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HomeMy WebLinkAboutWQ0002376_Residual Annual Report 2018_20190301INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0002376 SUBMITTAL DATED: 2/25/2019 Project Contact Information Rease provide information on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Brent Collins Email Address* Phone Number* brent.collins@emaresourcesinc.com 336-751-1441 Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0002376 Reviewer* Troy Doby Permittee * Chuck Smith Facility Name * City of Reidsville County* Rockingham r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Reidsville Annual Report - WQ0002376.pdf 9.06MB Application Form Engineering Aans, Specifications, Calculations, Etc.) For nein and modification permit applications, the paper copy is required to be subrrutted to the Di, vision Be advised, applications ivill not be considered complete until both the paper and electronic applications have been received_ The paper copy shall include the follo-kAmig: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineenng plan sets • 1 extra set of specifications (in addition to the set of specifications provided in the attachments) • Fee (if required) This shall be mailed to the following address: By U_S_ Postal Service: Division of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigb_ NC 27699-1613 By CourieriSpecial Delivery: Division of Water Resources- Non -Discharge Branch Ag Nathaniel Thornburg- 9th Floor, Office #942WN 512 N_ Salisbury St_ Raleigh,NC 27604 For questions or problems contact Tessa Monday at: 919.7073660 or TessaMonday([ icdcur-goo or Sonia GraxTs at 919.747.3657 or Sonia Graves(dpc&au.gov. * I;W By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Sign Submission Date 2/25/2019 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0002376 County: Rockingham County Year: Facility Name (as shown on permit): City of Reidsville Land Application Operator: EMA Resources Inc. 2018 Phone: 336-751-1441 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 104 Total number of fields utilized for land application during the year: 26 Total amount of dry tons applied during the year for all application sites: 339.22 Total number of acres utilizes for land application during the year: 348.05 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." e5 iA"moi 1ltq Permittee Name and Title (type or print) Signature of Permittee Date .2012 Z:�Z 1/22/2019 Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 4 A* I I M N O O O OO d' N O O a a H 71 (U m 0 C N N N 0 LL x z w 0 ai Q 0 0 U 0 o^o � `O '"•"' �� ^" F N M p p p O p M N O� 0000 00 N N O O O ~ O 00 m N N j N N 0O �D p kn �,O kn O� O O O 0 d M N 00 M v) O 00 N N -" kn 1,O N M N N nj ['� O O O M N N O N in to V1 Ln kn N O M kn N Ln N OC M nj N � N Z O oknO z 00 z z z z ' CL �' z O O R (U m 0 C N N N 0 LL x z w 0 a3 M a M N 0 O O 00 00 lktN O O 'i 0 0 N N m LL U) O LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 37.30 WQ0002376 Cation Exchange Capacity (non 503 only): Ronnie Marshall Owner: Catherine Neal Predominant Soil Series: CgB2 27.45 Acres Permitted: 27.45 Site #: RC004 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Com- posite Date 1 WWTP 4/4/18 21 WWTP 7/13/18 3 WTP 10/2/18 4 5 161 7J 1819 L9J1011 10 11 12 % Solids 1 1.46 1.1 2.18 Arsenic 3 5 15.1 Cadmium 2 1.9 1 0.07 0.66 0.62 Copper 180 204 109 Arsenic 0.000 0.007 0.019 0.000 0.000 0.000 0.000 0.000 Chromiurd 59.9 43.7 33.5 1 0.026 Cadmium 0.000 0.003 0.001 0.000 0.000 0.000 0.000 Lead 61.5 59.8 12.7 0.000 0.004 Copper 0.026 0.271 0.136 0.000 0.000 0.000 Mercury 2.96 0.8 0.0563 0.000 0.000 0.432 Chromium 0.009 0.058 0.042 0.000 0.000 Molyb- denum 5 6.84 2.84 0.000 0.000 0.000 0.108 Lead 1 0.009 0.079 0.016 0.000 Nickel 33.5 21.2 13.1 0.000 0.000 0.000 0.000 0.104 Mercury 0.000 0.001 0.000 Selenium 5 5 5 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- Zinc 509 552 32.9 denum 0.001 Total Phos- horus 15800 20500 1530 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Nickel Annual heavy Metal Field Loadings (Calculated in lbs/acre): Total 121 1 31 1415 61 171 L8J L9J1011 12 DT/Ac./ 0 0 App. a_ Event 0.07 0.66 0.62 y Arsenic 0.000 0.007 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.026 Cadmium 0.000 0.003 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.026 0.271 0.136 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.432 Chromium 0.009 0.058 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.108 Lead 1 0.009 0.079 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104 Mercury 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.001 0.009 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Nickel 0.005 0.028 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Selenium 0.001 0.007 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Zinc 0.073 0.732 0.041 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.846 Total Phos- 2.275 27.183 1.909 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 31.368 horus I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violatio�/ns". ;e� 4;:;: 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 0 3 E a 4 4-�-I 9) iz 0 0 O N LL 2 ry O LL X Z W 0 w � Z c4 N ¢¢ Q Q¢¢ Q O 0 C0 O ' ° Z Z Z Z Z Z Z o 0 0 0 0 0 Q ¢ vs N �j �q � ft3 b y 00 V1 � V1 � � O � ^ Z Z N N N N N 7 V L •,.i C w............. M Ammonia $' 0 0 0 0 0 0 0 0 0 0�� y�� � M00 Nitrogen E N r v 8 N It a n. a Z `c 0 0 0 0 0 0 Ln Ln F�- E r`Vv + Mineralization Rate*** Volatilization Rate** o 6 6 0 o c o a a o 0 a c o 0 0 Application Method* rn CIO V� cn C/� Cr w g o o o 0 0 Cj a 0. - V V V V V V V O h a 0 0 0 N O Q Q Q Q rn U Q 3 Q Q Q U 0 0 o u a d- H Fes- F H H a a 1 �3U 3333333 ¢vim° o�:;:;:: Cn N 74 C4 x U zxrz Ce aoo s, U 0� O M O V ¢ O O O O •-+ C N O N O C .•-� C 0 C 0 C 0 O 0 0 0 O a 0 C O ¢ 0 o N N U � Q O U O o 0 0 0 0 0 0 IDU Q• rj 00 W) d' O M O In .> Cn ''finn M V0 C C d U .. U d U Lj�UO� JOaleQ � � w = = - C8 Qo-UL1♦G. 4 4-�-I 9) iz 0 0 O N LL 2 ry O LL X Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual) WQ0002376 Cation Exchange Capacity (non 503 only): 29.29 Ronnie Marshall Owner: James Albert Predominant Soil Series: NaB 10.7 Acres Permitted: 10.7 Site #: RC005 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solid-. imp, Raw Percent © © d#1• Annuai heavy tvletal P leld Loadings (Ualculated in lbs/acre): Total W 1 21 L_3J m © a 1 71 1 8 LOJ 111112 com- DT/Ac./ _9j *q App. posite a Event 2.74 �. y Arsenic 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Cadmiuml 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.985 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.985 Chromium 0.328 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.328 Lead 0.337 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.337 Mercury 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Molyb0.027 denum denurn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Nickel 0.183 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.183 Selenium 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.027 Zinc 2.786 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.786 Total Phos- 86.489 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 86.489 horus Phos- :�� �. Annuai heavy tvletal P leld Loadings (Ualculated in lbs/acre): Total 1 21 L_3J 141L5J 1 61 1 71 1 8 LOJ 111112 DT/Ac./ _9j *q App. a Event 2.74 y Arsenic 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Cadmiuml 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.985 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.985 Chromium 0.328 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.328 Lead 0.337 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.337 Mercury 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Molyb0.027 denum denurn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Nickel 0.183 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.183 Selenium 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.027 Zinc 2.786 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.786 Total Phos- 86.489 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 86.489 horus I ceruiy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". zfz 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) W) O O Z i Z Q a ° � N O. y O LO O N C ,--i Ccjj O vUi VUi VUi vi C� LL N p O Q 0 0 p 0 0 O. O Z Z z Z O 0 0. V u C C5 Q C G C C C 16 . Q - d N C,� O O O O O O O Q D Q o 00000800c8 N �••� 6 6 0 6 C 00 ': i o y co00 0o a� _ m C as �: E N N N N �O; 40 . h Ammonia m o 0 0 ('3 yN =. 00 Nitrogen E N N N N N N N O N 00 �•" ,_, a 0 H N N N N E f= c o o 04 Mineralization Rate*** o 0 0 o w 2 ^+ c M u Volatilization Rate** o 0 0 o a 0 0 0 Applicationbi Method* x o 0 0 A4 0 W) v1 In kn ..0 M �c O � N' X M U Q Q Q Q C c U N v'1 ca 3U 3333 Ivo 3 3 3 3 = Q o 3 b xz xxxcx ood N O C� kn 00 0 O U 4 h Ol 00 O O O O O O O Q D O O M ?¢ C C C C C O O GO CO G C C7 O C C Q � O � � O 00 113 oE q"Uoyv LU I ° <CaUaa c� Q co 0 O N LL LL 2 cc O LL w Z W C ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): 18.25 Auman French Owner: Michael Bray Predominant Soil Series: CgB2 8.45 Acres Permitted: 8.45 Site #: RC009 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use ing/ke. % Solids use Raw Percent #): 0MVP 01 posite; Date N a _-0 Reid 3 Emma L5J6 NUMBEEM 89 Non 0 12 DT/AC./ ►-3 � App, >v Event 0.54 1.62 y Arsenic 0.004 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Cadmium 0.002 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.182 0.662 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.844 ChromiA 0.048 0.142 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.189 Lead 0.065 0.194 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.259 Mercury 0.001 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- d num 0.006 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Nickel 0.024 Total • .. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.093 Selenium Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 1 41 L5J6 L7J 89 10 11 12 DT/AC./ ►-3 � App, >v Event 0.54 1.62 y Arsenic 0.004 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Cadmium 0.002 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.182 0.662 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.844 ChromiA 0.048 0.142 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.189 Lead 0.065 0.194 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.259 Mercury 0.001 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- d num 0.006 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Nickel 0.024 0.069 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.093 Selenium 0.005 0.016 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Zinc 0.598 1.792 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.390 Total Phos- 24.165 66.543 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 90.708 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". C!:� 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 'Itt 00 +n 00 u u is m O O N N_ Ll. U) LL Q.' O LL w Z W 0 N rL 0. Z U w w w w N O o O 0 O 0 O 0 O 0 0 0 o C 0 Z 0 0 0 0 0 0 0 0 0 a v U O o 0 0 0 0 0 0 O Q .fl •-• (�N 00 'n O "•'" S aO 00 C O O O O O O O M N U cin N N O 0 0© C O O . . U U+ cn N N N E Z Z E cS o :::::::::: o Q Ammonia Nitrogen E ••� � N N ,� a c. v=, N ,p N r_ . . p) pp O O O Ex" rn LA. o 0 0 Mineralization Rate*** o o co o w z o N M M _ Volatilization�, v `� o N � Rate** o 0 0 o y 0 0 0 C6 o c _ Application Method* zn CIO cn CA w o 0 o o c NN r'1r" C V V V V O o Y O a h 00 FH n 3 3 3 3 = a N _ ,a Q 1. 3 •h Vi Vi lA N N w U Ce C O C s. U ti .ty h O o 0 0 0 0 0 0 0 0 0 0 0 0 M _, a¢ Q o v. U `i s.. U o C� 0 o 0 o 0 ami _0 10 N * C O C LC m C N G O u �^ U O C1, Z_ �j = Cj .fl ce U Q 00 o .° m O O N N_ Ll. U) LL Q.' O LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 2.90 WQ0002376 Cation Exchange Capacity (non 503 only): Auman French Owner: Michael Bray Predominant Soil Series: CgB2 6.1 Acres Permitted: 6.1 Site #: RC009 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft . . I posite E © © m © 6 D n L 9 � 111 i0 DT/Ac./ c App. Event 0.48 y Arsenic 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.161 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.161 Chromium 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Lead 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Nickel 0.022 Total Phos- .. �� 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Selenium Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 L2J L3J4 51 6 171 81 L 9 101 111 1121 DT/Ac./ c App. Event 0.48 y Arsenic 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.161 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.161 Chromium 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Lead 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Nickel 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Selenium 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Zinc 0.530 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.530 Total Phos- 21.420 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 21.420 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 2!:4e 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) N � a+ 0 MW Im i Q w A. 12 ai cv� U 74 0 0 N N_ LL LL O LL w Z W 0 M c. U Q O N rUi, C� Z............. O O O R. O O O N O O O O O O O O O O N O N G O 6 0 M : N� � 'O •� M M 'x N N ^ N ' O 4. Ammonia .x o o w c m Nitrogen E w 0 0b. o E- Eo w o c o Mineralization M M O N Rate*** s 0 Volatilization o 0 0 Rate** o o a o o vi Application PP Method* V1 CIO w N •O, aa3eq a c r`C C a - V V h eq -It 10 u dU�o��: M ' 3�33 a. a, °= Ca a U o 0 0 en ... x c o 0 N d � o " c� C O U o 0 • C * N o f > v O p Or > Zi Cdw U o U Z 'Uo gjuOw .i0 03EQ � da..Uaa 74 0 0 N N_ LL LL O LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): Auman French Owner: Dan Stocks Predominant Soil Series 8.4 Acres Permitted: 8.4 Site #: RC010 Field #: 7.97 RnD Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg % Solidg »Cp Raw Porrent iii• . ,v LIJ © © v © L6J 71 8 9 11011111 12 Com- DT/Ac./ c App. Nunn- posite' Event 0.20 0.75 no Date y Arsenic 1 0.001 0.005 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Cadmium 0.001 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.066 0.271 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.337 Chromium 0.017 0.090 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.108 Lead 1 0.023 0.093 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.116 Mercury 1 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- denum 0.002 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Nickel 0.009 0.051 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.059 Selenium 0.002 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Zinc 1 0.217 0.768 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.985 Lhorus 8.775 23.826 0.000 0.000 0.000 0.000 0.000 0.000 0.000 • �� :�� 32.601 .