DEQ-CFW_00063592

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DEQ-CFW 00063592

NPDES PERMIT NO. e C e00
FACILITY NAME j
OPF'RATOR IN RESPONSIBLE CH GE
CERTIFIED LABORATORIES (1)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGIN��,,Arid ONE COPY to:"� ,
ATTN: CENTRALF.ILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O. BOX 29535 JAN
RALEIGH, NC 27626-0535
MF+5 A* JAN18 19tf
EFFLUENT
DISCHARGE NO.C0 MONTH YEA J
CLASS_5 COUNTY /��✓
GRADES PHONE(C,>/()-) /-2 / c
cI (2)
PERSON(S) COLLECTING SAMPLES
X p , 60-jJ1
(SIGNATURE OF OPERA OR RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DATE
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DEM Form MR-1 � 1:'/93)
I
DEQ-CFW 00063593

:w
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant ;
x
All monitoring data and sampling frequencies do NOT meet permit requirements El'
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect Wequipment, operation, maintenance, etc.,
and a time table for improvements to be made. 1%0
See ,4-##-c-Ae,1 le-6�— � /�.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
67
Pe (Please p ' )
Sig. ature of Permittee** ate
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556 Oil & Grease
00951 Total Fluoride
00600 Total Nitrogen
01002 Total Arsenic
00610 Ammonia Nitrogen
00625 Total Kjeldhal
01027 Cadmium
Nitrogen
-
00630 Nitrates/Nitrites
01032 .Hexavalent Chromium
01034 Chromium
00665 Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total. Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
8.1551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the, reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by otherthanthe_permittee, delegation of signatory authority must be on file with the.state per 15A NCAC 2B .0506<(b)
(2) (D)•
It
DEQ-CFW 00063594

NPDES PERMIT NO. C V 00 3 57 72
FACILITY NAME L) k po"t
OPERATOR IN RESPONSIBLE CHARGE I
CERTIFIED LABORATORIES (I 14e-a
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT,
DEHNR 11
P.O. BOX 29535
RALEIGH, NC 27626-0535
I 95
EFFLUENT i S
DISCHARGE NO. 67e -;2 MONTH L eC ZAbKo- YEAR 1-ff-
CLASS 3 COUNTY
2C) bn-0,t'- - GRADER PHONE( 9/QJ,
> 'A, —(2)
PERSON(S) COLLECTING SAMPLES— A
A I A - ,
x 4 t--- M'­
( Tr-N AT OR I
S 'URE !�Pffl HA 'IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
- 96-
DATE
50050 00010 00400 150060 00310100610 00530 31616 003001 OOW 006651,901Sl I I I
ENTER PARAMETER CODE
FLOW m a rA ABOVE NAME AND UNITS --�
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DEM Form MR- I (12/93)
DEQ-CFW-00063595

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken_ in respecCto equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather -and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment -for knowing violations."
Permittee Address
00010
Temperature
00076
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
of
Phone Number
PARAMETER CODES
00556 Oil & Grease
00951 Total Fluoride
00600 Total Nitrogen
01002 Total Arsenic
00610 Ammonia Nitrogen
00625 Total Kjeldhal
01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites
01032 Hexavalent Chromium
01034 Chromium
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
Date
01067 Nickel
01077 Silver
01092 Zinc
-01105 Aluminum
01147 Total Selenium
331616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
Permit Exp. Date
50060 Total
Residual
Chlorine
71880 .Formaldehyde
71900 ,Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone],,extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the. reporting
facility's permit for reporting data.
* ORC must visit facility; and document visitationof facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authoritymust be on -file with, the stateper15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063596

DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
Y r
aUPONT
DuPont Automotive
January 11, 1995
A. Preston Howard, Jr. P.E.
Director - NCDEHNR
Division of Environmental Management
P.O. Box 29535
Raleigh, NC 27626-0535
RE: NPDES Permit No. N00003573
Dear Mr. Howard,
The Outfall 001 Total Suspended Solids (TSS) on December 6, 1994,
was measured as 3270 lb/day versus the NPDES Permit Daily Maximum
limit of 950 lb/day.
This apparent noncompliance was due to an analytical error. The
original analysis for that date by our commercial laboratory
indicated 440 mg/L TSS in the Outfall 001 effluent. Our own
internal TSS analysis of that sample showed only 6 mg/L TSS. Our
commercial laboratory re -analyzed the retained sample, which
resulted in no detectable (0 mg/L) TSS.
While our commercial laboratory has agreed that the initial
result had to have been in error, the re -analysis of the sample
exceeded the seven-day maximum hold time for TSS. Therefore, we
unfortunately must use the original result.
To prevent recurrence of this noncompliance, we are changing to a
commercial laboratory which promises to be more responsive in
identifying and correcting obviously questionable analytical
results.
If you should have any questions regarding this matter, please
feel free to contact me at [phone].
Michael E. Johnson
Environmental Coordinator
cc: Ms. Kitty Kramer, DEHNR-Fayetteville
E. I, du Pont de Nemours and Company
® Printed on Recycled Paper
FF-9522 Rev. M
DEQ-CFW 00063597

t oUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer Z
Fayetteville, NC 28302
January 12, 1995
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. 0. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for December, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219 or
Mike Johnson at 9910-678-1155.
RJG:ekw
Attachments
CC: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
M. E. Johnson - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063598

GK3DEX87/DR.
f
DAY
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM
MINIMUM
UNIT
STYPE
QSTATUS
LIMIT
DATE
C'OMPLIANCE- MONITORING - SIR REP
PER MIT--NC0003573 �JP E - - 0 0 1 i�ROf--912 LOC --- E
FACILITY--DUPONT-FAYETTEVILLE CLASS--2
LOCATION--FAYET•.TEVILLE REGION/CJiJNTY- 06 8LADEN
00010 00400
50050
Q/MGD//
1.11150/'
i . 7 9x0
. 8 9�
,9�
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PAGE 1
00310 00530 TGP3B 00556 00600
BOO RES/TSS CER17DPF OIL-GRSE TOTAL N
Zb� 55:0
16;rO 32705.0 5.900
20 58y0�' /
.00
7 44�fl
16-w 8
32.f33
74.00
lb. 0
LBS/JAY
CP I/I
IIANN
931201
21'eT. O
19 .0 ,
35.O
3-64. 0
327-0 '.0
364.2
3270.0
3 0
LBS/'JAY PASS/FAI
C P I/F ?? I/I
FFNNN NNNNN
931201 931201
5.000
5.000
5.000
5.000
5.000
5.fl0
G/L
GR I/I
NNNNN
931201
5.9
5.900
5.9 00
5.�
5.900
5.900
My/L
CP I/I
NNNNN
931201
DEQ-CFW 00063599

GKBDEX87/iR
GAY
O1
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
3C
31
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM
MINIMUM
UNIT
STYPE
OSTATUS
LIMIT
DATE
COMPLIANCE MONITORING — DMR REPORT
PERMIT--NC0003573 PIPE--001 DMR (YR/MO)--94/12 LOC---E
PACiLITY--DUP3NT—FAYETTEVILLE CLASS--2
LOCATION--F-AYETTEVILLE RE.ION/COUNTY--06 BLADEN
O1/19/95
PAGE 2
00665 32102 32103 34200 34205 34215 34220 34230
PHOS—TOT CARSNTET 12DICL=T ACENAPHT ACENAPHT ACRYLO?\II ANTHRACE BENZ3FLU
2.800
2.80' 0
208 00
2.8000
2.8030
2e8OOO
MG/L LBS/DAY
CP I/I ?? F/I
NNNNN
LBS/DAY LBS/DAY LBS/DAY LSS/DAY LBS/DAY LBS/DAY
?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I
931201 931201 931201 931201 931201 931201 931201 931201
DEQ-CFW 00063600

GK9DEX87/DR 01/19/95
COMPLIANCE MONITORI`JG - DMR REPORT PAGE 3
PERMIT--NCO003573 PIPE--001 DMR {YR/MO)--94/12 LOC---E
FACILITY--DUPi1NT-FAYETTEVILLE CLASS--2
' LOCATION--FAYETTEVILLE REGION/COUNTY--06 3LADEN
34242 34247 34301 34311 34320 34336 34341 34371
DAY BENZO(K) RENZO( A) CHLOROBE CHLJROET CHRYSENE DIFTHYLP DIMETHYL ETHYLBEN
01
G2
03
04
05
06
07
OE
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM!
MINIMUM
UNIT LBS/DAY L9S/JAY L8S/DAY LBS/3AY LEIS/DAY LDS/DAY LSS/DAY LESS/DAY
STYPE ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?"' F/I ?? F/I
QSTATUS NNNNN
LIMIT
DATE 931201 031201 931201 931201 931201 931201 931201 931201
DEQ-CFW 00063601

