NCS000041_Monitoring Reports 2018

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Sawple Receipt Chccklist (SRC-) rffeoi�,c Duo,
Client M A 4". /v f-1--.1 - I — - . : 0 . I , - - - , rl — -- - I'% —
+
rcceipt, UPS, j,J FedEx Lj Oihcr:
Wen. custody scals present ou the cooleo
El Ycj El NA 1 Pleaelll, WVC -,-kY illt= a.hd 11T1bTQ1Kej3?
PI-1 Strip TD: _J_B J. f1lol-ine Strip ID- Te-Sted Iw.-
49
Sillat tvnipcniture upon vereipT t]p ti).
wived fC-0tr,1C,1t:d) Winparature nprin rccej�m: %solid Snou-Cup [D
C
Method: �aTenverature
r.-C -C
131iink nApinsr Bortirs TR, Cilij) ID. lid (AM COrTeLlion Factor:
Nic-thod of coolant: cc, Facks El Dry I" None
yvs
0, , No
�ONA
3 If (ernprattre of a-,jy co4ler exc',eede4 COT, was 4'roj,5u Marmoger Nocified'.`
I'M wa's NeitifiNI try: pljollo .0.t,flco
7
, X11
NA
4. is ffic c, minemial eauricr'L.. packillA -Oip W111chod to this form.?
Yes
U No
5. M,= proper msttrd �' followcd,,
WeTe sample JD-i IiAA on. the CDC?
yt*
No
7 Wem s"Illip1r. IDS listed an all vilnPIC
YC5
L77__ No
1A.'as C'.111mcbmi date, tittie listed oil the COC,,'..,
Ye s
—i No
9, 1gas collection datc tape listed Ou 411 sample containem?
Did all camlijincr labet mfdrMation"11.0, dale, thILL) agrc -,4'jjli-rTje-,C0C,?
LJ yr.,
No
µ
.,2 y ms
0 No
-10,
I I %Vem test on the COO
-to be perfbnnc,,� limx-d
N c)
12. Did allsatqjcs zui-ive ill pr(mu�r contflincn for each wSt alld/of im Amid con iihon
(urtbroknn, Ws on, -,to.)')
YCS
=)N n
—'i4.
11."WW adequate S�impkvolurne available?
0 N a
Wete all !�al-I r, t1w hold hig, tinw m- 49 horms, whirl !'C.Vv.r C,03.1les, f Irit?
F/ No.
-MY `,3MPJC5 Cotita ij iers in j,sing x fercle One) SM!1_P_j6s COC7
Yes
D No
NA16
'Ver
orVOA and RSX-175 urnpics, were �Ilbbles IN"ent -'"Pca-,ize" (V,"ar 6nu-n itl di}JDACl) ill
-=�l
le
I
any oi"L?jt; VOA vials?
o
=-NA
7. WL re a! 14 DR 0!1 rr ta I s4) u U 'i u n t s . mn plcs received at a pJ4 of < 2ry
Yez
LNo
NAA,%
Ver4a alt q2midr lnpJes receiked 41; it pH > 12 and qflf1do,5,qiljpjt,,., receivuj al a tall % 97
2 yml
I]
D No
!"I NAtitle
nob'625 samples Jre(, of residual
01jorinc,
—;_ ", j1L — ..........
OY 17 No
NA rmarksmetp-sTs leqUeSLedJikj6nns, .14S!PL,1SD dosgnations,
IOln 111D COC bro tll-Coniffcro scction it) LIMP
YCS 4 No:
21.Wq. tlican-teituluburl;
.51cd or., ifie corimincy if
S31111JOPresemation
Sairple(.q) QrMCtIv PIT-Sehled alldlver,- adJu.AtJ nmirdingly
lin sample ronviving mL tff catie orat: TUS04., KNO2, HCJ, MOM I using SR 4
11me of PmSm"ation
If more. than me pi)ne7 valive. is mcdcd, please note in t11c comnieijLs brdcm-,
,kimula(s) ...........
......... .... .. Wc,,Tc rmrciv�,d ivith bubbIts.-f, lrl-n ill dic,!jjc-jv
S ip I an .. . ..................
.. . . . .. . w= rccc ived Tvith TR C -', 0.5 inn il, (Tf4 (1) is no'l, alyl Were
(Na;lS, 10 , 0;
, ) Mlh Shealy I D-.
ER barcodc Ukifls applied by. Date:
Comments:
. -I- . - — . -