� Annual Heavy ivietal rleld Loadings (Ualculated in lbs/acre): Total LIJ 2 J 3 4 v 151 L6J 71 8 9 11011111 12 DT/Ac./ c App. Event 0.20 0.75 y Arsenic 1 0.001 0.005 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Cadmium 0.001 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.066 0.271 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.337 Chromium 0.017 0.090 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.108 Lead 1 0.023 0.093 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.116 Mercury 1 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- denum 0.002 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Nickel 0.009 0.051 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.059 Selenium 0.002 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Zinc 1 0.217 0.768 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.985 Lhorus 8.775 23.826 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 32.601 11 certiuy, under penalty of taw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�f 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 06 06 0 O U R U Q 0., M e� d U x — pu "I E--, •o a � y � Z 12 N O Q ¢Z ¢ O O O p O O O O O a Z z O O ..' � U o 0 0 0 0 0 0 0 0 0 ¢� Z M 13 0 0 0 0 0 0 0 0 0 M S syr. � +✓ � N N eh %� � h Ammonia o o S w C Nitrogen E m W 00 0 z x O O N E E rn Nv � Cn 0 00 0 0 0 ... Mineralization M Rate*** o 0 o fz Z o N N M V O O O Volatilization . v , o P Rate** o 0 o a 0 0 0 Application Method* v w x o 0 0 o 0 0 OC y N � L a a x V V V y a 0 0 0 N O _ U w � � Q c 333 3F� •cam 333 Q U M�:::: o unun ¢� = O W at > > > cs nQw3 v o USoo�: s. U •� c �p .A O O S S ��; O O O O O O er d• O O O 0 0 0 0 0 0 0 0 0 0 0 0 Q' M O O O � O o o �. � O S OC O S N U dF 'Li Cn f0 M p .� •w N E Ll"OluaOXCI EE[-Z .o Y Q N Q Cd O rO+ tb M 0 O N N LL U- 0 LL w Z w CI ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 11.63 WQ0002376 Cation Exchange Capacity (non 503 only): Harry Sharpe Owner: Daisy Purgason Predominant Soil Series: NaB 19 Acres Permitted: 19 Site #: RCOl l Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #1: Corn- posite' Date Ill L2J3 1 41 1 5 6 7 non 9 10 11 12 DT/Ac./ c App. Event 0.61 y Arsenic 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.207 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.207 Chromium 0.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.054 Lead 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Nickel 0.028 Total • h 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Selenium Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Ill L2J3 1 41 1 5 6 7 8 9 10 11 12 DT/Ac./ c App. Event 0.61 y Arsenic 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.207 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.207 Chromium 0.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.054 Lead 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Nickel 0.028 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Selenium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Zinc 0.682 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.682 Total Phos- 27.540 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 27.540 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z, 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) F, oZ 0 0 U al 3■ 00 a Y! R Ow U L v O a 0 0 N N LL N U- 0 U- X Z W C) Nq q: :: -o U ..• U on .� Q °' p• U U V U �' zea U w w w w N............ OO Z Z Z c. O O S 88 O O IS O O O, V7 0 0 0 0 0 0 0 0 r t{ M M M M N N N N 140- Z Z E 's ,. . N �r .c oo N o 00 rn Ammonia Y O o O 0 O 0 O 0 Nitrogen E NM N N w o rr rr N;:: a a 0 h E 0000 000 011a, Clio, W O O C Mineralization M M M M O N Rate*** o 0 0 o W o N M .. O w Volatilization - S o 0 Rate** o 0 0 o a o c o w S S S kn Application Method 0 0 0 ^ a" x V V V V C O O O N 0 Q Q Q Q � C4O U Q 3 o U o 0 0 R 3333 QUNoOo�..;; �3� o ri .b W cV'V '> '> 'N aT3 b b 'O U z 1�reC4 o00 U O� U O O a Q C O C O C C O 0 0 0 GO O C O O CIO 0 0 0 0 a � •� U .�. o U � M OO O 'ty S C> v # N r0 N v`Oi wl d I •> Ea: o > cam. U U; Z o �U^oQ ujaow v oo o ami 0.00-- CL, v O a 0 0 N N LL N U- 0 U- X Z W C) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 29.36 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Acres Used: Harry Sharpe Owner: Daisy Purgason Predominant Soil Series: 19 Acres Permitted: 19 Site #: RC011 Field #: NaB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kLy. % Solids use Raw Percent #L• Com- .. Date WTP 10/2/18MBOMOU 1 31 4 1 51 1 61 BOUND 1 81 NONEotal LOJ 11 12 DT/Ac./ 0 App. �. Event 0.61 0.93 14 Arsenic 0.004 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Cadmium 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.207 0.203 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.410 Chromiuml 0.054 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117 Lead 0.074 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.097 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.007 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 enum •► .. Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 21 1 31 4 1 51 1 61 1 71 1 81 9 LOJ 11 12 DT/Ac./ 0 App. �. Event 0.61 0.93 14 Arsenic 0.004 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Cadmium 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.207 0.203 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.410 Chromiuml 0.054 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117 Lead 0.074 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.097 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.007 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 enum Nickel 0.028 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 Selenium 0.006 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.015 Zinc 0.682 0.061 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.743 Total Phos- 27.540 2.855 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 30.395 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/22/2019 Date DENR FORM MFLSF (12/2006) rn (D 3 561 r/1 u is is i V Cpl7; �`, N N ° 'y ¢ p• V U V V V V � � Z U w w w s Gi w N pp po .......... z z z z z z O O o O d O '.' a a� U o 0 0 o c o o Q d' 0 Oro a" O U C� ,'�.� l'^ d. '� 0 0 0 0 0 0 0 0 0 0 0 0 M a :. ..a Zcd Z E N N N N w Amnioma x O 0 O 0 O 0 O 0�� � 0 7 N�00 :. Nitrogen E "Zr) a 0 E�E 000, OCCOCC, � '71' w o 0 0 Mineralization Rate*** o 0 0 6 6 o w Z o o M w Volatilization Rate"o 0 o co d d ¢ Q o c a o00 w �' o o kn Application v) to V� V) cn CIO Method* 0 0 0 ryn p,•� O N M;;� ay. a - V V V V V V Oro m O O O N O -� n U •- rr v, R d O 00 m 3 3 3 3 3 Q U eMt et 00 o- N 7i Cn 44 �2 N V) p U •y C� C� 00 �v rt CN O O O O W.. c N N Vi C� 00 d' 0 0 0 0 0 0 M > Q � DD DD 0 IR � 0 0 0 0 (V (Il U v o U b O o a .f1 r0 t6 vii 00 � Vt •y ^fl as N ^ b (D — O.. >.c7 U� U �U¢ TUOW NNMM�o aoa��Q o �•� � a�� �- Q0.Uaa. Ad 0 O N N_ LL U) LL O LL w Z LU 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): Barry Knight Owner: Melba Merritt Predominant So 14.7 Acres Permitted: 14.7 Site #: RC018 4.07 it Series: CgB2 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Corn- .. Date 121 L 3j L.4.f51 1 61 1 7 81 L9]10 on 12 DT/Ac./ 0 App, Event 0.28 Arsenic 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Cadmiuml 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.120 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.120 Chromium 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Lead 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Mercury 1 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- den 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Nickel 0.013 TotalMonona P L :�� 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Selenium Annual Heavy Metal )Wield Loadings (Calculated in lbs/acre): Total 121 L 3j L.4.f51 1 61 1 7 81 L9]10 11 12 DT/Ac./ 0 App, Event 0.28 Arsenic 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Cadmiuml 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Copper 0.120 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.120 Chromium 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 Lead 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Mercury 1 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- den 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Nickel 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Selenium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Zinc 0.343 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.343 Total Phos- 12.631 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 12.631 horus "t cermy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". .Z -e 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) M 22 N O U 0 MF a 3 a� 4, Em X a� N ••� U V Q O � vVi o Z Z o 0 0 0 0 0 0 0 0$ S p, U o, U Z a g .�o $ S$ S S$ o S 0 $ 0 S 0 o o o, 0 0 0 0 0 o o a� y z z E L N w............. c 00 Ammonia CO 0 o 0 o Nitrogen E O �., O �,, O w N o M M N q... a a � 0 0 G m$ S tj rj S O o oho :: E N N W O O O Mineralization Rate*** o c W Z O N M M s o 0 0 Volatilization 0 0 Rate** o o y a. 0 0 0 0 a W w Application Method Ztc S S o o = r. N r in O N m00CA :: 0. V V cs O o O N 3 0 c= U o 00 Q0 co 0 0 i u o Q Y Q � � � •o o d• :;: w ;o b a V o 0 0 rn ... s. U O c U 0 Vl fV N 0 O 0 O 0 O O S O 0 O 0 O 0 O 0 O 0 O 0 < D O O M.. Q Q O C C C C 0 O C O C O C C O C Q O b � � Cn v �. U N O o •'a O� OLn f9 E 4juOw toa;-eQ ° Qavwa v 0 7I' 0 O N N LL U) U- 0 Z w 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 24.17 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Thomas Carter Owner: Mary Stanley Predominant Soil Series: CgB2 Acres Used: 8.5 Acres Permitted: 8.5 Site #: RC019 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Salidc nce Raw Perrent 01• Com- posite;4/4/18 Date 11 Reid 1 411 5 161 171 L8_191 11ol11 1 12 DT/Ac./ App. W, Event 2.24 0.61 14 Arsenic 0.013 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.017 Cadmium 0.009 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.560 0.218 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.778 Chromiunj 0.226 0.072 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0000.298 Lead 0.391 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.466 Mercury 0.004 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.008 d enum enurn 0.022 h . . 0.000 :,. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Nickel nnua eavy e a ie oa ings (Calculated in lbs/acre): Total 11 12131 1 411 5 161 171 L8_191 11ol11 1 12 DT/Ac./ App. W, Event 2.24 0.61 14 Arsenic 0.013 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.017 Cadmium 0.009 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.560 0.218 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.778 Chromiunj 0.226 0.072 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0000.298 Lead 0.391 0.074 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.466 Mercury 0.004 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.008 d enum enurn 0.022 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Nickel 0.094 0.041 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.135 Selenium 0.022 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Zinc 2.633 0.616 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 3.249 Total Phos- 14.330 19.118 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 33.448 horus I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/22/2019 Date DENR FORM MFLSF (12/2006) kn 06 In 06 Zw 0 U Ce w m a R Q a 0 O N _N U- CO LL 2 Of O LL w Z W 0 N CZ O U U oA CLO 4, C o¢ Z cv ww a� N O O O O O O OO O O O 0 O 0 O O O: O O O O O O O O O O' Q � CL N 00 N 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 M M _. 0 0 0 0 0 0 0 0 ��•� �,�� ^ate:: z z M o w............. Ammonia rn oC14 — C eh Nitrogen E a Cn A o p a. ..:... N w 0 0 O Mineralization M M00 Rate*** w o0 0 M v w D O O Volatilization N r- OI0t Rate** a N o 0 0 0 00 t- `� A lication pP Method* o o r. o co co v1 it L . V O w V a H 00 U d -CC- F Y U Q U r-^ n M M O O C� O M et CC, = F, z .