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Home My WebLink AboutWQ0005603_GroundwaterHistoricFileB_20190205�c�-•u %O=moo 000 ai��CDCDCD'�oC�^Nm N>= Cl) Cl) o 0 0 CD CD col 30 CL sL�cf)I O.Q. 0 o -n 'n C - W.0�. =r.CD '� CD N Sao' _ate CD M. 7 CA � = O 0 � d CD 0 c o 0 33=333333=3 003 CC) ca 0 cc ca cn cn cn cn n 3 3 ca o = =N ==== ==al = --= a KK;r,=moqppm>o-ozzkl -p t' s 1 3 1 i i 7 ?� C. M w 23 CD O -- Cv w w c,� N �- C1n C 0 O) Zz U3 0 �. 0 � 3 E a 00ID -4 �Ca 3`�3�i=-� w CD M 0vwz —z N -0 Z O m G co a 333333333333333 cQ co cn cn Coco cfl co ca cn ca cn cQ cn ct? ? CL 0ID o 9 C7 0 m � z 0 ow cry CD a a 3 p 0 �rr o CD 0 3a3(aCLK 0 O O C1 C2 C3..-..�. r syn (7 u n n zr TA o rs ro o I 0 � o a^� C) v 0>N -0Z K �.CD 3=cr ' ' ' -,oNrZ-C m 0)CDCD M CA Iz o o O CSD 00 z CL N O. 0 O 0 CD 1 :L c3333 2. c0 c0 (m ca CA C co T O 0 z m r r O D m O z 1Cl) Cl) -0 0—I -a 0z C7 C)0 o-aC= ,=0iNgOop Z v M. m O_ C�.-. CA NQ. D CD 0 tip p' t1 u 00 z30 .0 0m0.1 3 0 n. 0 Gr,z -2a C 0 w � o - I -n w U) Ncno 00 CD m CL t7 � r z O C a' m a � $vl CA 3 � a C o` .e O n 3 =r c 8 0 3 5 3�333333a3 00 to o o co co to ccs ED ca ;=( 3 3 to �. 3 . T /� /� /� /� �7 r• .:� Co 1 to (D G ? Q N SD =, :+ Ip CS I 1- 1 1 0 ,,;e C. c�3 C�c7�D-o'M m o �0--m SD ? •-% a�-ocM6-.3oo2z coo�.a �33.�3�`�2004 SCD - 033 3o�?w-"Ncl), CD w o�rnZ —Z su Irn Z O m . a a r_ tD Q m 333333333333333 co co to ca cc cc co cc Coo Co ca to to to c m CL 03cr CD 03 N t- Z N0 0 0)(xD Z _ 0 CO 0 CD 0 0 c CL N in O CL 0 n CD tv 0 1 1 1 1 c3333 y Pace Analytical Services Report Date Project No. <T; ASR Work Order No. ��` /V�„ctc�yRtNG �eI Page 5' . 1/04/. 9812-00600' o. Sample I Date Sampled Time Sampled Matrix Condition 05 MW -11 /93134591 12/17/1998 7:50 GW 4+2°C Test Performed Method Date Results Tech Analyzed Qual VOCs in GW SN: 6230D ZW 12/29/98 Benzene <0.5 ug/L ZW 12/29/98 Bromobenzene <0.5 ug/L ZW 12/29/98 Bromochloromethane <0.5 ug/L ZW 12/29/98 Bromodichloromethane <0.5 ug/L ZW 12/29/98 Bromoform <0.5 uS/L ZW 12/29/98 Bromomethane <0.5 ug/L ZW 12/29/98 n-Butylbenzene <0.5 ug/L ZW 12/29/98 sec-Butylbenzene <0.5 ug/L ZW 12/29/98 tent-Butylbenzene <0.5 ug/L ZW 12/29/98 Carbon tetrachloride <0.5 ug/L ZW 12/29/98 Chlorobenzene <0.5 ug/L ZW 12/29/98 Chloroethane <0.5 ug/L ZW 12/29/98 Chloroform <0.5 ug/L ZW 12/29/98 Chloromethane <0.5 ug/L ZW 12/29/98 2-Chlorotoluene <0.5 ug/L ZW 12/29/98 4-Chlorotoluene <0.5 ug/L ZW 12/29/98 Dibromochloromethane <0.5 ug/L ZW 12/29/98 1,2-Dibromo-3-chloropropane <0.5 u3/L ZW 12/29/98 1,2-Dibromoethane <0.5 ug/L ZW 12/29/98 Dibromomethane <0.5 ug/L ZW 12/29/98 Dichlorodifluoromethane <0.5 ug/L ZW 12/29/93 1,1-Dichloroethane <0.5 ug/L ZW 12/29;'98 1,2-Dichloroethane <0.5 ug/L ZW 12/29/98 1,1-Dichloroethene <0.5 ug/L ZW 12/29/96 cis-1,2-Dichloroethene <0.5 ug/L ZW 12/29/98 trans-1,2-Dichloroethene <0.5 ug/L ZW 12/29/98 1,2-Dichloropropane <0.5 ug/L ZW 12/29/98 1,3-Dichloropropane <0.5 ug/L ZW 111/29/98 2,2-Dichloropropane <0.5 ug/L ZW 12/29/98 1,1-Dichloropropene <0.5 ug/L ZW 12/29/98 Ethylbenzene <0.5 ug/L ZW 12/29/98 Hexachlorobutadiene <0.5 ug/L ZW 12/29/98 Isopropylbenzene <3.5 ug/L Zw 12/29/53 4-Isopropyltoluene <0.5 ug/L ZW 12/29/98 Methylene chloride <0.5 ug/L ZW 12/29/98 Naphthalene <0.5 ug/L ZW 12/29/98 n-Propylbenzene <0.5 ug/L ZW 12/29/98 Styrene <0.5 ug/L ZW 12/29/98 ---- Continued on Next Page ---- ae Analytical Services Report Date P ' ect No 'TER Work Order No (' lDttl�Or /N4 �C-1 f N o . Sample I OQS MW -1193134591 Page 1/04, 9812-0060 No. Sample ID Date Sampled Time Sampled Matrix Date Test Performed Method Results Tech Analyzed Qua! 1,1,1,2 -Tetrachloroethane <0.5 ug/L Zw 12/29/98 1,1,2,2 -Tetrachloroethane <0.3 ug/L Zw 12/29/93 Tetrachloroethene <0.5 ug/L ZW 12/29/98 Toluene <0.5 ug/L Zw 12/29/98 1,2,3-Trichlorobenzene <0.5 ug/L ZW 12/29/98 1,2,4-Trichlorobenzene <0.5 ua/L Zw 12,'29/98 1,1,1 -Trichloroethane <0.5 ug/L Zi+' 12/29/98 1,1,2 -Trichloroethane <0.5 ug/L Zw 12/29/98 Trichloroethene <0.5 ug/L ZW 12/29/58 Trichlorofluoromethane <0.5 ug/L ZW 12/29/98 1,2,3-Trichloropropane <0.5 ug/L Zw 12/29/98 1,2,4-Trimethyl:- !nzene <0.5 ug/L Zw 12/29/98 1,3,5-Trimethylbenzene <0.5 ug/L ZW 12/29/98 Vinyl chloride <0.5 ug/L ZW 12/29/98 o-Xvlene <0.5 ug/L ZW 12/29/98 m,p-Xylene <0.5 ug/L ZW 12/29/98 No. Sample ID Date Sampled Time Sampled Matrix Condition 006 MW -12 / 93134617 12/17/1998 8:05 GW c -2°C Dace Test Performed Method Results Tech Analyz..: Qual VOCs in GW SM 6230D ZW 12/29/98 Benzene <0.5 ug/L• Zw 12/29/98 Bromobenzene <0.5 ug/L ZW 12/29/98 Bromochloromethane <0.5 ug/L ZW 12/29/98 Bromodichloromethane <0.5 ug/L Zw 12/29/98 Bromoform <0.5 ug/L ZW 12/29/98 Bromomethane <0.5 ug/L Zw 12/29/98 n-Butylbenzene <0.5 ug/L ZW 12/29/98 sec-Butylbenzene <0.5 ug/L ZW 12/29/98 tert-Butylbenzene <0.5 ug/L Zw 12/29/98 Carbon tetrachloride <0.5 ug/L Zw 12/29/98 Chlorobenzene <0.5 ugjL Zw 12/29/98 Chloroethane <0.5 ug/L Zw 12/29/98 Chloroform <0.5 ug/L Zw 12/29/99 Chloromethane c0.5 ug/L ZW 12/29/98 2-Chlorotoluene <0.5 ug/L ZW 12/29/98 ---- Continued on Next Page ---- .p J) C/A -0 G n --I t� O z C7 C7 C7 ?! 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CD �j r- 0 0 w Q `< D 0. w c p 0 0 (n c CL CD Cl) a -n m a 0 U) CD o � c r at CD ,0 N c (D r 0 CD 0 m c 0 0 D -4 `"0 0 z W m Z ,n„ ) a 0 O Z --I U) 7) m o w 0 m 'T1 m' a -4� ;ENVIRONMENTAL TECF---IOLOGY, INC. ENVIRONMENTAL ANALYTICAL SERVICES FINAL REPORT OF ANALYSES PACE ANALYTICAL SERVICES, INC. 54 RAVENSCROFT DR. REPORT DATE: 12/30/97 ASHEVILLE, NC 28801- P.O. # 93 001621 COATS AMERICMW-1 SAMPLE NUMBER- 9668 SAMPLE ID- MW -11 # 1805 SAMPLE MATRIX- GW DATE SAMPLED- 12/16/97 TIME SAMPLED- 0830 DATE RECEIVED- 12/17/97 SAMPLER- P.P. RECEIVED BY- CLH TIME RECEIVED- 1025 DELIVERED BY- UPS Page 1 of 3 PROJECT NAME : COATS AMERICAN P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511 Telephone (919) 467-3090 Fax (919) 467-3515 ANALYSIS ANALYSIS METHOD DATE BY RESULT UNITS PQL VOLATILE ORGANIC COMPOUNDS 6230D 12/23/97 ALT BENZENE 6230D < 0.5 ug/L 0.5 BROMOBENZENE 6230D < 0.5 ug/L 0.5 BROMOCHLOROMETHANE 6230D <,0.5 ug/L 0.5 BROMODICHLOROMETHANE 6230D < 0.5 ug/L 0.5 BROMOFORM 6230D < 0.5 ug/L 0.5 BROMOMETHANE 6230D < 0.5 ug/L 0.5 n-BUTYLBENZENE 6230D < 0.5 ug/L 0.5 sec-BUTYLBENZENE 6230D < 0.5 ug/L 0.5 tert-BUTYLBENZENE 6230D < 0.5 ug/L 0.5 CARBON TETRACHLORIDE 6230D < 0.5 ug/L 0.5 CHLOROBENZENE 6230D < 0.5 ug/L 0.5 CHLOROETHANE 6230D < 0.5 ug/L 0.5 CHLOROFORM 6230D < 0.5 ug/L 0.5 CHLOROMETHANE 6230D < 0.5 ug/L 0.5 2-CHLOROTOLUENE 6230D < 0.5 ug/L 0.5 4-CHLOROTOLUENE 6230D < 0.5 ug/L 0.5 DIBROMOCHLOROMETHANE 6230D < 0.5 ug/L 0.5 1,2-DIBROMO-3-CHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,2-DIBROMOETHANE 6230D < 0.5 ug/L 0.5 DIBROMOMETHANE 6230D < 0.5 ug/L 0.5 P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511 Telephone (919) 467-3090 Fax (919) 467-3515 -.,;AL ENVIRONMENTAL TEC"LOGY, INC. ENVIRONMENTAL ANALYTICAL SERVICES Page 2 of 3 PROJECT NAME : COATS AMERICAN CONTINUATION OF DATA FOR SAMPLE NUMBER 139668 ANALYSIS ANALYSIS METHOD DATE BY RESULT UNITS PQL 1,2 -DICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,3 -DICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,4 -DICHLOROBENZENE 6230D 4.1 ug/L 0.5 DICHLORODIFLUOROMETHANE 6230D < 0.5 ug/L 0.5 1,1-DICHLOROETHANE 6230D < 0.5 ug/L 0.5 1,2-DICHLOROETHANE 6230D < 0.5 ug/L 0.5 1,1 DICHLOROETHENE 6230D < 0.5 ug/L 0.5 Cis-1,2-DICHLOROETHENE 6230D < 0.5 ug/L 0.5 trans-1,2-DICHLOROETHENE 6230D < 0.5 ug/L 0.5 1,2-DICHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,3-DICHLOROPROPANE 6230D < 0.5 ug/L 0.5 2,2-DICHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,1-DICHLOROPROPENE 6230D < 0.5 ug/L 0.5 Cis-1,3-DICHLOROPROPENE 6230D < 0.5 ug/L 0.5 trans-1,3-DICHLOROPROPENE 6230D < 0.5 ug/LL 0.5 ETHYLBENZENE 6230D < 0.5 ug/L 0.5 HEXACHLOROBUTADIENE 6230D < 0.5 ug/L 0.5 ISOPROPYLBENZENE 6230D < 0.5 ug/L 0.5 p-ISOPROPYLTOLUENE 6230D < 0.5 ug/L 0.5 METHYLENE CHLORIDE 6230D < 0.5 ug/L 0.5 NAPHTHALENE 6230D < 0.5 ug/L 0.5 n-PROPYLBENZENE 6230D < 0.5 ug/L 0.5 STYRENE 6230D < 0.5 ug/L 0.5 1,1,1,2 -TETRACHLOROETHANE 6230D < 0.5 ug/L 0.5 1,1,2,2 -TETRACHLOROETHANE 6230D < 0.5 ug/L 0.5 TETRACHLOROETHENE 6230D < 0.5 ug/L 0.5 TOLUENE 6230D < 0.5 ug/L 0.5 1,2,3-TRICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,2,4-TRICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,1,1 -TRICHLOROETHANE 6230D < 0.5 ug/L 0.5 1,1,2 -TRICHLOROETHANE 6230D < 0.5 ug/L 0.5 P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511 Telephone (919) 467-3090 Fax (919) 467-3515 _.(. AL ��ENVIRONMENTAL TEChr ,OLOGY, INC. ENVIRONMENTAL ANALYTICAL SERVICES Page 3 of 3 PROJECT NAME COATS AMERICAN CONTINUATION OF DATA FOR SAMPLE NUMBER 139668 ANALYSIS ANALYSIS METHOD DATE BY RESULT UNITS PQL TRICHLOROETHENE 6230D < 0.5 ug/L 0.5 TRICHLOROFLUOROMETHANE 6230D < 0.5 ug/L 0.5 1,2,3-TRICHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,2,4-TRIMETHYLBENZENE 6230D < 0.5 ug/L 0.5 1,3,5-TRIMETHYLBENZENE 6230D < 0.5 ug/L 0.5 VINYL CHLORIDE 6230D < 0.5 ug/L 0.5 o -XYLENE 6230D < 0.5 ug/L 0.5 m,p-XYLENES 6230D < 0.5 ug/L 0.5 SURROGATE a 6230D 91.1 percent - SURROGATE b 6230D 100 percent - PQL = Practical Quantitation Limit Results followed by the letter J are estimated concentrations. NC DEHNR CERTIFICATIONS: DWQ - 96; PUBLIC WATER SUPPLY - 37724 LABORATORY DIRECTOR P.O. 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CD 3 w 0(D Z Z N r 3 3 3 3 3 3 3 3 3 3 3 3 3'3 cccc�cQcccccQCQcc�cQcccQ�cc C) = =F Ci CD D N Cn r. -a o m 3• n O 3 O :? w Q -0N-UZ o CD D CD CO Q � CD n o (D 0 QCCDD -0 _ C o CD cr OL cn eld,sJ„:.ccc 333 CQ (Q (Q (C] (Q (Q CL TN07C3C=w- Z o W� CD �Z:r m ° an) CD O 0^Q m QQ =. fcDECD Q n CCD w Q`3Q n CD N Q Q z CD w• w2 CD PQ 33 nti w 7 O- O w CD _� c0 Q *-a O W wCD O CD w o 0 �p 3 m I V' W (n z /0� w- --zQ m N� m3 yD -a Q T� T� TI 0 -r—n I a 07 N CO G N0)0 n M j m a CD co CD �-- Fv CD O O C7 m m �70 0 CD O O CD cQ � r n cn m n CCD 3 n ; m a�. C n w cn m c c W ? < d < 77 N -a o CD CD �! m m 6 i m m3 C o 0 zmC a M� CD -n-a w` Safi `o o =) m m CD -o CD v n n -n -n I m z t%l a ti O 5- r U)0 O VV O s 7 N ._• m m cfl c a � w w CD v p O CDv � w I I < i� 1�. �-11 333-3c:,: 003 CD cQ cQ cQ cQ CD 33, ZKKA=MC)OOOW>Mzz ��cQ cQCDczrQww —�� -� o ' Q o o K=703 w �6CD Q - w wQ�ocn,�an� oz Z( 3wcDcc m..-_c3cccn00 �cn3� c3 ca., CD 03 3`. CD 3 w 0(D Z Z N r 3 3 3 3 3 3 3 3 3 3 3 3 3'3 cccc�cQcccccQCQcc�cQcccQ�cc C) = =F Ci CD D N Cn r. -a o m 3• n O 3 O :? w Q -0N-UZ o CD D CD CO Q � CD n o (D 0 QCCDD -0 _ C o CD cr OL cn eld,sJ„:.ccc 333 CQ (Q (Q (C] (Q (Q m m V, i m - CL D -a 70 -< m K O w CD W O Q p CD O CD CD w 'o _== CD w• CnD= cimpar O M O w 7 O- O w CD _� c0 mZm ®w *-a O W wCD O CD w o 0 �p 3 m o m : - o m =-a m N� L m3 yD -a m — C CD 3 I a 07 N CO 00 m n CD M j m a CD co CD �-- Fv O O C7 m m �70 0 CD O O CD cQ � r n cn m n 6 3 3 n ; m a�. C n w cn m c c < d < 77 N -a o CD CD �! m m 6 � m m3 C o 0 zmC a M� CD -n-a w` Safi `o o =) m m CD -o CD v n n -n -n I m z O �n ti O 5- r U)0 O VV O s 7 N m m V, i m - CL -a 70 -< m -V w• O m _� c0 : m m — MO-DZ z v Q' o - z 00 I I I I co CD r �70 cQ � O CD m m o 0) a m c N d < O D o 70 -n-+ v No m O n z `o o =) m clO I I CD z O 5- r U)0 O VV 3 CD s 7 N ._• m m cfl c a � w w CD v p O � w N m CL CD Mr. Jerry McKinney Page 2 Client Reference: Coats American Pace Analytical Service, 54 Ravenscroft Asheville, NC A Tel: 704-254-7176, Fax: 704-252-4618 January 06, 1997 PACE Project Number: A6120551� PACE Sample Number: 93 0315526 Date Collected: 12/10/96 Date Received: 12/11/96 Client Sample ID: GM -3 #1419 Parameter Units PRL Coats METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 Dichlorodifluoromethane ug/L 1.0 ND 12/18/96 Chloromethane ug/L 1.0 ND 12/18/96 Chloroethene (Vinyl chloride) ug/L 1.0 ND 12/18/96 Bromomethane ug/L 1.0 ND 12/18/96 Chloroethane ug/L 1.0 ND 12/18/96 Trichlorofluoromethane ug/L 1.0 ND 12/18/96 1,1-Dichloroethene ug/L 1.0 ND 12/18/96 Dichloromethane ug/L 1.0 ND 12/18/96 trans-1,2-Dichloroethene ug/L 1.0 ND 12/18/96 1,1-Dichloroethane ug/L 1.0 ND 12/18/96 cis-1,2-Dichloroethene ug/L 1.0 ND 12/18/96 2,2-Dichloropropane ug/L 1.0 ND 12/18/96 Chloroform ug/L 1.0 ND 12/18/96 Bromochloromethane ug/L 1.0 ND 12/18/96 1,1,1 -Trichloroethane ug/L 1.0 ND 12/18/96 1,1-Dichloro-l-propene ug/L 1.0 ND 12/18/96 Carbon tetrachloride ug/L 1.0 ND 12/18/96 1,2-Dichloroethane ug/L 1.0 ND 12/18/96 1,1,2 -Trichloroethene ug/L 1.0 ND 12/18/96 1,2-Dichloropropane ug/L 1.0 ND 12/18/96 Bromodichloromethane ug/L 1.0 ND 12/18/96 Dibromomethane ug/L 1.0 ND 12/18/96 cis-1,3-Dichloro-l-propene ug/L 1.0 ND 12/18/96 trans-1,3-Dichloro-1-propene ug/L 1.0 ND 12/18/96 1,1,2 -Trichloroethane ug/L 1.0 ND 12/18/96 1,3-Dichloropropane ug/L 1.0 ND 12/18/96 Tetrachloroethene ug/L 1.0 ND 12/18/96 Dibromochloromethane ug/L 1.0 ND 12/18/96 1,1,1,2 -Tetrachloroethane ug/L 1.0 ND 12/18/96 Bromoform ug/L 1.0 ND 12/18/96 1,1,2,2 -Tetrachloroethane ug/L 1.0 ND 12/18/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Mr. Jerry McKinney Page 3 Client Reference: Coats American - Pace Analytical Service 54 Ravenscroft t. ARhPVIIIP Nr. ')a. '... Tel: 704-254-7176. Fax: 704-252-4618 January 06, 1997 PACE Project Number: A612055. PACE Sample Number: 93 0315526 Date Collected: 12/10/96 Date Received: 12/11/96 Client Sample ID: GM -3 #1419 Parameter Units PRL Coats METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 1,2,3-Trichloropropane ug/L 1.0 ND 12/18/96 Bromobenzene ug/L 1.0 ND 12/18/96 " 2-Chlorotoluene ug/L 1.0 ND 12/18/96 4-Chlorotoluene ug/L 1.0 ND 12/18/96 1,3 -Dichlorobenzene uL 1.0D- �� 12/18/96 1,4 -Dichlorobenzene ug/L 1.0 (5.7' 12/18/96 1,2 -Dichlorobenzene ug/L 1.0 ND 12/18/96 1,2-Dibromo-3-chloropropane ug/L 1.0 ND 12/18/96 1,2,4-Trichlorobenzene ug/L 1.0 ND 12/18/96 Hexachlorobutadiene ug/L 1.0 ND 12/18/96 1,2,3-Trichlorobenzene ug/L 1.0 ND 12/18/96 Benzene ug/L 1.0 ND -12/18/96 Toluene ug/L 1.0 ND 12/18/96 Chlorobenzene ug/L 1.0 ND 12/18/96 Ethylbenzene ug/L 1.0 ND 12/18/96 Xylenes, (total) ug/L 1.0 ND 12/18/96 Styrene ug/L 1.0 ND 12/18/96 Isopropylbenzene ug/L 1.0 ND 12/18/96 n-Propylbenzene ug/L 1.0 ND 12/18/96 1,3,5-Trimethylbenzene ug/L 1.0 ND 12/18/96 t-Butylbenzene ug/L 1.0 ND 12/18/96 1,2,4-Trimethylbenzene ug/L 1.0 ND 12/18/96 s-Butylbenzene ug/L 1.0 ND 12/18/96 4-Isopropyltoluene ug/L 1.0 ND 12/18/96 n-Butylbenzene ug/L 1.0 ND 12/18/96 Naphthalene ug/L 1.0 ND 12/18/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. 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CL N w a O 6 fD Z 0 m OCD¢1 O O Q � � N 0 S O O O 0 CL O m � tD o O ^" Q) CL (j) O W Q. O m Q a A 0 W O M OJ (/) 0M -Cf) CO -0� O'er (D O ° n 000 Z—°fv�a-iUmoCi..fn!o r¢' W _ 3 *ocoo m CDg �� -n Z (D _ C cn 0 om i (n'S D m N CD O O O O Z1-lCt' �� W -i n N a (D (n CL �O� a. s -1 'n, ca c CDc m m�ZCD D R=x Z CD O1 Q 0 - D � ` OL C ro 0 O , c -DI m c ro Cr N 0) E C (D 0- CD 7 C w 0 CL K N O 0 O 72.N O 0 w O. CL N w a O 6 fD Z 0 m OCD¢1 O O Q � � N 0 S O O O 0 CL O m � tD o O ^" Q) CL (j) O W Q. O m Q a A 0 W I l a 335333333353 Ca CO O Ca (a CQ Ca CO CQ Co +(a j j Imo' 003 3310 ZKcQ;r%(a(Dc�Q WD=ZZ 0 ' 0> w �KK0K0030 0��cDO !:-t cim-0�a_c—, 62Z c(a�(n.� m 3 ��3r)p 3WCDc� 3c(n(a cDC•3 03 m3 �(nz i -Z 3 3 3 3 3 3 3 3 3 3 3 3 23 3 c0 c0 (a to ca c0 c0 cO cQ c0 ca cQ c0 c0 (a- --------------- n i O -a n zT ,CD C-Dt 0 0 O n C: 2.0 3 O c cn a w Q C: c c Ca CQ CQ -0N-0Z CD :3 Cr CD .= -f o o Nr - Z CD 0 o CD n a_ (D -0 2 o (D c O cr CLQL n (OD 3 3 3 Ca Ca Ca O M OJ (/) 0M -Cf) CO -0� O'er (D O ° n 000 Z—°fv�a-iUmoCi..fn!o r¢' —— wD-« =3 (n �' 0 ci O n *ocoo m CDg �� -n Z 3 N 0 o O 3 CCD 7CD � om i (n'S cD O.Q�9 N CD O O D oo -_�{ cp 3 Z1-lCt' �� W -i n N a 0�0 W - tv c �O� a. s -1 'n, c D co m�ZCD O o' CD O1 Q 0 (r o � ` OL ro 0 O , c CD 0 0 n CCL D I zol Lq , � (n s � = c S- n o 3 � 3 Q D 01 �`i a°•aN C CD C 0 v 0 C: z r w w � P �I n r lD CD fD o =3cn C 'a ` m w CD m - CD D O CD N cn CD n D w -n Fn =3 SD 0 3 a --q LA S 1 (0 I l a 335333333353 Ca CO O Ca (a CQ Ca CO CQ Co +(a j j Imo' 003 3310 ZKcQ;r%(a(Dc�Q WD=ZZ 0 ' 0> w �KK0K0030 0��cDO !:-t cim-0�a_c—, 62Z c(a�(n.� m 3 ��3r)p 3WCDc� 3c(n(a cDC•3 03 m3 �(nz i -Z 3 3 3 3 3 3 3 3 3 3 3 3 23 3 c0 c0 (a to ca c0 c0 cO cQ c0 ca cQ c0 c0 (a- --------------- n i O -a n zT ,CD C-Dt 0 0 O n C: 2.0 3 O c cn a w Q C: c c Ca CQ CQ -0N-0Z CD :3 Cr CD .= -f o o Nr - Z CD 0 o CD n a_ (D -0 2 o (D c O cr CLQL n (OD 3 3 3 Ca Ca Ca in O M OJ (/) 0M Dc A) M—w 0 M02C �S o (6D p• Q fD N (D r¢' O . � ccn (AN - — --o 0 AA) 3 O • o 0 O co -n Z m (*-0 N 0 o O 3 " N 7CD � om i (n'S cD O0 = "0 N CD O O D oo -_�{ cp 3 (D �� 0 y -i n N a v 3 CL N c D co m�ZCD o' m o � Z OL ro 0 O , c 0 0 n CCL D I zol r �1 , � (n Cr (D @ O< O = c S- n o 3 � 3 Q D m a°•aN C CD C 0 v 0 C: z r w w � .n r n r lD CD fD o =3cn C 'a ` m w CD m - CD D O CD cn CD n D w -n Fn =3 SD 0 3 a --q LA S CD C 0- (0 � a 0 ,n FTiv O m CD a in O M OJ (/) 0M jp m w p A � o R c m z c z O O CD M v-0� v om i (n'S z > M OJ (/) 0M O p R O CD M �} fOD o °co M C D oo -_�{ m- 0 y TI v m O v CL Z c m co o' m o � Z 0 O , c CCL D I zol O �N (n D C CD C 0 C I'' r w w � 0 o m Mr. Jerry McKinney Page 5 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS January 02, 1996 PACE Project Number: A51, 93 0156355 12/05/95 12/06/95 K80L-11 Units MDL #1031 DATE ANALYZED Dichlorodifluoromethane ug/L 1.0 ND _ 12/13/95 Chloromethane ug/L 1.0 ND 12/13/95 Chloroethene (Vinyl chloride) ug/L 1.0 ND 12/13/95 Bromomethane ug/L 1.0 ND 12/13/95 Chloroethane ug/L 1.0 ND 12/13/95 Trichlorofluoromethane ug/L 1.0 ND 12/13/95 1,1-Dichloroethene ug/L 1.0 ND 12/13/95 Dichloromethane ug/L 1.0 ND 12/13/95 trans-1,2-Dichloroethene ug/L 1.0 ND 12/13/95 1,1-Dichloroethane ug/L 1.0 ND 12/13/95 cis-1,2-Dichloroethene ug/L 1.0 ND 12/13/95 2,2-Dichloropropane ug/L 1.0 ND 12/13/95 Chloroform ug/L 1.0 ND 12/13/95 Bromochloromethane ug/L 1.0 ND 12/13/95 1,1,1 -Trichloroethane ug/L 1.0 ND 12/13/95 1,1-Dichloro-1-propene ug/L 1.0 ND 12/13/95 Carbon tetrachloride ug/L 1.0 ND 12/13/95 1,2-Dichloroethane ug/L 1.0 ND 12/13/95 1,1,2 -Trichloroethene ug/L 1.0 ND 12/13/95 1,2-Dichloropropane ug/L 1.0 ND 12/13/95 Bromodichloromethane ug/L 1.0 ND 12/13/95 Dibromomethane ug/L 1.0 ND 12/13/95 cis-1,3-Dichloro-l-propene ug/L 1.0 ND 12/13/95 trans-1,3-Dichloro-l-propene ug/L 1.0 ND 12/13/95 1,1,2 -Trichloroethane ug/L 1.0 ND 12/13/95 1,3-Dichloropropane ug/L 1.0 ND 12/13/95 Tetrachloroethene ug/L 1.0 ND 12/13/95 Dibromochloromethane ug/L 1.0 ND 12/13/95 1,1,1,2 -Tetrachloroethane ug/L 1.0 ND 12/13/.95 Bromoform ug/L 1.0 ND 12/13/95 1,1,2,2 -Tetrachloroethane ug/L 1.0 ND 12/13/95 0 ods I JAN 4 190, An Equal Opportunity Employer Gyy r Mr. Jerry McKinney Page 6 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS 1,2,3-Trichloropropane Bromobenzene 2-Chlorotoluene 4-Chlorotoluene 1,3-Dichlorobenzene-- 1,4-Dichlorobenzene ,3-Dichlorobenzene-1,4-Dichlorobenzene 1,2 -Dichlorobenzene 1,2-Dibromo-3-chloropropane 1,2,4-Trichlorobenzene Hexachlorobutadiene 1,2,3-Trichlorobenzene Benzene Toluene Chlorobenzene Ethylbenzene Xylenes Styrene Isopropylbenzene'* n-Propylbenzene - 1,3,5-Trimethylbenzene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 4-Isopropyltoluene n-Butylbenzene Naphthalene Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L MDL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 January 02, 1996 PACE Project Number: A51"L 93 0156355 12/05/95 12/06/95 K80L-11 #1031 DATE ANALYZED ND ND ND ND ND 5.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NO ND NO 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 12/13/95 0) .D 60_ W (D CD (D 0 C: O U) m a(D � w g� c 0 �o R (Q ID 0 CD ID d CL o Y M 0 0 N 0 3 •e 0 0) C1 O. m N N N cr 0 x Z O CD O C � N h � O O v 0 g ort rt (D 0 C. U N O (D W 0 00 A 0 CL rr 2) Cl) W �o-o c ��,i'�D��2Oc 0 o n �(DN O to„ __O Zps0pi c- mo(�--o 00p �'30o�(cDi,CD('m mm 33 Z30 9�aM � 00 cl N �_ N Q 0 0 CD :33 f., 0- 0 n Lei O (D .Fate I I c 1 I I I I I I 1 1 33�33333333 (O (c O Co (m (Q (0 CQ (Q (Q rrCQ In, 6o3 ZKK;r,= I0000w>mZZ Sv O CQ cc CD C =r a M =;4: ,-=f Y Y i O Y(n p) cnKK0ro 0 03 �in�C oN a�� -6 a6m.3oZZ c(0=3 C: CD-- 5c00 3WCCD �--��3 D c 3 0 3 CD 3 ZZ 3333333333333-33 cQ co cQ cQ co co cc cc co (c cQ cc cc cQ cc 0 p 1n CD (D �1 wC/)�_0 CD0 v o O C Q O.. 