DEQ-CFW_00068563

kv
_ WA • -t .V",-4
r
NCDENR
North Carolina Department of Environment and Natural Resources
DIVISION OF AIR QUALITY
Michael F. Easley, Governor William G. Ross Jr., Secretary
B. Keith Overcash, P.E., Director
May 30, 2008
Mr. Nichael E. Johnson
Environmental Manager
E.I. du Pont de Nemours & Co., LLC
DBA, DuPont Company — Fayetteville Works
22828NC Highway 87 West
Fayetteville, NC 28306
SUBJECT: Regional Office Review of Stack Test Results Emission Source Temporary Boiler
Air Quality Permit No. 03735T32
DuPont Fayetteville Plant
Facility ID: 0900009, Duart Township, Bladen County
Facility Classification: Title V
Dear Mr. Johnson:
The Division has reviewed your stack test report that was received by the DAQ Fayetteville
Office on 9 May 2008. This report is for the Visible Emission Test, EPA Method 9, which was
conducted on 29 April 2008 to emission source PS -Temp. On 30 May 2008, this Division determined
that the subject testing performed at your facility was an acceptable stack test. The review indicates that
compliance with Air Permit No. 03735T32 is indicated for this source.
Should you have any questions regarding this matter, please contact Robert Kennedy,
Environmental Engineer at [phone], in the Fayetteville Regional Office.
Sincerely,
Steven F. Vozzo
Regional Air Quality Supervisor
cc: Shannon Vogel, RCO-Stationary Source Compliance (w/ RO Review Form)
I)AQ Central Files (w/RO Review Form)
FRO Files
Fayetteville Regional Office - Division of Air Quality
Systel Building, 225 Green Street, Suite 714, Fayetteville_ North Carolina 28301-5094
Phone: [phone] / FAX: [phone] / Internet: www.ncair.org
An Equal Opportunity / Affirmative Action Employer - 50% Recycled/10%Post Consumer
One
Natitrally
DEQ-CFW 00068563

�
DIVISION OF AIR QUALITY'"I
FAYETTEVILLE REGIONAL OFFICE�j ;'
' 225 Green Street, Suite 714
DENR Fayetteville, NC 28301-5043 DENR
METHOD 9 VISIBLE EMISSIONS TEST REPORT EVALUATION FORM
Facility Name: �6u LOPQ Ale TT4: CntyPrem : 09 00005
Source (ID#) to be tested : f 1 e-u%.P
Assigned to:
Date of VE test: 20
Was FRO notified of VE test?:—Y— (Y/N), if so DATE
Did a FRO staff member observer the test? 1J (Ymr), if so Staff Member: .+
Facility Process Rate during test: Opacity Readings:
During Tests Maximum Design Rating Avera a Hieh Reading
Run (1) 33r 0oo ; //{�Si�"?�( ® O O
Run (2) �J3,
Run (3)
**************VISIBLE EMISSIONS TEST REPORT EVALUATION**************
1) Does the VE test appear to be accurately performed according to the reference method? Comments?
(including a check of position of observer; use file maps when necessary - - double check observers comments)
Yes
2) Is the VE test report acceptable?
YES
3) List the name and VE certification of the person that performed the VE test.
e~6- � t4 y ra,� ' >-1 A 124s4 7
4) Was the facility in compliance as result of the VE test?
\/Es --�u P, �� �S/,S-J-08
DAQ FRO Compliance Person Date
C�hl,� � SCE-�_:�%.�� i;l;� :� i �\ �.�L'�I' c,•r- j��.4j .�2/}�- ,
G:\DATA\DAQ\COMPLI-I\STACKTSnVE-REV.FRM
DEQ-CFW 00068564

w
aU PONT@
Mr. Steven F. Vozzo
NCDENR — Division of Air Quality
Fayetteville Regional Office
225 Green Street — Suite 714
Fayetteville, NC 28301
SUBJECT: Temporary Boiler (ID No. PS -Temp)
Method 9 Performance Test Results
Air Quality Permit No. 03735T32
Facility ID: 0900009
Dear Mr. Vozzo:
DuPont Fluoroproducts
22828 NC Highway 87 W
Fayetteville, NC 28306-7332
May 6, 2008
As required by Part 2.1(G)(2)(g)(iii) of the subject permit, attached are the April 29, 2008
Method 9 performance test results of the stack emissions from the rental boiler (ID No.
PS -Temp) at the DuPont Company — Fayetteville Works.
If you have any questions regarding these test results, or if you need additional information,
please call me at 678-1155.
Attachments
Michael E. Johnson
Environmental Manager
ZooB - 13s'S t
E.I. du Pont de Nemours and Company
DEQ-CFW 00068565

