certification #• 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.L.C. Page 2 of 13

1�;a'ceAnalj#ical'
mmpacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SW OUTFALL #02(13)
92405881
Analyses
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92405881001
BSW02
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
SM 254OD-2011
CEH
1
PASI-A
SM 521OB-2011
SMK
1
PASI-A
SM 5220D-2011
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 13

aceAnal ical
wmvpacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
Sample: BSW02 Lab ID: 92406881001 Collected: 11/05/18 06:07 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data
Analytical Method:
Collected By
DPJ
1
11/05/18 06:10
Collected Date
11/06/18
1
11/05/18 06:10
Collected Time
06:04
1
11/05/18 06:10
pH
6.9 Std. Units
0.10
1
11/05/18 06:10
Temperature
15.5 deg C
0.50
1
11/05/18 06:10
200.7 MET 1013
Analytical Method: EPA 200.7 Rev 4.4
1004 Pieparal[ion Method: EPA 2001 Rev 4.4 1004
Cadmium
ND ug/L
1.0
1
11/06/18 05:44
11108/18 23:49
7440-43-9
Chromium
5.0 ug/L
5.0
1
11/06/18 05:44
11/08,118 23:49
7440-47-3
Copper
50.0 ug/L
5.0
1
11/06/18 05:44
11/08/18 23:49
7440-50-8
Nickel
ND ug/L
5.0
1
11/06/18 05:44
11/08/18 23:49
7440-02-0
Zinc
42.2 ug/L
10.0
1
11/06/18 05:44
11/08/18 23:49
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 254OD-2011
Total Suspended Solids
21.8 mg/L
2.5
1
11/08/18 00:48
5210B BOD, 6 day
Analytical Method: SM 521 OB-2011
BOD, 5 day
ND mg/L
2.0
1
11/06/18 19:07
11/11/18 13:33
B3
5220D COD
Analytical Method: SM 5220D-2011
Preparation Method: SM 5220D-2011
Chemical Oxygen Demand
30.8 mg/L
25.0
1
11/08/18 19:11
11/09/18 00:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13

2ceAnalyfica('
t VMw.pacetabs.com
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 440463
Analysis Method:
EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994
Analysis Description: 200.7 MET
Associated Lab Samples: 92405881001
METHOD BLANK: 2419374
Matrix: Water
Associated Lab Samples: 92405881001
Blank
Reporting
Parairleler
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
11/08/18 23:12
Chromium
u0/t
ND
50
11/08/1823.12
Copper
ti0/l.
ND
5.0
11/08/18 23:12
Nickel
ug/L
ND
5.0
11/08/18 23:12
Zinc
ug/L
ND
10.0
11/0811823:12
LABORATORY CONTROL SAMPLE:
2419375
Spike
LCS
LCS % Rec
Parameter
Units
Colic.
Result
% Rec Limits Qualifiers
Cadmium
ug/L
500
480
96 85-115
Chromium
ug/L
500
484
97 85-115
Copper
ug/L
500
499
100 85-115
Nickel
ug/L
500
478
96 85-115
Zinc
ug/L
500
467
93 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419376
2419377
MS
MSD
92405896001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
ug/L NO
500
500
503
500 101 100
70-130
1
Chromium
ug/L ND
500
500
506
504 101 100
70-130
0
Copper
ug/L 0.0053
500
500
521
519 103 103
70-130
0
mg/L
Nickel
ug/L ND
500
500
493
490 98 97
70-130
1
Zinc
ug/L 0.011
500
500
502
499 98 98
70-130
1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2419378
2419379
MS
MSD
92405904001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc.
Colic.
Result
Result % Rec % Rec
Limits
RPD Qual
Cadmium
ug/L ND
500
500
498
501 100 100
70-130
1
Chromium
ug/L ND
500
500
503
504 101 101
70-130
0
Copper
ug/L ND
500
500
510
514 102 103
70-130
1
Nickel
ug/L ND
500
500
490
494 98 98
70-130
1
Zinc
ug/L 0.014
500
500
497
499 97 97
70-130
0
mg/L
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, I.I.C. Page 5 of 13

