NC0004812_Renewal Application_20190115

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•
ROY COOPER , ,f _�'
Governor Y, �,y',
MICHAEL S.REGAN ,!.L- ,, 4
Secretary ��
LINDA CULPEPPER NORTH CAROLINA
Director Environmental Quality
January 16, 2019
•
James L. Davis
Pharr Yarns Inc
PO Box 1939
Mc Adenville, NC 28101-1939
Subject: Permit Renewal
Application No. NC0004812
Pharr Yarns Industrial WWTP
Gaston County
Dear Applicant:
The Water Quality Permitting Section acknowledges the January 15, 2019 receipt of your permit renewal application and
supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting
branch. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The
permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a
timely manner to requests for additional information necessary to allow a complete review of the application and renewal
of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,(��
J €flL °Ail..
Wren Thetford
Administrative Assistant
Water Quality Permitting Section
ec: WQPS Laserfiche File w/application
North Carolina Departrn_nt of Environrnemts]Q�aat to I Divsiam of Water Resacrrc3s
D E r�' 1 orasvii�Reahnai Office 1510 East Center Avarua,3u to 301 I fdaorevt!e,Nortk Garonne 28115
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Please print or type in the unshaded areas only
(fill-in areas are spaced for elite type, i.e., 12 characters/inch). For Approved. OMB No. 2040-0086. Approval expires 5-31-92
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER
I Arta PAGENERAL INFORMATION
Consolidated Permits Program F NC0004812 T A D
GENERAL (Read the "General Instructions"before starting.) 1 2 13 14 15
LABEL ITEMS GENERAL INSTRUCTIONS
If a preprinted label has been provided,
I. EPA I.D. NUMBER affix it in the designated space. Review the
information carefully; if any of it is
incorrect cross through it and enter the
III. FACILITY NAME correct data in the appropriate fill-in area
below.Also, if any of the preprinted data is
absent (the area to the left of the label
V. FACILITY PLEASE PLACE LABEL IN THIS SPACE space lists the information that should
appear), please provide it in the proper fill-
MAILING LIST tECIC®(d - in area(s) below. If the label is complete
and correct you need not complete Items
2Q�9 I, III, V, and VI(except Vl-B which must be
VI. FACILITY JAN 1 completed regardless). Complete all items
if no label has been proved. Refer to the
LOCATION instructions for detailed item descriptions
A. ,t@f Resources and for the legal authorization under which
this data is collected.
II. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer"yes"to any
questions,you must submit this form and the supplemental from listed in the parenthesis following the question. Mark"X"in the box in the third column if
the supplemental form is attached. If you answer"no"to each question,you need not submit any of these forms. You may answer"no"if your activity is
excluded from permit requirements;see Section C of the instructions.See also,Section D of the instructions for definitions of bold-faced terms.
SPECIFIC QUESTIONS MARK"X'FORM SPECIFIC QUESTIONS MARK"XFORM
YES NO ATTACHED YES NO ATTACHED
A. Is this facility a publicly owned treatment works B. Does or will this facility (either existing or
which results in a discharge to waters of the ❑ X ❑ proposed) include a concentrated animal ❑ X ❑
U.S.?(FORM 2A) feeding operation or aquatic animal
production facility which results in a discharge
16 17 18 to waters of the U.S.?(FORM 2B) 19 20 21
C. Is this facility which currently results in ❑ x ❑ D. Is this proposal facility(other than those described ❑ x ❑
discharges to waters of the U.S. other than in A or B above)which will result in a discharge
those described in A or B above?(FORM 2C) 22 23 24 to waters of the U.S.?(FORM 2D) 25 26 27
E. Does or will this facility treat, store, or dispose of F. Do you or will you inject at this facility industrial or
hazardous wastes?(FORM 3) ❑ x ❑ municipal effluent below the lowermost stratum ❑ X ❑
containing, within one quarter mile of the well
bore, underground sources of drinking water?
28 29 30 (FORM 4) 31 32 33
G. Do you or will you inject at this facility any H. Do you or will you inject at this facility fluids for
produced water other fluids which are brought to special processes such as mining of sulfer by the 1
the surface in connection with conventional oil or ❑ X ❑ Frasch process,solution mining of minerals,in ❑ X ❑
natural gas production, inject fluids used for situ combustion of fossil fuel,or recovery of
enhanced recovery of oil or natural gas, or inject geothermal energy?(FORM 4)
fluids for storage of liquid hydrocarbons?
(FORM 4) 34 35 36 37 38 39
I. Is this facility a proposed stationary source J. Is this facility a proposed stationary source
which is one of the 28 industrial categories listed X which is NOT one of the 28 industrial categories ❑
in the instructions and which will potentially emit ❑ Ellisted in the instructions and which will potentially X ❑
100 tons per year of any air pollutant regulated emit 250 tons per year of any air pollutant
under the Clean Air Act and may affect or be regulated under the Clean Air Act and may affect
located in an attainment area? FORM 5 40 41 42 or be located in an attainment are? FORM 5 43 44 45
III. NAME OF FACILITY
c SKIP Pharr Yarns, LLC Industrial Wastewater Treatment Plant
1
15 16-29 30 69
IV. FACILITY CONTACT
A. NAME&TITLE(last, first, &title) B. PHONE(area code&no.)
C Davis James, Enviro. Manager 704 823 2310
2
15 16 45 46 48 49 51 52 55
V. FACILITY MAILING ADDRESS
A.STREET OR P.O. BOX
s P.O. Box 1939
15 16 45
B. CITY OR TOWN C. STATE D.ZIP CODE
c McAdenville NC 28101
4
15 16 40 41 42 47 51
VI. FACILITY LOCATION
A.STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
c 149 Willow Drive
15 16 45
B.COUNTY NAME
Gaston
46 70
C. CITY OR TOWN D.STATE E.ZIP CODE F.COUNTY CODE
c McAdenville NC 28101
6
15 16 40 41 42 47 51 52 54
EPA FORM 3510-1(8-90) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII. SIC CODES (4-digit, in order of priority)
A.FIRST B.SECOND
C (specify) 7 (specify)
7 7
15 16 17 15 16 19
C.THIRD D. FOURTH
C (specify) 7 (specify)
7 7
15 16 17 15 16 19
VIII. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
8 Pharr Yarns, LLC VIII-A also the owner?
18 19 55 E] YES XL] NO
C.STATUS OF OPERATOR(Enter the appropriate letter into the answer box;if"Other"specify.) D. PHONE(area code&no.)
F=FEDERAL M=PUBLIC(other than federal or state) p (specify) C 704 823 2310
S=STATE 0=OTHER(specify) A
P=PRIVATE 56 15 16 18 19 21 22 25
E.STREET OR PO BOX
P.O. Box 1939
26 55
F. CITY OR TOWN G.STATE H.ZIP CODE IX. INDIAN LAND
C McAdenville NC 28101 Is the facility located on Indian lands?
B ❑YES X❑ NO
15 16 40 42 42 47 51
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDES(Discharges to Surface Water) D. PSD(Air Emissions from Proposed Sources)
C T I NC0004812 C T 8
9 N15 16 17 18 30 15 16 17 18 30
B. UIC(Underground Injection of Fluids E.OTHER(specify) (Specify)
C 1 T I c T 8
9 U 9
15 16 17 18 30 15 16 17 18 30
C. RCRA(Hazardous Wastes) E.OTHER(specify) (Specify)
C T I c T 8
9 R 9
15 16 17 18 30 15 16 17 18 30
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the ma• area. See instructions for •recise re•uirements.
XII. NATURE OF BUSINESS (provide a brief description)
Pharr is a manufacturer of carpet and specialty yarns.
XIII. CERTIFICATION (see instructions)
I certify under penalty of law that/have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fine and imprisonment.
A. NAME&OFFICIAL TITLE(type opr )�` B.S,CiNATURE rV---r C. DAT SIG ED
)
- - L 1)9 ; c V•4&J 4--C.,( c=1 mac.; i q / 41
COMMENTS FOR OFFICIAL USE ONLY
C
C
15 16 55
EPA FORM 3510-1(8-90)

EPA I.D.NUMBER(copy from Item I of Form 1) Form Approved.
NC0004812 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
2 C EPA APPLICATIO FOR PERMIT TO DISCHARGE WASTEWATER
EXISTING MANUFACTURING,vCOMMERCIAL,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
1.OUTFALL LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(lint) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name)
g01 :3 /3 ' /G AJJ 8't y h.r,4/ 7 j South Fork of Catawba River
•
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3)The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
001 Dyeing and Heat Set Operation 0.034 mgd Biological treatment with Cfrernic,al 3-A 1-0
Non-Contact uooling Water 0.040 mgd Addition and Filtration. 2 E
Sanitary 0.035 mgd Chlutination and Deuttlutinatiun 2-F
OFFICIAL USE ONLY
O L (effluent guidelines sub categories)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
❑YES(complete the following table) ✓❑NO(go to Section III)
3.FREQUENCY 4.FLOW
a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mgd) (specify with units)
1.OUTFALL CONTRIBUTING FLOW (specify PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(list) (list) average) (specify average) AVERAGE DAILY AVERAGE DAILY (in days)
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
✓❑YES(complete Item III-B) ❑NO(go to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
✓❑YES(complete Item III-C) ❑NO(go to Section IV)
C.If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION 2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE c.OPERATION,PRODUCT,MATERIAL,ETC. (list outfall numbers)
(spec)
0.034 MGD Textile Yarn Dyeing and Heat Setting 001
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
❑YES(complete the following table) ❑✓ NO(go to Item IV-B)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
❑MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copy from Item I of Form I)
CONTINUED FROM PAGE 2 NCOOO4812
V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
None
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
El YES(list all such pollutants below) ❑✓ NO(go to hem Vl-B)
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE
1

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NC0004812
Pharr Yarns Industrial WWTP Facility X
Location
State Grid/Quad: F I4 SE/MT Holly,NC
Latitude: 35°15'40"N Longitude: 81°04'39"W
Receiving Stream: South Fork Catawba River Sub-Basin: 03-08-34 North Map not to scale
Drainage Basin: Catawba River Basin Stream Class: WS-V Gaston County

CONTINUED FROM THE FRONT
VII. SIC CODES (4-digit, in order of priority)
A.FIRST B.SECOND
c (specify) 7 (specify)
7 7
15 16 17 15 16 19
C.THIRD D.FOURTH
c (specify) 7 (specify)
15 16 17 15 16 19
VIII. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
a Pharr Yarns, LLC VIII-A also the owner?
18 19 55 ❑ YES X❑NO
C.STATUS OF OPERATOR(Enter the appropriate letter into the answer box;if"Other,"specify.) D.PHONE(area code&no.)
F=FEDERAL M=PUBLIC(other than federal or state) p (specify) c 704 ( 823 2310
S=STATE O=OTHER(specify) A
P=PRIVATE 56 15 16 18 19 21 22 25
E.STREET OR PO BOX
P.O. Box 1939
26 55
F.CITY OR TOWN G.STATE H.ZIP CODE IX. INDIAN LAND
c McAdenville NC 28101 Is the facility located on Indian lands?
B ❑YES X❑ NO
15 16 40 42 42 47 51
X. EXISTING ENVIRONMENTAL PERMITS
A.NPDES(Discharges to Surface Water) D. PSD(Air Emissions from Proposed Sources)
C T I NC0004812 C T 8
9 NP
15 16 17 18 30 15 16 17 18 30
B. UIC(Underground Injection of Fluids E.OTHER(specify) (Specify)
C T I c T 8
9 U 9
15 16 17 18 30 15 16 17 18 30
C.RCRA(Hazardous Wastes) E.OTHER(specify) (Specify)
C T I C T 8
9 R 9
15 16 17 18 30 15 16 17 18 30
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the ma. area. See instructions for .recise re•uirements.
XII. NATURE OF BUSINESS (.rovide a brief description)
Pharr is a manufacturer of carpet and specialty yarns.
)CIIII. CERTIFICATIONseeinstmctknMIIIIIIIIIIIIIIIMIMIIIMMIIIMIM
ns)
I certify under penalty of law that 1 have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fin ad imprisonment. _
A. NAME&OFFICIAL TITLE(type or p irit1 ,`sh� 0 B. GNAIy.JRE "'� C. DATE IGN
L a v✓ 43 L D 2,th s init A' r 7 i
COMMENTS FOR OFFICIAL USE ONLY
c
C
15 16 55
EPA FORM 3510-1(8-90)

EPA I.D.NUMBER(copy from Item I of Form I) Form Approved.
NC0004812 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
APPLICATIO
FOR PERMIT TO DISCHARGE WASTEWATER
ZC 4-/EPA EXISTING MANUFACTURING,NCOMMERCIAL,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFACE LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name)
301 al " ° '/G �� �l" t41 South Fork of Catawba River
Ai
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
001 uyelrIg and Heat Set Operation 0.034 mgd Biological treatment with Chemical 3-A 1-Q
Non-Contact Goofing Water 0.040 mgd Addition and Filtration. z-E
S'nlrary 0.035 mgd Chlorination and Deuhlorinaliun 2-F
OFFICIAL USE ONLY(effluent guidelines sub-categories)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

9 `
CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
❑YES(complete the following table) ✓❑NO(go to Section III)
3.FREQUENCY 4.FLOW
a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mgd) (specify with units)
1.OUTFALL CONTRIBUTING FLOW (speck PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(list) (list) average) (spec average) AVERAGE DAILY AVERAGE DAILY (in days)
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
✓❑YES(complete Item III-B) ❑NO(go to Section M
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
./❑YES(complete Item III-C) ❑NO(go to Section IV)
C.If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION
2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE c.OPERATION,PRODUCT,MATERIAL,ETC. (list outfall numbers)
(spec)
0.034 MGD Textile Yarn Dyeing and Heat Setting 001
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
❑YES(complete the following table) ❑NO(go to Item IV-B)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
❑MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