GK0DEX87/0R
DAY
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
.23
24
25
26
27
28
29
30
31
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM
MINIMUM
COMPLIANCE MONITORING - DMR REPORT
PERMIT--NCO0O3573 PIPE--001 DMR (YR/MO)--94/12 LOC---E
FACILITY--DUPONT-FAYETTEVILLE CLASS-2
LOCATION--FAYETTEVILLE REGION/COUNTY--06 3LADEN
01/19/95
PAGE 4
34376 34381 34396 34418 .34423 34447 34461 34469
FLUORANT FLU3RENE HEXACHLO METHYLCH METHYLEN NITROBEN PHENA'NTH PYR.ENE
UNIT LBS/DAY LBS/DAY LBS/DAY LBS/DAY LES/DAY LBS/DAY LBS/DAY LBS/DAY
STYPE ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I
QSTATUS
LIMIT
DATE 931201 931201 931201 931201 931201 931201 931201 931201
DEQ-CFW 00063602

GK'3DEX87/DR
DAY
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
COMPLIANCE MONITORING - DMR REPORT
PERMIT--NCO003573 PIPE--001 DMR (YR/MD)--94/12 LOC --- E
FACILITY--DUPONT-FAYETTEVILLE CLASS--2
LOCATIOd--FAYETTEVILLE REGION/COUNTY--06 BLADFN
01/19/95
PAGE 5
34475 34496 34501 34506 34511 34526 34536 34541
TETRACHL 11DIC4LO 11DICHLO 1.11TRICH 112TRICH BENZO(A) 12DICHLO 12DICHLO
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM
MINIMUM
UNIT LBS/DAY
STYPE ??_F/I
QSTATUS
LIMIT
DATE 931201
LBS/DA.Y LBS/DAY LBS/DAY LBS/DAY LBS/DAY LBS/DAY LBS/DAY
?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I ?? F/I
931201 931201 931201 931201 931201 931201 931201
DEQ-CFW 00063603

GK3DEX°7/uR 01/19/95
CJMPLIANCE MONITORING - DMR REPORT 'PAGE 6
PERMIT--NC0003573 PIPE--001 DMR (YR/MO)--94/12 LOC---E
FACILITY--DUPONT-FAYETTEVILLE CLASS--2
LOCATION--FAYETTE'VILLE REGION/COUNTY--06 9LADEN
34546 34551 34566 34571 34591 34601 34606 34611
DAY 12DICHLO 124TRICH 13DICHLO 14DIC4LO 2NITROPH 24DICHLO 24DIMETH 240INITR
01
02
03
04
05
Ora
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM
MINIMUM
UNIT LbS/DAY
STYPE ?? F/I
QSTATUS
LIMIT
GATE 931201
LBS/JAY L3S/DAY LBS/CAY LES/DAY LAS/CAY LBS/DAY LOS/JAY
?? F/I ?? F,/I ?? F/� ?? F/I ?? FCI ?? F/I - ?? F/I
931201 931201 9312101 931201 9.31201 931201 931201
DEQ-CFW 00063604

GKPDEX'87/DR. 01/19/95
COMPLIANCE MONITORING - DMR REPORT PAGE 7
P'ERMIT--NC0003573 PIPE--001 OM R (YR/MO)--94/12 LOC---E
FAC.ILITY--OUPONT-FAY=TTEVILLE CLASS--2
LOCATION--FAYETTEVILLE REGIOWCOUNTY--06 3LADEN
34616 34626 34646 34657 34696 39100 39110 39175
JAY 24DI -ITR 26DINITR 4NITR0PH 46DINITR NAPTHALE 82E PHTN DNB PHTH VINYLCHL
01
02
03.
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM
MINIMUM
UNIT LBS/DAY L3S/DAY
STYPE ?? F/I ?? F/I
QS TATUS
LIMIT
DATE 931201 931201
LBS/DAY
L3S/tDAY
L3S/DAY
LBS/DAY
LBS/DAY
LBS/tDAY
?? F/I
?? F/I
?? F/I
?? F/I
?? F/I
?? F/I
931201
931?01
931201
931201
931201
931201
DEQ-CFW 00063605

GKBDEX37/DR 01/19/95
COMPLIANCE MONIT`JRING - DMR REPORT PAGE 8
PERMIT--NCO0O3573 PIP;--001 DMR (YR/MO)--94/12 LOC---E
FACILITY--DUPONT-FAYETTEVILLE CLASS--2
LOCATION--FAYETTEVILLE REGION/COUNTY--06 BLADEN
39700 39702
DAY KB NEXCL.9D
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
REPORTED
AVERAGE
MAXIMUM
MINIMUM
COMPUTED
AVERAGE
MAXIMUM
MINIMUM
UNIT LSS/DAY LBS/DAY
STYPE ?? F/I ?? F/I
QSTATUS
LIMIT
DATE 931201 931201
DEQ-CFW 00063606

GKBDEt37/DR
CJMPLIANCE MONITORING - DMR REPORT
PERMIT--NC0003573 PIPE--002 MR (YR/MO)--94/12 LOC---E
FACILITY--DUPONT-FAYETTEVILLE CLASS--2
LOCATION--FAYETTFVILLE REGION/COUNTY--06 BLADE"S
50050 0 00400 00310 00340 00951
DAY G}/MOD EMP PH 303 COD FLUORIDE
01 16.15 22. 7ado-
0202 16.122. 7.
03 16. 0 22. 7.
04 16.1,0� 2;.� 7: FO-
05 16.1 00 2 50-
06 14.615 0 , 22. 7.Et7,�?/ 1344.0t1�
07 14 0 8 14 o'�CT 0� 2 3. W� , /
09 14. 23. 7.
10 14. 6�5 0� 2 3 . / � 7.
11 14.e,_300u 23:z 7.
12 14 . E►�5�0 0 L 2 . ba-' 7. Ef9'��
13 14 . _ -1-0-6 2 2. a-3-'' 7 . E7. �_t,C-f0 - 12 3 5 .
14 14. 3kjr 2 2 .� 7. i��o15 14.�t 16 14 . � 2 2 . /eA�I� 7.
17 14 .; 0� 2 2,
18 14.8'i 0 2 2 ..OII 7.3.R
19 14. � 2 0 .,1 7.
20 14.�00 21� 7.�� 1482.0w
21 13.8600 21.� 7.@�7//
22 13.8600 21..20� 7.b/
23 13.8600 21.-80/ 7 57'D�
24 13.3600 21.-0 / 7.�t50,
3.8600 21..A� 7:;E 0
26 3.860 ��- 7.Fo
3.8 Ofl 20.t' 7.2196.0028 3 600 20.097.
29 13*8600 20.@� 7.
30 13.8600 20. / -7
31 13.8600 20. t 7.5�
REPORTED
AVERAGE 14. 0 21.r0',� /� 1564.O6�
MAXIMUM 16.1_0 23.43� 8.._0�/' 219b.J�JO�
MINIMUM 13o8 0 20.� 7.500 1235.0A
COMPUTED
AVERAGE 1496529 21.51 1564.250
MAXIMUM 16.1500 23.00 8.800 2196.000�
MINIMUM 13.8600 20. 7.50 1235.000
UNIT MGo DEG.0 SU MG/L MG/L LBS/DAY
STYPE ?? I/I GR I/I GR. I/I ?? I/I ?? I/I CP I/I
0STATUS NNNNN NNNNN 4NINI NNNNN NNNNN NINNN
LIMIT
DATE 931201 931201 931201 931201 931201 931201
O1/19/95
PAGE 1
DEQ-CFW 00063607

