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HomeMy WebLinkAboutDEQ-CFW_00076663Ms. Teresa Rodriguez NCDENR Division of Water Quality NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699 - 1617 SUBJECT: NPDES Permit Renewal Application Addendum Revised Form 2C and Supplemental Information NPDES Permit No. NC0003573 Dear Ms. Rodriguez: DuPont Fluoroproducts 22828 NC Highway 87 W Fayetteville, NC 28306-7332 August 2, 2006 D AUG 4 2006 DE - WATER QUALITY POINT SOURCE BRANCH Enclosed are the revised Form 2C submittals for the subject renewal application. These forms include the omitted analytical data. Outfall 002 sampling showed unexpected positive results for cyanide, chloroform, dichlorobromomethane, and bis(2-ethylhexyl)phthalate; none of which are used or produced at this site. Also, you will find a revised Supplemental Information document that describes the proposed changes with the construction of a new manufacturing unit that will produce Polyvinyl Fluoride (PVF) polymer resins. It has been determined that the preferred means of controling solids from the PVF unit is a new clarifier which will be dedicated to the PVF wastewater. The discharge from this clarifier will be to the existing Outfall 001. Therefore, please ignore the original submittal's description of the PVF treated wastewater being discharged through and monitored at Outfall 006. A revised water balance sheet is enclosed which reflects the above treatment change. Should you have any questions, please feel free to call meat (91 0) 67R-1 155 Michael E. Johnson Environmental Manager Enclosures E.I. du Pont de Nemours and Company DEQ-CFW 00076663 DuPont Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information (Revised) Revised Supplemental Information — Permit Renewal Application — August 1, 2006 Proposed Changes in Operations PVF Manufacturing Facility: The DuPont Company — Fayetteville Works has been selected as the location for the DuPontTM Polyvinyl Fluoride (PVF) manufacturing process. The manufacturing facility is in the process of being designed, and will produce PVF polymer resins. PVF resin to be manufactured at the Fayetteville plant is used in DuPontTM Tedlar® fluoropolymer film business. Tedlar® film is manufactured at other DuPont site location (not the Fayetteville plant). Tedlar® is used in the photovoltaic industry in photovoltaic cells and the aircraft industry for interior cabin surfaces, as well as many other uses. This new facility construction will be completed in August 2007 and begin start up in October 2007. The manufacturing facility will be located near the existing Teflon® FEP resin manufacturing area. This process will produce polyvinyl fluoride (PVF) resin (CAS No. 24981-14-4). As with most fluorochemical processes, the wastewater from the PVF manufacturing process is expected to have very little or no biological oxygen demand (BOD5) value. Treatability tests have been performed on samples from another DuPont site which currently manufactures PVF. These studies have indicated use of non -biological treatment will meet effluent limitation of OCPSF NSPS guidelines of Subpart D—Thermoplastic Resins (40 CFR 414.40). DuPont will control solids in the wastewater from this new facility via a new dedicated clarifier whose discharge will go directly to Outfall 001. A suggested change to the language of the current permit's narrative in the "Supplement To Permit Cover Sheet" that would accommodate the new PVF Manufacturing Facility follows: 1. Continue to operate existing wastewater treatment facilities consisting of: • equalization; (etc) 2. To operate new wastewater treatment facilities consisting of: • clarifier for PVF process wastewater; 3. Discharge treated process wastewater from Butacite, Nafion, PVF, and Teflon® PMDF, process stormwater, sanitary wastewater, and co -neutralized regenerate form said treated facilities through internal outfall 001; The process wastewater is expected to contain unreacted vinyl fluoride (CAS No. 00075-02-5). The anticipated quantity of vinyl fluoride from the PVF Manufacturing Facility is 0.312 pounds per day. This quantity would equate to approximately 0.04 mg/L vinyl fluoride at Outfall 001 and 0.0035 mg/L vinyl fluoride at Outfall 002. Finally, non -contact cooling, condensate, and stormwater from the PVF Manufacturing Facility will be discharged directly to Outfall 002 via the site's Woodlined Ditch. DEQ-CFW 00076664 MONITORING REPORT(MR) VIOLATIONS for: Report Date: 05/24/06 Page: 1 of 1 PERMIT: NC0003573 FACILITY: E I DuPont de Nemours and Company - Dupont COUNTY: Bladen REGION: Fayetteville Fayetteville Works Limit Violation MONITORING OUTFALL VIOLATION UNIT OF CALCULATED REPORT / PPI LOCATION PARAMETER DATE FREQUENCY MEASURE LIMIT VALUE VIOLATION TYPE VIOLATION ACTION 03 - 2005 001 Effluent BOD, 5-Day (20 Deg. C) 03/30/05 3 X week Ibs/day 508.2 2,981 Daily Maximum Exceeded Proceed to NOV 03 - 2005 001 Effluent BOD, 5-Day (20 Deg. C) 03/31/05 3 X week Ibs/day 191.3 265.87 Monthly Average Exceeded Proceed to NOV 08 - 2004 001 Effluent Solids, Total Suspended 08/16/04 3 X week Ibs/day 1,030 1,125 Daily Maximum Exceeded No Action, BPJ 0 M p C� n I 0 0 0 14 rn rn rn DuPont Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information (Revised) Revised Supplemental Information — Permit Renewal Application — August 1, 2006 Proposed Changes in Operations PVF Manufacturing Facility: The DuPont Company — Fayetteville Works has been selected as the location for the DuPontTM Polyvinyl Fluoride (PVF) manufacturing process. The manufacturing facility is in the process of being designed, and will produce PVF polymer resins. PVF resin to be manufactured at the Fayetteville plant is used in DuPontTM Tedlar® fluoropolymer film business. Tedlar® film is manufactured at other DuPont site location (not the Fayetteville plant). Tedlar® is used in the photovoltaic industry in photovoltaic cells and the aircraft industry for interior cabin surfaces, as well as many other uses. This new facility construction will be completed in August 2007 and begin start up in October 2007. The manufacturing facility will be located near the existing Teflon® FEP resin manufacturing area. This process will produce polyvinyl fluoride (PVF) resin (CAS No. 24981-14-4). As with most fluorochemical processes, the wastewater from the PVF manufacturing process is expected to have very little or no biological oxygen demand (BOD5) value. Treatability tests have been performed on samples from another DuPont site which currently manufactures PVF. These studies have indicated use of non -biological treatment will meet effluent limitation of OCPSF NSPS guidelines of Subpart D—Thermoplastic Resins (40 CFR 414.40). DuPont will control solids in the wastewater from this new facility via a new dedicated clarifier whose discharge will go directly to Outfall 001. A suggested change to the language of the current permit's narrative in the "Supplement To Permit Cover Sheet" that would accommodate the new PVF Manufacturing Facility follows: 1. Continue to operate existing wastewater treatment facilities consisting of: • equalization; (etc) 2. To operate new wastewater treatment facilities consisting of: • clarifier for PVF process wastewater; 3. Discharge treated process wastewater from Butacite, Nafion, PVF, and Teflon® PMDF, process stormwater, sanitary wastewater, and co -neutralized regenerate form said treated facilities through internal outfall 001; The process wastewater is expected to contain unreacted vinyl fluoride (CAS No. 00075-02-5). The anticipated quantity of vinyl fluoride from the PVF Manufacturing Facility is 0.312 pounds per day. This quantity would equate to approximately 0.04 mg/L vinyl fluoride at Outfall 001 and 0.0035 mg/L vinyl fluoride at Outfall 002. Finally, non -contact cooling, condensate, and stormwater from the PVF Manufacturing Facility will be discharged directly to Outfall 002 via the site's Woodlined Ditch. DEQ-CFW 00076666 JUN -6 07 DEQ-CFW-00076667 Form 2C. Part III B: WATER BALANCE (Revised 4/15(06) DuPont - Fayetteville, NC Flows Unit: GPD Basis: All Production Manufacturing, using Maximum 30 day average of measured flows NPDES PERMIT APPLICATION River Chlorine NON CONTACT T COOLING Non -Contact Cooling Water -----+ 13043755 tofromeach —-------------------------------------------------------------------------------------------►15 unit I 1 R I.4R AY0 I Filtered Water Supply DEMINERALIZERS Neutralized Regenerate Groundwater Wdb 13C Chlorine Potable Water Supply Plant 8,000 EEvap. Sanitary BOI Fadlitles Stormwstar c 12,000 8,000 150,000 D 0 Stormwater from Process Area Pads Non -process Storrnwater 10,000 10t000 45,000 DYMETRO EPS TAP RX L=eMe�L 4WPCH & CUTTERS & & WASH GRUBBERS "1 1 1 10,000 1 10,000 1 45,000 760 BUTACITE FLAKE EXTRUSION RECYCLE 0 NAFION CAUSTIC ACID TREATERS & FPX SCRUBBERS SCRUBBERS PROCESS PROCESS & SCRUBBERS$ 1.180.439 86,000 102,700 Eva BIOfO�s JTo Landfill DI sal Biological WWTP ............... Dewabr/...................................... .....W Drying T 10 000 1,00 � BIOSOLIDS SOLID WASTE 001 fi"�c. 0 Phyekal SoaM Separation Tnatmnn Fi 12,286 4 0 c m v 177,OC Product Lw & Unit Evaporrtbn 1 67,700 1 aC)p1 DEQ-CFW 00076668 4 Form 2C. Part III B: WATER BALANCE (Revised 4115106) DuPont - Fayetteville, NC Flows Unit: GPD Basis: All Production Manufacturing, using Maximum 30 day average of measured flows ---C — NPDES PERMIT APPLICATION Fear River Chlorine NON CONTACT 16,478,794 COOLING Non -Contact Cooling Water ---- I. 13043755 to/fromeach - -------------------------------------------------------------------------------------------►15043755--------------------------- unit 