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Home My WebLink AboutWQ0002378_Residual Annual Report 2018_20190114Town of Mooresville NORTH CAROLINA 2018 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 E=0,,LEE of ��n JAN 1 4 2019 . W W4 RECEIVEDINCDEQIDWR JAN 14 2019 Non -Discharge Permitting Unit Annual Sludge Report, WQ0002378 Rocky River WWTP P.O. Box 878, Mooresville, N.C. 28115 Town of Mooresville NORTH CAROLINA ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 RECEIVED JAN 14 2019 NCDENR-DWQ 01 /07/ 19 LJM Information Processing Unit kiforID 1617 Mail Service Center Raleigh, NC 27699 Subject: 2018 Annual Sludge Report, WQ0002378 Surface Disposal of Class B Residuals Following is the information requested to accompany our annual sludge report. Facility - Rocky River WWTP (Location of onsite monofill) JAN 14 2019 369 Johnson Dairy Rd. Mooresville, N.C. 28115. Non -Discharge Phone # 704-662-8470. permitting Unit Responsible official and facility operator -Larry Hendren, Biosolids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone # 704-799-4063 Dry Metric Tons buried on site - No sludge was buried during 2018. All Class B belt press sludge was dewatered and placed in a lined land fill. Methane sampling was conducted August 27, 2018. No methane exceedances were noted during the monitoring event. The data from the sampling is included in this report. Residuals removed from the surface disposal unit - 364.1 tons or 264.2 dry metric tons (See attached hauling summary sheet). Residuals were placed in a lined land fill. BFI Landfill did not require new TCLP analysis for 2018 due to no change in the profile of the material. 2016 laboratory TCLP results are included in this report. Monitoring well data is not included in this report. All monitoring well data was incorporated into separate reports submitted in June 2018 and January 2019. I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: Larry Hendren, Biosolids Coordinator Signature: �y...�.�.�- 1 - -1 ' 7-0 1*1 Date 1-17 BLUE FLAME CREW A DIVISION OF BOOS RT GROUP August 27, 2018 Mr. Jamie Levis WWTP Town of Mooresville 369 Johnson Dairy Road Mooresville, N.0 28115 Re: WWTP Town of Mooresville 2018 Surface Emissions Monitoring Dear Mr. Levis: On August 27, 2018 Blue Flame Crew, LLC (Blue Flame) performed surface emissions monitoring for the Town of Mooresville Waste Water Treatment Plant (WWTP) during the Third quarter of 2018. This monitoring event was conducted in accordance with (1) regulation set forth in the New Source Performance Standard (NSPS), 40 CFR 60.755 (c) and (d); (2) 40 CFR 60, Appendix A Method 21, promulgated by the United States Environmental Protection Agency (USEPA). A Thermo Environmental Instruments flame ionization detector (FID) was used to perform the emissions monitoring. The FID was calibrated at the beginning of the event, prior to use, meeting Method 21 compliance requirements. Calibration logs were completed by the field technician performing the work, and are included in Attachment A. Weather Conditions Weather conditions recorded August 27th during the monitoring event were as follows: August 27 Clear Dry Ground Wind 0-5 mph Temperature approximately 86° Fahrenheit Relative humidity of 74 percent Barometric pressure of 30.24"Hg BLUE FLAME CREW A DIVISION OF BOOS