SHEALY ENVIRONMENTAL SERVICES, INC.
healy Environmental Services, Inc.
06 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 17 of 18

SHEAIX EnURONNIENTAL LABORATORIES
C I arian, f. —�,tjj W W NjVTP
Chain of CUSL(P(lv T127070
CII-TiMlt-MOUJA Willy West Phone. , (70 —
625 Fast Avenue Pax: [phone]
NIQunt'Holly, NC 2k 120
aMI)Ies:
Nhijnb�r of s ,Zy-' Sample tyJIL:
Swhf�]-, Collected Dy,
13Y.,
Pn'iit PlInI
r
ra
Sii-nauim,
Dwt ni iri
Grab Or
Location cownsite
ouvea 11 clo I (.1-n0b
Outfall 003 I Q ra b
Ourfall 004
Grab
005 Orah
'ub
Ond 11006 (T
Datee Time Analysis
Collected
O&e, BOD, C(A), TSS, Total Phenols,
0&0, BOD, COD, TSS, ToiaFP-F,e, 1s'
oulfid] 07 Gfab
1'r,'.Serlatives.reqUITed :Oil and B0
Total Phenols -.- yj.2SOj
I e 15t-) 1 O&U, BOD,
5,
O&G, BOD, COD, TSS, Total Phcnot� .. .. . . . . .
la-H
0&(-T, BOD, COD, TSS, 'I'otaJ.Phcno!s,
PH
O&G, B01), COD, TSS,Total Plicnols,
nonc., COD -1-12SO4.
� in uIs le Tate Received Date
........ ........
RcIbiouished hy: Date Tit=
Reoelved by: Date !Tirnr
LI

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Environmental Services, Inc.
�10. Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 15 of 18

Chain of Custody
•l
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 14 of 18

Inorganic non-metals
ND = Not detected at or N = Recovery is out of P = The RPD between two GC columns exceeds 40%
above the LOQ criteria
H = Out of holding time W = Reported on wet
weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Is
Page 13 of 18

Inorganic non-metals
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 5210B-
7.0
2.0
mg/L
1
COD
SM 5220D-
21
20
mg/L
1
PH
SM 4500-H B-2
6.5
su
1
Phenolics
420.4
0.14
0.0050
mg/L
1
TSS
SM 2540D-
7.0
4.2
mg/L
1
HEM (oil and
1664B
ND
4.4
mg/L
1
grease)
LOQ = Limit of Quantitation B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 18

0
HEM (oil and grease)
Inorganic non-metals
1664B ND 4.4 mg/L 1
LOQ = Limit of Quantitation
8 = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
ND = Not detected at or above
N = Recovery is out of P = The RPD between two GC columns exceeds 40%
the LOQ
criteria
H = Out of holding time
W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-006
West
Description: Outfal 1007 Matrix: Aqueous
Date Sampled: 09/26/2018
1906
Date Received: 09/27/2018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
kovu, o aay/ atvt 1 1 U/U2/2018 2256 AMR 09/27/2018 2254
521OB-2011 12272
1 (COD) SM 1 10/09/2018 1733 MGM 10/05/2018 1904
5220D-2011
1 (pH) SM 4500-H 1 09/27/2018 2341 SA1 84835
B-2011
1 (Phenolics) 420.4 1 10/09/2018 1128 MSG 10/08/2018 1111
85742
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 18