n
Company Name
%r _ _/
City /
if 9ZLl ey: //c`
Process E ipment
Point
VISIBLE EMISSION OBSERVATION FORM
Z f`;a/V /
State Zip
/✓C• M30�
Operatin Mode
tr Lc:3 DNA /oo
,/.^_�,,� Operating Mode
Height of Emission Point
Height Relative to Observer
Start �j End -
Distance to Emission Point
/
Direction to Point
Start 36 End 30
�Epmission
Start A�dKX End /�1)dt -
VerticalAngrle to Observation Pt.
Start Cf.s End
Direction to Observation Point
Start $'�� End
Describe Emissions
Start ��C
End �o��
Emission Color
If Water Droplet Plume (Circle)
�>:Start C End
Attached Detached N/A
—
Point In The Plume At Which Opacity Was Determined
Start
Start
/
End /
Describe Plume Background
Start C E�/L /3//A�
Endo
Background Color
Sky Condition
Start ��ll.: End (AR_
Start CIfAdZ End ��
Wind Speed
Wind Direction
Start,5 '- (� :E.d •
Start End
Ambient Temp r G
Wet Bulb RH Percent
/ ^
Start (yQ End GFf/
Temp
SOURCE LAYOUT SKETCH
Eb1ISSION
OBSERVATION
POTKI'
STACK
WITH
PLMIE
'
�h
DRAW
NORTTT ARROR'
SIN�
WLVll
��
SIIN
BS
OBSERVER'S POSITION
144 °
LOG4TT
���T1T1T1JJJ���TITITIJJJ
—�
Additional Information
Continue on reverse side
Observation Dat
m o8
Start Time
13:4r0
End T" e
Sec
Mi 0
15
30
45 Comments
z b
3
0
4
O
"0 VA
1 arr.�r�no�
mec�n�
g_
�eea�
�c�c�nn
lim
DEQ-CFW 00068566

•
�a®MM
®nsorov
®MrOMM
M
MMEN
meonn
®M
MM
mennr.N
m"roll=©
m"S
MM
mMEMO
msr.pur•-MM
mMMUS
MMMORM
m
IMMIM
MMM
.•
n
mrnoM
MM"S
m
nVol
n�a
MMM
t,
e
®AnoOM
®r.1"nrn
MMMM=
mrmner•�
®on
�.
s
meoso
MMON
�
�■r�MMM
mn
�•
o�
�mnr�
�•
s
MMMen
MM�
Additional Information
DEQ-CFW 00068567

jpl
VISIBLE EMISSION OBSERVATION FORM
Company Name _
Location
G l,Jcs t
City /
I
State
Zip
'IGo�C'
Process E uipment
Operating Mode
' �
uipment
Control Eq,A /t S �
s
Operating Mode
Describe Emission Point
� `—a4c1c
Height of Emission Point Height Relative to Observer
Start ZS/ End
Distance to Emission Point Direction to Emission Point
/ Nvle L.�i.
Start End � Start End A10f
Vertical An le to Observation Pt. Direction to Obs rvation Point
Start 6 End 4100 Start sp K. End SD
Describe Emissions
Start End ,,V01V
Emission Color
If Water Droplet Plume (Circle)
Start C(&",L_. End
Attached Detached
Point In The Plume At Which Opacity Was Determined
t /
Start / End J
Describe Plume Background
Start/ End
.
Background Color Sky Condition
Start t(,e End P(,(,e Start 01�% End
Wind Speed Wind Direction
Start ✓ 10 End S-, D Start C/ End
Ambient Temp Wet Bulb
RH Percent
0 o Temp
Start � End
SOURCE LAYOUT SKETCH
EMISSION
OBSERVATION
POINT
STACK
WITH
CZ:
DRAW
pL��
NORTTT ARROW
str
.�
OBSERVER'S POSMON
-
4VL141)
4R °
SUATION LLVE
-
000�+
•
©�000
■��wwww
LD.te
Additional Information
Continue on reverse side
DEQ-CFW 00068568

•
move°
m�enn
�
aWSM
mir.-Mnnr�
�■■
mnr.�nn
minn�WIN
�rj1
Vol
MM
mrRIeoo
mr.»n01
�MWOMM��
ms�eo
O
rw2M®M
M
MM
ramp-MCUM
®MM
Os
cA
®rVEROMM
®MMMM
�©
r. IN
®rom5��
�0MMM
®OSAOpm
�OSMUM
�MM
M
�MM
�M
M�
Additional Information
DEQ-CFW 00068569