RT GROUP As per the NSPS regulation, this monitoring event was performed during typical meteorological conditions. Monitoring Summary On August 27, 2018, a Blue Flame field technician monitored the Sites surface along the site -specific traverse pattern and at areas suspected, based on visual observations, of exceeding 500 PPM above the determined background methane, gas concentrations. No exceedances (FID readings greater than 500 PPM above background measurements) were detected during this monitoring event (see Attachment B — Daily Log). During the monitoring events, Blue Flame observed that the ground surface appeared to be in fair condition. Blue Flame did not notice any unusual odors. If you have any questions regarding this Letter Report, or any other matter, please do not hesitate to call me at (850)737-1355. Sincerely, Blue Flame Crew, LLC Matthew Woods Project Manager Attachments: A —Calibration Logs B — Daily Log C —Site Drawings BLUE FLAME CREW A DIVISION OF BOOS RT GROUP Attachment A I Blue Flame Crew, LLC P.O. Box 525 Naperville, Illinois 60566 CALIBRATION PROCEDURE AND BACKGROUND DETERMINATION REPORT LANDFILL NAME: TOW n of ♦`AC)Or[5V 111e MONITORING DATE: $JZI I ► B TIME: 1=00 INSTRUMENT MAKE: Thermo. Enviro. Instr. MODEL: TVA-1000 S/N: 30988640 CALIBRATION PROCEDURES: 1. Allow instrument to internally zero itself while introducing zero air. 2. Introduce the calibration gas into the probe. Stable reading = 130 ► ppm BACKGROUND DETERMINATION PROCEDURE: 1 Upwind reading (highest in 30 seconds): � tZ ppm (1) 2 Downwind reading (highest in 30 seconds): z3 ppm (2) Calculate Background Value: 1) + 2 2 PERFORMED BY: ma t-v Moods = .1-7 ppm I Blue Flame Crew, LLC P.O. Box 525 Naperville, Illinois 60566 CALIBRATION PRECISION TEST RECORD LANDFILL NAME: 'Town of M ooyesy' ft MONITORING DATE: ( 27 ( 18 TIME: I =00 f ,r. INSTRUMENT MAKE: Thermo. Enviro. Instr. MODEL: TVA-1000 S/N: 30988640 MEASURMENT #1 Meter Reading for Zero Air: .10 ppm (1) Meter Reading for Calibration Gas: Soo ppm (2) MEASURMENT #2 Meter Reading for Zero Air: • 1 `1" ppm (3) Meter Reading for Calibration Gas: 4-1 1 ppm (4) MEASURMENT #3 Meter Reading for Zero Air: • t 1 ppm (5) Meter Reading for Calibration Gas: So 1 ppm (6) CALCULATE PRECISION (per 40 CFR 60, Appendix A Method 21, Section 4.4.2): [500 - (2)] + [500 - (4)] + [500 - (6)] 1 100 3 x 500 x 1 = O % (must be < 10%) PERFORMED BY: woods, Blue Flame Crew, LLC P.O. Box 525 Naperville, Illinois 60566 INSTRUMENT RESPONSE TIME TEST RECORD LANDFILL NAME: 'Town of MoareSv"I%c MONITORING DATE: 8 I Z 7 I 1 8 TIME: I� 00? INSTRUMENT MAKE: Thermo. Enviro. Instr. MODEL: TVA-1000 SIN: 30988640 MEASURMENT #1: Stabilized Reading Using Calibration Gas: 499 ppm 90% of the Stabilized Reading: 449 ppm Time to Reach 90% of Stabilized Reading After Switching From Zero Air to Calibration Gas: 4.3 seconds (1) MEASURMENT #2: Stabilized Reading Using Calibration Gas: So 1 ppm 90% of the Stabilized Reading: 450 ppm Time to Reach 90% of Stabilized Reading After Switching From Zero Air to Calibration Gas: 4. G seconds (2) MEASURMENT #3: Stabilized Reading Using Calibration Gas: qg ppm 90% of the Stabilized Reading: 449 ppm Time to Reach 90% of Stabilized Reading After Switching From Zero Air to Calibration Gas: ¢. 