1!2ceAnalyfical(t)
vmvpacelabs.com
A: a ' * l: W
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
QC Batch: 440996 Analysis Method: SM 2540D-2011
QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92405881001
METHOD BLANK: 2421944 Matrix: Water
Associated Lab Samples: 92405881001
Blank Reporting
Parameter Units Result Limit Analytod Qualifiers
Total Suspended Solids mg/L ND 2.5 11/08/18 00:38
LABORATORY CONTROL SAMPLE:
2421945
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2421946
Parameter
Units
Total Suspended Solids
mg/L
Spike LCS LCS
Conc. Result % Rec
250 244 98
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
% Rec
Limits Qualifiers
90-110
92405900003 Dup
Result Result RPD Qualifiers
27.8 31.0 11 D6
SAMPLE DUPLICATE: 2421947
92405880005 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 16.4 18.2
RPD Qualifiers
10 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
.REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 13

a'ceAnalXlca(
vasrtvpacelabs.com
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
QC Batch: 440600
QC Batch Method: SM 521 OB-2011
Associated Lab Samples: 92405881001
METHOD BLANK: 2420066
Associated Lab Samples: 92405881001
Paramotor Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 2420067
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analysis Method: SM 521 OB-2011
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifara
ND 2.0 11/11/1813:26 B3
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 192 97 84.6-115 B3
SAMPLE DUPLICATE: 2420068
92405881001 Dup
Parameter Units Result Result
BOD, 5 day mg/L ND ND
RPD Qualifiers
B3
Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13

/�;a'ceAna1j6ca1'
wvmvpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
QC Batch: 441148 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92405881001
METHOD BLANK: 2422559
Associated Lab Samples: 92405881001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2422560
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 11/09/18 00:04
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
750 757 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422561 2422562
MS MSD
92406236003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 107 100 100 216 216 109 109 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422563 2422564
MS MSD
92405876001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 100 100 130 133 113 116 90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 13

aceAnalyfical
VAW..pacelabsxom
Project: SW OUTFALL #02(B)
Pace Project No.: 92405881
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI acciediled. Cunlaul yuui Pace PM fui the cunenl list of acciediled analyles.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:11 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

Pace Analytical Services, LLC
� G m �er� 9800 Kincey Ave. Suite 100
it i 1 Huntersviile, NC 28078
VMV.Pacetabs.com [phone]
Project:
SW OUTFALL #02(B)
Pace Project No.:
92405881
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92406881001
BSW02
92406881001
BSW02
EPA 200.7 Rev 4.4 1994
440463
EPA 200.7 Rev 4.4 1994
440492
92405881001
BSW02
SM 2540D-2011
440996
92405881001
BSW02
SM 521 OB-2011
440600
SM 521 OB-2011
440712
92405881001
BSW02
SM 5220D-2011
441148
SM 5220D-2011
441293
Date: 11/12/2018 06:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

ENE
BP1U-1l,.,Plasticunpfese,,,ed(N/A)DG9H40
■
AGIU-2 liter Amber Unpresemed (N/A) (Cl-)
NEWWAML,
ML VOA HCl (N/A)
■
ME
V/GK(3vbV­kit)-VPH/Gaskit(NJA)SP2T-2SO
ME
SPST-IZSmLSMrileP[astiC(N/A—lb)
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AH,vac - Bakers Plant
stolmff aer, Monitorin . - Q-t- EG-r—M
Sample Date: --// --Ta
Sample Location:
Person Collecting Samples:
Laboratory Performing A, nalysis:
Ana "I'calTechniques and Methods:
Results of Sample Analysis:
Parameter
BOO
COD
TSS
Cadmium
Chromium, total recoverable
Copper, total recoverable
Nickel, total recoverable
Zinc, total recoverable
pH
Drainage Area = 336,580s . ft. 7.8 acres
% Impervious = 15%
Dowa ® . '41'u
Pace 44"1
I --
40 CFR Part 136
Results (mg/1) Benchmark Values (mg/l)
A/ 1) 30
100
0.001
1
0.007
0.26
d17 1 0.067
(std units) 1 6-9 (std units)
Storm Date: -ZZ-L--r--Zd- Storm Duration: (Hrs.) inches of Rainfall: q
119ration of time preceding rain event exceeding 0.1 11: (firs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Wervious Area) + Wmpervious Area)
Q(tot., cfs) = (A x inches ra1n/12 inches/ft. x 7.8 acres x -85) +-9 X inches ra1n/12inches/ft. x 7.8 x.15)
Q(Total, cfs) = 0.2210 x _.. . /. 8 _ (Inches of rain) + 0.0878 x Z. (Inches of rain)

aceAnalytical
—pacWabs.com
f
November 12, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
pcCW
�yr
9e
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 16

aceAnalytical s
"m..pacetabs.com
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Ma6bachu6eW6 Cerlinuation #. M NCO30
North Carollna Drinking Water Certifcatlon M 3-1712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VlrglnlaNELAP Cerllfloatlon M: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 16