� a ' V o 0 0 IU � a, a pp pp pp pppp Q 0 � M � V] O L U p O Cn 00 qjuOw .10 aluct Qa UA.,a R Q a 0 O N _N U- CO LL 2 Of O LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 13.45 WQ0002376 Cation Exchange Capacity (non 503 only): Thomas Carter Owner: Mary Stanley Predominant Soil Series: CgB2 7.1 Acres Permitted: 7.1 Site #: RC019 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mP-/klt. % Solids use Raw Percent #): Com- posite'��M Date 0 N a a 6 7 L8J 0018000 101 ill 1121 DT/Ac./ c App, m Event 1.90 14 Arsenic 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.682 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.682 Chromium 0.227 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.227 Lead 0.233 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.233 Mercury 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.011 Molyb- denum 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.019 Nickel 0.127 h .. :�� 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.127 Selenium Annual Heavy Metal Meld Loadings (Calculated in lbs/acre): Total 121 1 31 41 1 51 6 7 L8J 9 101 ill 1121 DT/Ac./ c App, m Event 1.90 14 Arsenic 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.682 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.682 Chromium 0.227 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.227 Lead 0.233 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.233 Mercury 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.011 Molyb- denum 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.019 Nickel 0.127 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.127 Selenium 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Zinc 1.929 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.929 Total Phos- 59.882 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 59.882 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�z 4;:; 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) W Q a O A. N •� w C V Q O vVi vii vVi � R cq o p a o o p a o 0 • s. Z Z p• s. U d 0 0 0 0 C O C 0 O w ID 00 N U U N N N 6 Z z E w c ++ �„' a. N NS rn o Ammonia Y O 0 O o O m N Nitrogen E `' N `' o c N rn N -- oo •� N .. . a w (21, 00 N a .... rn H � Gz, 0 0 0 Mineralization M M M O o M Rate* « Volatilization Rate** a 0 0 0 a w Application Method* co o v c a - v v v 0 ��g3000 =voo— N d' oo �a�U 333¢U�o�OM: p v un X O N N C-1 W t IZI Z oppo � M Cq y a U U 0 0 0 M: •b 70� O ao 0 0 0 0 0 0 0 O sy. a .?: Q F kn O 7 M 0 0 0 0 0 0 0 0 0 Q' •-+ O ••• M C o o c o o d o d o 0 0 o c o o o v a p b ON O N Vel > r- O « .E L) LPUOW ao al -ea o ° �i O i�-� U C n ¢� a N Q 03 O bb 0 0 N LL U) LL C� O LL x Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): 20.55 Alton Pearson Owner: Alton Pearson Predominant Soil Series: CgB2 9.3 Acres Permitted: 9.3 Site #: RCO22 Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use meg/kff. % Solids use Raw Percent 01- OR 1VVj .EM 1 L3J4✓ o © o 9 10 11 12 Corn- DT/Ac./ 0 App. Non .. Event 0.51 1.70 no on i Date Arsenic 0.003 0.010 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.014 Cadmium 0.002 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Copper 0.172 0.613 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.784 Chromium 0.045 0.204 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.249 Lead 0.061 0.209 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.271 Mercury 0.001 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Molyb- denum 0.006 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Nickel 0.023 0.114 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.137 Selenium 0.005 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.022 Zinc 0.566 1.733 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.299 Total Phos- 22.860 53.783 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Total- 0.000 0.000 76.643 horus • . �� ;�� .. Annual Heavy lvletal field Loadings (Calculated in lbs/acre): Total 1 21 L3J4✓ L5J L 67 8 9 10 11 12 DT/Ac./ 0 App. Event 0.51 1.70 Arsenic 0.003 0.010 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.014 Cadmium 0.002 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Copper 0.172 0.613 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.784 Chromium 0.045 0.204 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.249 Lead 0.061 0.209 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.271 Mercury 0.001 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Molyb- denum 0.006 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Nickel 0.023 0.114 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.137 Selenium 0.005 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.022 Zinc 0.566 1.733 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.299 Total Phos- 22.860 53.783 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 76.643 horus 1 certily, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z: 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) (T�O;I�=Io Tj i 6 u L LIVA 3 3 E a Ri Q M Cp 0 O N LL U) LL O LL x Z W 0 N U a4 . w O � ¢ R ai ai vVi vVi C�. cOi O ,' a L � N Q d Q �' 0 0 0 CCC 0 0 0 .......... o O � Z z Z Z 0 R Q N Q O O O G O p O C O R O M O O O O CC O O O ,.. y 4 N N eh a b ::: w Ammonia ;' 0 0 0 0 g c oo. 76 Nitrogen E W) N Vn N N N «� N N N V7 O\ C06 ...' a a 6 Z Y o 0 o N E� E Mineralization M M M M O Rate* L u CQ C> v'i vi Volatilization v, �n v) v-, a O N N Rate* * c o 0 o Q o e+ v? 0 Application Method* V) Cr w c�N�:.:.. co 0 0 0 - V V V V v o w _ ZZ 05 U Q Q Q a Q ° U o N Y 0. 0 00 tea- h H H� 1 *0 3 3 3 3 Z O M M~ 'C w C4 G 77w 0 0 0 O R ¢ 0 0 0 FOM 00 N 0 0 0 0 0 ¢ 0 00 vii `O ' a¢ O C C •--� O GO O C 0 0 0 0 C O O Q O O ~ Chi '� V •y N# U b !�, N 'O 0 O O O O O O O O Gl ;> # O E c I N 9 U U Z �N Lito"OOZ, N N o o° a E H Q d U L1. 0. Ri Q M Cp 0 O N LL U) LL O LL x Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 6.33 WQ0002376 Cation Exchange Capacity (non 503 only): Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series: CaD 11.6 Acres Permitted: 11.6 Site #: RC041 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite _-Date,mm 11 2 131 4 5 6 7 181 9 1101 [11j 12 DT/Ac./ o App. Event 0.55 Arsenic 1 0.003 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.003 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.002 Copper 0.197 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.197 Chromium 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Lead 0.067 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.067 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 denum . , ..�EEEEEEEEEEE M Nickel AnnualHeavy Metal Field Loadings (Calculated in lbs/acre): Total 11 2 131 4 5 6 7 181 9 1101 [11j 12 DT/Ac./ o App. Event 0.55 Arsenic 1 0.003 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.003 Cadmium 0.002 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.002 Copper 0.197 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.197 Chromium 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.065 Lead 0.067 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.067 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 denum Nickel 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Selenium 0.005 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Zinc 0.556 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.556 Total Phos- 17.254 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 17.254 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z; 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ZW I � P4 0 Le Pt wa LO ro N U U ou .2 Q U Q O � Cd vvi rVn - od' Soo Z Z o 0 o 0 0 o c� Uo Q N p O O O O p°p O cbbc�� C P O O j . ..r cd Z 2 E � ............. Ammonia Nitrogen E C. w a� V1 00 M o n oo a z x o o E Nv fs c o p 00 . Mineralization M M O m00 N >: Rate*** o co w Z o rr �n M u w Volatilization o M Rate** 0 w r`"� g o o r Application Method xbf c o c V S. V V O N N C� O w v °° �� °3a� � 33 C C CA_ °Ca�3 d ts0 N r, M Or ry bb a V ooa xz z� ° o. sem. c O e* 0 0 0 0 0 0 0 0 0 0 O oM0 tl; 0 N M 0 0 0 0 0 0 0q 0 >° Q � .� �V o dam• v' 0 o O O O O U # C N M ° a• > -. b N O > �U U a w V "1 ° 71 U i�jUoy� �o � � � o l✓ zo a��Q d o a U a. 0 I R$ Q a 0 0 N N_ LL U) LL O LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series: 6.8 Acres Permitted: 5.54 CdB2 6.8 Site #: RC041 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . Com- posite Date 1 © © 1415 © D 7 8 91 10 11 1121 DT/Ac./ c App. Event 0.82 Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.005 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.293 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.293 Chromium 0.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.098 Lead 0.100 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.100 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 denum Total Phos- .. :�� Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 L2J 131 1415 6 7 8 91 10 11 1121 DT/Ac./ c App. Event 0.82 Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.005 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.293 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.293 Chromium 0.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.098 Lead 0.100 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.100 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 denum Nickel 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 Selenium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Zinc 0.830 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0000.000 0.000 0.000 0.830 Total Phos- 25.754 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 25.754 horus 911 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z. -e 4;:;_ �''_ 1 /22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 00 146 00 O U a Q C� N s O U O y �0 o Z L U ° Z G a, .Q `p C v C a U z�oq a 'E O •> � ^ U o ° � o Q;a U N a 0 o 0 0 0 0 0 0 0 o 0 S OO S o a C 0 o Z o o p•, t j C C O O C C C GO C C C C: Z? 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 00 0 o 0 d 0 o 16-4 0 U N CO O O O C C C O C O C N :: U C) N Z Z G w.......... ccc N 0 00 00 00 Ammonia x o Nitrogen E a CL m O f� Mineralization M O v o`O, n :. Rate*** z c M s Volatilization Rate** 0 x 0 0 0 0 y P6. w S o o ... Application Method* o o c ^ V ° a N 0..C. O •o c o C 00 -It r40 v'UQ3� Ca ° U o d o ca U N M 3 3 Q U a O W a Q ami 3 •> o .7 y M �' Z U C O O L V ,b Uw O O O C O 0 O 0 0 0 00 0C O O N Cn ¢ 0 U M U � c120 o �b O � � � .fl •7E � N C C > c d 40 U � IncJ LIJUOW ;z .10 awQ ,D F o � '� � 6.. � U C� s O O y �0 o Z L U ° Z G a, .Q `p C v C a w z�oq a 'E a o Z U o ° � o Q;a 0 0 N_ U- fA LL O LL I' Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 23.38 WQ0002376 Cation Exchange Capacity (non 503 only): Donald Lovelace Owner: Lofton Lovelace Predominant Soil Series: CgB2 19.4 Acres Permitted: 19.4 Site #: RC041 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ..-.o Com- ii •• MENE 3 J 14151 o 0000000 L8J 1111 1121 DT/Ac./ o pp App- Event Event 0.33 0.88 14 Arsenic 1 0.002 0.005 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.007 Cadmiuml 0.001 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.005 Copper 0.111 0.316 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.427 Chromium 0.029 0.105 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.134 Lead 0.039 0.108 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.147 Mercury 0.001 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.004 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 denum Total • .. i� :�� Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total L2J 3 J 14151 6 1 7 L8J 19110] 1111 1121 DT/Ac./ o pp App- Event Event 0.33 0.88 14 Arsenic 1 0.002 0.005 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.007 Cadmiuml 0.001 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.005 Copper 0.111 0.316 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.427 Chromium 0.029 0.105 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.134 Lead 0.039 0.108 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.147 Mercury 0.001 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.004 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 denum Nickel 0.015 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.074 Selenium 0.003 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Zinc 0.365 0.893 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1.258 Total Phos- 14.760 27.713 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 42.473 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�z 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ik 3k O a MW 3 r A • U a� N 3 O •C L ' � 0 bA °c. ^ O � •� U V a+ u U r=r !r 07NO CCS ,-1 a c O Z CJ C 0 p •CJ do = eue U Q, R R R{ O G> s� _ E U Q `n" U U U U • •L O N �r �'•' _� �i O R .G U G7 px C d N a o 0 0 0 0 0 g o o O Z z Z Z 0 0 0 0 0 0 O O o 0 o c o o c c c z`D G. vi o 00 00 �n `O M 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 00 M 4 00 0 0 0 0 0 0 0 00 O N U cr� ,�„ C C C C C C C C :: a z �z E N N N N N ::i:.':':':'::':':: o W............. s S~ oo °„ o0 � o, Ammonia x o 0 0 0 0 0 o 0 Nitrogen E N N N N y N o. ry N _ a o. 0 r N N N M E'•' E 00 O� OD Q� N et N � W O O O Mineralization M M M M O Rate*** o 0 o c> w Z o ? 4 M Volatilization Rate** o 0 0 y O y iZl w Application Method* CnV� CII) C xbf o 0 0 r o c ^ o 02 c V V V V O 0. G tV cV N J. w _ �3 o O N N v Q N QGo 5a^ HHH N p" w iYr U N N M ' xz C4C�Cerx 000 � V •=3 O M 'n 0 0 0 0 0 0 0 O 00 O1 O C O O C C C O C C O G O O O � O 7 �C O ^ � o Cq kn j D O U un U Z gjuOw ao alzQ o •3✓ � � U 0., 0 R O •C L ' � 0 bA °c. ^ Z V a+ u r=r !r 07NO CCS ,-1 a c O Z CJ C 0 p .p do = eue U Q, R R R{ O G> s� _ E a+ u ++ U p = • •L O N _� �i O R .G U G7 px C cd Q 0 0 N LL c(j) LLL O LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Johnie Carty Owner: Johnie Carty Predominant Soil Series: Acres Used: 11.4 Acres Permitted: 11.4 Site #: RC 118 Field #: 14.38 CcB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite 1 2 j 3 4 5 6 7 8 9 10 11 12 DT/Ac./ oyr App. Event 0.76 0.50 14 Arsenic 0.005 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Cadmium 0.003 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.275 0.203 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.478 Chromium 0.092 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.135 Lead 0.094 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.153 Mercury 0.005 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.008 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 enum Total •.mM phorus ENEEMENEEN Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 j 3 4 5 6 7 8 9 10 11 12 DT/Ac./ oyr App. Event 0.76 0.50 14 Arsenic 0.005 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Cadmium 0.003 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.275 0.203 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.478 Chromium 0.092 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.135 Lead 0.094 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.153 Mercury 0.005 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.008 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 enum Nickel 0.051 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.072 Selenium 0.008 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.013 Zinc 0.778 0.549 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.326 Total Phos- 24.142 20.377 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 44.519 horu5 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". zl�z 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) M w 0 0 04 N U- U - 0 w Z w 0 Li y •� � .O Q N O O 0 Oo 0 Q �' O 0 O O O O O S ... •Q., 0 0 0 0 0 � � j o 0 0 0 o c o o co 0 0 Q � 9 0 0 0 0 0 0 0 0 0 0 0 0 0 00 0 0 c�• o o � 0 0 0 0 0 '~ w............. w O c 'A � Ammonia °' o o Nitrogen E `'' a a• � 0 0 Ex EN �t 'C et Mineralization M M O Rate*** 0 0 w Z o N M M Volatilization o o Rate** 0 0 a 0 0 fz Application Method* O 0 0 0 ^ M ^ a) 2 � �r C V V p Or . � N; O CSS TT .� V] Q D Ca O C> O N uF. d00 CA C0 M .'.. 3 �✓ v 0 3 3 Q' U eF M 0 0 0 ,,, � Cn X ' > eh E w .b ^ � U o 't � U Q C C 0 0 0 0 0 0 C C O C G O O j Q o b � O U 0 O U N N O O O O o N U O C'4 cV� d M a c M y U O .