1 1 3 3.439 1 2.000.000 2,422,000 Filtered Water Filtered Water Supply DEMINERAL¢ERS Regenerate Chlorine Potable Water Supply Plant I Stormwater I Stommater from Process Area Pads Non -process Stonnwater kv+C ��2 sit±s: i I Sanitary BOILERS Facllldas I DYMETRO EPS TAPE TRX L QUENCH QUENCH & CUTTERS & & WASH WASH SCRUBBERS 1 1 I BUTACITE FLAKE I EXTRUSION RECYCLE NAFION a CAUSTIC ACID TREATERS & FPX MMF SCRUBBERS SCRUBBERS PROCESS PROCESS 8 5 g SCRUBBERS 102,700 Eva Biological WWTP Bhuolids oawmd......................................t......i 1To Landfill DI s oral - *--�—� 10 DDQ 1,000 Drying 1 i BIOSOUDS SOLID WASTE PVF Ph" ISoeds Sapantion Tnatm at 5 r QC Y g v 2 a ro c u Product Loss a une E"poraaon 1 67,700 1 DEQ-CFW 00076669 FORM U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. Number 1 GENERAL INFORMATION 6 TIA C GENERAL Consolidated Permits Program F NC0003573 I D + 2 13 t, 15 Read the "General Instructions" before starting.) LABEL ITEMS s GENERAL INSTRUCTIONS If a preprinted label has been provided, affix it in the designated space. F NC0003573 Review the information carefully; if any of it is incorrect, cross through it and enter the correct data in the appropriate fill—in area below. Also, if any of the DuPont Fayetteville Works y preprinted data is absent (the area to the left of the label space lists the 828 NC Hwy 87 W Fayetteville, information that should appear), please provide it in the proper fill—in area(s) NC 28306-7332 below. If the label is complete and correct, you need not complete Items, 1, III, V, and A (except VI-B which must be completed regardless). Complete all 22828 NC Hwy 87 W Duart items if no label has been provided. Refer to the instructions for detailed item Township, NC 28306 descriptions and for the legal authorizations under which this data is collected. II. POLLUTANT CHARACTERISTICS INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, you must submit this form and the supplemental form listed in the parenthesis following the questions. Mark "X" in the box in the third column if the supplemental form is attached. If you answer "no" to each question, you need not submit any of these forms. You may answer "no" if your activity is excluded from permit requirements; see Section C of the instructions. See also, Section D of the instructions for definitions of bold --faced terms. MARK'X' MARK W SPECIFIC QUESTIONS YES NO FORM ATTACHED SPECIFIC QUESTIONS YES No FORM ATTACHED A. Is this facility a publicly owned treatment works B. Does or will this facility (either existing or proposed) include a which results in a discharge to waters of the U.S. 7 X concentrated animal feeding operation or aquatic animal pro- X (FORM 2A) duction facility which results in a discharge to waters of the U.S? I6 17 i6 19 z, FORM 28 C. Is this a facility which currently results in discharges X X D. Is this a proposed facility (other than those described in A or B X to waters of the U.S. other than those described in above) which will result in a discharge to water of the U.S. ? 22 23 z+ 25 25 27 A or B above FORM 2C FORM 2D E. Does or will this facility treat, store, or dispose of F. Do you or will you inject at this facility industrial or municipal hazardous wastes? (FORM 3) X (1) effluent below the lowermost stratum containing, within one quarter mile of the well bore, underground sources of drinking X 28 29 30 31 33 water? FORM 4 G. Do you or will you inject at this facility any produced H. Do you or will you inject at this facility fluids for special process, water or other fluids which are brought to the surface such as mining of minerals, in situ combustion of fossil fuel, in connection with conventional oil or natural gas pro- X or recovery of geothermal energy ? X duction, inject fluids used for enhanced recovery of (FORM 4) oil or natural gas, or inject fluids for storage of liquid 34 35 36 37 3B 39 hydrocarbons? FORM 4 I. Is this facility a proposed stationary source which is J. Is this facility a proposed stationary source which is NOT one one of the 28 industrial categories listed in the in- X of the 28 industrial categories listed in the instructions and X structions and which will potentially emit 100 tons and which will potentially emit 250 tons per year of any air per year of any air pollutant regulated under the pollutant regulated under the Clean Air Act and may effect Clean Air Act and may affect or be located in an or be located in an attachment area's (FORM 5) attainment area ? FORM 5 +0 {t +2 143 ++ 45 III. NAME OF FACILITY 1 SKIP E.I. du Pont de Nemours & Company 30 CONTACT IV. FACILITY A. NAME & TITLE (Last, first, & Tffle) B. PHONE (area code & no) 2 Michael E. Johnson, Environmental Manager (910) 678 1155 16 ,6 45 46 46 1 49 - 51 52 55 V. FACILITY MAILING ADDRESS A. STREET OR P.O. BOX 3 22828 NC Hwy 87 W +5 15is B. CITY OR TOWN C. STATE ID.ZIPCODE 4 Fayetteville NC 8306=t382 VI. FACILITY LOCATION A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER i 5 22828 NC Hwy 87 W +5 15 B. COUNTY NAME Bladen 48 70 C. CITY OR TOWN D. STATE E. ZIP CODE; F. COUN7V CODE F41 Duart Township NC [:2� 7 011{0 52 5{. N - {2 EPA Form 3510-1 8-90 '(1) Permitted under Federal and State Laws No Forms 3 or 4 required,- s e-Atl1a6ment 1-1 DEQ-CFW 00076670 CONTINUED FROM THE FRONT VII. SIC CODES taapx wda...r,.lw+yt A. FIRST B. SECOND rill 2869 (specify) 7 NaflonO Solution, Vinyl Ether and HFPO monomers 2821 (specify) Teflon® FEP resin, Polyvinyl flouride resin Polyvinyl butyral Resin, Naflon® Resins - a C. THIRD D. FOURTH 7 3081 (specify) Naflon® Membrane, (specify) Butacite® sheeting, SentryGlas Plus ' r Vlll. OPERATOR INFORMATION B. Is the name listed in Item VIII-A also the A. NAME owner7 8 ® Yes ❑ No 75 16 E. I. DuPont de Nemours & Co., Inc. es ea C. STATUS OF OPERATOR D. PHONE NUMBER —� A— s-smr o-oe•tlx,.,,roe..ipx.al e.s� P (specify) NA ., 302 ., 09 774 e, 1000 E. STREET OR P.O. BOX 1007 Market Street .e C. STATE D. ZIP CODE IX. INDIAN LAND F. CITY OR TOWN 8 Wilmin ton DE 19898 Is the ciitLandsedonIndian Lands? 15 1e /e 41. 42 tl - 51 sx ❑Yes ® No X. EXISTING ENVIRONMENTAL PERMIT A. NPDES (Discharges to Surface Water D. RSSO Air Emissions from Proposed Sources 9 1s NC0003573 9 Title V - 0373ST28 (Major Source 17 ao B. UIC (Underground Injecdon of Fluids E. OTHERS S (specify) 9 NA 9 NA 15 16 17 C. RCRA Hazardous Wastes D. OTHERS S (specify) 9 1s 1e n NCD 047 368 642 and 90 day storage. tore a area 9 NA 1s m +� 30 XI. MAP Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the location of each of its existing and proposed intake an discharge structures, each of XII. NATURE OF BUSINESS (provide a brief description) > Manufacturing of DuPontTM Teflon® FEP resin. > Manufacturing of DuPontTM SentryGlas Plus® . > Manufacture of DuPontTm Naflon® Membrane, Naflon® Resins, Naflon® Solution, FLPR Vinyl Ether and HFPO monomers > Manufacture of Polyvinyl butyral (PVB) Resin and DuPontTM Butacite® Interlayer plastic sheeting > Manufacture of Ammonium perfluorooctanoate (APFO) > Manufacture of Polyvinyl flouride resin (PVF) XIII. CERTIFICATION (see Instructions) I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible fof obtaining the information cont A. NAME & OFFICIAL TITLE (type or print) B. SIGNATURE C. DATE SIGNE Barry L. Hudson, Plant Mgr -� COMMENTS FOR OFFICIAL USE ONLY 8 18 1s ,EPA Form 3510-1 (8-90) DEQ-CFW 00076671 Form Approved. Please print or type in the unshaded areas only. EPA I.D. NUMBER F N C0003573 OMB No. 2040-0086 I Approval expires 8-31-98 FORM 2V NPDES U.S. ENVIRONMENTAL PROTECTION AGENCY APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURAL OPERATIONS Consolidated Permits Program I. OUTFALL LOCATION each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. NUMBER (list) B. LATITUDE C. LONGITUDE D. RECEIVING WATER (name) 1. DEG 2. MIN. 3. SEC. 1.DEG. 1 2. MIN. 3. SEC. 001 34 50 25N 78 50 9W Cape Fear River via Outfall 002 002 34 50 22N 78 50 9W Cape Fear River 006 34 50 20N 78 49 55W ICape Fear River via Outfall 002 II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each outfall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff, (2) The average flow contributed by each operation, and (3) The treatment received by the wastewater. Continue on additional sheets if necessary. 