aceAnalytical
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1
SAMPLE ANALYTE COUNT
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92406879001
BSW03
EPA 200.7 Rev 4.4 1994
SH1
5
PASI-A
92405879002
BSW03
SM 5220D-2011
GC
1
PASI-A
92405879003
BSW03
SM 521OB-2011
SMK
1
PASI-A
92405879004
BSW03
SM 2540D-2011
CEH
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Sample: BSW03 Lab ID: 92405879001 Collected: 11/05/18 06:31 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data Analytical Method
Collected By
DPJ
1
11/05/18 06:32
Collected Date
11/06/18
1
11/05/18 06:32
Collected Time
06:25
1
11/05/18 06:32
pH
7.2
Std. Units
0.10
1
11/05/18 06:32
Temperature
15.7
deg C
0.50
1
11/05/18 06:32
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Cadmium
ND
ug/L
1.0
1
'11/06/18 05:44
'11/08/18 23:43
7440-43-9
Chromium
ND
ug/L
5.0
1
11/06/18 05:44
11/08/18 23:43
7440-47-3
Copper
11.8
ug/L
5.0
1
11/06/18 05:44
11/08/18 23:43
7440-50-8
Nickel
ND
ug/L
5.0
1
11/06/18 05:44
11/08/18 23:43
7440-02-0
Zinc
17.4
ug/L
10.0
1
11/06/18 05:44
11/08/18 23:43
7440-66-6
Date: 11/12/2018 06:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 16

aceAnalytieal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #03(13)
Pace Project No.: 92405879
Sample: BSW03 Lab ID: 92405879002 Collected: 11/05/18 06:30 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011
Chemical Oxygen Demand 33.1 mg/L 25.0 1 11/08/18 19:11 11/09/18 00:07
REPORT OF LABORATORY ANALYSIS
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Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 16

aceAnalj6cal @
—pacetabsxw
s
ANALYTICAL RESULTS
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW03 Lab ID: 92405879003 Collected: 11/05/18 06:28 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day Analytical Method: SM 521 OB-2011
BOD, 5 day ND mg/L 2.0 1 11/06/18 19:07 11/11/18 13:38 B3
Date: 11/12/2018 06:09 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 6 of 16

aceAnalX cal"
www.pacelabs.c=
I
ANALYTICAL RESULTS
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: BSW03 Lab ID: 92405879004 Collected: 11/05/18 06:26 Received: 11/05/18 09:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Total Suspended Solids
Date: 11/12/2018 06:09 PM
Analytical Method: SM 2540D-2011
16.3 mg/L 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/08/18 00:44
Page 7 of 16

aceAnalytical "
www.pacelabs.com
I
QUALITY CONTROL DATA
Project: SW OUTFALL#03(B)
Pace Project No.: 92405879
QC Batch: 440463 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92405879001
METHOD BLANK: 2419374
Matrix: Water
Associated Lab Samples: 92405879001
Blank
Roporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
11/08/18 23:12
Chrorniurn
ug/L
ND
6.0
11/08/18 23:12
Copper
ug/L
ND
5.0
11/08/18 23:12
Nickel
ug/L
ND
5.0
11/08/18 23:12
Zinc
ug/L
ND
10.0
11/08/18 23:12
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2419375
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
480
96
85-115
Chromium
ug/L
500
484
97
85-115
Copper
ug/L
500
499
100
85-115
Nickel
ug/L
500
478
96
85-115
Zinc
ug/L
500
467
93
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2419376
2419377
MS
MSD
92405896001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
503
500
101
100
70-130
1
Chromium
ug/L
ND
500
500
506
504
101
100
70-130
0
Copper
ug/L
0.0053
500
500
521
519
103
103
70-130
0
mg/L
Nickel
ug/L
ND
500
500
493
490
98
97
70-130
1
Zinc
ug/L
0.011
500
500
502
499
98
98
70-130
1
mg/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2419378
2419379
MS
MSD
92405904001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Cadmium
ug/L
ND
500
500
498
501
100
100
70-130
1
Chromium
ug/L
ND
500
500
503
504
101
101
70-130
0
Copper
ug/L
ND
500
500
510
514
102
103
70-130
1
Nickel
ug/L
ND
500
500
490
494
98
98
70-130
1
Zinc
ug/L
0.014
500
500
497
499
97
97
70-130
0
mg/L
Results presented on this page are in the units indicated by the
"Units' column except where an alternate unit is presented
to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16