Ri
Inorganic non-metals
ND = Not detected at or above N = Recovery is out P = The RPD between two GC columns exceeds 40%
the LOQ of criteria
H = Out of holding time W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-005
West Matrix: Aqueous
Description: O utfal l 006
Date Sampled: 09/26/2018
1903
Date Received:09127/2018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
l
(t3uu, 5 day) bm
1 10/02/2018 2256 AMR
09/27/2018
2254
521OB-2011
12272
1
(COD) SM
1 10/05/2018 1132 MGM
10/04/2018
1600
5220D-2011
1
(pH) SM 4500-H
1 09/27/2018 2337 SA1
84835
B-2011
1
(Phenolics) 420.4
1 10/09/2018 1127 MSG
10/08/2018
1111
85742
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-20,1,1
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and) 1664B
CAS Analytical
Parameter
Number Method
Result Q
LOCI
Units
Run
BOD, 5 day
SM 5210B-
5.4
2.0
mg/L
1
COD
SM 5220D-
54
20
mg/L
1
pH
SM 4500-H B-2
6.2
su
1
Phenolics
420.4
0.017
0.0050
mg/L
1
TSS
SM 2540D-
240
25
mg/L
1
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 18

Inorganic non-metals
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 521013-
29
2.0
mg/L
1
COD
SM 5220D-
91
20
mg/L
1
pH
SM 4500-H B-2
6.1
su
1
Phenolics
420.4
0.0051
0.0050
mg/L
1
TSS
SM 2540D-
30
13
mg/L
1
HEM (oil and grease)
1664B
ND
4.5
mg/L
1
LOD = Limit of Quantitation B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
a
Page 9 of 18

HEM (oil and grease)
Inorganic non-metals
1664B ND 4.4 mg/L 1
R
LOQ = Limit of Quantitation B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
ND = Not detected at or above N = Recovery is out of P = The RPD between two GC columns exceeds 40%
the LOQ criteria
H = Out of holding time W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-004
West Matrix: Aqueous
Description: 0 utfal 1005
Date Sampled:09/26/2018
1859
Date Received:09/27/2018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (BOD, 5 day) SM 1 10/02/2018 2256 AMR 09/27/2018 2254
5210E-2011 12272
1 (COD) SM 1 10/05/2018 1132 MGM 10/04/2018 1600
5220D-2011
1 (pH) SM 4500-H 1 09/27/2018 2333 SA1 84835
B-2011
1 (Phenolics) 420.4 1 10/09/2018 1124 MSG 10/08/2018 1111
85742
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 18

P
Inorganic non-metals
ND = Not detected at or above N = Recovery is out of P = The RPD between two GC columns exceeds 40% If
the LOQ criteria
H = Out of holding time W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-003
West Matrix: Aqueous
Description: Outfa 11004
Date Sampled:09/26/2018
1855
Date Received:09/2712018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1
(BOD, 5 day) SM
1
10/02/2018 2256 AMR
09/27/2018
2254
521OB-2011
12272
1
(COD) SM
1
10/09/2018 1733 MGM
10/05/2018
1904
5220D-2011
1
(pH) SM 4500-H
1
09/27/2018 2325 SA1
84835
B-2011
1
(Phenolics) 420.4
1
10/09/2018 1121 MSG
10/08/2018
1111
85742
1
(TSS) SM
1
09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1
09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 5210B-
3.5
2.0
mg/L
1
COD
SM 522013-
20
20
mg/L
1
pH
SM 4500-H B-2
6.1
su
1
Phenolics
420.4
ND
0.0050
mg/L
1
TSS
SM 2540D-
25
8.3
mg/L
1
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
q)
Page 7 of 18

Inorganic non-metals
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 521013-
9.7
2.0
mg/L
1
COD
SM 5220113-
58
20
mg/L
1
pH
SM 4500-H B-2
6.7
su
1
Phenolics
420.4
0.056
0.0050
mg/L
1
TSS
SM 2540D-
72
13
mg/L
1
HEM (oil and grease)
1664B
ND
4.3
mg/L
1
LOQ = Limit of Quantitation B = Detected in the E = Quantitalion of compound exceeded the calibration
method blank range
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
B
Page 6 of 18