1.OUTFALL NO (list) 2. OPERATION (S) CONTRIBUTING FLOW 3. TREATMENT a. OPERATION (list) b. AVERAGE FLOW (include units) a. DESCRIPTION b. LIST CODES FROM TABLE 2C-1 002 Outfall 001 965,039 GPD Discharge to Surface Water (Cape Fear River) 4-A Outfall 006 100,000 GPD Non -contact water 15,220,755 GPD Boiler B/D, Stormwater 193,000 GPD TOTAL 16,478,794 GPD 001 NAFION AREA: Biological Wastewater Treatment Plant: Neutralization 61,429 GPD WWTInfluent Sump 1-0 Treaters & FPX Process 12,286 GPD Equalization (equipped with Mixing & Aeration 1-0; 3-E MMF Process & Scrubber 12,286 GPD Emergency Retention Tank 1-0 BUTACITE AREA: Pre -Digester Tank 3-E - Flake 665,760 GPD Activated Sludge Tank 3-A -Extrusion 1,329 GPD Clarification 2 in -ground inparallel) 1-U - Recycle 292,350 GPD SENTRY GLASS AREA - Quench & Wash 10,000 GPD TEFLON AREA EPS Tape Quench & Wash 10,000 GPD TRX Cutters & Scrubbers 45,000 GPD Neutralized Regenerate 50,000 GPD Sanitary Sewer 8,000 GPD Contact Stormwater 12,000 GPD TOTAL 1,180,439 GPD 006 PVF PROCESS 1 100,000 GPD Solids Separation 1-U TOTAL 1 100,000 GPD OFFICIAL USE ONLY (effluent guidelines sub -categories) r-rH rorm sD Iu-.e , (u-au) PAGE 1 of 4 CONTINUE ON PAGE 2 DEQ-CFW 00076672 CONTINUED FROM PAGE 1 C. Except for storm runoff, leaks or spills, are any of the discharges described in Items II -A or B intermittent or seasonal? YES (complete the following table) X INO (go to Section 111) A.OUTFALL NUMBER (list) 2. OPERATIONS(s) CONTRIBUTING FLOW (list) 3. Frequency 4. Flow a. DAYS PER WEEK (specifyaverage) b. MONTHS PER YEAR (specifya-rage) a. FLOW RATE (in m4 d) b. TOTAL VOLUME (specify with units C. DURATION (in days) a. LONG TERM AVERAGE 2. MAXIMUM DAILY 1. LONG TERM AVERAGE 2. MAXIMUM DAILY Ill. PRODUCTION A. Does an effluent guideline limitation promulgated X by EPA under Section 304 of the Clean Water Act apply YES (complete Item III-B) to your facility? NO (go to Section IV) B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)? YES (complete Item Ill-C) X NO (go to Section IV) C. If you answered "Yes" to Item III-B, list the quantity which represents an actual measurement of your level of production expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outfalls. Not applicable 1.AVERAGE DAILY, PRODUCTION 2. AFFECTED OUTFALLS (list OUti2ll nurnbers) a. QUANTIT DAY b. UNITS OF MEASURE c. OPERATION, PRODUCT, MATERIAL, ETC. (specify) No production based applicable effluent guidelines IV. IMPROVEMENTS A.Are you now required by any Federal, State or Local authority to meet any implementation schedule for the construction, upgrading, or operation of wastewater treatment equipment or practices or any other environmental programs which may effect the discharges described in this application? This includes but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions. YES (complete the following Table) X NO (go to Section IV-B) 1. IDENTIFICATIONS OF CONDITION, AGREEMENT, ETC. 2. AFFECTED OUTFALLS 3. BRIEFDESCRIPTION OF PROJECT 4. FINAL COMPLIANCE DATEa A No. '.b. SOURCE DISCHARGEE a. REQUIRED B. PROJECTED OPTIONAL:B. You may attach additional sheets describing any additionahmer pollution control programs or other environmental projects w rc may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned and indicate your actual or planned schedules for construction. MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED EPA Form 3510-2C (8-90) PAGE 2 OF 4 CONTINUE ON PAGE 3 DEQ-CFW 00076673 Form Approved. EPA I.D. NUMBER (copy from Item 1 of Form 1) lApproval OMB No. 2040-0086 NC0003573 expires 8-31-98 CONTINUED FROM PAGE 2 V. INTAKE AND EFFLUENT CHARACTERISTICS A, B, & C : See instructions before proceeding - Complete one set of tables for each outfall - Annotate the outfall number in the space provided. Note: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9. D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession. 1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE None of the pollutants listed in Table 2C-3 of the instructions are believed to be present in the discharge. VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct? (Y IYES (list all such pollutants below) �NO (go to Section VI-B) Applicable guidelines require testing all V-C compounds identifying any potential discharges EPA Form 3510-2C (8-90) PAGE 3 OF 4 CONTINUE ON PAGE 4 DEQ-CFW 00076674 CONTINUED FROM PAGE 3 VII. BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? X YES (identify the test(s) and describe their purposes below) �NO (go to Section Vlll) North Carolina c. dubia Chronic Pass/Fail Reproduction Toxicity Tests performed each quarter in accordance with NPDES permit conditions. No toxicity effect reported during last 3 years of testing final discharge. NC DENR has copies of test results submitted with DMRs last 3 years. VIII. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? X YES (list the name, address, and telephone number of, �NO (go to Section IX) and pollutants analyzed by, each such laboratory or firm below) A. NAME B. ADDRESS C. TELEPHONE (area code & D. POLLUTANT ANALYZED (list) no. Pace Analytical 2225 Riverside Drive, 828.254.7176 Aquatic Toxicity Services, Inc. Ashville, NC 28804 TBL 2401 W. 5th Street 910.738.6190 Lumberton, INC BOD5, COD, TSS, Priority Pollutants, Fluoride, Total Phosphorous, Total Nitrogen IX. CERTIFICATION I certify under penalty of law this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. NAME & OFFICIAL TITLE (type of print) B. PHONE NO. (area code & no.) Barry L. Hudson, Plant Mgr (910) 678-1247 C. SIGNATURE D. DATE SIGNED 6 -K. k1l (d EPA Form 3510-2C (8-r' PAGE 4OF4 DEQ-CFW 00076675 -6 07 DEQ-CFW 00076676 0 r' n n Io 0 0 v rn rn v v UNITED STATES �? DEPARTMENT OF THE INTERIOR `� GEOLOGICAL SURVEY 78° 5 34° 52' 30" 1 NOW* I 31 5 4 DUART QUADRANGLE STATE OF NORTH CAROLINA NORTH CADRAN DEPARTMENT OF NATURAL RESOUR 7.5 MINUTE SERIES (TOPOGRAPHIC) w' AND COMMUNITY DEVELOPMENT SEJ4 SAINT PAULS IF QUADRANGLE , V RAL 253 tv N. C. ' S153 !V NE IrFnAR rREEKI �30„ 695 E m GRAYS CREEK 6 f li 697 1 � 12119 b 144 137 •ram, x i • _\\ 251 '' � 1 � I � - j, _ - i. � I I `11 ° _' r C. � 7sa� `�__ BervirT i �._ tb0 I� , �4 / o, lir 11' ,\. ' Mill �ek o II (I, ( � (r .I\\ I' 1 p, 21• � - -- k k so 58 1.Trok� � e. \ ` B 159 _ O� Tanks (`1 � nd was onds I t 7 tbstat 1 11. Huske toeka Dom No3 0 ° o' I I 9 0' t SITE \ e BOUNDARY V PI iv?) v Iif ,'I ,I 0. 7 pan ter d Lp \II, , em (Il nr I it 137 Radio o - _ Tower Boat Ramp 8 M Cho _ (\_ •�__ 1 \\ __zus As 1 ° 'am Wirt c 135 . , .I . "� noaa¢¢ssilde, l arDii lF.... 3952 • O - -` r� \ 1' \ �`..� / r 1' . `�Inn51 I I .\ BM 53� 7' 30" \� \ 11 \ \ f, a Form 2C. Part III B: NPDES PERMIT APPLICATION WATER BALANCE (Revised 4115106) DuPont - Fayetteville, NC Flows Unit: GPD Basis: All Production Manufacturing, using Maximum 30 day average of measured flows Fear River Outfall 002 Chlorine NON -CONTACT COOLING Non -Contact Cooling Water -- - -- 13043755 tolfrom each - - - -------- - - - - -- unit 1---------- I 1.F11. A10 1 Filtered Water Supply DEMINERALIZERS 1t,vo t,Ers E Neutralized Regenerate :Groundwater Wells Chlorine Potable Water Supply Plant Sanitary Facilities Stormwater Stormwater from Process Area Pads Non -process Stormwater BOILERS DYMETROL EPS TAPE TRX QUENCH & QUENCH & CUTTERS & WASH WASH SCRUBBERS 1 1 1 10,000 I 10,000 1 45,0U0 78,6791 45,000 5,000 1151000—I I 1 + BUTACITE FLAKE EXTRUSION rRECYCLE NAFION CAUSTIC ACID TREATERS & FPXJ MMF SCRUBBERS JSCRUBBERS PROCESS PROCESS & SCRUBBERS NEUTRAL- I DMSC IZATION STILL r rou Yaaa I oo,uve.. I' 102,700 [B ios . To-----ll --- ---- Landfi Biological WWiP Mol'i.d'3 ..................................10 000 1 000 BIOSOLIDS SOLID WASTE nz 129,000 -� 65 039 i ------- ----- ----- ---------- -- �� Outfa11001 Product Loss & Unit Evaporation 1 67,700 -� PVF Phys' solids m Separation 15 Treatment 0 U C O C C 3 0 a 3 0 a m N c U Outfall 006 DEQ-CFW 00076678 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information on separate sheets (use the same format) instead of completing these pages. SEE INSTRUCTIONS E P A. I . Number (copy from Item 1 of Form 1) NC0003573 Form Approved OMB No. 2040 0086 An 'm --a_a1 oa V. INTAKE & EFFLUENT CHARACTERISTICS (Continued from page 3 of Form 2-C) _ OUTFALL NO. -YouPART A must provide the resultsat o east one analysis or every po u an In Is to e. Complete one table or eac outtall ee Instructions or a I Iona e I s. 001 2. EFFLUENT 3. UNITS 4. INTAKE (optional) 1. POLLUTANT AND CAS NO a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (ifavailable) b. LONG TERM AVRG. VALUE (if available) d. NO. OF (Speciy if blank) a. LONG TERM AVERAGE VALUE ANALYSES b NO OF (ifavailable) CONCENTRATION (2) MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS aCONCENTRATION b. MASS (T) CONCENTRATION (2)MASS ANALYSES a. Biochemical Oxygen Demand 367.0 2981.2 33.30 265.90 9.70 72.30 169 MG/L PPD NA NA NA (BOD) b. Chemical Oxygen Demand NA NA NA NA MG/L PPD NA NA NA (COD) c. Total Organic Carbon (TOC) NA NA NA NA MG/L PPD NA NA NA d. Total Suspended Solids (TSS) 56.0 349.3 26.70 169.80 18.90 133.20 169 MG/L PPD NA NA NA e. Ammonia (as N) NA NA NA NA MG/L PPD NA NA NA I. Flow value 1.30 value 1 0 value 0.9 395 MGD value NA NA g. Temperature value value value value (winter) 23.0 18.7 17.2 79 °C NA NA h. Temperature value value value value (summer) 30.0 23.0 21 0 88 NA NA Minimum Maximum Minimum Maximum i. pH 6.9 8.0 NA NA 167 STANDARD UNITS PART B -Mark "X" in column 2a for each pollutant you know or have reason to believe is present. Mark "X" in column 2b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if b. NO. OF a. MMIMUM DAILY VALUE available) a. LONG TERM AVERAGE VALUE ANALYSES 7RES-,,,�T D. NO. OF 1. POLLUTANT & CAS NO. (ifavailable) b BELIEVED (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS ANALYSES 11j CONCENTRATION (2)MASS (1)CONCEN-TION (2)MASS ABSENT a. Bromide X ` NA NA NA NA (24959-67-9) NA NA NA b. Chlorine X NA NA NA NA Total Residual NA NA NA c. Color X NA NA NA NA NA NA NA d. Fecal X NA NA NA NA Coliform NA NA NA e. Fluoride X NA NA NA NA ( 16984-48-8 ) NA NA NA f. Nitrate— X NA NA NA NA Nitrite (as N) NA INA INA t_PA Form 3510-2c (8-90) PAGE V-1 ITEM V-B CONTINUED FROM PREVIOUS PAGE 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK " X" b. MAXIMUM 30 DAY VALUE (i1 c. LONG TERM AVRG. VALUE (il a. MAXIMUM DAILY VALUE a —fable) a table) a. LONG TERM AVERAGE VALUE (1favailable) (1) CONCENTRATION (2) MASS D. NO. OF ANALYSES a. BELIEVED PRESENT b.BELIEVED ABSENT (1) CONCENTRATION (2) MASS (i) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d. NO. OF ANALYSES (1) CONCENTRATION (2) MASS g. Nitrogen, Total Organic (as N) X NA NA NA NA NA NA NA h. Oil and Grease X 28 223 28 223 NA NA 14 MG1 PPD NA NA NA i. Phosphorus NA NA NA (as P) , Total X NA NA NA NA NA NA NA (7723-14-0) NA NA NA '. Radioactivity (1) Alpha, Total x NA NA NA NA NA NA NA (2) Beta, Total X NA NA NA NA NA NA NA (3) Radium, total X NA NA NA NA NA NA NA (4) Radium 226 Total X * NA NA NA NA NA NA NA k. Sulfate (as