5 seconds (3) CALCULATE RESPONSE TIME: (1) + (2) + (3) 3 = 4.46 seconds (must be < 30 seconds) PERFORMED BY: Mat+ W ood S BLUE FLAME CREW A DIVISION OF BOOS RF GROUP Attachment B I Blue Flame Crew, LLC P.O. Box 525 Naperville, Illinois 60566 DAILY MONITORING LOG LANDFILL NAME: Town aF Moorc&V �►►C MONITORING DATE: 8I 2-71 18 TIME: 1=60pr+ INSTRUMENT MAKE: Thermo. Enviro. Instr. MODEL: TVA-1000 SJN: 30988640 MONITORING SUMMARY NUMBER OF EXCEEDANCES: ID CONCENTRATION DISCRIPTIONILOCATION PERFORMED BY: Mcl o Wood$ llUl FLAME CREW A DIVISION OF BOOS RT GROUP Attachment C I I NOTE: WELL LOCATIONS TRANSFERRED FROM SURVEYED WELL LOCATIONS ON''TOWN OF MOORESVILLE, NC. MONITORNG WELLS" DRAWING PREPARED BY iem DATED 1/2016 LEGEND ■ * EXISTING MONITORING WELL MONITORNG WELL LOCATIONS Town of Mooresville 2018 Monofill Reclamation Hauling Summary Sheet DATE TONS TRANSPORTER DESTINATION COMMENTS 1/2/2018 11.71 Town of Mooresville CMS Landfill 1/2/2018 8.58 Town of Mooresville CMS Landfill 1/2/2018 12.00 Town of Mooresville CMS Landfill 1/2/2018 8.97 Town of Mooresville CMS Landfill 1/3/2018 12.44 Town of Mooresville CMS Landfill 1/3/2018 12.56 Town of Mooresville CMS Landfill 1/3/2018 13.87 Town of Mooresville CMS Landfill 1/4/2018 12.32 Town of Mooresville CMS Landfill 1/4/2018 13.84 Town of Mooresville CMS Landfill 1/4/2018 12.67 Town of Mooresville CMS Landfill 1/8/2018 11.37 Town of Mooresville CMS Landfill 1/8/2018 10.41 Town of Mooresville CMS Landfill 1/8/2018 11.08 Town of Mooresville CMS Landfill 1/8/2018 12.92 Town of Mooresville CMS Landfill 1/8/2018 12.17 Town of Mooresville CMS Landfill 1/9/2018 14.45 Town of Mooresville CMS Landfill 1/9/2018 16.29 Town of Mooresville CMS Landfill 1/9/2018 16.31 Town of Mooresville CMS Landfill 1/9/2018 12.72 Town of Mooresville CMS Landfill 1/9/2018 9.59 Town of Mooresville CMS Landfill 1/9/2018 12.69 Town of Mooresville CMS Landfill 1/10/2018 12.78 Town of Mooresville CMS Landfill 1/10/2018 13.24 Town of Mooresville CMS Landfill 1/10/2018 15.03 Town of Mooresville CMS Landfill 1/10/2018 16.85 Town of Mooresville CMS Landfill 1/10/2018 15.73 Town of Mooresville CMS Landfill 1/10/2018 16.18 Town of Mooresville CMS Landfill 1/10/2018 15.32 Town of Mooresville CMS Landfill I TOTAL 364.1 tons .AwLPFRISM LABORATORIES ING Full -Service Analytical & Environmental Solutions Town of Mooresville/RR VVVVTP Whitney Munroe P. O. Box 878 Mooresville, NC 28115 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Class B Monofill TCLP Lab Submittal Date: 11/03/2016 Prism Work Order: 6110085 Case Narrative 12/05/2016 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Terri W. Cole Project Manager Data Qualifiers Key Reference: " aD Reviewed By Terri W. Cole Project Manager CVL CCV result is below the control limits. LCS recovery within the limits. Analyte not detected in the sample. No further action taken. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit Sample Receipt Summary P R I S n /� I Full-Service,Environmental Analytical s 12/05/2016 fl � V � Environmental Solutions LABORATOHIE$ INC. Prism Work Order: 6110085 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received Class B 6110085-01 Solid 11/02/16 11/03/16 Samples were received in good condition at 4.2 degrees C unless otherwise noted. I ZP R I S M I Full -Service Analytical Environmental Solutions � . LABORATORIES - Town of