� Cd � ¢ gIuOw 10aU Q ° Q a v a a M w 0 0 04 N U- U - 0 w Z w 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Johnie Carty Owner: Johnie Carty Predominant Soil Series: Acres Used: 5.6 Acres Permitted: 5.6 Site #: RC 118 Field #: 4.75 CcB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . •-• Com - .. Date W .. ; © © w © 61 on n OMENS 11 J 0 DT/Ac./ c App' r. y Event 0.85 .. Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.305 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.305 Chromium 0.102 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 Lead 0.104 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- denum 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Nickel 0.057 phorusMENEENEENEEN 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.057 Selenium Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 21 3 4 5j 61 L7J8 9 10 11 J 12 DT/Ac./ c App' r. y Event 0.85 .. Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.305 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.305 Chromium 0.102 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.102 Lead 0.104 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.104 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- denum 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Nickel 0.057 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.057 Selenium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.008 Zinc 0.863 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.863 Total Phos- 26.797 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 26.797 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) a rd U E R Z CL U CU Q Z x U w a Q N O. Q O O pp O O O O O O O O O p O O O O O p O O O: O O z O O O O O O O O O C7 O O Q� Q �- o a" ooSS000<; tj N �. S .• � rq M d N .c _ � � ;:: O Ammonia O>Y oN Nitrogen E o N :: a d h w V) y V] c o h C � 00 � Z x o F-' � N Mineralization M O kn n o :: Rate*** o w z o •h: h s o W-� vi Volatilization Rate** 7 w oc hW) C4 h ,, ...... Application Method* x o 0 0 R - 'p U Q 3 Q = U N M u �tj����: a 3 o a� RG U� O c o y U C't 0 QQ O O C 0 N op 0 0 0 0 0 0 0 6 0 0 0 0 O 0 0 0 0 Q' O N O �' �n r`O•, :: : ? a O O C O G O O C C O C C O C Q O O U CA n, co 0 0 o 00 y d y U Z E U Z c�U rsQ TU'Dw .10 a1rQ a� o H Qo.Uaa 71 0 0 N LL U) LL 0 LL w Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): Thomas Carter 7.1 Owner: Thomas Carter Predominant Soil Series: Acres Permitted: 7.1 Site #: RCI 19 Field #: 0.79 CgB2 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date 11 L2J31 L_4j 1 51 L6J71 1 81 L9J10 11 1 12 DT/Ac./ c App. rt Event 0.11 y Arsenic 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.040 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.040 Chromium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Lead 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Nickel 0.007 Total ' .. 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Selenium Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 L2J31 L_4j 1 51 L6J71 1 81 L9J10 11 1 12 DT/Ac./ c App. rt Event 0.11 y Arsenic 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.040 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.040 Chromium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Lead 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Nickel 0.007 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Selenium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Zinc 0.113 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.113 Total Phos- 3.508 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.508 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". zl: 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ^O •C N Z N ai o, U x LA R, Q KE H, a3 Q M a 0 0 N N_ LL U) LL 2 ry O LL 0' Z W 0 N o � U Q vUi " a Z O Q ,O 00 0 0 0 Q. 10 0 0 0 0 0 0 00 0 0 0 0 'o a O M 0 0 0 0 0 0 0 0 0 0 U U. TS ai z m N e a �: z i M w............. Ammonia c M Nitrogen E d d 0 w M M o z y S E � o 0 0 Mineralization Rate*** C w Z o r M o M s M Volatilization wn O p N N Rate** o °, � o c o 0 n, 0 H w g (N rn r Application Method* x o 0 0 C O ry y aceq a,ts c V O �"' N :: CL+ vi O d• O rn O1 N C4 u a � do• r '" oo � d F., 00 U t U N N o p t y S WI '. CS.N .� G:r b y F+1 U O M i y.� O p w, U a N _ O S O O O O O O p O O O 000000 �p C C C C C C C C C 0 O C 0 0 ? Q O CO Q O � � U R3 # O U N v C p S p O J > " U L =S U o U d Ll"OluaOXCIu cv. CL p.. a3 Q M a 0 0 N N_ LL U) LL 2 ry O LL 0' Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Thomas Carter Owner: Acres Used: 19.1 Acres Permitted: Thomas Carter 19.1 Site #: 15.03 Predominant Soil Series: CgB2 RC 119 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date 1 11 © © L4 © 6 7 L 89 10 Em 12 DT/Ac./ 0 App. Event 0.79 •' Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.283 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.283 Chromium 0.094 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Lead 0.097 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.097 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 denum . . • , ..IENEENEENEEN M Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 11 2 J 3 L4 5 6 7 L 89 10 11 12 DT/Ac./ 0 App. Event 0.79 •' Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.283 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.283 Chromium 0.094 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Lead 0.097 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.097 Mercury 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 denum Nickel 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.053 Selenium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Zinc 0.801 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.801 Total Phos- 24.869 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 24.869 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 2:fle 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O E. a` � U x w � 0 Mr 'O N 'C3 N CUC (� ❑ O. •Cj � Q = U U U V G '�'� Z N O Q Q Q Q O ppp S o o pp Z Z 2 ZC O O O O O ty �j O C C C CO C C CO Q 0 0 U ai o0 M Oi O O C G C C C C N i IU rn 00 b❑ 'y 00 00 00 c�3 ',�^ N Z N N N N w............. s om" o, o Ammonia x 5 0 0 o N Nitrogen E N N N N N N N N oc o r M 4i a 0 Gz a) o O co a d• et pp z S o 0 o H EN d- N � N � N �• For. o co d Mineralization M M M M O 1r O Rate*** o c c o Z c M u R w Volatilization o g C) Rate a w o �_ N Application� Method* Cf) CIO CIOw Or- x o C o d -It h �. y u 00 a oo0 :. ;.. u 4 3 3 3 3 3 d U ry 0 O cu N Q a y N N N u Q O ce CYi p p L U v y ch et O O b 0 0 0 0 0 Vl D, d• V O O .-. H N O �+ •-+ M 0 O 0 O 0 O 0 O 0 C C O O ? C Q O C C O O C O C C C O C C O C Q 0 c O U a O p o 0 0 0 g y ro C7 cd v ce 6 " .i oa, > cu � U 0U d �v T�¢ y Y gjuOwo n c\ c\ O .ti O Qr. 0,Uwa H 0 0 N N_ LL U- 0 LL it Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 7.91 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 Acres Used: 8.5 Acres Permitted: 8.5 Site #: RC 119 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): C R rM Com- posite ___Date;NMMM E 2 L3J on ENEWEENNON 61 1 71 81 1 91 101 11 12 Ali , � • ___________ APP• y Event 0.93 Arsenic 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.335 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.335 Chromium 0.112 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.112 Lead 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 denum Total Phos- .� :�� Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 L3J L 4 51 61 1 71 81 1 91 101 11 12 DT/Ac./ APP• y Event 0.93 Arsenic 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Cadmium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Copper 0.335 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.335 Chromium 0.112 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.112 Lead 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 denum Nickel 0.062 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.062 Selenium 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.009 Zinc 0.948 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.948 Total Phos- 29.420 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 29.420 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/22/2019 Date DENR FORM MFLSF (12/2006) kn 00 W) 06 U 04 Lay t5 M 0 0 n LL U) LLO LL Cr Z W a Z U w N Z O O O O S pppp O 0 O 0 O 0 pppp O 0 O 0 O O : O 0 0 Q � _ O S pp O S S S w.. ... ... v M 00 00 M N Ammonia Y' S S N Nitrogen E N p O\ a 0 fA a, 00 r- O� O S vl Z O Cq O F E N N L/1 O i/i eh 00 0O .' Mineralization M M O � o n� :::::. Rate*** o co "0 S Z o O N X Volatilization ., c Rate** o o a o 0 0 0 y w wbfS o o Application Method* Ln O N M c w ti v/ O O O 1w... U .. . O oo Q� Q' O M M ? O Q � O U 0 0 0 0 -Uo � b d oar E_� p O a U Ll. O w v >��z -�¢ ULIIUOW ao alt'Q F M 0 0 n LL U) LLO LL Cr Z W a ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 16.83 WQ0002376 Cation Exchange Capacity (non 503 only): Thomas Carter Owner: Thomas Carter Predominant Soil Series: CgB2 13.5 Acres Permitted: 13.5 Site #: RCI 19 Field #: 9 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- .. ,MEMBEE posite 11 L2J31 1415 Nunn L7J ENEM 101 11 J 1121 DT/Ac./ O App. Event 0.94 0.31 " Arsenic 0.006 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Cadmium 0.004 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.338 0.126 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.464 Chromium 0.112 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.139 Lead 1 0.115 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.152 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.009 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 denum Total • .. Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 L2J31 1415 6 L7J 1 81 9 1 101 11 J 1121 DT/Ac./ O App. Event 0.94 0.31 " Arsenic 0.006 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Cadmium 0.004 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 0.338 0.126 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.464 Chromium 0.112 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.139 Lead 1 0.115 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.152 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.009 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 denum Nickel 0.063 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.076 Selenium 0.009 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Zinc 0.955 0.341 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.296 Total Phos- 29.641 12.669 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 42.310 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ze�z 4��_ 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) W" w O MW a Gdi 2 51 M 0 0 N N_ V1 U- 2 O LN LL Z W 0 N O O 0 0 O 0 0 0 0 0 0 0 0 0 0 0 0 O: .-. Z Z Z 0 Q Z Q •� p O. M v'I O00 O00 :; to R' O C O O 6 O O .: ~ (j v1 N O C C O O C C O CO C 00 . U � C• C p1 d' 7 N i" Q,,, M m ............. (� M N O M Ammonia Y o 0 0 N Nitrogen E `! N M a H E ��j• V] W V] C O C Mineralization M M M O Rate*** O C C 6 M 0 0 0 ,. .= Volatilization Cq Rate** o 0 0 c N N 0 0 0 0 G� w c 0 Application Method* V� CnC/I = 0 0 0 0 V V V CL,- �a o _ 00 r CA Q y q �1 Ca o U o rr u =3E� 333 QUd roM (� 'O kn N t- o 00 00 y U o 0 0 s. U U u O •� vNi 7 M O O S 0 0 0 0 0 0 Q O ... M Q O Q Q Q o b e o U C o a o o O o 0 0 0 0 N ># f6 N a o�_ o > Cz gTUOW N N o 51 M 0 0 N N_ V1 U- 2 O LN LL Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Gene Small Owner: Harvery Albert Predominant Soil Series: Acres Used: 9.9 Acres Permitted: 9.9 Site #: RC 125 Field #: 16.73 NaB 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 4/4/18 __2j 7/13/18 3 J 10/2/18 4 151 6 71 1819 1 101 [111 12 % Solids 1 1.46 1.1 0.6 Arsenic 3 5 5 admium 2 1.9 2.71 0.84 0.57 0.28 Copper 180 204 217 Arsenic 0.005 0.006 0.003 1 0.000 0.000 0.000 0.000 0.000 hromi I 59.9 43.7 46.4 0.014 Cadmium 0.003 0.002 0.002 0.000 0.000 0.000 0.000 Lead 61.5 59.8 62.1 0.000 0.007 Copper 0.302 0.233 0.121 0.000 0.000 0.000 Mercury 2.96 0.8 0.996 0.000 0.000 0.657 Chromium 0.101 0.050 0.026 0.000 0.000 Molyb- denum 5 6.84 7.52 0.000 0.000 0.000 0.176 Lead 0.103 0.068 0.035 0.000 Nickel 33.5 21.2 23.3 0.000 1 0.000 0.000 0.000 0.206 Mercury 0.005 0.001 0.001 Selenium 5 5 5 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.008 0.008 Zinc 509 552 620 0.000 0.000 0.000 0.000 0.000 0.000 0.020 denum Total Phos- horus 15800 20500 22800 Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 11 1213 41 L5]6 1 71 L8j9 1 1101ll 12 DT/Ac./ oyr App. Event 0.84 0.57 0.28 Arsenic 0.005 0.006 0.003 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Cadmium 0.003 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.302 0.233 0.121 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.657 Chromium 0.101 0.050 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.176 Lead 0.103 0.068 0.035 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.206 Mercury 0.005 0.001 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molyb- 0.008 0.008 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 denum Nickel 0.056 0.024 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.093 Selenium 1 0.008 0.006 0.003 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.017 Zinc 0.854 0.631 0.346 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.832 Total Phos- 26.512 23.452 12.722 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 62.687 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z�z 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) rn rn ii il� 1 Z R Z N i U 00 r- Im A 7 C c .i 1 C� N .t� �+ � � C o ^d U 4w L O ^ O p d •p O y bA o U � C � ~ U oo.2 Z w un C v L: Q bA R R O O w a c� yy Com' b� z U w w 6 w ai w v w u w N Z Z Z 0 0 0 0 0 0 O ' Z Z Z Z Z Z Z Z o co o c c o o D Q fA CY e1• e} 0 0 0 0 0 0 0 M M00 0 0 0 O 0 0 0 .r m • • • i, r7' 7 N N � V Q., � 411 Ammonia � N Nitrogen E N N N M n M n O O � 00 -• O et ;. a x' m N rr £ N N N 00 00 O O Vi Lir V] O O O O O 00 O .:.;. N N Mineralization M M M M M M 0 M 00 D\ "t 't Rate*** o 0 0 6 6 o s z o 6 o M Volatilization Rate** co o d o 0 o a 0 0 o o 0 co 0 W6 w o 0 _ 0 Application Method* Cncf� V) CrC/� V� o 0 0 QI N M a _ V V V V V V O O N O U c o c h CD en M — 3 3 3 3 3 3 3 d v C�� M o o w > ; ; Cqc 0. V o o c N ¢• y7 sU, C 00 QO 0 �D d• M^ M "D 0 0 0 0 0 0 0 0 0 0 0 0 d• M N M U ? ¢ d O G O O C O 0 0 0 0 0 0 O O C Q � O O p U a. n X U v v 0 o 0 0 0 0 o c O v O O v1 O N M i •� •7F N In IW •� vNi [� ? �'•' d � v 6. a0 V O J o « >� v Uz �U-1:id v Q 14luow EM4 o .10alua��oo �.