DEQ-CFW_00066048

0-,to4,ea
4M.DuPontFluoroproducts
Fayetteville Works Plant
22828 NC Highway87 West
Fayetteville, NC 28306-7332
CERTIFIED MAIL — RETURN RECEIPT REQUESTED
Mr. Steven F. Vozzo
IV nuary 20, 2012
NCDENR Division of Air Quality JAN
225 Green Street
Suite 714 UENH
Fayetteville, NC 28301-5043 FAYETTEVILLE REGIONAL OFFICE
SUBJECT: Miscellaneous Organic Chemical Manufacturing NESHAP (MON)
Compliance Report — July 1, 2011 through December 31, 2011 di
61��
0)Title V Permit Number 03537T37 �& ' r1'
Facility ID: 0900009 .;1( `� .,Hier
Dear Mr. Vozzo:
, A) q� )Ar
Al
Attached is the DuPont Company — Fayetteville Works' Compliance Report for the
Miscellaneous Organic Chemical Manufacturing NESHAP (40 CFR Part 63 Subpart
FFFF) for the reporting period from July 1, 2011 through December 31, 2011.
Enclosed is the required photocopy of this report.
If you should have any questions, please call me at 910-678-1155.
Michael E. Johnson
Environmental Manager
Attachment / Enclosure
cc: U.S. EPA Region 4, Air and EPCRA Enforcement Section, Atlanta, GA
E.I. du Pont de Nemours and Company
DEQ-CFW 00066048

Miscellaneotorg anic Chemical Manufacturing NVHAP (MON)
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
40 CFR 63.2520(e)(1) Company name and address:
DuPont Company — Fayetteville Works
22828 NC Highway 87 W
Fayetteville, NC 28306-7332
40 CFR 63.2520(e)(2) Statement by a responsible official with that official's name, title, and
signature, certifying the accuracy of the content of the report.
See Attachment 1 for this certification statement.
40 CFR 63.2520(e)(3) Date of report and beginning and ending dates of the reporting
period.
The date of this report is January 20, 2012. The reporting period of this report is from
July 1, 2011 through December 31, 2011.
40 CFR 63.2520(e)(4) For each SSM during which excess emissions occur, the compliance
report must include records that the procedures specified in your startup, shutdown, and
malfunction plan (SSMP) were followed or documentation of actions taken that are not
consistent with the SSMP, and include a brief description of each malfunction.
There are no sources subject to the Subpart FFFF NESHAP for which a startup, shutdown,
and malfunction plan (SSMP) is required.
40 CFR 63.2520(e)(5) The compliance report must contain the information on deviations, as
defined in §63.2550, according to paragraphs (e)(5)(i), (ii), (iii), and (iv) of this section.
There were no deviations from the emission limits, operating limits, or work practice
standards during the reporting period.
40 CFR 63.2520(e)(5)(i) If there are no deviations from any emission limit, operating limit or
work practice standard specified in this subpart, include a statement that there were no
deviations from the emission limits, operating limits, or work practice standards during the
reporting period.
There were no deviations from the emission limits, operating limits, or work practice
standards during the reporting period.
Page 1 of 3
DEQ-CFW 00066049