SO4) (14808-79-8) X * NA NA NA NA NA NA NA I. Sulfide (as S) X * NA NA NA NA * NA NA NA m. Sulfite (as S03) (14265-45-3 X NA NA NA NA NA NA NA n. Surfactants X * NA NA NA NA NA NA NA o. Aluminum, Total (7429-90-5) X NA NA NA NA NA NA NA p. Barium, Total (7440-39-3) X NA NA NA NA NA NA NA q. Boron, Total (7440-42-8) X NA NA NA NA NA NA NA r. Cobalt, Total (7440-48-4 ) X NA NA NA NA NA NA NA s. Iron, Total (7439-89-6) X NA NA NA NA NA NA NA I. Magnesium (7439-95-4) X NA NA NA NA NA NA NA u. Molybdenum, Total (7439-98-7) X NA NA NA NA NA NA NA v. Manganese, (7439-96-5) X NA NA NA NA NA NA NA w. Tin Total X NA NA NA NA NA NA NA (7440-31-5) x. Titanium,Total (7440-32-6) X NA NA NA NA NA NA NA EPA Form 3510-2C (8-90) PAGE V-2 CONTINUED ON PAGE V-3 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE 3 OF FORM 2-C NC0003573 1 001 Form Approved OMB No. 2040 0086 Annrn„.I ov — A_'2t_OA PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GCIMS fractions you must test for. Mark "X" in column 2 -a for all such GCIMS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2a (secondary industries, nonprocess wastewater outfalls, and nonrequired GCIMS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile 2,4 dinitrophenol, or 2-methyl-4,6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part, please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. VALUE a. MAXIMUM DAILY VALUE available) available) a. LONG TERM AVERAGE VALUE (If dvdildblfJ (1) d. NO. OF (1) b. NO. OF a TESTING I b. BELIEVED c.BELIEVED (1) REQUIRED PRESENT ABSENT (1)CONCENTRATIO (21 MASS CONCENTRATION 2 MASS ( J 1 CONCENTRATION ( I (2) MASS ANALYSES CONCENTRATION 1 (2) MASS CONCENTRATION 1 (2) MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony Total (7440-36-0) X NA NA NA NA NA NA NA 2M. Arsenic, Total (7440-38-2) X NA NA NA NA NA NA NA 3M. Beryllium, Total (7440-41-7) X NA NA NA NA NA NA NA Cadmium, Total (7440-43-9) X NA NA NA NA NA NA NA Chromium, I o a (7440-47-3) X NA NA NA NA NA NA NA 6M. Copper, Total (7440-50-8) X NA NA NA NA NA NA NA 7M. Lead, Total (7439-92-1) X NA NA NA NA NA NA NA 8M. Mercury, Total (7439-97-6) X NA NA NA NA NA NA NA 9M. Nickel, Total (7440-02-0) X NA NA NA NA NA NA NA 10M. Selenium, Total (7782-49-2) X NA NA NA NA NA NA NA 11 M. Silver Total (7440-22-4) X NA NA NA NA NA NA NA 12M. Thallium Total (7440-28-0) X NA NA NA NA NA NA NA 13M. Zinc, Total (7440-66-6) X NA NA I NA I NA NA NA NA 14M. Cyanide, Total (57-12-5) X NA NA NA NA NA NA NA 15M. Phenols, Total X NA NA NA NA NA NA NA DIOXIN 2,3,7,8 -TetrachloridIbenzo-P Dioxin (1764-01-6) X NA NA NA NA EPA Form 3510-2C (8-90) PAGE V-3 CONTINUED ON PAGE V-4 ITEM V-B CONTINUED FROM PREVIOUS PAGE 3. EFFLUENT 4. UNITS S. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" a. MAXIMUM DAILY h. MAXIMUM 30 DAY VALUE !il c. LONG TERM AVRG. VALUE (J VALUE avalablel avagable) a. LONG TERM AVERAGE VALUE (lfavailable) d. NO OF (I b. NO. OF a. TESTING b. BELIEVED c.BELIEVED (1) (1) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS ANALYSES (1) CONCENTRATION (2)MASS CONCENTRATION (21011— ANALYSES TILE C 1 V. Acrolein (107-02-8) X NA NA NA NA NA NA NA NA 2V. Acrylonitrile (107-13-1) X NA NA NA NA NA NA NA NA 3V. Benzene (71-43-2) X NA NA NA NA NA NA NA NA 4V. Bis (Chloromethyl) Ether (542-88-1) X NA NA NA NA NA NA NA NA 5V. Bromoform ( 75-25-2) X NA NA NA NA NA NA NA NA 6V. Carbon Tetrachloride (56-23-5) X NA NA NA NA NA NA NA NA 7V. Chlorobenzene (108-90-7) X NA NA NA NA NA NA NA NA 8V. Chlorodibromomethane (124-48-1) X NA NA NA NA NA NA NA NA 9V. Chloroethane (75-00-3) X NA NA NA NA NA NA NA NA 1OV. 2 Chlorohylvinyl Ether (110-75-8) X NA NA NA NA NA NA NA NA 11V. Chloroform (67-66-3) X NA NA NA NA NA NA NA NA 12V. Dichlorobromomethane (75-27-4) X NA NA NA NA NA NA NA NA 13V. Dichlorodifluoromethane (75-71- 8) X NA NA NA NA NA NA NA NA 14V. 1,1 Dichloroethane (75-34-3) X NA NA NA NA NA NA NA NA 15V. 1,2 Dichloroethane (107-06-2) X NA NA NA NA NA NA NA NA 16V. 1,1 Dichloroethylene (75-35-4) X NA NA NA NA NA NA NA NA 17V. 1,2 Dichloropropane (78-87-5) X NA NA NA NA NA NA NA NA 18V. 1,3 Dichloropropylene (542-75-6) X NA NA NA NA NA NA NA NA 19V. Ethylbenzene(100-41-4) X NA NA NA NA NA NA NA NA 2CV. Methyl Bromide (74-83-9) X NA NA NA NA NA NA NA NA 21V. Methyl Chloride (74-87-3) X NA NA NA NA NA NA NA NA r-rH r-orm so-lu-zu u-gut PAGE V-4 CONTINUED ON PAGE V-5 !1 1 , , -�J"i, 5 07 DEQ-CFW-00076683 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V4 I NC0003573 1 001 Form Approved OMB No. 2040 0086 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" a. MAXIMUM DAILY b. MAXIMUM SO DAY VALUE (il c. LONG TERM AVRG. VALUE (,f VALUE available) available) a. LONG TERM AVERAGE VALUE a. TESTING REQUIRED b. BELIEVED PRESENT c.BELIEVED ABSENT (1)CONCENTRATION (2)MASS (�) CONCENTRATION (2)MASS (�) CONCENTRATION (2)MASS (�) CONCENTRATION (2) MASS (If avalldble) tl. NO. OF ANALYSES (�) CONCENTRATION (2) MASS b. NO. OF ANALYSES GC/MS FRACTION —VOLATILE COMPOUNDS (continued) 22V Methylene Chloride (75-09-2) X NA NA NA NA NA NA NA NA 23V.1,1,2,2 Tetrachloro- ethane (79-34-5) X NA NA NA NA NA NA NA NA 24V. Tetrachloroethylene (127-18-4) X NA NA NA NA NA NA NA NA 25V. Toluene (108-88-3) X NA NA NA NA NA NA NA NA 26V. 1,2-TransDichloro- ethylene (156-60-5) X NA NA NA NA NA NA NA NA 27V. 1,1,1 Trichloroethane (71-55-6) X NA NA NA NA NA NA NA NA 28V. 1,1,2 Trichloroethane (79-00-5) X NA NA NA NA NA NA NA NA 29V. Trichloroethylene (79-01-6) X NA NA NA NA NA NA NA NA 30V. Trichlorofluoro- methane (75-69-4) X NA NA NA NA NA NA NA NA 31 V. Vinyl Chloride (75-01-4) X NA NA NA NA NA NA NA NA GC/MS FRACTION —ACID COMPOUNDS 1A. 2 Chlorophenol (95-57-8) X NA NA NA NA NA NA NA NA 2A 2,4 Dichlorohenol (120-83-2) X NA NA NA NA NA NA NA NA 3A. 2,4 Dimethylphenol (105-67-9) X NA NA NA NA NA NA NA NA 4A 4,6 Dinitro-O-Cresol (534-52-1) X NA NA NA NA NA NA NA NA 5A. 2,4 Dinitrohenol (51-28-5) X NA NA NA NA NA NA NA NA 6A.2-Nitrophenol(88-75-5) X NA NA NA NA NA NA NA NA 7A4-Nitrophenol(100-02-7) X NA NA NA NA NA NA NA NA 8A. P-Chloro-M-Cresol 59-50-7 X NA NA NA NA NA NA NA NA 9A. Pentachlorophenol (87-86-5) X NA NA NA NA NA NA NA NA 10A. Phenol (108-95-2) X NA NA NA NA NA NA NA NA 11A. 2,4,6 Trichloro- phenol (88-06-2) X NA NA NA NA NA NA NA NA EPA Form 3510-2C (8-90) PAGE V-5 CONTINUED ON PAGE V-6 CONTINUED FROM PAGE V-6 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" a. MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE (if c. LONG TERM AVRG. VALUE (if VALUE available) available) a. LONG TERM AVERAGE VALUE a TESTING REQUIRED b. BELIEVED PRESENT c.BELIEVEO ABSENT (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS (/(available) d_ NO. OF ANALYSES 1) CONCENTRATION (2)MASS b NO OF ANALYSES BASE/NEUTRAL COMPOUNDS iB. Acenaphthene (83-32-9) X NA NA NA NA NA NA NA NA 2B. Acenaphtylene (208-96-8) X NA NA NA NA NA NA NA NA 313. Anthracene (120-12-7) X NA NA NA NA NA NA NA NA 4B. Benzidine (92-87-5) X NA NA NA NA NA NA NA NA 5B. Benzo (a) Anthracene (56-55-3) X NA NA NA NA NA NA NA NA 6B. Benzo (a) Pyrene (50-32-8) X NA NA NA NA NA NA NA NA 763,4 Benzofluororanthene (205-99-2) X NA NA NA NA NA NA NA NA - 813. Benzo(ghi)Perylene (191-24-2) X NA NA NA NA NA NA NA NA 9B. Benxo (k) Fluoranthene (207-08-9) X NA NA NA NA NA NA NA NA 10B. Bis(2-Chloroethoxy) Methane (111-91-1) X NA NA NA NA NA NA NA NA 11 B. Bis(2-Chloroethyl) Ether (111-44-4) X NA NA NA NA NA NA NA NA 12B Bis(2Chlorolsopropyl) Ether (102-60-1) X NA NA NA NA NA NA NA NA 13B. Bis(2-Elthylhexyl) Phthalate (117-81-7) X NA NA NA NA NA NA NA NA 1413.413romophenyftenyl Ether (101-55-3) X NA NA NA NA NA NA NA NA 15B. Butyl Benzyl Phthalate (85-68-7) X NA NA NA NA NA NA NA NA 16B. 2-Chloronapthalene (91-58-7) X NA NA NA NA NA NA NA NA 17B.2-Chlorophenyl Phenyl Ether (7005-72-3) X NA NA NA NA NA NA NA NA 18B.Chrysene(218-01-9) X NA NA NA NA NA NA NA NA 19B. Dibenzo (a,h) Anthracene (53-70-3) X NA NA NA NA NA NA NA NA 20B. 1,2 Dichlorobenzene (95-50-1) X NA NA NA NA NA NA NA NA 21B. 1,3 Dichlorobenzene (541-73-1) 1X INA NA NA NA NA NA NA NA tPA Form 3510-2C (8-90) PAGE V-6 CONTINUED ON PAGE V-7 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-6 NC0003573 nn1 Form Approved OMB No. 2040 0086 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" a. MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE (if c. LONG TERM AVRG. VALUE (if VALUE available) available) a. LONG TERM AVERAGE VALUE a. TESTING REQUIRED b. BELIEVED PRESENT BELIEVED ABSENT (1) CONCENTRATION (2)MASS (1) CONCENTFATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (If available) tl NO. OF ANALYSES (1) CONCENTRATION (2)MASS U NO OF ANALYSES OCIMS FRACTION—B OMPOUNDS (Continued) 22B. 1,4 Dichlorobenzene (106-46-7) X NA NA NA NA NA NA NA NA 23B.3,3' Dichlorobenzidine (91-94-1) X NA NA NA NA NA NA NA NA 24B. Diethyl Phthalate (84-66-2) X NA NA NA NA NA NA NA NA 25B. Dimethyl Phthalate (131-11-3) X NA NA NA NA NA NA NA NA 266. Di-N-Butyl- Phthalate (84-74-2) X NA NA NA NA NA NA NA NA 27B. 2,4 Dinitro toluene (121-14-2) X NA NA NA NA NA NA NA NA 28B. 2,6 Dinitrotoluene (606-20-2) X NA NA NA NA NA NA NA NA 29B. Di-N-Octyl Phthalate (117-84-0) X NA NA NA NA NA NA NA NA' 30B. 1 2 Diphenylhydrazine (as Azobenzene) (122-66-7) X NA NA NA NA NA NA NA NA 31 B. Fluoranthene (206-44-0) X NA NA NA NA NA NA NA NA 32B. Fluorene (86-73-7) X NA NA NA NA NA NA NA NA 33B. Hexachlorobenzene (118-74-1) X NA NA NA NA NA NA NA NA 3413. Hexachlorobutadiene (87-68-3) X NA NA NA NA NA NA NA NA 35B. Hexachlorocyclo- pentadiene (77-47-4) X NA NA NA NA NA NA NA NA 36B. Hexachloroethane (67-72-1) X NA NA NA NA NA NA NA NA 37B.Indeno1,2,3 cdPyrene (193-39-5) X NA NA NA NA NA NA NA NA 38B. Isophorone (78-59-1) X NA NA NA NA NA NA NA NA 39B. Naphthalene (91-20-3) X NA NA NA NA NA NA NA NA 40B.Nitrobenzene (98-95-3) X NA NA NA NA NA NA NA NA 41 B. N-Nitrosodime- thylamine (62-75-9) X NA NA NA NA NA NA NA NA 42B. N-Nitrosodi-N- Propylamine (621-64-7) X NA NA NA NA NA NA NA NA tPA Form 3510-2C (8-90) PAGE V-7 CONTINUED ON PAGE V-8 CONTINUED FROM PAGE V-7 1. POLLUTANT AND CASE NO (lf available) 2. MARK "X" 3. EFFLUENT 4. UNITS S. INTAKE (ophbnal) a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (tl available) P. LONG TERM AVRG. VALUE (il available; 4 N a. LONG TERM AVERAGE VALUE (1) CONCENTRATION (2)MASS b. No. OF ANALYSES a TESTING I b BELIEVED REQUIRED PRESENT [.BELIEVED ABSENT (1)CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1)CONCFN I L/TON (2)HASS GCfMS FRACTION—B 43BN-NItrosodIphenylamIne (86-30-6) RALWMPOUNDIR X , NA NA NA NA Nfr NA NA NA 44B. Phenanthrene (85-01-8) X NA NA NA NA NA NA NA NA 45B. Pyrene (129-00-0) X NA NA NA NA NA NA NA NA 46B. 1,2,4Trihlorobenzene (120-82-1) X NA NA NA NA NA NA NA NA GC/MS FRACTION —PESTICIDES 1P. Aldrin (309-00-2) X NA NA NA NA NA NA NA NA 2P. a-BHC (319-84-6) X NA NA NA NA NA NA NA NA 3P. 3-1311C (319-85-7) X NA NA NA NA NA NA NA NA - 4P. y-BHC (58-89-9) X NA NA NA NA NA NA NA NA 5P. 6-13HC (319-86-8) X NA NA NA NA NA NA NA NA 6P. Chlordane (57-74-9) X NA NA NA NA NA NA NA NA, 7P. 4,4' DDT (50-29-3) X NA NA NA NA NA NA NA NA 8P. 4.4' DDE (72-55-9) X NA NA NA NA NA NA NA NA 9P. 4,4' DDD (72-54-8) X NA NA NA NA NA NA NA NA 10P. Diedrin (60-57-1) X NA NA NA NA NA NA NA NA 11 P. u-Endosulfan (115-29-7) X NA NA NA NA NA NA NA NA 12P. j3-Endosulfan (115-29-7) X NA NA NA NA NA NA NA NA 13P. Endosulfan Sulfate (1031-07-8) X NA NA NA NA NA NA NA NA 14P. Endrin (72-20-8) X NA NA NA NA NA NA NA NA 15P. Endrin Aldehyde (7421-93-4) X NA NA NA NA NA NA NA NA 16P. Heptachlor (76-44-8) X NA NA NA NA NA NA NA NA tNA corm 351U-zc (8-9U) PAGE V-8 CONTINUED ON PAGE V-9 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-8 I NC0003573 1 001 Form Approved OMB No, 2040 0086 Gnnr—1 c c A_11_OA 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" b. MAXIMUM 30 DAY VALUE (if c. LONG TERM AVRG. VALUE (if a. MAXIMUM DAILY VALUE available) available) a. LONG TERM AVERAGE VALUE (Ifavailable) (7) CONCENTRATION (2) MASS b. NO. OF ANALYSES EL� VED NT c.BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (t) CONCENTRATIO71111ASS d. NO OF ANALYSES (1) CONCENTRATION (2) MASS GC/MS FRACTION -PESTICIDES (Continued) 17P. Heptachlor Epoxide (1024-57-3) X NA NA NA NA NA NA NA 18P. PCB-1242 (53469-21-9) X NA NA NA NA * NA NA NA 19P. PCB-1254 (11097-69-1) X NA NA NA NA * NA NA NA 20P. PCB-1221 (11104-28-2) X NA NA NA NA NA NA NA 21 P. PCB-1232 (1114-16-5) X NA NA NA NA * * * NA NA NA 22P. PCB-1248 ' (12672-29-6) X NA NA NA NA * NA NA NA 23P. PCB-1260 (11096-82-5) X NA NA NA NA NA NA NA 24P. PCB-1016 (12674-11-2) X NA NA NA NA NA NA NA 25P.Toxaphene (8001-35-2) X NA NA NA NA NA NA NA rrH rorm saiu-zc (ts-au) PAGE V-9 E.P. A. I . Number (copy from Item 1 of Form 1) PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all NC0003573 Form Approved of this information on separate sheets {use the same format) instead of completing these pages. OMB No, 2040 0086 SEE INSTRUCTIONS Annrnval arnirnc A-`1-OA V. INTAKE & EFFLUENT CHARACTERISTICS (Continued from page 3 of Form 2-C) 11 OUTFALL NO. PART A -You must provide the results of at least one analysis for every pollutant In this table. -Complete one table for each outfall. See Instructions tor additional etas s. 002 2. EFFLUENT 3. UNITS 4. INTAKE (optional) 1. POLLUTANT AND CAS NO a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (i/available) b. LONG TERM AVRG. VALUE (ifavailable) d. NO. OF (Specify i/blank) a. LONGTERM AVERAGE VALUE (1) ANALYSES (1)RATION b. NO OF (flavailable) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS aCONCENTRATION b. MASS CONCENT(2)MASS ANALYSES a. Biochemical Oxygen Demand 212.0 9775.7 106.00 4887.90 26.50 1222.00 5 MG/L PPD NA NA NA (BOD) b. Chemical Oxygen Demand 102.0 11291.9 102.0 11291.9 57.8 4853.2 4 MG/L PPD NA NA NA (COD) c. Total Organic Carbon (TOC) NA NA NA NA MG/L PPD NA NA NA d. Total Suspended Solids (TSS) NA NA NA NA MG/L PPD NA NA NA e. Ammonia (as N) ' NA NA NA NA ' MG/L PPD NA NA NA f. Flow value 18.60 value 16.3 value 10.6 396 MGD value NA NA g. Temperature value value value value 22.0 16.7 14.9 128 °C (winter) NA NA h. Temperature value value value value surnrner ( ) 39.0 32.2 25.8 146 °C NA NA Minimum Maximum Minimum Maximum i. pH 6.2 8.6 NA NA 274 STANDARD UNITS PART B -Mark "X" in column 2a for each pollutant you know or have reason to believe is present. Mark "X" in column 2b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (ifavailable) b. NO. OF e. MAXIMUM DAILY VALUE a. LONG TERM AVERAGE VALUE ANALYSES a. BELIEVED PRESENT b. BELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS D NO. OF ANALYSES CONCENTRATION (2) MASS 1. POLLUTANT & CAS NO. (ifavailable) CONCENTRATION (2) MASS a. Bromide X NA NA NA NA ' (24959-67-9) NA NA NA b. Chlorine X NA NA NA NA Total Residual NA NA NA c. Color X NA NA NA NA NA NA NA d. Fecal X NA NA NA NA ' Coliform NA NA NA e. Fluoride X NA NA NA NA ( 16984-48-8) I I I NA I NA NA f. Nitrate— X NA NA NA NA Nitrite (as N) NA NA NA EPA Form 3510-2C (8-90) PAGE V-1 ITEM V-B CONTINUED FROM PREVIOUS PAGE 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" b. MAXIMUM 30 DAY VALUE (d c. LONG TERM AVRG. VALUE (if a. MAXIMUM DAILY VALUE available) available) a. LONG TERM AVERAGE VALUE (Ifavailable) (1) CONCENTRATION (2)MASS (1 CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS U.NO OF ANALYSES (7) CONCENTRATION (2) MASS b. NO. OF ANALYSES a. BELIEVED PRESENT b.BELIEVEO ABSENT (1) CONCENTRATION (2) MASS g. Nitrogen, X NA NA NA NA NA NA NA Total Organic (as N) h. Oil and Grease X NA NA NA NA NA NA NA i. Phosphorus NA NA NA (as P) , Total X 1.3 152.3 1.3 152.3 0.35 36.1 12 MG/i PPD NA NA NA (7723-14-0) NA NA NA J. Radioactivity (1) Alpha, Total X NA NA NA NA NA NA NA (2) Beta, Total X NA NA NA NA NA NA NA (3) Radium, total X NA NA NA NA * NA NA NA (4) Radium 226 Total X NA NA NA NA NA NA NA k. Sulfate (as SO4) (14808-79-8) X NA NA NA NA NA NA NA I. Sulfide (as S) X * NA NA NA NA NA NA NA m. Sulfite (as S03) (14265-45-3 X * NA NA NA NA NA NA NA n. Surfactants X NA NA NA NA NA NA NA o. Aluminum, Total (7429-90-5) X NA NA NA NA NA NA NA p. Barium, Total (7440-39-3) X NA NA NA NA NA NA NA q. Boron, Total (7440-42-8) X NA NA NA NA NA NA NA r. Cobalt, Total (7440-48-4 ) X NA NA NA NA NA NA NA s. Iron, Total (7439-89-6) X NA NA NA NA NA NA NA t. Magnesium (7439-95-4) X NA NA I NA NA NA NA NA u. Molybdenum, Total (7439-98-7) X NA NA NA NA NA NA NA v. Manganese, (7439-96-5) X NA NA NA NA NA NA NA w. Tin Total X NA NA NA NA NA NA NA (7440-31-5) x. Titanium,Total (7440-32-6) X NA NA NA NA NA NA NA EPA Form 3510-2C (8-90) PAGE V-2 CONTINUED ON PAGE V-3 EPA I.D. NUMBER (copy from Hem 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE 3 OF FORM 2-C NC0003573 1 002 Form Approved OMB No. 2040 0086 Annrn„?I n. .'ec 8_11 QA PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GCIMS fractions you must test for. Mark "X" in column 2 a for all such GCIMS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2a (secondary industries, nonprocess wastewater outfalls, and nonrequired GCIMS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile 2,4 dinitrophenol, or 2-methyl-4,6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part, please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK' X" b. MAXIMUM 30 DAY VALUE (J c. LONG TERM AVRG. VALUE (il a. MAXIMUM DAILY VALUE available) available) a. LONG TERM AVERAGE VALUE (lfavailable) a. TESTING b. BELIEVED c.BELIEVED (�) b. NO, OF O (�) b. NO, OF REQUIRED PRESENT ABSENT (1) CONCENTRATION (2) MASS CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony Total (7440-36-0) X NA NA NA NA NA NA NA 2M. Arsenic, Total (7440-38-2) X NA NA NA NA NA NA NA 3M. Beryllium, Total (7440-41-7) X NA NA NA NA NA I NA NA a mlum, total (7440-43-9) X NA NA NA NA NA NA NA Chromium, o a (7440-47-3) X NA NA NA NA NA NA NA 6M. Copper, Total (7440-50-8) X NA NA NA NA NA NA NA 7M. Lead, Total (7439-92-1) X NA NA NA NA NA NA NA 8M. Mercury, Total (7439-97-6) X NA NA NA NA NA NA NA 9M. Nickel, Total (7440-02-0) X NA NA NA NA NA NA NA 10M. Selenium, Total (7782-49-2) X NA NA NA NA NA NA NA 11 M. Silver Total (7440-22-4) X NA NA NA NA NA NA NA 12M. Thallium Total (7440-28-0) X NA NA NA NA NA NA NA 13M. Zinc, Total (7440-66-6) X NA NA NA NA NA NA NA 14M. Cyanide, Total (57-12-5) X NA NA NA NA NA NA NA 15M. Phenols, Total X NA NA NA NA NA NA NA It etrachloridibenzo PNA t78 64-01-6) X NA NA NA EPA Form 3510-2C (8-90) PAGE V-3 CONTINUED ON PAGE V-4 ITEM V-13 CONTINUED FROM PREVIOUS PAGE 1. POLLUTANT AND CASE NO 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. MAXIMUM DAILY b. MAXIMUM 10 DAY VALUE (,f c. LONG TERM AVRG. VALUE (i/ VALUE available) a vailablc) a. LONG TERM AVERAGE VALUE (/(available) d. NO OF ANALYSES (1) CONCENTRATION III MA b NO OF ANALYSES a. TESTING REQUIRED I b. BELIEVED PRESENT c.BELIEVED ABSENT (1) CONCENTRATION (21 MA- (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS C/MS FRACTNEEMENEF COMPOUNDS 1 V. Acrolein (107-02-8) X NA NA NA NA NA NA NA NA 2V. Acrylonitrile (107-13-1) X NA NA NA NA NA NA NA NA 3V. Benzene (71-43-2) X NA NA NA NA NA NA NA NA 4V. Bis (Chloromethyl) Ether (542-88-1) X NA NA NA NA I NA NA NA NA 5V. Bromoform ( 75-25-2) X NA NA NA NA NA NA NA NA 6V. Carbon Tetrachloride (56-23-5) X NA NA NA NA NA NA NA NA 7V. Chlorobenzene (108-90-7) x NA NA NA NA NA NA NA NA 8V. Chlorodibromomethane (124-48-1) X NA NA NA NA NA NA NA NA 9V. Chloroethane (75-00-3) X NA NA NA NA NA NA NA NA 1OV. 2 Chlorohylvinyl Ether (110-75-8) X NA NA NA NA NA NA NA NA 11V. Chloroform (67-66-3) X NA NA NA NA NA NA NA NA 12V. Dichlorobromomethane (75-27-4) X NA NA NA NA NA NA NA I NA 13V. Dichlorodifluoromethane (75-71- 8) X NA NA NA NA NA NA NA NA 14V. 1,1 Dichloroethane (75-34-3) X NA NA NA NA NA NA NA NA 15V. 1,2 Dichloroethane (107-06-2) X NA NA NA NA NA NA NA NA 16V. 1,1 Dichloroethylene (75-35-4) X NA NA NA NA NA NA NA NA 17V.1,2 Dichloropropane (78-87-5) X NA NA NA NA NA NA NA NA 18V. 1,3 Dichloropropylene (542-75-6) X NA NA NA NA NA NA NA NA 19V. Ethylbenzene(100-41-4) X NA NA NA NA NA NA NA NA 20V. Methyl Bromide (74-83-9) X NA NA NA NA NA NA NA NA 21V. Methyl Chloride (74-87-3) X NA NA NA NA NA NA NA NA tVA t-orm stiu-zL; is -au) PAGE V4 CONTINUED ON PAGE V-5 —1 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-4 I NC0003573 1 002 Form Approved OMB No. 2040 0086 e....