aceAnalytical
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Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
QC Batch: 440996
QC Batch Method: SM 2540D-2011
Associated Lab Samples: 92405879004
METHOD BLANK: 2421944
Associated Lab Samples: 92405879004
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE: 2421945
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2421946
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 2421947
Parameter
Total Suspended Solids
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D-2011
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 2.5 11/08/18 00:38
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
250 244 98 90-110
Units
92405900003
Result
Dup
Result
mg/L
27.8
31.0
Units
92405880005
Result
Dup
Result
mg/L
16.4
18.2
RPD Qualifiers
11 D6
RPD Qualifiers
10 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16

aceAnalX cal
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1
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
QC Batch: 440600
Analysis Method:
SM 521OB-2011
QC Batch Method: SM 521 OB-2011
Analysis Description:
5210B BOD, 5 day
Associated Lab Samples: 92405879003
METHOD BLANK: 2420066
Matrix: Water
Associated Lab Samples: 92405879003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
BOD, 5 day
mq/L
ND
2.0 11/11/18 13:26 B3
LABORATORY CONTROL SAMPLE: 2420067
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
BOD, 5 day
mg/L
198 192
97 84.6-115 B3
SAMPLE DUPLICATE: 2420068
92405881001 Dup
Parameter
Units
Result Result
RPD Qualifiers
BOD, 5 day
mg/L
ND
ND B3
Results presented on this page are in the units indicated by the 'Units' column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 16

aceAnalytical
—pace(abs.cwn
QUALITY CONTROL DATA
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
QC Batch: 441148 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Associated Lab Samples: 92405879002
METHOD BLANK: 2422559
Associated Lab Samples: 92405879002
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 11/09/18 00:04
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE. 2422500
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 757 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422561 2422562
MS MSD
92406236003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Chemical Oxygen Demand mg/L 107 100 100 216 216 109 109 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2422563 2422564
MS MSD
92405876001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 100 100 130 133 113 116 90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 16

Pace Analytical Services, LLC
1��a'cmnalj&al@ 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
I
QUALIFIERS
Project: SW OUTFALL #03(B)
Pace Project No.: 92405879
67=1 y1:IIIII 7:��
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L.
D6 The preclsluu t,elweeu the sample and sample duplicate exceeded lahuralwy uurrlrul Ilrrdts.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/12/2018 06:09 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16

aceAnalytical
—pacelabs.com
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
SW OUTFALL #03(B)
92405879
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92405879001
BSW03
92405879001
BSW03
EPA 200.7 Rev 4.4 1994
440463
EPA 200.7 Rev 4.4 1994
440492
92405879004
BSW03
SM 2540D-2011
440996
92405879003
BSW03
SM 521OB-2011
440600
SM 521OB-2011
440712
92405879002
BSW03
SM 5220D-2011
441148
SM 5220D-2011
441293
Date: 11/12/2018 06:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 16

aceAnalytrca(
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑
Client Name:
Courier: HFed Ex
Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[
Project 1 9 405879
❑ Commercial ❑Pace "utner.
Custody Seal Present? ❑Yes QNo Seals intact? []Yes
❑Client III II 1111111111111111
g2405879
`❑ND
Date/iniitials Person Examining Content$.'
Packing Material: ❑Bubble Wrap ❑Bubble Bags ENone ❑ Other Blological Tissue Frozen?
Thermomet0-: ❑yes ❑No ENJA
,[]IR Gun ID: 92TO45 Type of Ice: [_jUJet ❑Blue ❑None
v
Loafer temp (`C): Cattactiorr Factor: Add/51.lbtiact (°C) _p_
Temp Should be above freezing to 6°C
Cooler Temp Corrected j'C): i ❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
14—mil and Puartn Rirnt7 i lyps i lNo
Comments/Discrepancy:
Chain of Custody Present?
i6Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
f
❑Yes
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
11es
ON.
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
r
- No
❑N/A
4.
Sufficient Volume?
Yes
ON.
❑N/A
5.
x
Correct Containers Used?
joVY s
❑No
❑NIA
6.
-Pace Containers Used?
Ojes
❑No
❑N/A
Containers intact?
6yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
❑No
[]NIA
8.
Sample Labels Match COC?
❑yes
ONO
❑N/A
9.
'
-includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
❑Yes
No
f.
°: N/A
10.
Trip Blank Present?
❑Yes
❑No
❑N/A
11.
Trip Blank Custody Seals Present?
❑Yes
❑No
❑NIA
COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: ` Date:
Page 14 of 16