� Q 0. U Q 0. F- C� .t� �+ � � C o N ut R 4w L O ^ O p d •p O y bA � C � Z w un C v L: 2 bA R R O O w a c� yy Com' b� O R G> •x so, M cfl 0 0 N N_ U- U - 0 0 w w Z w ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 5.94 WQ0002376 Cation Exchange Capacity (non 503 only): Gene Small Owner: Harvery Albert Predominant So 9.5 Acres Permitted: 9.5 Site #: RC125 it Series: CgB2 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . -INEEN posite Date 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ 0 App. r+ Event 0.63 1 4 Arsenic 1 0.004 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.225 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.225 Chromium 0.075 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.075 Lead 0.077 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.077 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.006 Total Phos- i phorus MENEENEENE00- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 d num Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ 0 App. r+ Event 0.63 1 4 Arsenic 1 0.004 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.225 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.225 Chromium 0.075 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.075 Lead 0.077 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.077 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 d num Nickel 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Selenium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Zinc 0.636 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.636 Total Phos- 19.750 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 19.750 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ;!!:fe 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) M N_ `r' U �G i� i� 0 iz O Ix iS L a Q C, 3 s Q 0 a 0 0 N LL U) LL 0 LL It Z W O U ,--� U bq .2 O, •U Q O V z U w O o a o 0 0 0 0 o o o Z o 0 0 0 0 00 0 o Q Q 0 a� U c o 0 0 0 0 0 0 0 0 c o Q ti z n o0 0 0 o 0 Q 0 o 0 4c� o 0 o a o rn r. °O00 C+ 0 0 0 0 0 0 c N U O O O O O0 O O O Q O ..• a r zz E N w 0 Ammonia rn N Nitrogen E p N T a � o z Y o w o o H E Mineralization 0 rn N orZ Rate*** o M Volatilization " C Rate** o 0 0 0 0 0 0 0 w w 90 0 0 Application Method* V� 0 o c N N _ O r M O :: CS w 0 �U��3� Q •°�- U O M e1• 0 0 0 d V v M '. 'O Q U 'O ✓� O O O y U U A~ p O N G N �O Q Q O O O O O O O O O O p O O O O O O O O M M R a O O C C O C C C 0 0 0 0 0 0 0 Q � � � o O U a. � U U O � � O �p �• N Ce O ;t4 .� �U �Q LITUOW 103JUQ � � raU CL. P, Q 0 a 0 0 N LL U) LL 0 LL It Z W ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Gene Small Owner: Harold Sharpe Predominant Soil Series: Acres Used: 25 Acres Permitted: 25 Site #: RC 125 Field #: 20.38 RnD Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): PEM .•,o Com- posite .Date 1 11 © © v © v v o v 10 Ill 12 DT/Ac./ _5j App. Event 0.67 0.15 14 Arsenic 0.004 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Cadmium 0.003 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.239 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.305 Chromium 0.080 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Lead 0.082 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.100 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.007 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 denum Total Phos- phorus Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 11 1 21 L3J4 6 1 71 8 9 10 Ill 12 DT/Ac./ _5j App. Event 0.67 0.15 14 Arsenic 0.004 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Cadmium 0.003 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.239 0.065 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.305 Chromium 0.080 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.094 Lead 0.082 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.100 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.007 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 denum Nickel 0.045 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 Selenium 0.007 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.008 Zinc 0.677 0.186 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.863 Total Phos- 21.01.4 6.840 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 27.854 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/22/2019 Date DENR FORM MFLSF (12/2006) W) N N U M Mr N b 4. O I u is is RS N .0 w � C o � U ar N "O f1. O y N � •� O O U .= V1 -• a U cq .� ca Q tin R Q. Z21 C6 U Z U w w w N O pp p .. z Z z z ¢ J U C C C C C C C C C 0 Q N Zy _ eq c S S S S S S S S S a 0 0 0 a; o o 6 0 0 0OC o c c o U y °O00v rn w . "' n � °° O0 C, O ' Ammonia0 O 0 O 0 Nitrogen E C'q � d O o E^ E 7" UA GTr Ln O O O O. O 000 N Mineralization Rate*** a+ Volatilization v v o c c c Rate** C C C Q C C o 0 w w 0 0 Application 0 r Method* 0 0 0 O ..5� O N CL N VJ N L v1 v1 V1 a a y v v v C � U o 0 0 O ECn 3 3 3 y > > M 110 a, ��,w3 ebb av000M:;:: y V "d C.�-� N U O ¢ M M •-� O O O O ? C C C 0 0 GO C O C O O C C C 0 O o y a •C1 y.- O O O O O O O v7 NN N > •�' dF er •k N E > � U5 7;LIJ>- uo I/� M N Q .10 alluQ O O G. U C1. 0. RS .0 w � C o � ar N O y bA a ca tin R Q. Z21 C6 U 0 0 0 N U- 0 LL x Z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): 94.79 WQ0002376 Cation Exchange Capacity (non 503 only): Auman French Owner: State of N.C. Predominant Soil Series: CgB2 34 Acres Permitted: 34 Site #: RC 126 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Com- posite: D.. 1 11 21 31 1415j 6 1 71 81 9 1 1101ll 1 112 DT/Ac./ oyr App. Event 2.35 0.44 Arsenic 0.014 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Cadmium 0.009 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.588 0.179 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.766 Chromium 0.237 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.275 Lead 0.411 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.463 Mercury 0.004 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.024 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 denum Total Phos- .. �� �i Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 11 21 31 1415j 6 1 71 81 9 1 1101ll 1 112 DT/Ac./ oyr App. Event 2.35 0.44 Arsenic 0.014 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Cadmium 0.009 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.588 0.179 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.766 Chromium 0.237 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.275 Lead 0.411 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.463 Mercury 0.004 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.024 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 denum Nickel 0.099 0.019 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.118 Selenium 1 0.024 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Zinc 2.764 0.484 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.247 Total Phos- 15.040 17.958 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 32.998 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 2!:: f,e 4�� 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 7 M V O w Q, Q a U 1~ EC Z c y L a� 7i N vCi L O O O y Q Z � w u 15 ?: 1 O O UCL R R .0 Cj u w Q ^% v� w U a. O y D n i U +•� O +' C CC c NU GG � ee •- ca c,o Z O Cc C. , C�.' O Q # •max � •*x• N ZZZZZZZZ00000 o a� ¢� �•" 0 0 0 0 C Q\ ' U m.' V1 Vl Vl Vl Vl Vl 7 ch 7 cF N N "i ^ ',Z^ ',Z^ E N N N N N N N N O M ............. Ammonia Y o, o, o, o, rn Nitrogen E O'+ D D D C. vM vM O �- N N N eh M 'n oc N a J C E.•y ef• eh ch N eh eY N�c o0 00 �O 00 Ic Gz+ cn p O oo C O N N N P Mineralization Rate*** Volatilization v v n v v n n n O O o c_ Rate** o 0 0 0 0 o co o fl° 0 0 0 w w Application x S o 0 ^ Method* o 0 0 O, N a s V V V V V V V V y 0 0 0 N o _ vl� w) o u a�, U ° " ti V ti ti ti 3 3 3 ^ c cv eqeq S S M •� 'O ^O a U O C C M... O o Zo y U U tz. zU. c N C1 W O L- l M N S S S S Ln r- < ¢ ❑ Cn cl °� v* O b o o S S S oN 0 S 0 S ° O ON O O M O v -i oho > ^fl # •cd N 0'O C W w.c.� rig c E ccm y oww � vU �a.a 1I1IIOWM N ao a��Q Ln o`o o ;_ S.. c o Q rs. V R. E o, CC 7i N vCi L O O O y Q Z � w u 15 ?: 1 R R Cj u w Q ^% v� w U a. O y D n i U +•� O +' C CC c NU GG � ee •- ca c,o Z O Cc C. , C�.' O Q # •max � •*x• a 0 0 N N n LL CO U- 0 LL of Z w ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Reidsville Total Dry Tons Applied (Annual): 6.17 Permit #: WQ0002376 Cation Exchange Capacity (non 503 only): Operator: Auman French Owner: Marian French Predominant Soil Series: CgB2 Acres Used: 17.15 Acres Permitted: 17.15 Site #: RC 126 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ..-. Com- posite R © on © 6 on ENEM 1j 1121 DT/Ac./ o App. Event 0.36 14 Arsenic 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.002 Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Copper 0.122 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.122 Chromium 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Lead 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.043 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 denum TotalDate- • .. Nickel Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Ill L2J31 141L5J 6 71 8 J L9]10] 1j 1121 DT/Ac./ o App. Event 0.36 14 Arsenic 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.002 Cadmium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Copper 0.122 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.122 Chromium 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Lead 0.043 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.043 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 denum Nickel 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Selenium 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.004 Zinc 0.401 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.401 Total Phos- 16.200 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 16.200 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1/22/2019 Date DENR FORM MFLSF (12/2006) �I�IOIkn O u i.: is CQ � C w N �D W •0 O O UCL � '^ v�'i a 0Y •O RS ,C -0 r•i � O a� o on C ^o lapcc U n. R = • � .0 C � 8 o u ��+ y Z N ozzoSoog000So d o o c o 6 o d o 0 0 a. O knO n 00 0 0 p 0p 0 0 0 0 p 0p 0 0o 0tn 0 0"' 0 0 4 C> U 00 C C O O O C O O G Z z ............. Ammonia Nitrogen E a E�. 00 00 w o00 Mineralization Rate*** Q o41 o w Volatilization o Rate** O a 0 0 6 0 _ bj o o S Application Method* x o 0 0 r Q N N a V V y 0 0 0 C> N. .r s, cNn 00 00 C9 fj N"C00 u d iC .-. G � 3 E 3 3 d v o 0 0 Ca F., V ¢ Q 'b N 0 0 0 0 75 8 U U c �? F Cq N 0 0 0 0 00 0 0 O 0 0 0 0 0 Q' 0 O O O M :; Q C O O G O C C C C C C C 0 0 0 Q � a c, U o c o o E � �u Ljluow ao OIL> CQ � C w N �D W � '^ v�'i a 0Y •O RS G� � .�.� r•i � O a� o on C ^o lapcc U R = • � .0 C � 8 o u ��+ v R3 Q 0 0 04 LL U) U- M CK 0 U - x Z LU 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: City of Reidsville Total Dry Tons Applied (Annual): WQ0002376 Cation Exchange Capacity (non 503 only): Ken Martin Owner: Ken Martin Predominant Soil Series: 21 Acres Permitted: 21 Site #: RC130 Field #: 41.48 CmB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1/2/18 2 4/4/18 _3j 7/13/18 4j 5 6 7 181 L 9 10 11 12 % Solids 0.67 1.46 1.1 Arsenic 3.33 3 5 Cadmium 2 2 1.9 Copper 169 180 204 Event 0.56 0.32 1.09 Chromium 44.3 59.9 43.7 Arsenic 0.004 0.002 0.011 1 0.000 0.000 0.000 1 0.000 Lead 60.2 61.5 59.8 0.000 1 0.017 Cadmium 0.002 0.001 0.004 0.000 0.000 0.000 Mercury 1.12 2.96 0.8 0.000 0.000 0.008 Copper 0.190 0.115 0.446 0.000 0.000 Molyb- denum 5.63 5 6.84 0.000 0.000 0.000 0.751 Chromium 0.050 0.038 0.096 0.000 Nickel 22.8 33.5 21.2 0.000 0.000 0.000 0.000 0.184 Lead 0.068 0.039 0.131 Selenium 1 5 5 5 0.000 0.000 0.000 0.000 0.000 0.238 Mercury 0.001 0.002 Zinc 557 509 552 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.006 Total Phos- horus 22500 15800 20500 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 denum Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 61 7 8 9 1101 111112 y DT/Ac./ 0 r. APP• y Event 0.56 0.32 1.09 Arsenic 0.004 0.002 0.011 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.017 Cadmium 0.002 0.001 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.190 0.115 0.446 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.751 Chromium 0.050 0.038 0.096 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.184 Lead 0.068 0.039 0.131 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.238 Mercury 0.001 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Molyb- 0.006 0.003 0.015 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 denum Nickel 0.026 0.021 0.046 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.093 Selenium 0.006 0.003 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 1 0.626 0.326 1.207 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 2.159 Total Phos- 25.290 10.112 44.813 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 80.215 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". z:z4�re _ 1/22/2019 Signature of Land Applier Date DENR FORM MFLSF (12/2006) N O a M E CE Z N E o U U u C� x RS w � y � O •id � V �•' O H y U >> ZL U � 4w o U •� ~ L) O4 .2 _ w � b Q �4 U O •� p" ,� N U v U o U N o U o U v U v U U v A N E �O U ai Q Q 'o a o ea CG 3 Q.o Z Z %•• U U w U w U w U w U w U w U w U w U w U w I--� N Q Q ' U Z Z Z Z Z Z Z Z Z Z Q Q O N M O 00 h- M 00 n O O O �: p•" 01 l� 00 C) . d' � j 06 C� 06 4 O O y z z Z w o 41 W, *0i� p, Ammonia Y 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o Nitrogen E kn M V, MN kn MN N N M V1 M M V1 M V'1 M V1 M V'1 •� N N p N N N G ...� Z Y 0 0 0 0 0 0 0 0 0 0 W y N OO 00 �y W% cc W% 00 W) 00CIA N 00 �C 00 IC11C 00 00 IC 00 10IC 00 00 E- E w o o d Mineralization Rate*** Volatilization Rate** o 6 6 6 0 0 0 6 0 o n a o o p 0 W Application rn v1 V� V� V� Cn �n Cn �n cn w Method* c o o 2 V V V V V V V V V Q" N 01 N' CZ a _ o o d O _ •� N •� i.' 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O Y d i dm ti j ; Z Q R N U 2 U Z J Q to � N Z Q O O CO R yII N N (Q -6 - y C Fes•' � N J 0 0 0 0 0 0 0= O O d w n LL U� v E 0 ZU) o c N Rr O m w N V N Em .0 LL U o a ti T 3 m m S n 3 o 8. °w"00 t C 3 `° N CO n N O N O � N IL LO 0) tQ v co m V E 3 7 Z Z = � 3 aai tvi � Q N O O o 0 0 C.1) O O co CD r 00 0 0 N N N V) 0 O Ct O O V m m E 4 a co � 0 0 � a_ O 0 d m N E a ' Z E m J Z FY— U Z C7 C� U oo O = — NC') Z_oooooooOOo Q LO N N _____ O J Cl) O O O O O O O O O D O o 0 CD CO 0 cO 0 CO 0 C0 CO CO LO U Z Q O tq U LO CO to to O C0 CO 0 C0 c0 CO C0 w C0 cO c0 O O It M M M O O N O O O O 't O O O M M r tt d' O CD CO U7 CD CO CO aO t1) 00 aD CD O C0 M r r O r r r r r r r r r r r O O r �- 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N N N N N N N N N N N N N N N N N O O O N O O O O M O O O m O O O O O O O O O O O O O O O O O O O O O O O o O o 0 0 0 O O O O o O0 0 0 O 0 O O O O O O O O O O O O d• r r r r Cn M 0 to to N O O 00 0 0000 0000 N O CM LO 0 C j � M O COD O N O d' r M O N M C0 � CO LO LO r O V M M 7 � N � Cm 0) 0000 M COO N 0 r O c}' r O O N O O r Cl) C: a� O C fn N N Z2 E ? E ai O Z r .c E 'm E 3 c c m CU 0 `0� 0) 0. U Z Z 7 X oL d (A U 20 too 0 CO O c .