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07 �} 0 m z a O L c CL I I z Q vcn W f�SD C 7 N CD ^ 0 c 0 U N �o 7 0 Ip T IN CD C �- [D _ I N C O R P O R A T E D THE ASSURANCE OF QUALITY Mr. Jerry McKinney Page 9 Client Reference: Coats American May 02, 1995 PACE Project Number: A50412: PACE Sample Number: 93 0079539 Date Collected: 04/11/95 Date Received: 04/11/95 Client Sample ID: K80L-11 Parameter Units MDL ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS Date Extracted, Base/Neutrals and Acids Date 041795 N-Nitrosodimethylamine ug/L 5.0 ND bis(2-Chloroethyl)ether ug/L 6.0 ND Phenol ug/L 5.0 ND 2 -Chlorophenol ug/L 5.0 ND 1,3 -Dichlorobenzene ug/L 5.0 ND 1,4 -Dichlorobenzene ug/L 5.0 ND 1,2 -Dichlorobenzene ug/L 5.0 ND bis(2-Chloroisopropyl)ether ug/L 6.0 ND Hexachloroethane ug/L 5.0 ND N-Nitrosodi-n-propylamine ug/L 5.0 ND Nitrobenzene ug/L 5.0 ND 3,5,5-Trimethyl-2-cyclohexanone ug/L 5.0 ND 2-Nitrophenol ug/L 5.0 ND 2,4 -Dimethylphenol ug/L 5.0 ND bis(2-Chloroethoxy)methane ug/L 5.0 ND 2,4-Dichlorophenol ug/L 5.0 ND 1,2,4-Trichlorobenzene ug/L 5.0 ND Naphthalene ug/L 5.0 ND Hexachlorobutadiene ug/L 5.0 ND 4-Chloro-3-methylphenol ug/L 5.0 ND Hexachlorocyclopentadiene ug/L 5.0 ND 2,4,6 -Trichlorophenol ug/L 5.0 ND 2-Chloronaphthalene ug/L 5.0 ND Acenaphthylene ug/L 5.0 ND Dimethyl phthalate ug/L 5.0 ND 2,6-Dinitrotoluene ug/L 5.0 ND Acenaphthene ug/L 5.0 ND 2,4-Dinitrophenol ug/L 42 ND 2,4-Dinitrotoluene ug/L 6.0 ND 4-Nitrophenol ug/L 5.0 ND 54 Ravenscroft Drive Asheville, NC 28801 TEL: 704-254-7176 rAV - ins nr" Ar,r AY 2 3 10 An Equal Opportunity Employer ® I N C O R P O R A T E D THE ASSURANCE OF QUALITY Mr. Jerry McKinney Page 10 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS REPORT OF LABORATORY ANALYSIS,, Units MDL May 02, 1995 PACE Project Number: A504125 93 0079539 04/11/95 04/11/95 K80L-11 Fluorene ug/L 5.0 ND 4-Chlorophenyl phenyl ether ug/L 5.0 ND Diethyl phthalate ug/L 5.0 ND 2-Methyl-4,6-dinitrophenol ug/L 24 ND N-Nitrosodiphenylamine ug/L 5.0 ND 4-Bromophenyl phenyl ether ug/L 5.0 ND Hexachlorobenzene ug/L 5.0 ND Pentachlorophenol ug/L 5.0 ND Phenanthrene ug/L 5.0 ND Anthracene ug/L 5.0 ND Di -n -butyl phthalate ug/L 5.0 ND Fluoranthene ug/L 5.0 ND Benzidine ug/L 50 ND Pyrene ug/L 5.0 ND Benzyl butyl phthalate ug/L 5.0 ND 3,3-Dichlorobenzidine ug/L 17 ND Benz[a]anthracene ug/L 8.0 ND Chrysene ug/L 5.0 ND bis(2-Ethylhexyl)phthalate ug/L 5.0 7.6 Di-n-octylphthalate ug/L 5.0 ND Benzo[b]fluoranthene ug/L 5.0 ND Benzo[k]fluoranthene ug/L 5.0 ND Benzo[a]pyrene ug/L 5.0 ND Indeno[1,2,3,-cd]pyrene ug/L 5.0 ND Dibenz[a,h]anthracene ug/L 5.0 ND Benzo[g,h,i]perylene ug/L 5.0 ND Surrogate - 2-Fluorophenol % 26 -- Surrogate - Phenol -d5 � Surrogate - Nitrobenzene -d5 % Surrogate - 2-Fluorobiphenyl Surrogate - 2,4,6-Tribromophenol % 172� 54 Ravenscroft Drive Asheville, NC 28801 TEL: 704-254-7176 rnV "inn XII A(I1 MAY 2 31995 r �I N C 0 R P 0 R A T E D THE ASSURANCE OF QUALITY Mr. Jerry McKinney Page 11 Client Reference: Coats American REPORT OF LABORATORY ANALYSIS PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter Units MDL ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS May 02, 1995 PACE Project Number: A504125, 93 0079539 04/11/95 04/11/95 K80L-11 Surrogate - Terphenyl-d14 % 66 VOLATILE ORGANICS Chloromethane ug/L 1.0 ND Bromomethane ug/L 1.0 ND Dichlorodifluoromethane ug/L 1.0 ND Chloroethene (Vinyl chloride) ug/L 1.0 ND Chloroethane ug/L 1.0 ND 1,1-Dichloroethene ug/L 1.0 ND Trichlorofluoromethane ug/L 1.0 ND Dichloromethane ug/L 1.0 ND trans-1,2-Dichloroethene ug/L 1.0 ND 1,1-Dichloroethane ug/L 1.0 ND 2,2-Dichloropropane ug/L 1.0 ND cis-1,2-Dichloroethene ug/L 1.0 ND Bromochloromethane ug/L 1.0 ND Chloroform ug/L 1.0 ND Dibromomethane ug/L 1.0 ND 1,1,1 -Trichloroethane ug/L 1.0 ND Carbon tetrachloride ug/L 1.0 ND 1,2-Dichloroethane ug/L 1.0 ND 1,1,2 -Trichloroethene ug/L 1.0 ND 1,1-Dichloro-l-propene ug/L 1.0 NO 1,2-Dichloropropane ug/L 1.0 ND Bromodichloromethane ug/L 1.0 ND trans-1,3-Dichloro-l-propene ug/L 1.0 ND cis-1,3-Dichloro-l-propene ug/L 1.0 ND 1,1,2 -Trichloroethane ug/L 1.0 ND 1, 3-Dichloropropane ug/L 1.0 ND Tetrachloroethene ug/L 1.0 ND ��i IM� �; Dibromochloromethane 1,1,1,2 ug/L 1.0 ND t, 199 -Tetrachloroethane ug/L 1.0 ND MAY r 54 Ravenscroft Drive ' An Asheville, NC 28801 TEL: 704-254-7176 LL rAv-'inn acs ario THE ASSURANCE OF OUALITY Mr. Jerry McKinney Page 12 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS REPORT OF LABORATORY ANALYSIS Units MDL May 02, 1995 PACE Project Number: A5041, 930079539 04/11/95 04/11/95 K80L-11 Bromoform ug/L 1.0 ND 1,2,3-Trichloropropane ug/L 1.0 ND 1,1,2,2 -Tetrachloroethane ug/L 1.0 ND Hexachlorobutadiene ug/L 1.0 ND Benzene ug/L 1.0 ND Toluene ug/L 1.0 ND Chlorobenzene ug/L 1.0 ND Ethylbenzene ug/L 1.0 ND Xylenes ug/L 1.0 ND Styrene ug/L 1.0 ND Isopropylbenzene ug/L 1.0 ND Bromobenzene • ug/L 1.0 ND n-Propylbenzene ug/L 1.0 ND 2-Chlorotoluene ug/L 1.0 ND 4-Chlorotoluene ug/L 1.0 ND 1,3,5-Trimethylbenzene ug/L 1.0 ND t-Butylbenzene ug/L 1.0 ND 1,2,4-Trimethylbenzene ug/L 1.0 ND 1,3 -Dichlorobenzene ug/L 1.0 ND s-Butylbenzene ug/L 1.0 ND 1,4 -Dichlorobenzene ug/L 1.0 ND 4-Isopropyltoluene ug/L 1.0 ND 1,2 -Dichlorobenzene ug/L 1.0 ND n-Butylbenzene ug/L 1.0 ND 1,2,4-Trichlorobenzene ug/L 1.0 ND Naphthalene ug/L 1.0 ND 1,2,3-Trichlorobenzene ug/L 1.0 ND 54 Ravenscroft Drive Asheville, NC 28801 TEL: 704-254-7176 rev. -,n. gra nr— I LI 31995 MAY 2 An Equa,.Opportunity Ert ployer rn W CD IG a 3 A CD cD o - r D r CD c m a(D 3 60 ;q r - o � y m 7 n O O a� 0 n O T. 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" m?O z 03 i CL C)zm w O� cm v( A D0 m� �(D cn a m O z SEMIVOLATILE ORGANICS REPORT - DEM LAB LAB NUMBER:4G-1:35 SUPERVISOR LAB #:4G-1:35 DATE 3 REPORTED BYg0a CHECKED BY ENTERED BY REVIEWED BY CHECKED BY -�+ SAMPLE TYPE, WATER DILUTION FACTOR CONC. CAS NUMBER TQL ANALYTE NAME UG%L X 1 108-95-2 10 PHENOL tT 111-44-4 10 BIS(2-CHLOROETHYL) ETHER U 95-57-8 10 2 -CHLOROPHENOL U 541-73-1 10 1,3 -DICHLOROBENZENE U 106-46-7 10 1,4 -DICHLOROBENZENE U 100-51-6 20 BENZYL ALCOHOL U 95-50-1 10 1,2 -DICHLOROBENZENE U 95-48-7 10 2 -METHYL PHENOL TJ 108-60-1 10 BIS(2-CHLOROISOPROPYL) ETHER U 106-44-5 10 4 -METHYL PHENOL U 621-64-7 10 N-NITROSO-DI-N-PROPYLAMINE U 67-72-1 10 HEXACHLOROETHANE TJ 98-95-:3 .10 NITROBENZENE U 78-59-1 10 ISOPHORONE U 88-75-5 10 2 -NITRO PHENOL U 105-67-9 10 2,4 -DIMETHYL PHENOL U 65-85-0 50 BENZOIC ACID TJ 111-91-1 10 BIS(2-CHLOROETHOXY) METHANE U 120-83-2 10 2,4-DICHLORO PHENOL U 120-82-1 10 1,2,4-TRICHLOROBENZENE U 91-20-:3 10 NAPHTHALENE U 106-47-8 20 4-CHLOROANILINE U 87-68-3 10 HEXACHLOROBUTAPIENE U 59-50-7 20 4 -CHLORO -3 -METHYL PHENOL U 91-57-6 10 2 -METHYL NAPHTHALENE U 77-47-4 10 HEXACHLOROCYCLOPENTADIENE U 88-06-2 10 2,4,6-TRICHLORO PHENOL U 95-95-4 10 2,4,5-TRICHLORO PHENOL U 91-58-7 10 2 -CHLORO NAPHTHALENE tr 88-74-4 50 2-NITROANALINE U 131-11-3 10 DIMETHYL PHTHALATE U 203-96-8 10ACENAPHTHYLENE U 606-20-2 10 2,6-DINITROTOLUENE U 99-09-2 50 3-NITROANALINE. U 83-32-9 10 ACENAPHTHENE U 51-28-5 50 2,4-DINITRO PHENOL -U 100-02-7 50 4 -NITRO PHENOL U 132-64-9 10 DIBENZOFURAN IJ 121-14-2 10 2,4-DINITROTOLUENE tT 84-66-2 10 DIETHYL PHTHALATE U 7005-72-3 10 4-CHLOROPHENYL PHENYL ETHER tT 2 ;- 73-7 10 FL UOR.ENE U 5:;4-52-"1 50 4, 6-DINITRO-2-METHYL PHENOL LT 86-30-6 10 N-NITROSODIPHENYLAMINE U 101-55-3 10 4-BROMOPHENYL PHENYL ETHER U 118-74-1 10 HEXACHLOROBENZENE U 87-86-5 50 PENTACHLORO PHENOL U 85-01-8 10 PHENANTHRENE U 120-12-7 10 ANTHRACENE U 84-74-2 10 DI -N -BUTYL PHTHALATE U 206-44-0 10 FLUORANTHENE U 129-00-0 10 PYRENE U 85-68-7 10 BUTYLBENZYL PHTHALATE U 91-94-1 20 3,31-DICHLOROBENZIDINE U 56-55-3 10 BENZO(A)ANTHRACENE U 218-01-9 10 CHRYSENE _U 117-81-7 10 BIS(2-ETHYLHEXYL) PHTHALATE U 117-84-0 10 DI-N-OCTYL PHTHALATE U 205-99-2 10 BENZO(B)FLUORANTHENE U 207-08-9 10 BENZO(K)FLUORANTHENE U 50-32-8 10 BENZO(A)PYRENE U 193-39-:5 10 INDEN6(1,2,3-CD)PYRENE U 53-70-3 10 DIBENZO(A,H)ANTHRACENE U 191-24-2 10 BENZO(G,H,I)PERYLENE U OTHER SEMIVOLATILE ORGANICS FOR SAMPLE NUMBER ; 4G-1:35 BUTOXYETHOXY ACETATE ETHANOL CIO.H2O,0 37 E TQL= TARGETQUANTITATION LIMIT T= TENTATIVELY IDENTIFIED ESTIMATED CONCENTRATION E= ESTIMATED CONCENTRATION U= COMPOUND ANALYZED FOR NOT DETECTED N= COMPOUND NOT ANALYZED FOR D= DETECTED BELOW QUANTITATION LIMIT H= HOLDING TIME EXCEEDED TQT SUBJECT TO CHANGE DUE TO INSTRUMENT SENSITIVITY EHNR/DEM LABORATORY VOLATILE ANALYTICAL REPORT was NO, 4G135 REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE: WATER SUPERVISOR DATE a ENTERED BY CHECKED BY ANALYSIS RESULTS CAS# VOA TARGET COMPOUND TQL DETECTED ug/l ug/l 75-35-4 1,1-Dichloroethene 0.75 U 75-09-2 Methylene Chloride 0.25 U 156-60-5 trans-1,2-Dichloroethene 0.75 U 75-34-3 1,1-Dichloroethane 0.25 U 590-20-7 2,2-Dichloropropane 0.25 U 156-59-4 cis-1,2-Dichloroethene 0.25 U 67-66-3 Chloroform 0.25 U 74-97-5 Bromochloromethane 0.75 U 71.55-6 1,1,1 -Trichloroethane 0.25 U 563-58-6 1,1-Dichloropropene 0.25 U 56-23-5 Carbon Tetrachloride 0.75 U 107-06-2 1,2-Dichloroethane 0.25 U 79-01-6 Trichloroethene 0.25 U 78-87-5 1,2-Dichloropropane 0.25 U 75-27-4 Bromodichloromethane 0.25 U -74-95-3 Dibromomethane 1 U 10061-01-5 cis-1,3-Dichloropropene 0.25 U 10061-02-6 trans-1,3-Dichloropropene 0.25 U 79-00-5 1,1,2 -Trichloroethane 0.25 U 127-18-4 Tetrachloroethene 0.25 U 142-28-9 1,3-Dichloropropane 0.25 U 124-48-1 Dibromochloromethane 0.75 U 106-93-4 1,2-Dibrozoethane 1 U 108-90-7 Chlorobenzene 0.25 U 630-20-6 1,1,1,2 -Tetrachloroethane 0.25 U 75-25-2 Bromoform 0.5 U 79-34-5 1,1,2,2 -Tetrachloroethane 0.75 U CAS# VOA TARGET COMPOUND TQL DETECTED ua/l ug/1 96-18-4 1,2,3-Trichloropropane 108-86-1 Bromobenzene 95-49-8 2-Chlorotoluene 106-43-4 4-Chlorotoluene 541-73-1 1,3 -Dichlorobenzene 106-46-7 1,4 -Dichlorobenzene 95-50-1 1,2 -Dichlorobenzene 96-12-8 1,2-Dibromo-3-Chloropropane 120-82-1 1,2,4-Trichlorobenzene 87-68-3 Hexachlorobutadiene 87-61-6 1,2,3-Trichlorobenzene 1634-04-4 Methyl -test -butyl ether 71-43-2 Benzene 108-88-3 Toluene 100-41-4 Ethyl benzene 108-38-3 m,p-Xylenes 95-47-6 o -Xylene 100-42-5 Styrene 98-82-8 Isopropylbenzene 103-65-1 n-Propylbenzene 108-67-8 1,3,5-Trimethylbenzene 98-06-6 tert-Butylbenzene , 95-63-6 1,2,4-Trimethylbenzene 135-98-8 sec-Butylbenzene 99-87-6 p-isopropyltoluene 104-51-8 n-Butylbenzene 91-20-3 Naphthalene 0.25 1 0.25 0.25 0.25 0.25 0.25 1 0.25 0.25 0.75 5 1 U U U U U U U U U U U U U 1 1.0 T 1 U 2 U l U 1 U 1 U 1 U 1 U 1 U 1 U 1 U l U I U i U TQL- Target Quantitation Limit Subject to Other purgeables detected Detected change due to instrument sensitivity (up to 10 highest peaks) ug/l T- Tentatively Identified, not confirmed E- Estimated Value U- Samples analyzed for this compound but not detected N- Sample not analyzed for this compound D Detected below quantitation limit M- GC/MS Analysis performed COMMENTS: D CD 0 C/ �N m I I cl I I I I I I I_e 33�3333333c3 cv cQ O cv cQ CO cc cv cn (Q_« cv c)63 3 3c ZKK;r, c ORO sv DsZZ �vcn ca ��= CD O O 0 0WE O^Z cn -0 3 Q-P.c 3.2 z_0 3WCDC: C: =3 0) cv3.3o. 3 30mm Z Z -v 7 r W 333333333333333 cc cQ cv cQ cv cv cv cc cc to ca cc cQ cv cv (Ao CDD : � Z r40 CD 'O" ' NrZ C/5 0CD0Avi c O (n Q (D CD C)C in O �� an CD =3 Q Tj \� cc cc cc 333cQ 1 � Q o cQ 3 � Zcu•�� su o sn C7 y 0 5 o (D O a = G 3 %.Z 59 3 4 7 -� cn --:0 -s- oW ' = Q a cQ cn m c� C: `�• ^' o 2 (D O 0 N ' Q R 0— (j m � C_• e w F �i 7a mO m m o A cFo o z m vgv0 -ZZ 0 p _u (n Y' �C, com C U c0 co CD 0 70 v CDCD -Ti -1) c m Q. Z v v �• s z b � c s = CC) d (j �i A z p _u (n Y' C U c0 0 v -Ti Q. —iC/)Cf) -0-1. ,�>0—I� z ��mc,mwmi C 0 R P 0 R A T L o REPORT OF LABORATORY ANALYSIS THE ASSURANCE Of UUAI.ITY Coats American P.O. Box 368 Hwy 221 N. Marian; NC 28652 Attn: Mr. Jerry McKinney Client Reference: Monitoring Wells PACE Sample Number: Date Collected: Date Received: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS IN WATER -METHOD 502.2 lr- --•tib f-� fir y L °.;� May 10, 1993 ND PACE Project Number: A3O42� Bromomethane E', 0.5 ND ND ND Dichlorodifluoromethane ug/L 0.5 ND 93 0028632 93 0028640 93 0028659 04/20/93 04/20/93 04/20/93 04/20/93 04/20/93 04/20/93 K8OL-2 K8OL-10 K8OL-I1 Units MDL Background Ash Pond Ash Pond Chloromethane ug/L 0.5 ND ND ND Bromomethane ug/L 0.5 ND ND ND Dichlorodifluoromethane ug/L 0.5 ND ND ND Vinyl chloride ug/L 0.5 ND ND ND Chloroethane ug/L 0.5 ND ND ND 1,1-Dichloroethylene ug/L 0.5 NO ND ND Trichlorofluoromethane ug/L 0.5 NO ND ND Methylene chloride ug/L 0.5 ND NO NO trans-1,2-Dichloroethylene ug/L 0.5 ND ND ND 1,1-Dichloroethane ug/L 0.5 ND ND ND 2,2-Dichloropropane ug/L 0.5 ND ND ND cis-1,2-Dichloroethylene ug/L 0.5 ND ND ND Bromochloromethane ug/L 0.5 ND ND ND Chloroform ug/L 0.5 2.1 0.55 ND Dibromomethane ug/L 0.5 ND ND ND 1,1,1 -Trichloroethane ug/L 0.5 0.6 ND NO Carbon tetrachloride ug/L 0.5 ND ND ND 1,2-Dichloroethane ug/L 0.5 ND ND ND 1,1,2 -Trichloroethylene ug/L 0.5 ND ND ND 1,1-Dichloro-l-propene ug/L 0.5 ND ND ND 1,2-Dichloropropane ug/L 0.5 ND ND ND Bromodichloromethane ug/L 0.5 ND NO ND 2-Chloroethylvinyl ether ug/L 0.5 ND ND ND trans-1,3-Dichloro-l-propene ug/L 0.5 NO ND ND cis-1,3-Dichloro-l-propene ug/L 0.5 ND ND ND 1;1,2 -Trichloroethane ug/L 0.5 ND ND ND 1,3-Dichloropropane ug/L 0.5 NO NO NO 1,1,2,2 -Tetrachloroethylene ug/L 0.5 ND ND NO 54 Ravenscroft Drive Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina An Equal Opportunity Employer Asheville, NC 28801 Tampa, Florida Asheville, North Carolina TEL: 704-254.7176 Iowa City, Iowa New York, New York FAX: 704252-4618 San Francisco, California Pittsburgh, Pennsylvania Kansas City, Missouri Denver, Colorado 1 Los Angeles, California REPORT OF LA ORATORY ANALYSIS -i C 0 R P 0 R A T E D THE ASSURANCE Of QUALITY Mr. Jerry McKinney Page 2 Client Reference: Monitoring Wells PACE Sample Number: Date Collected:. Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS May 10, 1993 PACE Project Number: A3042L 93 0028632 93 0028640 93 0028659 04/20/93 04/20/93 04/20/93 04/20/93 04/20/93 04/20/93 KBOL-2 K80L-10 K80L-11 Units MDL Background Ash Pond Ash Pond VOLATILE ORGANICS IN WATER -METHOD 502.2 Dibromochloromethane ug/L 0.5 ND ND ND 1,2-Dibromoethane ug/L 0.02 ND ND NO 1,1,1,2-1'etrachloroethane ug/L 0.2 ND - - 1,1,1,2 -Tetrachloroethane ug/L 0.5 - ND ND Bromoform ug/L 0.5 ND NO ND 1,2,3-Trichloropropane ug/L 0.5 ND ND ND 1,1,2,2 -Tetrachloroethane ug/L 0.5 ND ND ND 1,2-Dibromo-3-chloropropane ug/L 0.02 ND ND ND Hexachlorobutadiene ug/L 0.5 2.1 ND ND Methyl tert-butyl ether ug/L 0.5 ND ND ND Benzene ug/L 0.5 ND ND ND Toluene ug/L. 0.5 ND ND ND Chlorobenzene ug/L 0.5 ND ND ND Ethyl benzene ug/L 0.5 ND ND ND Xylenes ug/L 0.5 ND ND ND Styrene ug/L 0.5 ND ND ND Cumene ug/L 0.5 ND ND ND Bromobenzene ug/L 0.5 ND ND ND n-Propylbenzene ug/L 0.5 ND ND ND 0-Chlorotoluene ug/L 0.5 ND ND ND p-Chlorotoluene ug/L 0.5 ND ND ND 1,3,5-Trimethylbenzene ug/L 0.5 ND ND ND tert-Butylbenzene ug/L 0.5 ND ND ND 1,2,4-Trimethylbenzene ug/L 0.5 ND ND ND M -Dichlorobenzene ug/L 0.5 ND ND ND sec-Butylbenzene ug/L 0.5 ND ND ND 1,4 -Dichlorobenzene ug/L 0.5 ND ND ND p-Cymene ug/L 0.5 ND ND ND 0 -Dichlorobenzene ug/L 0.5 ND ND ND n-Butylbenzene ug/L 0.5 ND ND ND 1,2,4-Trichlorobenzene ug/L 0.5 ND ND ND 54 Ravenscroft Drive Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina An Equal Opportunity Employer Asheville, NC 28801 Tampa, Florida Asheville, North Carolina TEL: 704254-7176 Iowa City, Iowa New York, New York FAX: 704.252.4618 San Francisco, California Pittsburgh, Pennsylvania Kansas City, Missouri Denver, Colorado Los Anneles. California R_ P 0� T f o ' REPORT OF LABORATORY ANALYSIS', Mr. Jerry McKinney Page 3 Client Reference: Monitoring Wells May 10, 1993 PACE Project Number: A3042 PACE Sample Number: 93 0028632 93 0028640 93 0028659 Date Collected: 04/20/93 04/20/93 04/20/93 Date Received: 04/20/93 04/20/93 04-/20/93 Client Sample ID: K80L-2 K80L-10 K80L-11 Parameter Units MDL Background Ash Pond Ash Pond ORGANIC ANALYSIS VOLATILE ORGANICS IN WATER -METHOD 502.2 Napthalene ug/L 0.5 ND ND ND 1,2,3-Trichlorobenzene ug/L 0.5 ND ND ND These data have been reviewed and are approved for release. Waltir L. Miller Regional Director 54 Ravenscroft Drive Offices Serving: Minneapolis, Minnesota Charlotte; North Carolina An Equal Opportunity Employer Asheville, NC 28801 Tampa, Florida Asheville, North Carolina TEL: 704.254.7176 Iowa City, Iowa New York, New York FAX: 704-2524618 San Francisco, California Pittsburgh, Pennsylvania Kansas City, Missouri Denver, Colorado Los Angeles, California h-ac=T (22: a) I ��W(D0 C1 nCL(p ^o±?000 3 CDCD ZOO Nj O mm S30 CL 0 � Q- 50 c _� v z K o �- , m �,� ` �CL 33=3333333:33 c}OO 003 CQ Ca Q O CQ CO CO CQ CO CQa (O �0 a GO 3 3 (O o , to CD °DTz 3 ((n�m - -a3 a _ 3 z 3 ,Q :3 3.c3=cnw0) CD C: c33� N �.3 Z Z r 'Yt r Cli 3..3333333333333-3 0-(o(an(a aa(Q(a(acc(a( (a(a(a C C c CQ CQ CQ �-0N-0Z CD=3a' �. 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BOX 16387 209 WEST ANTRIM DRIVE GREENVILLE, SOUTH CAROLINA 29606-6387 CERTIFICATE OF ANALYSIS Sample ID No. 92-34-7612 *Priority Pollutant Volatiles EPA 8240 1,1,1 -Trichloroethane, ppb <2.00 1,1,2,2 -Tetrachloroethane, ppb <2.00 1,1,2 -Trichloroethane, ppb <2.00 1,1-Dichloroethane, ppb <2.00 1,1-Dichloroethylene, ppb <2.00 1,2 -Dichlorobenzene, ppb <2.00 1,2-Dichloroethane, ppb <2.00 1,2-Dichloropropane, ppb <2.00 1,2-trans-Dichloroethylene, ppb <2.00 1,3 -Dichlorobenzene, ppb <2.00 1,4 -Dichlorobenzene, ppb <2.00 2-Chloroethylvinyl ether, ppb <2.00 Acrolein, ppb <20.0 Acrylonitrile, ppb <20.0 Benzene, ppb <2.00 Bromoform, ppb <2.00 Carbon Tetrachloride, ppb <2.00 Chlorobenzene, ppb <2.00 Chlorodibromomethane, ppb <2.00 Chloroethane, ppb <2,00 Chloroform, ppb <2.00 Dichlorobromomethane, ppb <2.00 Dichlorodifluoromethane, ppb <2.00 Ethylbenzene,ppb <2.00 Methyl Bromide, ppb <2.00 Methyl Chloride, ppb <2,00 Methylene Chloride, ppb <2.00 Tetrachloroethylene, ppb <2.00 Toluene, ppb <2.00 Trichloroethylene, ppb <2.00 Trichlorofluoromethane, ppb <2.00 Vinyl chloride, ppb <2.00 cis-1,3-Dichloropropylene, ppb trans-1,3-Dichloropropylene Sample Markings e Location: K8 1i'= #7 ` Date: 12i/ 9 =i Time: 0 Collected by: Phi .ipcpi n Type sample: C3 South Carolina Lab Identification No. 23101^ North Carolina Certification No. 24 Outside Laboratory Certification No. 10120 9 AREA CODE 803 TELEPHONE: 271-3256 FAX: 803-235-8340 Date Analyst Time 1/6/93 JRU 1812 O 3 m 3 < ro W in N �TI O (D 0 o N. cnCDa �D c w CL _N N C CD7 m O n 0 CD3 -o CD; m a n 0 CDc o 0 w X, m O v 0 a CD 0 a, 0 cr r - O 3 m 3 < ro W in N �TI O (D 0 o N. cnCDa �D c w CL _N N C CD7 m O n 0 CD3 -o CD; m a n 0 CDc o 0 w X, m O v 0 a CD 0 a, 0 cr D tD X 0 2 O a CD O OC �Q�-0o r� ]J o a D O O d O DSOD n� Dv 3 0 G �n D ooW Z D cnrn �o �� o0 Z CD CD =r =r � r � rn, r 70 O m .0 Q " 3 (D Z -I O O a". o CD o m <r 0 (Nil 4 i Q 7Jcn0r-0 ID O 8 3 3. 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C Z c: W CD ca a `n & c pi I CD n Z w c W c 0 c' v a m m r c 0 m E v_ T 0 zo 0c m' z ' <� �o 0 Z - -m7 zz �30 a�:r Z.rrt M m m?0 a� ,) Z m 0� cm_ v �o aA 0 MR N m q 0 z k BHNR/DEM LABORATORY VOLATILE ANALYTICAL REPORT . �G 15fiI PORTED BY SUPERVISQR ECKED BY DATE Z ?