•
EPA I.D.NUMBER(copy from hem I of Form 1)
CONTINUED FROM PAGE 2 NC0OO4812
V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
None
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
YES(list all such pollutants below) ❑✓ NO(go to Item VI-B)
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

•
CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
✓❑YES(ident fy the test(s)and describe their purposes below) ❑NO(go to Section VIII)
Ceriodaphnia dubia.Check for chronic toxicity of discharge.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
10 YES(list the name,address,and telephone number of and pollutants analyzed by, ❑NO(go to Section IX)
each such laboratory or firm below)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
Shealy Environmental Services 106 Vantage Point Drive 803-791-9111 2C test Copy included
West Columbia SC 29172
IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there
are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(type or print) M I)010 t B.PHONE NO.(area code&no.)
Tam L (D7aAJcs rn -4t- c9 c-I R 13 .. Z? l CJ
C.SIGNAT E D.DATE SIGNED
♦ram-- <k
EPA For -2C(8-90) PAGE 4 of 4

1 '
•
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy from Item I of Form I)
on separate sheets(use the same format)instead of completing these pages. NC0004812
SEE INSTRUCTIONS.
OUTFACE NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Fonn 2-C)
PART A—You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (specify((blank) (optional)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (If available) (favailable) AVERAGE VALUE
(1) (t) ' d.NO.OF a.CONCEN- tob.NO.OF
1.POLLUTANT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Biochemical Oxygen 202 � 178 52
Demand(BOD)
b.Chemical Oxygen 368 445 52
Demand(COD)
c.Total Organic Carbon 30 15 1
(TOC)
d.Total Suspended 44 54 52
Solids(TSS)
e.Ammonia(as N) 5.6 6.8 52
f.Flow VALUE 0.150 VALUE VALUE 365 VALUE
g.Temperature VALUE 16 VALUE VALUE 130 oC VALUE
(winter)
IL Temperature VALUE 28 VALUE VALUE 130 oC VALUE
(summer)
I pH MINIMU6 O MAXIMUM MINIM SMAXIM
UM 52 STANDARD UNITS
PART B— Mark"X"In column 2-a for each pollutant you know or have reason to believe Is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly,or indirectly but expressly,In an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant.For other pollutants for which you mark column 2a,you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE
AND a. b, a.MAXIMUM DAILY VALUE (if available) (If available) VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of-available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide v
(24959-67-9)
b.Chlorine,Total x 30
Residual
o.Color `X 70
d.Fecal Coliform 7� 50
Fluoridee.(1
(16984-48 ,-8) X 0.53
f.Nitrate-Nitrite(as N) 2 2 1.87
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

•
ITEM V-S CONTINUED FROM FRONT
2.MARK"X 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
AND a. b. a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- 1 b.NO.OF
(favatlable) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen, \ ,
Total Organic(as X 17.14 52 mg/L
VI
h.Oil and
Grease
i.Phosphorus `
(as Total X 1.00 52 mg/L
(7723-14-0)
j.Radioactively
(1)Alpha,Total
(2)Beta,Total
(3)Radium,
Total
(4)Radium 226,
Total
k.Sulfate
Or SO.)
(14e08-79-6) 280 1 mg/L
I.Sulfide X
(as S)
m.Sulfite
(as SO,)
(14265-45-3)
n.Surfactants
o.Aluminum,
Total 6000
(7429-90-5) 1 ug/L
p.Barium,Total v 45(7440-39-3) ^ 1 ug/L
q.Boron,Total �/ 67
(7440-42-8) /� 1 ug/L
r.Cobaf,Total
(7445-4-4) 75 1 ug/L
s.Iron,Total �/
(7439-89-6) X 000 1 ug/L
t.Magnesium,
Total X 1700 1 ug/L
(7439-95-4)
u.Molybdenum,
Total �/
(7439-98-7) X
v.Manganese,
Total
(7439-96-5) 37 1 ug/L
w.Tin,Total \�
(7440-31-5) /\
z.Titanium,
Total X(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

•
EPA I.D.NUMBER(copy from Item I of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC0004812 001
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark"X"in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,nonprocess wastewater outfalls,and nonrequired GC/MS
fractions),mark"X"in column 2-b for each pollutant you know or have reason to believe is present.Mark'X'In column 2-c for each pollutant you believe Is absent.If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant If you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4 dinnrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions for
additional details and requirements.
2.MARK'X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BEUEVED BELIEVED (1) (i) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ilavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M.Antimony,Total X 53 1 ug/L
(7440-36-0)
2M.Arsenic,Total
(7440-38-2)
3M.Beryllium,Total
(744041-7)
4M.Cadmium,Total �/
(744043-9) �\
5M.Chromium, X 0.100 0.027 52 ug/L lbs.
Total(744047-3)
6M.Copper,Total X 35 1 ug/L
(744050-8)
7M.Lead,Total X
(7439-92-1)
8M.Mercury,Total \/
(7439-97-6) �\
9M.Nickel,Total X 6.4 1 ug/L
(7440-02-0)
10M.Selenium, X
Total(7782-49-2)
11M.Silver,Total X
(7440-22-4)
12M.Thallium, X
Total(7440-28-0)
(1744asrrs)Total X 420 1 ug/L
14M.Cyanide, �/
Total(57-12-5) X
15M.Phenols,Total X 0.297 0.013 52 mg/L lbs.
DIOXIN
2,3,7,8-Tetra \ / DESCRIBE RESULTS
chlorodibenzo-P- /X\
Dioxin(1764-01-6)
EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE

•
CONTINUED FROM THE FRONT
2.MARK'X' 3.EFFLUENT - 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(If available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-VOLATILE COMPOUNDS
IV.Accrolein v
(107-02-8)
2V.Acrylonitrile
(107-13-1) X
3V.Benzene v
(71-43-2)
m e l hero-
` ,
thyy!))Ether X
(542-88-1)
5V.Bromoform v
(75-25-2)
6V.
Tetrachloride
de
(56-23-5)
7V.Chlorobenzene X(108-90-7)
8V.Chlorodi-
bromomethene X
(124-48-1)
9V.Chloroethane X(75-00-3)
10V.2-Chloro-
ethyleinyl Ether X
(110-75-8)
11 V.Chloroform X
(67-66-3)
12V.Dichloro-
bromomethane X
(75-27-4)
13V.Dichloro-
di0uoromethane X
(75-71-8)
14V.1,1-Dichloro-
ethane(75-34-3) X
15V.1,2-Dichloro-
ethane(107-06-2)
16V.1,1-Dichloro-
v
ethylene(75-35-4)
17V.1,2-Dichloro- �/
propane(78-87-5)18V. /<
prop l,n-Dlohloro-
`
42 -6 X
(542-75-6) •
19V.Ethylbenzene X(100414)
20V.Methyl
Bromide(74-83-9)
21V.Methyl X
Chloride(74-87-3)
EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) - (I) d.NO.OF a.CONCEN- (1) b.NO.OF
(favailnhle) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS(continued)
22V.Methylene v
Chloride(75-09-2)
Tetrachloroethane X
(79-34-5)
24V.Telrachloro- �/
ethylene(127-18-4) /�
• 25V.Toluene X
• (108-88-3)
26V.1, Trans-Droh ` '
Dichloroethylene X
(156-60-5)
27V.1,1,1-Trichloro- �/
ethane(71-55-6)
28V.1,1,2-Trichloro- X
ethane(79-00-5)
29V Trichloro- �/
ethylene(79-01-6)
30V.Trichloro- ` '
Bu0roromethane X
(75-69-4)
31V.Vinyl Chloride
(75-01-4)
GC/MS FRACTION—ACID COMPOUNDS
IA.2-Chlorophenol X
• (95-57-8)
2A.2 4-Dichloro- �/
phenol(120-83-2)
3A.2,4-Dimethyl- X
phenol(105-67-9)
• 4A.4,6-Dinitro-O-
Cresol(534-52-1)
5A.2,4-Dinitro-
phenol �/
(51-28-5)
6A.2-Nitrophenol X
(88-75-5)
7A.4-Nitrophenol X
(100-02-7)
8A.P-Chloro-M- \/
Cresol(59-50-7) >\
9A.Pentachloro-
phenol(87-86-5)
10A.Phenol �/
(108-95-2) X\
11A.2 4,6-Trichloro-
phenol(88-05-2)
EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE

� y
CONTINUED FROM THE FRONT
2.MARK"X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (If available) VALUE(If available) AVERAGE VALUE
CAS NUMBER - TESTING BEUEVED BELIEVED (1) (I) (1) tl.NO.OF a.CONCEN- (1) b.NO.OF
(Ifm+oilable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS
113.Acenaphthene
(83-32-9) X
2B.Acenaphtylene >/
(208-96-8) /�
3B.Anthracene �/
(120-12-7) /X
4B.Benzldine v
(92-87-5) /X
5B.Benzo(a)
Anthracene �/
(56-55-3) /�
6B.Benzo(a) >/
Pyrene(50-32-8) /�
7B.3,4-Benzo-
8uoranthene X
(205-99-2)
88.Benzo(ghi) >/
Perytene(191-24-2)
98.Benzo(k)
Fluoranthene �/
(207-08-9) /�
10B.Bis(2-Chloro-
ethauy)Methane
(111-91-1)
11B.Bis(2-Chloro-
ethy)Ether >/
(11144-4)
12B.Bis(2-
C(doroaopropyl) �/
Ether(102-80-1) /�
BIs( el-he
hesyf)Phthalate
(117-81-7)
14B.4-Bromophenyl
Phenyl Ether >/
(101-55-3) X
158.Butyl Benzyl >/
Phthalate(85-68-7) /�
168.2-Chloro-
naphthalene �/
(91-58-7) /�
17B.4-Chloro-
phenyl Phenyl Ether �/
(7005-72-3) /�
18B.Chrysene >/
(218-01-9) /�
19B.Dibenzo(a,h)
Anthracene
(53-70-3) X
20B.1,2-Dichloro-
�/
benzene(95-50-1) /<
218.1,3-DI-chloro-
benzene(541-73-1) /X
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

•
CONTINUED FROM PAGE V-6
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(opbnna()
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a b. c a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (I I (1) •
(1) d.NO.OF a.CONCEN- (1) b.NO.OF
(faalable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
22B.1 4-Dichloro-
benzene(106-46-7)
236.3,3-Dichloro-
benzidine(91-94-1)
24B.Diethyl
Phthalate(84-66-2)
258.Dimethyl
Phthalate
(131-11-3)
• 268.Di-N-Butyl
Phthalate(84-74-2)
276.2,4-Din8ro-
toluene(121-14-2)
28B.2,6-Dinitro-
toluene(606-20-2)
29B.Di-N-Octyl •
Phthalate(117-84-0)
306.1,2-Diphenyl •
-
hydrazine(as Azo-
benzene)(122-66-7)
318.Fluorenthene
(206-44-0)
32B.Fluorene
(86-73-7)
338.Hexachloro-
benzene(118-74-1)
346.Hexachloro-
butadiene(87-68-3)
35B.Hexachloro-
cyclopentadiene
(77-47-4)
36B Hexachloro-
3thane(67-72-1)
378.Indeno
(1,2,3-cd)Pyrene
(193-39-5)
386.Isophorone
(78-59-1)
•
39B.Naphthalene
(91-20-3)
408.Nitrobenzene v
(98-95-3)
41B.N-Nitro-
sodimethylamine
(62-75-9)
428.N-Nitrosodi-
N-Propylamine
(621-64-7)
EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BEUEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N-Nilro-
sodiphenylamine
(86-30-6)
44B.Phenanthrene X
(85-01-8)
45B.Pyrene
(129-00-0)
468.1,2,4-Tri-
chlorobenzene
(120-82-1)
GC/MS FRACTION—PESTICIDES
1P.Aldan X
(309-00-2)
2P.a-BHC X
(319-84-6)
3P.p-BHC X
(319.85-7)
4P.y-BHC >/
(58-89-9)
5P.8-BHC X(319-86-8)
6P.Chlordane v
(57-74-9)
7P.4,4'-DDT �/
(50-29-3) X
8P.4,4'-DDE X(72-55-9)
9P.4,4'-DDD �/
(72-54-8) /<
10P.Dieldrin v
(60-57-1)
11P.a-Enosulfan X(115-29-7)
12P. -Endosutfan X(115-29-7)
13P.Endosulfan
Sulfate �/
(1031-07-8) /�
14P.Endrin X
(72-20-8)
15P.Endrin
Aldehyde
(7421-93-4)
16P.Heptachlor �/
(76-44-8) �\
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

a
EPA LD.NUMBER(cropyfrom Item I of Form I) OUTFALL NUMBER
NC00048121 001
CONTINUED FROM PAGE V-8
2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (I) • (1) 9.NO.OF a.CONCEN- III b.NO.OF
Waved/able) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS _CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—PESTICIDES(continued)
17o.Heptachlor X
Epoxide
(1024-57-3)
18P.PCB-1242 X
(53469-21-9)
19P.PCB-1254 X
(11097-69-1)
20P.PCB-1221 X
(11104-28-2)
21P.PCB-1232 X
(11141-16-5)
22P.PCB-1248 X
(12672-29-6)
23P.PCB-1260 X
(11096-82-5)
24P.PCB-1016 X
(12674-11-2)
25P.Toxaphene X
(8001-35-2)
EPA Form 3510-2C(8-90) PAGE V-9