HEM (oil and grease)
Inorganic non-metals
1664B 10 4.4 mg/L 1
LOQ = Limit of Quantitation
B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
ND = Not detected at or above
N = Recovery is out P = The RPD between two GC columns exceeds 40%
the LOQ
of criteria
H = Out of holding time
W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-002
West Matrix: Aqueous
Description: 0 utfa 11003
Date Sampled:09/26/2018
1850
Date Received: 09/27/2018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1
(BOD, 5 day) SM
1 10/02/2018 2256 AMR
09/27/2018 2254
521OB-2011
12272
1
(COD) SM
1 10/05/2018 1132 MGM
10/04/2018 1600
5220D-2011
1
(pH) SM 4500-H
1 09/27/2018 2320 SA1
84835
B-2011
1
(Phenolics) 420.4
1 10/02/2018 1147 MSG
10/01/2018 1415
85077
Shealy Environmental Services, Inc.
106 Vantage Point Drive
West Columbia, SC 29172
[phone] Fax [phone]
www.shealylab.com
Page 5 of 18

Inorganic non-metals
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Client:Clariant West Laboratory ID:TI27070-001
Description: Outfall 001 Matrix: Aqueous
Date Sampled:09/26/2018 1846
Date Received: 09/27/2018
un rrep rvietnou
Analytcal metnoo Duutlon Analysis Date Analyst
Prep Date
Batch
1
(BOD, 5 day) SM
1 10/02/2018 2256 AMR 09/27/2018
2254
521OB-2011
12272
1
(COD) SM
1 10/05/2018 1132 MGM 10/04/2018
1600
5220D-2011
1
(pH) SM 4500-H
1 09/27/2018 2314 SA1
84835
B-2011
1
(Phenolics) 420.4
1 10/02/2018 1146 MSG 10/01/2018
1415
85077
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method Result Q
LOQ Units
Run
.............
BOD, 5 day
SM 5210B- 41
2.0 mg/L
1
COD
SM 5220D- 91
20 mg/L
1
pH
SM 4500-H B-2 6.1
su
1
Phenolics
420.4
0.080
0.0050
mg/L 1
TSS
SM 2540D-
78
25
mg/L 1
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 18

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Clariant West
Lot Number: T127070
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Outfall001
Aqueous
09/26/20181846
09/27/2018
002
Outfall003
Aqueous
09/26/20181850
09/27/2018
003
Outfall004
Aqueous
09/26/20181855
09/27/2018
004
Outfall005
Aqueous
09/26/20181859
09/27/2018
005
Outfall006
Aqueous
09/26/20181903
09/27/2018
006
Outfall007
Aqueous
09/26/20181906
09/27/2018
(6 samples)
Page 3 of 18

E
Case Narrative
Clariant West
Lot Number: T127070
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Inorganic Non -Metals
Antifoam reagent was added to samples -001 and -006 for phenolics analysis due to the sample matrix.
The antifoam may contribute a high bias to the phenolics results
The pH analysis associated with the samples in this report were performed after the method
recommended 15 minute holding time.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 18

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Clariant West
625 East Catawba Avenue
Mount Holly, NC 28120
Attention: Clay Dunn
Project Name: WWTP Testing
Lot Number:T127070
Date Completed:10/10/2018
10/11/2018 10:47 AM
Approved and released by:
Project Manager: Kelly M. Nance
ra iAM
ACC RE D 1 7 ED
qBQ. xo euc
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Page I of 18

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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Clariant West
625 East Catawba Avenue
Mount Holly, NC 28120
Attention: Clay Dunn
Project Name: WWTP Testing
Lot Number:T127070
Date Completed:10/10/2018
10/11 /2018 10:47 AM
Approved and released by:
Project Manager: Kelly M. Nance
AM
41ag
ACC RE 31 T ED
0 ELFE
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Page I of 18