� 'VIE'WED BY ENTERED BY X44- CHECKED BY 1PLS TYPE: WATER ANALYSIS RESULTS CAS# VOA TARGET COMPOUND TQL DETECTED CAStt VOA TARGET COMPOUND TQL DETECTED ua/l ua/I aa; l _ua,'1 75-35-4 1,1-Dichloroethene 0.15 U 95-18-4 1,2,3-Trichloropropane 0.25 75-09-2 Methylene chloride 0.25 U 108-86-1 Bromobenzene 1 156-60-5 trans-1,2-Dichloroethene 0.75 U 95-49-8 2-Chlorotoluene 0.25 75-34-3 1,1-Dichlorcethane 0.25 U 1106-43-4 4-Chlorotoluene 0.25 590-20-7 2,2-Dichloropropane 0.25 U 541-73-1 1,3 -Dichlorobenzene 0.25 156-59-4 cis-1,2-Dichloroethene 0.25 U 106-46-7 1,4 -Dichlorobenzene 0.25 67-66-3 Chloroform 0.25 U 95-50-1 1,2 -Dichlorobenzene 0.25 74-97-5 Bromochloromethane " 0.75 U 96-12-8 1,2-Dibromo-3-Chloropropane 1 71-55-6 1,1,1 -Trichloroethane 0.25 U 120-32-1 1,2,4-Trich1crobenzene 0.25 563-58-6 1,1-Dichloropropene 0.25 U - 87-68-3 Hexachlorobutadiene 0.25 56-23-5 Carbon Tetrachloride 0.75 U 87-61-6 1,2,3-Trichlorobenzene 0.15 107-06-2 1,2-Dichloroathane 0.25 U 1634-04-4 Methyl-tert-butyl ether 5 79-01-6 Trichloroethene 0.25 U 71-43-2 Benzene 1 78-87-5 1,2-Dichloropropane 0.25 U 108-88-3 Toluene 1 75-27-4 Bromodichloromethare 0.25 U 100-41-4 Ethyl benzene 1 74-95-3 Dibromomethane 1 U 108-38-3 m,p-Xylenes 1 u061-01-5 cis-1,3-Dichloropropene 0.25 U 95-47-6 o -Xylene 1 0061-02-6 trans-1,3-Dichloropropene 0.25 U 100-42-5 Styrene 1 79-00-5 1,1,2 -Trichloroethane 0.25 U 98-82-8 Isoprcpylbenzene 1 127-18-4 Tetrachloroethene 0.25 U 103-65-1 n-Propylyenzene 1 142-28-9 1,3-Dichloropropane 0.25 U 108-61-8 1,3,5-Trimethylbenzene 1 124-48-I Dibromochloromethane 0.75 U 98-06-6 tert-Butylbenzene 1 106-93-4 1,2-Dibromoethane 1 U 95-63-6 1,2,4-Trimethylbenzene 1 108-90-7 Chlorobenzene 0.25 U 135-98-8 sec-Butylbenzene 1 630-20-6 1,1,1,2 -Tetrachloroethane 0.25 U 99-87-6 p-isopropyltoluene 1 75-25-2 Bromoform 0.5 U 104-51-8 n-Butylbenzene L 79.34-5 1,1,2,2 -Tetrachloroethane 0.75 U 91-20-3 Naphthalene 1 TQL- Target Quantation Limit- Subject to Other purgeables detected change due to instrument sensitivity (up to 10 highest peaks) T- Tentatively Identified, not confirmed B- Estimated Value NO VOLATILE ORGANIC COMPOUNDS QUANTITATED U Samples analyzed for this compound but BY GC/PID. not detected N Sample not analyzed for this compound -D- Detected below quantitation limit M- GC/MS Analysis performed "MINTS: Detected ug/l U U U U U U U U ,U U U U U U U U U U U U U 0F1,a; SPL.0 COUNTY: MCDOWELL DATE SAMPLED *-Y-031-5-05 ALKALINITY,TO pH 4.5 ALKALINITY,TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM .5 '2 _ CARBONATE CHLORIDE CHROMIUM,TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS3 © 44-0 ® U0 FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM M BAS MAGNESIUM 40 / /6 MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN ORTHOPHOSPHATE pH `/ is . 3 y 6.3 / (v o yy I (o, °% PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE % % SULFATE / O /'?o 1-.J o TOC (UNFILTERED) S &I , , `k i 3 TOX TSS VOC n(U %Y ZINC STATIC WATER LEVEL /!, ' //,o /40 Red Ink=Sample taken by facility -WELL NO.: K80113 COATS AMERICAN COUNTY: MCDOWELL DATE SAMPLED ALKALINITY,TO pH 4.5 ALKALINITY,TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM 40 _ CARBONATE CHLORIDE //O Q `f //0 CHROMIUM,TOTAL ---//o COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS '�Fa2 D%�� 5 D h FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM MBAS MAGNESIUM 3 ` MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN ORTHOPHOSPHATE pH 6-3 PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE SULFATE TOC (UNFILTERED) 66 t .2 D -5- u TOX TSS VOC 44-6TACHEDZINC STATIC WATER LEVEL • /� !� • Y /a /�+. �• Red Ink=Sample taken by facility RESA M PLC DATE SAMPLED-�� -.3 aD-G,•c�� /�..,��-i7-off ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE `f IfD CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS FLUORIDE / 4-10 HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM DATE SAMPLED ±Lloo-3 MBAS ; MAGNESIUM,J3 MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN pH PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE SULFATE % o TOC (UNFILTERED) TOX TSS VOC v.Su ZINC STATIC WATER LEVEL, DATE SAMPLED ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM 3 CARBONATE CHLORIDE CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS 1.3 0 3 4- 0 b FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM Red Ink = Sample taken by facility WELL NO. COUNTY: I SOI C Q o W F—L L DATE SAMPLED f �G ,� fid° 9 i -�®, y9 /.C-/_3 I.? =`f r d- � 4-If-00 MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN pH PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIE CONDUCTANCE SULFATE cl z/ //0. r TOC (UNFILTERED)y TOX TSS VOC o' ZINC STATIC WATER LEVELa J o O , , j Q e �o / , !' D % / o `J % G% 0 Red Ink = Sample taken by facility DATE SAMPLED D`v�� _. `% /.7-/G ti°� `�_/ %�-!' % �� YY /a- %' 79 ALKALINITY, TO pH 4.5 ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE / % I ! 36 31 CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS 70 a-5-0 % 9 0 co I e o /0 FLUORIDE HARDNESS CaCo3 HARDNESS, NON CARB IRON LEAD LITHIUM Red Ink = Sample taken by facility WELL NO. K YO X / COUNTY: /�'l C D® WZ L L DATE SAMPLED �'� � Y7 1 -e6 -y% � -�f 9 ��1- q MBAS MAGNESIUM /7 MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN i PH d �. ra �. • r 7,0 G� PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE SULFATE / , O z— TOC (UNFILTERED) TOX TSS VOC ZINC STATIC WATER LEVEL 7, d 9,7 Red Ink = Sample taken by facility r 0 le%3 COUNTY M C 0 W 6 L Z- ' DATE SAMPLED ALKALINITY, TO pH 4.5 ALI<ALLINITY, TO pia 8. ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM 3-3- 30 CARBONATE CHLORIDE 4'7 1� CHROMIUM, TOTAL COBALT COD 1 COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANID DISSOLVED SOLIDS 0 Cj FLUORIDE HARDNESS CaCo HARDNESS, NON -CARBONATE IRON LEAD LITHIUM Red Ink = Sample taken by facility DATE SAMPLED MBAS MAGNESIUM at /7-0 T v� MANGANESE MERCURY NICKEL NITROGEN. AMMONIA NITROGEN, KJELDAHL NITRATE && NITRITE ORGANIC SCAN PH U 7.0 PHENOLS PHOSPHORUS. TOTAL POTASSIUM SELENIUM � O t�U�_ t. U . UU SILVER. SODIUl SPECIFIC CONDUCTANCE SULFATE TOC (UNFILTERED), 3 ! aZ TOX TSS IA VOC -TTA c 14 EO ZINC STATIC WATER LEVEL �° 5�� T / � . 5 %. � � � , � ` /0- `f DATE SAMPLED' ALhALINITY, TO pH 4.5 ALP.ALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM >C Y. CARBONATE CHLORIDE -:5-7 / /®Z CHROMIUM, TOTAL COBALT COD f �/ /171 % / 16, COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS _S O --310 -340 --3.5 V %0 3 3 o FLUORIDE HARDNESS CaCo, HARDNESS, NON -CARBONATE IRON LEAD LITHIUM DATE SAMPLED MBAS MAGNESIUM / 7 % 9 `� MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN � LCTriE FH 6 �•>�' PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM PCS �" .e 0 00-5, L Q. 0,9.5 AID t. SILVER SODIUM SPECIFIC CONDUCTANCE SULFATE % / I %% < TOC ( UNFILTERED) �� C s/• ,spa , Ja�, (� TOX TSS 7 'g `% 13 voc N4 IVd -51-60C r ZINC STATIC WATER LEVEL 9.9" /c). - ,0. o'. ✓ i couNTY MC DATE SAMPLED ALKALINITY, TO pH 4.5 f%� f ?- i l - �-?:�' _� oZ - /- 9 `�._ •! ALKALINITY, TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE c/ t% CHROMIUM, TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS !) -70 o FLUORIDE HARDNESS CaCo, HARDNESS, NON -CARBONATE IRON LEAD LITHIUM Red Ink = Sample taken by facility COUNTY /"/c DOWELL DATE SAMPLED //- / 7- 9�Z 3 "�? : !-3� _: 3 - / 9 y- MBAS MAGNESIUM �f. G �, { �• ��•d MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, P.JELDAHL NITRATE & NITRITE ORGANIC SCAN Ar--rrA -rrc-o srrE� PH �. of (o• '� � 6.1 �• % �aa 7' PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM O. 00 o' oc' 4 0. oo3- AID SILVER SODIUM SPECIFIC CONDUCTANCE SULFATE e J� �-5 `� �,/ 23 TOC (UNFILTERED) � -3, 6q 3 • ef LS TOX TSS 3 .3 vOc ,� 7' •7 A f �l�d s,r - Al ig7"P•Ac ¢f E® .,�6Ta',-�c�AE'ta ZINC GRj/I P//cc3sP Rc>5' STATIC WATER LEVEL S'��' ' / `� 7 ' lo : f /L M m 134 COUNTY DATE SAMPLED% -— Al .2 _ 3-_ 7 Voc -7:-- ®d 5(l 7-0 CV C s(,- -?a i COUNTY: —MCQ0WEI-1- DATE SAMPLED ®,�.•�� b' a a�-S - �i o�/�- J „-toCn-0G7AC7-4-0 02 0001,10 z—own CD cn ix ��OcaO D' Oo O.. w in z TI `i1 m y _ _ o . -� -n -- CD �O -w � O i 94 -� o� v CD j m � I � ! b ro O 33:r333333'3 663 ro s�cD 0toQ p(Qcnq�tp_=:Ps 3 3� a c ;r,-7 -n C)co>o-nzz tC] CQ CD G Q Sy W F�:j =r i ro �a O3 0C)t�A�-0-0 0 `�° cD 0�1 -a� M.3 0 0 Z co c CD .. � 3 C-0 � dN �wC� Q 3 3 �'' in CD E' W 0 m3 Sb cD z z cn z 4 1 d ❑. 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C) Z7 C -4 Z p, pz M M a� N f m m 00 0 m cn 1 _ c 14nalytical www.pacelabs.com Lab Sample No: 923592828 Client Sample ID: MW#13 GRAB #1667 Pace Analytical Sere, 2225 Riversi, Asheville, NC . Phone: 828.254.; Fax: 828.252.4t Lab Project Number: 9255106 Client Project ID: MONITORING WELLS Project Sample Number: 9255106.020 Date Collected: 12/03/03 09:25 Matrix: Water Date Received: 12/03/03 13:50 Parameters Results Units Report Limit Analyzed 11:42 By CAS No. Dual RegLmt GC Volatiles NO ug/l 0.50 12/06/03 11:42 STC 95.49.8 GC VOCs in Water Method: SM 6230D 0.50 12/06/03 11:42 STC 106-43.4 Benzene NO ug/l 0.50 12/06/03 11:42 STC 71.43-2 Bromobenzene NO ug/l 0.50 12/06/03 11:42 STC 108-86-1 Bromochloromethane ND ug/l 0.50 12/06/03 11:42 STC 74-97-5 Bromodichloromethane ND ug/l 0.50 12/06/03 11:42 STC 75-27.4 Bromoform ND ug/l 0.50 12/06/03 11:42 STC 75-25.2 Bromomethane ND ug/l 0.50 12/06/03 11:42 STC 74.83-9 n-Butylbenzene NO ug/l 1.0 12/06/03 11:42 STC 104-51-8 sec-Butylbenzene NO ug/l 0.50 12/06/03 11:42 STC 135-98-8 tert-Butylbenzene NO ug/l 0.50 12/06/03 11:42 STC 98.06-6 Carbon tetrachloride ND ug/l 0.50 12/06/03 11:42 STC 56.23-5 Chlorobenzene ND ug/l 0.50 12/06/03 11:42 STC 108.90.7 Chloroethane ND ug/l 0.50 12/06/03 11:42 STC 75-00-3 Chloroform ND ug/l 0.50 12/06/03 11:42 STC 67-66.3 Chloromethane ND ug/l 2.0 12/06/03 11:42 STC 74.87-3 2-Chlorotoluene NO ug/l 0.50 12/06/03 11:42 STC 95.49.8 4-Chlorotoluene NO ug/l 0.50 12/06/03 11:42 STC 106-43.4 1,2-Dibromo-3-chloropropane NO ug/l 2.0 12/06/03 11:42 STC 96-12-8 Dibromochloromethane NO ug/l 0.50 12/06/03 11:42 STC 124-48-1 1,2-Dibromoethane (EDB) NO ug/l 0.50 12/06/03 11:42 STC 106-93-4 Dibromomethane NO ug/l 0.50 12/06/03 11:42 STC 74-95-3 1,2 -Dichlorobenzene NO ug/l 1.0 12/06/03 11:42 STC 95-50.1 1,3 -Dichlorobenzene ND ug/l 1.0 12/06/03 11:42 STC 541.73-1 1,4 -Dichlorobenzene ND ug/l 1.0 12/06/03 11:42 STC 106.46-7 Dichlorodifluoromethane ND ug/l 0.50 12/06/03 11:42 STC 75.71.8 1,1-Dichloroethane ND ug/l 0.50 12/06/03 11:42 STC 75-34-3 1,2-Dichloroethane ND ug/l 0.50 12/06/03 11:42 STC 107.06-2 1,1-Dichloroethene ND ug/l 0.50 12/06/03 11:42 STC 75-35-4 cis-1,2-Dichloroethene ND ug/l 0.50 12/06/03 11:42 STC 156.59-2 trans-1,2-Dichloroethene NO ug/l 0.50 12/06/03 11:42 STC 156.60.5 1,2-Dichloropropane NO ug/l 0.50 12/06/03 11:42 STC 78-87-5 1,3-Dichloropropane NO ug/l 0.50 12/06/03 11:42 STC 142.28.9 2.2'-Dichloropropane NO ug/l 0.50 12/06/03 11:42 STC 594-20-7 1,1-Dichloropropene NO ug/l 0.50 12/06/03 11:42 STC 563.58.6 cis-1,3-Dichloropropene ND ug/l 0.50 12/06/03 11:42 STC 10061-01-5 trans-1,3-Dichloropropene ND ug/l 0.50 12/06/03 11:42 STC 10061-02.6 Diisopropyl ether ND ug/l 0.50 12/06/03 11:42 STC 108-20-3 Ethylbenzene ND ug/l 0.50 12/06/03 11:42 STC 100.41-4 Date: 12/17/03 REPORT OF LABORATORY ANALYSIS Page: 22 of 46 I til Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IN NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 N A��ago NC Drinking Water 37706 SC Environmental 99030- SC 99006 FL NELAP E87648 nefac = FL NELAP E87627 d Analytical www acelabs com Pace Analytical Seri, 2225 Rivers, Asheville, NC . Phone: 828.254. p Fax. 828.252.4L I Lab Project Number: 9255106 Client Project ID: MONITORING WELLS Lab Sample No: 923592828 Client Sample ID: MW#13 GRAB #1667 Project Sample Number: 9255106-020 Matrix: Water Date Collected: 12/03/03 09:25'•. Date Received: 12/03/03 13:50 Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt Hexachloro-1,3-butadiene NO ug/l 2.0 12/06/03 11:42 STC 87-68-3 Isopropylbenzene (Cumene) NO ug/l 0.50 12/06/03 11:42 STC 98-82.8 p-Isopropyltoluene NO ug/l 1.0 12/06/03 11:42 STC 99-87.6 Methylene chloride NO ug/l 2.0 12/06/03 11:42 STC 75-09-2 Methyl-tert-butyl ether NO ug/1 0.50 12/06/03 11:42 STC 1634-04.4 Naphthalene NO ug/l 2.0 12/06/03 11:42 STC 91.20.3 n-Propylbenzene NO ug/l 0.50 12/06/03 11:42 STC 103.65-1 Styrene ND ug/l 0.50 12/06/03 11:42 STC 100.42-5 1,1,1,2 -Tetrachloroethane NO ug/l 0.50 12/06/03 11:42 STC 630-20-6 1,1,2,2 -Tetrachloroethane NO ug/l 0.50 12/06/03 11:42 STC 79-34-5 Tetrachloroethene NO ug/l 0.50 12/06/03 11:42 STC 127-18-4 Toluene ND ug/l 0.50 12/06/03 11:42 STC 108-88-3 1,2,3-Trichlorobenzene ND ug/l 2.0 12/06/03 11:42 STC 87-61-6 1,2,4-Trichlorobenzene NO ug/1 2.0 12/06/03 11:42 STC 120-82-1 1,1,1 -Trichloroethane NO ug/l 0.50 12/06/03 11:42 STC 71.55-6 1,1,2 -Trichloroethane NO ug/l 0.50 12/06/03 11:42 STC 79-00-5 Trichloroethene NO ug/l 0.50 12/06/03 11:42 STC 79-01-6 Trichlorofluoromethane NO ug/l 0.50 12/06/03 11:42 STC 75-69.4 1,2,3-Trichloropropane NO ug/l 0.50 12/06/03 11:42 STC 96-18-4 1,2,4-Trimethylbenzene NO ug/l 0.50 12/06/03 11:42 STC 95-63-6 1.3,5-Trimethylbenzene NO ug/l 0.50 12/06/03 11:42 STC 108-67-8 Vinyl chloride NO ug/l 0.50 12/06/03 11:42 STC 75-01-4 m&p-Xylene NO ug/1 0.50 12/06/03 11:42 STC = o -X Y lene NO u /l 9 0.50 12/06/03 11:42 STC 95.47-6 n 1-Chloro-3-fluorobenzene (S) 99 12/06/03 11:42 STC 625-98-9 Tl rn Date: 12/17/03 REPORT OF LABORATORY ANALYSIS C --__...e_.,._ 5 Page: 23 of 46 Asheville Certification IN This report shall not be reproduced, except in full, Charlotte Certification ID NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 N aF'-FoA NC Drinking Water 37706 p �_�. �4ym SC Environmental 99030 Sc 99006 FL NELAP E87648 lac. FL NELAP E87627 -n -o -n ,1 o -0 C :7 0 0 2 • 0 0 0 0 ;p' m W CD m 0^ r) v n oD� CD 5- hoc o ? � =5 E H •c � � D� CD CD (D m m" 3 3 Im 0 3 o Q� _CD Q0 m =� � L _cn m zT�Z`'. 3 0 �y z m y. 'o fy o `_ m 0. 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Fax: 828.252.461 t. Lab Project Number: 9249663 Client Project ID: MONITORING WELL ANALYSIS Project Sample Number: 9249663-002 Matrix: Water Date Collected: 08/26/03 08:15 Date Received: 08/26/03 13:08 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs Results Units Report Limit Analyzed By CAS No. Qual Reg 12 Parameters 37712 ,N a oRo NC Drinking Water 37706 SC Environmental 99030a la c GC Volatiles 99006 FL NELAP E87648 ? nelac = FL NELAP E87627 GC VOCs in Water Method: SM 6230D ND ug/l 0.50 08/30/03 21:58 STC 71-43-2 Benzene ND ug/l 0.50 08/30/0321:58 STC 108-86-1 Bromobenzene ND ug/l 0.50 08/30/03 21:58 STC 74-97.5 Bromochloromethane Bromodichloromethane ND ug/l 0.50 08/30/03 21:58 STC 75-27-4 Bromoform NO ug/l 0.50 08/30/03 21:58 STC 75-25.2 Bromomethane NO ug/l 0.50 08/30/03 21:58 STC 74-83-9 n-Butylbenzene NO ug/l 1.0 08/30/03 21:58 STC 104-51-8 sec-Butylbenzene NO ug/l 0.50 08/30/03 21:58 STC 135-98.8 tert-Butylbenzene NO ug/1 0.50 08/30/03 21:58 STC 98-06.6 Carbon tetrachloride NO ug/l 0.50 08/30/03 21:58 STC 56-23.5 Chlorobenzene ND ug/1 0.50 08/30/03 21:58 STC 108-90-7 Chloroethane ND ug/l 0.50 08/30/03 21:58 STC 75-00-3 Chloroform ND ug/l 0.50 08/30/03 21:58 STC 67-66-3 Chloromethane ND ug/l 2.0 08/30/03 21:58 STC 74.87-3 2-Chlorotoluene ND ug/l 0.50 08/30/03 21:58 STC 95.49-8 4-Chlorotoluene NO ug/l 0.50 08/30/03 21:58 STC 106.43-4 1,2-Dibromo-3-chloropropane NO ug/l 2.0 08/30/03 21:58 STC 96.12-8Dibromochloromethane ND ug/l 0.50 08/30/03 21:58 STC 124.48-1 i2m (EDB) NO ug/l 0.50 08/30/03 21:58 STC 106-93-4 Cn1,2-Dibromoethane Dibromomethane NO ug/l 0.50 08/30/03 21:58 STC 74-95.3�1,2 Dichlorobenzene ND ug/l 1.0 08/30/03 21:58 STC 95 -50 -11,3 -Dichlorobenzene NO ug/l 1.0 08/30/03 21:58 STC 541-73-1 orb 1,4 -Dichlorobenzene. NO ug/l 1.0 08/30/03 21:58 STC 106-46.7 Dichlorodifluoromethane NO ug/1 0.50 08/30/03 21:58 STC 75-71.8 n==� 10::21 1,1-Dichloroethane ND ug/l 0.50 08/30/03 21:58 STC 75-34-3 "� "- 1,2 Dichloroethane NO ug/1 0.50 08/30/03 21:58 STC 07-06-2 15-35-4 -----� 1,1-Dichloroethene NO ug/l 0.50 08/30/03 21:58 STC 75 35 4 cis-1,2-Dichloroethene ND ug/l 0.50 08/30/03 21:58 STC 156-59-2 trans-1,2.-Dichloroethene ND ug/l 0.50 08/30/03 21:58 STC 156-60.5 1,2-Dichloropropane ND ug/l 0.50 08/30/03 21:58 STC 78-87-5 1,3-Dichloropropane NO ug/l 0.50 08/30/03 21:58 STC 142-28-9 2,2-Dichloropropane NO ug/l 0.50 08/30/03 21:58 STC 594-20-7 1,1-Dichloropropene NO ug/l 0.50 08/30/03 21:58 STC 563-58.6 cis-1,3-Dichloropropene NO ug/l 0.50 08/30/03 21:58 STC 10061.01-5 trans-1,3-Dichloropropene ND ug/l 0.50 08/30/03 21:58 STC 10061-02-6 Diisopropyl ether ND ug/l 0.50 08/30/03 21:58 STC 108-20-3 Ethylbenzene ND ug/l 0.50 08/30/03 21:58 STC 100-41-4 _ - Page: 3 of 14 Date: 09/03/03 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12 NC Drinking Water 37712 ,N a oRo NC Drinking Water 37706 SC Environmental 99030a la c SC 99006 FL NELAP E87648 ? nelac = FL NELAP E87627 Pace Analytical ServiCL 2225 RiversidE.. ., Nnalytical ' Asheville, NC 2c Phone: 828.254.77, www.pacelabs.com Fax: 828.252.461, Lab Project Number: 9249663 Client Project ID: MONITORING WELL ANALYSIS Lab Sample No: 923280259 Client Sample ID: MW #13 GRAB #1557 Project Sample Number: 9249663-002 Date Collected: 08/26/03 08:15 Matrix: Water Date Received: 08/26/03 13:08 ParametersResults NO Units Report Limit Analyzed 21:58 By CAS No. Qual RegLmt Hexachloro-1,3-butadiene NO ug/1 2.0 08/30/03 21:58 STC 87-68-3 Isopropylbenzene (Cumene) NO ug/l 0.50 08/30/03 21:58 STC 98-82-8 p-Isopropyltoluene ND ug/l 1.0 08/30/03 21:58 STC 99-87-6 Methylene chloride NO ug/1 2.0 08/30/03 21:58 STC 75-09.2 Methyl-tert-butyl ether ND ug/l 0.50 08/30/03 21:58 STC 1634-04-4 Naphthalene NO ug/l 2.0 08/30/03 21:58 STC 91-20-3 n•Propylbenzene NO ug/1 0.50 08/30/03 21:58 STC 103-65-1 Styrene NO ug/l 0.50 08/30/03 21:58 STC 100-42-5 1,1,1,2 -Tetrachloroethane NO ug/l 0.50 08/30/03 21:58 STC 630-20-6 1,1,2,2 -Tetrachloroethane NO ug/l 0.50 08/30/03 21:58 STC 79-34-5 Tetrachloroethene ND ug/l 0.50 08/30/03 21:58 STC 127-18-4 Toluene NO ug/l 0.50 08/30/03 21:58 STC 108-88-3 1,2,3-Trichlorobenzene NO ug/1 2.0 08/30/03 21:58 STC 87-61-6 1,2,4-Trichlorobenzene ND ug/l 2.0 08/30/03 21:58 STC 120.82-1 1,1,1 -Trichloroethane NO ug/l 0.50 08/30/03 21:58 STC 71-55-6 1,1,2 -Trichloroethane ND ug/1 0.50 08/30/03 21:58 STC 791-00-5 Trichloroethene NO ug/l 0.50 08/30/03 21:58 STC 79-01.6 Trichlorofluoromethane ND ug /1 0.50 08/30/03 21:58 STC 75-69.4 1,2,3-Trichloropropane NO ug/l 0.50 08/30/03 21:58 STC 96-18-4 1,2,4-Trimethylbenzene NO ug/l 0.50 08/30/03 21:58 STC 95-63-6 1,3,5-Trimethylbenzene NO ug/l 0.50 08/30/03 21:58 STC 108-67-8 Vinyl chloride NO ug/l 0.50 08/30/03 21:58 STC 75-01-4 m&p-Xylene NO ug/l 0.50 08/30/03 21:58 STC o -Xylene ND ug/l 0.50 08/30/03 21:58 STC 95-47.6 1-Chloro-3-fluorobenzene (S) 96 % 08/30/03 21:58 STC 625-98-9 Date: 09/03/03 REPORT OF LABORATORY ANALYSIS Asheville Certification IDs This report shall not be reproduced, except in full, NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. 