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NC0004812
Pharr Yarns Industrial WWTP Facility x
Location
State Grid/Quad: F 14 SE/MT Holly,NC
Latitude: 35°15'40"N Longitude: 81°04'39"W
Receiving Stream: South Fork Catawba River Sub-Basin: 03-08-34 North
�,*�2 Map not to scale
Drainage Basin: Catawba River Basin Stream Class: WS-V 1 b Gaston County

Please print or type in the unshaded areas only
(fill-in areas are spaced for elite type, i.e., 12 characters/inch). For Approved. OMB No. 2040-0086. Approval expires 5-31-92
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER
\"iEPA GENERAL INFORMATION F NC0004812 TtA o
Consolidated Permits Program
GENERAL (Read the "General Instructions"before starting.) 1 2 13 14 15
LABEL ITEMS GENERAL INSTRUCTIONS
If a preprinted label has been provided,
I. EPA I.D. NUMBER affix it in the designated space. Review the
information carefully; if any of it is
incorrect cross through it and enter the
III. FACILITY NAME correct data in the appropriate fill-in area
below.Also, if any of the preprinted data is
absent (the area to the left of the label
V. FACILITY PLEASE PLACE LABEL IN THIS SPACE space fists the information that should
a a ear) please provide it in the proper fill-
MAILING LIST in area(s) below. If the label is complete
and correct you need not complete Items
I, Ill, V, and VI(except Vl-B which must be
completed regardless). Complete all items
VI. FACILITY if no label has been proved. Refer to the
LOCATION instructions for detaied item descriptions
and for the legal authorization under which
this data is collected.
II. POLLUTANT CHARACTERISTICS
INSTRUCTION : omplete A through J to determine whether you need to submit any permit application orms to the EPA. If you answer"yes"to any
questions,you must submit this form and the supplemental from listed in the parenthesis following the question. Mark"X"in the box in the third column if
the supplemental form is attached. If you answer"no"to each question,you need not submit any of these forms. You may answer"no"if your activity is
excluded from permit requirements;see Section C of the instructions.See also,Section D of the instructions for definitions of bold-faced terms.
SPECIFIC QUESTIONS MARK"X" MARK
SPECIFIC QUESTIONS MARK"X"FORM
YES NO YES NO
ATTACHED ATTACHED
•
A. Is this facility a publicly owned treatment works B. Does or will this facility (either existing or
which results in a discharge to waters of the ❑ x ❑ proposed) include a concentrated animal ❑ X ❑
U.S.?(FORM 2A) feeding operation or aquatic animal
production facility which results in a discharge
16 : 17 18 to waters of the U.S.?(FORM 2B) ----19 20 21
C. Is this facility which currently results in ❑ ' X El D. Is this proposal facility(other than those described ❑ X Eldischarges to waters of the U.S. other than in A or B above)which will result in a discharge
those described in A or B above?(FORM 2C) 22 23 24 to waters of the U.S.?(FORM 2D) 25 26 27
E. Does or will this facility treat, store, or dispose of F. Do you or will you inject at this facility industrial or
hazardous wastes?(FORM 3) ❑ X ❑ municipal effluent below the lowermost stratum ❑ x ❑
containing, within one quarter mile of the well
bore, underground sources of drinking water?
28 29 30 (FORM 4) 31 32 33
G. Do you or will you inject at this facility any H. Do you or will you inject at this facility fluids for
produced water other fluids which are brought to special processes such as mining of sulfer by the
the surface in connection with conventional oil or ❑ X ❑ Frasch process,solution mining of minerals,in ❑ X ❑
natural gas production, inject fluids used for situ combustion of fossil fuel,or recovery of
enhanced recovery of oil or natural gas, or inject geothermal energy?(FORM 4)
fluids for storage of liquid hydrocarbons?
(FORM 4) 34 I 35 36 37 38 39
I. Is this facility a proposed stationary source 1J. Is this facility a proposed stationary source
which is one of the 28 industrial categories listed X which is NOT one of the 28 industrial categories ❑ X El
the instructions and which will potentially emit ❑ ❑ listed in the instructions and which will potentially
100 tons per year of any air pollutant regulated emit 250 tons per year of any air pollutant
under the Clean Air Act and may affect or be . regulated under the Clean Air Act and may affect -
located in an attainment area? FORM 5 40 41 42 or be located in an attainment are? FORM 5 43 44 45
III. NAME OF FACILITY
D SKIP Pharr Yarns, LLC Industrial Wastewater Treatment Plant
1
15 16-29 30 69
IV. FACILITY CONTACT
A. NAME&TITLE(last, first, &title) B. PHONE(area code&no.)
D Davis James, Enviro. Manager 704 823 2310
2
15 16 45 ' 46 48 49 51 52 55
V. FACILITY MAILING ADDRESS
A. STREET OR P.O. BOX
3 P.O. Box 1939
15 16 45
B. CITY OR TOWN C.STATE D.ZIP CODE
c McAdenville NC 28101
4
15 16 40 41 42 47 51
VI. FACILITY LOCATION
A. STREET, ROUTE NO.OR OTHER SPECIFIC IDENTIFIER
c 149 Willow Drive
15 16 45
B. COUNTY NAME
Gaston
46 70
C. CITY OR TOWN D. STATE E.ZIP CODE F.COUNTY CODE
c McAdenville NC 28101
6
15 16 40 41 42 47 51 52 54
EPA FORM 3510-1 (8-90) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII. SIC CODES (4-digit, in order of.riorit )
A. FIRST B. SECOND
(specify) 7 (specify)
7 7
15 16 17 15 16 19
C.THIRD D. FOURTH
(specify) 7 (specify)
7 7
15 16 17 15 16 19
VIII. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
c Pharr Yarns, LLC VIII-A also the owner?
8 ❑ VES X❑NO
18 19 55
C. STATUS OF OPERATOR(Enter the appropriate letter into the answer box;if"Other,"specify.) D. PHONE(area code&no.)
F=FEDERAL M=PUBLIC(other than federal or state) p (specify) C 704 823 2310
S=STATE 0=OTHER(specify) A
P=PRIVATE 56 15 16 18 19 21 22 25
E. STREET OR PO BOX
P.O. Box 1939
26 55
F. CITY OR TOWN G. STATE H.ZIP CODE IX. INDIAN LAND
c McAdenville NC 28101 Is the facility located on Indian lands?
0 YES X❑ NO
15 16 40 42 42 47 51
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDES (Discharges to Surface Water) D. PSD(Air Emissions from Proposed Sources)
9 N 1 NC0004812 CC TT 8
15 16 17 18 30 15 16 17 18 30
B. UIC(Underground Injection of Fluids E.OTHER(specify) (Specify)
C T I C T 8
9 U 9
15 16 17 18 30 15 16 17 18 30
C. RCRA(Hazardous Wastes) E.OTHER(specify) (Specify)
C T I C T 8
9 R 9
15 16 17 18 30 15 16 17 18 30
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the ma• area. See instructions for •recise re•uirements.
XII. NATURE OF BUSINESS (•rovide a brief descri.tion)
Pharr is a manufacturer of carpet and specialty yarns.
XIII. CERTIFICATION (see instructions)
1 certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fine imprisonment.
A. NAME&OFFICIAL TITLE(type or print) B. S NATURE C. DATE SIGN D
dVI,P_iJ L V f L%k�' C i /
COMMENTS FOR OFFICIAL USE ONLY
C
C
15 16 55
EPA FORM 3510-1 (8-90)

•
EPA I.D.NUMBER(copy from Item I of-Form I) Form Approved.
NC0004812 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
APPLICATIO
FOR PERMIT TO DISCHARGE WASTEWATER
2C k'kEPA EXISTING MANUFACTURING,JCOMMERCIAL,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFACE LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3 SEC. D.RECEIVING WATER(Home)
J01 :3 /.r l yG �i/V gi'` C? ' 3(i`t,.1 South Fork of Catawba River
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(hq) (include units) a.DESCRIPTION TABLE 2C-1
001 uyeing and Neat Set Operation 0.034 mgd Biological treatment with Ctlernical 3-n 1-0
Non-contact cootIng Water 0.040 mgd Addition and Filtration. 2 E
Sant'ra y 0.035 mgd Chlorination arid Deellluriiidtioil 2-F
OFFICIAL U E ONLY((effluent�idelinessub-cate ories
>
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
❑YES(complete the following table) ✓❑NO(go to Section III)
3.FREQUENCY 4.FLOW
a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mgd) (specify with units)
1.OUTFALL CONTRIBUTING FLOW (specify PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(list) (list) average) (specify average) AVERAGE DAILY AVERAGE DAILY (in days)
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
✓❑YES(complete Item III-B) ❑NO(go to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
✓❑YES(complete Item III-C) ❑NO(go to Section IV)
C.If you answered"yes"to Item Ill-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION 2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE C.OPERATION,PRODUCT,MATERIAL,ETC. (list outfall numbers)
(spec)
0.034 MGD Textile Yarn Dyeing and Heat Setting 001
IV.IMPROVEMENTS
A. Are you now required by arty Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
❑YES(complete the following table) ❑✓ NO(go to Item IV-B)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
❑MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copy from hem I of Form I)
CONTINUED FROM PAGE 2 NCOOO4812
V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
None
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
❑YES(list all.such pollutants below) LINO(go to Item VI-B)
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
❑✓ YES(identify the test(s)and describe their purposes below) ❑NO(go to Section VII/)
Ceriodaphnia dubia. Check for chronic toxicity of discharge.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
YES(list the name,address,and telephone number of and pollutants analyzed by, ❑NO(go to Section IX)
each such laboratory or firm below)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
Shealy Environmental Services 106 Vantage Point Drive 803-791-9111 2C test Copy included
West Columbia SC 29172
IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there
are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(type or print) &dl L j .t 2 D B.PHONE NO.(area code&no.)
L j)( c iv►nlc A C. t"✓L : O L( Z 3 ,. Z 3
C.SIGNATUR j D.DATE SIG ED
EPA Form (8-90) PAGE 4 of 4
Il

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy from Item I of Form I)
on separate sheets(use the same format)instead of completing these pages. NC0004812
SEE INSTRUCTIONS. I
OUTFALL NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C)
PART A—You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (speciifblank) (optional)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
Ill (I) d.NO.OF a.CONCEN- Ill b.NO.OF
1.POLLUTANT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Biochemical Oxygen 202 178 52
Demand(BOD)
b.Chemical Oxygen 368 445 52
Demand(COD)
c.Total Organic Carbon 30 15 1
(TOC)
d.Total Suspended 44 54 52
Solids(TSS)
e.Ammonia(as M 5.6 6.8 52
f Flow VALUE 0.150 VALUE VALUE 365 VALUE
g.Temperature VALUE 16 VALUE VALUE 130 oC VALUE
(winter)
h.Temperature VALUE 28 VALUE VALUE 130 aC VALUE
(summer)
UMi.pH MINIM6.0 MAXIMUM MINIM 6.0 MAXIMUM 52 STANDARD UNITS
PART B— Mark'X"in column 2-a for each pollutant you know or have mason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly,or indirectly but expressly,in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant.For other pollutants for which you mark column 2a,you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE
AND a. b. a.MAXIMUM DAILY VALUE (if available) (if available) VALUE
CAS NO. BELIEVED BELIEVED (II (1) (1) d.NO.OF a.CONCEN- Ill b.NO.OF
(if available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide v
(24959-67-9)
b.Chlorine,Total >/ 30
Residual
a Color `X 70
d.Fecal Conform 7( 50 ',
e.Fluoride
(16984-48-8) X 0.53
f.Nitrate-Nitrite(as M �\\/ 2.2 1.87
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
AND a. b. a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(favai(ob(e) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen, ` /
Total organic(as X 17.14 52 mg/L
•
h.Oil and
Grease
I.Phosphorus ` ,
(as P),Total X 1.00 • 52 mg/L
(7723-14-0)
j.Radioactivity
(I)Alpha,Total
(2)Beta,Total
(3)Radium,
Total
(4)Radium 226,
Total
k.Sulfate
(or SO( X 280 1 mg/L
(14808-79-8)
I.Sulfide X
as S)
m.Sulfite
(os SOi) X
(14265-45-3)
n.Surfactants
o.Aluminum,
Total X 6000 1 ug/L
(7429-90-5)
p.Barium,Total ug/L 45 1 u /L
(7440-39-3)
q.Boron,Total
(7440-42-8) X 67 1 ug/L
•
r.Cobalt,Total �/
(7440-48-4) X 75 1 ug/L
s.Iron,Total �/
(7439-89-6) X 1000 1 ug/L
1.Magnesium, X
Total 1700 1 ug/L
(7439-95-4)
u.Molybdenum,
Total X
(7439-98-7)
v.Manganese, X
Total 37 1 ug/L
(7439-96-5)
w.Tin,Total X
(7440-31-5)
x.Titanium,
Total X
(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copy from Oem l of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC0004B12 001
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark'X'in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,nonprocess wastewater outfalls,and nonrequired GC/MS
fractions),mark"X"in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each pollutant you believe is absent.If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein.acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must ether submit at least one analysis or •
briefly describe the reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions for
additional details and requirements.
2.MARK"X“ 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M.Antimony,Total
(7440-36-0) X 53 1 ug/L
2M.Arsenic,Total v
(7440-38-2)
3M.Beryllium,Total
(7440-41-7)
4M.Cadmium,Total v
(7440-43-9)
TM.Chrom1( 4 0.100 0.027 52 ug/L lbs.
Total(7440-47-3) g
6M.Copper,Total(7440-50-8) X 35 1 ug/L
7M.Lead,Total v
(7439-92-1)
BM.Mercury,Total v
(7439-97-0)
9M.Nickel,Total X 6.4 1 ug/L
(7440-02-0)
10M.Selenium,
Total(778249-2)
11 M.Silver,Total �/
(7440-22-4) /�
12M.Thallium, v
Total(7440-28-0)
13M.Zinc,Total
(7440-66-6) X 420 1 ug/L
14M.Cyanide, v
Total(57-12-5)
Total Phenols, X 0.297 0.013 52 mg/L lbs.
DIOXIN
2,3,7,8-Tetra- \ / DESCRIBE RESULTS
chlorodibenzo-P- ,X\
Dioxin(1764-01-6)
EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE

•
CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT _ 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) 'd.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS
IV.Accrolein �/
(107-02-8)
2V.Acrylonhrile v
(107-13-1)
3V.Benzene v
(71.43-2)
methyl)Ether X(542-88-I)
5V.Bromoform
(75-25-2)
6V.Carbon
Tetrachloride
(56-23-5)
7V.Chlorobenzene �/
(108-90-7)
C
bro no m tha \
bromomethane /X\
(124-48-1)
9V.Chloroethane
(75-00-3)
10V.2-Chloro-
ethylvinyl Ether
(110-75-8)
11 V.Chloroform v
(67-66-3)
12V.Dichloro-
bromomethane
(75-27-4)
13V.Dichloro-
di8uoromethane
(75-71-8)
14V.1,1-Dichloro-
ethane(75-34-3) X 15V.1,2-Dichloro-
ethane(107-06-2) v
16V.1,1-Dichloro-
ethylene(75-35-4)
17V.1,2-Dichloro- �/
propane(78-87-5)
l,iDichloro-
prop `
propylene X
(542-75-6)
19V.Ethylbenzene �/
(100-41-4)
20V.Methyl
Bromide(74-83-9)
21V.Methyl
Chloride(74-87-3)
EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
• AND a. b, e. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION CONCENTRATION (1) ANALYSES TRATION b.MASS CONCENTRATIONANALYSES
(2)MASS (2)MASS CONCENTRATION (2)MASS (2)MASS
GC/MS FRACTION—VOLATILE COMPOUNDS(continued)
22V.Methylene
Chloride(75-09-2)
Tetrachloroethane X
(79-34-5)
24V.Tetrachloro- �/
ethylene(127-184)
25V.Toluene
(108-88-3)
26V.1,2-Trans- ` ,
Dichloroethylene X
(156-605)
27V.I,t,1-Trichloro- �/
ethane(71-55-6)
28V.1,1,2-Trichloro- X ethane(79-00-5)
29V Trichloro-
ethylene v
(79-01-6)
30V.Trichloro- ` ,
Ouoromethane X
(75-69-4)
31V.Vinyl Chloride
(75-01-4)
GC/MS FRACTION—ACID COMPOUNDS
IA.2-Chlorophenol �/
(95-57-8)
2A.2,4-Dichloro-
phenol(120-83-2)
3A.2,4-Dimethyl-
phenol(105-67-9)
4A.4,6-Dinitro-O- \/
Cresol(534-52-1) �\
5A.2,4-Dinitro-
phenol �/
(51-28-5)
6A.2-Nitrophenol X
(88-75-5)
7A.4-Nitrophenol v
(100-02-7)
8A.P-Chloro-M-
Cresol(59-50-7)
9A.Pentachloro-
phenol(87-86-5)
10A.Phenol �/
(108-95-2)
11A.2,4,6-Trichloro-
phenol(88-05.2)
EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE

•
CONTINUED FROM THE FRONT
2.MARK"X" _ 3.EFFLUENT 4.UNITS 5.INTAKE(oplionafl
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) 'b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS
113.Acenaphthene X
(83-32-9)
28.Acenaphtylene X
(208-96-8)
3B.Anthracene X
(120-12-7)
48.Benzidine �/
(92-87-5) X
58.Benzo(a)
Anthracene X
(56-55-3)
6B.Benzo(a) X
Pyrene(50-32-8)
78.3,4-Benzo-
8uoranthene X
(205-99-2)
813.Benzo(ghi) >/
Perylene(191-24-2) X
9B.Benzo(k)
Fluoranthene X
(207-08-9)
10B.Bis(2-Ch/ono-
ethonv)Methane X
(111-91-1)
11 B.Bis(2-Chloro-
ethyl)Ether X
(111-44-4)
12B.Bis(2-
Chloroisopr py0 X
Ether(102-80-1)
13B.Bis(2-Ethyl- X
hazy/)Phthalate
(117-81-7)
148.4-Bromophenyl
Phenyl Ether X
(101-55-3)
15B.Butyl Benzyl X
Phthalate(85-68-7)
•
16B.2-Chloro-
naphthalene X
(91-58-7)
17B.4-Chloro-
phenyl Phenyl Ether X
(7005-72-3)
18B.Chrysene X
(218-01-9)
19B.Dibenzo(a,h)
Anthracene X
(53-70-3)
208.1,2-Dichloro- X
benzene(95-50-1)
218.1,3-Di-chloro- �/
benzene(541-73-1) /<
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE C.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
available REQUIRED PRESENT ABSENT CONCENTRATION NT NT ANALYSES TRATION b.MASS (1) ANALYSES
(! ) (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continuer)
22B.1,4-Dichloro-
benzene(106-46-7)
23B.3,3-Dichloro-
benzidine(91-94-1)
24B.Diethyl
Phthalate(84-66-2)
256.Dimethyl
Phthalate
(131-11-3)
26B.Di-N-Butyl v
Phthalate(84-74-2)
2713.2,4-Dinitro-
toluene(121-14-2)
28B.2,6-Dinhro- v
toluene(606-20-2)
298.Di-N-Octyl v
Phthalate(117-84-0)
30B.1,2-Diphenyl-
hydrazine(as Azo-
benzene((122-66-7)
31B.Fluoranthene v
(206-44-0)
32B.Fluorene v
(86-73-7)
33B.Hexachloro-
benzene(118-74-1)
34B.Hexachloro- v
butadiene(87-68-3)
358.Hexachloro-
cyclopentadiene X 1
(77-47-4)
36B Hexachloro- v
ethane(67-72-1)
(193-39-5)
38B.Isophorone v
(78-59-1)
39B.Naphthalene >/
(91-20-3)
40B.Nitrobenzene X(98-95-3)
b. yso dimethethylalamine X
(62-75-9)
42B.N-Nitrosodi-
N-Propylamine
(621-64-7)
EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) REOUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N-Nhro-
sodiphenylamine
(86-30-6)
44B.Phenanthrene
(85-01-8)
456.Pyrene
(129-00-0) n
46B.1,2,4-Tri-
chlorobenzene �/
(120-82-1)
GC/MS FRACTION—PESTICIDES
P.Aldrin(309-00-2)
v
309-00-2)
2P.a-BHC �/
(319-84-6) �\
3P.9-BHC X
(319-85-7)
4P.y-BHC v
(58-89-9)
5P.&BHC
(319-86-8)
6P.Chlordane �/
(57-74-9)
7P.4,4'-DDT X
(50-29-3)
8P.4,4'-DDE v
(72-55-9)
9P.4,4'-DDD v
(72-54-8)
10P.Dieldrin v
(60-57-1)
11P.a-Enosulfan v
(115-29-7)
12P.5-Endosulfan
(115-29-7)
13P.Endosulfan
Sulfate X(1031-07-8)
14P.Endrin �/
(72-20-8)
15P.Endrin
Aldehyde >/
(7421-93-4) X
16P.Heptachlor �/
(76-44-8)
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
NC00048121 001
CONTINUED FROM PAGE V-8
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) • (1) d.NO.OF a.CONCEN- (1) b.NO.OF
wailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—PESTICIDES(continued)
o.Heptachlor E ` '
Epoxide X
(1024-57-3) -
18P.PCB-1242 \/
(53469-21-9) >\
19P.PCB-1254 v
(11097-69-1)
20P.PCB-1221 \/ - -
(11104-28-2) X\
21P.PCB-1232 \/
(11141-16-5) �\
22P.PCB-1248 - -
(12672-29-6) _
23P.PCB-1260 v
(11096-82-5)
24P.PCB-1016 - -
(12674-11-2)
25P.Toxaphene
(8001-35-2)
EPA Form 3510-2C(8-90) PAGE V-9

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NC0004812
Pharr Yarns Industrial WWTP Facility x
Location
State Grid/Quad: F 14 SE/MT Holly,NC
Latitude: 35°15'40"N Longitude: 81°04'39"W Mapnot to scale
Receiving Stream: South Fork Catawba River Sub-Basin: 03-08-34 JOY,��Z
I)rainage Basin: Catawba River Basin Stream Class: WS-V North Gaston County

SIIEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Pharr Yarns, Inc.
PO Box 1939
McAdenville, NC 28101
Attention: James Davis
Project Name: McAdenville 2C Permit Renewal
Lot Number:TK08047
Date Completed:12/06/2018
12/06/2018 3:15 PM
Approved and released by:
Project Manager: Grant Wilton
..
TNIi
BORptoP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page I of 45

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Case Narrative
Pharr Yarns, Inc.
Lot Number: TK08047
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy')Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy policies. Any
exceptions to the NELAC standards,the QAMP, SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Semivolatile Organic Analysis—Method 625.1
The sample was analyzed at a 10X dilution due to the high concentration of non-target analytes present.
The reporting limits were raised accordingly.
Pesticide/PCB Analysis—Method 608.3
The sample was analyzed for PCB's at a 10X dilution due to the high concentration of non-target analytes
present. The reporting limits were raised accordingly. Low surrogate recoveries due to matrix
interference.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172(803)791-9700 Fax[phone] www.shealylab.com
Page 2 of 45

SHEALY ENVIRONMENTAL ONMENTAL SERVICES, INC.
�
Sample Summary
Pharr Yarns, Inc.
Lot Number: TK08047
Project Name: McAdenville 2C Permit Renewal
Project Number:
Sample Number Sample ID Matrix Date Sampled Date Received
001 Effluent Aqueous 11/08/2018 0900 11/08/2018
002 Effluent Aqueous 11/08/2018 0900 11/08/2018
(2 samples)
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Page 3 of 45

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
' Pharr Yarns, Inc.
Lot Number: TK08047
Project Name: McAdenville 2C Permit Renewal
Project Number:
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 Effluent Aqueous Bromide 300.0 0.60 mg/L 5
001 Effluent Aqueous Fluoride 300.0 0.56 mg/L 5
001 Effluent Aqueous Sulfate 300.0 280 mg/L 5
001 Effluent Aqueous TOC SM 5310C- 30 mg/L 5
001 Effluent Aqueous Aluminum 200.8 6000 ug/L 10
001 Effluent Aqueous Antimony 200.8 53 ug/L 10
001 Effluent Aqueous Barium 200.8 45 ug/L 10
001 Effluent Aqueous Boron 200.8 67 ug/L 10
001 Effluent Aqueous Chromium 200.8 15 ug/L 10
001 Effluent Aqueous Cobalt 200.8 75 ug/L 10
001 Effluent Aqueous Copper 200.8 35 ug/L 10
001 Effluent Aqueous Iron 200.8 1000 ug/L 10
001 Effluent Aqueous Magnesium 200.8 1700 ug/L 10
001 Effluent Aqueous Manganese 200.8 37 ug/L 10
001 Effluent Aqueous Nickel 200.8 6.4 ug/L 10
001 Effluent Aqueous Zinc 200.8 420 ug/L 10
002 Effluent Aqueous MBAS(calculated as LAS) SM 5540C- 0.32 mg MBAS/L 11
002 Effluent Aqueous Platinum-Cobalt Color SM 2120B- 25 color units 11
(18 detections)
i
1
I
1
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106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 4 of 45

Inorganic non-metals
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-001
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Bromide)300.0 1 11/27/2018 2248 SLU 90748
2 (Fluoride)300.0 5 11/30/2018 1556 HKL 91082
2 (Sulfate)300.0 5 11/30/2018 1556 HKL 91079
1 (TOC)SM 5310C-2011 10 11/09/2018 2030 DMA 89159
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Bromide 300.0 0.60 0.20 mg/L 1
Fluoride 16984-48-8 300.0 0.56 0.50 mg/L 2
Sulfate 300.0 280 5.0 mg/L 2
TOC SM 5310C- 30 10 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
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106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 5 of 45