Mooresville/RR VWVfP Attn: Whitney Munroe P. O. Box 878 Mooresville, NC 28115 Project: Class B Monofill TCLP Sample Matrix: Solid Laboratory Report 12/05/2016 Client Sample ID: Class B Prism Sample ID: 6110085-01 Prism Work Order: 6110085 Time Collected: 11/02/16 16:30 Time Submitted: 11/03/16 17:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters Solids 80.0 % by 0.100 0.100 1 *SM2540 G 11/14/16 16:35 JLB P61(0342 Weight Paint Filter Liquids Pass g 1.0 0.0 1 *9095A 11/10/16 11:30 EGC P61<0240 Polychlorinated Biphenyls (PCBs) by GC/ECD Aroclor 1016 BRL mg/kg dry 0.062 0.011 1 *8082A 11/9/16 18:45 JMC P61<0214 Aroclor 1221 BRL mg/kg dry 0.12 0.050 1 *8082A 11/9/16 18:45 JMC P61<0214 Aroclor 1232 BRL mg/kg dry 0.12 0.016 1 *8082A 11/9/16 18:45 JMC P61<0214 Aroclor 1242 BRL mg/kg dry 0.062 0.016 1 '8082A 11/9/16 18:45 JMC P61<0214 Aroclor 1248 BRL mg/kg dry 0.062 0.012 1 *8082A 11/9/16 18:45 JMC P61<0214 Aroclor 1254 BRL mg/kg dry 0.062 0.015 1 *8082A 11/9/16 18:45 JMC P61<0214 Aroclor 1260 BRL mg/kg dry 0.062 0.0095 1 *8082A 11/9/16 18:45 JMC P61<0214 Surrogate Recovery Control Limits TCLP Extraction by EPA 1311 Tetrachloro-m-xylene Decachlorobiphenyl 37 % 18 % 36-182 34-182 SR TCLP Extraction Complete N/A 1 *1311 ZHE 11/10/16 9:00 ANG P61<0222 TCLP Extraction Complete N/A 1 1311 11/16/16 6:50 JAB P61<0346 TCLP Metals Mercury BRL mg/L 0.010 0.000030 1 '7470A 11/17/16 12:39 JAB P61<0396 Arsenic BRL mg/L 0.050 0.012 1 *6010D 11/16/16 18:45 bgm P61<0374 Barium BRL mg/L 5.0 0.0065 1 '6010D 11/16/16 18:45 bgm P61<0374 Cadmium BRL mg/L 0.025 0.00065 1 *6010D 11/16/16 18:45 bgm P61<0374 Chromium BRL mg/L 0.25 0.0038 1 '6010D 11/16/16 18:45 bgm P61<0374 Lead BRL mg/L 0.050 0.0080 1 *6010D 11/16/16 18:45 bgm P6K0374 Selenium BRL mg/L 0.10 0.022 1 *6010D 11/16/16 18:45 bgm P61<0374 Silver BRL mg/L 0.25 0.00050 1 *6010D 11/16/16 18:45 bgm P61<0374 TCLP Organochlorine Pesticides by GC/ECD Chlordane BRL mg/L 0.0025 0,000094 1 *8081B 12/2/16 14:19 JMC P61<0381 Dieldrin BRL mg/L 0.00050 0.000022 1 *8081 B 12/2/16 14:19 JMC P61<0381 Endrin BRL mg/L 0.00050 0.000020 1 *8081 B 12/2/16 14:19 JMC P61<0381 gamma-BHC BRL mg/L 0.00050 0.000013 1 *8081 B 12/2116 14:19 JMC P61<0381 Heptachlor BRL mg/L 0.00050 0.000015 1 *8081B 12/2/16 14:19 JMC P61<0381 Heptachlor Epoxide BRL mg/L 0.00050 0.000018 1 *8081B 12/2/16 14:19 JMC P61<0381 Methoxychlor BRL mg/L 0.00050 0.000033 1 *8081 B 12/2/16 14:19 JMC P61<0381 Toxaphene BRL mg/L 0.025 0.00032 1 *8081 B 12/2/16 14:19 JMC P61<0381 Surrogate Recovery Control Limits Decachlorobiphenyl 71 % 13-186 Laboratory Report ZPRISM I Full -Service Analytical s 12/05/2016 Environmental Solutions LABORATORIES INC Town of Mooresville/RR VWVfP Project: Class B Monofill TCLP Client Sample ID: Class B Attn: Whitney Munroe Prism Sample ID: 6110085-01 P. O. Box 878 Prism Work Order: 6110085 Mooresville, NC 28115 Sample Matrix: Solid Time Collected: 11/02/16 16:30 Time Submitted: 11/03/16 17:30 Parameter Result Units Report MDL Limit Dilution Factor Method Analysis Analyst Date/Time Batch ID 2,4,5-Trichlorophenol BRL mg/L 0.25 0.0016 1 '8270D 11/17/16 23:19 JMV P61<0380 2,4,6-Trichlorophenol BRL mg/L 0.10 0.0018 1 `8270D 11/17/16 23:19 JMV P61<0380 2,4-Dinitrotoluene BRL mg/L 0.050 0.0014 1 "8270D 11/17/16 23:19 JMV P6K0380 2-Methylphenol BRL mg/L 0.050 0.0018 1 `8270D 