IJo �O\j
d`2 Co vv-w-A-e-Ls 4 ---
V`A c)f- I=>� � �o
All
DEQ-CFW 00063608

• 4 p
EFFLUENT
,�F QAN 0 ISi9951
NPDES PERMIT NO. 3 DISCHARGE NO. ®© MONTH YEAR 1�
FACILITY NAME CLASS-_ COUNTY �3
OPERATOR IN RESEA1 C GRADE& PHONE a t
` CERTIFIED LABORtA) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF OVERATOR IN RESPONSIBLE CHARGE) A- y
DEHNR BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS �c
P.O. BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.,,
RALEIGH, NC 27626-0535
DEM Form MR-1 (12/93) "° C n '1) A "-J /- D N �B,4c-K
DEQ-CFW 00063609

t
Facilify Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
All monitoring data and sampling frequencies do NOT meet permit requirements
Q
Compliant
ED-
Noncompliant
If the facility is noncompliant, please comment on corrective actions tieing taken in respect to,equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
�e2 64/�l�d 4tsfTelf 6�ea�luc�l-ra !-todt e6hao%4li�o
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those q uY Pe p g y persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibilityof fines and imprisonment for knowing violations."
yy
Permittee (Please pri" type)
Sigfiature of P 'ttee** Date
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00556
Oil & Grease
00951
Total Fluoride
00076 Turbidity
00600
Total Nitrogen
01002
Total Arsenic
00080 Color (Pt -Co)
00610
Ammonia Nitrogen
00082 Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00095 Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
00300 Dissolved Oxygen
01034
Chromium
00310 BOD5
00665
Total Phosphorous
00340 COD
00720
Cyanide
01037
Total Cobalt
00400 pH
00745
Total Sulfide
01042
Copper
00530 Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
01045
Iron
00545 Settleable Matter
00940
Total Chloride
01051
Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliforrn
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
50060 Total'
Residual'
Chorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at (919) 733=5083, extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility'spermit for reporting data.
* ORC must visit facility and documentvisitation of facility as required per 15A NCAC 8A .0202 (b) (5)`(B).
* * If signed by other than the permitted, delegation of signatory authority must -be on file with the state per 15A NCAC 2B .0506 (b)
(2)'(D)•
DEQ-CFW 00063610

j) LJAN b 61995,
NPDES PERMIT NO. N C 000 35 -7;
FACILITY NAME[/L On;pi '
OPERATOR IN RESPONSIBLE CHARGE 1
CERTIFIED LABORATORIES ")
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O. BOX 29535
RALEIGH, NC 27626-0535
50050
0001
FLOW
W
*
E U
H y
y
a
EFF ❑
EFFLUENT
DISCHARGE NO. 00--� MONTHAZQdPg, P YE�°'R2j-
CLASS .3 COUNTY %3
fir , GRADES PHONEaL,0 l 78
(2)
P SRE ON(S) COLLECTING SAMPLES D�
(SIGNATURE OF OPENATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
50060 00310 00610 00530 31616 00300 00600 00665 3 U d0ynfl
ENTER PARAMETER CODE
a z A A z ABOVE NBELOW D UNITS
Z
W
C0
WW
p20 �
�o s
WZ
aO
W
gO
O
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am
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1
71
UG/L I MG/I, I MG/L I MG/L
DEMForm MR- 1 (12/93)
+ C0 menu �- 6,J 13 FIGK
DEQ-CFW 00063611

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements_
ED-
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made. '
14
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Pe ttee (Please p ' )
Signature of Pe `ttee* * Date
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556
Oil & Grease
00951 Total Fluoride
01067 Nickel
00600
Total Nitrogen
0-1002 Total Arsenic
01077 Silver
00610
Ammonia Nitrogen
01092 Zinc
00625
Total Kjeldhal
01027 Cadmium
01105 Aluminum
Nitrogen
00630
Nitrates/Nitrites
01032 Hexavalent Chromium
01147 Total Selenium
01034 Chromium
31616 Fecal Coliform
00665
Total Phosphorous
32730 Total Phenolics
00720
Cyanide
01037 Total Cobalt
34.235 Benzene
00745
Total Sulfide
01042 Copper
34481 Toluene
00927
Total Magnesium
38260 MBAS
00929
Total Sodium
01045 Iron
395-16 PCBs
00940
Total Chloride
01051 Lead
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with_thestate per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063612

DuPont Automotive Products
P. 0. Drawer Z
Fayetteville, NC 28302
DuPont Automotive Products
December 23, 1994
A. Preston Howard, Jr. P.E.
Director - NCDEHNR
Division of Environmental Management
P.O. Box 29535
Raleigh, NC 27626-0535
RE: NPDES Permit No. NC0003573
Dear Mr. Howard,
During the week of November 21, 1994, both BOD-5 and TSS for
Outfall 001 were tested once versus 3/week as required by the
referenced NPDES permit. During that same week, the Outfall 002
weekly Fluoride analysis was not performed.
This noncompliant monitoring was due to our contract laboratory
closing Thursday and Friday of that week for Thanksgiving. Our
sample collection days are Tuesday, Wednesday, and Thursday. We
were not aware of the laboratory's holiday schedule until it was
too late to submit the Wednesday and Thursday samples.
To prevent recurrence of these noncompliances, we have worked
closely with our laboratory to ensure that three daily samples
are analyzed during the weeks affected by Christmas and New
Year's. We are also considering changing to a laboratory whose
work schedule does not interfere with our analytical
requirements.
If you should have any questions regarding this matter, please
feel free to contact me at [phone].
Sincerely,
Michadl E. Johnson
Environmental Coordinator
cc: Kitty Kramer, DEHNR-Fayetteville
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063613

oUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer
Fayetteville, NC 28302
December 22, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for November, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219.
RJG:ekw
Attachments
cc: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
M. E. Johnson - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063614

let
EFFLUENT C rtirC Q
1 i99
NPDES PERMIT NO C 0003 3 DISCHARGE NO. 601 MONTH OG A,- YE /f `
FACILITY NAME CLASS 3 COUNTY / I-eW
OPERATOR IN RESPONSIBLE CHANGE (O,RC) o�w GRADE_ PHONE(
CERTIFIED LABORATORIES (1), ALC L (2)
CHECK BOX IF ORC HAS CHANGED F-] PERSON(S) COLLECTING SAMPLES Qt:�-A-#'`� .
F
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF OPERATQA IN RESPONSIBLE CHARGf.;: _ ATE
DEHNR BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
P.O. BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH, NC 27626-0535
ITEM Form MR-1 (12/93) * "-Pj-,4"JT A w� D o cjo rJ
DEQ-CFW 00063615

a lu"
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permitrequiremenfs
Compliant
All monitoringdata and sampling frequencies do NOT meet
p g eq permit requirements'
Noncompliant°
If the facility is noncompliant, please comment on corrective actions being taken 'in respect to equipment; operation; maintenance, ete.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or sup- ervision'in accordance-
`
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant`
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES.
00010 Temperature '. , j00556 Oil & Grease 00951 Total Fluoride
00076 Turbidity ,
00600 Total Nitrogen
01002 Total Arsenic
00080 Colo% (Pt -Co)
00610 Ammonia Nitrogen
00082 Color (ADMI)
00625 Total Kjeldhal
01027
Cadmium
Nitrogen
00095 Conductivity
00630 N_ itrates/Nitrites
01032
Hexavalent Chromium
00300 Dissolved Oxygen
01034
Chromium
00310 BODS
00665 Total Phosphorous
00340 COD
00720 Cyanide
01037
Total Cobalt
00400 pH
00745 Total Sulfide
01042
Copper
00530 Total Suspended
00927 Total Magnesium
Residue
00929 Total Sodium
01045
Iron
00545 Settleable Matter
00940 Total Chloride
01051
Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension `581`or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
* * If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063616

/
EFFLUENT [�
0
NPDES PERMIT NO./ /C000 5 2s DISCHARGE NO. 4574V-12- MONTH"
FACILITY NAME OW CLASS 3 COUNTY
OPERATOR IN RESPONSIBLE CHARGE ORC) GRADE 3 PHONEC9�� G%8%/F
CERTIFIED LABORATORIES (1) _ (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES--
Mail ORIGINAL and ONE COPY to: c
ATTN: CENTRAL FILES x
DIV. OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF�OOR IN RESPONSIBLE CHARGE) DATE
DEHNR BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
P.O. BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH, NC 27626-0535
DEM Form MR-1 (12/93) -*'? L jq'q S h'*T 'bQ "O /J
DEQ-CFW 00063617

Facility Status: (Please check one of the following)
ti
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to jequipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am'aware that are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing vioikions "
Pe " tee (Please print or type)
Signat of Permit * Cl ja�te
Permittee Address Phone Number Permit Exp. Bate
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556 Oil & Grease
00951 Total Fluoride
00600 Total Nitrogen `
01002 Total' Arsenic
00610 Ammonia Nitrogen
00625 Total Kjeldhal
01027 Cadmium
Nitrogen
00630 Nitrates/Nitrites
01032 Hexavalent Chromium
01034 Chromium
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS'
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900` Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at (919) 733-50831 extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the permittee, delegation of signatory authority must be on file with the stateper 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063618

aUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer Z
Fayetteville, NC 28302
November 22, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for October, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219.
RJG:ekw
Attachments
CC: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
M. E. Johnson - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
® Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063619