� Z `- Q UiV 0 'c a+i o 5 O Cl) .y m d N 3 m C: 0 cn a) CD U) Z m c O E c O U N N Y N m T O O c to m Q C) U X C) U) m m L O .3 a m c 0 m U) 0) 767 Q fm'; E M O M t0 V N � v N T c 00 C = X ° C. ce N >, M -* R c a, 3 � M C c v 3 d .0 C 3 m N t8 P, N O N y N O � N a U) rn � 9 C\l r � L d1 d � C E O Z Z +� C Q u � Q N w N Cca O 0 N z c N Y Q U g LO o w F- H V C U) O O O 0 O ce) o o w w r r w O O O LO N 0 v 27 v o 0 (4 J LLZ Q C) I-. Q W m 0 0 0 O C) "T o to o r O O 'IT O 0 0 0 0 (O CO fO W W ?) w O w O N N O O U co M N w 6 6 w oD N tf) C6 tri r r O r w w w w w w w w w 0 0 0 0 0 0 0 0 0 N N N N N N N N N O O O O O O O O O Z cn 0 P 0 0 0 0 o o o o u LO tri to Ci o 6 r tri m tri LO o O o O tT ItM O V N V V 3 c s 3 U :3 a O` Y N U O >+ U Z -i E2 0 Q cn i m m2 m m m m 1� i2 uj LU U) O a w D a w U z Q J a O U ir O LL F- 0 O z z LU c9 O x z U z (7 cr L( 0 w Q E U L- J 0 Z fn U7 U) 3 c� c O N m N z c O E c O U N N Y .0 m a a� 0 c cn m a. a� U X N to .N L LM 3 L co c O d m m Q U a Waypolt.. ANALYTICAL 7/24/2018 EMA Resources Inc 755 Yadkinville Road Mocksville, NC, 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 www.waypointanalytical.com Ref: Analytical Testing Report Number: 18-198-0205 Project Description: Reidsville Waypoint Analytical Virginia, Inc. received sample(s) on 7/17/2018 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, &,`- Iff 0&7- Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Arizona AZ0629 Pennsylvania 68-03109 Virginia 460014 South Carolina 93007 New Jersey VA011 Florida E871087 North Carolina 257 +y. Page 1 of 7 Admolk Waypoint'�O ANALYTICAL Client: EMA Resources Inc Project: Reidsville Lab Report Number: 18-198-0205 Date: 7/24/2018 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 www.waypointanalytical.com CASE NARRATIVE Nitrate + Nitrite Nitrogen Method 4500NO3F-2011 Sample 61743 Analyte: NO3+NO2-N QC Batch No: E65156 The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. Solids Total Mercury Analysis - CVAA Method SW -7471 B Sample 61673 Analyte: Hg QC Batch No: E65182 MS/MSD Recovery failed, PDS confirmed matrix interference Page 2 of 7 Waypoint-0 ANALYTICAL Report Number: 18-198-0205 Client Project Description: Reidsville 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 www.waypointanalytical.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61745 Reidsville Solids 07/13/2018 09:15 07/17/2018 61745 Reidsville Solids 07/13/2018 09:15 07/17/2018 6010D WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 3 of 7 r� m (0 0- �V E M N V o Z n Q U M Z OO Q r O d' = OO OOOOOOOZLCLI O 00O 00 N N Z O ) JQ M E 0 0 0 i � O 0 O O O O O _ _ O _ _ O Z) O L LL 00 O (O (o O CD co CD CD CD CD CD O U) U Z N t-1 N N N N C/) Ln V ULLC) .�wj V 0 E 3 --� N g v u 2 c a •c 0 c d' 3 a a a7 co Q O d p, O M O Mr O O N MO N N MO N MO N N MO N MO N N N N O O O d 0) MO M O 0 V E V O O O 6i OM OM OM OM O OOOC 3Cm 00 00 oo 00 00 oo 00 OD co co0 C N d R d r O r O r O r O _00 O r O r O r O _co O r 0 r 0 r Q r O r 0 r O r O r O ko RN N N N N N N Cl N N N N N N N N N O p p n n co v v 4 v- 4 4 v v a• v 00 0o rn r r r N N N N N N N N NQ N r r ti n n i n n i. n iZ ti ti 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0cu vi cu m F- m > > > is U Q) o r d Mn o m a a Z z J VLL' 0 0 0 0 0 0 0 o Q o 0 0 0 0 0 0 0 m c CR O c; O O O O Lo c; O 0 Uf O O O N c e E O J uj _t O ca O 0 0 0 0 0 0 0 0 0 �' N O O N O 00 LO O N Q M m Itr O O In M Ln y CD O Cl) N O � CD N U) 0 r N •` a; - CY N r �- r r M V a) - co O v F O0) N O M M Ln W COD � ONO LQ LLICY N O r r• O e- r Cl) O X O y a) s N Q C co N _ r N 0 0 O tT O 3 co m m w lN, Z N E _ a� a 0CD o c a) Lo y c as c J x .. Z cm`° z ° t, E 2 Lo o O 3 Z Z cc 7 E N Z > C H 'C CL O a) Y O E 'N E c CO c U Z + 0 p Z (n O d L. 7 a) c M O O 'c L �2 C EQ � '�•' � ,�. n U n 2 U •N ¢ O z s o r� m (0 0- M w G O N co li CL O N -Z m m m 3 w v 3 c � 3 :D s .r- 3 m �g N t0 n 3 U') O O co LO 0) 0o NN T L d 7 Z Z as 0 m Q N v d ,0 - IL a W a N U O C O N LT U Z C a) -0LO 0 .� ¢ } U Lu ti H 'a C N O O � o O O 00 O 00 T T N N N M r N i o 0 m (� O O _O O O_ O LO O O O O O O j CO O CD t0 cD (D m M M M M M O M 0 M M 0 0 0 0 0 0 0 0 T T T T T T T T T T N N N N N N N N N N W r qr Q N � � � r- n � I- ti O O O O O O O O O O s 2 Q U. C) 0 W C4 a) N N M 60 O U) T T N 1l- N a0 O Cl O 0 IT w v- N LoV O V co r- O a D a. W U Z L a c0 c0 J 0c - r � L O U O U. F- O Z Z w O O H Z � U O Z U) c ¢ C7 O ti ZO a N Z o c c ¢ 7co I- U Z cr- -i <C � aF� W M) U u ZU) El 'i = c ny !@ e Waypoint(D ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com Cooler Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 18-198-0205 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 Other: 0 UPS 0 Client 0 Courier Thermometer ID: � Shipping container/cooler uncompromised? 0 Yes 0 No Number of coolers received F1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Required Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Required Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? I* Yes 0 No COC properly completed Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes 0 No Comments: Signature: Worgaw Tichacek Date & Time: 7/17/2018 13:33:43 Page 6 of 7 Page 7uf7 Waypoint.0 ANALYTICAL 10/11/2018 EMA Resources Inc 755 Yadkinville Road Mocksville, NC, 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 www.waypointanalytical.com Ref: Analytical Testing Report Number: 18-276-0205 Project Description: Reidsville WWTP Waypoint Analytical Virginia, Inc. received sample(s) on 10/3/2018 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, or O—r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Arizona AZ0629 Pennsylvania 68-03109 Virginia 460014 South Carolina 93007 New Jersey VA011 Florida E871087 North Carolina 257 • , iA Page 1 of 6 WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2 of 6 (2)Whitepine Waypoint 7621 Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 18-276-0205 Client Project Description: Reidsville WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 SM-2540G WTN 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 SW-74718 WTN 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 SM-4500-NH3C TKN WTN 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 4500NO3F-2011 WTN 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 6010D WTN 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 SM-4500-NH3C WTN 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 9045D WTN 62984 Reidsville WWTP Solids 10/02/2018 10:30 10/03/2018 ADAC 955.01 WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2 of 6 M kO mO to Q n u N cco C = LLC ° 0 CL CC 3 t�0 C!1 6! n C N CO Ly G 7 � �g N t0 n J Q o J Q W m 2 - CL a O 0 M O O O r O CO CO r N N N M N N O r O O O M O N co C%4 I- r N > N to N m U = Z 00 (0m ,j-0 a) CO .N ch Y N t7 'j Cn d t0 O E 7 LO W 4) = Z ay ~ C O Z E CO) m Q J Z F U Z Z O N 0= O❑❑ Q O O O❑❑❑❑ Z Q Ii N N ? OO O O O o O O o O O O N O CD d 0 CD CD (fl Co CD CD CO LO Q Zd CO U) LO o CO U v M M O OD M M CO CO M M M M CO CO O O N O M LO CD O M O O O O O O d Oi O O O N c i t i r r N r r N N T r r r N N r r T r r r r r r r T r r r r 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N N N N N N N N N N N N N N N N N O O O O O O O O O O O O d d d O 6 r r r r r T T r T T r r r T T T T a a w z w 2 2 w w w w w w a. ❑ U U U -~i pYp n Y Y n� ~� � U co O O O O O O p O p O O O O O O p M _0 Or l00 COO t00 C00 N 00 t00 0 N 0 C00 r V O O O O O O O O O O O N M 00 O O O O CD N N - N [t - N Ct N 0 LOND N N N V Od O p co V C� N 4 N O 4 mN O O m N N O r N O r N 0) c N O O c b m Z Od Z Cn Cc 7 O Z r a a E Eam Z d N O 3 Z O t E u) 7 C i C U t _� c _� c CO a O "c -0 N ca O .8 � V O O c m B. 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In o o r o 0 0 ko r N N C'7 to O to Or (V J s �a W at O O to O O N C0 Imp Lf) � N CND to L6 r0 V O V V 0) Fj- O O to r In tl- C) Qi le V to LO co N CU O Fd>- O = 0 N 9 c cDLO hm UCD N NU Z N j ,� C(n X CO N w m a rn 0 Q U tN0 co — = Lr)E wF- Z Z U C F— E E cuy OC 0 3 Z D E U �' 7 'c E c a w a C6 m a o y Y 2 a) v d >, E co U Co o U Z Q cn oa I° 0 N .N CO 3 ca c O Cn N Z C O E 0 U N N d E F- C_ a O 2 V c O A d m .. m fflm Waypoint-W ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytfcal.com Cooler Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 18-276-0205 Shipping Method O Fed Ex O US Postal O Lab 0 UPS O Client O Courier J Other: Thermometer ID: Shipping container/cooler uncompromised? 0 Yes O No Number of coolers received F__1 Custody seals intact on shipping container/cooler? O Yes 0 No 0 Not Required Custody seals intact on sample bottles? 0 Yes O No 0 Not Required Chain of Custody (COC) present? 0 Yes O No COC agrees with sample label(s)? Yes 0 No COC properly completed Yes O No Samples in proper containers? Yes O No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes O No All samples received within holding time? 0 Yes O No Cooler temperature in compliance? is Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes 0 No Water - Sample containers properly preserved O Yes No N/A Water - VOA vials free of headspace O Yes O No N/A Trip Blanks received with VOAs O Yes O No N/A Soil VOA method 5035 — compliance criteria met O Yes 0 No N/A High concentration container (48 hr) Low concentration EnCore samplers (48 hr) High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? O Yes 0 No Comments: Signature: lBrandi Watson Date & Time: 10/03/2018 14:51:22 Page 5 of 6 CL U E^ W y U Pace 6 of 6 � N Y � rn Q � � O � H c 3 0 � ~ U 2 n $i N X N d c N0.0 _ G @ a o O c - � E v . o � P4. � Y V 2 O C =Z ~ Q�ii t d E a, B _:: _ = 2' c m —o o _ ro IC - N 0 =' 2 N a �u 6 y 7 2 � m '0 _ � � w = y Z a c m - ci v o QCJ oU d 3Cc_ H U y QOIL- 7 3 e Y = V a ad CA = U tuo r, f !U Pace 6 of 6 *ESC 1. N. ANALYTICAL REPORT April 13, 2018 EMA Resources Sample Delivery Group: L983661 Samples Received: 04/06/2018 Project Number: Description: Reidsville Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By: Cassandra Foster Technical Service Representative Results relate only to the Items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. " `' =MESC o s�OtlOrory of ��A.�,�,yyl� TABLE OF CONTENTS ONE LAB, NATIONWIDE Ss: Sample Summary Cn: Case Narrative Sr: Sample Results REIDSVILLE L983661-01 Qc: Quality Control Summary Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260B Chlorinated Acid Herbicides (GC) by Method 8151A Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270D GI: Glossary of Terms Sc: Sample Chain of Custody 3 4 5 5 7 7 8 9 10 11 12 13 15 16 17 19 2,'-,-, 21 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L983661 04/13/1816:28 2 of 21 SAMPLE SUMMARY ONE LAB. NATIONWIDE. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L983661 04/13/1816:28 3 of 21 Collected by Collected date/time Received date/time REIDSVILLE L983661-01 Waste Brent Collins 04/05/18 09:30 04106,218 08:45 Method Batch Dilution Preparation Analysis Analyst date/time date/time Preparation by Method 1311 WG1095886 1 04110/1810:15 04/10/1810:15 TM Preparation by Method 1311 WG1095939 1 04/10/1811:15 04/10/1811:15 RT Wet Chemistry by Method 9012 B WG1095472 1 04/10/18 09:39 04/11/1810:57 KK Wet Chemistry by Method 9034-90308 WG1096347 1 04/11/18 23:20 04/11/18 23:20 JLJ Wet Chemistry by Method 90450 WG1095044 1 04/07/18 09:17 04/07/1811:20 EEM Wet Chemistry by Method D93/1010A WG1095613 1 04/10/1810:09 04/10/1810:09 TH Mercury by Method 7470A WG1096398 1 04/11/18 08:04 04/11/1816:30 EL Metals (ICP) by Method 6010D WG1096414 1 04/11/18 08:32 04/11/1811:55 TRB Volatile Organic Compounds (GC/MS) by Method 8260B WG1096448 1 04/11/1818:12 04/11/1818:12 JBE Chlorinated Acid Herbicides (GC) by Method 8151A WG1096408 1 04/11/18 08:36 04/12/1813:03 KLM Pesticides (GC) by Method 8081B WG1096466 1 04/12/18 07:14 04/12/1817:45 TD Semi Volatile Organic Compounds (GC/MS) by Method 8270D WG1096463 1 04/11/1811:45 04/12/1815:59 LA ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L983661 04/13/1816:28 3 of 21 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All radiochemical sample results for solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet weight was requested by the client. All Method and Batch Quality Control are within established I Ss criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. SSr PC Cassandra Foster Technical Service Representative Project Narrative gSc All Reactive Cyanide results reported in the attached report were determined as totals using method 90128. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/90306. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L983661 04/13/18 16:28 4 of 21 REIDSVILLE SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. 4* Collected date/time: 04/05/18 09:30 L983661 Preparation by Method 1311 Result Qualifier Prep Batch Analyte date / time date / time TCLP Extraction 4/10/201810:15:56 AM WGIO95886 TCLP ZHE Extraction 4/1012018 11:15:32 AM WG1095939 Fluid 1 4/10/201810:15:56 AM WG1095886 Initial pH 7.43 4/10/201810:15:56 AM WG1095886 Final pH 4.99 4/10/201810:15:56 AM WG1095886 Wet Chemistry by Method 9012 B mg/I date / time Result Qualifier RDL Dilution Analysis Batch Analyte mg/kg mg/kg date /time Reactive Cyanide ND 0.250 1 04/11/201810:57 Wet Chemistry by Method 9034-9030B Result Qualifier RDL Dilution Analysis Batch Analyte mg/kg mg/kg date / time Reactive Sulfide ND 25.0 1 04/11/2018 23:20 Wet Chemistry by Method 9045D 0.20 1 04/11/201816:30 Result Qualifier Dilution Analysis Batch Analyte su Result date / time Corrosivity by pH 7.34 T8 1 04/07/201811:20 Sample Narrative: mg/I date / time L983661-01 WG1095044: 7.34 at 20.4C 0.100 5 Wet Chemistry by Method D93/1010A Barium ND 0.100 Result Qualifier Dilution Analysis Batch Analyte Deg. F date /time Ignitability DNI at 170 1 04/10/201810:09 Mercury by Method 7470A Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date / time Mercury ND 0.0100 0.20 1 04/11/201816:30 Metals (ICP) by Method 6010D ND 0.0500 0.50 1 04/11/201818:12 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date / time Arsenic ND 0.100 5 1 04/11/201811:55 Barium ND 0.100 100 1 04/11/201811:55 Cadmium ND 0.100 1 1 04/11/201811:55 Chromium ND 0.100 5 _ 1 04/11/201811:55 Lead ND 0.100 5 1 04/11/201811:55 Selenium ND 0.100 1 1 04/11/201811:55 Silver ND 0.100 5 1 04/11/201811:55 Volatile Organic Compounds (GC/MS) by Method 8260B 9 Sc Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date I time Benzene ND 0.0500 0.50 1 04/11/201818:12 Carbon tetrachloride ND 0.0500 0.50 1 04/11/201818:12 Chlorobenzene ND 0.0500 100 1 04/11/201818:12 Chloroform ND 0.250 6 1 04/11/201818:12 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L983661 04/13/1816:28 5 of 21 9 Sc REIDSVILLE SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. 