Semivolatile Organic Compounds by GC/MS
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-001
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 10 1 11/25/2018 2056 CMP2 11/13/2018 1856 89450
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 625.1 ND 16 ug/L 1
Acenaphthylene 208-96-8 625.1 ND 16 ug/L 1
Anthracene 120-12-7 625.1 ND 16 ug/L 1
Benzidine 92-87-5 625.1 ND 80 ug/L 1
Benzo(a)anthracene 56-55-3 625.1 ND 16 ug/L 1
Benzo(a)pyrene 50-32-8 625.1 ND 16 ug/L 1
Benzo(b)fluoranthene 205-99-2 625.1 ND 16 ug/L 1
Benzo(g,h,i)perylene 191-24-2 625.1 ND 16 ug/L 1
Benzo(k)fluoranthene 207-08-9 625.1 ND 16 ug/L 1
4-Bromophenyl phenyl ether 101-55-3 625.1 ND 16 ug/L 1
Butyl benzyl phthalate 85-68-7 625.1 ND 16 ug/L 1
bis(2-Chloro-1-methylethyl)ether 108-60-1 625.1 ND 16 ug/L 1
4-Chloro-3-methyl phenol 59-50-7 625.1 ND 16 ug/L 1
bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 16 ug/L 1
bis(2-Chloroethyl)ether 111-44-4 625.1 ND 16 ug/L 1
2-Chloronaphthalene 91-58-7 625.1 ND 16 ug/L 1
2-Chlorophenol 95-57-8 625.1 ND 16 ug/L 1
4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 16 ug/L 1
Chrysene 218-01-9 625.1 ND 16 ug/L 1
Dibenzo(a,h)anthracene 53-70-3 625.1 ND 16 ug/L 1
1,2-Dichlorobenzene 9550-1 625.1 ND 16 ug/L 1
1,3-Dichlorobenzene 54173-1 625.1 ND 16 ug/L 1
1,4-Dichlorobenzene 106-46-7 625.1 ND 16 ug/L 1
3,3'-Dichlorobenzidine 91-94-1 625.1 ND 80 ug/L 1
2,4-Dichlorophenol 120-83-2 625.1 ND 16 ug/L 1
Diethylphthalate 84-66-2 625.1 ND 16 ug/L 1
Dimethyl phthalate 131-11-3 625.1 ND 16 ug/L 1
2,4-Dimethylphenol 105-67-9 625.1 ND 16 ug/L 1
Di-n-butyl phthalate 84-74-2 625.1 ND 16 ug/L 1
4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 80 ug/L 1
1 2,4-Dinitrophenol 51-28-5 625.1 ND 80 ug/L 1
2,4-Dinitrotoluene 121-14-2 625.1 ND 32 ug/L 1
2,6-Dinitrotoluene 606-20-2 625.1 ND 32 ug/L 1
Di-n-octylphthalate 117-84-0 625.1 ND 16 ug/L 1
1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 16 ug/L 1
bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 80 ug/L 1
Fluoranthene 206-44-0 625.1 ND 16 ug/L 1
Fluorene 86-73-7 625.1 ND 16 ug/L 1
Hexachlorobenzene 118-74-1 625.1 ND 16 ug/L 1
Hexachlorobutadiene 87-68-3 625.1 ND 16 ug/L 1
Hexachlorocyclopentadiene 77-47-4 625.1 ND 80 ug/L 1
Hexachloroethane 67-72-1 625.1 ND 16 ug/L 1
Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 16 ug/L 1
Isophorone 78-59-1 625.1 ND 16 ug/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quartitation of compound exceeded the calibration range
ND=Not detected at or above the LOG N=Recovery is out of criteria P=The'RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 6 of 45

Semivolatile Organic Compounds by GC/MS
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-001
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 10 11/25/2018 2056 CMP2 11/13/2018 1856 89450
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Naphthalene 91-20-3 625.1 ND 16 ug/L 1
Nitrobenzene 98-95-3 625.1 ND 16 ug/L 1
2-Nitrophenol 88-75-5 625.1 ND 32 ug/L 1
4-Nitrophenol 100-02-7 625.1 ND 80 ug/L 1
N-Nitrosodimethylamine 62-75-9 625.1 ND 16 ug/L 1
N-Nitrosodi-n-propylamine 621164-7 625.1 ND 16 ug/L 1
N-Nitrosodiphenylamine(Diphenylamine) 86I.30-6 625.1 ND 16 ug/L 1
Pentachlorophenol 87-86-5 625.1 ND 80 ug/L 1
Phenanthrene 85-01-8 625.1 ND 16 ug/L 1
Phenol 108-95-2 625.1 ND 16 ug/L 1
Pyrene 129-00-0 625.1 ND 16 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 625.1 ND 16 ug/L 1
2,4,6-Trichlorophenol 88-06-2 625.1 ND 16 ug/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
2-Fluorobiphenyl 58 37-129
2-Fluorophenol 32 24-127
Nitrobenzene-d5 46 38-127
Phenol-d5 37 28-128
Terphenyl-d14 42 10-148
2,4,6-Tribromophenol 58 41-144
1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 7 of 45
I

Organochlorine Pesticides and PCBs
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-001
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 608.3 3665A 608.3 10 11/20/2018 1808 CHG 11/15/2018 1714 89666
2 608.3 3665A 608.3 1 11/17/2018 1722 CHG 11/15/2018 1714 89666
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aldrin 309-00-2 608.3 ND 0.40 ug/L 1
Aroclor 1016 12674-11-2 608.3 ND 0.40 ug/L 2
Aroclor 1221 11104-28-2 608.3 ND 0.40 ug/L 2
Aroclor 1232 11141-16-5 608.3 ND 0.40 ug/L 2
Aroclor 1242 53469-21-9 608.3 ND 0.40 ug/L 2
Aroclor 1248 12672-29-6 608.3 ND 0.40 ug/L 2
Aroclor 1254 11097-69-1 608.3 ND 0.40 ug/L 2
Aroclor 1260 11096-82-5 608.3 ND 0.40 ug/L 2
gamma-BHC(Lindane) 58-89-9 608.3 ND 0.40 ug/L 1
alpha-BHC 319-84-6 608.3 ND 0.40 ug/L 1
beta-BHC 319-85-7 608.3 ND 0.40 ug/L 1
delta-BHC 319-86-8 608.3 ND 0.40 ug/L 1
Chlordane 57-74-9 608.3 ND 4.0 ug/L 1
4,4'-DDD 72-54-8 608.3 ND 0.40 ug/L 1
4,4'-DDE 72t55-9 608.3 ND 0.40 ug/L 1
4,4'-DDT 50f29-3 608.3 ND 0.40 ug/L 1
Dieldrin 60-57-1 608.3 ND 0.40 ug/L 1
Endosulfan I 959-98-8 608.3 ND 0.40 ug/L 1
Endosulfan II 33213-65-9 608.3 ND 0.40 ug/L 1
Endosulfan sulfate 1031-07-8 608.3 ND 0.40 ug/L 1
Endrin 72-20-8 608.3 ND 0.40 ug/L 1
Endrin aldehyde 7421-93-4 608.3 ND 0.40 ug/L 1
Heptachlor 76-44-8 608.3 ND 0.40 ug/L 1
Heptachlor epoxide 1024-57-3 608.3 ND 0.40 ug/L 1
Toxaphene 8001-35-2 608.3 ND 4.0 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q %Recovery Limits Q %Recovery Limits
Decachlorobiphenyl 31 20-131 N 19 20-131
Tetrachloro-m-xylene 43 30-132 47 30-132
1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
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106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 8 of 45

CVAA
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-001
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 245.1 1 11/17/2018 1341 JCF 11/15/2018 1512 89588
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Mercury 7439-97-6 245.1 ND 0.00020 mg/L 1
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
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Page 9 of 45

1
ICP-MS
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-001
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 200.2 200.8 1 12/02/2018 0857 BNW 11/15/2018 1718 89657
2 200.2 200.8 1 12/05/2018 0010 BNW 11/15/2018 1718 89657
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aluminum 7429-90-5 200.8 6000 40 ug/L 1
Antimony 7440-36-0 200.8 53 2.0 ug/L 1
Arsenic 7440-38-2 200.8 ND 2.0 ug/L 1
Barium 7440-39-3 200.8 45 5.0 ug/L 1
Beryllium 7440-41-7 200.8 ND 0.40 ug/L 1
Boron 7440-42-8 200.8 67 50 ug/L 2
Cadmium 7440-43-9 200.8 ND 0.50 ug/L 1
Chromium 7440-47-3 200.8 15 5.0 ug/L 1
Cobalt 7440-48-4 200.8 75 5.0 ug/L 1
Copper 7440-50-8 200.8 35 5.0 ug/L 1
Iron 7439 89-6 200.8 1000 50 ug/L 1
Lead 7439-92-1 200.8 ND 1.0 ug/L 1
Magnesium 7439-95-4 200.8 1700 400 ug/L 1
Manganese 7439-96-5 200.8 37 5.0 ug/L 1
Molybdenum 7439-98-7 200.8 ND 10 ug/L 1
Nickel 7440-02-0 200.8 6.4 5.0 ug/L 1
Selenium 7782-49-2 200.8 ND 5.0 ug/L 1
Silver 7440-22-4 200.8 ND 1.0 ug/L 1
Thallium 7440-28-0 200.8 ND 0.50 ug/L 1
Tin 7440-31-5 200.8 ND 20 ug/L 1
Titanium 7440-32-6 200.8 ND 5.0 ug/L 1
Zinc 7440-66-6 200.8 420 10 ug/L 1
1
I
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 10 of 45

Inorganic non-metals
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-002
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 10-204-00-1-X (Cyanide-To)SM 4500-CN E- 1 11/20/2018 1820 MSG 11/20/2018 1328 90145
1 (MBAS(calcul)SM 5540C-2011 1 11/09/2018 1938 KFE 11/09/2018 1840
1 (Platinum-Cob)SM 2120E-2011 1 11/03/2018 1148 KFE
1 (Sulfide)SM 4500-S2 F-2011 1 11/09/2018 1616 KFE 89207
1 (HEM(oil and)1664E 1 11/20/2018 1017 ARP 90095
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Cyanide-Total 57-12-5 SM 4500-CN E- ND 0.010 mg/L 1
MBAS(calculated as LAS) SM 5540C- 0.32 * 0.050 mg MBAS/L 1
Platinum-Cobalt Color SM 2120B- 25 * 5.0 color units 1
Sulfide 18496-25-8 SM 4500-S2 F- ND 1.0 mg/L 1
HEM(oil and grease) 1664B ND 4.9 mg/L 1
Footnote(s): *True Color:pH 7.84;MBAS:LAS MW 340.0
LOQ=Limit of Quantitation B=Detected in the method blank E=Quaintitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 11 of 45

Volatile Organic Compounds by GC/MS
Client:Pharr Yarns,Inc. Laboratory ID:TK08047-002
Description:Effluent Matrix:Aqueous
Date Sampled:11/08/2018 0900 Project Name:McAdenville 2C Permit
Date Received:11/08/2018 Project Number:
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 624.1 624.1 1 11/17/2018 0037 MNS 89846
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acrolein 107-02-8 624.1 ND 5.0 ug/L 1
Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L 1
Benzene 71-43-2 624.1 ND 1.0 ug/L 1
Bromodichloromethane 75-27-4 624.1 ND 1.0 ug/L 1
Bromoform I 75-25-2 624.1 ND 1.0 ug/L 1
Bromomethane(Methyl bromide) I 74-83-9 624.1 ND 2.0 ug/L 1
Carbon tetrachloride 561-23-5 624.1 ND 1.0 ug/L 1
Chlorobenzene 108L90-7 624.1 ND 1.0 ug/L 1
Chloroethane 75-00-3 624.1 ND 2.0 ug/L 1
2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L 1
Chloroform 67-66-3 624.1 ND 1.0 ug/L 1
Chloromethane(Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1
Dibromochloromethane 124-48-1 624.1 ND 1.0 ug/L 1
1,2-Dichlorobenzene 95-50-1 624.1 ND 1.0 ug/L 1
1,3-Dichlorobenzene 541-73-1 624.1 ND 1.0 ug/L 1
1,4-Dichlorobenzene 106-46-7 624.1 ND 1.0 ug/L 1
Dichlorodifluoromethane 75-71-8 624.1 ND 2.0 ug/L 1
1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1
1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1
1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L 1
cis-1,2-Dichloroethene 156-59-2 624.1 ND 1.0 ug/L 1
trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1
1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L 1
cis-1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L 1
trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L 1
Ethylbenzene 100-41-4 624.1 ND 1.0 ug/L 1
Methylene chloride 75-09-2 624.1 ND 1.0 ug/L 1
1,1,2,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L 1
Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L 1
Toluene I 108-88-3 624.1 ND 1.0 ug/L 1
1,2,4-Trichlorobenzene 120-82-1 624.1 ND 1.0 ug/L 1
1,1,1-Trichloroethane 711-55-6 624.1 ND 1.0 ug/L 1
1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L 1
Trichloroethene 79-01-6 624.1 ND 1.0 ug/L 1
Trichlorofluoromethane 75-69-4 624.1 ND 1.0 ug/L 1
Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L 1
Run 1 Acceptance
Surrogate Q %Recovery Limits
Bromofluorobenzene 110 70-130
1,2-Dichloroethane-d4 112 70-130
Toluene-d8 114 70-130
Footnote(s): *True Color:pH 7.84;MBAS:LAS MW 340.0
LOQ=Limit of Quantitation B=Detected in the method blank E=Quantitation of compound exceeded the calibration range
ND=Not detected at or above the LOQ N=Recovery is out of criteria P=The RPD between two GC columns exceeds 40%
H=Out of holding time W=Reported on wet weight basis
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 12 of 45
I

QC Summary
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 13 of 45

Inorganic non-metals - MB
Sample ID:TQ89159-001 Matrix: Aqueous
Batch:89159
Analytical Method:SM 5310C-2011
Parameter Result Q DII LOQ Units Analysis Date
TOC ND 1 1.0 mg/L 11/09/20181743
1
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] fjax(803)791-9111 www.shealylab.com
Page 14 of 45

Inorganic non-metals - LCS
Sample ID:TQ89159-002 Matrix: Aqueous
Batch:89159
Analytical Method:SM 5310C-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q DII %Rec Limit Analysis Date
TOC 20 20 1 99 90-110 11/09/20181727
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 15 of 45

Inorganic non-metals - MB
Sample ID:TQ89207-001 Matrix: Aqueous
Batch:89207
Analytical Method:SM 4500-S2 F-2011
Parameter Result Q Dil LOQ Units Analysis Date
Sulfide ND 1 1.0 mg/L 11/09/2018 0000
LOQ=Limit of Quantitation P=The RPD betweeh two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 16 of 45