EFFLUENT �Q�
NPDES PERMIT NO C OOO9S73 DISCHARGE NO. OO/ MONTH 'i��f 7
FACILITY NAME ^"- CLASSY COUNTY^/
OPERATOR IN RESPON IBLE CHARGE (O Cy GRADE 3 PHONE62/a -%Z/mil'
CERTIFIED LABORATORIES (1) LI ` (2)
CHECK BOX IF ORC HAS CHANGED 47 PERSON(S) COLLECTING SAMPLESy
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES ��" �✓®�/���
DIV. OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF 009RATOR IN RESPONSIBLE CHARGE) DATE
DEHNR BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
P.O. BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH, NC 27626-0535
DEM Form MR-1 (12/93)
DEQ-CFW 00063620

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements EEr
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
fief/Sr EL G'` �
Permittee Please pri r
/o
Eignaiiire of Pern&tee* Date
Permittee Address Phone Number PermitBxp. Date
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00610 Ammonia Nitrogen 01092 Zinc Chlorine
00625 Total Kjeldhal 01027 Cadmium .01105 Aluminum
Nitrogen
00630 Nitrates/Nitrites 01032 Hexavalent Chromium
01034 Chromium
00665 Total Phosphorous
00720 Cyanide 01037 Total Cobalt
00745 Total Sulfide 01042 Copper
00927 Total Magnesium
00929 Total Sodium 01045 Iron
00940 Total Chloride 01051 Lead
01147 Total Selenium
71880 Formaldehyde
31616 Fecal Coliform
71900 Mercury
32730 Total Phenolics
81551 Xylene
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCBs
50050 Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of -facility as required per 15A NCAC 8A .0202 (b) (5).(B).
** If signed -by other than the permittee, delegation of signatory authority must be on file with -the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063621

NPDES PERMIT
FACILITY NAME^/�cY�
OPARATOR IN RESPONSIBLE CHARGE
CERTIFIED LABORATORIES (1)�
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O. BOX 29535
EFFLUENT
DISCHARGE NO.00-2 MONTHS �� YEAR 1f 7 —
CLASS COUNTY ����.✓
GRADE 3 PHONES'/.9
J (2)
PERSON(S) COLLECTING SAMPLES
.TURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DEM Form MR-1 (12/93)
DEQ-CFW 00063622

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoringdata and sampling frequencies do NOT meet p gpermit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respecLA6c quipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified .personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
nle7 _
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556
Oil & Grease
00951
Total Fluoride
00600
Total Nitrogen
01002
Total Arsenic
00610
Ammonia Nitrogen
00625
Total Kjeldhal
01027
Cadmium
Nitrogen
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01034
Chromium
00665
Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 M BAS
39516 PCBs
50050 Flow
50060 Total
Residual
Chlorine
71-880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) {B).
** If signed by other than the permittee, delegation of signatory authority must be on file with -the state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063623

oUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer Z
Fayetteville, NC 28302
October 14, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for September, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219.
RJG:ekw
Attachments
CC: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
M. E. Johnson - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063624

NPDES PERMIT NO. k-, U U 5
FACILITY NAME I ti � tl .\)
OPERATOR IN RESPONSIBLE CH,
CLRTIFIED LABORATORIES (1) i
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.n. Box 29535
�P
AMB Sf P 1919%,
EFFLUENT
DISCHARGE NO.- 0 0 1 MONTH -�- YE4kR. 67 g L
CLASS 3 COUNTY A;-d
.GE (ORC) GRADE 3 PHONE
PERSON(S) COLLECTING SAMPLES
(SIGNATURE OF OP ATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DEM Form MR-1 (12/93)
DEQ-CFW 00063625

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect% equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
R2:2.9tioc q Fvat Ar �u s� 3 /ter �r�/ l.�.OS i,�iAt�ii er�-TL y.vr To C� a�+•G
�G.�i o.� of 1�' Lf N�.erT,•v 6�' �f�G s SB' �r� �a"el�f,0
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualifiedpersonnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. "
Mr'e -/at L li�' • //` YAA)?WY
Permittee (Please print o'M�Z" /Y�
Signature of Pe 'ttee**C�3atl
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00556 Oil & Grease
00951 Total Fluoride
01067 Nickel
50060 Total
00076 Turbidity
00600 Total Nitrogen
01002 Total Arsenic
01077 Silver
Residual
00080 Color (Pt -Co)
00610 Ammonia Nitrogen
01092 Zinc
Chlorine
00082 Color (ADMI)
00625 Total Kjeldhal
01027 Cadmium
01105 Aluminum
Nitrogen
00095 Conductivity
00630 Nitrates/Nitrites
01032 Hexavalent Chromium
01147 Total Selenium
71880 Formaldehyde
00300 Dissolved Oxygen
01034 Chromium
31616 Fecal Coliform
71900 Mercury
00310 BOD5
00665 Total Phosphorous
32730 Total Phenolics
81551 Xylene
00340 COD
00720 Cyanide
01037 Total Cobalt
34235 Benzene
00400 pH
00745 Total Sulfide
01042 Copper
34481 Toluene
00530 Total Suspended
00927 Total Magnesium
38260 MBAS
Residue
00929 Total Sodium
01045 Iron
39516 PCBs
00545 Settleable Matter
00940 Total Chloride
01051 Lead
50050 Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at (919) 733=5083, extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
* * If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063626

NPDES PERMIT NO. C 000 3 5 f73
FACILITY NAME V (A d-)
OPERATOR IN RESPONSIBLE CHARGE I
CERTIFIED LABORATORIES (1)/41
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O. BOX 29535
RALEIGH, NC 27626-0535
FLOW
Z
*
EFF ❑
OF
O
A�
EFFLUENT I�AM`B su 1 9 q-
DISCHARGE NO. ©O a MONTH / � 1al- YEAR `9 �?V
CLASS 3 COUNTY
GRADE `S PHONEj�g 6 7P- l ZL 9
PERSON(S) COLLECTING SAMPLES
(SIGNATURE OF OPE ATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
00310 00610
ENTER PARAMETER CODI
Z.
z
OVE ND UNITS
BELOW
zU
C
w0cac
<
E*0D
Eoavi
FH,�M
W
ys
5
'OF
OFFxOo
aAB
09u
z
a
1
MG/L I MG/L
0
/S-
D
7. 918
30
MME
r #,
30
7a
....f.....;.T
i 4
a
3
-149
AVERAGE
%
Z
MINIMUM
4C}tGTr{G1
Monthly Limit
/
2 I fo Z
DEM Form MR-1 (12/93)
DEQ-CFW 00063627

Facility Status; (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect6 equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of -fines and imprisonment for knowing violations."
"t♦�
fC"/f, F, e- E /v/ ydeP/y
Permittee (Please pri e)
gna ure of Permittee* / Date
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature
00556
Oil & Grease
00951 Total Fluoride
01067 Nickel
50060 Total
00076 Turbidity
00600
Total Nitrogen
01002 Total Arsenic
01077 Silver
Residual
00080 Color (Pt -Co)
00610
Ammonia Nitrogen
01092 Zinc
Chlorine
00082 Color (ADMI)
00625
Total Kjeldhal
01027 Cadmium
01105 Aluminum
Nitrogen
00095 Conductivity
00630
Nitrates/Nitrites
01032 Hexavalent Chromium
01147 Total Selenium
71880 Formaldehyde
00300 Dissolved Oxygen
01034 Chromium
31616 ;Fecal Coliform
71900 Mercury
00310 BOD5
00665
Total Phosphorous
32730 Total Phenolics
81551 Xylene
00340 COD
00720
Cyanide
01037 Total Cobalt
34235 Benzene
00400 pH
00745
Total Sulfide
01042 Copper
34481 Toluene
00530 Total Suspended
00927
Total Magnesium
38260 MBAS
Residue
00929
Total Sodium
01045 Iron
39516 PCBs
00545 Settleable Matter
00940
Total Chloride
01051 _Lead
50050 Flow
Parameter Code assistance
may obtained by calling the Water Quality Compliance Group at [phone], extension 591 or 534.
The monthly average for fecal coliforin is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facilityand document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (13).
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b)
(2) (D)•
DEQ-CFW 00063628

08/12/94 16:09 FAX [phone] HERITAGE ENVIRO CM 008
HERITAGE ENVIRONMENTAL SERVICES, INC. ���
4132 Pompano Road
Charlotte, NC 28216
Phone:[phone]
FAX: [phone]
August 11, 1994
Bruce Youtsey
Dupont Polymers
Rt. 87 South
Fayetteville, N.C. 28302
Dear Mr. Youtsey,
Heritage Laboratories, Inc., regrets to inform you that the BM sample#
B127984 (08-04-94 9:OOAM) was inadvertently shipped to our Indianapolis
facility and subsequently missed the holding time. The sample results
will be forth coning with the holding time comment.
Please except our apology for the inconvenience this has caused.
Sincerely,
Pen Biggers
Heritage Enviromental Labs
DEQ-CFW 00063629

. aUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer
Fayetteville, NC 28302
September 14, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for August, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219 or
Bruce Youtsey at 910-678-1155.
BWY/RJG:ekw
Attachments
CC: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
B. W. Youtsey - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063630

car EFFLUENT bus 2 21994
�4- �g �+�
NPDES PERMIT NO. G OOD3� 73 DISCHARGE NO.MONTH --J (4 AR / 9-1
FACILITY NAMEit
OPFRATOR IN RESPONSIBLE C
CERTIFIED LABORATORIES (I) —
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY t
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR ZQ
P.O. BOX 29535
RALEIGH, NC 27626-0535
CLASS, COUNTY .-/Vd--e-�
)RC):?71, �, &ZQ4 GRADE-3 PHONEZ9'!0) (— S —/Z 1
—v (2)
PERSON(S)COLLECTING SAMPLES
12�
J; (SIGNATURE OF OP ATOR IN RESPONSIBLE CHARGE) DATE
' p BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
50050 00010 00400 50060 00310 00610 005301 31616 00300 00600 00665
d FLOW ENTER PARAMETER CODE
• a ABOVE NAME AND UNITS
W W W W z W p BELOW
w ►�.`� o� v� INF ❑ E"E Da AV O0 M -< aCw7 -<0 c0
y
fir? 4p ° w a QO O° O 0>4FO E+rah awa a �>1
E 4 rA fir O g co�
OF O �F aw �z Uc5 q0 z a
O q� 1bs
HRS HRS Y/N MGD °C UNITS UG/L -MI6f6 MG/L #/100ML MG/L MG/L MG/L %�7 y
®' 1/ I MME
EMIMMIFAM
� — um. e
I. -Ma UMMIN
AVERAGE j+
MINIMUM I. a+'l / I o?O 17.
Limit
0
r
DEM Form MR-1 (12/93)
DEQ-CFW 00063631

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements -
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on convective actions being taken in respect to eeipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Permittee (Please prin r type)
Signature of Permittee** , Date
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
PARAMETER CODES
00556 Oil & Grease
00951
Total Fluoride
01067 Nickel
50060
Total
00600 Total Nitrogen
01002
Total Arsenic
01077 Silver
Residual
00610 Ammonia Nitrogen
01002 Zinc
Chlorine
00625 Total Kjeldhal
01027
Cadmium
01105 Aluminum
Nitrogen
00630 Nitrates/Nitrites
01032
Hexavalent Chromium
01147 Total Selenium
71880
Formaldehyde
01034
Chromium
31616 Fecal Coliform
71900
Mercury
00665 Total Phosphorous
32730 Total Phenolics
81551
Xylene
00720 Cyanide
01037
Total Cobalt
34235 Benzene
00745 Total Sulfide
01042
Copper
34481 Toluene
00927 Total Magnesium
38260 MBAS
00929 Total Sodium
01045
Iron
39516 PCBs
00940 Total Chloride
01051
Lead
50050 Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to bereported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B):
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D)•
DEQ-CFW 00063632

C�� A�UG 1 91994
NPDES PERMIT NO. ® ✓ `l3
FACILITY NAME 0
OPERATOR IN RESPONSIBLE CHARGE i
CERTIFIED LABORATORIES (1)
CHECK BOX IF ORC HAS CHANGED
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O. BOX 29535
RALEIGH, NC 27626-0535
EFFLUENT
DISCHARGE NO. c002 MONTH —Z-Cd V YEAR I114,
CLASS 3 COUNTY / •�
ch B �3, �iLiu GRADE 3 PHONE /O 6 %�-� 1 4
1 (2)
PERSON(S) COLLECTING SAMPLES
x /p®z--e'� �t etl�01 / 'e
(SIGNATURE OF OPEPATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
50050 00010 00400 50060 00310 00610 00530 31616 003001 00600 00665 /
W y FLOW ENTER PARAMETER CODE
• e W ABOVE NAME AND UNITS
U E: w y EFF ❑ ►a w r� z 1`y�d BELOW
�Ww wz z
w tvF z.04
�Hz= �Hpo owwU EE.
U z zG
1-�
HRS HRS Y/N MGD °C 1 UNITS UG/L MG/L MG/L 1 MG/L 1 #/100ML MG/L MG/L MG/L A S
,3
(b
DEM Form MR-1 (12/93)
DEQ-CFW 00063633

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, ilia
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
'ttee (Please ritype) 11/
4-112
elmlf it
Signature of Permit * * a
Permittee Address Phone Number Permit Exn
PARAMETER CODES
00010 Temperature
00556
Oil & Grease
00951 Total Fluoride
01067 Nickel
50060 Total
00076 Turbidity
00600
Total Nitrogen
01002 Total Arsenic
01077 Silver
Residual
00080 Color (Pt -Co)
00610
Ammonia Nitrogen
01092 Zinc
Chlorine
00082 Color (ADMI)
00625
Total Kjeldhal
01027 Cadmium
01105 Aluminum
Nitrogen
00095 Conductivity
00630
Nitrates/Nitrites
01032 Hexavalent Chromium
01147 Total Selenium
71880 Formaldehyde
00300 Dissolved Oxygen
01034 Chromium
31616 Fecal Coliform
71900 Mercury
00310 BOD5
00665
Total Phosphorous
32730 Total Phenolics
81551 Xylene
00340 COD
00720
Cyanide
01037 Total Cobalt
34235 Benzene
00400 pH
00745
Total Sulfide
01042 Copper
34481 Toluene
00530 Total Suspended
00927
Total Magnesium
38260 MBAS
Residue
00929
Total Sodium
01045 Iron
39516 PCBs
00545 Settleable Matter
00940
Total Chloride
01051 Lead
50050 Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at(919) 733-5083, extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
NN
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063634

CERTIFICATE OF ANALYSIS
Service Location
Received
Project
Lab ID
HERITAGE ENVIRONMENTAL SERVICES, INC.
07-JUL-94
B127413
COMMERCIAL LABORATORY OPERATIONS
complete
Po Number
4132 POMPANO ST.
15-JUL-94
LFN-173201
CHARLOTTE, NC 28216
Printed
Sampled
[phone]
15-JUL-94
06-JUL-94 09:00
Report To
BRUCE YOUTSEY
DUPONT POLYMERS
ROUTE 87 SOUTH
P.O. DRAWER Z
FAYETTEVILLE, NC 28302
Bill To
ACCOUNTS PAYABLE
DUPONT COMPANY
P.O. BOX 4917
BEAUMONT, TX 77704
Sample Description
DESCRIPTION: EFFLUENT
SAMPLE TYPE: GRAB - OCPSF - ANNUALLY - JULY
NPDES PERMIT NUMBER: NC0003573
SAMPLING LOCATION: OUTFALL 001
Parameter
Result
ACRYLONITRILE
BDL
......................:::::.:.::::::.::::::::::::::.::.-:::::::::::::::::::::...::::::::::::::::::::::::::::::::::::.;::;..;::........;::;::;;::.:.r.
::::.::::::.:.:::::::::.::::::::::::.::::::...... :.......:
:.$.EN -ENE:::.:::::::::::::::::.-:::::.:::::::::::.:::::::::::...,...
;BDL ....::.: ......::: :::::::::::
....,.............
CARBON TETRACHLORIDE
BDL
;:�.�::....... _::.�:::::::::::::::::
a r��:.:::::::::::::::::
:.......:::::::.
.........
.......
...,...
BDL
:::CHLOROETHANE..........................................
::.HLOROFORM :::::::::::.:::::::.:.::::::::.::::::.:::::::.::..:::
1,1-DICHLOROETHANE
BDL
1.;:: 2_:.:I:GHLO 0...:THAN {'`;'''':.:;.:.:"':":(,........................................:'
.............................................................................. ...........:::.:..........
..1..,.1_-D.ICHLOROETHENE..................................................................................................BDL
.....:2 :D : ;O:RO PROPANE ..... ; : as : ;s> >::: ;:; :::;
ICHL :....................................:::....
::::>:> : ; ::::;;::; ;
B .
1,3-DICHLOROPROPENE
BDL
:::
: H D L;:: : :; : >:::::::::........................
CHLOROMETHANE....(METHY:LENSCHLOR:I:D:E)
BDL....................................................
:::DI .. ...... . .::.:.::::::::::::::.:..................
;:CHL;OROMf Tt#.:�:.......................................:::::::::::::;:�::>:�:�:;�
�::. ?:
D:L::>;::::::::::::;'
TETRACHLOROETHENE
BDL
......... .................
TOLUEHE .::::::::::::::::>:::'::::' :::::::::::::;::::>:;:;:::::::::::';::::::'......................................................................
......................................................................................................................
.
:::
;:BDL':::::;::::;::;::;::;:>;::::::::..:::::::::
TRANS.-.1-,.2-.DI CHLOROETHENE................................................................................BDL....................................................
.........:::TRICHLOROETHANE:::::;;;;::_:::::::;:;:;::: ;::::.:.:::.....:::...:::......
Det. Limit Units
......................70...... u9/..�...:.
.............:'.....:'':U
5 ug/L
..............:::::...........: ......
.,..,.................................. .............. ..._.
1,1,2-TRICHLOROETHANE
BDL
: T I:CFI.LO :NTH N.:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::..:::::::::::::::::.::
OL::::::::::::::::.:::::::::::::::::.:::::...............
VINYL CHLORIDE
BDL
H 0R06 NZENE : ::::::;:.....::;
1:,:2:-DI.C:HLOROB:ENZENE�:�s:�;O-.DIC E )
::BDL....
1,3-DICHLOROBENZENE (M-DICHLOROBENZENE)
BDL
.:}.4.:;DIt' Ha;ORO$:CNZLN.....(.R...DCHL........._..............).....................................D...................................................
................:...:::.,................................::::::::::::::::::::.::::::::::.
SURR ;::: COVERY::::::::`::::;:::::::::::::::::>::::::::;::::::::::::::::::::;;:::;;:;:::::::::::::
OGAT:E.. RE
--------------------------------
D::GH:L OR..Q.THAN::::::::::::::::::::::::::::;:::::;;::;:::;;::::::::::::::::::::::;:::;:::::::;:::::::::::::::::...................................................................
TOLUENE-D8
95
:................:............. .:::..::::.::::::::.::::..::::.-:::.:-:.-:::......::::::::.:.:...:-::::.
4-BR.OMOFLUOR.OB:ENZENE:: ;:; :: :> ...... : :>
_:::::.................................::::.::.::::.:.:::::
:
5 ug/L
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Page 2 (continued on next page)
DEQ-CFW-00063636