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P m 'a_ -<� o C: Q 3 v CD o CL CLd 0 a, o A o 0 0 a a n 1Z �, 0 N ('� -; C7 �'' o a d ro w ,i a S 11 VII of n;�. D,,0. o IR, zC 15 1 t`, L e i (j o O Qco V O c3333 ca ce.cP o 9Prg U FE Q E JAN aceAnalytical TM wvnv.pace/abs.COm GROUNDWATER SECTION ASHEVILLE REGIONAL ONICE Lab Sample No: 931415749 Client Sample ID: MW #13 GRAB #1162 Pece AntlrflaI S#rvlee, 9800 Kincey AY6U. Sur, tAr&sWfie, NC 2� Phone: 704 875 Far 704.8759909. Lab Project Number: 9239125 Client Project ID: Coats American 9334729 Project Sample Number: 9239125-010 Date Collected: 12/03/02 09:15 Matrix: Water Date Received: 12/03/02 11:44 Page: 14 of 29 Date: 12/13/02 t a6oMw Certi$gtt4[11Di Laboratory• ai atioa IDs REPORT OF LABORATORY ANALYSIS ICY Drinking water 90090 NC Wastewater 12VA Drinking Water 213 NC Drinking Water 3770fi This report shall not be reproduced, except fuN, E87627 SC 99006 without the written consent of Pace Analytical Servkes. Inc. FL NELAP Results units Report Limit DF Analyzed By CAS No. Qual ReaLmt Parameters GC Volatiles GC VOCs in Water Method: SM 6230D ND ug/1 0.50 1.0 12/12/02 04:46 STC 71-43-2 Benzene ND ug/l 0.50 1.0 12/12/02 04:46 STC 108-86-1- Bromobenzene ND ug/1 0.50 1.0 12/12/02 04:46 STC 74-97-5 Bromochloromethane ND ug/l 0.50 1.0 12/12/02 04:46 STC 75-27-4 Bromodichloromethane ND ug/l 0.50 1.0 12/12/02 04:46 STC 75-25-2 Bromoform ND ug/1 0.50 1.0 12/12/02 04:46 STC 74-83-9 Bromomethane ND ug/l 1.0 1.0 12/12/02 04:46 STC 104-51-8 n-Butylbenzene ND ug/1 0.50 1.0 12/12/02 04:46 STC 135-98-8 sec-Butylbenzene ND ug/1 0.50 1.0 12/12/02 04:46 STC 98-06-6 tert-Butylbenzene ND ug/l 0.50 1.0 12/12/02 04:46 STC 56-23-5 Carbon tetrachloride ND ug/l 0.50 1.0 12/12/02 04:46 STC 108-90-7 Chlorobenzene ND ug/1 0.50 1.0 12/12/02 04:46 STC 75-00-3 Chloroethane ND ug/l 0.50 1.0 12/12/02 04:46 STC 67-66-3 Chloroform ND ug/1 2.0 1.0 12/12/02 04:46 STC 74-87-3 Chloromethane ND ug/l 0.50 1.0 12/12/02 04:46 STC 95-49-8 2-Chlorotoluene ND ug/1 0.50 1.0 12/12/02 04:46 STC 106-43-4 4-Chlorotoluene ND ug/1 2.0 1.0 12/12/02 04:46 STC 96-12-8 1,2-Dibromo-3-chloropropane ug/l 0.50 1.0 12/12/02 04:46 STC 124-48-1 Dibromochloromethane ND ND ug/1 0.50 1.0 12/12/02 04:46 STC 106-93-4 1,2-Dibromoethane (EDB) ND ug/l 0.50 1.0 12/12/02 04:46 STC 74-95-3 Dibromomethane ND ug/1 1.0 1.0 12/12/02 04:46 STC 95-50-1 1,2 -Dichlorobenzene ug/1 1.0 1.0 12/12/02 04:46 STC 541-73-1 1,3 -Dichlorobenzene ND ND ug/1 1.0 1.0 12/12/02 04:46 STC 106-46-7 1,4 -Dichlorobenzene ug/1 0.50 1.0 12/12/02 04:46 STC 75-71-8 Dichlorodifluoromethane ND ug/1 0.50 1.0 12/12/02 04:46 STC 75-34-3 1,1-Dichloroethane ND ND ug/1 0.50 1.0 12/12/02 04:46 STC 107-06-2 1,2-Dichloroethane ug/l 0.50 1.0 12/12/02 04:46 STC 75-35-4 1,1-Dichloroethene ND ug/l 0.50 1.0 12/12/02 04:46 STC 156-59-2 cis-1,2-Dichloroethene ND ND ug/1 0.50 1.0 12/12/02 04:46 STC 156-60-5 trars-1,2-Dichloroethene ND ug/l 0.50 1.0 12/12/02 04:46 STC 78-87-5 1,2-Dichloropropene ND ug/l 0.50 1.0 12/12/02 04:46 STC 142-28-9 1,3-Dich'_oropropane ND ug/1 0.50 1.0 12/12/02 04:46 STC 594-20-7 2,2-Dichloropropane ug/1 0.50 1.0 12/12/02 04:46 STC 563-58-6 1,1-Dichloropropene ND ND ug/1 0.50 1.0 12/12/02 04:46 STC 10061-01-5 cis-1,3-Dichloropropene ug/l 0.50 1.0 12/12/02 04:46 STC 10061-02-6 trans-1,3-Dichloropropene ND ug/1 0.50 1.0 12/12/02 04:46 STC 108-20-3 Diisopropyl ether ND ug/l 0.50 1.0 12/12/02 04:46 STC 100-41-4 Ethylhenzene ND Page: 14 of 29 Date: 12/13/02 t a6oMw Certi$gtt4[11Di Laboratory• ai atioa IDs REPORT OF LABORATORY ANALYSIS ICY Drinking water 90090 NC Wastewater 12VA Drinking Water 213 NC Drinking Water 3770fi This report shall not be reproduced, except fuN, E87627 SC 99006 without the written consent of Pace Analytical Servkes. Inc. FL NELAP v • vnv. cs.com � ,,��, �`� tr aceAnal ical 1 � Lab Sample No: 931415749 Client Sarple ID: MW #13 GRAB #1162 VI E OROUNDWA�E SEGTON, ASHEVILLE RE(7i0NAL OFFICE �l Pace Matyt/d' Service 9800 KZWAvenue, Sur,. tirgmille, NC 26 Phone: 704.875.90., fax 704.8759091 1 Lab Project Number: 9239125 Client Project ID: Coats American 9334729 Project Sample Number: 9239125-010 Date Collected: 12/03/02 09:15 Matrix: Water Date Received: 12/03/02 11:44 Page: 15 of 29 Data: 12/13/02 I abofatory Certification II?s I aboratory erti,icatfon los REPORT OF LABORATORY AN KY Drinking Water 90090 NC Wastewater 12 This report strall not be reproduced, except in full, VA Drinking Water 213 NC Drinking Water 37706 E87627 Sc 99006 without the written consent of Pace Analytical Servkes, Inc. FL NEIAP Results Units Report Limit DF Analyzed By CAS No. Qual ReaLmt Parameters ug/1 2.0 1.0 12/12/02 04:46 STC 87-68-3 Bexachloro-1,3-butadiene ND ug/1 0.50 1.0 12/12/02 04:46 STC 98-82-8 Isopropylbenzene (Cumene) ND ND ug/l 1.0 1.0 12/12/02 04:46 STC 99-87-6 p-Isopropyltoluene ug/1 2.0 1.0 12/12/02 04:46 STC 75-09-2 Methylene chloride ND ug/l 0.50 1.0 12/12/02 04:46 STC 1634-04-4 Meth ert-butyl ether y„ ND 2.0 1.0 12/12/02 04:46 STC 91-20-3 Naphthalene NDug/l ug/l 0.50 1.0 12/12/02 04:46 STC 103-65-1 n-propylbenzene ND ug/l 0.50 1.0 12/12/02 04:46 STC 100-42-5 Styrene ND ug/1 0.50 1.0 12/12/02 04:46 STC 630-20-6 � Tetrachloroethane 1,1,1,.. ND ug/1 0.50 1.0 12/12/02 04:46 STC 79-34-5 1,1,2,2 -Tetrachloroethane ND ug/1 0.50 1.0 12/12/02 04:46 STC 127-18-4 Tetrachloroethene ND' ug/l 0.50 1.0 12/12/02 04:46 STC 108-88-3 Toluene ND ug/1 2.0 1.0 12/2/02 04:46 STC 87-61-6 1,2,3-Trichlorobenzene ND ug/l 2.0 1.0 12/12/02 04:46 STC 120-82-1 1,2,4-Trichlorobenzene ND ug/l 0.50 1.0 12/12/02 04:46 STC 71-55-6 1,1,1 -Trichloroethane ND ug/1 0.50 1.0 12/12/02 04:46 STC 79-00-5 1,1,2 -Trichloroethane ND ug/l 0.50 1.0 12/12/02 04:4 6 STC 79-01-6 Trichloroethene ND ug/1 0.5.0 1.0 12/12/02 04:96 STC 75-69-4 methane Trichlorofluoromethane ND ug/l 0.50 1.0 12/12/02 04:46 STC 96-18-4 ND ug/l 0.50 1.0 12/12/02 04:46 STC 95-63-6 1,2,4- rimethylbenzene ND ug/l 0.50 1.0 12/12/02 04:46 STC 108-67-8 1,3,5-Trimethylbenzene ND u g/ 1 0.50 1.0 12/12/02 04:46 STC 75-01-4 Viny`_ c'_oride ND ug/1 0.50 1.0 12/12/02 04:46 STC m&p-Xylene ND ug/1 0.50 1.0 12/12/02 04:46 STC 95-47-6 o -Xylene � 1.0 12/12/02 04:46 STC 625-98-9 1-Chloro-3-fluorobenzene (S) 127 Page: 15 of 29 Data: 12/13/02 I abofatory Certification II?s I aboratory erti,icatfon los REPORT OF LABORATORY AN KY Drinking Water 90090 NC Wastewater 12 This report strall not be reproduced, except in full, VA Drinking Water 213 NC Drinking Water 37706 E87627 Sc 99006 without the written consent of Pace Analytical Servkes, Inc. 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C.. .. �,,. z Z mmm m 0 m� Ez 0 bm n 0 m M D m m(—"( :5J,O m2m mu:5 Z O M mZO mea C -i Z Qp Z v-4 is mm m M o N 00i m m o m -� tJ p �p N T 3' � CD $ m m rT Q �{ >_ o � 0 o 3 © jj{ X � G Q to I :2D o M I� C: 3 o Z > O z i1 a m 0 9 0b z z m M D m m(—"( :5J,O m2m mu:5 Z O M mZO mea C -i Z Qp Z v-4 is mm m M o N 00i m m -dc6Ana1yVcaf` uwsvr.lk-rt�tRSs:corn q s Pace Analytical Services, Inc: 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone.- 704.875.9092 Fax. 704.875.9091 -- -� Lab Project Number: 9235982 Client Project ID: Coats American 9332033 Lab Sample No: 931318711 Project Sample Number 9235982-001 Date Collected: 08/27/02 07:45 Client Sample ID: MW #13 GRAB #1012 Matrix: Water Date Received: 08/27/02 12:55 ParameCere Results Units Report Limit DF Analyzed BY CAS No. Oual Re Lm GC Volaftl©$ -- GC VOCs in Water Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tent-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2 -Dichlorobenzene 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans -1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Date: 09/05/02 Method: SM 6230D ND ug/1 ND ug/1 ND ug/1 ND ug/l ND ug/l ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 ND ug/1 0.50 1.0 09/05/02 00:08 STC 71-43-2 0.50 1.0 09/05/02 00:08 STC 108-86-1 0.50 1.0 09/05/02 00:08 STC 74-97-5 0.50 1.0 09/05/02 00:08 STC 75-27-4 0.50 1.0 09/05/02 00:08 STC 75-25-2 0.50 1.0 09/05/02 00:08 STC 74-83-9 1.0 1.0 09/05/02 00:08 STC 104-51-8 0.50 1.0 09/05/02 00:08 STC 135-98-8 0.50 1.0 09/05/02 00:08 STC 98-06-6 0.50 1.0 09/05/02 00:08 STC 56-23-5 0.50 1.0 09/05/02 00:08 STC 108-90-7 0.50 1.0 09/05/02 00:08 STC 75-00-3 0.50 1.0 09/05/0200:08 STC 67-66-3 2.0 1.0 09/05/02 00:08 STC 74-87-3 0.50 1.0 09/05/02 00:08 STC 95-49-8 0.50 1.0 09/05/02 00:08 STC 106-43-4 2.0 1.0 09/05/02 00:08 STC 96-12-8 0.50 1.0 09/05/02 00:08 STC 124-48-1 0.50 1.0 09/05/02 00:08 STC 106-93-4 0.50 1.0 09/05/02 00:08 STC 74-95-3 1.0 1.0 09/05/02 00:08 STC 95-50-1 1.0 1.0 09/05/02 00:08 STC 541-73-1 1.0 1.0 09/05/02 00:08 STC 106-46-7 0.50 ., 1.0 09/05/02 00:08 STC 75-71-8 0.50 1.0 09/05/02 00:08 STC 75-34-3 0.50 1.0 09/05/02 00:08 STC 107-06-2 0.50 1.0 09/05/02 00:08 STC 75-35-4 0.50 1.0 09/05/02 00:08 STC 156-59-2 0.50 1.0 09/05/02 00:08 STC 156-60-5 0.50 1..0 09/05/02 00:08 STC 78-87-5 0.50 1.0 09/05/02 00:08 STC 142-28-9 0.50 1.0 09/05/02 00:08 STC 594-20-7 0.50 1.0 09/05/02 00:08 STC 563-58-6 0.50 1.0 09/05/02 00:08 STC 10061-01-5 0.50 1.0109/05/02 00:08 STC 10061-02-6 0.50 1.0 09/05/02 00:08 STC 108-20-3 0.50 1.0 09/05/02 00:08 STC 100-41-4 i ahDratDry fortification IDS REPORT OF LABORATORY ANALYSIS NC Wastewater 12 NC Drinking Water 37706 This report shall not be reproduced, except in full, Sc 99006 without the written consent of Pace Analytical Services, Inc. KY Drinking Water 90090 VA Drinking Water 213 FL NELAP E87627 Lab Sample No: 931318711 Client Sample ID: MW #13 GRAB #1012 ` Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Phone: 704.875.9092 Far: 704.875.9091 Lab Project Number: 9235982 Client Project ID: Coats American 9332033 Project Sample Number: 9235982-001 Date Collected: U8/27/UZ U7:flb Matrix: Water Date Received: 08/27/02 12:55 Parameters �/ Results Units Report Limit DF Analyzed By CAS No. ual Re Lm Hexachloro-1,3-butadiene ND ug/1 2.0 1.0 09/05/02 00:08 STC 87-68-3 Isopropylbenzene (Cumene) ND ug/l 0.50 1.0 09/05/02 00108 STC 98-82-8 p-isopropyltoluene ND ug/1 1.0 1.0 09/05/02 00:08 STC 99-87-6 Methylene chloride ND ug/l 2.0 1.0 09/05/02 00:08 STC 75-09-2 Methyl-tert-butyl ether ND ug/1 0.50 1.0 09/05/02 00:08 STC 1634-04-4 Naphthalene ND ug/l 2.0 1.0 09/05/02 00:08 STC 91-20-3 n-Propylbenzene ND ug/l 0.50 1.0 09/05/02 00:08 STC 103-65-1 ND ug/1 0.50 1.0 09/05/02 00:08 STC 100-42-5 Styrene 1,1,1,2 -Tetrachloroethane ND ug/1 0.50 1.0 09/05/02 00:08 STC 630-20-6 1,1,2,2 -Tetrachloroethane ND ug/1 0.50 1.0 09/05/02 00:08 STC 79-34-5 Tetrachloroethene ND ug/1 0.50 1.0 09/05/02 00:08 STC 127-18-4 ND ug/l 0.50 1.0 09/05/02 00:08 STC 108-88-3 Toluene 1,2,3-Trichlorobenzene ND ug/1 2.0 1.0 09/05/02 00:08 STC 87-61-6 1,2,4-Trichlorobenzene ND ug/l 2.0 1.0 09/05/02 00:08 STC 120-82.1 1,1,1 -Trichloroethane ND ug/l 0.50 1.0 09/05/02 00:08 STC 71-55-6 1,1,2 -Trichloroethane ND ug/l 0.50 1.0 09/05/02 00:08 STC 79-00-5 Trichloroethene ND ug/l 0.50 1.0 09/05/02 00:08 STC 79-01-6 Trichlorofluoromethane ND ug/1 0.50 1.0 09/05/02 00:08 STC 75-69-4 1,2,3-Trichloropropane ND ug/l 0.50 1.0 09/05/02 00:08 STC 96-18-4 1,2,4-Trimethylbenzene ND ug/l 0.50 1.0 09/05/02 00:08 STC 95-63-6 1,3,5-Trimethylbenzene ND ug/l 0.50 1.0 09/05/02 00:08 STC 108-67-8 vinyl chloride ND ug/l 0.50 1.0 09/05/02 00:08 STC 75-01-4 m&p-Xylene ND ug/1 0.50 1.0 09/05/02 00:08 STC ND ug/l 0.50 1.0 09/05/02 00:08 STC 95-47-6 o -Xylene (S) 98 % 1.0 09/05/02 00:08 STC 625-98-9 1-Chloro-3-fluorobenzene Date: 09/05/02 SEP 2 3 2002 I �. GROUNDWATER SECTION '' ASHEVILLE REGIONAL OFFICE I ahorato Certification IDst ahoratory Certification I Ds NC Wastewater ,z REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090 NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213 Sc 99006 without the written consent of Pace AnaVical Services, Inc. FL NELAP E87627 Page: 2 IC 0> N 'U Z 3 :3 3 ' -� C) CD 5. no 0 3 m C z 3 Q OL In At 7 L1 O 3 n CD 0 0 c3333 o2 000 ,moo -ac=r ::0M ooO> o Zo C7^ 0 W �. * a do b cn30cnc�m C rnm ° 33 � 3 oa o �z -n m I _ ml � --i- N CA O n tv : CD Q Q- —€ e � — n CD r ' p ' a_ — � O'DO .{ t � w 3 >v � R !? fQ Q Cl 3ca 3c 3oc3 3 S 3 oc3 10 pc _zcn n`�0 a�z=`e 3 3qz sL c ,(o(Dc=rCLSDw ::� ;n 0 K� O3 C?C3rn�� CO m n O C CD o ill At sv 7 r 3.c' coot �D CD��Co Io -to3 �_� E' 33..w�.M CD sn cn ( azz m z' O O 9� W a 333333333333333a cca ccs ccs co � u� co cca cs� cc cn ccs cn cso cn a, c. 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Praject IdeWird as Coats.Amerlcan, collected 05 December 2001) 1. volatile Organics Detecobn EPA Method 62301) t4wits tAW-X3 I,1-l�ichlotucthane OAO! 2,2-T3ichloropropane 0.001 Chlorafotm 0.001 1,1,1 -Trichloroethane 0.001 1,1-ptcblorOpropene 0-001 - Carbon Tetrachloride 0,001 Btnme 0,001 1,2-Diohloroethw 0.001 Trichlorocttletle O.00I 1,2-Dicblorepropene 0.001 Dibromomediane 0.001 Toluene 0.001 1,1,2-Trlrhlaroctltatte Q.QO1 1,3,Dlohloropmpane 0.001 Tetrachlorcetheme O.00I l,E,1,2-TetraohloCacthana 0.001 1,1,2,24caacb1orcethana 0 001 1,2,11-Trichlompropane 0.001 Flexublotobutadiene 0.001 Brot116beAzene 0-001 Ethylbenzcne 0-00) Styrene 1 0-001 Bromofatrn 0-001 p-ienpropyltoluene 0.001 N-Butylbenzene 01001 Naphthalene 0.001 1,3,5-Wmathylbenwna 0,001 1,2,4-Trimotby1be=ne 0.001 1,2,4 -Tri 40orobettzeoe 0.001 I "-Ttitehlombemene 0.001 Clikrobenzene 0.001 2-Chlorotoluene 0.00) 4-Cblorotoluene 0.001 Tert-Butylbenzene 0.001 5ce-)3utylban4onc 0.001, 1,3 -,Dichlorobenzene 0.001 1,2-Dicl4orobenzene 0.001 I-Propylbcozene 0.001 N-Ptupy$enzene 0.001 1,3 -Dichlorobenzene 0.001 Dibromachiorotnethane 0.001 Dichlorodifluoromethane 0.001 Chlorometbane 0.001 Vinyl Chloride 0.001 Hrdmotnethhne 1 0.001 Chloroethane 0.001 Trichloroiluorornethane 0.001 I, I-Dichloroethene 0.001 Metbylene Chloride 0.001 Trans-1.2-Dichlotoethene 0.001 Cie•":2-Dichlo:0ethenc 0.001 $YOrpaQt�hloromet)1Rno O.OQ1 Bromochlororncdtane 0.001 Cis-i:a-Dichtoroaropeno 0.001 Tans-1,3-Dichieropropene 0.001 Toral XyL-nes 0.001 A1ludon tactor Sataplo Nurnbcr Sample Dur Sample Ttrtto (HM) mglL = milligrams Per Ljrer, = Pane Par Million BDL BDL BDL VOL BAT - BDL DDL BDL BDL BDL BDL BDL BDI. 13DL 1LDL 13DL BDL BDL HDL BDL BDL BDL BDL uni- BAJL BDL BDL BDL BDl_ BDL DLBDLUDI- BDL BDL HDL BDL 0.0011 BBL BD,L BDL BDL BDL BDL BDL AM BDL BDL BDL BDL BAL BDL 13DL BBL Bni. aDL BDL .BDi- 1 438651 12I0�/Ol 1010 8DL = Below Detection Limits P- 6/8. 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P r,L'd0 Ma " y N30/03111'132d 0� c� p o i+7 y. w 2 awn FL CL 3 3 CO O O D a n. n -n r C, I! 11 II S z� o� 10 a Q 10 J 03 -uZ 1 ' �0N�z c5 .00 00 P. o 0 3 cD O tt N W C. 0 n 0 ZcmB � ` V m z 0 n n ..��nalytical www.pacelahs.com Pace Analytical Servr, 9800 Kincey Avenue, Si., Huntersville, NC Phone: 704.875.5, Fax: 704.875.96; Lab Project Number: 9225689 Client Project ID: Coats American/9322945 Lab Sample No: 93963775 Project Sample Number: 9225689-003 Date Collected: 08/28/01 08:15 Client Sample ID: MW #13 GRAB #475 Matrix: Water Date Received: 08/28/01 10:18 Parameters GC Volatiles GC VOCs in Water Dichlorodifluoromethane Chloromethane Vinyl chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Methylene chloride trans-1,2-Dichloroethene 1,1-Dichloroethane cis-1,2-Dichloroethene Bromochloromethane Chloroform 2,2-Dichloropropane 1,2-Dichloroethane 1,1,1 -Trichloroethane 1,1-Dichloropropene Carbon tetrachloride Dibromomethane 1,2-DichLoropropane Trichloroethene Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane 1,3-Dichloropropane Dibromochloromethane 1,2-Dibrommethane (EDB) Tetrachloroethene 1,1,1,2 -Tetrachloroethane Chlorobenzene Bromoform 1,1,2,2 -Tetrachloroethane 1,2,3-Trichloropropane Bromobenzene Date: 09/06/01 Page: 5 Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit Prep/Method: SM 6230D / SM 6230D ND ug/L 0.50 1.0 09/05/01 07:56 KST 75-71-8 ND ug/L 0.50 1.0 09/05/01 07:56 KST 74-87-3 ND ug/L 0.50 1.0 09/05/01 07:56 KST 75-01-4 ND ug/l 0.50 1.0 09/05/01 07:56 KST 74-83-9 ND ug/l 0.50 1.0 09/05/01 07:56 KST 75-00-3 ND ug/l 0.50 1.0 09/05/01 07:56 KST 75-69-4 ND ug/L 0.50 1.0 09/05/01 07:56 KST 75-35-4 ND ug/l 0.50 1.0 09/05/01 07:56 KST 75-09-2 ND ug/t 0.50 1.0 09/05/01 07:56 KST 156-60-5 ND ug/1 0.50 1.0 09/05/01 07:56 KST 75-34-3 ND ug/t 0.50 1.0 .09/05/01 07:56 KST 156-59-2 ND ug/t 0.50 1.0 09/05/01 07:56 KST 74-97-5 ND ug/l 0.50 1.0 09/05/01 07:56 KST 67-66-3 ND ug/l 0.50 1.0 09/05/01 07:56 KST 594-20-7 ND ug/l 0.50 1.0 09/05/01 07:56 KST 107-06-2 ND ug/l 0.50 1.0 09/05/01 07:56 KST 71-55-6 ND ug/l 0.50 1.0 09/05/01 07:56 KST 563-58-6 ND ug/l 0.50 1.0 09/05/01 07:56 KST 56-23-5 ND ug/l 0.50 1.0 09/05/01 07:56 KST 74-95-3 ND ug/L 0.50 1.0 09/05/01 07:56 KST 78-87-5 ND ug/L 0.50 1.0 09/05/01 07:56 KST 79-01-6 ND ug/L 0.50 1.0 09/05/01 07:56 KST 75-27-4 ND ug/L 0.50 1.0 09/05/01 07:56 KST 10061-01-5 ND ug/L 0.50 1.0 09/05/01 07:56 KST 10061-02-6 ND ug/L 0.50 1.0 09/05/01 07:56 KST 79-00-5 ND ug/L 0.50 1.0 09/05/01 07:56 KST 142-28-9 ND ug/L 0.50 1.0 09/05/01 07:56 KST 124-48-1 ND ug/L 0.50 1.0 09/05/01 07:56 KST 106-93-4 ND ug/L 0.50 1.0 09/05/01 07:56 KST 127-18-4 ND ug/t 0.50 1.0 09/05/01 07:56 KST 630-20-6 ND ug/l 0.50 1.0 09/05/01 07:56 KST 108-90-7 ND ug/L 0.50 1.0 09/05/01 07:56 KST 75-25-2 ND ug/l 0.50 1.0 09/05/01 07:56 KST 79-34-5 ND ug/l 0.50 1.0 09/05/01 07:56 KST 96-18-4 ND ug/1 0.50 1.0 09/05/01 07:56 KST 108-86-1 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS NC Wastewater 12 This report shall not be reproduced, except in full, NC Drinking Water 37706 without the written consent of Pace Analytical Services, Inc. Sc 99006 ,N �CCpgo Laboratory Certification IN KY Drinking Water 90090 VA Drinking Water 213 FL NELAP E87627 Date: 09/06/01 Page: 6 Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IN NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213 Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627 \N ACCOA Pace Analytical Servib. 9800 Kincey Avenue, Sp. Vic a Huntersville, NC Phone: 704.875:9 www.pacelabs.com Fax: 704.875.90: Lab Project Number: 9225689 Client Project ID: Coats American/9322945 Lab Sample No: 93963775 Project Sample Number: 9225689-003 Date Collected: 08/28/01 08:15 Client Sample ID: MW #13 GRAB #475 Matrix: Water Date Received: 08/28/01 10:18 Parameters Results Units Report Limit Dilution Analyzed CAS No. Ftnote Reg Limit 2-Chlorotoluene ND ug/l 0.50 1.0 09/05/01 07:56 KST 95-49-8 4-Chlorotoluene ND ug/l 0.50 1.0 09/05/01 07:56 KST 106-43-4 1,3 -Dichlorobenzene ND ug/l 1.0 1.0 09/05/01 07:56 KST 541-73-1 1,4 -Dichlorobenzene 3.8 ug/l 1.0 1.0 09/05/01 07:56 KST 106-46-7 1,2 -Dichlorobenzene ND ug/l 1.0 1.0 09/05/01 07:56 KST 95-50-1 1,2-Dibromo-3-chloropropane ND ug/l 2.0 1.0 09/05/01 07:56 KST 96-12-8 1,2,4-Trichlorobenzene ND ug/l 2.0 1.0 09/05/01 07:56 KST 120-82-1 Hexachloro-1,3-butadiene ND ug/L 2.0 1.0 09/05/01 07:56 KST 87-68-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1.0 09/05/01 07:56 KST 87-61-6 MethyL-tert-butyl ether ND ug/L 0.50 1.0 09/05/01 07:56 KST 1634-04-4 Diisopropyl ether ND ug/L 0.50 1.0 09/05/01 07:56 KST 108-20-3 Benzene ND ug/l 0.50 1.0 09/05/01 07:56 KST 71-43-2 Toluene ND ug/l 0.50 1.0 09/05/01 07:56 KST 108-88-3 EthyLbenzene ND ug/l 0.50 1.0 09/05/01 07:56 KST 100-41-4 m&p-Xylene ND ug/L 0.50 1.0 09/05/01 07:56 KST Styrene ND ug/L 0.50 1.0 09/05/01 07:56 KST 100-42-5 o -Xylene ND ug/L 0.50 1.0 09/05/01 07:56 KST 95-47-6 Isopropylbenzene (Cunene) ND ug/l 0.50 1.0 09/05/01 07:56 KST 98-82-8 n-Propylbenzene ND ug/L 0.50 1.0 09/05/01 07:56 KST 103-65-1 1,3,5-Trimethylbenzene ND ug/L 0.50 1.0 09/05/01 07:56 KST 108-67-8 tert-Butylbenzene ND ug/L 0.50 1.0 09/05/01 07:56 KST 98-06-6 1,2,4-Trimethylbenzene ND ug/l 0.50 1.0 09/05/01 07:56 KST 95-63-6 sec-Butylbenzene ND ug/L 0.50 1.0 09/05/01 07:56 KST 135-98-8 p-Isopropyltoluene ND ug/l 1.0 1.0 09/05/01 07:56 KST 99-87-6 n-Butylbenzene ND ug/L 1.0 1.0 09/05/01 07:56 KST 104-51-8 Naphthalene ND ug/l 2.0 1.0 09/05/01 07:56 KST 91-20-3 1-Chloro-3-fluorobenzene (S) 108 % 1.0 09/05/01 07:56 KST 625-98-9 Date: 09/06/01 Page: 6 Laboratory Certification IN REPORT OF LABORATORY ANALYSIS Laboratory Certification IN NC Wastewater 12 KY Drinking Water 90090 NC Drinking Water 37706 This report shall not be reproduced, except in full, VA Drinking Water 213 Sc 99006 without the written consent of Pace Analytical Services, Inc. 