Inorganic non-metals - LCS
Sample ID:TQ89207-002 Matrix: Aqueous
Batch:89207
Analytical Method:SM 4500-S2 F-2011
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
Sulfide 10 9.9 1 99 80-120 11/09/20181616
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 17 of 45

Inorganic non-metals - MB
Sample ID:TQ90145-001 Matrix: Aqueous
Batch:90145 Prep Method: 10-204-00-1-X
Analytical Method:SM 4500-CN E-2011 Prep Date: 11/20/2018 1328
Parameter Result Q Dil LOQ Units Analysis Date
Cyanide-Total ND 1 0.010 mg/L 11/20/2018 1744
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 18 of 45

Inorganic non-metals - LCS
Sample ID:TQ90145-002 Matrix: Aqueous
Batch:90145 Prep Method: 10-204-00-1-X
Analytical Method:SM 4500-CN -2011 Prep Date: 11/20/2018 1328
I Spike
Amount Res It %Rec
Parameter (mg/L) (mIL) Q Dil %Rec Limit Analysis Date
Cyanide-Total 0.10 0.11 1 106 90-110 11/20/2018 1745
LOQ=Limit of Quantitation P=The RPD betweeh two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 19 of 45

Inorganic non-metals - MB
Sample ID:TQ90748-001 Matrix: Aqueous
Batch:90748
Analytical Method:300.0
Parameter Result Q Dil LOQ Units Analysis Date
Bromide ND 1 0.20 mg/L 11/27/20181854
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 20 of 45

Inorganic non-metals - LCS
Sample ID:TQ90748-002 Matrix: Aqueous
Batch:90748
Analytical Method:300.0
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
Bromide 8.0 7.9 1 99 90-110 11/27/20181912
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 21 of 45

Inorganic non-metals - MB
Sample ID:TQ91079-001 Matrix: Aqueous
Batch:91079
Analytical Method:300.0
Parameter Result Q Dil LOQ Units Analysis Date
Sulfate ND 1 1.0 mg/L 11/30/20181436
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed bgfore rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. + QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] pax(803)791-9111 www.shealylab.com
Page 22 of 45

Inorganic non-metals - LCS
Sample ID:T091079-002 Matrix: Aqueous
Batch:91079
Analytical Method:300.0
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
Sulfate 20 20 1 101 90-110 11/30/20181414
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 23 of 45

Inorganic non-metals - MB
Sample ID: TQ91082-001 Matrix: Aqueous
Batch:91082
Analytical Method:300.0
Parameter Result Q Dil LOQ Units Analysis Date
Fluoride ND 1 0.10 mg/L 11/30/20181436
l
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result 1 LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected atlor above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 24 of 45
1

Inorganic non-metals - LCS
Sample ID:T091082-002 Matrix: Aqueous
Batch:91082
Analytical Method:300.0
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
Fluoride 4.0 4.1 1 102 90-110 11/30/20181414
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 25 of 45

Inorganic non-metals - MB
Sample ID:TQ90095-001 Matrix: Aqueous
Batch:90095
Analytical Method: 1664B
Parameter Result Q Dil LOQ Units Analysis Date
HEM(oil and grease) ND 1 4.0 mg/L 11/20/2018 1017
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 26 of 45

Inorganic non-metals - LCS
Sample ID:TQ90095-002 Matrix: Aqueous
Batch:90095
Analytical Method: 1664E
Spike
Amount Result %Rec
Parameter (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
HEM(oil and grease) 40 39 1 97 78-114 11/20/2018 1017
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Ii
Page 27 of 45

1
Volatile Organic Compounds by GC/MS - MB
Sample ID:TQ89846-001 Matrix: Aqueous
Batch:89846 Prep Method: 624.1
Analytical Method:624.1
Parameter Result Q Dil LOQ Units Analysis Date
Acrolein ND 1 5.0 ug/L 11/16/2018 2253
Acrylonitrile ND 1 5.0 ug/L 11/16/2018 2253
Benzene ND 1 1.0 ug/L 11/16/2018 2253
Bromodichloromethane ND 1 1.0 ug/L 11/16/2018 2253
Bromoform ND 1 1.0 ug/L 11/16/2018 2253
Bromomethane(Methyl bromide) ND 1 2.0 ug/L 11/16/2018 2253
Carbon tetrachloride ND 1 1.0 ug/L 11/16/2018 2253
Chlorobenzene ND 1 1.0 ug/L 11/16/2018 2253
Chloroethane ND 1 2.0 ug/L 11/16/2018 2253
2-Chloroethylvinylether ND 1 5.0 ug/L 11/16/2018 2253
Chloroform ND 1 1.0 ug/L 11/16/2018 2253
Chloromethane(Methyl chloride) ND 1 2.0 ug/L 11/16/2018 2253
Dibromochloromethane ND 1 1.0 ug/L 11/16/2018 2253
1,2-Dichlorobenzene ND 1 1.0 ug/L 11/16/2018 2253
1,3-Dichlorobenzene ND 1 1.0 ug/L 11/16/2018 2253
1,4-Dichlorobenzene ND I 1 1.0 ug/L 11/16/2018 2253
Dichlorodifluoromethane ND 1 2.0 ug/L 11/16/2018 2253
1,1-Dichloroethane ND 1 1.0 ug/L 11/16/2018 2253
1,2-Dichloroethane ND 1 1.0 ug/L 11/16/2018 2253
1,1-Dichloroethene ND 1 1.0 ug/L 11/16/2018 2253
cis-1,2-Dichloroethene ND 1 1.0 ug/L 11/16/2018 2253
trans-1,2-Dichloroethene ND 1 1.0 ug/L 11/16/2018 2253
1,2-Dichloropropane ND 1 1.0 ug/L 11/16/2018 2253
cis-1,3-Dichloropropene ND 1 1.0 ug/L 11/16/2018 2253
trans-1,3-Dichloropropene ND 1 1.0 ug/L 11/16/2018 2253
Ethylbenzene ND 1 1.0 ug/L 11/16/2018 2253
Methylene chloride ND 1 1.0 ug/L 11/16/2018 2253
1,1,2,2-Tetrachloroethane ND 1 1.0 ug/L 11/16/2018 2253
Tetrachloroethene ND 1 1.0 ug/L 11/16/2018 2253
Toluene ND 1 1.0 ug/L 11/16/2018 2253
1,2,4-Trichlorobenzene ND 1 1.0 ug/L 11/16/2018 2253
1,1,1-Trichloroethane ND 1 1.0 ug/L 11/16/2018 2253
1,1,2-Trichloroethane ND 1 1.0 ug/L 11/16/2018 2253
Trichloroethene ND 1 1.0 ug/L 11/16/2018 2253
Trichlorofluoromethane ND 1 1.0 ug/L 11/16/2018 2253
Vinyl chloride ND 1 1.0 ug/L 11/16/2018 2253
Acceptance
Surrogate I Q %Rec Limit
Bromofluorobenzene 108 70-130
1,2-Dichloroethane-d4 109 70-130
Toluene-d8 112 70-130
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 28 of 45

Volatile Organic Compounds by GC/MS - LCS
Sample ID:TQ89846-002 Matrix: Aqueous
Batch:89846 Prep Method: 624.1
Analytical Method:624.1
Spike
Amount Result %Rec
Parameter ! (ug/L) (ug/L) Q Dil %Rec Limit Analysis Date
Acrolein 200 2001 1 102 60-140 11/16/2018 2133
Acrylonitrile 40 34 1 1 85 60-140 11/16/2018 2133
Benzene 20 16 1 82 65-135 11/16/2018 2133
Bromodichloromethane 20 16 1 82 65-135 11/16/2018 2133
Bromoform 20 16 1 82 70-130 11/16/2018 2133
Bromomethane(Methyl bromide) 20 18 1 91 15-185 11/16/2018 2133
Carbon tetrachloride 20 16 1 82 70-130 11/16/2018 2133
Chlorobenzene 20 16 1 81 65-135 11/16/2018 2133
Chloroethane 20 18 1 92 40-160 11/16/2018 2133
2-Chloroethylvinylether 20 15 1 76 1-225 11/16/2018 2133
Chloroform 20 16 1 80 70-135 11/16/2018 2133
Chloromethane(Methyl chloride) 20 15 1 76 1-205 11/16/2018 2133
Dibromochloromethane 20 16 1 82 53-149 11/16/2018 2133
1,2-Dichlorobenzene 20 16 1 79 65-135 11/16/2018 2133
1,3-Dichlorobenzene 20 16 1 78 70-130 11/16/2018 2133 1
1,4-Dichlorobenzene 20 16 1 78 65-135 11/16/2018 2133
Dichlorodifluoromethane 20 15 1 77 60-140 11/16/2018 2133
1,1-Dichloroethane 20 16 1 82 70-130 11/16/2018 2133
1,2-Dichloroethane 20 17 1 85 70-130 11/16/2018 2133
1,1-Dichloroethene 20 15 1 77 50-150 11/16/2018 2133
cis-1,2-Dichloroethene 20 16 1 80 70-130 11/16/2018 2133
trans-1,2-Dichloroethene 20 16 1 79 70-130 11/16/2018 2133
1,2-Dichloropropane 20 17 1 84 35-165 11/16/2018 2133
cis-1,3-Dichloropropene 20 17 1 84 25-175 11/16/2018 2133
trans-1,3-Dichloropropene 20 17 , 1 84 50-150 11/16/2018 2133
Ethylbenzene 20 17 1 83 60-140 11/16/2018 2133
II
Methylene chloride 20 16 1 81 60-140 11/16/2018 2133
1,1,2,2-Tetrachloroethane 20 16 1 80 60-140 11/16/2018 2133
1 Tetrachloroethene 20 16 1 79 70-130 11/16/2018 2133
Toluene 20 16 1 81 70-130 11/16/2018 2133
1,2,4-Trichlorobenzene 20 17 1 87 60-140 11/16/2018 2133
1,1,1-Trichloroethane 20 16 1 80 70-130 11/16/2018 2133
1,1,2-Trichloroethane 20 17 1 84 70-130 11/16/2018 2133
Trichloroethene 20 17 1 83 65-135 11/16/2018 2133
Trichlorofluoromethane 20 18 1 91 50-150 11/16/2018 2133
Vinyl chloride 20 17 1 87 5-195 11/16/2018 2133
Acceptance
Surrogate Q %Rec Limit
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 106 70-130
Toluene-d8 108 70-130
LOQ=Limit of Quantitation 1 P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected aI or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 29 of 45

Volatile Organic Compounds by GC/MS - LCSD
Sample ID:TQ89846-003 Matrix: Aqueous
Batch:89846 Prep Method: 624.1
Analytical Method:624.1
Spike
Amount Result %Rec %RPD
Parameter (ug/L) (ug/L) Q Dil %Rec %RPD Limit Limit Analysis Date
Acrolein 200 200 1 102 0.47 60-140 20 11/16/2018 2207
Acrylonitrile 40 34 1 86 0.87 60-140 20 11/16/2018 2207
Benzene 20 17 1 84 2.3 65-135 20 11/16/2018 2207
Bromodichloromethane 20 17 1 83 1.8 65-135 20 11/16/2018 2207
Bromoform 20 17 1 83 1.2 70-130 20 11/16/2018 2207
Bromomethane(Methyl bromide) 20 19 1 94 3.3 15-185 20 11/16/2018 2207
Carbon tetrachloride 20 17 1 86 4.4 70-130 20 11/16/2018 2207
Chlorobenzene 20 17 1 83 1.8 65-135 20 11/16/2018 2207
Chloroethane 20 20 1 98 5.5 40-160 20 11/16/2018 2207
2-Chloroethylvinylether 20 15 1 77 1.0 1-225 20 11/16/2018 2207
Chloroform 20 17 i 1 83 3.8 70-135 20 11/16/2018 2207
Chloromethane(Methyl chloride) 20 16 i 1 79 3.7 1-205 20 11/16/2018 2207
Dibromochloromethane 20 17 1 84 1.6 53-149 20 11/16/2018 2207
1,2-Dichlorobenzene 20 16 1 80 1.6 65-135 20 11/16/2018 2207
1,3-Dichlorobenzene 20 16 1 80 2.5 70-130 20 11/16/2018 2207
1,4-Dichlorobenzene 20 16 1 79 1.1 65-135 20 11/16/2018 2207
Dichlorodifluoromethane 20 16 1 79 3.5 60-140 20 11/16/2018 2207
1,1-Dichloroethane 20 17 1 85 3.3 70-130 20 11/16/2018 2207
1,2-Dichloroethane 20 17 1 87 1.6 70-130 20 11/16/2018 2207
1,1-Dichloroethene 20 16 1 81 5.8 50-150 20 11/16/2018 2207
cis-1,2-Dichloroethene 20 17 1 83 3.8 70-130 20 11/16/2018 2207
trans-1,2-Dichloroethene 20 16 1 82 3.5 70-130 20 11/16/2018 2207 '
1,2-Dichloropropane 20 17 1 87 4.2 35-165 20 11/16/2018 2207
cis-1,3-Dichloropropene 20 17 1 86 2.5 25-175 20 11/16/2018 2207
trans-1,3-Dichloropropene 20 17 1 85 0.87 50-150 20 11/16/2018 2207
Ethylbenzene 20 17 1 86 2.5 60-140 20 11/16/2018 2207
Methylene chloride 20 17 1 83 2.0 60-140 20 11/16/2018 2207
1,1,2,2-Tetrachloroethane 20 16 1 81 1.0 60-140 20 11/16/2018 2207
Tetrachloroethene 20 17 1 83 4.5 70-130 20 11/16/2018 2207
Toluene 20 17 1 85 4.4 70-130 20 11/16/2018 2207
1,2,4-Trichlorobenzene 20 17 1 85 2.5 60-140 20 11/16/2018 2207
1,1,1-Trichloroethane 20 17 1 85 5.4 70-130 20 11/16/2018 2207
1,1,2-Trichloroethane 20 17 1 83 0.46 70-130 20 11/16/2018 2207
Trichloroethene 20 17 1 84 1.6 65-135 20 11/16/2018 2207
Trichlorofluoromethane 20 19 1 1 96 5.7 50-150 20 11/16/2018 2207
Vinyl chloride 20 18 j 1 90 4.1 5-195 20 11/16/2018 2207
Acceptance
Surrogate Q %Rec Limit
Bromofluorobenzene 103 70-130
1,2-Dichloroethane-d4 107 70-130
Toluene-d8 110 70-130
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 30 of 45