HERITAGE ENVIRONMENTAL SERVICES, INC.
Lab Sample ID: B127413
Sample Comments
BDL Below Detection Limit
Sample chain of custody number 30910.
This Certificate shall not be reproduced, except in full,
without the written approval of the lab.
-
41
Quality Assurance Officer:
Page 3 (last page)
DEQ-CFW 00063637

. oUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer Z
Fayetteville, NC 28302
August 18, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for July, 1994. If you have
any questions, contact Robert Geddie at 910-678-1219 or
Bruce Youtsey at 910-678-1155.
BWY/RJG:ekw
Attachments
cc: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
B: W. Youtsey - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5193
DEQ-CFW 00063638

NPDES PERMIT NO. G 000 36 -1
FACILITY NAME
OPERATOR IN RESPONSIBLE Cf 4RGl
CERTIFIED LABORATORIES (1) Her-1
CHECK BOX IF ORC HAS CHANGED C
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF ENVIRONMENTAL MANAGEMENT
DEHNR
P.O. BOX 29535
RALEIGH, NC 27626-0535
FFLUENT AVM � JUL 26 lO�E
HARGE NO. �EJ MONTH �� �► G YEAR 1 �' `�
CLASS_ COUNTY / .�-Ames✓
_ bw f C e is GRADES PHONgMa) G 76 - 42-14
b (2)
PERSON(S) COLLECTING SAMPLES
(SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DEM Form MR-1 (12/93)
DEQ-CFW 00063639

Facility Status: (Please check one of the following
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet1permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the .
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Permittee Address
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
Permittee (Pleas . `t or
ljtc�)qq-
Si attire of Permttee** Date
Phone Number
PARAMETER CODES
Permit Exp.
00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00610 Ammonia Nitrogen 01092 Zinc Chlorine
00625 Total Kjeldhal 01027 Cadmium 01105 Aluminum
Nitrogen
00630 Nitrates/Nitrites 01032 Hexavalent Chromium
01034 Chromium
00665 Total Phosphorous
00720
Cyanide
01037
Total Cobalt
00745
Total Sulfide
01042
Copper
00927
Total Magnesium
00929
Total Sodium
01045
Iron
00940
Total Chloride
01051
Lead
01147
Total Selenium
71880 Formaldehyde
31616
Fecal Coliform
71900 Mercury
32730
Total Phenolics
8 551 Xylene
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCBs
50050
Flow
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
* * If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063640

AM -'41JL 2.61
EFFLUENT
NPDES PERMIT NO. / "_r 0O_D �S -2 3 DISCHARGE NO. 49ov� MONTH � u tlt' YEAR 9 Lk
FACILITY NAMEGpod--- CLASS .�9 COUNTY 15j--Wzj ta,J
OPERATOR IN RESPONSIBLE CHARGE (ORC) GRADE PHONEfG? ! [3) G 7 B- 1 Z 1 9
CERTIFIED LABORATORIES (1) t? r i `j"►4c, e L r4 (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES K, S. 6
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES X j W ouoXJ�-C.
DIV. OF ENVIRONMENTAL MANAGEMENT (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
DEHNR BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
P.O. BOX 29535 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
RALEIGH, NC 27626-0535
FLOW
E
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EFF ❑
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C
ENTER PARAMETER CODI
ABOVE NAME AND UNITS
BELOW
F�
Q
a
DEM Form MR-1 (12/93)
DEQ-CFW 00063641

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements EEI
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on convective actions being taken in respect 1p equipment, operation, maintenance, etc.,
and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true; accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
7/227-V/z4C NG
Permittee Address
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
Permittee (Please print r type) '
igna ure o e ittee" Jate
Phone Number
PARAMETER CODES
00556
Oil & Grease
00951 Total Fluoride
01067 Nickel
00600
Total Nitrogen
01002 Total Arsenic
01077 Silver
00610
Ammonia Nitrogen
01092 Zinc
00625
Total Kjeldhal
01027 Cadmium
01105 Aluminum
Nitrogen
00630
Nitrates/Nitrites
01032 Hexavalent Chromium
01147 Total Selenium
01034 Chromium
31616 Fecal Coliform
00665
Total Phosphorous
32730 Total Phenolics
00720
Cyanide
01037 Total Cobalt
34235 Benzene
00745
Total Sulfide
01042 Copper
34481 Toluene
00927
Total Magnesium
38260 MBAS
00929
Total Sodium
01045 Iron
39516 PCBs
00940
Total Chloride
01051 Lead
50050 Flow
Permit Exp.
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assistance may obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534.
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data.
ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5)'(B)
** If signed by other than the permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b)
(2) (D).
DEQ-CFW 00063642

r t -
oUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer Z
Fayetteville, NC 28302
July 21, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for June, 1994. If you have
any questions, contact Robert Geddie at 910-678-1219 or
Bruce Youtsey at 910-678-1155.
BWY/RJG:ekw
Attachments
CC: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
B. W. Youtsey - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063643

DuPont Automotive
P.O. Drawer Z
Fayetteville, NC 28302
oUPONT
DuPont Automotive
July 19, 1994
Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, NC 27607
RE: BOD Reporting
DuPont -Fayetteville, NPDES #NC0003573
During the month of June 1994, DuPont-Fayetteville's NPDES analysis
laboratory, Heritage Laboratories, Inc., experienced two BOD analysis
problems.
The first one occurred June 7, 1994 (composite date 6/6/94) where there
was no BOD result due to laboratory error. The second omission occurred
June 23, 1994 (composite date 6/22/94) due to an inadvertent omission in
the analysis run. Attached is a letter from the laboratory for each of
the days.
If you have any questions, please contact me at [phone] or Pen
Biggers, Project Coordinator, Heritage Environmental Services, Inc.
Sincerely,
�sey'Bruce You
attachments (2)
cc: Kitty Kramer, NCDEHNR, Fayetteville
E. I. du Pont de Nemours and Company ® Printed on Recycled Paper
FF-9522 Rev. 5/93
DEQ-CFW 00063644