40 Collected date/time: 04/05/18 09:30 L983661 Volatile Organic Compounds (GC/MS) by Method 8260E ACCOUNT: PROJECT: SDG: DATEMME: PAGE: EMA Resources L983661 04/1318 16:28 6 of 21 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date / time 1,2-Dichloroethane ND 0.0500 0.50 1 04/11/201818:12 1,1-Dichloroethene ND J3 0.0500 0.70 1 04/11/201818:12 2-Butanone (MEK) Tetrachloroethene ND ND 0.500 0.0500 200 0.70 1 1 04/11/201818:12 04/11/201818:12 3 SS Trichloroethene ND J3 0.0500 0.50 1 04/11/201818:12 Vinyl chloride ND J3 0.0500 0.20 104/11/201818:12 4 (S) Toluene d8 103 80.0-120 120 04/11/201818:12 -- Cn (S) Dibromofluoromethone (S)a,a,a-Trifluorotoluene 104 972 76.0-123 80.0-120 123 120 04/11/201818:12 04/11/201818:12 (S) 4-Bromofluorobenzene 94.1 80.0-120 120 04/11/201818:12 Chlorinated Acid Herbicides (GC) by Method 8151A Rc Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date / time GI 2,4,5 -TP (Silvex) ND 0.00200 1 1 04/12/201813:03 2,4-D ND 0.00200 10 1 04/12/201813:03 (S) 2,4-Dichlorophenyl Acetic Acid 80.1 14.0-158 158 04/12/201813.03 -•--' Pesticides (GC) by Method 80818 9Sc Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time ^- Chlordane ND 0.00500 0.03 1 04/12/201817:45 Endrin ND 0.00500 0.02 1 04/12/201817:45 Heptachlor ND 0.00500 0.0080 1 04/12/201817:45 Lindane ND 0.00500 0.40 1 04/12/201817:45 Methoxychlor ND 0.00500 10 1 04/12/201817:45 Toxaphene ND 0.0100 0.50 1 04/12/201817:45 (S) Decochlorobiphenyl 81.2 10.0-144 144 04/12/20181745 (S) Tetrachloro-m-xylene 62.9 10.0-135 135 04/12/201817.45 Semi Volatile Organic Compounds (GC/MS) by Method 8270D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,4 -Dichlorobenzene ND 0.100 7.50 1 04/12/201815:59 2,4-Dinitrotoluene ND 0.100 0.13 1 04/12/201815:59 Hexachlorobenzene ND 0.100 0.13 1 04/12/201815:59 Hexachloro-1,3-butadiene ND 0.100 0.50 1 04112/201815:59 Hexachloroethane ND 0.100 3 1 04/12/201815:59 Nitrobenzene ND 0.100 2 1 04/12/201815:59 Pyridine ND 0.100 5 1 04/12/201815:59 3&4 -Methyl Phenol ND 0.100 400 1 04/12/201815:59 2-Methylphenol ND 0.100 200 1 04/12/201815:59 Pentachlorophenol ND 0.100 100 1 04/12/201815:59 2,4,5 -Trichlorophenol ND 0.100 400 1 04/12/201815:59 2,4,6 -Trichlorophenol ND 0.100 2 1 04/12/201815:59 (S) 2-Fluorophenol 41.4 10.0-120 120 04/12/201815:59 (S) Phenol -d5 271 10.0-120 120 04712/201815:59 _r (S) Nitrobenzene -d5 52.7 10.0-126 126 04/12/201815:59 (S) 2-Fluorobiphenyl 62.2 22.0-127 127 04/12/201815:59 (S)2,4,6-Tribromophenol 62.8 10.0-153 153 04/12/201815.59 (S)p-Terphenyl-d14 69.2 29.0-141 141 04/12/201815:59 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: EMA Resources L983661 04/1318 16:28 6 of 21 E I F ( Fucl:I ® F51 p O m � N M E o 0 C� � M m m O M E o d R d m m Y M m a6 O M E CO 03 O v 0 0 M V CO ry � � a � V Q Q O N Q cn O Ln O M 00 m J 0 C� E O J -.�R oN d m p p a O a O v aQ a M O co � O V 0 r 3 O O 0 a Y O O =Da o 0 E o m a v � m C m o O E z m V � u a � V) U J C) U Q v/ � I O' U i 0 cu 0 M J U J N 0- U) U) O 0 U 0 (6 O co J w U Q � E CO nG W U .a D Q X c� C Q X c� G (n O N 0- V) V) O O M 61 M 00 rn J W W N W H � w r m d o V 1 0 a El W z 0 H Q z cn Q W z 0 r---- _ PIFu Fc�] ® Fo A 2 J 0 � Y E O � � E N v U Q to O y E m cn O N Q 6 N cn 'It CO J V) U J y U Q y Q Ln O U 0 O .Q M J V J_ Q) Q. 0 O v O O 9 J E J O v d' � Y N Q? o� J E � v 5. a � W N a a co U W 0 a U Z D O O a a a W W z 0 F- a m a Lu z O 0 v 0 v U 3 r--- L-- -Im tl d N� v cy� W N a a rn co W N w co r- m Q 0 0 V W O M IL . ,p� / / / % ■ 3 2 / � \\. s�\® - � � � \�� � ) 0 § * / 3 § \ / \ E1 p o � - O M m O 2 E O 7 � v 0 0 � - M O O E o GI M w - O J E O J E o 2, m Q � F FD VC/ G v U Q N Q X C� G c�c G Q X cn O Q E M U) Co C O 0 LD m 00 G) J E J O 0 00 � V d O N ri O � rn O O � M � N N O � N N � N m E O � E o O Ni o: coOJ 15, O, - O O E Z �1 M M K � N E CD y — O O CL o 0 N E O w 00 w00 Q O O M 4j ry Q /:D V / O LL �; z O .. 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CD 000 ix o ry h V O N O n O V d0' N N V N N M N N N tJ V, co rn N O O Jo Ltd I� h In tp cD M m ICJ W W M V Q> O N OCD m o � co M O V M Q h � Ln Lf7 N N M M M M � Jof p O O p p p p p p p O O E Z O O Z Z Z Z Z Z Z O O W n Y) Y n J M M NU p O O E z p p p p p p O O J E Z O O Z Z Z Z Z Z Z O O C E a x 0 0 0 0 0 0 0 0 0 0 0 d x 0 0 0 0 0 0 0 0 0 0 0 y — LP LP L.f) In O O Cf In C. O O O 9 LS) In Ln D. at O O O O C! O O In E o 0 0 0 0 0 0 0 0 0 0 0 o an o o ^' o v C O O U O O OZ 1E O O_ o g o a 3 ts t0 X X X J LSA a N M 2 N N w a a D to E N 10 Ll� W O _ to L)E E Y Q V) U Q Q x c�c G Q X a+ CO G U) O W Q E m V) c O d M 00 J N E J n d M Q1 M LP c0 N O (P Cp O h tP LY Se N N M M co M 't N N V N N d N E n o N o o o v o o M o o o y U O O O O O O O O O O O O O O O O d,Q N c0 �V Vim' O GO O O ry N O O O 0 o — — O M 6 O N r M O Ol N c6 O n W I� N Q) W M t0 W � 3° Ln r r O Ln to d- � Ln c0 r h Lry tp t0 NI M � Lo N � u N � Ln L o d Q.' N � N M M M M N ry N N N M M M O 2 E O O O O o CO 0 0 0 0 0 0 N O � —' V M r M V N ON W to 1 V M M M M N M M M 2 E o 0 0 0 0 0 0 0 0 0 0 0 N OLov m c 'cn — a� 0 0 O a O O E z z z z z z z Z z z Z z C 7 N E � a W 0 0 0 0 0 0 0 0 0 0 0 0 Y — O O O O O O O O O O O O G. ZT Lq Ln Ln Ln 1P LSA I ? Ltd Ln Lq Ljl In O O O O O O O O O O 6 O 0 0 U w � a a o 7 M °J v —, N c d Q C L 6 _O O O O. O L co W N tD L m O 00 N m J v 0 a GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. u Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, or if concentrations of analytes in the sample are higher than the Dilution highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J3 The associated batch QC was outside the established quality control range for precision. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit. T8 Sample(s) received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L983661 04/13/18 16:28 19 of 21 FSc ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE, # ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model Is conducive to accelerated productivity, decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held bythe laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. Alabama 40660 Nebraska NE -OS -15-05 Alaska 17-026 Nevada TN -03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TN002 California 2932 New Mexico' n/a Colorado TN00003 New York Connecticut PH-0197 North Carolina Env3 Env375 Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia 923 North Dakota R-140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C -TN -01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky " 90010 South Carolina 84004 Kentucky Z 16 South Dakota Louisiana A130792 Tennessee'" 20 2006 Louisiana' LA180010 Texas T 104704245-17-14 Maine TN0002 Texas' LAB0152 Maryland 324 Utah TN00003 Massachusetts M-TN003 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047.999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyoming A2LA A2LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2LA — ISO 170251 1461.02 DOD Canada 1461.01 USDA 1461.01 P330-15-00234 EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L983661 04/13/18 16:28 20 of 21 N`141 1 91 F�m 4 s a V!� Air, MCA sal 6i. Y M fi N3 C C i q�e t j e t > R b O d N -a D-li 1! ` dlal k C cc 14 a n ti r C i �L R i o �y� m .. - yu _y £- � ? •; �• '�' � Wi L remix "1d^ G .Lig � Ute. tri t1 a„F � y � � ifl } � ►. 5+ ' Gi -a. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WWTP Name: Monitoring Period: City of Reidsville Reidsville WWTP From 1/1/2018 WQ Permit Number: WQ0002376 NPDES Number: NCO024881 To 3/31/2018 Pathogen Reduction (15A NCAC 02T.11061 - Pleace indiento levPl aehiPvndl anti ,.,,-r ------ �— -- ^�---�' �w as sa aa♦ r j./v11V1111Gu. Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ ........... If applicable to alternative performed (Class A or Class B) com Tete the following monitor' g data: Parameter Allowable Level Pathogen Density g � Number o Excee- Frequency Sample Analytical inimu Geo. Mean axim Units in Sludge ences of Analysis Type Tech-nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 24187 36396 49207 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) kms.,♦. ♦ . —, vim, i ,A i V I I - A W43V 111ulu'utc altuFnative peniormea: Alt.l (VS reduction) Q Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ Alt. 4 (Spec. Oz uptake) El— Alt. Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ 1�1rnmUPT4" ♦ mTl%ILT C1T ♦ TTl.rT 1•ir� \ i Xlk 1 11' A%—P% A 1V1\ 0 1 ti 1 jr lvir.1,4 I kpiease cnecx the appropriate statement) El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) t,�, 4e Z�ZG��- 1/22/2019 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Reidsville WWTP Name: Reidsville WWTP Monitoring Period: From 4/1/2018 WQ Permit Number: WQ0002376 NPDES Number: NCO024881 To 6/30/2018 Pathogen Reduction (15A NCAC 02T.1106) - Please indicate level achievers and alternative ni-rfnrmatj. Class A ..... Alt. A time/tem ❑ Alt B Alk Treatment ❑ Alt. C ( p) ( ) (Prior Testing) ❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g Number o Excee- dences Frequency of Analysis Sample Type Analytical Tech-nique Minimurr Geo. Mean Maximurr Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1669 3692 6261 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 M per 4 grams total solid (dry weight) • � a l�r..u{.41V11 �i.�n 1�\,Lyti VL1 .���,� - riCa�e lilulcitie aliernairve perIormea: Alt.1 (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) R1 Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization p Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ v jr�n r jLr 1 ti 1 i"iN a 1 A i hivir.iv i tpiease check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) __ C?oi� 02A: 25�e 1/22/2019 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Reidsville WQ Permit Number: WWTP Name: Reidsville WWTP NPDES Number: Monitoring Period: From 7/1/2018 To 9/30/2018 WQ0002376 NCO024881 Pathogen Reduction (15A NCAC 02T.1106) -Please indicate level achieved and alternative erformed• Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ P Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra E3Gamma Ra ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density 2 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g � Number o Excee- ences Frequency of Analysis Sample Type Analytical Tech-nique inim Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 770 1017 2371 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) tT,...t.. A tea___ _�! _ 3 MPN per 4 grams total solid (dry weight) n _ A__ i� r . �a..�. 1�VuuL11V11 `1_7L'11.i L>t V41 .11V,1 - r►ease Inulcate anernative perIormecl: Alt.1 (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) © Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt -7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ l W"gFlTTT!� A Tid-%l T = ♦ -.r �_lil\ 1111VL'i 11111\ 01H1L' lvlr 1,4 1 kpiease cnecK the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer Name and Title (type or print) Signature of Preparer* Date Brent Collins; Director of Technical Services Land Applier Name and Title (if applicable)(type or print) -- 2!�4;2�_ 1/22/2019 Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Reidsville WWTP Name: Reidsville WWTP Monitoring Period: From 10/1/2018 WQ Permit Number: NPDES Number: To 12/31/2018 Pathogen Reduction (15A NCAC 02T.1106) - Pleace inrliratP iptim -:m h -A --A —14 WQ0002376 NCO024881 a..— "IX" aa�clliA�iVG (JCI"lUrmea: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ ST A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density R-11—Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ JAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class BWing monitoring data: Allowable Level Pathogen Density um er o en Parameter g y Frequency Sample Analytical in Sludge Minimurr, Geo. Mean Maximury Units Excee- of Analysis 'type Tech-nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 4848 8131 15584 col/g 0 Quarterly G SM9222D 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) Vector Attraction Reduction115A NCAC--02T.-1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) R1 4 (Spec. Oz uptake) ❑ JAlt. Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 71 -Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION ATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 9' 1/22/2019 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Contact: Brent Collins Client: BMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 ReportDate: 1/19/2018 Date Sample Rcvd: 1/9/2018 Meritech Work Order # 01091818 Sample: Reidsville WWTP 1 Grab 1/9/18 Parameters Result Analysis pate Reporting Limit Method % Total Solids 1.08% 1/10/18 0-100 % SM 2540B Fecal Coliform (Sludge) 28,619 col/g dry wt 1/9/18 352 col/g dry wt SM 9222D Meritech Work Order # 01091819 Sample: Reidsville WWTP - 2 Grab 1/9/18 Parameters Result Analysis Date Reporting Limi Method % Total Solids 1.09 % 1/1.0/18 0-100 % SM 2540B Fecal Coliform (Sludge) 36,697 col/g dry wt 1/9/18 352 col/g dry wt SM 9222D Meritech Work Order # 01091820 Sample: Reidsville WWTP - 3 Grab 1/9/18 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.08 % 1/10/18 0-100 % SM 2540B Fecal Coliform (Sludge) 35,354 col/g dry wt 1/9/18 352 col/g dry wt SM 9222D Meritech Work Order # 01091821 Sample: Reidsville WWTP- 4 Grab 1/9/18 Parameters $gs Analysis Date Reporting Limit Method % Total Solids 0.93 % 1/10/18 0-100 % SM 2540B Fecal Coliform (Sludge) 43,988 col/g dry wt 1/9/18 352 col/g dry wt SM 9222D Meritech Work Order # 01091822 Sample: Reidsville WWTP - 5 Grab 1/9/18 Parameters Result Analysis Date Reporting Limit Method % Total Solids 0.94% 1/10/18 0-100% SM 2540E Fecal Coliform (Sludge) 43,520 col/g dry wt 1/9/18 352 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 2 Report Date: 1/19/2018 Date Sample Rcvd: 1/9/2018 Meritech Work Order # 01091823 Sample: Reidsville WWTP - 6 Grab 1/9/18 Parameters % Total Solids Fecal Coliform (Sludge) ResultAnalysis Date Reporting Limit Method 1.09 % 1/10/18 0-100 % SM 2540E 24,187 col/g dry wt 1/9/18 352 col/g dry wt SM 9222D Meritech Work Order # 01091824 Sample: Reidsville WWTP - 7 Grab 1/9/18 Parameters % Total Solids Fecal Coliform (Sludge) es It Analysis Date Reporting Limit Method 1.09 % 1/10/18 0-100 % SM 25408 49,207 col/g dry wt 1/9/18 352 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 X12 >' (%.