Semivolatile Organic Compounds by GC/MS - MB
Sample ID:TQ89450-001 Matrix: Aqueous
Batch:89450 Prep Method: 625.1
Analytical Method:625.1 Prep Date: 11/13/2018 1856
Parameter Result Q Dil LOQ Units Analysis Date
Acenaphthene ND 1 1.6 ug/L 11/25/2018 1200
Acenaphthylene ND 1 1.6 ug/L 11/25/2018 1200
Anthracene ND 1 1.6 ug/L 11/25/2018 1200
Benzidine ND 1 8.0 ug/L 11/25/2018 1200
Benzo(a)anthracene ND 1 1.6 ug/L 11/25/2018 1200
Benzo(a)pyrene ND 1 1.6 ug/L 11/25/2018 1200
Benzo(b)fluoranthene ND 1 1.6 ug/L 11/25/2018 1200
Benzo(g,h,i)perylene ND 1 1.6 ug/L 11/25/2018 1200
Benzo(k)fluoranthene ND 1 1.6 ug/L 11/25/2018 1200
4-Bromophenyl phenyl ether ND 1 1.6 ug/L 11/25/2018 1200
Butyl benzyl phthalate ND 1 1.6 ug/L 11/25/2018 1200
bis(2-Chloro-1-methylethyl)ether ND 1 1.6 ug/L 11/25/2018 1200
4-Chloro-3-methyl phenol ND 1 1.6 ug/L 11/25/2018 1200
bis(2-Chloroethoxy)methane ND 1 1.6 ug/L 11/25/2018 1200
bis(2-Chloroethyl)ether ND 1 1.6 ug/L 11/25/2018 1200
2-Chloronaphthalene ND 1 1.6 ug/L 11/25/2018 1200
2-Chlorophenol ND 1 1.6 ug/L 11/25/2018 1200
4-Chlorophenyl phenyl ether ND 1 1.6 ug/L 11/25/2018 1200
Chrysene ND 1 1.6 ug/L 11/25/2018 1200
Dibenzo(a,h)anthracene ND 1 1.6 ug/L 11/25/2018 1200
1,2-Dichlorobenzene ND I 1 1.6 ug/L 11/25/2018 1200
1,3-Dichlorobenzene ND ! 1 1.6 ug/L 11/25/2018 1200
1,4-Dichlorobenzene ND 1 1.6 ug/L 11/25/2018 1200
3,3'-Dichlorobenzidine ND 1 8.0 ug/L 11/25/2018 1200
2,4-Dichlorophenol ND 1 1.6 ug/L 11/25/2018 1200
Diethylphthalate ND 1 1.6 ug/L 11/25/2018 1200
Dimethyl phthalate ND 1 1.6 ug/L 11/25/2018 1200
2,4-Dimethylphenol ND 1 1.6 ug/L 11/25/2018 1200
Di-n-butyl phthalate ND 1 1.6 ug/L 11/25/2018 1200
4,6-Dinitro-2-methylphenol ND 1 8.0 ug/L 11/25/2018 1200
2,4-Dinitrophenol ND 1 8.0 ug/L 11/25/2018 1200
2,4-Dinitrotoluene ND 1 3.2 ug/L 11/25/2018 1200
2,6-Dinitrotoluene ND 1 3.2 ug/L 11/25/2018 1200
Di-n-octylphthalate ND 1 1.6 ug/L 11/25/2018 1200
1,2-Diphenylhydrazine(as azobenzene) ND 1 1.6 ug/L 11/25/2018 1200
bis(2-Ethylhexyl)phthalate ND 1 8.0 ug/L 11/25/2018 1200
Fluoranthene ND 1 1.6 ug/L 11/25/2018 1200
Fluorene ND 1 1.6 ug/L 11/25/2018 1200
Hexachlorobenzene ND 1 1.6 ug/L 11/25/2018 1200
Hexachlorobutadiene ND 1 1.6 ug/L 11/25/2018 1200
Hexachlorocyclopentadiene ND 1 8.0 ug/L 11/25/2018 1200
Hexachloroethane ND 1 1.6 ug/L 11/25/2018 1200
Indeno(1,2,3-c,d)pyrene ND 1 1.6 ug/L 11/25/2018 1200
Isophorone ND 1 1.6 ug/L 11/25/2018 1200
I
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 31 of 45

Semivolatile Organic Compounds by GC/MS - MB
Sample ID:TQ89450-001 Matrix: Aqueous
Batch:89450 Prep Method: 625.1
Analytical Method:625.1 Prep Date: 11/13/2018 1856
Parameter Result Q Dil LOQ Units Analysis Date
Naphthalene ND 1 1.6 ug/L 11/25/2018 1200
Nitrobenzene ND 1 1.6 ug/L 11/25/2018 1200
2-Nitrophenol ND 1 3.2 ug/L 11/25/2018 1200
4-Nitrophenol ND 1 8.0 ug/L 11/25/2018 1200
N-Nitrosodimethylamine ND 1 1.6 ug/L 11/25/2018 1200
N-Nitrosodi-n-propylamine ND I 1 1.6 ug/L 11/25/2018 1200
N-Nitrosodiphenylamine(Diphenylamine)ND I 1 1.6 ug/L 11/25/2018 1200
Pentachlorophenol ND 1 8.0 ug/L 11/25/2018 1200
Phenanthrene ND 1 1.6 ug/L 11/25/2018 1200
Phenol ND 1 1.6 ug/L 11/25/2018 1200
Pyrene ND 1 1.6 ug/L 11/25/2018 1200
1,2,4-Trichlorobenzene ND 1 1.6 ug/L 11/25/2018 1200
2,4,6-Trichlorophenol ND 1 1.6 ug/L 11/25/2018 1200
Surrogate Q %Rec Acceptance Limit
2-Fluorobiphenyl 52 37-129
2-Fluorophenol 35 24-127
Nitrobenzene-d5 56 38-127
Phenol-d5 43 28-128
Terphenyl-d 14 84 10-148
2,4,6-Tribromophenol 43 41-144
I
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia, C 29172 [phone] Fax[phone] www.shealylab.com
l'age 32 of 45

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: TQ89450-002 Matrix: Aqueous
Batch:89450 Prep Method: 625.1
Analytical Method:625.1 Prep Date: 11/13/2018 1856
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q DII %Rec Limit Analysis Date
Acenaphthene 20 14 I 1 70 47-145 11/25/2018 1224
Acenaphthylene 20 13 I 1 66 33-145 11/25/2018 1224 i
Anthracene 20 16 1 79 27-133 11/25/2018 1224
Benzidine 100 4.1 1 4.1 1-150 11/25/2018 1224
Benzo(a)anthracene 20 16 1 80 33-143 11/25/2018 1224
Benzo(a)pyrene 20 15 1 77 17-163 11/25/2018 1224
Benzo(b)fluoranthene 20 16 1 79 24-159 11/25/2018 1224
Benzo(g,h,i)perylene 20 18 1 90 1-219 11/25/2018 1224
Benzo(k)fluoranthene 20 17 1 83 11-162 11/25/2018 1224
4-Bromophenyl phenyl ether 20 14 1 70 53-127 11/25/2018 1224
Butyl benzyl phthalate 20 18 1 91 1-152 11/25/2018 1224
bis(2-Chloro-1-methylethyl)ether 20 16 1 78 36-166 11/25/2018 1224
4-Chloro-3-methyl phenol 20 14 1 71 22-147 11/25/2018 1224
bis(2-Chloroethoxy)methane 20 13 1 67 33-184 11/25/2018 1224
bis(2-Chloroethyl)ether 20 16 1 78 12-158 11/25/2018 1224
2-Chloronaphthalene 20 14 1 68 60-120 11/25/2018 1224
2-Chlorophenol 20 12 1 61 23-134 11/25/2018 1224
4-Chlorophenyl phenyl ether 20 14 1 71 25-158 11/25/2018 1224
Chrysene 20 17 1 84 17-168 11/25/2018 1224
Dibenzo(a,h)anthracene 20 18 1 91 1-227 11/25/2018 1224
1,2-Dichlorobenzene 20 13 1 64 32-129 11/25/2018 1224
1,3-Dichlorobenzene 20 13 1 63 1-172 11/25/2018 1224
1,4-Dichlorobenzene 20 13 1 64 20-124 11/25/2018 1224
3,3'-Dichlorobenzidine 20 7.0 1 35 1-262 11/25/2018 1224
2,4-Dichlorophenol 20 13 1 64 39-135 11/25/2018 1224
Diethylphthalate 20 17 1 85 1-120 11/25/2018 1224
Dimethyl phthalate 20 16 I 1 81 1-120 11/25/2018 1224 i
2,4-Dimethylphenol 20 16 1 78 32-120 11/25/2018 1224
Di-n-butyl phthalate 20 17 1 86 1-120 11/25/2018 1224
4,6-Dinitro-2-methylphenol 20 13 1 66 1-181 11/25/2018 1224
2,4-Dinitrophenol 40 18 1 46 1-191 11/25/2018 1224
2,4-Dinitrotoluene 20 18 1 89 39-139 11/25/2018 1224
2,6-Dinitrotoluene 20 16 1 81 50-158 11/25/2018 1224
Di-n-octylphthalate 20 14 1 71 4-146 11/25/2018 1224
1,2-Diphenylhydrazine(as azobenzene) 20 16 1 82 1-150 11/25/2018 1224
bis(2-Ethylhexyl)phthalate 20 19 1 94 8-158 11/25/2018 1224
Fluoranthene 20 16 1 80 26-137 11/25/2018 1224
Fluorene 20 15 1 74 59-121 11/25/2018 1224
Hexachlorobenzene 20 14 1 70 1-152 11/25/2018 1224
Hexachlorobutadiene 20 11 1 54 24-120 11/25/2018 1224
Hexachlorocyclopentadiene 100 24 1 24 1-150 11/25/2018 1224 '
Hexachloroethane 20 12 1 61 40-120 11/25/2018 1224
I ndeno(1,2,3-c,d)pyrene 20 18 1 91 1-171 11/25/2018 1224
Isophorone 20 15 1 73 21-196 11/25/2018 1224
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected ail or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 33 of 45

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID:TQ89450-002 Matrix: Aqueous
Batch:89450 Prep Method: 625.1
Analytical Method:625.1 Prep Date: 11/13/2018 1856
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil %Rec Limit Analysis Date
Naphthalene 20 14 1 69 21-133 11/25/2018 1224
Nitrobenzene 20 14 1 72 35-180 11/25/2018 1224
2-Nitrophenol 20 14 1 72 29-182 11/25/2018 1224
4-Nitrophenol 40 29 1 72 1-132 11/25/2018 1224
N-Nitrosodimethylamine 20 14 1 71 1-150 11/25/2018 1224
N-Nitrosodi-n-propylamine 20 17 1 83 1-230 11/25/2018 1224
N-Nitrosodiphenylamine(Diphenylamine) 20 14 1 71 1-150 11/25/2018 1224
Pentachlorophenol 40 21 1 52 14-176 11/25/2018 1224
Phenanthrene 20 15 1 77 54-120 11/25/2018 1224
Phenol 20 11 1 56 5-120 11/25/2018 1224
Pyrene 20 18 1 88 52-120 11/25/2018 1224
1,2,4-Trichlorobenzene 20 131 1 63 44-142 11/25/2018 1224
2,4,6-Trichlorophenol 20 13 1 63 37-144 11/25/2018 1224
Surrogate Q % Limit Rec AcceptanceLimit
2-Fluorobiphenyl 67 37-129
2-Fluorophenol 43 24-127
Nitrobenzene-d5 71 38-127
Phenol-d5 58 28-128
Terphenyl-d 14 85 10-148
2,4,6-Tribromophenol 69 41-144
I
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 34 of 45