Case Narrative
Clariant West
Lot Number: T127070
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Inorganic Non -Metals
Antifoam reagent was added to samples -001 and -006 for phenolics analysis due to the sample matrix.
The antifoam may contribute a high bias to the phenolics results.
The pH analysis associated with the samples in this report were performed after the method
recommended 15 minute holding time.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 18

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Clariant West
Lot Number: T127070
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
Outfall001
Aqueous
09/26/20181846
09/27/2018
002
Outfall003
Aqueous
09/26/20181850
09/27/2018
003
Outfall004
Aqueous
09/26/20181855
09/27/2018
004
Outfall005
Aqueous
09/26/20181859
09/27/2018
005
Outfall006
Aqueous
09/26/20181903
09/27/2018
006
Outfall007
Aqueous
09/26/20181906
09/27/2018
(6 samples)
Page 3 of 18

Inorganic non-metals
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172
791-9700 Fax [phone] www.shealylab.com
Client:Clariant West Laboratory ID:TI27070-001
Description: Outfall 001 Matrix: Aqueous
Date Sampled:09/2612018 1846
Date Received: 09/27/2018
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1
(BOD, 5 day) SM
1
10/02/2018 2256 AMR
09/27/2018
2254
5210B-2011
12272
1
(COD) SM
1
10/05/2018 1132 MGM
10/04/2018
1600
5220D-2011
1
(pH) SM 4500-H
1
09/27/2018 2314 SA1
84835
B-2011
1
(Phenolics) 420.4
1
10/02/2018 1146 MSG
10/01/2018
1415
85077
1
(TSS) SM
1
09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1
09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 6210B
41
2.0
mg/L
1
COD
SM 5220D-
91
20
mg/L
1
pH
SM 4500-H B-2
6.1
Sul
1
Phenolics
420.4
0.080
0.0050
mg/L
1
TSS
SM 2540D-
78
25
mg/L
1
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 18

R
HEM (oil and grease)
Inorganic non-metals
1664E 10 4.4 mg/L 1
LOQ = Limit of Quantitation
8 = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
NE) = Not detected at or above
N = Recovery is out P = The RPP behveon two t;C columns cxaoodc 40%
the LOQ
of criteria
I I = Out of holding time
W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-002
West
Matrix: Aqueous
Description: Outfall 003
Date Sampled:09126/2018
1850
Date Received: 09/27/2018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1
(BOD, 5 day) SM 1
10/02/2018 2256 AMR
09/27/2018 2254
5210E-2011
12272
1
(COD) SM 1
10/05/2018 1132 MGM
10/04/2018 1600
5220D-2011
1
(pH) SM 4500-H 1
09/27/2018 2320 SA1
84835
B-2011
1
(Phenolics) 420.4 1
10/02/2018 1147 MSG
10/01/2018 1415
85077
Shealy Environmental Services, Inc.
106 Vantage Point Drive
West Columbia, SC 29172
[phone] Fax [phone]
www.shealylab.com
Page 5 of 18

Inorganic non-metals
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 521013-
9.7
2.0
mg/L
1
COD
SM 5220D-
58
20
mg/L
1
pH
SM 4500-H B-2
6.7
su
1
Phenolics
420.4
0.056
0.0050
mg/L
1
TSS
SM 2540D-
72
13
mg/L
1
HEM (oil and grease)
1664B
ND
4.3
mg/L
1
LOQ = Limit of Quantitation B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 18