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DATE: 12/18/00 PAGE: 9 Pace Project Number: 9219112 Client Project ID: Coats American-9316932 Pace Sample No: 93736940 Date Collected: 12/06/00 Matrix: Water Client Sade ID:MW #13 GRAB #845 Date Received: 12/06/00 Parameters --------------------------------- Results ---------- Units --------- PRL ---------- App. -------- DF Analyzed -------- Analyst CAS# Footnotes ----- ---------- ---------- GC Volatiles GC VOCs in Water Method: SM 6230D Prep Method: SM 6230D Dichlorodifluoromethane ND ug/l 0.5 1.00 12/15/00 MAG 75-71-8 Chloromethane ND ug/l 0.5 1.00 12/15/00 MAG 74-87-3 Vinyl Chloride NO ug/t 0.5 1.00 12/15/00 MAG 75-01-4 Bromomethane NO ug/t 0.5 1.00 12/15/00 MAG 74-83-9 Chloroethane NO ug/l 0.5 1.00 12/15/00 MAG 75-00-3 Trichlorofluoromethane NO ug/l 0.5 1.00 12/15/00 MAG 75-69-4 1,1-Dichloroethene ND ug/l 0.5 1.00 12/15/00 MAG 75-35-4 Methylene Chloride NO ug/l 0.5 1.00 12/15/00 MAG 75-09-2 trans-1,2-Dichloroethene NO ug/l 0.5 1.00 12/15/00 MAG 156-60-5 1,1-Dichloroethane NO ug/l 0.5 1.00 12/15/00 MAG 75-34-3 cis-1,2-Dichloroethene ND ug/t 0.5 1.00 12/15/00 MAG 156-59-2 Bromochloromethane ND ug/l 0.5 1.00 12/15/00 MAG 74-97-5 Chloroform NO ug/l 0.5 1.00 12/15/00 MAG 67-66-3 2,2-Dichloropropane NO ug/t 0.5 1.00 12/15/00 MAG 594-20-7 1,2-Dichloroethane NO ug/l 0.5 1.00 12/15/00 MAG 107-06-2 1,1,1-Trichloroethane NO ug/l 0.5 1.00 12/15/00 MAG 71-55-6 1,1-Dichloropropene ND ug/l 0.5 1.00 12/15/00 MAG 563-58-6 Carbon Tetrachloride ND ug/l 0.5 1.00 12/15/00 MAG 56-23-5 Dibromomethane ND ug/l 0.5 1.00 12/15/00 MAG 74-95-3 1,2-Dichloropropane NO ug/t 0.5 1.00 12/15/00 MAG 78-87-5 Trichloroethene ND ug/l 0.5 1.00 12/15/00 MAG 79-01-6 Bromodichloromethane NO ug/l 0.5 1.00 12/15/00 MAG 75-27-4 cis-1,3-Dichloropropene NO ug/l 0.5 1.00 12/15/00 MAG 10061-01-5 trans-1,3-Dichloropropene ND ug/t 0.5 1.00 12/15/00 MAG 10061-02-6 1,1,2-Trichloroethane NO ug/l 0.5 1.00 12/15/00 MAG 79-00-5 1,3-Dichloropropane ND ug/t 0.5 1.00 12/15/00 MAG 142-28-9 Dibromochloromethane ND ug/l 0.5 1.00 12/15/00 MAG 124-48-1 1,2-Dibromoethane NO ug/l 0.5 1.00 12/15/00 MAG 106-93-4 Tetrachloroethene NO ug/l 0.5 1.00 12/15/00 MAG 127-18-4 1,1,1,2-Tetrachloroethane ND ug/t 0.5 1.00 12/15/00 MAG 630-20-6 Chlorobenzene NO ug/l 0.5 1.00 12/15/00 MAG 108-90-7 Bromoform NO ug/l 0.5 1.00 12/15/00 MAG 75-25-2 1,1,2,2-Tetrachloroethane ND ug/l 0.5 1.00 12/15/00 MAG 79-34-5 1,2,3-Trichloropropane NO ug/t 0.5 1.00 12/15/00 MAG 96-18-4 Bromobenzene NO ug/t 0.5 1.00 12/15/00 MAG 108-86-1 2-Chlorotoluene ND ug/t 0.5 1.00 12/15/00 MAG 95-49-8 - ✓ Pace Analytical Sr. ace Analytical TMt 9800 Kincey Aivnb, Huntersviile. , ;. - www.pacelabs.com Phone. 704. 8,, Fax: 704.87;:, DATE: 12/18/00 PAGE: 10 Pace Project Number: 9219112 Client Project ID: Coats American -9316932 Pace Sample No: 93736940 Date Collected: 12/06/00 Matrix: Water Client Sample ID: MW #13 GRAB #845 Date Received: 12/06/00 Parameters Results Units PRL App. DF Analyzed -------- Analyst CAS# Footnotes ----- ---------- ---------- --------------------------------- 4-Chlorotoluene ---------- ND --------- ug/t ---------- 0.5 -------- 1.00 12/15/00 MAG 106-43-4 1,3 -Dichlorobenzene ND ug/l 1 1.00 12/15/00 MAG 541-73-1 1,4 -Dichlorobenzene ND ug/t 1 1.00 12/15/00 MAG 106-46-7 1,2 -Dichlorobenzene ND ug/l 1 1.00 12/15/00 MAG 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/l 2 1.00 12/15/00 MAG 96-12-8 1,2,4-Trichlorobenzene ND ug/l 2 1.00 12/15/00 MAG 120-82-1 Hexachloro-1,3-butadiene ND ug/l 2 1.00 12/15/00 MAG 87-68-3 1,2,3-Trichlorobenzene ND ug/t 2 1.00 12/15/00 MAG 87-61-6 Methyl-tert-butyl Ether ND ug/L 0.5 1.00 12/15/00 MAG 1634-04-4 Diisopropyt ether ND ug/l 0.5 1.00 12/15/00 MAG 108-20-3 Benzene ND ug/L 0.5 1.00 12/15/00 MAG 71-43-2 Toluene ND ug/L 0.5 1.00 12/15/00 MAG 108-88-3 Ethylbenzene ND ug/t 0.5 1.00 12/15/00 MAG 100-41-4 m&p-Xylene ND ug/t 0.5 1.00 12/15/00 MAG 7816-60-0 Styrene ND ug/t 0.5 1.00 12/15/00 MAG 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/t 0.5 1.00 12/15/00 MAG 95-47-6 Isopropylbenzene (Cumene) ND ug/l 0.5 1.00 12/15/00 MAG 98-82-8 n-Propylbenzene ND ug/l 0.5 1.00 12/15/00 MAG 103-65-1 1,3,5-Trimethylbenzene ND ug/t 0.5 1.00 12/15/00 MAG 108-67-8 tert-Butylbenzene ND ug/L 0.5 1.00 12/15/00 MAG 98-06-6 1,2,4-Trimethylbenzene ND ug/t 0.5 1.00 12/15/00 MAG 95-63-6 sec-Butylbenzene ND ug/t 0.5 1.00 12/15/00 MAG 135-98-8 p-Isopropyltoluene ND ug/l 1 1.00 12/15/00 MAG 99=87-6 n-Butylbenzene ND ug/l 1 1.00 12/15/00 MAG 104-51-8 Naphthalene ND ug/L 2 1.00 12/15/00 MAG 91-20-3 1-Chloro-3-fluorobenzene (S) 104 % 1.00 12/15/00 MAG 625-98-9 ID CD tom— a 000> CD .-� cn >= aNC=-��OCOO ycD ^ "r. 0 N � Z _CD p:CL m �-<a Z'3n ai �a;33 CD3Nr=Z o —.� 2. z 0 O __. 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CD C CD -G z3n o CD CD �CLM ® 0 M Cl) Q M Cl) z 2, a O m®(n D) o zZ N(no a II 0 CD CD I o ~ •» s Sv m ' z o a 'O CL m C 33=•3333333 to cc o ccs to cca co co ccs --uc 0 o p 0 0 � S3 Im 0 -n ca CD d 3 O O 3 m N cD n O 003 33`, cL c KK7T2'r1OC)C OM>O-DZZ W Hca iCCCDCCL 2) ID 7;Z.===; O �'O mC� IDiD CD �^ 02Z co�Nnoo�3Q-oc3• CD C cn•3�t cD .. 3• C 3 C 'O Lo ( O " 3 -G CD o 3 = ..w " M Cl) cD3 m®(n o zZ CD I ' z o CL Ca CL 333333333333333n c cn ccs cn co cry cn co co cn cc cn (m ccs cn �. O>N-vZ 5,3��_. cD o NrZ -0 3•��0 C m Q. Z Ic — 0 3 3 cD -0 = o C= a N Q7 1�1 IA ------------- Pace Sample No: 93428365 Client Sample ID: MW -13 - Pace Analytical Services, 9800 Kincey Avenue, Suite Huntersville, NC 2! Tel: 704-875-9092 Fax: 704-875-9091 DATE: 12/22/99 PAGE: 9 Pace Project Number: 9210642 Client Project ID: Coats American 939712 Date Collected: 12/08/99 Matrix: Water Date Received: 12/09/99 Parameters Results Units PRL App. DF Analyzed Analyst CAS# Footnotes ---------------------------------------------------------------------- -------- --------------- ---------- GC Volatiles GC VOCs in Water Method: SM 6230D Prep Method: SM 6230D Dichlorodifluoromethane ND ug/L 0.5 1.00 12/21/99 CLL 75-71-8 Chloromethane ND ug/L 0.5 1.00 12/21/99 CLL 74-87-3 Vinyl Chloride ND ug/t 0.5 1.00 12/21/99 CLL 75-01-4 Bromomethane ND ug/L 0.5 1.00 12/21/99 CLL 74-83-9 Chloroethane ND ug/L 0.5 1.00 12/21/99 CLL 75-00-3 Trichlorofluoromethane ND ug/l 0.5 1.00 12/21/99 CLL 75-69-4 1,1-Dichloroethene ND ug/t 0.5 1.00 12/21/99 CLL 75-35-4 Methylene Chloride ND ug/L 0.5 1.00 12/21/99 CLL 75-09-2 trans-1,2-DichLoroethene ND ug/t 0.5 1.00 12/21/99 CLL 156-60-5 1,1-Dichloroethane ND ug/l 0.5 1.00 12/21/99 CLL 75-34-3 cis-1,2-Dichloroethene ND ug/l 0.5 1.00 12/21/99 CLL 156-59-2 BromochLoromethane ND ug/l 0.5 1.00 12/21/99 CLL 74-97-5 Chloroform ND ug/l 0.5 1.00 12/21/99 CLL 67-66-3 2,2-Dichloropropane ND ug/l 0.5 1.00 12/21/99 CLL 594-20-7 1,2-Dichloroethane ND ug/L 0.5 1.00 12/21/99 CLL 107-06-2 1,1,1 -Trichloroethane ND ug/t 0.5 1.00 12/21/99 CLL 71-55-6 1,1-Dichtoropropene ND ug/t 0.5 1.00 12/21/99 CLL 563-58-6 Carbon Tetrachloride ND ug/t 0.5 1.00 12/21/99 CLL 56-23-5 Dibromomethane ND ug/I. 0.5 1.00 12/21/99 CLL 74-95-3 1,2-Dichloropropane ND ug/t 0.5 1.00 12/21/99 CLL 78-87-5 Trichloroethene ND ug/L 0.5 1.00 12/21/99 CLL 79-01-6 Bromodichloromethane ND ug/L 0.5 1.00 12/21/99 CLL 75-27-4 cis-1,3-Dichloropropene ND ug/L 0.5 1.00 12/21/99 CLL 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.5 1.00 12/21/99 CLL 10061-02-6 1,1,2 -Trichloroethane ND ug/l 0.5 1.00 12/21/99 CLL 79-00-5 1,3-Dichloropropane ND ug/l 0.5 1.00 12/21/99 CLL 142-28-9 Dibromochtoromethane ND ug/1 0.5 1.00 12/21/99 CLL 124-48-1 1,2-Dibromoethane ND ug/l 0.5 1.00 12/21/99 CLL 106-93-4 TetrachLoroethene ND ug/l 0.5 1.00 12/21;'99 CLL 127-18-4 1,1,1,2 -Tetrachloroethane ND ug/l 0.5 1.00 12/21/99 CLL 630-20-6 Chlorobenzene ND ug/l 0.5 1.00 12/21/99 CLL 108-90-7 Bromoform ND ug/l 0.5 1.00 12/21/99 CLL 75-25-2 1,1,2,2 -Tetrachloroethane ND ug/L 0.5 1.00 12/21/99 CLL 79-34-5 1,2,3-TrichLoropropane ND ug/L 0.5 1.00 12/21/99 CLL 96-18-4 Bromobenzene ND ug/L 0.5 1.00 12/21/99 CLL 108-86-1 2-Chlorotoluene ND ug/L 0.5 1.00 12/21/99 CLL 95-49-8 Laboratory Certification IDs Laboratory Certification IDs NC ter 12 aWater REPORT OF LABORATORY ANALYSIS rinkinWater 90090 KY DUST NC Drnkng37706 N List Sc 99006 This report shall not be reproduced, except in full, VA Drinking Water 213 without the written consent of Pace Analytical Services, Inc. i Pace Analytical Services;' 9800 Kincey Avenue, Suite 1 Huntersville, NC 28C Tel: 704-875-9092 Fax: 704-875-9091 DATE: 12/22/99 PAGE: 10 Pace Project Number: 9210642 Client Project ID: Coats American 939712 Pace Sample No: 93428365 Date Collected: 12/08/99 Matrix: Water Client Sample ID: MW -13 Date Received: 12/09/99 Parameters --------------------------------- Results ---------- Units --------- PRL App. DF Analyzed Analyst CAS# Footnotes 4-Chlorotoluene ND ug/t ---------- 0.5 -------- 1.00 -------- 12/21/99 ----- CLL ---------- ---------- 106-43-4 1,3 -Dichlorobenzene ND ug/I. 1 1.00 12/21/99 CLL 541-73-1 1,4 -Dichlorobenzene ND ug/t 1 1.00 12/21/99 CLL 106-46-7 1,2 -Dichlorobenzene ND ug/l 1 1.00 12/21/99 CLL 95-50-1 1,2-Dibromo-3-Chloropropane ND ug/L 2 1.00 12/21/99 CLL 96-12-8 1,2,4-Trichlorobenzene ND ug/L 2 1.00 12/21/99 CLL 120-82-1 Hexachtorobutadiene ND ug/t 2 1.00 12/21/99 CLL 87-68-3 1,2,3-Trichlorobenzene ND ug/t 2 1.00 12/21/99 CLL 87-61-6 Methyl-tert-butyl Ether ND ug/I. 0.5 1.00 12/21/99 CLL 1634-04-4 Isopropyl Ether ND ug/l 0.5 1.00 12/21/99 CLL 108-20-3 Benzene ND ug/l 0.5 1.00 12/21/99 CLL 71-43-2 Toluene ND ug/l 0.5 1.00 12/21/99 CLL 108-88-3 EthyLbenzene ND ug/l. 0.5 1.00 12/21/99 CLL 100-41-4 m&p-Xylene ND ug/l 0.5 1.00 12/21/99 CLL 7816-60-0 Styrene ND ug/t 0.5 1.00 12/21/99 CLL 100-42-5 o -Xylene (1,2 -Dimethylbenzene) ND ug/L 0.5 1.00 12/21/99 CLL 95-47-6 IsopropyLbenzene (Cumene) ND ug/t 0.5 1.00 12/21/99 CLL 98-82-8 n-Propylbenzene ND ug/L 0.5 1.00 12/21/99 CLL 103-65-1 1,3,5-Trimethylbenzene ND ug/l. 0.5 1.00 12/21/99 CLL 108-67-8 tert-Butylbenzene ND ug/L 0.5 1.00 12/21/99 CLL 98-06-6 1,2,4-Trimethylbenzene ND ug/l 0.5 1.00 12/21/99 CLL 95-63-6 sec-Butylbenzene ND ug/l 0.5 1.00 12/21/99 CLL 135-98-8 p-IsopropyLtoluene ND ug/L 1 1.00 12/21/99 CLL 99-87-6 n-Butylbenzene ND ug/L 1 1.00 12/21/99 CLL 104-51-8 Naphthalene ND ug/t 2 1.00 12/21/99 CLL 91-20-3 1-Chloro-3-fLuorobenzene (S) 96 % 1.00 12/21/99 CLL 625-98-9 Laboratory Certification IQs Laboratory Certification IDs NC Wastewater REPORT ®F LABORATORY Drinking 90090 W12 NC Drinkin Water 37706 ANALYSIS N Sc 99006 This report shall not be reproduced, except 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CD p, �' 3 n m Ca a 0 0 o a = CL 0_ a r- * * * ,7 11 n II 0• Z a. Iro v 0 0 3.30aZ CD . v��O �Z �svP7 CD CD 0 Z o O OCO o 0 CL cl W w c3333 y, ca �ea cr` M CA I z O m m m m M, ao C0 CD __ c, c o d CD ci w o� ACL u ks 2. 6 of CDO co v ( c Q to cD o CL c0cr Cl) CD o Q 0 0 a n 000 CD O 0 -0 Lrk w Q co 0) C B] C .g I_ C) m � !D w m n In CD 0r' c 0 0 w N m m N m CL M55 5 5 CD 3 tip a 3r :s CO C N t9 N - o m o co N n ? 0 0 aS a o � n; m N � N N 0 m DA m a 0 0 CD Z w B O m O O •mp � 0 .� o CDm 0 .c rr c V CC N Z w d CD 0 0 m q CO 0 o % m m o nCD v a o r O ( , m I a W (.0 Q m Z X no_wrn o Z c -DI 0 3 O Z N m Z 0 wm Q - m � O W 0 TRITEST, INC. L a b o r a t o r y R e p o r t Page 8 Pace Analytical ServicesReport Date 1/04/5. a� Work Orc_r No. 9512-00600` due lie / No. SampleLDD Date Sampled Time Sampled Matrix Condition 097 MW -13 34625 12/17/1998 8:12 GW 4±2°C Project No. Date Test Performed Method Results Tech Analyzed Qual VOCs in GW SM 6230D ZW. 12/2 /93 Benzene <0.5 ug/L ZW 12/29/98 Bromobenzene <0.5 ug/L ZW 12/29/98 Bromochloromethane <0.5 ug/L ZW 12/29/98 Bromodichloromethane <0.5 ug/L Zw 12/2°/98 Bromoform <0.5 ug/L Z 12/29/96 Bromomethane <0.5 uq/L ZW 12/29/98 n-Butylbenzene <0.5 ug/L ZW 12/29/98 sec-Butylbenzene <0.5 ug/L ZW 12/29/98 tert-Butylbenzene <0.5 ug/L ZW 12/29/98 Carbon tetrachloride <0.5 ug/L ZW 12/29/98 Chlorobenzene <0.5 ug/L ZW 12/29/98 Chloroethane <0.5 ug/L ZW 12/29/98 Chloroform <0.5 ug/L ZW 12/29/98 Chloromethane <0.5 ug/L ZW 12/29/98 2-Chlorotoluene <0.5 ug/L ZW 12/29/98 4-Chlorotoluene <0.5 ug/L ZW 12/29/98 Dibromochloromethane <0.5 ug/L ZW 12/29/98 1,2-Dibromo-3-chloropropane <0.5 ug/L Zw 12/29/98 1,2-Dibromoethane <0.5 ug/L ZW 12/29/98 Dibromomethane <0.5 ug/L ZW 12/29/98 Dichlorodifluoromethane <0.5 Ug/1' Zw 12/29/98 1,1-Dichloroethane <0.5 ug/L ZW 12/29/98 1,2-Dichloroethane <0.5 ug/L ZW 12/29/98 1, 1-Dichloroethene <0.5 ug/L Z:7 12/29,'98 cis-1,2-Dichloroethene <0.5 ug/L ZW 12/29/98 trans-1,2-Dichloroethene <0.5 ug/L ZW 12/29/98 1,2-Dichloropropane <0.5 ug/L ZW 12/29/98 1,3®Dichloropropane <0.5 ug/L ZW 12/29/98 2,2-Dichloropropane <0.5 ug/L Zw 12/29/98 1,1-Dichloropropene <0.5 ug/L ZW 12/29/98 Ethylbenzene <0.5 ug/L ZW 12/29/98 Hexachlorobutadiene <0.5 ug/L ZW 12/29/98 Isopropylbenzene <0.5 ug/L ZW 12/29/98 4-Isopropyltoluene <0.5 ug/L ZW 12/29/98 Methylene chloride <0.5 ug/L ZW 12/29/9.8 Naphthalene <0.5 u5/L Zw 12/29/98 n-Propylbenzene <0.5 ug/L ZW 12/29/98 Styrene <0.5 ug/L ZW 12/29/98 ---- Continued on Next Page ---- TRITEST, INC.' Page L a b o r a t o r y R e p o r t Pace Analytical Services Report bate 1/04, Project No.- ,.� R, 3�M Work Order No. 9812-0060 Nd. Sample ID 0 7 MW -13 93134625 Test Performed Method Results Tech Date Analyzed Qual 1,1,1,2 -Tetrachloroethane <0.5 ug/L ZW 12/29/99 1,1,2,2 -Tetrachloroethane <0.5 ug/L ZW 12/29/98 Tetrachloroethene <0.5 ug/L ZW 12/29/98 Toluene <0.5`uy/1AJ ZW 12/29/98 1,2,3-Trichlorobenzene <0.5 ug/L Zw 12/29/98 1,2,4-Trichlorobenzene <0.5 ug/L Zw 12/29/98 1,1,1 -Trichloroethane <0.5 ug/L ZW 12/29/98 1,1,2 -Trichloroethane <0.5 ug/L ZW 12/29/98 Trichloroethene <0.5 ug/L ZW 12/29/93 Trichlorofluoromethane <0.5 ug/L ZW 12/29/98 1,2,3-Trichloropropane <0.5 ug/L ZW 12/29/98 1,2,4-Trimethylbenzene <0.5 ug/L ZW 12./29/98 1,3,5-Trimethylbenzene <0.5 ug/L ZW 12/29/98 Vinyl chloride <0.5 ug/L ZW 12/29/98 o -Xylene <0.5 ug/L ZW 12/29/98 m,p-Xylene <0.5 ug/L ZW 12/29/98 No � Sample ID 008 MW Date Sampled Time Sampled Matrix Condition -14 /,13134633 12/17/1998 8:22 GW 4-20C Test Performed Method Results Tech Analyzed Qual VOCs in GW SM 6230D ZW 12/29/98 Benzene <0.5 ug/L ZW 12/29/98 Bromobenzene <0.5 ug/L ZW 12/29/98 Bromochloromethane <0.5 ug/L ZW 12/29/98 Bromodichloromethane <0.5 ug/L ZW 12/29/98 Bromoform <0.5 ug/L ZW 12/29/98 Bromomethane c0.5 ug/L ZW 12/29/98 n-Butylbenzene <0.5 ug/L ZW 12/29/98 sec-Butylbenzene <0.5 ug/L ZW 12/29/98 tert-Butylbenzene <0.5 ug/L ZW 12/29/98 Car:;cn tetrachloride <0.5 ug/L Zv; 12/:.9/38 Chlorobenzene <0.5 ug/L ZW 12/29/98 Chloroethane <0.5 ug/L ZW 12/29/98 Chloroform <0.5 ug/L ZW 12/29!98 Chloromethane <0.5 ug/L ZW 12/29/98 2-Chlorotoluene <0.5 ug/L ZW 12/29/98 ---- Continued on Next Page ---- .» c 02 L�n��OO Nm .-. 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O M: CD COLD 0 O CCD r 0 m :5 aCD = M 0_ a w I CD C .0-P CD cn g--! o w z v 1J w m c w co G w 1 F m .` CD o o g M 6 � �. a z cn�m w CD a w O 3 o 0 D z m e D CD h a Cl)� Z� 0 0 M M M N 0p �. v Q( op c D I I 0 n ohi CD ,�,.. CL M 2C �. Cl) 7) 0 CD C m c C) N m CD 0 3 N U) c a 3 3 3 3 3 3 33 Z) 3 003 zr3 cc (o o(acocococQ(o(Q eco 3 3cc -=i` O � � � � � � O � =- ZKKT=MC)oC)oM>MZZ sv Z3 co i co CD c Z' o_ W W Z 0 cn Cn��® �o 03 C)C)00 CD CD asll -occ- =.3o^Z cccC° Ln.c ccDD -- 3 �'3 3 c p0 3wconc� �--Ic3 cv?Ca,.. 0c3 03 cn c`DD 3 — z Z cn -Q 333333333333333 c0 cQ co co cn co co co co co co cQ co (Q co 0 O CD (D CD o - o m 0 � c `< 2. C7 3 0 c 0 Q 0 w 0 Q = N -0 Z CD :3 CY . o = o_ 5 CD C7 0 CD a CD -80 2 o CD cn n. COD 0 Iffilow I/0'3!A1JOS.lj � c c c 3 3 3 c0 c0 cQ cQ c0 co D�0ti� m� m m CD a 0 0 o. 0 0= = �p> CADS c 0Eo r M w �' M 0 o w 3 w o`Q 3 0 w nz m—n o w-o 0w 0 5 -CR C) CD o CD cn CD M m �c c a m �m 6 N a" 70-zzz Sc mc) -00 C z M s - Q- a CD M rcn� =� -0 "mmpao . n CD .� w 07 .. O M: CD COLD 0 O CCD r 0 m :5 aCD = M 0_ a w I C .0-P CD cn g--! o w z v 1J w m c w co G w 1 F m .` CD o o g M 6 � �. a F cn�m w CD a w O 3 o 0 D z m e D CD h a Cl)� Z� 0 0 M M M N 0p �. v Q( D I I 0 n ohi CD ,�,.. M 2C �. Cl) 7) 0 CD C m c C) I -- � b n 6 V 0 0 m a 0 IV- N= o �� m 0 Dm 9: c 0 70-zzz mc) -00 C z o "mmpao zD O�En m O I I y D I I r Q m O w o w o v 1J w m c DM w a w 0 o a I v a F O a w Q z W o' M o =, p z W I I 0 CD 2C �. Cl) 7) CD C m c m o 0 CD 0 N U) c a -�%;AL r,m ;ENVIRONMENTAL TECH-- Y, INC. ENVIRONMENTAL ANALYTICAL SERVICES FINAL REPORT OF ANALYSES PACE ANALYTICAL SERVICES, INC. 54 RAVENSCROFT DR. ASHEVILLE, NC 28801 - COATS AMERIC MW -13 REPORT DATE: 12/30/97 P.O. # 93 001621 SAMPLE NUMBER- 139670 SAMPLE ID- MW -13 #1813 SAMPLE MATRIX- GW DATE SAMPLED- 12/16/97 TIME SAMPLED- 1000 DATE RECEIVED- 12/17/97 SAMPLER- P.P. RECEIVED BY- CLH TIME RECEIVED- 1025 DELIVERED BY- UPS Page 1 of 3 PROJECT NAME COATS AMERICAN ANALYSIS ANALYSIS METHOD DATE BY RESULT UNITS PQL VOLATILE ORGANIC COMPOUNDS 6230D 12/23/97 ALT BENZENE 6230D < 0.5 ug/L 0.5 BROMOBENZENE 6230D < 0.5 ug/L 0.5 BROMOCHLOROMETHANE 6230D < 0.5 ug/L 0.5 BROMODICHLOROMETHANE 6230D < 0.5 ug/L 0.5 BROMOFORM 6230D < 0.5 ug/L 0.5 BROMOMETHANE 6230D < 0.5 ug/L 0.5 n-BUTYLBENZENE 6230D < 0.5 ug/L 0.5 sec-BUTYLBENZENE 6230D < 0.5 ug/L 0.5 tert-BUTYLBENZENE 6230D < 0.5 ug/L 0.5 CARBON TETRACHLORIDE 6230D < 0.5 ug/L 0.5 CHLOROBENZENE 6230D < 0.5 ug/L 0.5 CHLOROETHANE 6230D < 0.5 ug/L 0.5 CHLOROFORM 6230D < 0.5 ug/L 0.5 CHLOROMETHANE 6230D < 0.5 ug/L 0.5 2-CHLOROTOLUENE 6230D < 0.5 ug/L 0.5 4-CHLOROTOLUENE 6230D < 0.5 ug/L 0.5 DIBROMOCHLOROMETHANE 6230D < 0.5 ug/L 0.5 1,2-DIBROMO-3-CHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,2-DIBROMOETHANE 6230D < 0.5 ug/L 0.5 DIBROMOMETHANE 6230D < 0.5 ug/L 0.5 P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511 Telephone (919) 467-3090 Fax (919) 467-3515 �"AL rENVIRONMENTAL TECOLOGY, INC. ENVIRONMENTAL ANALYTICAL SERVICES Page 2 of 3 PROJECT NAME : COATS AMERICAN CONTINUATION OF DATA FOR SAMPLE NUMBER 139670 P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511 Telephone (919) 467-3090 Fax (919) 467-3515 ANALYSIS ANALYSIS METHOD DATE BY RESULT UNITS PQL 1,2 -DICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,3 -DICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,4 -DICHLOROBENZENE 6230D 6.3 ug/L 0.5 DICHLORODIFLUOROMETHANE 6230D < 0.5 ug/L 0.5 1,1-DICHLOROETHANE 6230D < 0.5 ug/L 0.5 1,2-DICHLOROETHANE 6230D < 0.5 ug/L 0.5 1,1 DICHLOROETHENE 6230D < 0.5 ug/L 0.5 cis-1,2-DICHLOROETHENE 6230D < 0.5 ug/L 0.5 trans-1,2-DICHLOROETHENE 6230D < 0.5 ug/L 0.5 1,2-DICHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,3-DICHLOROPROPANE 6230D < 0.5 ug/L 0.5 2,2-DICHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,1-DICHLOROPROPENE 6230D < 0.5 ug/L 0.5 cis-1,3-DICHLOROPROPENE 6230D < 0.5 ug/L 0.5 trans-1,3-DICHLOROPROPENE 6230D < 0.5 ug/L 0.5 ETHYLBENZENE 6230D < 0.5 ug/L 0.5 HEXACHLOROBUTADIENE 6230D < 0.5 ug/L 0.5 ISOPROPYLBENZENE 6230D < 0.5 ug/L 0.5 p-ISOPROPYLTOLUENE 6230D < 0.5 ug/L 0.5 METHYLENE CHLORIDE 6230D < 0.5 ug/L 0.5 NAPHTHALENE 6230D < 0.5 ug/L 0.5 n-PROPYLBENZENE 6230D < 0.5 ug/L 0.5 STYRENE 6230D < 0.5 ug/L 0.5 1,1,1,2 -TETRACHLOROETHANE 6230D < 0.5 ug/L 0.5 1,1,2,2 -TETRACHLOROETHANE 6230D < 0.5 ug/L 0.5 TETRACHLOROETHENE 6230D < 0.5 ug/L 0.5 TOLUENE 6230D < 0.5 ug/L 0.5 1,2,3-TRICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,2,4-TRICHLOROBENZENE 6230D < 0.5 ug/L 0.5 1,1,1 -TRICHLOROETHANE 6230D < 0.5 ug/L 0.5 1,1,2 -TRICHLOROETHANE 6230D < 0.5 ug/L 0.5 P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511 Telephone (919) 467-3090 Fax (919) 467-3515 -:,AL '\,ENVIRONMENTAL TEC1- ,LOGY, INC. ENVIRONMENTAL ANALYTICAL SERVICES Page 3 of 3 PROJECT NAME : COATS AMERICAN CONTINUATION OF DATA FOR SAMPLE NUMBER 139670 1 LABORATORY DIRECTOR P.O. Box 12298 • Research Triangle Park, NC 27709 Shipping: 102-A Woodwinds Industrial Court • Cary, NC 27511 Telephone(919)467-3090 Fax(919)467-3515 ANALYSIS ANALYSIS METHOD DATE BY RESULT UNITS PQL TRICHLOROETHENE 6230D < 0.5 ug/L 0.5 TRICHLOROFLUOROMETHANE 6230D < 0.5 ug/L 0.5 1,2,3-TRICHLOROPROPANE 6230D < 0.5 ug/L 0.5 1,2,4-TRIMETHYLBENZENE 6230D < 0.5 ug/L 0.5 1,3,5-TRIMETHYLBENZENE 6230D < 0.5 ug/L 0.5 VINYL CHLORIDE 6230D < 0.5 ug/L 0.5 o -XYLENE 6230D < 0.5 ug/L 0.5 m,p-XYLENES 6230D < 0.5 ug/L 0.5 SURROGATE a 6230D 93.7 percent - SURROGATE b 6230D 99.7 percent - PQL = Practical Quantitation Limit Results followed by the letter J are estimated concentrations. NC DEHNR CERTIFICATIONS: DWQ - 96; PUBLIC WATER SUPPLY - 37724 1 LABORATORY DIRECTOR P.O. 