Miscellaneous•Or anic Chemical Manufacturing NPHAP (MON)
g g
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
40 CFR 63.2520(e)(5)(ii) For each deviation from an emission limit, operating limit, and
work practice standard that occurs at an affected source where you are not using a
continuous monitoring system (CMS) to comply with the emission limit or work practice
standard in this subpart, you must include the information in paragraphs (e) (5) (ii) (A) through
(C) of this section. This includes periods of SSM.
There were no deviations from the emission limits, operating limits, or work practice
standards during the reporting period.
40 CFR 63.2520(e)(5)(iii) For each deviation from an emission limit or operating limit
occurring at an affected source where you are using a CMS to comply with an emission limit
in this subpart, you must include the information in paragraphs (e)(5)(iii)(A) through (L) of
this section. This includes periods of SSM.
There were no deviations during the reporting period. In addition, no affected sources at
this facility use a continuous monitoring system to comply with an emission limit in this
subpart.
40 CFR 63.2520(e)(5)(iv) If you documented in your notification of compliance status report
that an MCPU has Group 2 batch process vents because the non -reactive HAP is the only
HAP and usage is less than 10, 000 lb/yr, the total uncontrolled organic HAP emissions from
the batch process vents in an MCPU will be less than 1, 000 lb/yr for the anticipated number
of standard batches, or total uncontrolled hydrogen halide and halogen HAP emissions from
all batch process vents and continuous process vents in a process are less than 1,000 lb/yr,
include the records associated with each calculation required by §63.2525(e) that exceeds an
applicable HAP usage or emissions threshold.
This section is not applicable.
40 CFR 63.2520(e)(6) If you use a CEMS, and there were no periods during which it was
out -of -control as specified in §63.8(c)(7), include a statement that there were no periods
during which the CEMS was out -of -control during the reporting period.
This section is not applicable. No affected sources at this facility use a continuous
emission monitoring system.
Page 2 of 3
DEQ-CFW 00066050

Miscellaneotorg anic Chemical Manufacturing NPHAP (MON)
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
40 CFR 63.2520(e)(7) Include each new operating scenario which has been operated since
the time period covered by the last compliance report and has not been submitted in the
notification of compliance status report or a previous compliance report. For each new
operating scenario, you must provide verification that the operating conditions for any
associated control or treatment device have not been exceeded and that any required
calculations and engineering analyses have been performed. For the purposes of this
paragraph, a revised operating scenario for an existing process is considered to be a new
operating scenario.
This section is not applicable. This site does not have any new operating scenarios that
have been operating since the submittal of the notification of compliance status report.
40 CFR 63.2520(e)(8) Records of process units added to a PUG as specified in
§63.2525(i)(4) and records of primary product redeterminations as specified in
§63.2525(i) (5).
This section is not applicable. This site does not have any process unit groups.
40 CFR 63.2520(e)(9) Applicable records and information for periodic reports as specified
in referenced subparts F, G, H, SS, UU, WW, and GGG of this part and subpart F of 40 CFR
part 65.
The periodic report for Subpart UU as specified in 40 CFR 63.1039(b) is provided as
Attachment 2.
40 CFR 63.2520(e)(10) Notification ofprocess change.
This section is not applicable. Since the submittal of the notification of compliance status
report, this site has not made any process changes that are not within the scope of an
existing operating scenario.
Page 3 of 3
DEQ-CFW 00066051

Miscellaneoutorg anic Chemical Manufacturing NIHAP (MON)
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
ATTACHMENT 1
Certification of Report Accuracy
As required by 40 CFR 63.2520(e)(2), this document is the statement by a responsible official
certifying the accuracy of the content of the subject MON compliance report.
By my signature below, I certify under penalty of law that I have personally examined and am
familiar with the information submitted in this document and all attachments and that, based
on my inquiry of those individuals immediately responsible for obtaining the information, I
believe that the information is accurate. I am aware that there are significant penalties for
submitting false information, including the possibility of fine and imprisonment.
Ellis H. McGa
Plant Manager
JanuM 19, 2012
Date
JAN 23 2012
DENR
FAYETTEVILLE REGIONAL OFFICE
DEQ-CFW 00066052