> a O 0 u Q N O Ind C V p - 0 'O fl- -..� O Z .� H ..r a u m CL C fin, N N � N Ila N H 61 • uj X :: .+ m z a ti w CA. c N E c Q 0 N O L 1 CL N =sU,A C W c .� O n Oo •e-Y� -h � SZ � � N .. 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Environmental Laboratory k Laboratory Certification No. 165 Ir Contact: Brent Collins Report Date: Page 1 4/11/2018 Client: BMA Resources, Inc 755 Yadkinville Road Mocksvilie, NC 27028 Date Sample Rcvd: 4/4/2018 Meritech Work Order # 04041808 Sample: Reidsville - 1 Grab 4/4/18 Parameters Result Analysis Date Reporting Limit Mgthod % Total Solids 5.99 % 4/4/18 0-100 % SM 2540B Fecal Coliform (Sludge) 1669 col/g dry wt 4/4/18 352 col/gdrywt SM 9222D Meritech Work Order # 04041809 Sample: Reidsville - 2 Grab 4/4/18 ,Parameters Result Analysis Date Rellorting Limit Method % Total Solids 4.83 % 4/4/18 0-100 % SM 2540B Fecal Coliform (Sludge) 3388 col/g dry wt 4/4/18 352 col/g dry wt SM 9222D Meritech Work Order # 04041810 Sample: Reidsville - 3 Grab 4/4/18 Paramej Result Analysis Date Reporting Limit Method % Total Solids 3.40% 4/4/18 0-100 % SM 2540B Fecal Coliform (Sludge) 5882 col/g dry wt 4/4/18 352 col/g dry wt SM 9222D Meritech Work Order # 04041811 Sample: Reidsville - 4 Grab 4/4/18 Parameters Res`ul_t Analysis Date Reporting Limit Method % Total Solids 3.63 % 4/4/18 0-100% SM 2540B Fecal Coliform (Sludge) 6261 col/g dry wt 4/4/18 352 col/g dry wt SM 9222D Meritech Work Order # 04041812 Sample: Reidsville - 5 Grab 4/4/18 Parameters Result Analysis Date Rgporting Linnet Ngthod %Total Solids 3.73 % 4/4/18 0-100 % SM 2540B Fecal Coliform (Sludge) 4143 col/g dry wt 4/4/18 352 col/g dry wt SM 9222D 642 Tameo Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Meritech Work Order # 04041813 Sample: Reidsville - 6 Grab Parameters Page 2 Report Date: 4/11/2018 Date Sample Rcvd: 4/4/2018 4/4/18 % Total Solids 3.06% 4/4/18 0-100 % SM 2540B Fecal Coliform (Sludge) 4159 col/g dry wt 4/4/18 352 col/g dry wt SM 9222D Meritech Work Order # 04041814 Sample: Reidsville - 7 Grab 4/4/18 Parameters Resul Analyfits Date Reporting Limit Method % Total Solids 6.80 % 4/4/18 0-100 % SM 2540E Fecal Coliform (Sludge) 2607 col/g dry wt 4/4/18 352 col/g dry wt SM 9222D 1 hereby certify that I have reviewed and approve these data. a, zdl Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)3424748 fax.(336)342-1522 of a p0 ry _ CL.: C J W so £ O 37 a 5 L in a N ,A MP L 73 Q [j7�,✓, ++ a, O. 7 1 qki E `O c tio E E h Jy O o V) 4 to .. •'' W * .7 a o c� N OL xL L C m G + c w h LL O � L a p CL 7 3 t L t\v,�� Y m a. m c N Ix EJ tLocx c O c u V) Z � CL M1 Q O fl m d U Q a u° c Z a E Q of 41 F- s c E i= E P E P w > c r' O ry E O r Q m `} y o Q aa�o n ui m 0 04 0 COCC m M u O a CLI o t � ai v U C bio � � `a � a •' O u V Lu CL tf "O Z @ ELU V) o 0 p E2 i!f a m ,�1„ o .E U r4 mz C _ O w ° Q vii 7ul Z y w — U H N fh on, tD aC i- O C v ja V C N E E Q 9 v 3 c c c c _ :.:: O w � m ac m z � IL m` ,� 41 tL N L 4.1 � LL C O ra `0 `r Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Contact: Brent Collins Report Date: 7/20/2018 Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Date Sample Rcvd: 7/11/2018 Meritech Work Order # 07111825 Sample: Reidsville -1 Grab 7/11/18 Parameters Result Analysis Date Reporting Limi Method %Total Solids 1.15 % 7/11/18 0-100 % SM 2540B Fecal Coliform [Sludge) 2371 col/g dry wt 7/11/18 352 col/g dry wt SM 9222D Meritech Work Order # 07111826 Sample: Reidsville - 2 Grab 7/11/18 Parameters Resul Ana is Date Reporting Limit Method % Total Solids 1.14% 7/11/18 0-100% SM 2540B Fecal Coliform (Sludge) 797 col/g dry wt 7/11/18 352 col/g dry wt SM 9222D Meritech Work Order # 07111827 Sample: Reidsville - 3 Grab 7/11/18 Parameters Result Analysis Date Reporting Limit Method %Total Solids 1.16% 7/11/18 0-100 % SM 2540B Fecal Coliform (Sludge) 784 col/g dry wt 7/11/18 352 col/g dry wt SM 9222D Meritech Work Order # 07111828 Sample: Reidsville - 4 Grab 7/11/18 Parameters Result Analysis Dale Reporting, Liml Metho % Total Solids 1.16 % 7/11/18 0-100% SM 2540B Fecal Coliform (Sludge) 1567 col/g dry wt 7/11/18 352 col/g dry wt SM 9222D Meritech Work Order # 07111829 Sample: Reidsville - 5 Grab 7/11/18 Parameters Resul Analysis Date Reporting Limit Method %Total Solids 1.14% 7/11/18 0-100 % SM 2540B Fecal Coliform (Sludge) <797 col/g dry wt 7/11/18 797 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Meritech Work Order # 07111830 Sample: Reidsville - 6 Grab Para Meters Result Analysis Date Page 2 Report Date: 7/20/18 Date Sample Rcvd: 7/11/2018 7/11/18 Reporting Limit Mgthod % Total Solids 1.15 % 7/11/18 0-100 % SM 2540B Fecal Coliform (Sludge) 790 col/g dry wt 7/11/18 352 col/g dry wt SM 9222D Meritech Work Order # 07111831 Sample: Reidsville - 7 Grab 7/11/18 Parameters Result AllalWs Date Reporting Limit Method % Total Solids 1.18 % 7/11/18 0-100 % SM 2540B Fecal Coliform (Sludge) <770 col/g dry wt 7/11/18 770 col/g dry wt SM 9222D Meritech Work Order # I 07111832 Sample: VS In Composite 7/11/18 Parameters Result Analysis Date Reporting Limit Method % Volatile Solids 27.7 % 7/17/18 0-100 % SM 2540E Total Solids 10600 mg/L 7/11/18 10.0 mg/L SM 2540B Volatile Solids 2970 mg/L 7/11/18 10.0 mg/L SM 2540E Meritech Work Order # 07111833 Sample; VS Out Composite r 7/11/18 Parameters Result Analysis Date Reporting Limit Method % Volatile Solids 31.4% 7/17/18 0-100 % SM 2540E Total Solids 10200 mg/L 7/11/18 10.0 mg/L SM 2540B Volatile Solids 3200 mg/L 7/11/18 10.0 mg/L SM 2540E II � I I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 ° O O CL N O Q O '''.'J tF y m E oCL y b a fl LLJJ N N c v 01 z a to O c cL O Q O d u c m EnE v to Ir z a_ LL u,, OL o: m c y m AA LL *' X. O .,,"+► O ±+ to Q N r w 0 C Y c 1 c V ° CL a c y aP -p oa ti � a p LL v v v Z a, C C O L � r� iri {.i d U ro C Z F CL M v o v u Q Q a u o L a � 0 aU E a E E E ' i-+ N �~y LU OLn N O W of d E o°°% Q M m LA w 3 Q Q 0m m cu E 0 O a g m m v O e n o U 0 Wa �~ O tLL -0{LQ L a L 0mw M V)LU 0 .� Z '.► L Y N 0 _ W N f6 4-J LLJ V E L N a N 0) �" a tn wZ o T "' N E w E aj IS U F� G Q O � ai : O n v v C \ N N c `Z' C E Q or c v c a E- Z z m O V 4-- 0 4- Lu a� pv Q. +n U_ o = w o E vi � s zto tn 2i N P Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 1 Contact: Brent Collins Page Date: 10/9/2018 age age 1 Client: h'MA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Date Sample Rcvd: 10/2/2018 Meritech Work Order # 10021813 Sample: Reidsville WWTP Grab 10/2/18 Param ters Result Analysis Date Reporting Limit Method % Total Solids 0.70 % 10/3/18 0-100 % SM 2540B Fecal Coliform (Sludge) 15584 col/g dry wt 10/2/18 352 cal/g dry wt SM 9222D Meritech Work Order # 10021814 Sample: Reidsville WWTP Grab 10/2/18 Parameter$ Result AnalysiN Date Reportine Limit Method % Total Solids 0.71 % 10/3/18 0-100 % SM 2540B Fecal Coliform (Sludge) 6401 col/g dry wt 10/2/18 352 col/g dry wt SM 9222D Meritech Work Order # 10021815 Sample: Reidsville WWTP Grab 10/2/18 Parameters Resul Analysis Date Reporting LIMI Method %Total Solids 0.74 % 10/3/18 0-100 % SM 2540E Fecal Coliform (Sludge) 11057 col/g dry wt 10/2/18 352 col/g dry wt SM 9222D Meritech Work Order # 10021816 Sample: Reidsville WWTP Grab 10/2/18 Parameters Result Analysis Date Reporting Limit Method % Total Solids 0.77 % 10/3/18 0-100 % SM 2540B Fecal Coliform (Sludge) 5903 col/g dry wt 10/2/18 352 col/g dry wt SM 9222D Meritech Work Order # 10021817 Sample: Reidsville WWTP Grab 10/2/18 Parameters Resul Analysis Date Reporting Limit Method % Total Solids 0.75 % 10/3/18 0-100 % SM 2540E Fecal Coliform (Sludge) 4848 col/g dry wt 10/2/18 352 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 teI.(336)342-4748 fax.(336)342-1522 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Meritech, Inc. Environmental. Laboratory Laboratory Certification No. 165 Page 2 Report Date: 10/9/2018 Mocksville, NC 27028 Date Sample Rcvd: 10/2/2018 Meritech Work Order # 10021818 Sample: Reidsville WWTP Grab 10/2/18 Parameters Result AA,illysis Date Reporting Limit Method % Total Solids 0.72 % 10/3/18 0-100 % SM 25403 Fecal Coliform (Sludge) 10101 col/g dry wt 10/2/18 352 col/g dry wt SM 9222D Meritech Work Order # 10021819 Sample: Reidsville WWTP Grab 10/2/18 Para eters Result Analysis Date Reporting Limit Method % Total Solids 0.74% 10/3/18 0-100 % SM 2540B Fecal Coliform (Sludge) 7372 col/g dry wt 10/2/18 352 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. �& Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tei.(336)342-4748 fax.(336)342-1522 x Y Y E o O O a a d m s r p ti U a }" a L r T J F' 10^.. ZO a O I Q - .a `` a y 4 �# E E e -I N ro m on E 40 Ln N M1 o tS M M o Y N M M A vs W X J O a X cr "' .• ` LL a ° c t - CL { _ —41 0 CLU -a rLLn Q r u C O m v V a w w n m � ',� O m a CL a °a1 o G� _c E v� O L p C ti m Cn• F - n, GJ ,'a F� 12 C . v 4 q 0. d a E p E F E F= E w F-- c i N ULnW V n 41 'O y ti P+ m + 'N ch Z � a Y! Q O S3 O p ADA ,�O v V o= ~ O m m Q o a s U bA F: axe V;E U. '� o W CD 1 � W Z 'xN p W ° n z v Q ..' N M ?• H 4 z w y�'c p � " ny t�0 ce \ v v , E N Q vi C C p W cc 0i ¢ d ac 4— o � o �-' CLco � o v�t Meritech, Inc. Environmental Laboratory Jr Laboratory Certification No.165 Contact: Brent Collins CIient: EMA Resources, Inc Report Date: 1/5/2018 755 Yadkinville Road Mocksville, NC 27028 Project: Date Sample Rcvd; Reidsville 1/2/2018 Meritech Work Order # 01021866 Sample: Reidsville VS In Composite 1/2/18 Parameters suit Analjrsis Date R _- ortir Li ze 2ortin ._. imp d % Volatile Solids Total Solids Volatile Solids 75.4% 7188 m g/L 5420 mg/L 1/3/18 0-100 1/3/18 10.0 mg/L 1/3/18 10.0 mg/L SM 2540E SM 2540B SM 2540E Meritech Work Order # 01021867 Sample: Reidsville VS Out Composite 1/2/18 Paraau, t -rc Result Analyst_ Datg Religrti T unit ethod % Volatile Solids Total Solids Volatile Solids 48.0 % 5860 mg/L 2810 mg/L 1/3/18 0-100 % 1/3/18 10.0 mg/L 1/3/18 10.0 mg/L SM 2540E SM 2540E SM 2540E I hereby certify thatl have reviewed and approve these data, Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 N M CL rL � 4-1-1 10 abo 13 O o b T �b` ¢ 72,a O d o f„1 < �. 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Environmental Laboratory �.'v Laboratory Certification No. 165 Contact: Brent Collins Report Date: 7/31/2018 Client: EMA Resources, Inc 755 Yadkinville Road Project: Mocksville, NC 27028 Date Sample Rcvd: 6/26/2018 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test_ Meritech Work Order # 06261810 Sample: Reidsville Composite 6/26/18 Total Solids Volatile Solids % Volatile Solids Week 1 1.35 0.980 0.725 Week 2 1.23 0.880 0.711 Week 3 1.10 0.770 0.700 Week 4 1.12 0.780 0.696 Week 5 1.13 0.790 0.702 Van Kleek Reduction (%): 10.66 Pass or Fail Pass I hereby certify that I have reviewed and approve these data. iLI Lah6ratory Representative 642 Tarnco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 J Y 0 0 a Q N C Q m m Q a a �SD C Y - E O ui ci s v * E 0 M 0 LU C Z m u.. w o`_ CL f6 C c N E d a+ 41 Mv s- w E V 7 CC z CL y v c y �5 m Im,w o �A O 3 4+ a £ v a Z N U r i L 6 r- c Q. �' o v tA E E E • W l.J ai 1 Y Mme+ m N +� Q P o 0 0 1 to M m Q tC ba o ao > C. L a� a _ m m 0 W H d w(U - •0 0% n o �' U ; ° e '- uj 40- 0 o n, �� 5 N c u z 1 h V �} �° y cc m .. 0 Nb Ott' U E C: 0 O u o z w 43 _" C V 4" 1 h N p Q O tt v O a v v m t0 E a C C C a; .. lJ - a4; - a - a 41 u Fi `m Vf O N ? "yr *� o \Qj � %Ac'n r s . . 11 J Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: Brent Collins Report Date: 8/15/2018 Client: EMA Resources, Inc 755 Yadkinville Road Project: Reidsville Mocksville, NC 27028 Date Sample Rcvd: 7/11/2018 Vector Attraction Reduction /Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 07111834 Sample: Reidsville Composite 7/11/18 lotal Solids Volatile Solids % Volatile Solids Week 1 1.02 0.690 0.676 Week 2 1.07 0.730 0.683 Week 3 1.13 0.780 0.689 Week 4 1.05 0.730 0.695 Week 5 0.910 0.620 0.688 Van Kleek Reduction (%): -5.59 I hereby certify that I have reviewed and approve these data. Pass or Fail Pass �z Labv atory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 � Y Y O 00 `t G 00 z a N O CL dF 0 v z a CL 0 E e E v i '' p 3 n . z a as H o E o a y iy w C - cU# L. c a a Z LL w a a M1• � � N N I cc L fA N /� V y-- J� e N O CLw C , a A Q �. 'tS J -CL m41 O M a v v 3 ,N m a z a z ar > m O x CL Ew vi a E I cc 1 U C(� CO f6 iri O V m u z a a c c Y aF- a v E Ot? V U d Q a a u c 0 { �a N r dL '1 E ai W t-- p p F E � m v � tu l/1 W V W a N {n C oN`-i O COW of y CV u Q� Q n ❑ ❑ a r• ® OCen cx ftk m M M u ® = O Q O 0 �CL ~ OV �� G 0 � �` W M- E m O ' Z @J _ m N G 4+ 0 uu �® c {� m -" y N °� = Q M (U _o 5- m ;N E c v a� -� O WN cc u z 0 W a vi u Fm > Q p � p G _9 w d E (O Cu E 7 G J C J G m C O U a s o°1c O ' O .."J O -c E a U Q M. � LL o E a v 17111 011, Meritech, Inc. Environmental Laboratory Awl Laboratory Certification No. 165 Contact: Brent Collins Report Date: 11/9/2018 Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Date Sample Rcvd: 10/2/2018 Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 10021820 Sample: Reidsville WWTP Composite 10/2/18 Total Solids Volatile Solids % Volatile Solids Week 1 0.590 0.390 0.657 Week 2 0.530 0.340 0.631 fttk 3 0.550 0.350 0,634 Week 4 0.510 0.330 0.641 Week 5 0.480 0.310 0.646 Van Kleek Reduction (%): 5.07 Pass or Fail PASS I hereby certify that I have reviewed and approve these data. 4 6wrco'k-'� .Laboratory epresentative 642 Tarnco Road, _Ref Reidsville North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 a CL CL ry O, U , a 4 }= = *_ Y 4 ro d Z J o� O c m t�I i 1 N pppp Ln Ln O H Q � r 1 V C G a+ R Q LO lC7 G K Q M M sa x a= m E o 0 °.. i6 V 2 a of w L X V1 LL la 0 QOi a V CL M N 00{.. � �1= i N O 3 �' c%i w Y OC uU m Y w K Cf n p. 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