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Recei t(SCUR) Pa e 1 of 2
'MAnalytical' Document No.: issuing Authority:
F-CAR-CS-033-Rev,06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project" �����
verified and within the acceptance range for preservation
samples. RM: MWB Due Date: 11/14/18
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/BOiS (water) DOC, LLHg CLIENT: 92-AI 1 Vaa NC _
**Bottom half of box is to list number of bottle
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Date preservation adjusted
Time preservation
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added
tot ff
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Note: Whenever there is a discrepancy affecting North Larouna compliance sampies, a Lupy ul t 1z ,w,,,, — ---
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 15 of 16

0�
tormwater Monitoring
Grain -of %'-ustady Rvcurd -
Project Number/Name: SW Outfall #03(B)
Project Location: ATI SM - Bakers
Sam ler's Si nature:
Date:
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Temp: I: ; % (°C) Sample Time:
Analysis Time: • -3�
Analysis Time: •,? y
Meter Calibrated. Y85
Thermometer Calibrated: t0 / N
Sampling and field analysis cam leted by:,.
Relinquished By:
Received y:_'�;
Date: Yl-,5 l`
Time: C/�!L�
Date: f y`
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Relinquished By:
Received By:
Date:
Time:
Date:
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EHS-SW-Chain of Costody Outfall 03-Rev 001 Page 16 of 16

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1�;5'ceAnalXical'
www.pacel8bs.com
F
t
i
October 31, 2018
Scott Ryan
Allvac
Monroe, NC
RE: Project: NonContact Cooling Water
Pace Project No.: 92403862
Dear Scott Ryan:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Joe Hinkle, Allvac
David Pope, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

aeeAnalyiical
—pacelabs.com
f
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # L.A170028
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification #• M-N(:030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Vir0iniaNFL AP Certification #• 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 19

Pace Analytical Services, LLC
acte 100
eAnalytical w 9800Huntersv lle, NCKincey Ave. 128078
www.pacelabs.com [phone]
1
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
NonContact Cooling Water
92403862
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92403862001
NonContact #1
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862002
NonContact #2
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862003
NonContact #3
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862004
NonContact #4
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI A
92403862005
NonContact #5
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862006
NonContact #6
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862007
NonContact #7
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
92403862008
NonContact #8
EPA1664B
JMS
1
PASI-C
SM 4500-CI G-2011
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

aceAnalj&al
wwwpacelabs.com
I
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #1 Lab ID: 92403862001 Collected: 10/16/18 07:45 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 10/31/18 03:39
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.34 mg/L 0.024 1 10/18/18 23:12 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

1��a'cmnalXicalo
www.pacetabsxom
f
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #2 Lab ID: 92403862002 Collected: 10/16/18 08:05 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 10/31/18 03:39
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, fotal Residual 0.038 mg/L 0.024 1 10/18/18 23:21 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

aceAnalyticai@
—pacetabs.com
t
1
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #3 Lab ID: 92403862003 Collected: 10/16/18 08:27 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 10/31/18 03:39
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.49 mg/L 0.024 1 10/18/18 23:26 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

aeeAna1j4 cal
—pacelabs.com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #4 Lab ID: 92403862004 Collected: 10/16/18 08:50 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 10/31/18 03:40
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.093 mg/L 0.024 I 10/18/18 23:30 1 /82-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

aceAnalytical
—pacelabs.com
I
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #5 Lab ID: 92403862005 Collected: 10/16/18 09:15 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 10/31/18 03:40
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.46 mg/L 0.024 1 10/18/18 23:35 7782-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I.L.C.
Page 8 of 19

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #6 Lab ID: 92403862006 Collected: 10/16/18 09:37 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 10/31/18 03:40
4600CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.028 mg/L 0.024 1 10/18/18 23:40 7 /82-50-5 H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 19

aceAnalj cal
—pacWabs.c=
ANALYTICAL RESULTS
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NonContact #7 Lab ID: 92403862007 Collected: 10/16/18 10:00 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 10/31/18 03:41
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlurine, Total Residual 0.030 mg/L 0.024 '1 10/18/18 23:4b / /82-bO-b H3
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

aceAnaly4ieal "
www.pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: NonContact Cooling Water
Pace Project No.: 92403862
Sample: NonContact #8 Lab iD: 92403862008 Collected: 10/16/18 10:23 Received: 10/17/18 08:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 10/31/18 03:41
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G-2011
Chlorine, Total Residual 0.097 ing/L 0.024 1 10/18/18 23.50 7782-50 5 H3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2018 03:28 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 19