Organochlorine Pesticides and PCBs - MB
Sample ID:TQ89666-001 Matrix: Aqueous
Batch:89666 Prep Method: 608.3 Cleanup: 3665A
Analytical Method:608.3 1 Prep Date: 11/15/2018 1714
Parameter Result Q DiI LOQ Units Analysis Date
Aldrin ND 1 0.040 ug/L 11/20/2018 1737
Aroclor 1016 ND 1 0.40 ug/L 11/19/2018 0000
Aroclor 1221 ND 1 0.40 ug/L 11/19/2018 0000
Aroclor 1232 ND 1 0.40 ug/L 11/19/2018 0000
Aroclor 1242 ND 1 0.40 ug/L 11/19/2018 0000
Aroclor 1248 ND 1 0.40 ug/L 11/19/2018 0000
Aroclor 1254 ND 1 0.40 ug/L 11/19/2018 0000
Aroclor 1260 ND 1 0.40 ug/L 11/19/2018 0000
gamma-BHC(Lindane) ND 1 0.040 ug/L 11/20/2018 1737
alpha-BHC ND 1 0.040 ug/L 11/20/2018 1737
beta-BHC ND 1 0.040 ug/L 11/20/2018 1737
delta-BHC ND 1 0.040 ug/L 11/20/2018 1737
Chlordane ND 1 0.40 ug/L 11/20/2018 1737
4,4'-DDD ND 1 0.040 ug/L 11/20/2018 1737
4,4'-DDE ND 1 0.040 ug/L 11/20/2018 1737
4,4'-DDT ND 1 0.040 ug/L 11/20/2018 1737
Dieldrin ND 1 0.040 ug/L 11/20/2018 1737
Endosulfan I ND 1 0.040 ug/L 11/20/2018 1737
Endosulfan II ND 1 0.040 ug/L 11/20/2018 1737
Endosulfan sulfate ND 1 0.040 ug/L 11/20/2018 1737
Endrin ND 1 1 0.040 ug/L 11/20/2018 1737
Endrin aldehyde ND I 1 0.040 ug/L 11/20/2018 1737
Heptachlor ND 1 0.040 ug/L 11/20/2018 1737
Heptachlor epoxide ND 1 0.040 ug/L 11/20/2018 1737
Toxaphene ND 1 0.40 ug/L 11/20/2018 1737
Surrogate Q %Rec Ac L mt tote
Decachlorobiphenyl 57 20-131
Tetrachloro-m-xylene 68 30-132
1
I
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 35 of 45

Organochlorine Pesticides and PCBs - LCS
Sample ID:TQ89666-002 Matrix: Aqueous
Batch:89666 Prep Method: 608.3 Cleanup: 3665A
Analytical Method:608.3 Prep Date: 11/15/2018 1714
Spike
Amount Result %Rec
Parameter (ug/L) (ug/L) Q Dil %Rec Limit Analysis Date
Aldrin 0.80 0.68 1 85 54-130 11/20/2018 1753
gamma-BHC(Lindane) 0.80 0.73 1 92 43-130 11/20/2018 1753
alpha-BHC 0.80 0.70 1 87 49-130 11/20/2018 1753
beta-BHC 0.80 0.69 1 87 39-130 11/20/2018 1753
delta-BHC 0.80 0.70 1 87 51-130 11/20/2018 1753
4,4'-DDD 0.80 0.71 1 89 48-130 11/20/2018 1753
4,4'-DDE 0.80 0.7 1 92 54-130 11/20/2018 1753
4,4'-DDT 0.80 0.76 1 95 58-130 11/20/2018 1753
Dieldrin 0.80 0.80 1 100 36-146 11/20/2018 1753
Endosulfan I 0.80 0.71 1 89 57-141 11/20/2018 1753
Endosulfan II 0.80 0.69 1 86 22-171 11/20/2018 1753
Endosulfan sulfate 0.80 0.80 1 100 38-132 11/20/2018 1753
Endrin 0.80 0.73 1 91 51-130 11/20/2018 1753
Endrin aldehyde 0.80 0.61 1 76 60-140 11/20/2018 1753
Heptachlor 0.80 0.65 1 81 43-130 11/20/2018 1753
Heptachlor epoxide 0.80 0.76 1 95 57-132 11/20/2018 1753
Acceptance
Surrogate Q %Rec Limit
Decachlorobiphenyl 43 20-131
Tetrachloro-m-xylene 70 30-132
1
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia, 29172 [phone] Fax[phone] www.shealylab.com
''age 36 of 45

1
ICP-MS - MB
Sample ID:TQ89657-001 Matrix: Aqueous
Batch:89657 Prep Method: 200.2
Analytical Method:200.8 Prep Date: 11/15/2018 1718
Parameter Result Q Dil LOQ Units Analysis Date
Aluminum ND 1 40 ug/L 12/02/2018 0752
Antimony ND 1 2.0 ug/L 12/02/2018 0752
Arsenic ND 1 2.0 ug/L 12/02/2018 0752
Barium ND 1 5.0 ug/L 12/02/2018 0752
Beryllium ND 1 0.40 ug/L 12/02/2018 0752
Boron ND 1 50 ug/L 12/04/2018 2358
Cadmium ND 1 0.50 ug/L 12/02/2018 0752
Chromium ND 1 5.0 ug/L 12/02/2018 0752
Cobalt ND 1 5.0 ug/L 12/02/2018 0752
Copper ND 1 5.0 ug/L 12/02/2018 0752
Iron ND 1 50 ug/L 12/02/2018 0752
Lead ND 1 1.0 ug/L 12/02/2018 0752
Magnesium ND 1 400 ug/L 12/02/2018 0752
Manganese ND 1 5.0 ug/L 12/02/2018 0752
Molybdenum ND 1 10 ug/L 12/02/2018 0752
Nickel ND 1 5.0 ug/L 12/02/2018 0752
Selenium ND I 1 5.0 ug/L 12/02/2018 0752
Silver ND 1 1.0 ug/L 12/02/2018 0752
Thallium ND 1 0.50 ug/L 12/02/2018 0752
Tin ND 1 20 ug/L 12/02/2018 0752
Titanium ND 1 5.0 ug/L 12/02/2018 0752
Zinc ND 1 10 ug/L 12/02/2018 0752
1
i
I
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 37 of45

ICP-MS - LCS
Sample ID:TQ89657-002 Matrix: Aqueous
Batch:89657 Prep Method: 200.2
Analytical Method:200.8 Prep Date: 11/15/2018 1718
Spike
Amount Result %Rec
Parameter j (ug/L) (ug/L) Q DII %Rec Limit Analysis Date
Aluminum - 100 98 1 98 85-115 12/02/2018 0758
Antimony 100 93 1 93 85-115 12/02/2018 0758
Arsenic 100 96 I 1 96 85-115 12/02/2018 0758
Barium 100 100 1 100 85-115 12/02/2018 0758
Beryllium 100 92 1 92 85-115 12/02/2018 0758
Boron 100 98 1 98 85-115 12/05/2018 0004
Cadmium 100 98 1 98 85-115 12/02/2018 0758
Chromium 100 100 1 100 85-115 12/02/2018 0758
Cobalt 100 96 1 96 85-115 12/02/2018 0758
Copper 100 100 1 101 85-115 12/02/2018 0758
Iron 1000 990 1 99 85-115 12/02/2018 0758
Lead 100 89 1 89 85-115 12/02/2018 0758
Magnesium 1000 910 1 91 85-115 12/02/2018 0758
Manganese 100 100 1 100 85-115 12/02/2018 0758
Molybdenum 100 95 1 95 85-115 12/02/2018 0758
Nickel 100 98 1 98 85-115 12/02/2018 0758
Selenium 100 100 1 101 85-115 12/02/2018 0758
Silver 100 98 1 98 85-115 12/02/2018 0758
Thallium 100 92 1 92 85-115 12/02/2018 0758
Tin 100 99 1 99 85-115 12/02/2018 0758
Titanium 100 100 1 103 85-115 12/02/2018 0758
Zinc 100 110 1 106 85-115 12/02/2018 0758
1
I
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected a or above the LOQ
Note: Calculations are performed before rounding to avoid ro�nd-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 38 of 45
1
l

CVAA - MB
Sample ID: TQ89588-001 Matrix: Aqueous
Batch:89588 Prep Method: 7470A
Analytical Method:245.1 Prep Date: 11/15/2018 1512
Parameter Result Q Dil LOQ Units Analysis Date
Mercury ND 1 0.00020 mg/L 11/17/20181324
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 39 of 45

CVAA - LCS
Sample ID:TQ89588-002 Matrix: Aqueous
Batch:89588 Prep Method: 7470A
Analytical Method:245.1 Prep Date: 11/15/2018 1512
Spike
Amount Result %Rec
Parameter (mg/L) (mglL) Q Dil %Rec Limit Analysis Date
Mercury 0.0020 0.0020 1 98 85-115 11/17/20181326
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 40 of 45

CVAA - MS
Sample ID: TK08047-001 MS Matrix: Aqueous
Batch:89588 Prep Method: 7470A
Analytical Method:245.1 Prep Date: 11/15/2018 1512
Sample Spike
Amount Amount Result %Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil %Rec Limit Analysis Date
Mercury ND 0.0020 0.0025 1 123 70-130 11/17/20181344
1
I
I
1
I
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,$C 29172 [phone] Fax[phone] www.shealylab.com
IJ rage 41 of 45
I

CVAA - MSD
Sample ID:TK08047-001MD Matrix: Aqueous
Batch:89588 Prep Method: 7470A
Analytical Method:245.1 Prep Date: 11/15/2018 1512
Sample Spike
Amount Amount Result %Rec %RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil %Rec %RPD Limit Limit Analysis Date
Mercury ND 0.0020 0.0021 1 105 16 70-130 20 11/17/20181351
LOQ=Limit of Quantitation P=The RPD between two GC columns exceeds 40% N=Recovery is out of criteria
DL=Detection Limit J=Estimated result<LOQ and>DL +=RPD is out of criteria
LOD=Limit of Detection ND=Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round-off errors in calculated results
Shealy Environmental Services,Inc. QC Data for Lot Number:TK08047
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 42 of 45

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 43 of 45

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I Note:All samples are retained for six weeks from receipt unless other lAD U8t OMLY �� D"' F rim, Ile J
lRecalemt• T�np,Baia----- er ampemenu are made Received nn Iw(Chock} N OkePock r
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error:Om Date 24-2l 20-7

SHEALY ENVIRONMENTAL SERVICES, INC.
.hr.'y F.-krimnsnerr:nl Senrier.,Inc PHU 1 ed 1
DDvun ntNrnr4er:MEID18C-Ia Efk[ave Date.&:i2DI
Sample Rleceipt Checklist ( RC)
chew: • ,r } VP/ia,..�. C:ooler Inspected by:date: $ 1 Lot : JtiOgb
Means of recei ti I_i-'iro,i j Client ❑ 11PS , l F if'N CI Other.
L i Yes No i crc custody seals present on the cooler?
❑i'cs l' No ❑NA 2. If custody aesis tiv:t'c present,wc;C they intact and unbroken?
'pH Strip ID: l -'+(a :Ili Chlorine Strip ID:j '1 '- Tested by: (;et„
Original terpperoture upon receipt f Derived(Corrected)lempornlure upon receipt: %Solid Snap-Cup ID:
. ,G . °C °C +__cC /�
Method: ®Telhperatuf-Blli ❑Against Bottles III Gun TD: Y ITR Gust Orme-non Factor 0 "C
Method of coolant: 1] Wet Ice ❑ Ice Packs ❑ Dry lee 0 None
. Q N 3. if temperature of any cooler exceeded 6.0'C,was Project Manager Notified?
1-1 Yes ❑ No
r t was Naufted by:phone/email i face-la-farm(circle one).
❑ Yes ❑No NA+4. Is the colrmercial courier's packing slip attached to this form?
pes 0 No 5_ Were proper custod rc y prn crius(relinquished/received)followed'?
eti ❑No 6. Were sample IDs listed at the COC? '
L ❑No! ?. Were sample IDs listed an all sample containers?
0 Nu S. Was collection dare&time listed on the COC?
t`I cs CINo 9_ Was collection date&tonne listed on all sample contraltos"
0 No 10. 1.'Iid all container label information(ID,date,time)agree with the CCC f
r Ycs 0 No 11.Were tests to be performed listed on the COC?
Yes ❑No 12,Did all samples arrive in the proper containers for each test and`nr in good condition
(unbroken,lads on,etc.)?
No 13.Was adequate sample volume available?
l�Yes ❑Nyl 14.Were all samples received within:14 the holding tune or 48 hours,whichever comes first!
�❑Yes ne-No 15 Were any samples containers missing/excess(circle one)samples Not listed on COC?
❑,NA 16 For VOA and RSK-175 samples, were bubbles prrccre 'pea-size"(W'or Gnun in diameter)in
❑ Yes NO any of the VOA vials?
1 0"S'cs L1 No. 'N.4 17.Were all DRO+metals/nutrient samples received at a pH of<2?
g s d No ❑NA 18.Were all cyanide samples received at a pll-> 12 and sulfide samples received at a pH>9?
19.Were all applicable NI .TKN/cyanidelpheim11625(<O.5mi fI.l samples free ofresidual
1-el ❑No ,]_ �A chlorine? _
❑Yrc E No -rJ,.NA 20.Were client nernarkstnequesta(he.requested dilutions,MS/MSI)designations,etc_..)
correctly transcribed from the COC inut the comment section in LiMS?
C 'sus "I. y c;, 21.Was the quote number listed on the container label?If yes.Quote x _
S3mpie Preservation (Must he completed for any sample(s)incorrectly preser ed or with headspacc.) LL
sample(x) were received incorrectly preserved and were adjusted accordingly
in sample receiving with mL of circle one:H2SO4.HNO3,HCI,NaOH using SR l
'lime of preservation . if more than one preservative is needed,please note in the comments below,
Sample(s) _ were received with bubbles>6 rem in diameter
Samples(s) were received with TRC 0.5 m 'L(!f*19 is no)and were
adjusted uceordingly in sample receiving with 3cxlitur:hiosulfatc(Na2S=O3)with Shcaly ID:
SR barcode labels applied by: 17jU Ths1e: //
Comments:
•
•
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax[phone] www.shealylab.com
Page 45 of 45
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