—,— 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" a. MAXIMUM DAILY b. MAXIMUM 70 DAY VALUE c. LONG TERM AVRG. VALUE (iI VALUE available) available) a. LONG TERM AVERAGE VALUE a. TESTING b. BELIEVED c.BELIEVED (1) (1)TION 11 (/available ( ) I NO OF ANALYSES (1) 1 NO. OF REQUIRED PRESENT ABSENT (1) CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRA (2) MASS CONCENTRATION (2) MASS CONCENTRATION (2J MASS ANALYSES GC/MS FRACTION —VOLATILE COMPOUNDS (continued) 22V Methylene Chloride (75-09-2) X NA NA NA NA NA NA NA NA 23V.1,1,2,2 Tetrachloro- ethane (79-34-5) X NA NA NA NA NA NA NA NA 24V. Tetrachloroethylene (127-18-4) X NA NA NA NA NA NA NA NA 25V. Toluene (108-88-3) X NA NA NA NA NA NA NA NA 26V. 1,2-Tra nsDichloro- ethylene (156-60-5) X NA NA NA NA NA NA NA NA 27V. 1,1,1 Trichloroethane (71-55-6) X NA NA NA NA NA NA NA NA 28V. 1,1,2 Trichloroethane (79-00-5) X NA NA NA NA NA NA NA NA 29V. Trichloroethylene (79-01-6) X NA NA NA NA NA NA NA NA 30V. Trichlorofluoro- methane (75-69-4) X NA NA NA NA NA NA NA NA 31V. Vinyl Chloride (75-01-4) X NA NA NA NA NA NA NA NA GC/MS FRACTION —ACID COMPOUNDS 1A. 2 Chlorophenol (95-57-8) X NA NA NA NA NA NA NA NA 2A 2,4 Dichlorohenol (120-83-2) X NA NA NA NA NA NA NA NA 3A. 2,4 Dimethylphenol (105-67-9) X NA NA NA NA NA NA NA NA 4A 4,6 Dinitro-O-Cresol (534-52-1) X NA NA NA NA NA NA NA NA 5A. 2,4 Dinitrohenol (51-28-5) X NA NA NA NA NA NA NA NA 6A.2-Nitrophenol(88-75-5) X NA NA NA NA NA NA NA NA 7A4-Nitrophenol(100-02-7) X NA NA NA NA NA NA NA NA 8A. P-Chloro-M-Cresol 59-50-7 X NA NA NA NA NA NA NA NA 9A. Pentachlorophenol (87-86-5) X NA NA NA NA NA NA NA NA 10A. Phenol (108-95-2) X NA NA NA NA NA NA NA NA 11A. 2,4,6 Trichloro- phenol (88-06-2) X NA NA NA NA NA NA NA NA EPA Form 3510-2C (8-90) PAGE V-5 CONTINUED ON PAGE V-6 CONTINUED FROM PAGE V-6 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" a. MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE (,l c. LONG TERM AVRG. VALUE (,f VALUE available) available) a. LONGTERM AVERAGE VALUE a TESTING REQUIRED b BELIEVED PRESENT c BELIEVED ABSENT (i)CONCENTRATION 12)MAS$ (1)CONCENTRATION (2)MASS (1)CONCENTRATKNJ (2)MASS (1)CONCENTRATION (2)MASS (Ifavailable) d NO. OF ANALYSES (1)CONCENTRATION (2)MASS b NO OF aNALYSES GC/MS FRACTION—BASE/NE S 1 B Acenaphthene (83-32-9) X NA NA NA NA NA NA NA NA 2B. Acenaphtylene (208-96-8) X NA NA NA NA NA NA NA NA 3B. Anthracene (120-12-7) X NA NA NA NA NA NA NA NA 4B. Benzidine (92-87-5) X NA NA NA NA NA NA NA NA 5B. Benzo (a) Anthracene (56-55-3) X NA NA NA NA NA NA NA NA 6B. Benzo (a) Pyrene (50-32-8) X NA NA NA NA NA NA NA NA 7B3,4 BenzoFluororanthene (205-99-2) X NA NA NA NA NA NA NA NA - 8B. Benzo(ghi)Peryiene (191-24-2) X NA NA NA NA NA NA NA NA 9B. Benxo (k) Fluoranthene (207-08-9) X NA NA NA NA NA NA NA NA 10B. Bis(2-Chloroethoxy) Methane (111-91-1) X NA NA NA NA NA NA NA NA 11 B. Bis(2-Chloroethyl) Ether (111-44-4) X NA NA NA NA NA NA NA NA 12B Bis(2Chlorolsopropyl) Ether (102-60- 1 ) X NA NA NA NA NA NA NA NA 13B. Bis(2-Elthylhexyl) Phthalate (117-81-7) X NA NA NA NA NA NA NA NA 14BABromophenylPhenyl Ether (101-55-3) X NA NA NA NA NA NA NA NA 158. Butyl Benzyl Phthalate (85-68-7) X NA NA NA NA NA NA NA NA 16B. 2-Chloronapthalene (91-58-7) X NA NA NA NA NA NA NA NA 17B.2-Chlorophenyl Phenyl Ether (7005-72-3) X NA NA NA NA NA NA NA NA 18B.Chrysene(218-01-9) X NA NA NA NA NA NA NA NA 19B. Dibenzo (a,h) Anthracene (53-70-3) X NA NA NA NA NA NA NA NA 20B. 1,2 Dichlorobenzene (95-50-1) X NA NA NA NA NA NA NA NA 21B. 1,3 Dichlorobenzene (541-73-1) X NA NA NA NA NA NA NA NA crA Form 35lu-2C (6-au) PAGE V-6 CONTINUED ON PAGE V-7 JUN -6 07 DEQ-CFW-00076695 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-6 NC0003573 nn, Form Approved OMB No, 2040 0086 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK -X- a. MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE c. LONGTERM AVRG. VALUE (rr VALUE available) available) a. LONG TERM AVERAGE VALUE a TESTING REQUIRED b. BELIEVED PRESENT c BELIE`✓EU .. (1,CONCENTRATION ll7t.I4SS (1)C1jNCEJTR—nN (2)Mv 6S, I )CONCENTRATION (2)MASS 1) CONCE NTRATION (2)MASS (Ifavailable) b NO OF ANALYSES (1) CONCENTRATION (2)MASS b NO OF ANALYSES GC/MS FRACTION—BASE/NEUTRAL POUNDS (Continued) - - 22B. 1 A Dichlorobenzene (106-46-7) X NA NA NA NA NA NA NA NA 23B.3,3' Dichlorobenzidine (91-94-1) X NA NA NA NA NA NA NA NA 24B. Diethyl Phthalate (84-66-2) X NA NA NA NA NA NA NA NA 25B. Dimethyl Phthalate (131-11-3) X NA NA NA NA NA NA NA NA 26B. Di-N-Butyl- Phthalate (84-74-2) X NA NA NA NA NA NA NA NA 27B. 2A Dinitro toluene (121-14-2) X NA NA NA NA NA NA NA NA 28B. 2,6 Dinitrotoluene (606-20-2) X NA NA NA NA NA NA NA NA 29B. Di-N-Octyl Phthalate (117-84-0) X NA NA NA NA NA NA NA NA 30B. 1 2 Diphenylhydrazine (as Azobenzene) (122-66-7) X NA NA NA NA NA NA NA NA 31 B. Fluoranthene (206-44-0) X NA NA NA NA NA NA NA NA 32B. Fluorene (86-73-7) X NA NA NA NA NA NA NA NA 33B. Hexachlorobenzene (118-74-1) X NA NA NA NA NA NA NA NA 34B. Hexachlorobutadiene (87-68-3) X NA NA NA NA NA NA NA NA 35B. Hexachlorocyclo- pentadiene (77-47-4) X NA NA NA NA NA NA NA NA 36B. Hexachloroethane (67-72-1) X NA NA NA NA NA NA NA NA 37B.Indeno1,2,3 cdPyrene (193-39-5) X NA NA NA NA NA NA NA NA 3813. Isophorone (78-59-1) X NA NA NA NA NA NA NA NA 39B. Naphthalene (91-20-3) X NA NA NA NA NA NA NA NA 40B.Nitrobenzene (98-95-3) X NA NA NA NA NA NA NA NA 41 B. N-Nitrosodime- thylamine (62-75-9) X NA NA NA NA NA NA NA NA 42B. N-Nitrosodi-N- Propylamine (621-64-7) X NA NA NA NA NA NA NA NA t-FAForm3510-ZC (B-90) PAGE V-7 CONTINUED ON PAGE V-8 CONTINUED FROM PAGE V-7 1. POLLUTANT AND CASE NO (if available) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (opfonal) a- MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (d avalable) c. LONG TERM AVRG. VALUE (J—dable) d, NO. OF ANALYSE$ a. LONG TERM AVERAGE VALUE (1)CONCENTRATION (2)MASS b. NO. OF ANALYSES a TESTING REOUIREO b. BELIEVED PRESENT c BELIEVED ABSEIJT .rN,.EI ual ,` 7: 1.1„ti� (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MAS$ (1) CONCENTRATION (2)MA$S GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS 43BN-Nitrosodiphenylamine (86-30-6) X (Continued) NA NA NA NA NA NA NA 44B. Phenanthrene (85-01-8) X NA NA NA NA NA NA NA NA 45B. Pyrene (129-00-0) X NA NA NA NA NA NA NA NA 46B. 1,2,4Trihlorobenzene (120-82-1) X NA I NA NA NA NA NA NA NA 0AS FRACTION —PESTICIDES 1P. Aldrin (309-00-2) X NA NA NA NA NA NA NA NA 2P. u-BHC (319-84-6) X NA NA NA NA NA NA NA NA 3P. (1-BHC (319-85-7) X NA NA NA NA NA NA NA NA 4P. y-BHC (58-89-9) X NA NA NA NA NA NA NA _ NA 5P. 6-13HC (319-86-8) X NA NA NA NA NA NA NA NA 6P. Chlordane (57-74-9) X NA NA NA NA NA NA NA NAB 7P. 4,4' DDT (50-29-3) X * NA NA NA NA NA NA NA NA 8P. 4.4' DDE (72-55-9) X NA NA NA NA NA NA NA NA 9P. 4,4' DDD (72-54-8) X NA NA NA NA NA NA NA NA 1 OP. Diedrin (60-57-1) X NA NA NA NA NA NA NA NA 11 P. u-Endosulfan (115-29-7) X NA NA NA NA NA NA NA NA 12P. (3-Endosulfan (115-29-7) X NA NA NA NA NA NA NA NA 13P. Endosulfan Sulfate (1031-07-8) X NA NA NA NA NA NA NA NA 14P. Endrin (72-20-8) X NA NA NA NA NA NA NA NA 15P. Endrin Aldehyde (7421-93-4) X NA NA NA NA NA NA NA NA 16P. Heptachlor (76-44-8) X NA NA NA NA NA NA NA NA EPA Form 3510-2C (8-90) PAGE V-8 CONTINUED ON PAGE V-9 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-8 I NC0003573 1 002 Form Approved OMB No. 2040 0086 Ate.,... l o A_11 oa 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" b. MAXIMUM 30 DAY VALUE (if c. LONG TERM AVRG. VALUE (if a. MAXIMUM DAILY VALUE available) available) a. LONG TERM AVERAGE VALUE (Ifavailable) (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS d NO. OF ANALYSES (1) CONCENTRATION (2) MASS b NO OF ANALYSES a. TESTING REQUIRED b. BELIEVED PRESENT c.BEUE1E1 ABSENT (1) CONCENTRATION 12) MASS GC/MS FRACTION —PESTICIDES (Continued) 17P. Heptachlor Epoxide (1024-57-3) X NA NA NA NA NA NA NA 18P. PCB-1242 (53469-21-9) X NA NA NA NA NA NA NA 19P. PCB-1254 (11097-69-1) X NA NA NA NA NA NA NA 20P. PCB-1221 (11104-28-2) X NA NA NA NA * NA NA NA - 21 P. PCB-1232 (1114-16-5) X NA NA NA NA * NA NA NA 22P. PCB-1248 (12672-29-6) X NA NA NA NA NA NA NA 23P. PCB-1260 (11096-82-5) X NA NA NA NA NA NA NA 24P. PCB-1016 (12674-11-2) X NA NA NA NA * NA NA NA 25P.Toxaphene (8001-35-2) X NA NA NA NA NA FNAT A rrN rorm 3D IU-ZL, to-uu) PAGE V-9 E P. A I . Number (copy from Item 1 of Form 1) PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all NC0003573 Form Approved of this information on separate sheets fuse the same format) instead of completing these pages. OMB No. 2040 0086 SEE INSTRUCTIONS Annmval e><nirec A-31-PA V. INTAKE & EFFLUENT CHARACTERISTICS (Continued from page 3 of Form 2-C) OUTFALL NO. PART A -You must provide the results of at least one analysis for every pollutant in—t-F—istable. Complete one table for each o—uTall. See Instructions foradditional details. 