/IceAnalXical"
wwwpacelabs,00m
1
QUALITY CONTROL DATA
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 439353 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92403862001, 92403862002, 92403862003, 92403862004, 92403862005, 92403862006, 92403862007,
92403862008
METHOD BLANK: 2414537 Matrix: Water
Associated Lab Samples: 92403862001, 92403862002, 92403862003, 92403862004, 92403862005, 92403862006, 92403862007,
92403862008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Crease m0/l. ND 4 8 10/31/18 03.37
LABORATORY CONTROL SAMPLE:
2414538
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
38.5 38.7
101
78-114
MATRIX SPIKE SAMPLE:
2414539
92403774004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 38.5
38.4
99
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2018 03:28 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

aeeAnalytieal
—pacelabs.com
QUALITY CONTROL DATA
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 437083 Analysis Method: SM 4500-CI G-2011
QC Batch Method: SM 4500-CI G-2011 Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92403862001, 92403862002, 92403862003, 92403862004, 92403862005, 92403862006, 92403862007,
92403862008
METHOD BLANK: 2404409 Matrix: Water
Associated Lab Samples: 92403862001, 92403862002, 92403862003, 92403862004, 92403862005, 92403862006, 92403862007,
92403862008
Parameter
Units
Blank
Result
Reporting
Limit Analyzed Qualifiers
Chlorine, total kesidual
mg/L
ND
0.024 10/18/18 23:08
SAMPLE DUPLICATE: 2404410
92403862001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Chlorine, Total Residual
mg/L
0.34
0.34 1 H3
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2018 03:28 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

ai✓eAnaljftal
—pacelabs.com
QUALIFIERS
Project: NonContact Cooling Water
Pace Project No.: 92403862
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a spocifio matrix.
8 Surrogale
,1,2 Diphenylhydrazlno decomposes to and oannot be separated from Azobenzene using Method 8210. 1 he result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/31/2018 03:28 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

aeeAnalytieal
www.pace/abs.c=
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NonContact Cooling Water
Pace Project No.: 92403862
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92403862001
NonContact#1
EPA1664B
439353
92403862002
NonContact #2
EPA 1664B
439353
92403862003
NonContact #3
EPA 1664E
439353
92403862004
NonContact #4
EPA1664B
439353
92403862005
NonContact#5
EPA1664B
439353
92403862006
NonContact #6
EPA1664B
4393.53
92403862007
NonContact#7
EPA1664B
439353
92403862008
NonContact #8
EPA 1664B
439353
92403862001
NonContact#1
SM 4500-CIG-2011
437083
92403862002
NonContact#2
SM 4500-CIG-2011
437083
92403862003
NonContact #3
SM 4500-CI G-2011
437083
92403862004
NonContact #4
SM 4500-CI G-2011
437083
92403862005
NonContact #5
SM 4500-CI G-2011
437083
92403862006
NonContact #6
SM 4500-CI G-2011
437083
92403862007
NonContact #7
SM 4500-CI G-2011
437083
92403862008
NonContact #8
SM 4500-CI G-2011
437083
Date: 10/31/2018 03:28 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 19

Document Name:
Document Revised: February 7, 2018
b
_ aceAnatytica!
Sample Condition Upon Receipt(SCUR)
Page i of 2
Document No.:
Issuing Authority:
F-CAR-CS-D33-Rev.06
Pace Carolinas Qualit Office �__
Laboratory receiving samples: 1
Asheville ❑ Eden❑ Greenwood ❑ HuntersvilWL) Raleigh❑ Mechanicsville❑
Client Name: j Project WO#• 9 0VV2
• �. � � ( i'i:
Courier: Fed Ex ❑UISS ❑LISPS ❑Client
❑ Commercial L/ Place ❑Other: 92403862
Custody Seal Present? ❑Yes TJNlo Seals Intact? ❑Yes jNo
Packing Material: ❑Bubble wrap UBubble Bags ❑None ❑ Other
Thermometer:, 7
I Gun ID:
92TO45 Typo of tee: (4wet []Blue
Y /-J'
Cooler Temp (°C): -2 1 r `i - o Correction Factor: Add/Subtract (°C) i
Cooler Temp Corrected ('C)' ..
USDA Regulated Soil N/A, water sample)
Did samples ofi'nate in quarantine zone within the United States: CA, NY, or SC (check maps)?
nyes thin
Date/initials Person Examining Co Lftnts:l
Biclogl a ai Tissue Frozen?
[--]None ❑Yes' -❑No ❑N/A
Tamp should be above froozing to WC
❑Samples out of temp criteria. Samples on ice, cooling process
hasbegun
Did samples originate from a foreign source n (internationally,
1...41- 14—ii —4 lh—tn W-1� r"Ivne t-
Comments/Discrepancy:
Chain of Custody Present?
t]Ves
[IN.
N/A
1.
(-
Samples Arrived within Hold Time?
&es
❑No
N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
Q Oo
[-]N/A
3.
Rush Turn Around Time Requested?
❑Yes
` o
❑N/A
4.
Sufficient Volume?
❑Yes
No
❑N/A
S.
Correct Containers Used?
Yes
[]No
❑N/A
6.
-Pace Containers Used?
`"�, r Yef
❑No
[]NIA
Containers intact?
s
[]No
N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
❑No
N/A
8.
Sample Labels Match COC?
[]No
[]NIA
9.
(j 1y,Yes
-includesDate/Time/ID/Analysis Matrix:
U v
Headspace in VOA Vials (>5.6mm)?
❑Yes
17,1No
/A
14.
Trip Blank Present?
❑Yes ❑trio
t ❑N/a
1
11.
Trip Blank Custody Seals Present?
[]Yes
❑JNo
t N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted-
Date/Time:
Field Data Required? ❑Yes ❑Na
rV
Project Manager SCURF Review: � Date: i <; nj
Project Manager SRF Review: A Date: C I ( 1
I
Page 16 of 19