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', ocCD t w t,3 -0 1 m o co m n a m m �ctn cr n O 1NC m o a C 0 m �y m " 0 * m n nyi o 3 w 3 c, to S m C C1 In �. z�m 3 m� CD r r- CD m o C/)cr�CD CD _ v a o v 4 Z CD C CD CD -na v D K w m w0 a o r CD CD 3 �� a� A v n -n-n m v a.: 1\1 mCD 0 w I o z 0 OI D a I a CD all n o w cD a C) a Q � c 0 :3 0 to I � CD w 0• D� aZ CD 3 W CD o J O N a CD 0 El m 0m K co Cl) � � N fQ C A Do 2E 0 v F d Yp T H (D a m Cp m Z 0 z O m v 0. 0, z M M m a w0><G) W v N m N N Cr m i O � f7 cnCo Za0 z cl —ni m ca M, O z S .i mono c v -v= "0m0Co cn y m D y O C°m m .o m m C 0 D d m —1 n o v CL co Cl) � � N fQ C A Do 2E 0 v F d Yp T H (D a m Cp m Z 0 z O m v 0. 0, z M M m a w0><G) W v N m N N Cr m i O � f7 cnCo Za0 z cl —ni m ca M, O z Pace Analytical Services, i, 54 Ravenscroft Driv, analytical Asheville, NC 28801' Tel: 704-254-7176 Fax: 704-252-4618 Mr. Jerry McKinney Page 13 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter INORGANIC ANALYSIS INDIVIDUAL PARAMETERS Calcium Magnesium January 06, 1997 PACE Project Number: A61205519' 93 0315712 12/10/96 12/11/96 GM -5 #1426 Units PRL Coats METHOD DATE ANALYZED mg/L 0.10 26 200.7 12/21/96 mg/L 0.20 20 200.7 12/21/96 PACE Sample Number: 93 0315763 Date Collected: 12/10/96 Date Received: 12/11/96 Client Sample ID: GM -5 #1429 Parameter Units PRL Coats METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 Dichlorodifluoromethane ug/L 1.0 ND 12/19/96 Chloromethane ug/L 1.0 ND 12/19/96 Chloroethene (Vinyl chloride) ug/L 1.0 NO 12/19/96 Bromomethane ug/L 1.0 ND 12/19/96 Chloroethane ug/L 1.0 ND 12/19/96 Trichlorofluoromethane ug/L 1.0 ND 12/19/96 1,1-Dichloroethene ug/L 1.0 ND 12/19/96 Dichloromethane ug/L 1.0 NO 12/19/96 trans-1,2-Dichloroethene ug/L 1.0 ND 12/19/96 1,1-Dichloroethane ug/L 1.0 ND 12/19/96 cis-1,2-Dichloroethene ug/L 1.0 ND 12/19/96 2,2-Dichloropropane ug/L 1.0 ND 12/19/96 Chloroform ug/L 1.0 ND 12/19/96 Bromochloromethane ug/L 1.0 ND 12/19/96 1,.1,1 -Trichloroethane ug/L 1.0 ND 12/19/96 1,1-Dichloro-l-propene ug/L 1.0 ND 12/19/96 Carbon tetrachloride ug/L 1.0 ND 12/19/96 1,2-Dichloroethane ug/L 1.0 ND 12/19/96 1,1,2 -Trichloroethene ug/L 1.0 ND 12/19/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services, . 54 Ravenscroft Drip A n a l yt i c a l Asheville NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Jerry McKinney Page 14 Client Reference: Coats American January 06, 1997 PACE Project Number: A6120551, PACE Sample Number: 93 0315763 Date Collected: 12/10/96 Date Received: 12/11/96 Client Sample ID: GM -5 #1429 Parameter Units PRL Coats METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 1,2-Dichloropropane ug/L 1.0 ND 12/19/96 Bromodichloromethane ug/L 1.0 ND 12/19/96 Dibromomethane ug/L 1.0 ND 12/19/96 cis-1,3-Dichloro-l-propene ug/L 1.0 ND 12/19/96 trans-1,3-Dichloro-l-propene ug/L 1.0 ND 12/19/96 1,1,2 -Trichloroethane ug/L 1.0 ND 12/19/96 1,3-Dichloropropane ug/L 1.0 ND 12/19/96 Tetrachloroethene ug/L 1.0 ND 12/19/96 Dibromochloromethane ug/L 1.0 ND 12/19/96 1,1,1,2 -Tetrachloroethane ug/L 1.0 ND 12/19/96 Bromoform ug/L 1.0 ND 12/19/96 1,1,2,2 -Tetrachloroethane ug/L 1.0 ND 12/19/96 1,2,3-Trichloropropane ug/L 1.0 ND 12/19/96 Bromobenzene ug/L 1.0 ND 12/19/96 2-Chlorotoluene ug/L 1.0 ND 12/19/96 4-Chlorotoluene ug/L 1.0 ND 12/19/96 1,3 -Dichlorobenzene 1,4 ug/L 1.01� 12/19/96 -Dichlorobenzene ug/L 1.0 2.2, 12/19/96 1,2 -Dichlorobenzene ug/L 1.0 ND 12/19/96 1,2-Dibromo-3-chloropropane ug/L 1.0 ND 12/19/96 1,2,4-Trichlorobenzene ug/L 1.0 ND 12/19/96 Hexachlorobutadiene ug/L 1.0 ND 12/19/96 1,2,3-Trichlorobenzene ug/L 1.0 ND 12/19/96 Benzene ug/L 1.0 ND 12/19/96 Toluene ug/L 1.0 ND 12/19/96 Chlorobenzene ug/L 1.0 ND 12/19/96 Eth lbenzene Y ug/L 1.0 ND 12/19/96 Xylenes, (total) ug/L 1.0 ND 12/19/96 Styrene ug/L 1.0 ND 12/19/96 Isopropylbenzene ug/L 1.0 ND 12/19/96 n-Propylbenzene ug/L 1.0 ND 12/19/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. Pace Analytical Services,, 54 Ravenscroft Drip, Analytical Asheville, NC 28801 Tel: 704-254-7176 Fax: 704-252-4618 Mr. Jerry McKinney January 06, 1997 Page 15 PACE Project Number: A61205519 Client Reference: Coats American PACE Sample Number: 93 0315763 Date Collected: 12/10/96 Date Received: 12/11/96 Client Sample ID: GM -5 #1429 Parameter Units PRL Coats METHOD DATE ANALYZED ORGANIC ANALYSIS VOLATILE ORGANICS 502.2 1,3,5-Trimethylbenzene ug/L 1.0 ND 12/19%96 t-Butylbenzene ug/L 1.0 ND 12/19/96 1,2,4-Trimethylbenzene ug/L 1.0 ND 12/19/96 s-Butylbenzene ug/L 1.0 ND 12/19/96 4-Isopropyltoluene ug/L 1.0 ND 12/19/96 n-Butylbenzene ug/L 1.0 ND 12/19/96 Naphthalene ug/L 1.0 ND 12/19/96 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. ;q *I ICD C CD Cr CD O w O LT Q Q. 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WgM K0030 wCa^ (D CD OMMwWCD cWmc'ccm3 c9. 32cOm CD X033 3-Iinw cD3 0z —z N N m i G "I I N 3333333333333'33 cc cc cc cc to cc cc cc cc cc to cc cc cc cc o Q � -0 N -0 Z pG= = CD O Cr CD Nft cn Z c1'CD om�'am 3 o = CD (\I o � U CL c1 -0 c CD o O c o/ C. f l o c�—D N c�—D — n 0a w Q 0 = o= O 0= o Cl m �' co 3 .. w Z CL w N to CD ES 0, N FDca CD O w �w o w ' ct o �"a N N a �9 C: C: 333 cQ to co ca cc cQ f l o c�—D N c�—D — n 0a w Q 0 = o= O 0= o Cl m �' co 3 .. w Z CL w N to CD ES 0, N FDca CD O w �w o w ' ct o �"a N N a r4\ N cn >a C) CD 3 0 � mbtn�'�� c,� �, �' o O r , CD o _, CD N 0 o CD Cn CD mS'1 O CD 0'a3 Qvaw� Q w m o 0�� 0 Z w o wco a' r rnn r CD m i c� ID C } a CDZ V N C N p N m 3 co�. � o I,n p CD ccDD cQ ;c a � c� �''I c v 1 - , " m N v 0 o O Cmn o m I M z c o v o: 0CD O� m I I I m ® O m m o Z m� $ a Q c m o° q a Z� c o` co m N CL go CD I I -Zi O O �� s 33 tCD 0 C n'G - Ll i5 i liZr ' .Jyy;A' u�lk � trcli 1 3 CL co Mr. Jerry McKinney. Page 9 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS Dichlorodifluoromethane Chloromethane Chloroethene (Vinyl chloride) Bromometh ane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Dichloromethane trans-1,2-Dichloroethene 1,1-Dichloroethane cis-1,2-Dichloroethene 2,2-Dichloropropane Chloroform Bromochloromethane 1,1,1 -Trichloroethane 1,1-Dichloro-l-propene Carbon tetrachloride 1,2-Dichloroethane 1,1,2 -Trichloroethene 1,2-Dichloropropane Bromodichloromethane Dibromomethane cis-1,3-Dichloro-l-propene trans-1,3-Dichloro-l-propene 1,1,2 -Trichloroethane 1,3-Dichloropropane Tetrachloroethene Dibromochloromethane 1,1,1,2 -Tetrachloroethane Bromoform 1,1,2,2 -Tetrachloroethane January 02, 1996 PACE Project Number: A512> 93 0156371 12/05/95 12/06/95 K80L-13 Units MDL #1033 DATE ANALYZED ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND -- 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/t 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95. ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 ug/L 1.0 ND 12/13/95 PANALYTMICALSERVI!CES,!INC.1 Mr. Jerry McKinney Page 10 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter Units ORGANIC ANALYSIS VOLATILE ORGANICS, 1,2,3-Trichloropropane ug/L Bromobenzene ug/L 2-Chlorotoluene ug/L .4-Chlorotoluene ug/L 1,3 -Dichlorobenzene ug/L 1,4 -Dichlorobenzene ug/L 1,2 -Dichlorobenzene ug/L 1,2-Dibromo-3-chloropropane ug/L 1,2,4-Trichlorobenzene ug/L Hexachlorobutadiene ug/L 1,2,3-Trichlorobenzene ug/L Benzene - ug/L Toluene ug/L Chlorobenzene ug/L Ethylbenzene ug/L Xylenes ug/L Styrene ug/L Isopropylbenzene ug/L n-Propylbenzene ug/L 1,3,5-Trimethylbenzene ug/L t-Butylbenzene . ug/L 1,2,4-Trimethylbenzene ug/L s-Butylbenzene ug/L 4-Isopropyltoluene ug/L n-Butylbenzene ug/L Naphthalene ug/L January 02, 1996 PACE Project Number: A5120. 93 0156371 12/05/95 12/06/95 K80L-13 MDL #1033 DATE ANALYZED 1.0 NO 12/13/95 1.0 ND 12/13/95- 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 3.0 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 °1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 1.0 ND 12/13/95 CA) m CD CD O c CD Q D CQ C DC7 -i-0 p Z a 3-0=6'0 0 C) n 000 CLWCD0C)^off p m =r LF o 0 Zen CAW CD =Q�.... � � —j CL � co z CD d ti i C o A -m m o icjo N f1? a O CCD + Ep �. n Z 'T o l — 0 cm m U fD f _ N' 71 O Z 0 0 O: Lim( CD ? n O 0 �0 �c CL N (D = cD f ty CD 0 O "* 72 = N . cn 3 CA O C fl. 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(D -• w 70 3 0 CD S o -m-I N � �� r, C ' Q. Q 3 4 rCL Cn CD '71 1 N ® w m m m 0- CD m�� c =- 00 ,oi Q -m Cn CD 0 CD (D c>3 m �o cn CD c� a 3 CD -0 CL a w 3 D C: (n c m � 0 �. z Z qr o. m cr (n cr m w o — 3 0 D ° @ CD Z CD c cn "a v D K w m ¢' N - o CD v Cl 3 Q\ 0 -0 o� -Tl -71 M D) O Ic mo CL N O w O 0 ZS (n :0 CCD N ^ nl;�Tllw 3 C c c 3 3 3 v r7 f w, Q -z 3 Cn CD I� cm d ao m On zzz v--00 c v "-Umvoco cnui'm n \ Oo p m D� .� m o� Z co m N Z O O COD z O p :9 Cl) (n :0 CCD N ^ 7 co c v CD v r7 f w, T CD T! N C CD fl CD I N C O R P O R A T E D THE ASSURANCE OF QUALITY Mr. Jerry McKinney Page 17 Client Reference: Coats American REPORT OF LABORATORY ANALYSIS May 02, 1995 PACE Project Number: A5041250; PACE Sample Number: ug/L 5.0 93 0079555 Date Collected: Dimethyl phthalate 'ug/L 04/11/95 Date Received: ��,..,4 ,. r-,,- 2, 6 -Deni trotol uene 04/11/95 Client Sample ID: NDk , K80L-13 Parameter Units MDL �QU ORGANIC ANALYSIS ug/L 6.0 ND�4'�,J BASE/NEUTRALS AND ACIDS Date Extracted, Base/Neutrals and Acids Date 4-Nitrophenol 041795 N-Nitrosodimethylamine ug/L 5.0 ND bis(2-Chloroethyl)ether ug/L 6.0 ND Phenol ug/L 5.0 ND 2 -Chlorophenol ug/L 5.0 ND 1,3 -Dichlorobenzene ug/L 5.0 ND 1,4 -Dichlorobenzene ug/L 5.0 ND 1,2 -Dichlorobenzene ug/L 5.0 ND bis(2-Chloroisopropyl)ether ug/L 6.0 ND Hexachloroethane ug/L 5.0 ND N-Nitrosodi-n-propylamine ug/L 5.0 ND Nitrobenzene ug/L 5.0 ND 3,5,5-Trimethyl-2-cyclohexanone ug/L 5.0 ND 2-Nitrophenol ug/L 5.0 ND 2,4 -Dimethylphenol ug/L 5.0 ND bis(2-Chloroethoxy)methane ug/L 5.0 ND 2,4-Dichlorophenol ug/L 5.0 ND 1,2,4-Trichlorobenzene ug/L 5.0 ND Naphthalene ug/L 5.0 ND Hexachlorobutadiene ug/L 5.0 ND 4-Chloro-3-methylphenol ug/L 5.0 ND Hexachlorocyclopentadiene ug/L 5.0 ND 2,4,6 -Trichlorophenol ug/L 5.0 ND 2-Chloronaphthalene ug/L 5.0 ND Acenaphthylene ug/L 5.0 ND Dimethyl phthalate 'ug/L 5.0 ND „ _ ��,..,4 ,. r-,,- 2, 6 -Deni trotol uene uggL 5.0 NDk , Acenaphthene 2,4-Dinitrophenol u L ug/L 5.0 42 ND ND `,7 �QU 2,4-Dinitrotoluene ug/L 6.0 ND�4'�,J MAY 2 3�99 4-Nitrophenol ug/L 5.0 NDI a s iter Section 54 Ravenscrott Drive An Equal Opportunity Employer Asheville, NC 28801 TEL: 704-254-7176 INC0RFDRATED REPORT OF LABORATORY ANALYSIS THE ASSURANCE OF QUALITY Mr. Jerry McKinney Page 18 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter Units MDL ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS May 02, 1995 PACE Project Number: A504125L 93 0079555 04/11/95 04/11/95 K80L-13 Fluorene ug/L 5.0 ND 4-Chlorophenyl. phenyl ether ug/L 5.0 ND Diethyl phthalate ug/L 5.0 ND 2-Methyl-4,6-dinitrophenol ug/L 24 ND N-Nitrosodiphenylamine ug/L 5.0 ND 4-Bromophenyl phenyl ether ug/L 5.0 ND Hexachlorobenzene ug/L 5.0 ND Pentachlorophenol ug/L 5.0 ND Phenanthrene ug/L 5.0 ND Anthracene ug/L 5.0 ND Di -n -butyl phthalate ug/L 5.0 ND Fluoranthene ug/L 5.0 ND Benzidine ug/L 50 ND Pyrene ug/L 5.0 ND Benzyl butyl phthalate ug/L 5.0 ND 3,3-Dichlorobenzidine ug/L 17 ND Benz[a]anthracene ug/L 8.0 ND Chrysene ug/L 5.0 ND bis(2-Ethylhexyl)phthalate ug/L 5.0 37 Di-n-octylphthalate ug/L 5.0 ND Benzo[b]fluoranthene ug/L 5.0 ND Benzo[k]fluoranthene ug/L 5.0 ND Benzo[a]pyrene ug/L 5.0 ND Indeno[1,2,3,-cd]pyrene ug/L 5.0 ND Dibenz[a,h]anthracene ug/L 5.0 ND Benzo[g,h,i]perylene ug/L 5.0 ND Surrogate - 2-Fluorophenol % 30 Surrogate - Phenol -d5 % 20 Surrogate - Nitrobenzene -d5 % 49 Surrogate - 2-Fluorobiphenyl % 48 Surrogate - 2,4,6-Tribromophenol % 74 54 Ravenscroft Drive Asheville, NC 28801 TEL: 704-254-7176 rnv — "1 1 L11 lu� MAY 2 31995 r..... . An Equal Opportunity Employer go -at —' I N C O R P O R A T E D THE ASSURANCE OF QUALITY Mr. Jerry McKinney Page 19 Client Reference: Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRALS AND ACIDS REPORT OF LABORATORY ANALYSIS Units MDL May 02, 1995 PACE Project Number: A5041250 93 0079555 04/11/95 04/11/95 K80L-13 Surrogate - Terphenyl-d14 % 63 VOLATILE ORGANICS Chloromethane ug/L 1.0 ND Bromomethane ug/L 1.0 ND Dichlorodifluoromethane ug/L 1.0 ND Chloroethene (Vinyl chloride) ug/L 1.0 ND Chloroethane ug/L 1.0 ND 1,1-Dichloroethene ug/L 1.0 ND Trichlorofluoromethane ug/L 1.0 ND Dichloromethane ug/L 1.0 ND trans-1,2-Dichloroethene ug/L 1.0 ND 1,1-Dichloroethane ug/L 1.0 ND 2,2-Dichloropropane ug/L 1.0 ND cis-1,2-Dichloroethene ug/L 1.0 ND Bromochloromethane ug/L 1.0 ND Chloroform ug/L 1.0 ND Dibromomethane ug/L 1.0 ND 1,1,1 -Trichloroethane ug/L 1.0 ND Carbon tetrachloride ug/L 1.0 ND 1,2-Dichloroethane ug/L 1.0 ND 1,1,2 -Trichloroethene ug/L 1.0 ND 1,1-Dichloro-l-propene ug/L 1.0 ND 1,2-Dichloropropane ug/L 1.0 ND Bromodichloromethane ug/L 1.0 ND trans-1,3-Dichloro-l-propene ug/L 1.0 ND cis-1,3-Dichloro-l-propene ug/L 1.0 ND 1,1,2 -Trichloroethane ug/L 1.0 ND 1,3-Dichloropropane ug/L 1.0 ND Tetrachloroethene ug/L 1.0 ND Dibromochloromethane ug/L 1.0 ND 1,1,1,2 -Tetrachloroethane ug/L 1.0 ND MAY 2 31995 54 Ravenscroft Drive An Equal Opportunity Employer Asheville, NC 28801 TEL: 704-254-7176 rAv 1— 1c1 .r— I N C O R P O R AT E D THE ASSURANCE OF QUALITY Mr, Jerry McKinney Page 20 Client Reference': Coats American PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS REPORT OF LABORATORY ANALYSIS Units MDL May 02, 1995 PACE Project Number: A504125C 93 0079555 04/11/95 04/11/95 K80L-13 Bromoform ug/L 1.0 ND 1,2,3-Trichloropropane ug/L 1.0 ND - 1,1,2,2 -Tetrachloroethane ug/L 1.0 ND Hexachlorobutadiene ug/L 1.0 ND Benzene ug/L 1.0 NO Toluene ug/L 1.0 ND Chlorobenzene ug/L 1.0 ND Ethylbenzene ug/L 1.0 ND Xylenes ug/L 1.0 ND Styrene ug/L 1.0 ND Isopropylbenzene ug/L 1.0 ND Bromobenzene ug/L 1.0 ND n-Propylbenzene ug/L 1.0 ND 2-Chlorotoluene ug/L 1.0 ND 4-Chlorotoluene ug/L 1.0 ND 1,3,5-Trimethylbenzene ug/L 1.0 ND t-Butylbenzene ug/L 1.0 ND 1,2,4-Trimethylbenzene ug/L 1.0 ND 1,3 -Dichlorobenzene ug/L 1.0 ND s-Butylbenzene ug/L 1.0 ND 1,4 -Dichlorobenzene ug/L 1.0 ND 4-Isopropyltoluene ug/L 1.0 ND 1,2 -Dichlorobenzene ug/L 1.0 ND n-Butylbenzene ug/L 1.0 ND 1,2,4-Trichlorobenzene ug/L 1.0 NDr4- Naphthalene ug/L 1.0 ND 1,2,3-Trichlorobenzene ug/L 1.0 NDIj MAY 2! 3199 JL it 1G Off 54 Ravenscroft Drive An Equal Opportunity Employer Asheville, NC 28801 TEL: 704-254-7176 r1v 1— X11 nr— CD 3_ ISO (a CD l CCD Y' IM c AU)cn -uSL)Dn 000 � N Q p N==_ 70-0 C SN @ te a _c2 :c ° 000 gm Z 0 Qj Q N CD � O (7 O a 00 CD N• � �3a� CD CD Q N uCDicDam Z n N 0 CL m O Q Sy (nz -n -n ! 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''m�mmm D�'0m 'S p � N Q p N==_ 'En; (� D N !� a N � O c, Z1 Z CD N• � 0 Sp su o 0 m w m CD=_0 N CD CD ! E --1 D CD Q CD �� N m„zzz vs cn -n m. O - (nrh S 0 N CD v X �. mV4 (n C -En-r �n o 0• CY* CD Co N, 3 - CD 0 CD ` o m g r �. ?° it w = C) 3 5T g CD M -< c N CD SD v 0 C * Z w g CD CD 0. � w v m4 TI n >,Z az CL CD 3 CD m crY p I: O mw�Vi CD c v CD =3 (D D w f -a 0 m (n m A K w h 'En; T1 N � O c, iry v CD fm CL0 0• v ?: m w c � v m„zzz z -n m. O - rn S 0 v mow ZA 0 �n 0( m CD -< n O COD w f -a 0 m (n o 'En; m m c, ET 0• v ?: m w c � m„zzz z O - S 0 mow ZA 0 0( m CD I I COD w O CD m a w v m4 c CD iv a o D m v -o m ' B 'En; O ET 0• v ?: a 0 O - COD 3'd P `e 3 3`3 CQ � CQ O :p Cn (n 5, 'ohCD o �o c s' °C "o 0 R. ,p T N N c °- w Z C,) K O z O M m 0 R P 0 R A T E RESORT OF ORATORY ANALYSIS ?HE ASSURANCE Of QUALITY Mr. Jerry McKinney Page 5 Client Reference: Coats American January 13, 1995 PACE Project Number: A41213507 PACE Sample Number: 93 0045944 Date Collected: 12/13/94 Date Received: 12/13/94 Client Sample ID: K80L-13 Parameter Units PRL 634-637 METHOD DATE ANALYZED TIME ANALYZED ORGANIC ANALYSIS DRINKING WATER REGULATED VOLATILES EPA 502.2 Benzene ug/L 0.5 ND 12/22/94 Carbon tetrachloride ug/L 0.5 ND 11:20 1,2-Dichloroethane ug/L 0.5 ND 1,2 -Dichlorobenzene ug/L 0.5 ND 1,4 -Dichlorobenzene ug/L 0.5 ND 1,1-Dichloroethene ug/L 0.5 ND c-1,2-Dichloroethene ug/L 0.5 ND t-1,2-Dichloroethene ug/L 0.5 ND Dichloromethane (Methylene Chloride) ug/L 1.4 ND 1,2-Dichloropropane ug/L 0.5 ND Ethylbenzene ug/L 0.5 ND Chlorobenzene ug/L 0.5 ND Styrene ug/L 0.5 ND Tetrachloroethene ug/L 0.5 ND Toluene ug/L 0.5 ND 1,2,4-Trichlorobenzene ug/L 0.5 ND 1,1,1 -Trichloroethane ug/L 0.5 ND 1,1,2 -Trichloroethane ug/L 0.5 ND Trichloroethene ug/L 0.5 ND Vinyl chloride ug/L 0.5 ND Xylenes`(total) ug/L 1.0 ND CBP (Surrogate Recovery) % 71 FB (Surrogate Recovery) 107 54 Ravenscroft Drive An Equal Opportunity Employer Asheville, NC 28801 TEL: 704-254-7176 FAX: 704-252-4618 I Ick 0) CD '0 Co (D 3 CD (D 0 D c 0 M.N 0 - oil o N 0 en a(D aro 3a d g� ro 0 (DD y (D c d 0 N 0 0 0 -2. 0 0 0 w CZ C]. m ro N N fil a 0 6 tD Z 0 CD CD' c� O S TT -1Ocl)-0 Oz C.)C)0 _�)DC�—I-a A0-0c=r-='O=vy Za)0ai: 000 WCDOC7^to!? _,;� 0 a �o c 06 D z30 �"0�`CDg�33 m-0 A r O 7 N C' O CCD 30 m w o n *3 nz 0 z O :3'� --1C1 r� ..[ p g -n -nQ a Q g,,m �4 3 `` 's a( °,,d O crno :Q� (D o O ^� m fn ct r `tea N CSD 0 a o CD r MCDCD 0 110 m C)-0 v c e Q o Nv 01 ca CDSt r m evm o m v �I„n m 0 o a � o "� CD `D O CD -n_ D� � F E N O &fh p CD CD n. n 3 m ('• v 0 S0 m CCD Q t� a Cn�y-g •• r N 3353333333c3 .L .l 003 c0(0 0cQcacQ(aca(acQ ;:i: (a 3 310 ZKK;rImm 0000m>-oZZ CQ (a CD c =' C1 A) W= r+ C '0 0 3 O O Mc� 0 m co u) a�co a n 0-o 3 6- �•3 oZZ 3Wmc� o..�.c3cvic,0rQ 0 CD 3`� 033 3�..� cD3 �' 0cnZ Z iQ J � 3 3 3 3 3 3 3 3 3 3 3 3 3 3 an (a cc (a cc cc (a cc cQ cQ cc ca cn cc cc 00 ,9N c0i CD CDLA (D 0(D . 7 n. o 3 o � � c O . a Q kA -0N-0Z p CD :3 _ 0 a o 0 NrZ CD o 0 CD CO CD CL m ccc 3�j 333 �' (Q Ct] CQ CQ CQ CQ m 0 Q CL Z N c CD �J cl) o nfCL)r 0) m CD O CD c�D CD c o m a o y— _= m-0 A r O 7 N C' O CCD n m w o n *3 nz 0 O O r- CD = <n <h� r� m C^D 1 " Z - a Q g,,m �4 3 `` 's a( °,,d 11 crno :Q� m � m p CA N Cf) ct r CD o 3 m o CD r MCDCD 0 Q m C)-0 v c co c m C z r m evm o m v �I„n m 0 o a � o "� CD `D O CD -n_ D� � F E N O &fh p CD CD n. n 3 m ('• v 0 S0 m CCD Q m 0 Q CL Z N c CD �J cl) o ni a m-0 A ,_, c m nz 0 z O D CD N CD w m z O O Z O m v MON N CD Q. c� (D 3 C�l Z 0 m o a) o_ CD Q. rA � rn 0 0 CL CD cD (D M —p I I =I I I I I I I P 33=;-3333333=33 cQ CQ O LQ CO CQ CQ CQ CQ CQ r+(0 6o3 3 3, ZKK;rll=-noo oow>mZZ �cQ cQ CD o W CD O ((D O O w w �c SO a=)(aUynO- c- o— 3ozZ mco o 3•c3��00 3W Cm (n 033 3�"� c 0 u 3 z —Z N � M C Ilk R ` C 3333333333333-33 00 0 m CD cn rrm O n � C7 3 0 c Q Q -0N-0Z p (D Q C � 0 0 N r- z 0 (D n QN O CD a c W a,Z z m 3 CD ,+-4 CA A 0 w CM/) CD 0 Dr�ZDJ , � 0 mW � Q o � .Q cu (D m m -" n-0 O o m In VuCD o c� 0 70 3 n vi m o w CD o m _0 vi cru m fJ EY O c m 0 Q 3 z �.` o �c z CD- ` — K 0 N C/) � o C/) y Ql0 C n� m 7t7 �ID 9 m Q m CDD � my, i cr CD %N 0 Ory p W Cr Cr CD m r 0 r m � CD 0 CD cy u m N h o ari v w M 03w3g -0_(D r- M Qn w -n o D ' v 0 ce c c CD o 'O N o �. v �` z ?: w cQ w CD CD 70 m m � R m w c v c 0 CD p z v> CD K 0 - =T Fn =3 =r cn -0 0 p m m cQ ". �H DQ 3 n LIN� , v hil -n ,n ,-i -• a,Z z m 3 CD ,+-4 CA A 0 w CM/) CD 0 z , m -" w m fJ EY O c m o �c z o — K 0 �7 co ��m z 7 y Ql0 C n� �ID w m CDD � 0 CDD m n o ari v w M e� C cD n w -n o D ' m o 'O N o ft^ v y• T `s ?: co m 0 co z , O _o cn cn 7 y Ql0 C n� �ID w r � r^ 9 m S.� 0 w m� 3�0 r n a' c c a 3 trj 0 LZ o Cl) m CD � r �o av O n C �Z M r m El M O m z 0 r n 3 0IL 3 n r m� ml vv0m r Vy a C Z g N � 0 c 3 (DQ p (D co m Z E a a d 0 Q \ 6� 3CD -a a � ZC -c w f 1 CD 110 o — TI D —I v wa 1 0 (A m �-0 70 0 D> wo cn 0 10-1w ®� D ) 44 -i o 0 �w m 3 ZOO 0 a o cn cm ® Cn p Z c -n O o m w r < 0 CC) c) c (D O Ti ?: CD v m C00 mss :3 �CCDCo Q°.A 0 mN x 0(fl CD p < A m 0 O 0 S 0 G) � O - m (D N O y ° 0 O _ m Ami 7 < O 0 m N c N m .U. 