R
Inorganic non-metals
ND = Not detected at or above N = Recovery is out of P = The RPD between two GC columns exceeds 40%
the LOQ criteria
H = Out of holding time W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-003
West
Matrix: Aqueous
Description: Outfal 1004
Date Sampled:09/26/2018
1855
Date Received:09/2712018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1
(BOD, 5 day) SM
1 10/02/2018 2256 AMR
09/27/2018
2254
521OB-2011
12272
1
(COD) SM
1 10/09/2018 1733 MGM
10/05/2018
1904
5220D-2011
1
(pH) SM 4500-H
1 09/27/2018 2325 SA1
84835
B-2011
1
(Phenolics) 420A
1 10/09/2018 1121 MSG
10/08/2018
1111
85742
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Numbor Mothod
Rosult Q
LOQ
Units
Run
BOD, 5 day
SM 521013-
3.5
2.0
mg/L
1
COD
SM 5220D-
20
20
mg/L
1
pH
SM 4500-H B-2
6.1
su
1
Phenolics
420.4
ND
0.0050
mg/L
1
TSS
SM 2540D-
25
8.3
mg/L
1
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 18

R
HEM (oil and grease)
Inorganic non-metals
1664B ND 4.4 mg/L 1
LOQ = Limit of Quantitation
B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
NO = Not detectcd at or abovo
N - Recovery is out of P - The RPD between two OC Lolurnns exceeds 40%
the LOQ
criteria
H = Out of holding time
W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-004
West
Matrix: Aqueous
Descrlptlon: Outfal l 006
Date Sampled:09/26/2018
1859
Date Received: 09/27/2018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1
(BOD, 5 day) SM 1
10/02/2018 2256 AMR
09/27/2018 2254
521OB-2011
12272
1
(COD) SM 1
10/05/2018 1132 MGM
10/04/2018 1600
5220D-2011
1
(pH) SM 4500-H 1
09/27/2018 2333 SA1
84835
B-2011
1
(Phenolics) 420.4 1
10/09/2018 1124 MSG
10/08/2018 1111
85742
Shealy Environmental
Services, Inc.
106 Vantage Point Drive
West Columbia, SC 29172
[phone] Fax [phone]
www.shealylab.com
Page 8 of 18

Inorganic non-metals
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 52106-
29
2.0
mg/L
1
COD
SM 5220D-
91
20
mg/L
1
pH
SM 4500-H B-2
6.1
su
1
Phenolics
420.4
0.0051
0.0050
mg/L
1
TSS
SM 2540D-
30
13
mg/L
1
HEM (oil and grease)
1664B
ND
4.5
mg/L
I
LOQ = Limit of Quantitation B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 18

Inorganic non-metals
0
ND = Not detected at or above N = Recovery is out P = The RPD between two GC columns exceeds 40
the LOQ of criteria
H = Out of holding time W = Reported on wet
weight basis
Client:Clariant Laboratory ID:TI27070-005
West
Matrix: Aqueous
Description: Outfall 006
Date Sampled:09/26/2018
1903
Date Received:09127/2018
in Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1
(BOD, 5 day) SM
1
10/02/2018 2256 AMR
09/27/2018
2254
521 OB-2011
12272
1
(COD) SM
1
10/05/2018 1132 MGM
10/04/2018
1600
5220D-2011
1
(pH) SM 4500-H
1
09/27/2018 2337 SA1
84835
B-2011
1
(Phenolics) 420.4
1
10/09/2018 1127 MSG
10/08/2018
1111
85742
1
(TSS) SM
1
09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1
09/28/2018 1052 ARP
84858
and) 1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Unite
Run
BOD, 5 day
SM 5210B-
5.4
2.0
mg/L
1
COD
SM 522013-
54
20
mg/L
1
pH
SM 4500-H B-2
6.2
su
1
Phenolics
420.4
0.017
0.0050
mg/L
1
TSS
SM 2540D-
240
25
mg/L
1
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 18