07/19/94 14:27 FAX [phone] INERITAGE ENVIRO
IM 002
HERITAGE TREATMQIFT BMW�•
4132 Pompano Road
CharloRe, NC 28216
Phone:[phone]
FAX: [phone]
July 7, 1994
Bruce Youtsey
Dupont Polymers
Route 87 South
Fayetteville, NC 28302
Dear Mr. Youtsey:
Heritage Laboratories, Inc., regrets to inform you that there are
no BOD results for your sample B127210 (6/23/94 9:00A). The sample
was inadvertently omitted in the anklysis run. When the error was
caught, the sample was outside of the holding time for that test.
Corrective action has been taken to ensure this does not happen
again. Please accept our sincere apology for any inconvenience
this may have caused.
We thank you for your business and look forward to serving your
analytical needs.
Sincerely,
Pen Biggers
Project Coordinator
Heritage Environmental Services, Inc.
,i 100% Rar„- —Paper
DEQ-CFW 00063645

HERITAGE ENVIRONMENTAL SERVICES, INC.
4132 Pompano Road
Charlotte, NC 28216
Phone:[phone]
FAX: [phone]
June 22, 1994
Bruce Youtsey
DuPont Polymers
Route 87 South
P. 0. Drawer Z
Fayetteville, NC 28302
Dear Mr. Youtsey:
Sample # B126728 (Effluent from 6/7/94) had no results for BOD due
to laboratory error.
Please accept our apology for any inconvenience.
Sincerely,
Heritage Environmental Services, Inc.
TIM
Pen Biggers
Lab Specialist
DEQ-CFW 00063646

.
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Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements Q�
( Compliant)
All monthly averages and / or other limitation donot meet permit monitoring requirements a
' F ( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
I certify that this R ort is accurate
and complete to st f m nowledge:
Signa ure f Per i tee
PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
0ln02
Total Arsenic
01087
Total Vanadium
39941
Roundup
D0076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max. flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
H#xavalent
01105
Total Aluminum
50048
Min. flow during
Oxygen
Nitrogen
Chromium
24-hr. period
00310
SODS
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flo
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
NliO
Total Phenolics
81318
Ferrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Tine
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063648

_ . EFFLUENT
NPDES PERMIT NO: IV6 0003s3 �DISCHARGE NO: Do12
MONTH:
AMA '2' -EAR: L4
FACILITY NAME: �k V00d
CLASS:.3COUNTY: 13fv/q-dPA1
OPERATOR IN RESPONSIBLE CHARGE (ORC):
G�'
GRADE: -�
CERTIFIED LABORATORY: d-
C-6 -- '
PERSON (S) COLLECTIN SAMPLES:
CHECK BLOCK IF ORC HAS CHANGED
Mail original and one copy to:
I CERTIFT MAT THIS REPORT
ATT: Central Files
Division of Environmental Management
IS ACCURATE AND COMPLETE TO
N C Department of NRCO
PO Box 27617
THE BEST OF MT NNOWlED6E.
be
Q
Raleigh. North Carolina 27611
X
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_f
Si
nature of
o orator in sponsible charge
011so
01010
10402
00545
50060
00310
00340
00610
1 8 500
00530
31616
300
IS
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DEM Fonn MR-1 (11/E4
DEQ-CFW 00063649

Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements EEr
( Compliant)
All monthly averages and / or other limitation do.got meet permit monitoring requirements
r ( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
certify that this Report is accurate
and co to t ' f knowledge:
Signature of P tt
PARAMETER CODES
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
00010 Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max. flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min. floe during
Oxygen
Nitrogen
Chromium
24-hr. period
00310
BODS
00665
Total Phosphorous
01034
Chromic
01147
Total Selenium50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Colifozm,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iran
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
3i730
Total Phenolics
81318
Ferroeyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Time
Solids146,
DEQ-CFW 00063650

oUPONT
DuPont Automotive Products
DuPont Automotive Products
P.O. Drawer
Fayetteville, NC 28302
June 20, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for April, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219 or
Bruce Youtsey at 910-678-1155.
BWY/RJG:ekw
Attachments
cc: M. E.
R. J.
J. E.
D. G.
B. W.
D. G.
File:
Gell - ENGR, Charlotte
Geddie - FW
Hagle - FW
Cain - FW
Youtsey - FW
Sorensen - FW
F-1-3-4 - FW
E. I. du Pont de Nemours and Company
®Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063651

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Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements
( Compliant)
All monthly averages and / or other limitation drot meet permit monitoring requirements =
►1 ( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
I certify that this Report is accurate
i�an omplete to the best o my knowledge:
l �rr_ ,0 -lant Manager
Signature of Permittee
PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max. flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min, flow during
oxygen
Nitrogen
Chromium
24-hr. period
00310
RODS
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
pa
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
33i30
Total Phenolics
81318
Ferrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063653

. _ .
. - i 4
EFFLUENT
AMBAh,07 19MI ,
NPDES PERMIT NO:IC o0-03S73
DISCHARGE NO:
MONTH: ,%L YEAR: IM?
FACILITY NAME: Dt4gw 4"
CLASS: 3 COUNTY: Z?419dA-�
OPERATOR IN RESPONSIBLE CHARGE (ORC) : 20 &-'� I
GRADE: 3
CERTIFIED LABORATORY: I-cj -j' C-G'r-
PERSON (s) COLLECTING AMPLES :
CHECK BLOCK IF ORC HAS CHANGED r
Mail original and one copy to:
I CERTNV TNAT TNIS REPORT
ATT: Central Files
Division of Envirprnental Management
1S ACCURATE AND COMPLETE TO
N C pO Bo7 oiNRCD
TRE REST OF MT KNOWLEDGE.
Raleigh. North Carolina 27611
X
Si nature of operator
in sponsible
charge
51150
01116
10401
00545
50060
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10340
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DEM Form MR-1 (11/E4
DEQ-CFW 00063654

:`
Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements
( Compliant)
All monthly averages and / or other limitation.donot meet permit monitoring requirements
( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
1 certify that this Report is accurate
a mplete to tho best ofamy knowledge:
�� O�
ich_ael_E. _MM y, Plant Mana&er
Signature of Permittee
PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00063
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max. flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min. flow during
Oxyg—
Nitrogen
Chromium
24-hr. period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
31130
Total Phenolics
81318
Ferrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063655

. oUPONT
DuPont Automotive Products
DuPont Automotive Products
P. 0. Drawer
Fayetteville, NC 28302
May 23, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for April, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219 or
Bruce Youtsey at 910-678-1155.
RJG:ekw
Attachments
CC: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
B. W. Youtsey - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063656

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DEQ-CFW 00063657

u
Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements
( Compliant)
All monthly,Vftges and / or other limitation donot meet permit monitoring requirements 0
�.° •`' ( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
SEE Co vc-' 9 Lc ► rE 2-----------------_-------
1 certify that this Re ort is accurate
and.cp o -f m nowledge:
Signature of Per ee
PARAMETER CODES
00010
Temperature
00556
Oil and Crease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max, flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min. flow during
Oxygen
Nitrogen
Chromium
24-hr. period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
33130
Total Phenolics
81318
Ferrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063658

EFFLUENT
NPDES PERMIT NO : �JC QA99573 DISCHARGE NO: OD a
MONTH: i¢ YEAR:
FACILITY •NAME : D y i2&-�`-
CLASS: 1 COUNTY: l'¢�
OPERATOR IN RESPONSIBLE CHARGE (ORC) : �� �•" `� �-
G'e-�d GRADE: 3
CERTIFIED LABORATORY:
i2a.. 12 4-
PERSON (S) COLLECTIN SAMPLES: G
CHECK BLOCK IF ORC HAS CHANGED
Mail original and one copy to:
ATT: Central Files
I MKTR' THAT TNIS REPORT
Ck
Division of Environmental Management
IS ACCURATE AND COMPLETE TO
/ v
N C Department of NRCD
PO Eioz 27687
THE REST OF MI KNOWLEDGE
.VO
n (�
rid
Raleigh, North Carolina 27611
X (l�Q�
Si nature of oVerator
in ros onsibie
charge
$1160
01010
10401
10545
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DEQ-CFW 00063659