006 2. EFFLUENT 3. UNITS 4. INTAKE (oplional) 1. POLLUTANT AND CAS NO a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) b. LONG TERM AVRG. VALUE (i/ available) d. NO. OF (Specify it blank) a. LONGTERM AVERAGE VALUE ANALYSES b.NO.OF (if available) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS a CONCENTRATION b. MASS CONCENTRATION (2)MASS ANALYSES a. Biochemical Oxygen Demand N/A N/A NA NA NA NA N!A MG/L PPD NA NA NA (BOD) b. Chemical Oxygen Demand N/A N/A NA NA NA NA N/A MG/L PPD NA NA NA (COD) c. Total Organic Carbon (TOC) N/A N/A NA NA NA NA N/A MG/L PPD NA NA NA d. Total Suspended Solids (TSS) NA NA NA NA N/A MG/L PPD NA NA NA e. Ammonia (as N) N/A N/A NA NA NA NA N/A MG/L PPD NA NA NA f. Flow value N/A value NA NA value NA N/A MGD value NA NA g. Temperature value N/A value NA NA value NA N/A value winter oC NA NA h. Temperature value value value value (summer) N/A NA NA NA N/A °C NA NA Minimum Maximum Minimum Maximum i i. pH N/A N/A NA NA N/A STANDARD UNITS PART B -Mark "X" in column 2a for each pollutant you know or have reason to believe is present. Mark "X" in column 2b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE (if available) b. NO. OF a. MAXIMUM DAILY VALUE a. LONG TERM AVERAGE VALUE ANALYSES a BELIEVED b. BELIEVED (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS D. NO. OF ANALYSES (1) CONCENTRATION (2)MASS 1. POLLUTANT & CAS NO. (ifavailable) t1) (2)MASS PRESENT ABSENT CONCENTRATION a. Bromide X N/A N/A NA NA NA NA N/A N/A N/A (24959-67-9) NA NA NA b. Chlorine X N/A N/A NA NA NA NA N/A N/A N/A Total Residual INA NA NA C. Color X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA d. Fecal X N/A N/A NA NA NA NA N/A N/A N/A Coliform NA NA NA e. Fluoride X N/A N/A NA NA NA NA N/A N/A N/A ( 16984-48-8 ) NA NA NA f. Nitrate— X N/A N/A NA NA NA NA N/A N/A N/A Nitrite (as N) NA NA NA EPA Form 3510-2C (8-90) PAGE V-1 ITEM V-B CONTINUED FROM PREVIOUS PAGE 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK 'W' b. MAXIMUM 30 DAY VALUE ff c. LONG TERM AVRG. VALUE (if a. MAXIMUM DAILY VALUE available) avaJablci a. LONG TERM AVERAGE VALUE (1(available) (1)CONCENTRATION (2)MASS b. NO OF ANALYSES a. BELIEVED PRESENT b.BELIEVED ABSENT (1) CONCENTRATION (2)MASS (I I CONCENTRATION (2)MASS (i) CONCENTRATION (2)MASS b NO. OF ANALYSES (1)CONCENTRATION (2)MASS g. Nitrogen, Total Organic (as N) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA h. Oil and Grease X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA i. Phosphorus NA NA NA (as P), Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (7723-14-0) NA NA NA J. Radioactivity (1) Alpha, Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (2) Beta, Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (3) Radium, total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (4) Radium 226 Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA k. Sulfate (as SO4) (14808-79-8) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA I. Sulfide (as S) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA m. Sulfite (as S03) (14265-45-3 X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA n. Surfactants X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA o. Aluminum, Total (7429-90-5) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA p. Barium, Total (7440-39-3) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA q. Boron, Total (7440-42-8) X N/A N/A NA NA NA NA N/A NA NA NA N/A N/A r. Cobalt, Total Cobalt, (7440- X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA s. Iron, Total (7439-89-6) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA It. Magnesium (7439-95-4) X N/A N/A NA NA NA NA NIA N/A N/A NA NA NA u. Molybdenum, Total (7439-98-7) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA v. Manganese, (7439-96-5) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA w. Tin Total X N/A N/A NA NA NA NA N/A NA NA NA (7440-31-5) N/A N/A x. Titanium,Total (7440-32-6) X N/A N/A NA NA NA NA N/A N/A N/A NA NA ANA EPA Form 3510-2C (8-90) PAGE V-2 CONTINUED ON PAGE V-3 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE 3 OF FORM 2-C NC0003573 1 006 Form Approved OMB No. 2040 0086 Annrn—I .-- A_11 OA PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2 a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2c for each pollutant you believe is absent. if you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acroiein, acrylonitrile 2,4 dinitrophenol, or 2-methyl-4,6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part, please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional details and requirements. 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" b. MAXIMUM 30 DAY VALUE c. LONG TERM AVRG. VALUE ` a. MAXIMUM DAILY VALUE available) availab;c'� a. LONG TERM AVERAGE VALUE a. TESTING b BELIEVED c. BELIEVED (11 (Ifavailable) IT) d NO. OF (1) b NO. OF REQUIRED PRESENT ABSENT (1) CONCENTRATION (2)MASS CONCENTRATION (21 MASS 111 CONCENTRATIO (2) MASS ANALYSES CONCENTRATION (2) MASS CONCENTRATION (2) MASS ANALYSES METALS, CYANIDE, AND TOTAL PHENOLS 1 M. Antimony Total (7440-36-0) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 2M. Arsenic, Total (7440-38-2) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 3M. Beryllium, Total (7440-41-7) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA a mium, 1 otal (7440-43-9) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA Chromium, Total (7440-47-3) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 6M. Copper, Total (7440-50-8) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 7M. Lead, Total (7439-92-1) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 8M. Mercury, Total (7439-97-6) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 9M. Nickel, Total (7440-02-0) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 10M. Selenium, Total (7782-49-2) X N/A N/A NA NA I NA NA N/A N/A N/A NA NA NA 11 M. Silver Total (7440-22-4) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 12M. Thallium Total (7440-28-0) X N/A N/A NA NA NA NA N/A N/A IN/A NA NA NA 13M. Zinc, Total (7440-66-6) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 14M. Cyanide, Total (57-12-5) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 15M. Phenols, Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA DIOXIN 2,3,7,8-Tetrachloridibenzo-P Dioxin (1764-01-6) X N/A NA NA NA EPA Form 3510-2C (8-90) PAGE V-3 CONTINUED ON PAGE V4 ITEM V-B CONTINUED FROM PREVIOUS PAGE 3. EFFLUENT 4. UNITS S. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK „ ' a. MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE pf c. LONG TERM AVRG. VALUE pf VALUE available) available) LONG TERM AVERAGE VALUE r (Ifavailable) d. NO. OF ANALYSES (1) (2)MASS b NO OF ANALYSES a. TESTING REQUIRED b. BELIEVED PRESENT C.BELIEVED ABSENT (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASSNCENTRATION GICIMS FRACTION —VOLATILE COMPOUNDS 1V. Acrolein (107-02-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 2V. Acrylonitrile (107-13-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 3V. Benzene (71-43-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 4V. Bis (Chloromethyl) Ether (542-88-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 5V. Bromoform ( 75-25-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 6V. Carbon Tetrachloride (56-23-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 7V. Chlorobenzene (108-90-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 8V. Chlorodibromomethane (124-48-1) X N/A N/A NA NA NA NA N/A N/A NA NA NA 9V. Chloroethane (75-00-3) X N/A N/A NA NA NA NA N/A N/A NA NA NA 1OV. 2 Chlorohylvinyl INA Ether (110-75-8) X N/A N/A NA NA NA NA N/A N/A NA NA NA 11V. Chloroform (67-66-3) X N/A N/A NA NA NA NA N/A N/A NA NA NA 12V. Dichlorobromomethane (75-27-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 13V. Dichlorodifluoromethane (75-71- 8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 14V. 1,1 Dichloroethane (75-34-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 15V. 1,2 Dichloroethane (107-06-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 16V. 1,1 Dichloroethylene (75-35-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 17V. 1,2 Dichloropropane (78-87-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 18V. 1,3 Dichloropropylene (542-75-6) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 19V. Ethylbenzene(100-41-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 20V. Methyl Bromide (74-83-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 21V. Methyl Chloride (74-87-3) X N/A N/A NA NA NA NA NA N/A NIA NA NA NA LPA Form 3510-2C 8-90) PAGE V-4 CONTINUED ON PAGE V-5 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-4 I NC0003573 1 006 Form Approved OMB No. 2040 0086 Annrn—.