Document Name:
Document Revised: February 7, 2018
26Anayttcal m
Sample Condition Upon Receipt(SOUR)
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR•CS-033-Rev.06 _ __
___Pace-CarolinasQuality_Office
*Check mark top half of box If pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box Is to list number of bottle
PM: MWB Due Date: 10/31/18
CLIENT: 92-Allvac NC
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pH Adjustment Log for Preserved Samples
Sample to
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
—Cat 1;—
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form win be sent to the North caronna utrmn Cerrmcaoon Crime p.e.
Out or hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 19

I
spe6llty Materials
CONTACT)
Bakers North
Chain of Custody Record
Project Number/Name: NonContact Cooling Water
page st
Project Location: Allvac Bakers
Sampler's Signature:
D a t e Zo-/ "j
6
to LA
®
�-
C
a)
®
®
c�
v
17
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Requested Test
Parameters
&,Artii 1
G
G
HCL
Y
, g'04
Oil & Grease
MCM 444A
IpS'�
G
G
HCL
Y
ds.3'°e
Oil & Grease
4ievnt
G
G
HCL
Y
.
Oil &Grease
�04�AC!1
:$O....
G
G
HCL
Y
'e
Oil & Grease
d/1C'D�t Ad#S"
g"„®
G
G
I HCL
Y
.�•�
Oil &Grease
G' fRdf"{
•:37a�
G
G
HCL
Y
a, g�
Oil & Grease
h4v "t# 7
G
G
HCL
Y
°�
pil &Grease
C
JO •' .3..
G
G
HCL
Y
Oil & Grease
Meter Calibrated: C/N
Thermometer Calibrated: [Qj J N
Sampling and Field analysis completed by:
Relinquished By:
Relinquished By:'�
Jr
Date : p"
Time: IDate
: x-.r-j : -t Time: p
Relinquished By:
C �`
Relip is ed )3yij / R
Date : , j "Time:
i
pate i ( "
T46: --5
t -1 na Ker South 5W REV 8 G 5/l0/2016
Page 18 of 19

Storm Water Monitorin;i;
(NON CONTACT)
Bakers North
Chain of Custody Record
/ %I I
Specialty Materials
page #1
Project Number/Name: NonConta t Cooling Water
Project Location: Alivac Bakers
Sampler's Signature:
Date: Al -14 -J
to
°•,
CL
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Requested Test
CL
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Parameters
S
CL
O
i
LL
4 �
ly
+'
o
H
`Ci;y' �-
G
G/49
None
Y
.�'®c
Residual Chlorine
�¢
: jj5,,,
G
G/S
None
Y
23,31e,
Residual Chlorine
m..
G
G/8
None
Y
.311c
Residual Chlorine
Alm Cu„ Ra'f
S:5A
G
GAP
None
Y
14
Residual Chlorine
/i/ 0„4:4- '
9.15�.
G
G/®
None
Y
1p°
Residual Chlorine
paCdn (
,m,.
G
GJ(D
None
Y
'e
Residual Chlorine
pnCb Ae
:pp.,,
G
Go
None
Y
, -7'a.
Residual Chlorine
aCdnfRcf
lI '
G
GAPNone
Y
'c
Residual Chlorine
Meter Calibrated:
/ N
IThermorneter Calibrated
/ N
Sampling and Field analysis completed by:,
-.c.
Relinquished By:
IReceived BY:
x
Date:
Time: a...
Rater
t
Time: __.
Relinquished By:
�, .
ec ived y
c;
Date:
ITime: j
_
bate': t
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Time:
EHS Baker South SW REV # 2 5/10/2016
Doi
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(U o 6
0 ,, -7
cbz�'--'
Page 19 of 19