R
HEM (oil and grease)
Inorganic non-metals
1664E ND 4.4 mg/L 1
LOQ = Limit of Quantitation
B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
NO = Not detected at or above
N = Recovery is Out of P = The RPD between two GC columns exceeds 40%
the LOQ
criteria
H = Out of holding time
W = Reported on wet
weight basis
Client:Clariant Laboratory IU:T127070-006
West Matrix: Aqueous
Description: Outfall 007
Date Sampled:09/26/2018
1906
Date Received:09/27/2018
un Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (BOD, 5 day) SM 1 10/02/2018 2256 AMR 09/27/2018 2254
5210E-2011 12272
1 (COD) SM 1 10/09/2018 1733 MGM 10/05/2018 1904
5220D-2011
1 (pH) SM 4500-H 1 09/27/2018 2341 SA1 84835
B-2011
1 (Phenolics) 420.4 1 10/09/2018 1128 MSG 10/08/2018 1111
85742
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 18

Inorganic non-metals
1
(TSS) SM
1 09/29/2018 1918 KFE
84972
2540D-2011
1
(HEM (oil
1 09/28/2018 1052 ARP
84858
and)1664B
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
BOD, 5 day
SM 521013-
7.0
2.0
mg/L
1
COD
SM 5220D-
21
20
mg/L
1
pH
SM 4500-H B-2
6.5
su
1
Phenolics
420.4
0.14
0.0050
mg/L
1
TSS
SM 2540D-
7.0
4.2
mg/L
1
1 IEM (oil and
1664B
NU
4A
mg/L
1
grease)
LOQ = Limit of Quantitation B = Detected in the E = Quantitation of compound exceeded the calibration
method blank range
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 18

Inorganic non-metals
NO = Not detected at or N = Recovery is out of P = The RPO between two GC columns exceeds 40%
above the LOQ criteria
H = Out of holding time W = Reported on wet
weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 13 of 18

Chain of Custody
MM
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 14 of 18

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 15 of 18

SHEATY MrMONTYIENTAL LABORATORIES
(Aariant-Mow'iL Hugly West
625 R.ast (.'v_,uiwba ek-venUe
"Mount HollvNC 28120
Sample tylic:
--1,s'JJW WV/TP
Chain of CusLody
T127070
Phom,, (70 Fax : ('0104) 8221-2523
IX
sftlnph�'s Coflec'texl By D'?:
Print Print
.Namt: N,� a
_j
w.
'e It
Signature-
Q
Date/Timc 1 CID
samplc Grab or
Location
Vatel Time
Collected
("'Iutf� 11 CID I —L—crab f'�q
Analysis
Requirod-_­­­ J
0&(�. 3OD 01), C, TSS, '_Voial Pbenols, 1
BOD, COD, TSS, Toial Phtnols,
Outfall 003 (Jr ra b 1 (e� I I nH
,__Outfiall 004 Grab
Outfall 0 1
Grab
0 'R
11d, N 0(6�Ori b
Outfall 0 Grab
?raSCII13tiVCq MqUirod : Oil and Grcsys(,�
' Y I
Minguished bv: Date ' T"i m­ c'"
c'6
Rrh,3icuissbed by:
ej
0&0, BOD, ("'i
I Tom' Ptenols,
0&(j, BOO, COD, TSS, I'otal PhenoN,
li?03lJ11 . . ...........
O&G, F301), COD, TSS, Total Phcnofs-I
DIT&SX01) -.-. noncl, COD ­H2SO4.
.Date / 71 Received b y .
Date /Time
)ate ! Timc

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 17 of 18

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tl ID: 4GY: _ _ C:h10 ine' tl'll? IC!_ �� ."_ - Tinted Jar:
rigin 1T tv.17.1jWrattlrc U"Poll 'rec8il t ; (: cr'1ved {n orrectud) tvmperature npon r e eAAnw: °%asol rd Sn,ro-Cup ID-
Method: „ Ti.tt pelature lilt rlk F !Agpinm T' ortIts VTR, 0un [D. � ? TT JR (All) CorCeC`lim Factor: 0 C
Method Of Coolant: Wet lc�- C , Icc. Fac. is -.-J iJrr f" None
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