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CD ` N Ca O: p o 's CD 0 n S N CL 3 Q1; 35 ri Z n �o a3-3 neo Zn3 Cv� 0 o© "1 nC � CD 0.a P� (D 71 CD Z a m m c Q 0 C El i n m r M a -o z� m O m p C: m —I Ct) m o z = m CD o CL `c C1 6 O CDc 3 mc 1 Ti 3 f - co cn 3 CD O C: N' 2 C1 0 v_ N 0 Zv 00 m^ <o MR Z- C Z<Z 0 O m=� D� S Z =' 2 0 Im m c y�zti 0 c C; vM >� m� M o m n 0 Z SEMIVOLATILE ORGANICS REPORT — DEM LAB LAS NUMBER: 4G138 SUPERVISOR LAB ": 4G138 DATE REPORTED BY SYS / CHECKED BY ENTERED BY REVIEWED BY CHECKED BY SAMPLE TYPE: WATER DILUTION FACTOR CONC, CAS NUMBER TQL ANALYTE NAME UG i L X 108-95-2 10 PHENOL tT 111-44-4 10 BIS(2—CHLOROETHYL) ETHER U 95-57-8 10 2—CHLOROPHENOL U 541-73-1 io 1,3—DICHLOROBENZENE tT 106-4h-7 10 1 , 4-DICTHL OROBENZENE U 100-51-6 20 BENZYL ALCOHOL U y5-50-1 10 ;,2—DICHLOROBENZENE U y5-48-7 10 2—METHYL PHENOL U 108-50-1 10 B_S(2-CH_LORO±SOPROPYL) ETHER tT 106-44-5 10 4—METHYL PHENOL U 621-64-7 10 N—NITROSO—DI—N-PROPYLAMINE it fi 7-72-1 10 HEXACHL0ROETHAN B tr 98-95-: "i0 NTTROBENZENE U 78—:59-1 10 TSOPHORONE tr $8-75-5 10 2—NITRO PHENOL U 105-67-9 10 2,4—DIMETHYL PHENOL tr 65-85-0 50 BENZOIC. ACID U 111-91-1 10 BTSi2—CHLOROETHOXYi METHANE U 120-83-2 10 2;4—DICHLORO PHENOL U 120-82-1 10 1,2,4-TRICHLOROBENZENE U 91-20-3 10 NAPHTH_ALElf:E U 1-06-47-8 20 4—CHLOROA.NIL INE U — u-3 10 HEXACHLOROBUTADIENE U 59-50-7 20— —A—CHLORO-3-METHYL PHENOL rT 91-57-6 10 2—METHYL NAPHTHALENE U 77-47-4 10 Z�XACHLOROCYCLOPENTADIENE U 88-06-2 10 2,4;6—TRICHLORO PHENOL tT y5-95-4 10 2,4,5—TRICHLO_R_O PHENOL U 91-58-7 10 2 --CHLORO NAPHTHALENE U 88-74-4 50 2—NITROA14ALINE U 131-11-3 10 DIMETHYL PHTL +SATE U 208-96-3 10 ACENAPHTHYLENE U 606-20-2 10 2,5—DINITROTOLUENE U 99-09-2 50 3—N'TTROANALINE U 83-32-9 10 A"-.ENAPHTHENE tT 51-28-5 50 2,?—DINITRO PHENOL, t_r 1-00-02-7 50 —NITRO PHENOL U 132-64-9 1 () DIBENZOFURfiN U 1-21-14-2 10 2, 4—DINITROTOL rTENE U 84-66-2 10 DIETHYL PHTHJ;A,LATE it 1005— (>-: l C) =-f HT QR_OP4E-,IV7 P_- NYL ETHER 11 t 00-0? — titin =—NTTROAN TnL= TARGET QUANTTTATION LIMIT T= TENTATIVELY IDENTIFIED ESTIMATED CONCENTRATION B= ESTIMATED CONCENTRATION U= COMPOUND ANALYZED FOR NOT DETECTED N= COMPOUND NOT Al�ALYZED FOR Ejj-TTI I D= DETECTED BELOW IJNTITA=-'T LIMIT H= T-4-0LDING TIME EX-7EEDED TQ_ .91,JBJECT, TO C'H_A_NGE DUE TIC -._N3T_,RUME_-,!T -SENSITIVITY SEMIVOLATILE ORGANICS REPORT DEM LAB 86-30-6 10 N-NITROSODIPHENYLAMINE U 101-55-3 10 4-BROMOPHENYL PHENYL ETHER U 118-74-1 10 HEXACHLOROBENZENE U 87-86-5 50 PENTACHLORO PHENOL U 85-01-8 10 PHENANTHRENE U 120-1-2-7 10 ANTHRACENE U 84-74-2 10 DI -N -BUTYL PHT14-ALATE 11 206-44-0 10 FLUORANTHENE U 12-9-00-0 1-0 PYRENE U 85-68-7 10 BUTYLBENZYL PHTHALATE U 91-94-1 20 3,31-DICHLOROBENZIDINE U -56-55-3 10 BENZO(A)ANTHRACENE u 218-01-9 10 CHRYSENE T-1 117-81-7 10 BIS(2-ETHYLHEXYL) PHTHALATE U 117-84-0 10 DI-N-OCTYL PHTHALATE U 205-99-2 10 BENZO(B)FLUORANTHENE U 207-08-9 10 BENZO jK:)FLUOR_ANTHENE U 50-32-8 10 BENZO(A)PYRENE 11 193-3q-5 1-0 INDENO('L;,2;.3-CD)PYRENE U 53-70-3 10 DIBENZO(AjH)A_NTHRACENE U 141-24-2 10 BENZO(G,H,I)PERYLENE U OTHER SEMIVOLATILE ORGANICS FOR SAMPLE NUMBER 4G138 BUTOXYETHOXY ACETATE ETHANOL ClO.H20.04 2-2 T TnL= TARGET QUANTTTATION LIMIT T= TENTATIVELY IDENTIFIED ESTIMATED CONCENTRATION B= ESTIMATED CONCENTRATION U= COMPOUND ANALYZED FOR NOT DETECTED N= COMPOUND NOT Al�ALYZED FOR Ejj-TTI I D= DETECTED BELOW IJNTITA=-'T LIMIT H= T-4-0LDING TIME EX-7EEDED TQ_ .91,JBJECT, TO C'H_A_NGE DUE TIC -._N3T_,RUME_-,!T -SENSITIVITY -'� GHRH/DEN LABORATORY VOLATILE ANALYTICAL REPORT � -leo TED BY J' SUPERVISOR CHECKED BY DATE 3 � REVIEWED BY � ENTERED BY CHECKED BY SAMPLE TYPE: WATER ANALYSIS RESULTS CAS# VOA TARGET COKPOURD qL DETECTED CAS# VOA TARGET COKPOUND TQL DETECTED g/l u Ig 1 Dg/l ug/1 75-35-4 1,1-Dichloroethene 0.75 U 96-18-4 1,2,3-Trichloropropane 0.25 U 75-09-2 Kethylene Chloride 0.25 U 108-86-1 Broiobenzene 1 U 156-60-5 trans-1,2-Dichloroethene D.75 U 95-49-8 2-Chlorotoluene 0.25 U 75-34-3 1,1-Dirhloroethane 3.25 U 106-43-4 4-Chlorotoluene 0.25 0 590-20-7 2,2-Dichloropropane 1.25 U 541-73-1 1,3 -Dichlorobenzene 0.25 7 156-59-4 cis-1,1-Dichloroethene 0.25 U 106-46-7 1,4 -Dichlorobenzene 0.25 D 67-66-3 Chlorofori ?.25 U 95-50-1 1,2 -Dichlorobenzene 0.25 U 74-97-5 Broiochloroiethane 0.75 U . 36-12-8 1,2-Dibroio-3-Chloropropane i U 71-55-6 1,1,1 -Trichloroethane 1.25 U- 120-82-1 1,2,4-Trichlorobenzene 0.25 U 563-58-6 1,1-Dirhloropropene 1.25 U 37-68-3 Hexachlorobutadiene 0.25 U 56-23-5 Carbon Tetrachloride 1.75 U 87-61-6 1,2,3-Trichlorobenzene 0.75 U 107-06-2 1,2-Dichloroethane 0.25 U 1634-04-4 Kethyl-tert-butyl ether 5 U 79-01-6 Trichloroethene 3.25 U 71-43-2 Benzene 1 U 78-87-5 1,2-Dichloropropane 3.25 0 108-88-3 Toluene i I 75-27-4 Broiodichloroiethane 0.25 U 100-41-4 Ethyl benzene 1 U 74-95-3 Dibromethane i U 108-38-3 n,p-1ylenes_ 2 U 10061-01-5 cis-1,3-Dichloropropene 0.25 U 95-47-6 o-iylene 1 U 10061-02-6 trans-1,3-Dichloropropene 0.25 U 100-42-5 Styrene 1 U 79-04-5 1,1,2 -Trichloroethane 0.25 D 98-82-8 Isopropylbenzene 1 U 127-18-4 Tetrachloroethene D.25 U 103-65-1 n-Propylbenzene 1 U 142-28-9 1,3-Dichloropropane 1.25 U 108-67-8 1,3,5-Triiethylbenzene 1 U 124-48-1 Dibroiochloroiethane x`.75 U 98-06-6 tert-Butylbenzene 1 U 106-93.4 1,2-Dibroioethane 1 U 95-63-6 1,2,4-Triiethplbenzene 1 U 108-90-7 Chlorobenzene 11J.25 U 135-98-8 sec-Butylbenzene 1 630-20-6 1,1,1,2 -Tetrachloroethane 1.25 D 99-87-6 p-isopropyltoluene i 1.5 75-25-2 Broiofori 0.5 U 104-51-8 n-Butylbenzene 1 U 79-34-5 1,1,2,2 -Tetrachloroethane r.75 U 91-20-3 Naphthalene 1 U TQL- Target Quantitation Likt- Su -Meet to Other purgeables detected Detected change due to instruient sen:-ti7ity (up to 10 highest peaks) ug/l T- Tentati7ely Identified, not "nfiried E- Estiiated Value U- Saiples analyzed for this ccrcund but not detected N- Saiple not analyzed for this %�ipound D- Detected below quantitation :Jit X- GC/KS Analysis perforied COl�NTS: �o-0 c =r �)D�o I ST0 CD � � QO5..O-0 0 0 0 Z n C7 C � (D c Q ,I 0 0 o -n -n N ID 8- qo to f,y'< 333333333 3` 003 cQ co o co co co co co co co ,=.- cD 3 = zKKX:c-n00�C��oD�zz �zco �cDcW 3� S comm 3 >-0 m �— W CD 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C' cnpc0 O�mW m m o w m c m z b s r: o m z O -ucn C --a : CD 5, 0ar c a - s o c c c 3 3 3 I a I co cQ co co co co z C6 CD CD O o n' CD i—�U)Cl) `0:L 0>C� Z W CD =;;CD N (� O O °CMD n Q z30 CD 0 0 Cl o CL 0 33533,33333533 003 (a (a 0n(acn(a(amc0 ;:;cQ33, cc zKK;rlsca CD c � � �.D=r =3 (a _ ' 0� CSD c�Ka inn Eo'Z W CD o 03 0-Z'c'3.2 ZO CD � 3 o � Pzz -0 \1 333333333333333 co(a(acncc(acac0(acacQ(a(acQc0 ®� N 25rN 0. N Z _ moo 0 (n 1 1 CO CO CO CO CO cO rpTI,;Z CDD_CD C WO QAC cT.. _= n' � CnCL � lv O CD 3 o i 0 _D c/) ro O _ =3 r� �2 3— Z,� 3i 0 f �• CD Cn c C °- m Aj � F CD �+ mCD 0_I na= p a 0- In 2c ro DL I m .z D C4 "a t�D O \ K lr, c� O a o m � m w mm10 0 C 9Fa -I m oO C D �moW p�in'm D a? 0CD SD D ro 0 CA r� m c o o _ 0 �. m v cr s 0 m � lv O i 0 _D c/) N F 0 c �2 r 0 f �• CD c C °- m i. 'F r o H A i t o --ht ASSUHANLt 0 U U A I I I I Coats American P.O. Box 368 Hwy 221 N. Marion, NC 28652 Attn: Mr. Jerry McKinney Client Reference: Monitoring Wells PACE Sample Number: Date Collected: Date Received: Client Sample ID: ORGANIC ANALYSIS VOLATILE ORGANICS IN WATER -METHOD 502.2 Chloromethane Bromomethane Dichlorodifluoromethane Dichlorodifluoromethane Vinyl chloride Chloroethane REPORT OF U4dORATORY ANALYSIS April 16, 1993 PACE Project Number: A30325; 93 0021107 93 0021115 93 002112- 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 K80L-2 K80L-12 K80L-13 Units MDL ug/L 0.5 NO ND ND ug/L 0.5 ND ND ND ug/L 0.2 - - ND ug/L 0.5 ND ND - ug/L 0.5 ND ND ND ug/L 0.5 ND ND ND 1,1-Dichloroethylene ug/L 0.5 ND 1.3 ND Trichlorofluoromethane ug/L 0.5 ND ND ND Methylene chloride ug/L 0.5 ND ND ND trans-1,2-Dichloroethylene ug/L 0.5 ND ND ND 1,1-Dichloroethane ug/L 0.5 ND ND ND 2,2-Dichloropropane ug/L 0.5 ND ND NO cis-1,2-Dichloroethylene ug/L 0.5 ND ND ND Bromochloromethane ug/L 0.5 ND ND ND Chloroform ug/L 0.5 2.6 ND ND Dibromomethane ug/L 0.5 ND ND ND 1,1,] -Trichloroethane ug/L 0.5 ND ND ND Carbon tetrachloride ug/L 0.5 ND ND NO 1,2-Dichloroethane ug/L 0.5 ND ND ND 1,1,2 -Trichloroethylene ug/L 0.5' ND ND ND 1,1-Dichloro-l-propene ug/L 0.5 ND NO ND 1,2-Dichloropropane ug/L 0.5 ND ND ND Bromodichloromethane ug/L 0.5 ND ND ND 2-Chloroethylvinyl ether ug/L 0.5 ND ND ND trans-1,3-Dichloro-l-propene ug/L 0.5 ND ND ND cis-1,3-Dichloro-l-propene ug/L 0.5 ND ND NO 1,1,2 -Trichloroethane ug/L 0.5 ND ND ND 1,3-Dichloropropane ug/L 0.5 ND ND ND 54 Ravenscroft Drive Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina An Equal Opportunity Employer Asheville, NC 28801 Tampa, Florida Asheville, North Carolina TEL: 704.254.7176 Iowa City, Iowa New York, New York FAX: 704252.4618 San Francisco, California Pittsburgh. Pennsylvania Kansas City, Missouri Denver, Colorado Los Angeles, California REPORT OF BORATORY ANALYSIS .. I H i A,l j li H Ah L'1 U! UUAl1 Mr. Jerry McKinney April 16, 1993 Page 2 PACE Project Number: A303i Client Reference: Monitoring Wells PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS IN WATER -METHOD 502.2 Units MDL 93 0021107 93 0021115 93 002112 03/25/93 03/25/93 03/25/93 03/25;93 03/25/93 03/25/93 K80L-2 K80L-12 K80L-13 1,1,2,2 -Tetrachloroethylene ug/L 0,5 ND ND 0.56 Dibromochloromethane ug/L 0.5 ND ND ND 1,2-Dibromoethane ug/L 0.02 ND ND ND 1,1,1,2 -Tetrachloroethane ug/L 0.5 ND ND ND Bromoform ug/L 0.5 ND ND ND 1,2,3-Trichloropropane ug/L 0,5 ND ND ND 1,1,2,2 -Tetrachloroethane ug/L 0.5 ND ND ND 1,2-Dibromo-3-chloropropane ug/L 0.02 - ND ND 1,2-Dibromo-3-chloropropane ug/L 0.5 ND- Hexachlorobutadiene ug/L 0.02 ND - - Hexachlorobutadiene ug/L 0.5 - ND ND Methyl tert-butyl ether ug/L 0.5 ND ND ND Benzene ug/L 0.5 ND ND ND Toluene ug/L 0.5 ND ND ND Chlorobenzene ug/L 0.5 ND ND ND Ethyl benzene ug/L 0.5 ND ND ND Xylenes ug/L 0.5 ND ND ND Styrene ug/L 0.5 ND ND ND Cumene ug/L 0.5 ND ND ND Bromobenzene ug/L 0.5 ND ND ND n-Propylbenzene ug/L 0.5 ND ND ND 0-Chlorotoluene ug/L 0.5 ND ND ND p-Chlorotoluene ug/L 0.5 ND ND ND 1,3,5-Trimethylbenzene ug/L 0.5 ND ND ND tert-Butylbenzene ug/L 0.5 ND ND ND 1.2,4-Trimethylbenzene ug/L 0.5 ND ND ND M -Dichlorobenzene ug/L 0.5 ND ND ND sec-Butylbenzene ug/L 0.5 ND ND ND 1,4 -Dichlorobenzene ug/L 0.5 ND ND ND p-Cymene ug/L 0.5 ND ND ND 0 -Dichlorobenzene ug/L 0.5 ND ND ND 54 Ravenscrott Drive An Equal Opportunity Employer Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina Asheville, NC 288D1 Tampa, Florida Asheville, North Carolina TEL: 704-254-7176 Iowa City, Iowa New York, New York FAX: 704252-4618 San Francisco, California Pittsburgh, Pennsylvania Kansas City, Missouri Denver, Colorado Los Angeles, California -'0 R P 0 R A T E BVW -r 41 ASS UA ANCI OF 0UAIiIY Mr. Jerry McKinney Page 3 Client Reference: Monitoring Wells PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS VOLATILE ORGANICS IN WATER -METHOD 502.2 REPORT OFQBORATORY ANALYSIS, April 16, 1993 PACE Project Number: A303L 93 0021107 93 0021115 93 002112 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 K80L-2 K80L-12 K80L-13 Units MDL n-Butylbenzene ug/L 0.5 ND NO ND 1,2,4-Trichiorobenzene ug/L 0.5 ND NO ND Napthalene ug/L 0.5 ND ND ND 1,2,3-Trichlorobenzene ug/L 0.5 ND ND ND SEMIVOLATILE ORGANICS -625A 4-Chloro-3-methylphenol ug/L 10 ND ND - 4-Chloro-3-methylphenol ug/L 11 - - ND 2 -Chlorophenol ug/L 10 ND ND - 2 -Chlorophenol ug/L 11 - - ND 2,4-Dichlorophenol ug/L 10 ND ND - 2,4-Dichlorophenol ug/L 11 - - ND 2,4 -Dimethylphenol ug/L 10 ND ND - 2,4 -Dimethylphenol ug/L 11 - - ND 2,4-Dinitrophenol ug/L 51 - ND - 2,4-Dinitrophenol ug/L 52 ND - - 2.4-Dinitrophenol ug/L 53 - - ND 2-Methyl-4,6-dinitrophenol ug/L 51 - ND - 2-Methyl-4,6-dinitrophenol ug/L 52 ND - - 2-Methyl-4,6-dinitrophenol ug/L 53 - - ND 2-Nitrophenol ug/L 10 ND ND - 2-Nitrophenol ug/L 11 - - ND Pentachlorophenol ug/L 10 ND ND - Pentachlorophenol ug/L 11 - - ND Phenol ug/L 10 ND ND - Phenol ug/L 11 - - ND 2,4,6 -Trichlorophenol ug/L 10 ND ND - 2,4,6 -Trichlorophenol ug/L 11 - - ND BASE/NEUTRAL SEMIVOLATILE ORGANICS -625B Acenaphthene ug/L 10 ND ND - Acenaphthene ug/L 11 - - ND Acenaphthylene ug/L 10 ND ND - 54 Ravenscrolt Drive Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina An Equal Opportunity Employer Asheville, NC 28801 Tampa, Florida Asheville, North Carolina TEL: 704254.7176 Iowa City. Iowa New York, New York FAX`: 104.252.4618 San Francisco, California Pittsburgh, Pennsylvania A Kansas City, Missouri Denver, Colorado Los Angeles, California _.�(�► REPORT F F F i t RBORATORY ANALYSIS' uJ.UnAAL[ UI U U A LI!1 Mr. Jerry McKinney Page 4 Client Reference: Monitoring Wells PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRAL SEMIVOLATILE ORGANICS -625B April 16, 1993 PACE Project Number: A3O3L 93 0021107 93 0021115 93 00211:: 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 K80L-2 K80L-12 K8OL-13 Units MDL Acenaphthylene ug/L 11 - - ND Anthracene ug/L 10 ND ND - Anthracene ug/L 11 - - ND Benzo(a)anthracene ug/L 10 ND ND - Benzo(a)anthracene ug/L 11 - - ND Benzo(a)pyrene ug/L 10 ND ND - Benzo(a)pyrene, ug/L 11 - - ND Benzo(b)fluoranthene ug/L 10 ND ND - Benzo(b)fluoranthene ug/L 11 - - ND Benzo(k)fluoranthene ug/L 10 ND ND - Benzo(k)fl,uoranthene ug/L 11 - - ND Benzo(g,h;i)perylene ug/L 10 ND ND - Benzo(g,h,i)perylene ug/L 11 - - ND Bis(2-chloroethoxy)methane ug/L 10 ND ND - Bis(2-chloroethoxy)methane, ug/L 11 - - ND Bis(2-chloroethyl)ether ug/L 10 ND ND - Bis(2-chloroethyl)ether ug/L 11 - - ND Bis(2-chloroisopropyl)ether ug/L 10 ND ND - Bis(2-chloroisopropyl)ether ug/L 11 - - ND Bis(2-ehtylhexyl)phthlate ug/L 10 ND ND - Bis(2-ehtylhexyl)phthlate ug/L 11 - - 20 4-Bromophenol phenyl ether ug/L 10 ND ND - 4-Bromophenol phenyl ether ug/L 11 - - ND Benzyl butyl phthalate ug/L 10 ND ND - Benzyl butyl phthalate ug/L 11 - - ND 2-Chloronaphthalene ug/L 10 ND ND - 2-Chloronaphthalene ug/L 11 - - ND 4-Chlorophenyl phenyl ether ug/L 10 ND ND - 4-Chlorophenyl phenyl ether ug/L 11 - - ND Chrysene ug/L 10 ND ND - Chrysene ug/L 11 - - ND 54 Ravenscroft Drive Asheville, NC 2BB01 Offices Serving: Minneapolis. Minnesota Tampa, Florida Charlotte, North Carolina Asheville, North Carolina An Equal Opportunity Employer TEL: 704.2547176 FAX: 704-2524616 Iowa City, Iowa San Francisco, California New York, New York Pittsburgh, Pennsylvania Kansas City. Missouri Denver, Colorado Los Angeles, California .--C C H P 0 R A T E 6 E ASSURANC.E 0f 0UA 7 Mr. Jerry McKinney Page 5 Client Reference: Monitoring Wells PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRAL SEMIVOLATILE ORGANICS -625B Dibenzo(a,h)anthracene Dibenzo(a,h)anthracene 1,2 -Dichlorobenzene 1,2 -Dichlorobenzene 1,3 -Dichlorobenzene 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene 1,4 -Dichlorobenzene 3,3-Dichlorobenzidine Diethyl phthalate Diethyl phthalate Dimethyl phthalate REPORT OF BORATORY ANALYSIS, Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L April 16, 1993 PACE Project Number: A303e, 93 0021101 93 0021115 93 002112 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 K80L-2 K80L-12 K80L-13 MDL 10 11 10 11 10 11 10 11 21 10 11 10 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND Dimethyl phthalate ug/L 11 - - ND Di -n -butyl phthalate ug/L 10 ND ND - Di -n -butyl phthalate ug/L 11 - - ND 2,4-Dinitrotoluene ug/L 10 ND ND - 2,4-Dinitrotoluene ug/L 11 - - ND 2,6-Dinitrotoluene ug/L 10 ND ND - 2,6-Dinitrotoluene ug/L 11 - - ND Di-n-octylphthalate ug/L 10 ND ND - Di-n-octylphthalate ug/L 11 - - ND Fluoranthene ug/L 10 ND ND - Fluoranthene ug/L 11 - - ND Fluorene ug/L 10 ND ND - Fluorene ug/L 11 - - ND Hexachlorobenzene ug/L 10 ND ND - Hexachlorobenzene ug/L 11 - - ND Hexachlorobutadiene ug/L 10 ND ND - Hexachlorobutadiene ug/L 11 - - ND Hexachloroethane ug/L 10 ND ND - Hexachloroethane ug/L 11 - - ND 54 Ravenscroft Drive Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina An Equal Opportunity Employer Asheville. NC 28801 Tampa, Florida Asheville, North Carolina TEL: 704-254-7176 Iowa City, Iowa New York, New York FAX: 704 252.4618 San Francisco, California Pittsburgh, Pennsylvania Kansas City, Missouri Denver, Colorado Los Angeles, California O R P D F g1 E coREPORT OF �� ORATORY ANALYSIS`,, .%- ?M! ASSURAN t.! UI U U A I I I V Mr. Jerry McKinney April 16, 1993 Page 6 PACE Project Number: A3O32` Client Reference: Monitoring Wells PACE Sample Number: Date Collected: Date Received: Client Sample ID: Parameter ORGANIC ANALYSIS BASE/NEUTRAL SEMIVOLATILE ORGANICS -625B Units MDL 93 0021107 93 0021115 93 00211_ 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 03/25/93 K8OL-2 KBOL-12 K8OL-13 Indeno(1,2,3,-cd)pyrene ug/L 10 ND ND - Indeno(1,2,3,-cd)pyrene ug/L 11 - - ND Isophorone ug/L 10 ND ND - Isophorone ug/L 11 - - ND Naphthalene ug/L 10 ND ND - Naphthalene ug/L 11 - - ND Nitrobenzene ug/L 10 ND ND - Nitrobenzene ug/L 11 - - ND N-Nitrosodi-n-propylamine ug/L 10 ND ND - N-Nitrosodi-n-propylamine ug/L 11 - - ND N-Nitrosodiphenylamine ug/L 10 ND ND - N-Nitrosodiphenylamine ug/L 11 - - ND Phenanthrene ug/L 10 ND ND - Phenanthrene ug/L 11 - - . I ND Pyrene ug/L 10 ND ND - Pyrene ug/L 11 - - ND 1,2,4-Trichlorobenzene ug/L 10 ND ND - 1,2,4-Trichlorobenzene ug/L 11 - - ND Hexachlorocyclopentadiene ug/L 10 ND ND - Hexachlorocyclopentadiene ug/L 11 - - ND N-Nitrosodi-n-methylamine ug/L 10 ND ND - N-Nitrosodi-n-methylamine ug/L 11 - - ND 54 Ravenscrolt Drive Offices Serving: Minneapolis, Minnesota Charlotte, North Carolina Asheville. NC 28801 Tampa, Florida Asheville, North Carolina TEL: 704254.7176 Iowa City, Iowa New York, New York FAX: 704252.4618 San Francisco, Calilornia Pittsburgh, Pennsylvania Kansas City, Missouri Denver, Colorado Los Angeles, California An Equal Opportunity Employer �o-� c �� )DC7�� Po C) o = „ RRC) Z�nCD��c�'� Q CD 3 0 CL co 0s rja rQ N � 33=333333353 003 ca CO o ca ca to ca to ca ca ;:;:(a3 3 cQ Zr.Kxm-poCJ o DmZZ W H ca ca (D c =r CD CD � ,C�C� � o ^ Z CD ate'_3 z 3 �3 30�c�n �ZZ t a 333333333333333 ca co ca ca co caca(acncaco(a(a(a(a —Z N R (� rte^ �Z so C/5 aa�,0 m CD 0 m'� 0 CD y CD o c p o N ca C C m Z 0 C .m K o� N 51 11/ 4= "e Z,F t �o-� c �� )DC7�� Po C) o = „ RRC) Z�nCD��c�'� Q CD 3 0 CL co 0s rja rQ N � 33=333333353 003 ca CO o ca ca to ca to ca ca ;:;:(a3 3 cQ Zr.Kxm-poCJ o DmZZ W H ca ca (D c =r CD CD � ,C�C� � o ^ Z CD ate'_3 z 3 �3 30�c�n �ZZ t a 333333333333333 ca co ca ca co caca(acncaco(a(a(a(a —Z N R (� rte^ �Z so C/5 aa�,0 cmc 33 (Q(Q� rpm�m m m o c >`n p a or CD 3 o �' Z ?F CD oo U = �0p z •Y `$c3 CO �' .c FoFp— Ao��' s iT CD a: 0�Q (Dv a' r cn c N '54) t C0 A D� :3 8 _0 o' N � 7 CD �i ft 1-1 a N a 0 Z 0 W ON • CD �I 0 0 CD IOL) Dom, CL z ED- EP) CD 50 m Dm C !=i m - C vop� �m0coo �nCl)y m r m s 0 mm c m 0 m 0 Z 0 m ° z pcn m s s, . g. p C o o Vi c N c °- 0 CD 3 o m _. C) 51 cmc 33 (Q(Q� rpm�m m m o c >`n p a or CD 3 o �' Z ?F CD oo U = �0p z •Y `$c3 CO �' .c FoFp— Ao��' s iT CD a: 0�Q (Dv a' r cn c N '54) t C0 A D� :3 8 _0 o' N � 7 CD �i ft 1-1 a N a 0 Z 0 W ON • CD �I 0 0 CD IOL) Dom, CL z ED- EP) CD 50 m Dm C !=i m - C vop� �m0coo �nCl)y m r m s 0 mm c m 0 m 0 Z 0 m ° z pcn m s s, . g. p C o o Vi c N c °- COMMONWEALTH LABORATORIES OF S.C., INCORPORATED P. O. BOX 16387 209 WEST ANTRIM DRIVE GREENVILLE, SOUTH CAROLINA 29606-6387 AREA CODE 803 TELEPHONE: 271-3256 FAX: 803-235-8340 Page 6 CERTIFICATE OF ANALYSIS Coats American Sample ID No. Parameter 92-34-7614 Date Analyst Time *Priority Pollutant Volatiles EPA 8240 1/6/93 JRU 1919 1,1,1 -Trichloroethane, ppb <2.00 1,1,2,2 -Tetrachloroethane, ppb <2.00 1,1,2 -Trichloroethane, ppb <2.00 1,1-Dichloroethane, ppb <2.00 i,l-Dichloroethylene, ppb <2.00 1,2 -Dichlorobenzene, ppb <2.00 1,2-Dichloroethane, ppb <2.00 1,2-Dichloropropane, ppb <2.00 1,2-trans-Dichloroethylene, ppb <2.00 1,3 -Dichlorobenzene, ppb <2.00 1,4 -Dichlorobenzene, ppb <2.00 2-Chloroethylvinyl ether, ppb <2.00 Acrolein, ppb <20.0 Acrylonitrile, ppb <20.0 Benzene, ppb <2.00 Bromoform, ppb <2.00 Carbon Tetrachloride, ppb <2.00 Chlorobenzene, ppb <2.00 Chlorodibromomethane, ppb <2.00 Chloroethane, ppb <2.00 Chloroform, ppb <2.00 Dichlorobromomethane, ppb <2.00 Dichlorodifluoromethane, ppb <2.00 Ethylbenzene,ppb <2.00 Methyl Bromide, ppb <2.00 Methyl Chloride, ppb <2.00 Methylene Chloride, ppb <2.00 Tetrachloroethylene, ppb <2.00 Toluene, ppb <2_00 Trichloroethylene, ppb <2.00 Trichlorofluoromethane, ppb <2.00 Vinyl chloride, ppb <2.00 cis-1,3-Dichloropropylene ppb <2.00 trans-1,3-DichloropryleMw pbt <2.00 Sample Markings r C Location:` #K 3 #290 Date: i 1 1/?2 Time: 1 k Collected bl�i,f' <y lip Pittman Type sample:-- South Carolina Lab Identification No. 23101 -North Carolina Certification No. 24 * Outside Laboratory Certification No. 10120 i o D co ° C= 07 a c� m U 70 ?" c c po r a O -� Z - D� > c > Dv 2s ' z00 �o mo CD H CO ^ , (j)acQ (D O w w So x z CD A c 0 0 �0 � Q O $ n o e- (D �� CD W Cl) V o p fD N F 0 Q m S S Mo 0 z `^ <D CD 0 - A y y 0 w ca 07 mm ro. o V s mx a0,o yho (D N C N CDN ca w w n - 17cn0r0 t11 m 7_ c p\n C cD y d 3 m Z u �ZZ W > m 0 o n N n c3 o tp 0 CD 3 CL CDD w N 2. ZEN m m z m (D � � m Is o D co ° C= 07 a c� m U 70 ?" c c po r a O o Z a u Z D� :3 Dv 2s ' �o mo CD H CO ^ , So D C/) c 0 0 �0 � z D O $ n o e- (D �� s m W Cl) ^ ti o 0 O '` O 0 w m Q. CL Mo 0 z `^ <D CD w o V O 0 � 17cn0r0 t11 m w w o g p\n C .