11/17/16 23:19 JMV P61<0380 3/4-Methylphenol BRL mg/L 0.050 0.0015 1 '8270D 11/17/16 23:19 JMV P6K0380 Hexachlorobenzene BRL mg/L 0.050 0.0013 1 '8270D 11/17/16 23:19 JMV P61<0380 Hexachlorobutadiene BRL mg/L 0.050 0.0021 1 '8270D 11/17/16 23:19 JMV P61<0380 Hexachloroethane BRL mg/L 0.050 0.0017 1 '8270D 11/17/16 23:19 JMV P6K0380 Nitrobenzene BRL mg/L 0.050 0.0026 1 '8270D 11/17/16 23:19 JMV P6K0380 Pentachlorophenol BRL mg/L 0.25 0.0012 1 '8270D 11/17/16 23:19 JMV P6K0380 Pyridine BRL mg/L 0.25 0.0010 1 '8270D 11/17/16 23:19 JMV P6K0380 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 89 % 43-140 2-Fluorobiphenyl 76 % 44-119 2-Fluorophenol 42 % 19-119 Nitrobenzene-d5 71 % 44-120 Phenol-d5 27 % 11-52 Terphenyl-d14 86 % 50-134 TCLP Volatile Organic Compounds by GC/MS 1,1-Dichloroethylene BRLCVL mg/L 0.035 0.000083 1 "8260B 11/15/16 18,55 KDM P61<0356 1,2-Dichloroethane BRL mg/L 0.025 0.000066 1 '8260B 11/15/16 18:55 KDM P6K0356 1,4-Dichlorobenzene BRL mg/L 0.38 0.000050 1 '8260B 11/15/16 18:55 KDM P61<0356 Benzene BRL mg/L 0.025 0.000048 1 '8260B 11/15/16 18:55 KDM P6K0356 Carbon Tetrachloride BRL mg/L 0.025 0.00011 1 `8260B 11/15/16 18:55 KDM P61<0356 Chlorobenzene BRL mg/L 5.0 0.000062 1 '8260B 11/15/16 18:55 KDM P61<0356 Chloroform BRL mg/L 0.30 0.000076 1 '8260B 11/15/16 18:55 KDM P61<0356 Methyl Ethyl Ketone (2-Butanone) BRL mg/L 10 0.00024 1 '8260B 11/15/16 18:55 KDM P6K0356 Tetrachloroethylene BRL mg/L 0.035 0.000098 1 '8260B 11/15/16 18:55 KDM P6K0356 Trichloroethylene BRL mg/L 0.025 0.000078 1 '8260B 11/15/16 18:55 KDM P6K0356 Vinyl chloride BRLCVL mg/L 0.010 0.000097 1 '8260B 11/15/16 18:55 KDM P6K0356 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 80-124 Dibromofluoromethane 104 % 75-129 Toluene-d8 115 % 77-123 2 Sample Extraction Data Prep Method: Default Prep GenChem Lab Number Batch Initial Final Date/Time 6110085-01 P6K0240 100 g 100 mL 11/10/16 11:30 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 6110085-01 P6K0342 30 g 30 g 11/14/16 16:35 Prep Method: 3646 Lab Number Batch Initial Final Date/Time 6110085-01 P6K0214 30.26 g 10 mL 11/09/16 12:00 Prep Method: 1311 Lab Number Batch Initial Final Date/Time 6110085-01 P6K0222 25 g 500 mL 11/09/16 15:30 6110085-01 P6K0346 100 g 2000 mL 11/15/16 14:30 Prep Method: 3010A Lab Number Batch Initial Final DateTme 6110085-01 P61<0374 10 mL 50 mL 11/16/16 12:15 Prep Method: 7470A Lab Number Batch Initial Final Date/Time 6110085-01 P6K0396 20 mL 30 mL 11/17/16 8:50 Prep Method: 3610C GC Lab Number Batch Initial Final Date/Time 6110085-01 P6K0381 200 mL 10 mL 11/16/16 14:00 Prep Method: 3610C MS Lab Number Batch Initial Final Date/Time 6110085-01 P6K0380 200 mL 1 mL 11/16/16 13:00 Prep Method: 6030E Lab Number Batch Initial Final Date/Time 6110085-01 P6K0356 10 mL 10 mL 11/15/16 8:48 Subcontracted Analyses The following analyses were subcontracted to Analytical Environmental Services, Inc. Lab Number Analysis 6110085-01 Herbicides TCLP (Sub) "�� PR I S M I Full -Service Analytical qV' Environmental Solutions uWi Jxt'��i LABORATORIES, INC. 449 Springbrook Road • Charlotte, NC 28217 Phone 7041529-6364 - Fax: 704/525-0409 Client Company Name: Report To/Contact Name: iiii ru, Reporting Address: P-iD CYrJ Phone: =104 tyl0 ✓4 — 5awFax (Yes) (No): Email Address: WMUVtrro�[cia-iMK�1Lo-� EDD Type: PDF_,L /Excel_Other Site Location Name: Site Location Physical Address: CHAIN OF CUSTODY RECORD LAB USE ONLY PAGE OF J_ QUOTE # TO ENSURE PROPER BILLING: ,dry i p p �,, � �� SaiTlples INTACT upon arrival? Project Name: i( 4LS /V MOCi L Received ON WET ICE? Short Hold Analysis: (No) UST Project: es) ( O PROPER PRESERVATIVES indicated? *Please ATTACH any project specific reporting (QC LEVEQ)I III IV) Received WITHIN HOLDING TIMES? provisions and/or QC Requirements CUSTODY SEALS INTACT? Invoice To: =Lttilyt M rres Aa. VOLATILES rec'd WJOUT HEADSPACE? Address: PROPER CONTAINERS used? TEMP: Therm ID:- _ tI Observed: Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLIN Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL "Working Days" ❑ 6-9 Days )i(Standard 10 days ❑ Pre -Approved hWok Must Be SC OTHER Samples received after 14:00 will be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES �I RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) p p CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRESERVA- TIVES ,J ANALYSIS REQUESTED 1:/� yy� (� REMARKS ,y} 4 Q+� \ X. *TYPE SEE BELOW NO. SIZE C. Ss i I [P ; 30 I C., e:7- A i AJ Me - A Sampler's Signature Sampled By (Print Name) 0 M VJJIJ4 Affiliation % Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. ReJ'in quis e : (Signat re ' e y: (Signature) Date Military/Hours �ours ,Q� 11 �� 31� Additional Comments: 7SItt. Relinquished By: (S n ure) Re ived By: (Signature) Date Fiek elinqui had By: (Signature) ^,J'� Received F7 Laborat s B • Date it 7 -y� Mile M od of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. C Group No. SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COCywpTIL RECEIVED AT THE LABORATORY ;! n ❑ Fed Ex 7 UPS ❑ Hand -delivered ❑ Prism Field Service ❑ Other ,�J() i\ NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA DFILL OTHER: ❑NC❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC ❑SC ❑NC❑SC El ]SC❑SCI ❑NC ❑SC *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) Aces ANAMCAL, INC. ANALYTICAL REPORT CLIENT Prism Laboratories PO Box 240543 Charlotte NC 282240543 ATTENTION Terri W. Cole PROJECT ID 6110085 LABORATORY REPORT NUMBER 1611650 Primary Data Review By Chris Pafford Project Manager, AES PLEASE NOTE: DATE November 14, 2016 Secondary Data Review By Ashley Amick Project Manager, Access Analytical aamick(n),axs-inc.com - Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. - AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 I I i ISMFull Service Analytical & Environmental Solutions LA 30RATOMEa INC. SUBCONTRACT ORDER Certific o :_ NELAC_ USACE_ Prism Laboratories, Inc. SC Other 6110085 SENDING LABORATORY: RECEWING LABORATORY: Prism Laboratories, Inc. Analytical Environmental Services, Inc. P. O. Box 240543 3080 Presidential Parkway Charlotte, NC 28224-0543 Atlanta, GA 30340 Phone: 800-529-6364 Phone :(770) 457-8177 Fax: 704-525-0409 Fax: NA Project Manager: Terri W. Cole Analysis Due Expires Laboratory ID Comments W a Sample ID: 6110085-01 Solid Sampled:11/02/16 16:30 Herbicides TCLP (Sub) 11/09/16 16:30 Containers Supplied. `1 o z U/?