VISIBLE EMISSION ORSFRVATION FORM
DEQ-CFW 00068570

0
•
®asses
mee�c�n
®aces
mnonn
®sons
mic�or�n
mo�er�
mess
m©es�
mesas
mnr�r�e�
�r�esn
mosoe
mimeos
mosom
mo©r-�s
moms
®oven
®Hann
®s"r.�n
m�mnn
m0
MdP
M
NOW,
MAMMSaw
MMMMA
M0MMEM
-----
--_M-
Additional Information
DEQ-CFW 00068571

DuPont Fluoroproducts
22828 NC Highway 87 W
Fayetteville, NC 28306-7332
` y `_; April 4, 2008
iUd
Ms. Criristy Richardson
NCDENR- Division of Air Quality
Fayetteville Regional Office
225 Green Street - Suite 714
Fayetteville, NC 28301
SUBJECT: Rental Boiler (ID No. PS -Temp) Method 9 Testing
Protocol Submittal Form - Opacity
North Carolina Air Permit No. 03735T32
Dear Ms- Richardson:
Enclosed is the required signed Protocol Submittal Form for the Method 9 test that will be
performed, Pursuant to Part 2.1(G)(2)(d) of the subject permit, to determine the opacity of the
stack emissions from the temporary boiler (ID No. PS -Temp).
If you have any questions regarding this protocol, or if you need additional information, please
call me at 678-1155.
Michael E. Johnson
Environmental Manager
2oog-13§57T
E.I. du Pont de Nemours and Company
DEQ-CFW 00068572

FA
RIM
NCDENR
PROTOCOL SUBMITTAL FORM - OPACITY
DIVIRION OF AIR 01TALITY
Purpose: The primary goals of the Protocol Submittal Form are to initiate communication between representatives of the permitted facility, the testing
consultants, and the DAQ as well as to identify and resolve any specific testing concerns prior to testing. Instructions: Submit all forms and additional
information to the DAQ Regional c,,yernisor at least 45 days prior to testing. Please type or print clearly. This form applies to EPA Method 9
visible emissions evaluations only. If this form does not supply sufficient space to completely answer all questions or if additional relevant
information is necessary, attach additional documentation and/or information to the original form. Questions and/or comments should be directed to the
appropriate Regional Supervisor.
Specify Appropriate Regional Office: (check one)
❑ Asheville
® Fayetteville
❑Mooresville
❑ Raleigh
I ❑ Washington
1 ❑ Wilmington
❑ Winston-Salem
Facility Name: DuPont Company - Fayetteville Works
Testing Company:
RB,EIVED
Facility Address/City/County:
Testing Company Address:
22828 NC Highway 87 W
APR 0 7 2008
Fayetteville, NC 28306-7332
Bladen County
®ENR
Contact Person: Michael E. Johnson
Contact Person: FAYETTEVILLE ;i [ OFFICE
Phone: [phone]
Fax: [phone]
Phone: 7Fax:
Air Permit Number: 03735T32
Permitted Source Name and ID No.: See Section 2.1
Permitted Maximum Process Rate:
Maximum Normal Operation Process Rate:
Target Process Rate for Testing:
70,000 lb/hr steam
33,000 lb/hr
33,000 lb/hr
1.])List
all state and federal regulations that apply to the proposed testing: 15A NCAC 2D.0524 and 40 CFR Part 60 Subpart Dc
1.2)
Will all testing be conducted in strict accordance with the applicable test methods? If answer is no, please attach
complete documentation of all modifications and/or deviations to the applicable test methods,
®Yes
❑ No
L3)
Please speck if any VE observations will be performed concurrently (DAQ advises no more than 2):
❑ Yes
® No
1.4)
What is the proposed test schedule? The DAO Regional Supervisor must be notified at least 30 daysprior to the actual test date(s)
jApril
25, 2008
Additional Comments:
er ted faci and the contracted testing company must provide signatures below certifying that
Signatures: Representa ' �ided�
the in on this for and any attached information is accurate and complete.
Perm' to epresentative Date
Testing Company Representative Date
Name: Michael E. Johnson
Name:
Title: Environmental Manager
Title:
Company: DuPont Company = Fayetteville Works
Company:
VERSION 1.1 (2006-09-15)
This form is available from the DAQ website http://daq.state.ne.us/enf/sourcetest/)
'11%.
- Am_ � 1
DEQ-CFW 00068573

2.1) Please provide a complete list of the permitted emissions sources and a description of tree transfer points for VE observations:
Permitted Source
Description and ID
Subject to
NSPS
Proposed Transfer Point Description(s)
Comments
Temporary Boiler
ID PS-Tem
®Yes
❑ No
Boiler stack
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes.
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
❑ Yes
❑ No
VERSION 1.1 (2006-09-15)
This form is available from the DAQ website http://daq.state.nc.us/enf/sourcetest/)
DEQ-CFW 00068574