� 3 3 a 3 m Z u �ZZ m rtt o n c3 El 0 CD 3 2. ZEN m m z (D � m Fi O o v o � v CD CD CD a m Z c=D m_ Q c o mo H ° CO ^ v_ N_ O zo O( Z� m� z Cm Z S. z moo Z C) C) m m Mo y m_ o_ C) Z m O� C Cm cvm C y C N� m q O Z EHNR/DEM LABORATORY VOLATILE ANALYTICAL REPORT K0. 2G 1565 REPORTED BY CHECKED BY REVIEWED BY SAMPLE TYPE; WATER ANALYSIS RESULTS CASv VOA TARGET COMPOUND TQL DETECTED Bromobenzene 1 ua/1 uq; l 0.25 106-43-4 4-Chlorotoluene 0.25 75-35-4 1,1-Dichloroethene 0.75 U 75-09-2 Methylene Chloride 0.25 U 156-60-5 trans-1,2-Dichloroethene 0.75 U 75-34-3 1,1-Dichloroethane 0.25 U 590-20-7 2,2-Dichloropropane 0.25 U 156-59-4 cis-1,2-Dichloroethene 0,25 U 67-66-3 Chloroform 0.25 U 74-97-5 Bromochloromethane 0.75 U 71-55-6 1,1,1 -Trichloroethane 0.25 U 563-58-6 1, 1-Dichloropropene 0.25 U 56-23-5 Carbon Tetrachloride 0.75 U 107-06-2 1,2-Dichloroethane 0.25 U 79-01-6 Trichloroethene 0.25 U 78-87-5 1,2-Dichloropropane 0.25 U 75-27-4 Bromodichloromethane 0.25 U ~74-95-3 Dibromomethane i U 10061-01-5 cis-1,3-Dichloropropene 0.25 U 10061-02-6 trans-1,3-Dichloropropene 0.25 U 79-00-5 1,1,2 -Trichloroethane 0.25 U, 127-18-4 Tetrachloroethene 0.25 U 142-28-9 1,3-Dichloropropane 0.25 U 124-48-1 Dibromochloromethane 0.75 U 106-93-4 1,2-Dibromoethane 1 U 108-90-7 Chlorobenzene 0.25 U 630-20-6 1,1,1,2 -Tetrachloroethane 0.25 U 75-25-2 Bromoform 0.5 U 79-34-5 1,1,2,2 -Tetrachloroethane 0.75 U TQL- Target Quantation Limit- Subject to change due to instrument sensitivity T- Tentatively identified, not confirmed E- Estimated Value U- Samples analyzed for this compound but not detected N- Sample not analyzed for this compound D- Detected below quantitation limit M- GC/MS Analysis performed SUPERVISOR DATE/ 9 —1-- ED BY CHECK CHECKED BY � CAS# VOA TARGET COMPOUND %L DETECTED ua/l ua/l 96-18-4 1,2,3-Trichlorcpropane 0.25 103-86-1 Bromobenzene 1 95-49-8 2-Chlorotoluene 0.25 106-43-4 4-Chlorotoluene 0.25 541-73-1 1,3 -Dichlorobenzene 0.25 106-46-7 1,4-DlchlorobenZene 0.25 95-50-1 1,2 -Dichlorobenzene 0.25 96-12-8 1,2-Dibromo-3-Chloropropane 1 120-82-1 1,2,4-Trichlorobenzene 0.25 87-68-3 Hexachlorobutadiene 0.25 87-61-6 1,2,3-Trichlorobenzene 0.75 1634-04-4 Methyl-tert-butyl ether 5 71-43-2 Benzene 1 108-88-3 Toluene 1 100-41-4 Ethvl benzene 1 103-32-3 m,p-Xylenes 1 95-47-6 o -Xylene 1 100-42-5 Styrene 1 98-82-8 Isopropylbenzene 1 103-65-1 n-Propylbenzene 1 108-67-8 1,3,5-Trimethylbenzene 1 98-06-6 tert-Butylbenzene 1 95-63-6 1,2,4-Trimethylbenzene 1 135-98-8 sec-Butylbenzene 1 99-87-6 p-isopropyltoluene 1 104-51-8 n-Butylbenzene 1 91-20-3 Naphthalene 1 Other purgeables detected (up to 10 highest peaks) NO VOLATILE ORGANIC COMPOUNDS QUANTITATED BY GC/ELCD D Detected ug/l TU U U U U U U U U U U U U U U U U U U U U - U U U U U 'Departure ,sof Natural ,.)Zesources and Commnty Del U Division of Environmental Management P.O. Box 27687 - Raleigh, N.C. 27611 WELL ABANDOMENT JUL 2 0 19qz RECORD t Groundwater Protection Inc. CONTRACTOR RtG. NO: 1. WELL LOCATION: (Show a sketch of the location on back of form.) Nearest Town: Marion County Mdbwell Quadrangle No. (Road, Community, Subdivision, Lot No.) 2. OWNER: acats American 3. 4. . 5. 1 6. 7. 8. IDDRESS : P.O. Bmc 670, Toccoa, GA 70POGRAPHY: draw, slope, hilltop, valley, flat 1SE OF WELL: Mmitoring DATE:6-10-92 10TAL DEFIH: 20.0' DL44=: 2.0" :�'- feet diameter 20.0 2.0" )EALING MATERIAL: Neat cEment Sand cement bags of cement 11 bags of cement gals. of water yds. of sand gals. of water Other Type material Portland Bentrnite aurry Amotmt 11 - 100 1b. bags EULAIN MQHOD OF II4UCEMW OF MATERIAL Pour Method Dmrtlrilled 20 ft., palled well grouted to surface I do hereby certify that this well abandonmen record is and exact. 6/18/92 S' tore of Contractifr or Agent Date WELL DIAGRAM: Draw a detailed sketch of the well showing total depth, depth and diameter of screens teraining in the well, gravel interval., intervals of,,cns, and depths and types of i (013`mo-NA c�,t;TtQCE MLLIGH, P}G /0• SC,eeen A10 .S4nc) N'c 6 ,ee, cL.T Submrit original to the Division of Environmental Management, one copy to the Driller, and one copy to the Owner. G,-30 Revised 10/1/80 ,t -V. Draw a loci ion sketch showing the direction and of the well to at least two (2) nearby reference points such as roads, intersections and streams. Identify roads with State Highway road indentification numbers. - WELL DATA TABULATION POLLUTION SOURCE MONITORING SITE Facility Name: ��ir� rll%'Q County: HJ)6W'P /1 Pollution Source (lagoon, landfill, etc.) j o A6t Latitude:.�?S°7' Permit No: Longitude: gZ6C / • Non -Discharge: NPDES: ,/ Well Const.: DHS: Quad No: 1`� l?o Sampled By: Draw a diagram on the reverse side of this form showing map location of the site and the location (direction and distance) of each well with respect to the pollution source and to each other. Indicate sampling schedule, parameters and any changes to schedule. GW -51 Revised 8/20/84 Well No. o,,Cs Date Installed ole /g Total Depth (ft) Diam. (in) Screen(S)/ Open hole (OH) (ft -ft) Grout Interval (ft -ft) Gravel/Sand Pack Interval (ft -ft) Remarks ao' it S/ 0-/0 /0--20 7- S110-.20 0-/10 /o ..20 2 lo lig 20, z,1 S ho ao o --/o 16-120 Draw a diagram on the reverse side of this form showing map location of the site and the location (direction and distance) of each well with respect to the pollution source and to each other. Indicate sampling schedule, parameters and any changes to schedule. GW -51 Revised 8/20/84 1rAL9Tq �q NOR i. CAROLIN, _zPARTMENT OF NATURAL RESOURCES_ COMMUNi_ DEVELOPMENT WELL RECORD DIVISION OF ENVIRONMENTAL MANAGEMENT, GROUNDWATER SECTION 4 � ni P.O. BOA 27687 - RALEIGH, N.C. 27611 . _--- -- -- 1. WELL LOCATION: (Show sketch of the location below) Nearest Towne �i�{/l 2. or Subdivigion ands t No.) ty:� _ Tangle No. �- fKFG s- /yL -Zli 76 — DRILLING LOG 3 Z' -t 7 3 3 3. ADDRESS: 21 2t 1/4/ DEPTH gZ O l l 4. TOPOGRAPHY: draw ,v .le hillto flat(c rcle one) FROM TO FORMATION DESCRIPTION y,slope, p, 5. USE of WELL: DATE: (� 6. DOES THIS *LL REPLACE AN EXISTING WELL? / f 7. TOTAL DEPTH �_ RIG TYPE OR METHOD: 8. FORMATION SAMPLES COLLECTED: YES NO 9. CASING: Depth Inside Wall thick. type Dia. or weight/ft.j From-0—to20fta /I V Z 10. GROUT: Depth Material Method From to/0 ft z3_ eMEE:: 11. SCREEN: Depth Dia. Type & Opening D�` 'A If additional ace is needed, use ac o orm From to ft LOCATION SKETCH Show di�tanc�e/to numbered roads or other map reference points) /Y 12. GRAVEL: Depth Size Materi 1 s From ---to /0 ft 13. WATER ZONES(depth): 'A If additional ace is needed, use ac o orm From to ft LOCATION SKETCH Show di�tanc�e/to numbered roads or other map reference points) /Y 12. GRAVEL: Depth Size Materi 1 From ---to /0 ft 13. WATER ZONES(depth): 14. j� above STATIC WATER LEVEL: (/ ft *below top of casing Casing is � ft. above land surface ELEV: 15. YIELD(gpm): METHOD OF TESTING: 16. PUMPING WATER LEVEL: ft. after hours`at (^1' L�1 qpm. 17. CHLORINATION: Type Amount 18. WATER QUALITY: TEMPERATURE(0F) " V 19. PERMANENT PUMP: Date Installed //µQkI well e Type Capacity (gpm)HP Make Intake Depth 7 Airline Depth 20. HAS THE OWNER BEEN PROVIDED A COPY OF THIS RECORD AND INFORM D OF THE RECOMMENDATIONS? DEPARTMENTS REQSIREMENTS AND 21. REMARKS I do hereby certify that this well was constructed in accordance with N.C. Well Construction Regulations and Standards and t t this w record i rus.and exact. � iJIS/1 Form GW -1 Revised 11/3/77 suhei+_nr_t..9...7 �,. �--•--.---�__ .._ _. , _ n - ® f-/3-efD -/ -9f 7'30 1.2 -17 - ALKALINITY, TO PH 4.5 ALKALINITY, TO PH 8.3 — ALUMINUM - ARSENIC ! 1 BARIUM BICARBONATE CADMIUM CALCIUM A14 l f 0 < 6 3 65- eZ 03 - CARBONATE CARBONATE - r CHLORIDE .0 / v2 To 31.3 3/ 1 -2 f ? 21® q0 3,� 3 2HROMIUM, TOTAL ` OLIFORM F ECAL COLIFORM TOTAL ( _ I -F I I COPPER ; CYANIDE DISSOLVED SOLIDS %f L� `f ® / mZ ( l . D D /} .314 %` G%® % 31 A /07 FLUORIDE HARDNESS, CaCO L� HARDNESS NON -CARBONATE IRON LEAD MBAS _ MAGNESIUM AlY, � �.t _r . — Z�- ;�0 MANGANESE (— MERCURY — -- NITROGEK?.AMMONIA NITRATE & NITRITE--- ORGANIC SCAN (x/0,9 IR�ppg7 OE?cCYE� EE ��'jgcfE y PHENOLS PHOSPHORUS, TOTAL [POTASSIUM SELENIUM SILVER . (�� , oo,� .C, Uoa c , 00 Z o, 0 00-6 i 'SODIUM SPECIFIC CQVUMANCE t SULFATE ' 3,2 13.6- .. 7 1 3 (c . � � � � ` 45.1 30 13 -3..S - TOC (UNFILTERED) 1 J'[ IZINC © 7HoPltos�l� Tc= -;2l : Z)3 a a __dANITY CaCO3 To pH- 8.3 To pH 4.5 .340 J Aluminum :• G6�P.!r Arsenic Bicarbonate 444 ? ` Cadmium t 44 Calcium Carbonate7.7 Chloride 0 Chlorinated Hydrocarbon - Chromium, Hexavalent Chromi um, Total COD Coliform, Fecal , `Col i form, Total Cyanide Dissolved Solids 9v 11610 l3� G 1100 Fluoride y Z'*'/ Hardness as CaCO �►b {. ?O Hardness, Non-carbonate 300 _ i�70 Iron Lead a,otc, 1 4. Lithium WAS _ [0'z«.55 36e. 6 j Magnesium Manganese �•�p Mercury �, p6®a -KIPLEQ I2In, 48 fib'? 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WATER i CAS* VOA Target Compound DATE ENTERED BY q CHECKED BY ANALYSIS RESULTS TQL Cone I CAS* VOA Target Compound ug /L Detected M-� unh I TO. Cone ug/t Detected P4S! 11.1 it 1 i__ 55-�i; l r{ D>�chither�e - - -t1-r5 0 7► �TE� �96-18-4i�2.3-Trichlorou�+?ne__ __-1 0.15- ` ----_ _:. � U 75-09-2! MetN. lene chloride } 0'25 i- i1 )?Ori 1-O i 5rcis-1 y t-02-5 U i i t C1--1 8rorr4ente f +lJ I56-60-Sitrans- 1 2-Dthioroethom i 0.751 _ 1 1 - U ! 1 U 1 1 95-49-5 2-Chlorotoiuene i 025 U i _ 75 3-1 3�1 jt Dichioruetharte i 0.25-1 2-i-.�---.-i-l�106 Tetrachioroethe e � 43-4 4-Chlorotoiuene� -j 0.= _ j U i i 5 l -24 -?i2 2-Dichl rano ! t�.2'3 I U 1 541-73-i I} 3 -Dichlorobenzene 0.25 D 1 T i i 156-59-41 c -_1 _{ ►ia oeti L Q.fS I i U 1 U U�1 i -46-71 I �4`Dichla-obenze�ne_ E 025_ t 1-5 I > 7-66 3�Chloroform _ ` 0.25 _ _U _ 1 95-50-1 i 2-Dichloreben ene ' 0.25 2.2- _ _79`34 _5L_�2 74-97-518rom+u hlorwethane _..._. ._._ U _L_91 -2G-3 Nghthalene _ _ ! 0.751 i U I I 46-12-8 t 2-Dibramo-3-r-hlor -a 1 !� -� I U. 1 � 7i-55 of i ,i 1 irichlor uethanz 10_�P _i .T !_ 120-82-1 Ij,24-Trichioroberzene ; 0.25 I D T ' 563 -5S -6't .1-Dlc.hlor wrnnenL, 10 125 ". 1 11 1 I 1 n iK 1 I it 1 ! 56-23-51 Carbon Tetraonioride 07-06-21' 1 ,Diihlo-o th4Le y- am2__._. 7"1-6 Trichloreethene 10.75 I 1 U i 1 87-61-6! 1,2,3-Trichlorobenzene-__ � 0.75 I1 U I` I A 7A1 ��-1-�-04-4'Me 1-tert-but tether T g —._.�U _ _ ! - --- - -------�.� . _ _ 0.251 ! 1 71-43-2 Benzene ± 78-87-511 ilichior'oPane _ _..__ ± ��= 1-- 75 2 41 Br omodichlorornethane 1 25 i 1 U 1 108_-88-3 Toluene j 1 U .I. ___— -- i 0.251 U 100-41-4 E 1 benzene U 1 1 74-85-31 Dibromomethane ! t i U 1 108-38-31 m X lentis i 1 1, i1 )?Ori 1-O i 5rcis-1 y t-02-5 .3-Dichloropr trans -1 3-Dichlar r ene 0.25 0.25 ( __.__._. __ j_� _ _ i5 -4? -6 a -} lone i _ _ _. _ _ - -U-�1 1 f i U I t 1 -42-5 S rine _ 1 1 - U ! I 79-00-511,I 2 -Trichloroethane 0.25 ' U 98-82-81 Isw benzene I _I U 1 . j 12 18 4 Tetrachioroethe e � U 103-0-1 n-Prop1ber�zene i- U 142-28-9.1 3-Dichbr ane 10.251 U_ 108-67-811 3 5-T ]benzene I l U 1 124-48-1 106-93-411 Dibromochioromethane 10.751 .2-Dibromoethant ��-' i U 1 1 98-06-6 tert-Butt' benzene �5-63-6 1 4-Trimet lbenzene I i U 1 U 1 108-90-7 i Chlorobenzene 10.25 ID ! i 135-98-8 1 sec -B tr benzene 1 U I 630-20-6 i 75-25.2 1 j1� 1,2 -Tetrachloroethane Bromoform - i t 0.25 1 ____.__ _._ �U _ 99_-8 r -6 -Iswv )toluene U `104-51-8 n -Bu benzene ____ i U � �.�__ _.�__.� U! _ _79`34 _5L_�2 �-a trachloroethane�t�.75 i� _..._. ._._ U _L_91 -2G-3 Nghthalene _ _ 1 _ 1 ^ TQ-- target quantitation limit T- tentatively identified cid E- estimated Yalue U- compound was analyzed for but not detected 14 t�t7t an for this compound D- detftifd beiew quant!#-atlrn 11" MS-- X-6CIMS analysis performed TOL subject to change due to instrument sensitivity COMPUTS Cone Other purgeables (up to 10 hit peaks) Deteoted ug/L NO VOLATILE MANIC COMPOUNDS QUANTITATED BY OC/PID. cn cn -o I -i 'o 0 n C) n r 0 -n O ,— p -n o 'o C= w _. _. — cD w O= w o 0 0 w w. -t m �, m `° m m m 0 m -� m m O C7 ^ w -CT — z a- o z m w o �. �� O o o w p CD CD =r < CO w � SD m 3 3 w w w : o j=mQ_ '0r Da C. n 3 wn� Z n o o ww m o m -n z m vg ' a w n o m W ca D :3O w _ 0 o7- cD CD nu 71 Z .-r m w O ` CD w r O cD m X11 C AT CD OL `�°s D crCDa cn _ O 'cn is o 3 R �. -O CD < 'o � 0 o o m m c' N z m' Fn 3 3 3 3 3 3 3 3 3 c 3 o o 3 m z -� f "'� 0 (a cQ o o (a (a cQ cQ (Q (o _, cc o o (° 0 w CL 0 O m, —M CD — — — — — — — — — — 00 c o _ `Ia N Z Z D z 2' n n C7 C7 C7 Do D_ -0 Z Z c o 3 afii w . 3 cfl a (O (D = t1 w w ' = a Q O (Q (D ` ' 1 a i a a 0 r a CD W N pj w C> n cn O Q 3 C) 0 0o D a w twn n c CD O n O w w pi (D O O iw w w C w (D -< < t C CL =3 co w o o a 3 a n 3 z z �' .0 ® 7o c (° :3v' ° -0 3W CD c w ct m m 3� Cl)' 3 m o 3` 3 3 m ° w w e.o ° w ° a Z m t a� m n C/3m CD w C (D m o (D o m D ^ > o 0 3 3 ® a —I 0 N CF (D CD CD ° ^ - C) 3 3' 3 3 3 3 3 3 3' 3 3' 3 3 3 '3 ° I I ( m� c v �. t0 (° co to (m cc m co c0 f0 to (° (Q we m Rl �. m o n d to r co -_ ` �' c — — — — — — — — — — — ro d `° $„z o z (D A (Q z T- D i� moo o c „3yr v N z° `moo o ti' 005 p m <CD lozo U� tD 3 0- OL ° v -0 mO rt , o w n m (ro o !� ° N r? o °3' Q rem C (n n w r o _.CD D m 6 07 M 'a"5 ; [ N a o CD m R (D w -0 to W o p p/ 3 ^► O �. a' -0 W N K �N x. \Q �E�j3p m c N of '4 N d i n r w —I -� j� (D N O _0 m .�� V `.n—« CD bw x y00 N 3 0 �' O � m n v d c 6 5' CD a c c c c c c c c X 3 3 3 co 3 O c° c° ct? cfl m (Q (Q fl c° (fl (Q m " c m m cD — — — i — — — — — — — m a O -10m m m D C 2 O m N m D O m z ;rl o'o C = w =r O= CA o o O w w- w cD ——— Z a� CD Cl m v O C� cn p 0 m m w v cD m m _Z o m aw D CD D p C/)0 ° � _a CD 3 3 o M. o W m o3 w w o a 3a mC7 0 0 Co n -n z m o>> o -- — -n rw M m v Z cD E n m vi r o p -m w a w m -p (D 7 i = m c N w (� m 2 3 _ _ a D z , j ; —a S a J CD m RI v I G •-41 OCr -�D `� n G w m . 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O .. m ° O (D O rrI Q° 3 3 0cn m C n O a N m O Cl)Z� A D -I 3 N � c D m (D r, -i n Y C z O C) b o O D rD m f �, 3 a m O "� ° m T 3 _0 m D O. z R _ r m Q m c CD m m z m O D (D O� Z7 C .m m Y ;a ro CD m O W' m co C/) z T O Z c O m m 3 � CD - a <` Y n O O rn (D := 3 O m W A D N � (D r, n •' O C) b o O D rD m 3 _0 m D O. z R _ r m Q m c CD m z ro m W' m co c CD - a <` Y m O (D := 3 O m W c N � •' C (D m POLLUTION SOURCE MONITORING SITE Facility Name:IrPQ� County: kcbe00e// Pollution Source (lagoon, landfill, etc.) Latitude: ,?s"° 47 Permit No: Longitude: gZoo / Non -Discharge:_ t y 4 / NPDES: Well Const.:_ 5's -aoo - M -l� 6L9 OHS: Quad No: K20j- Sampled By: i Well No. Date Installed 3S 'f 7 33 RK _55- 2 t�o..Q y 241 Total Depth (ft) Imam Screen(S)/ Open hole (OH) (ft -ft) POLLUTION SOURCE MONITORING SITE Facility Name:IrPQ� County: kcbe00e// Pollution Source (lagoon, landfill, etc.) Latitude: ,?s"° 47 Permit No: Longitude: gZoo / Non -Discharge:_ t y 4 / NPDES: Well Const.:_ 5's -aoo - M -l� 6L9 OHS: Quad No: K20j- Sampled By: i Well No. Date Installed 3S 'f 7 33 RK _55- 2 t�o..Q y 241 Total Depth (ft) Diam. (in) Screen(S)/ Open hole (OH) (ft -ft) Grout Interval (ft -ft) Gravel/Sand Pack Interval (ft -ft) Remarks 9 9MA J? 7- 00o s .o-Ro 0/ 19 s io ao S io -o Z� 0-/0 /0 ao 0-/'o /0 -.20 Draw a diagram on the reverse side of this form showing map location of the site and the' location (direction and distance) of each well with respect to the pollution source and each other. Indicate sampling schedule, parameters and any changes to schedule. GW -51 Revised 8/20/84 .YY DRILLING CONTRACTOR: Crrotm� te p�tion Inc DRILLER REGISTRATION NUMBER: 1 1105 WELL LOCATION: (Show sketch of the location belowounty: Nearest Town: DEPTH DRILLING LOG (Road, Community, or Subdivision and Lot No.) From To Formation Description 2. OWNER 0.0' 3.0' Lk BM' Si1tY Clay ADDRESS P.O. Box 670 15-01— Olive GM Silty MW (Street or Route No.) 3.0' Zb�roa GA 30577 State Zip Code City or Town l"L�LifAY 3. DATE DRILLED --6--11-92 USE OF WELL 4. TOTAL DEPTH 15.0 ft. 5. CUTTINGS COLLECTED YES ❑ NOM 6. DOES WELL REPLACE EXISTING WELL? YES ❑ i.4 r� l,•l ,s� �c, 7. STATIC WATER LEVEL Below Top of Casing: FT.�,j (Use "+" if Above Top of Casing) j - t FT. Above Land Surface* 8. TOP OF CASING IS t p iec•' * Casing Terminated at/or below land surface is illegal unless a variance is issued in accordance with 15A NCA 2C .0118 l�il�.�t S� L i g. YIELD (gpm): � --METHOD OF TEST RALEIGH, MC 10 WATER ZONES (depth): �- STATE WELL CONSTRUCTION PERMIT NUMBER: 55-0001-WM-0064 f 11. NA Amount NA — If additional space is needed use back of form CHLORINATION, Type 12. CASING: LOCATION SKETCH Wall Thickness Show direction and distance from at least two State Depth Diameter or Weight/Ft. Material Roads, or other map reference points) From --To Ft. --' From— To Ft. From To Ft. 13. GROUT: Material Method Depth From n 0- . To 0-5 F •-- t. Portland B�ta�� to S] -tin' From _To Ft. 14, SCREEN: Depth Diameter Slot Size Material To- Ft 2.0 in. .010 in. _y �'' 1 From 0.0 From _ To Ft. in. in. __---- From _ To _Ft, in. in. 15. SAND/GRAVEL PACK Material Depth Size From _3.0-- To 15_0— Ft. Fina Silica Sid From — To _-=- Ft. _--- 0.5 to 3.0 feet. MARKS' 16. RE RDANCE WITH 15A NCAC 2C, WELL 1 DO HEREBY CERTIFY THAT THIS WELATVA CORY OF THIS RD ORD HIN OS BEEN PROVIDED TO THE WELL OWNER. CONSTRUCTION STANDARDS, AND TH NT DATE SIGNATURE OF ONTRACTOR OR to well owner. GWA REV. 9/91 Submit original to Division of Environmental Manag e. and copy DEPART!:.:` :'1ATURAi RESOURCES AND COMI�t' EVELOPMENT, SIOli of F1wIRUNt¢.NrAL MANAGT l WELL AND PUMP INSPECTION REPORT Date Well location -SE V 1 G A Area (Town, Corm., Subdivision and Lot No.) County Owner C o A -r-s A M CR I CAN Road/Street 5R 1554 - Address P• (� • r3 Dx 3 G _ quad No. ,<$0,P /3 %vjA/c�fDN� NG . f%S,rZ Serial No. 137`15^0 34r ylai g'a 0i /9 Lat. Long. WELL CONSTRUCTION Drilling Contractor 0,10, V0 VVA—rcR Reg. # Name Address Meets Min. Standards Measure Yes No Remarks Permit _._.._._ Location'' Distance from Pollution source -- Other Aocation standards Total Depthp� ------ Casing ./ Depth Diameter Weight/thickness n, Height: Drive shoe //1 Exception approved by owner 1 Grout; Type �,• rv, i3� nCT"OA p —T Thickness 3'X 3� ! _U9tS Depth �•S� �= 1�' •'" Screens Development r►'' I. D. Plate Abandonment (temporary/permanent) Water level Welt test PAIA ----f— Chlorination NIA Cuttings' Reports Water Aamp a (appearance) ,Y� F WELL NO.: K80113 COATS AMERICAN COUNTY: MCDOWELL DATE SAMPLED ALKALINITY,TO pH 4.5 ALKALINITY,TO pH 8.3 ALUMINUM ARSENIC BARIUM BERYLLIUM BICARBONATE CADMIUM CALCIUM CARBONATE CHLORIDE CHROMIUM,TOTAL COBALT COD COLIFORM, FECAL COLIFORM, TOTAL COPPER CYANIDE DISSOLVED SOLIDS FLUORIDE HARDNESS CaC�CARB�� HARDNESS, NO IRON LEAD LITHIUM MBAS MAGNESIUM MANGANESE MERCURY NICKEL NITROGEN, AMMONIA NITROGEN, KJELDAHL NITRATE & NITRITE ORGANIC SCAN ORTHOPHOSPHATE pH PHENOLS PHOSPHORUS, TOTAL POTASSIUM SELENIUM SILVER SODIUM SPECIF. CONDUCTANCE SULFATE TOC (UNFILTERED) TOX TSS VOC ZINC STATIC WATER LEVEL Red Ink=Sample taken by facility