Miscellaneous Organic Chemical ManufacturingtESHAP (MON)
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
ATTACHMENT 2
Periodic "Monitoring, Summary
Report: R807
Report Date- 1433,2012 12--34:43PT%4
Reportfronr 2011-7-100 To 2011-12-31
Compliance Group.
HFP0
Percent
Lite
Non
Leaking
Instlecte
Le-aldn
Rfnni
Revairable
VALVES
JULY
0
0
0. GO
0
0
-kUGU'-,,'T
0
1771
0-00
0
0
SEPTEMBER
0
0
0-00
0
0
0
0
0.00
0
0
NON -ENIBER
0
176
0-00
0
0
DECENIBER
0
0
0.00
0
0
PUMPS
47-ILY
0
1
0.00
0
0
AUGUST
0
3
0.00
0
0
SEPTENIBER
0
0
0-00
0
0
OCTOBER
0
3
0-00
0
0
NNOVENIBER
0
3
0-00
0
0
DECEMBER
0
3
0-00
0
0
COMPRESSORS
JULY
0
0.00
0
0
AUGUIST
0
0
0.00
0
0
SEPTENIBER
0
0
0-00
0
0
OCTOBER
0
0
0.00
0
0
NOITNMER
0
0
0-01)
0
0
DECEMBER
0
0
0,0t3
0
0
AGITATORS
JULY
0
0
0,00
0
0
AUGUST
0
0
0-00
0
0
SEPTEMBER
0
0
0,00
0
0
OCTOBER
0
0
0,00
0
0
NOV'EMBER
0
0
0,013
0
0
DECENMER
0
0
0,00
D
0
CONNECTORS
JUTLY
0
0
0,00
0
0
AUGUNS T
0
0
0-03
0
0
SEPTEMBER
0
0
0-00
0
0
OCTOBER
0
0
0,00
0
0
-NOVEMBER
0
16
0.00
0
0
DECE.MBER
0
0
0.00
0
0
Page I of 4
DEQ-CFW-00066053

Miscellaneous Organic Chemical Manufacturing NESHAP (MON)
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
ATTACHMENT 2
Periodic 'Monitorilicy SuInInIry
Report: R807
Report Date- V13,2012 12:34A3PM
Report ftoin: 2011-7-100 To 2011-12-31
Carr phaure Group -
POLYMERS',
Percent
Lace
Non
Leakino
Inspected
L,-akin
Repair
Rmairable
VALIVES
JULY
0
0
0-00
0
0
AUGUST
0
6.1
0-00
0
0
SEPT EAMBER
0
0
0-00
0
0
OCTOBER
0
0
0-00
0
0
NU%T-NME,R
0
651
OM
0
0
DEC'EMBER
0
0
0.00
0
0
PUMPS
JULY
0
1
0-00
0
0
AUGUST
0
2
0.00
0
0
SEPTENIBER
0
0
0-00
0
0
OCTOBER
0
0-00
0
0
NOVENIBER
0
2
0-00
0
0
DECEINIBER
1
50.00
0
0
COMPRE.-SSORS
JUTLY
0
0
0.00
0
0
AUGUST
0
0
0-00
0
0
SEPTENIBER
0
0
OM
0
0
OCTOBER
0
0
0-00
0
0
N-OV'ENIBER
0
0
0,00
0
0
DECETNIBER
0
0
0.00
0
0
AGITATORS
JULY
0
0
0.00
0
1)
AUGUST
0
0
0,00
0
0
SEP-1EMBEF,
0
0
0.010
0
0
OCTOBER
0
0
0-00
0
0
NOVIMBER
0
0
000
0
0
DECEINIBER
0
0
OM
0
0
CONNECTORS
JUTLY
0
0
0-00
0
0
AUCTU-ST
0
0
Mo
0
0
S --EPTE INIBER
O
0
0-00
0
0
OCTOBER
0
0
0-00
0
0
NOVENIBER
0
0
0-00
0
0
DECENIBER
0
0
0-00
0
0
Page 2 of 4
DEQ-CFW-00066054