-- R_i1 .R 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" a. MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE ff LONG TERM AVRG. VALUE (,f VALUE available) available) a. LONG TERM AVERAGE VALUE a. TESTING b. BELIEVED C BELIEVED (�) (1) (I/d✓d%Idble) d. NO. OF ANALYSES (�) b. NO. OF ANALYSES REQUIRED PRESENT ABSENT 17)CONCENTRATION (2)MASS CONCENTRATION (2) MASS CONCENTRATION (2) MASS CONCENTRATION 12) MASS CONCENTRATION (2) MASS GC/MS FRACTION —VOLATILE COMPOUNDS (continued) 22V Methylene Chloride (75-09-2) X N/A N/A NA NA NA NA NA N/A NIA NA NA NA 23V.1,1,2,2 Tetrachloro- ethane (79-34-5) X N/A NIA NA NA NA NA NA N/A NA NA NA NA 24V. Tetra chloroethylene (127-18-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 25V. Toluene (108-88-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 26V. 1,2-TransDichloro- ethylene (156-60-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 27V. 1,1,1 Trichloroethane (71-55-6) X N/A N/A NA NA NA NA NA N A N/A NA NA NA 28V. 1,1,2 Trichloroethane (79-00-5) X N/A N/A NA NA NA NA NA NIA N/A NA NA NA 29V. Trichloroethylene (79-01-6) X N/A N/A NA NA NA NA NA NIA N/A NA NA NA 30V. TrichloroFluoro- methane (75-69-4) X NIA N/A NA NA NA NA NA NIA NIA NA NA NA 31V. Vinyl Chloride (75-01-4) X NIA NIA NA NA NA NA NA N'A N/A NA NA NA GC/MS FRACTION —ACID COMPOUNDS 1A, 2 Chlorophenol (95-57-8) X N/A N/A NA NA NA NA NA NIA I �/A NA NA NA 2A 2,4 Dichlorohenol (120-83-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 3A. 2,4 Dimethylphenol (105-67-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 4A 4,6 Dinitro-O-Cresol (534-52-1) X N/A NIA NA NA NA NA NA N/A N/A NA NA NA 5A. 2,4 Dinitrohenol (51-28-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 6A.2-Nitrophenol(88-75-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 7A4-Nitrophenol(100-02-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 8A. P-Chloro-M-Cresol 59-50-7 X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 9A. Pentachlorophenol (87-86-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 10A. Phenol (108-95-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 11A. 2,4,6 Trichloro- —j phenol (88-06-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA EPA Form 3510-2C (8-90) PAGE V-5 CONTINUED ON PAGE V-6 CONTINUED FROM PAGE V-6 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK „X„ a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE ff vailable) t. LONG TERM AVRG. VALUE (d vailable) a. LONG TERM AVERAGE VALUE a. TESTING RECAJIRED b. BELIEVED PRESENT cBELIEVED ABSENT (1) CONCENTRATION (2)MASS (i) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1iCONCEf\TRATION (2)MASS (Ifavailable) d NO OF ANALYSES (1)CONCENTRATIOi�I ,"'1f.1AS5 b. NO. OF ANALYSES MPOUNDS 18. Acenaphthene (83-32-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 2B. Acenaphtylene (208-96-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 38. Anthracene (120-12-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 4B. Benzidine (92-87-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 5B. Benzo (a) Anthracene (56-55-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 6B. Benzo (a) Pyrene (50-32-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 7B3,4 Benzofluororanthene (205-99-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA - 8B. Benzo(ghi)Perylene (191-24-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 9B. Benxo (k) _ Fluoranthene (207-08-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 10B. Bis(2-Chloroethoxy) Methane (111-91-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 11 B. Bis(2-Chloroethyl) Ether (111-44-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 12B Bisf2Chlorolsopropyl) Ether(102-60-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 13B. Bis(2-Elthylhexyl) Phthalate (117-81-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 14B.413romophenylPhenyl Ether (101-55-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 15B. Butyl Benzyl Phthalate (85-68-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 166. 2-Chloronapthalene (91-58-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 17B.2-Chlorophenyl Phenyl Ether (7005-72-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 18B.Chrysene(218-01-9) X N/A N/A NA NA NA NA NA N/A N/A I NA NA NA 19B. Dibenzo (a,h) Anthracene (53-70-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 208. 1,2 Dichlorobenzene (95-50-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 21B. 1,3 Dichlorobenzene (541-73-1) X I N/A I N/A NA NA NA NA NA N/A N/A I NA NA NA EvA Form saiu-« (o-au) PAGE V-6 CONTINUED ON PAGE V-7 EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-6 I NC0003573 I nna Form Approved OMB No. 2040 0086 1. POLLUTANT AND CASE NO 2. MARK "X" 3. EFFLUENT 4. UNITS S. INTAKE (optional) a. MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE (i/ c. LONG TERM AVRG. VALUE IJ VALUE evadable) a 'vadaDlej e. LONG TERM AVERAGE VALUE a. TESTING REQUIRED b BELIEVED PRESENT c BELIEVED I ABSENT (1) CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1)CONCENTRA PION (2)MASS (lfavailable) a N'.r (1)GONGFNTRAI ION (2)MASS b NO OF ANA!. USES GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS (Continued) 22B. 1,4 Dichlorobenzene (106-46-7) X N/A N,A NA NA NA NA NA N/A N/A NA NA NA 23B.3,3' Dichlorobenzidine (91-94-1) X N/A WA NA NA NA NA NA N/A N/A NA NA NA 24B. Diethyl Phthalate (84-66-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 25B. Dimethyl Phthalate (131-11-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 26B. Di-N-Butyl- Phthalate (84-74-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 27B. 2,4 Dinitro toluene (121-14-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 28B. 2,6 Dinitrotoluene (606-20-2) X N/A N A NA NA NA NA NA N/A N/A NA NA NA 29B. Di-N-Octyl Phthalate (117-84-0) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 30B. 1 2 Diphenylhydrazine (as Azobenzene) (122-66-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 31B. Fluoranthene (206-44-0) X N/A N/A NA NA NA NA NA NIA NIA NA NA NA 32B. Fluorene (86-73-7) X N/A N/A NA NA NA NA NA NIA NIA NA NA NA 33B. Hexachlorobenzene (118-74-1) X N/A N'A NA NA NA NA NA N/A NIA NA NA NA 34B. Hexachlorobutadiene (87-68-3) X N/A N/A NA NA NA NA NA N/A NA NA NA NA 35B. Hexachlorocyclo- pentadiene (77-47-4) X N/A N/A NA NA NA NA NA N/A NIA NA NA NA 36B. Hexachloroethane (67-72-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 37B.Indeno1,2,3 cdPyrene (193-39-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 38B. Isophorone (78-59-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 39B. Naphthalene (91-20-3) X N/A N/A NA NA I NA NA NA N/A N/A NA NA NA 40B.Nitrobenzene (98-95-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 41B. N-Nitrosodime- thylamine (62-75-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 42B. N-Nitrosodi-N- Propylamine (621-64-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA trA rorm saTu-zt, to-uut PAGE V-7 CONTINUED ON PAGE V-8 CONTINUED FROM PAGE V-7 1. POLLUTANT AND CASE NO 'Ifavailable) 2. MARK "X" 3. EFFLUENT 4. UNITS 5. INTAKE (optional) a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if available) c. LONG TERM AVRG. VALUE rl—,)l ble) OF Av SES a. LONG TERM AVERAGE VALUE ..;! NTR/.TION (2)P1 -- "S a TESTING REQUIRED b. BELIEVED PRESENT c BELIEVED ABSENT (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2)MASS (1) CONCENTRATION (2) MASS C�,J�E^.ITR-T , INN _ ,,, GCIMS FRACTION—BAS 43BN-Nitrosodiphenylamine (86-30-6) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 44B. Phenanthrene (85-01-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 45B. Pyrene (129-00-0) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 46B. 1,2,4Trihlorobenzene (120-82-1) X N/A �r/A NA NA NA NA NA N/A N/A NA NA NA GC/MS FRACTION —PESTICIDES 1 P. Aldrin (309-00-2) X N/A N,A NA NA NA NA NA N/A N/A NA NA NA 2P. a-BHC (319-84-6) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 3P. (1-BHC (319-85-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 4P. y-BHC (58-89-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 5P. 6-BHC (319-86-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 6P. Chlordane (57-74-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA_ 7P. 4,4' DDT (50-29-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 8P. 4.4' DDE (72-55-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 9P. 4,4' DDD (72-54-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 10P. Diedrin (60-57-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 11 P. a-Endosulfan (115-29-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 12P. (3-Endosulfan (115-29-7) X N/A NiA NA NA NA NA NA N/A N/A NA NA NA 13P. Endosulfan Sulfate (1031-07-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 14P. Endrin (72-20-8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 15P. Endrin Aldehyde (7421-93-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 16P. Heptachlor (76-44-8) X WA N/A NA NA NA NA NA N/A N/A NA NA NA LFA corm 3biu-eL; (u-9U) PAGE V-8 CONTINUED ON PAGE V-9 w EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-8 NC0003573 1 006 Form Approved OMB No. 2040 0086 A c c 8_31 OC 3. EFFLUENT 4. UNITS 5. INTAKE (optional) 1. POLLUTANT AND CASE NO 2. MARK "X" b. MAXIMUM 30 DAY VALUE (if c. LONG TERM AVRG. VALUE (if a. MAXIMUM DAILY VALUE available) available) a. LONG TERM AVERAGE VALUE (If available) (1) CONCENTRATION (2) MASS (1) CONCENTRA T ION (2) MASS (1) CONCENTRATION (2) MASS d NO OF ANALYSES 11) CONCENTRATION (2) MASS b NO OF ANALYSES 1EE EVED ENT c. BELIEVED ABSENT (1) CONCENTRATION (2) MASS GC/MS FRACTION —PESTICIDES (Continued) 17P. Heptachlor Epoxide (1024-57-3) X N/A N/A NA NA NA NA I N/A N/A N/A NA NA NA 18P. PCB-1242 (53469-21-9) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 19P. PCB-1254 (11097-69-1) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 20P. PCB-1221 (11104-28-2) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA . 21 P. PCB-1232 (1114-16-5) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 22P. PCB-1248 (12672-29-6) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 23P. PCB-1260 (11096-82-5) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 24P. PCB-1016 (12674-11-2) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 25P.Toxaphene (8001-35-2) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA r-f-A rurrn as ru-zu to-uu) PAGE V-9 JUN - 6 07 ♦ s a` a DEQ-CFW 00076708