/� r ed By Vate Received By ' Date ZZ_ i( Ah f, i 11,Kd tC1 i0J2<- Released By Date! Received By Date I Analytical Environmental Services, Inc Date: 14-Nov-16 Client: Prism Laboratories Client Sample ID: CLASS B Lab Order 1611650 Tag Number: 6110085-01 Project Name: 6110085 Collection Date: 11/2/2016 4:30:00 PM Lab ID: 1611650-OOIA Matrix: Solid Analyses Result Qual MDL ReportingUnits BatchID DF DateAnalyud Analyst Limit HERBICIDES, TCLP SW1311/8151A (SW3510C) 2,4,5-TP (Silvex) BRL 0.064 0.20 mg/L 232611 1 11/11/201618:24 AW 2,4-D BRL 0.076 0.20 mg/L 232611 1 11/11201618:24 AW Surr: DCAA 95.9 0 50.1-148 %REC 232611 1 11/11/2016 18:24 AW . Qualifiers: ' Value exceeds maximum ooutaminam level E Estimated value above cl antitation range ------------ Analytical Client Work Order Number l!o/l�oS Checklist completed by 4udl Signature ate Carrier name: FedEx `—UPS Courier Client US Mail Other Shipping container/cooler in good condition? Yes ✓ No _ Not Present _ Custody seals intact on shipping container/cooler? Yes =� No _ Not Present _ Custody seals intact on sample bottles? Yes _ No _ Not Present / Container/Temp Blank temperature in compliance? (00_<60C)*Yes ✓ No _ Cooler #1 X le —Cooler #2 Cooler #3 Cooler #4 Cooler#5 Cooler #6 Chain ✓ of custody present? Yes No _ Chain of custody signed when relinquished and received? Yes ✓ No — Chain of custody agrees with sample labels? Yes ✓ No _ Samples in proper container/bottle? Yes i/ No _ Sample containers intact? Yes y No _ Sufficient sample volume for indicated test? Yes `� No All samples received within holding time? Yes ✓ No _ Was TAT marked on the COO. Yes _ No ; Proceed with Standard TAT as per project history? Yes No _ Not Applicable _ Water - VOA vials have zero headspace? No VOA vials submitted Yes _ No — Water - pH acceptable upon receipt? Yes _ No _ Not Applicable ✓ / Adjusted? Checked by Sample Condition: Good ✓ Other(Explain) (For diffusive samples or AMA lead) Is a known blank included? Yes _ No _ See Case Narrative for resolution of the Non -Conformance. 7i Environmental Services, Inc Date: 14-Nov-16 Prism Laboratories ANALYTICAL QC SUMMARY REPORT le: 6110085 1611650 BatcblD: 232611 MB-232611 Client ID: Units: mg/L Prep Date: 11/09/2016 Run No: 329553 MBLK TestCode: HERBICIDI+ TCLP sw1311/8151A BatchlD: 232611 Analysis Date: 11/10/2016 Seq No: 7158619 Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual ex) BRL 0.20 BRL 0.20 0.4087 0 0.5000 81.7 50.1 148 LCS-232611 Client ID: Units: mg/L Prep Date: 11/09/2016 Run No: 329553 LCS TestCode: HERBICIDES, TCLP SW1311/8151A BatehID: 232611 Analysis Date: 11/10/2016 Seq No: 7158620 Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual ex) 0.3754 0.20 0.5000 75.1 52.5 126 0.3511 0.20 0.5000 70.2 50.5 132 " 0.4091 0 0.5000 81.8 50.1 148 1611532-004DMS Client ID: Units: mg/L Prep Date: 11/09/2016 Run No: 329553 MS TestCode: HERBICIDES, TCLP SW1311/9151A BatchID: 232611 Analysis Date: 11/10/2016 Seq No: 7158622 Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val a/oRPD RPD Limit Qual ex) 0.4186 0.20 0.5000 83.7 49.4 131 0.4060 0.20 0.5000 81.2 44.1 137 0.5101 0 0.5000 102 50.1 148 F� t: (heater than Result value < Less than Result value B Analyte detected in the associated method blank IRL Below reporting limit E Estimated (value shove quamitavoo range) H Holding times far preparation or analysis exceeded t Estimated value detected below Repotting Limit N Analyte not NELAC certified R RPD outside limits due to matrix Page 5 of 5 tpt Lim Reporting Limit S Spike Recovery outside limits due to matrix rr