Miscellaneous Organic Chemical Manufacturing NESHAP (MON)
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
ATTACHMENT
Periodic Monitoring Sin-amary
Report: R807
Report Date- V13/2012 12-34:43PM
Report froin: 2011-7-100 To 2011-12-31
Compliance Group:
VE'NORTH
percent
Late
2iga—
Lenk-jua
Insnected
Leakan
Rey air
Revairable
V.AL:%T-S
JULY
0
0
0.01)
0
0
AUGUSIT
I
is"
0J5
0
0
SEPTENIABER
0
0
0.00
0
0
OCTOBER
0
1
0:00
0
0
N101vTEMBER
0
183
0.00
0
0
DEC2N,f BER
0
0
0-00
0
0
PUMPS
R)LY
0
=
001)
0
0
AL. GUST
0
0-00
0
0
SEPTEIABER
0
0
0.00
0
0
OCTOBER
0
5
0A
0
0
N-01YUNIBER
0
0.00
0
0
DECEMBER
0
5
0-00
0
0
COMPRESSORS
JULY
0
0
000
0
0
AUGUST
0
0
0-00
0
0
bEPTEMBER
0
D
Un
0
0
OCTOBER
0
0
0-00
0
0
NONT-11ABER
0
0
0:00
0
0
DECEIABER
0
0
0-00
0
0
AGIT-A.TOR�
JULY
0
1
0-00
0
0
AT-7GUST
0
1
000
0
0
SEPTENIEBER
0
0
0-00
to
0
OCTOBER
0
1
0A
0
0
NTO%,T-MBER
0
1
000
0
0
DECE,'VIBER
0
1
0.00
0
0
CON--\T-CTOR,
0
0
0-00
0
0
AT,GU-.'-jT
0
0
0-00
0
0
SEPTEIMBER.
0
0
0-00
0
0
OCTOBER
0
0
0,00
0
0
NOVEMBER
0
0
0-00
0
1)
DECF-',YIBER
0
0
0- w-
0
0
Page 3 of 4
DEQ-CFW-00066055

Miscellaneous Organic Chemical Manufacturing NESHAP (MON)
Part 63 Subpart FFFF
Compliance Report
40 CFR 63.2520(e)
DuPont Company — Fayetteville Works
North Carolina Title V Air Permit No. 03537T37
Reporting Period from July 1, 2011 through December 31, 2011
ATTACHMENT 2
Periodic Alonitoilngg Summary
Report: R807
Report Date: 1/13/2012 12:34:43PNI
Report frona: 2011-7-100 To 2,011-12-31_
Compliance Group.
VE SOUTH
Percent
Late
Nan
Leaking
Inspected
Leaking
Repair
Repairable
VALVES
JULY
0
0
000
0
0
AT -GUST
0
182
0.00
0
0
SEPTENNIBER
0
0
0.00
0
0
OCTOBER
J
0
0,00
0
0
N0'v`EIVIBER
0
182
0-00
0
0
DECEMBER
0
0
0,00
0
0
PI-7-1111ps
JULY
0
6
0,04)
0
0
AUGUST
0
6
OM
0
0
:SEPTE'VIBER
0
0
0-00
0
0
OCTOBER
0
6
0.00
0
0
N'O-`ENIBER
0
6
000
0
0
DECETIVIBER
0
6
000
0
0
COMPRESSORS
JULY
0
0
0-00
0
0
AUGUST
0
0
000
0
0
SEPTONIBER
0
0
GM
0
0
OCTOBER
0
0
0.00
0
0
N1,01'EIVIBER
0
0
0.04)
0
0
DECENIBER
0
0
000
0
0
.AGITATORS
JULY
0
0
0.00
0
0
AUGUST
0
0
0-00
0
0
S'EPTENIBER
0
0
0011)
0
0
OCTOBER
0
0
000
0
0
NON�TIVIBER
0
0
0-00
0
0
DECEMBER
0
0
0,00
0
0
CON-NIECTORS
JULY
0
0
0-00
0
0
AT--GTJS,T
0
0
0-00
0
0
SEPTEMBER
0
0
OM
0
0
OCTOBER
0
0
O-CA)
0
0
NO EMBER
0
0
0-00
0
0
DECENIBER
0
0
0-0
0
0
Page 4 of 4
DEQ-CFW-00066056