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Environmental
Quality
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit https:Hdeq.nc.gov/about/divisions/energy-mineral-land-
resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab4
Permit No.: NlC/SID/-0I AIJ/,Z/g/ or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/
Facility Name: Ar_r 41li-W -,5AXe.r's
County: &41'4A Phone No. 70�i'.i�9-'yam//
litspectol. PA,✓IX fit:
Date of Inspection:�8
Time of Inspection: G •o?dpc...
Total Event Precipitation (inches): AS
All permits require qualitative monitoring to be performed during a "measurable storm event."
A `measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or Designee)
1. Outfall Description:
Outfall No. Structure (pipe, ditch, etc.): -50AI Wt f
Receiving Stream:
rk
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of the
(light, medium, dark) as descriptors:
Ilh-
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): ALeh &
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids iii
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
2 3 4 5
7. Is there any foam in the stormwater discharge? O Yes (g)No.
8. Is there an oil sheen in the stormwater discharge? OYes eNo.
9. Is there evidence of erosion or deposition at the outfall? O Yes 0 No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017

(,Writonm( nrut
Qw,hr"y
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on falling out this form, please visit littps://deq.nc.gov/about/divisionsienergy-inineral-land-
resourcesrenercy-mineral-land-permits/stormwater-permits/nudes-industrial-sw#tab-4
Permit No.: NIC/S / 610 / D l l 11/ or Certificate of Coverage No.: N/C/G/—/s/_/_/_/�/
Facility Name: ,��.Z AllniG
County: a, pn Phone No.
hispectut: LLWILI AweS•.
Date of Inspection:/-.S /Q
Time of Inspection:(] O
Total Event Precipitation (inches): /.8
All pen -nits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
............ .....
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Outfall Description:
Outfall No. 5WO,,? Structure (pipe, ditch, etc.): e-
Receiving Stream:
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: a
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stonfiawater discharge, -where i is no solids and 5 is extremely muddy:
(� 2 3 4 5
7. Is there any foam in the stormwater discharge? ® Yes No.
91
am
Is there an oil sheen in the stormwater discharge? 0Yes No. —
Is there evidence of erosion or deposition at the outfall? O Yes No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe ,?
Note: Love clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242, Last modified 07/28/2017

f_ o 4 a on men Cat
Qua Itty
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit littps://deg.nc.gov/about/divisions/eneray-mineral-land-
resources/energy-mineral-land-uerrmits/stonnwater-permits/nudes-industrial-sw#tab-4
Permit No.: N/C/S/O l ®l D /3/62/jl or Certificate of Coverage No.: N/C/G/e%/—/_/_/_/
Facility Name: AIAO,G - Ax&-s
County: &,I %Di! Phone No. 7d oe
Inspector: �iwia� - J/'.
01
Date of Inspection: &-5=/�
Time of inspection: &
Total Event Precipitation (inches): /.g
All permits require qualitative monitoring to be performed during a "measurable storm event."
A "measurable storm event" is a storm event that results in an actual discharge from the permitted site
outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm
interval does not apply if the permittee is able to document that a shorter interval is representative for
local storm events during the sampling period, and the permittee obtains approval from the local DEMLR
Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee Kr Designee)
1. Outfall Description:
Outfall No. 6,5WO
Receiving Stream:
Structure (pipe, ditch, etc.): Aze e ll%�% y Gck
Describe the industrial activities that occur within the outfall drainage area:
Page 1 of 2
SWU-242, Last modified 07/28/2017

2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: — cz"V
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): A119.42 e
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids and 5 is the surface covered with floating solids:
2 3 4 5
C-V
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
a
Ell
VA
(9 2 3 4 5
Is there any foam in the stormwater discharge? 0 Yes (9 No.
Is there an oil sheen in the stormwater discharge? OYes ICN
&,)No.
Is there evidence of erosion or deposition at the outfall? 0 Yes No.
10. Other Obvious Indicators of Stormwater Pollution:
List and describe /Vaq e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may Jbk�"
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 07/28/2017