6
i
Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements EEI�
( Compliant)
All monthly avrages and / or other limitation do not meet permit monitoring requirements =
Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
certify that this Report is accu ate
and complete to th t f m nowledge: `-
Signat re of Per i ee
PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver •
39516: •�
PCSS. '
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
399.41.
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max, flow„wring
24-hr. ptiiod
00300
Dissolved
00625
Total Kjeldahl
01032
Nexavalent
01105
Total Alum*§*
'�0048' +
Min. flov'during
Oxygen
Nitrogen
Chromium
24-hr. period
00310
SOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selpdium
'--'50050'
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine• ;
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube,
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coli£oim
•71900,:
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
3F'f30
Total Pheaglics
81318•_
Ferrocyanid;s
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652,
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063660

tq
Z-7564 REY.." s
F
a�PONT
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.C. 28302
April 11, 1994
Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, NC 27607
RE: Chronic Toxicity Final Report
DuPont -Fayetteville, NPDES #NC0003573
Attached please find DuPont-Fayettevilles Effluent Toxicity report for
pipe #002. This analysis was started in February 1994 in compliance
with our NPDES permit. However, due to circumstances beyond our
control, the analysis was aborted twice by the analyzing laboratory,
Burlington Research. Attached please find communication describing each
occurrence. .
DuPont -Fayetteville hopes the Environmental Science Branch will consider
our excellent compliance history and accept our chronic toxicity report.
If you have any questions, please call me at [phone].
Sincerely,
Bruce Youtsey
cc: Kitty Kramer, NCDEHNR, Fayetteville
Better Things for Better Living
DEQ-CFW 00063661

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/30/94
Facility: DUPONT NPDES#: NC0003573 Pipe#: 002County: BLADEN
Laboratory Performing Tqst: BURLINGTON RESEARCH, INC.
T ' / _ / , n _ A 7J r Comments: * organism accidentally
rS�gnature of 00dralor in Responsiblq Charge I lost.
Environmental Sciences Branch
Mail original to: Div. of Environmental Management
N.C. Dept. of EHNR
4401 Reedy Creek Road
Raleigh, North Carolina 27607-6445
North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Bioassay Mork Order: 94-03-483-01
Control Organisms
1 2 3 4 5 6 7 8 9 10 11 12
Test Results
Calculated t = 0.272
# Young Produced
25
13
2323
012
25
28292115
j.,Chronic
rtality Avg.Reprod.
0.00
Control
21.18
Control
Adult Wive Mead
L
L
L
L*
L
L
L
L
L
L
L
0•00
Treatment 2
20•42
Treatment 2
Effluent x: 3.3%
Treatment 2 Organisms 1 2 3 4 5 6 7 8 9 10 11 12
x control
PASS FAIL
# Young Produced
22
IL
19
27
2312512
19
12
25
18
30
23
organisms
producing
3rd brood
Fxl ❑
Adult Wive Mead
L
L
L
IL
IL
L
L
L
L
L
L
827.
Check One
1st sample 1st sample 2nd sample
PH
Control 8.06 7.47 7.59 7.53 M
Treatment 2 7.61 7.47 7.47 7.60
s s s
t e t e t a
a n a n a n
r d r d r d
t t t
1st sample let sample 2nd sample
D.O.
Control 7.4 7.7
Treatment 2 6.85 7.9 7.9 7.9 8.0 7.9
LC50/Acute Toxicity Test
(Mortality expressed as x, combining replicates)
x
x
x
r.
x
x
r.
x
Ir.
r.
x
x
x
r.
r.
x
r.
x
x
x
Complete This For Either Test
Test Start Date: 03/23/94
Collection (Start) Date
Sample 1: 03/21/94 Sample 2: 03/24/94
Sample Type/Duration
2nd
1st
P/F
Grab
Comp.
Duration
D
I S
S
Sample 1
X
24 hrs
L A
A
U M
M
Sample 2
X
24 hrs
T P
P
Hardness(mg/l)
42`_..........
__�....
Spec. Cond.(pmhos)
158
189
399
Chlorine(mg/l)
n/a
n/a
Sample temp. at receipt(°C)
..,...,...
1.3
2.5
Note: Please
Concentration Complete This
Section Also
Mortality
start/end start/end
LC50 = x
Method of Determination
95% Confidence Limits
Moving Average _ Probit _
% -- x
Spearman Kerber _ Other _
Organism Tested: Ceriodaphnia dubia
Copied from DEM form AT-1 (3/87) rev. 8/91
Control
High
Co. —
PH D.O.
DEQ-CFW 00063662

Aquatic Bioassay Testing • Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments • NPDES Testing
[Ell Reporting & Data Handling Services
BUR E A R ON
=RESEARCH H 615 Huffman Mill Road • Burlington, NC 27215-5122 • [phone] • Fax [phone] Ext. 202
ANALYTICAL REPORT
CUSTOMER: DUPONT WORK ORDER #: 94-03-483-01
FACILITY: Highway 87 South
REPORT TO: Mr. Bruce Youtsey COLLECTED: 03/22/94
RECEIVED: 03/23/94
SAMPLE: March TOX. Monitoring REPORTED: 03/31/94
002 Comp. 3/21-22/94
PARAMETER METHOD STARTED ANALYZED RESULT
Ceriodaphnia Mini -chronic NCDEM 9/89 03/23/94 03/30/94 Pass
DEQ-CFW 00063663

Z-5" REV. Met
aUPONT
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.0 28302
March 21, 1994
Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
RE: Chronic Toxicity Reporting
. DuPont -Fayetteville, NPDES #NC0003573
Attached, please find a Burlington Research letter dated March 18, 1994
explaining failure of DuPont -Fayetteville to report toxicity compliance
data to NCDEM for February 1994.
The test was terminated due to the failure of 60% of the control
organisms to produce a third brood.
'We are committed to making every effort to complete our compliance
monitoring, and will complete a retest March 25, 1994.
if you have any questions please call me at [phone].
Sincerely,
Bruce Youtsey
enclosure
cc: Kitty Kramer, NCDEHNR, Fayetteville
DEQ-CFW 00063664

r
r
0
BURLINGTON
RESEARCH
March 18, 1994
Mr. Bruce Youtsey
Dupont - Fayetteville
P.O. Drawer Z
Fayetteville, NC 28302
Re: February 1994 Toxicity Testing
Dear Mr. Youtsey:
Aquatic Bioassay Testing
Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments
NPDES Testing
Reporting & Data Handling Services
This is a letter of explanation regarding the failure of Dupont Fayetteville to report toxicity
compliance data to NCDEM for February 1994.
A test (BRI # 94-03-204-01) initiated 3/9/94 with.a composite sample collected from 3/7 through
3/8/94. The test was renewed once with the first sample and. once with.. a second composite
collected from 3/ 10/94 to 3/ 11/94.. The test was terminated 3/ 16/94. It was invalid due to the
failure of 60% of the control organisms to produce a third brood.
Dupont Fayetteville has been scheduled for a retest the week of March 21, 1994.
Again, we apologize for any inconvenience that may have been caused Dupont during this period.
We are committed to making every effort to facilitate your compliance monitoring. Please call
if you have any questions.
Thank you.
Sincerely,
BURLINGTON RESEARCH, INC.
Linda C. Ehrlich, Ph.D. - Ext. 289
Manager, TIE and Special Services
615 Huffman Mill Road • Burlington, NC 27215 • Tel. [phone] • Fax [phone] Ext. 202
DEQ-CFW 00063665

J
Z•544 REV.10189
(OP ONT
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.0 28302
March 8, 1994
Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
RE: Chronic Toxicity Reporting
DuPont, Fayetteville Works, NPDES #NC0003573
Attached, please find a letter from Burlington Research Lab referencing
a missed chronic toxicity sample holding time and a sample receipt
confirmation. This missed holding time will constitute a failure to
achieve test requirements for February as cited in our NPDES Permit.
We recognize it is the responsibility of the permittee to submit reports
timely, not the contract laboratory. Unfortunately, we had built a
false trust with this laboratory expecting them to perform as a service
company. Procedures are being set in place to follow-up on all toxicity
samples to avoid such an issue in the future.
A re -sampling period has begun and will be completed by the end of the
week. Fayetteville Works hopes the Environmental Sciences Branch will
consider our excellent compliance history and accept our chronic
toxicity report.
If you have any questions, please call me at [phone].
Sincerely,
Bruce7Yutsey
cc: Kitty Kramer, NCDEHNR, Fayetteville
DEQ-CFW 00063666

r
t
BURLINGTON
RESEARCH
March 8, 1994
Mr. Bruce Youtsey
Dupont - Fayetteville
P.O. Drawer Z
Fayetteville, NC 28302
Re: February 1994 Toxicity Testing
Dear Mr. Youtsey:
Aquatic Bioassay Testing
Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments
NPDES Testing
Reporting & Data Handling Services
This is a letter of explanation regarding the failure of Dupont Fayetteville to report toxicity
compliance data to NCDEM for February 1994.
A test was initiated 3/2/94 with a composite sample collected from 2/28 through 3/l/94. The test
was not renewed because the second sample was out of hold time by the second renewal date
of 3/7/94. The second composite was collected from 0900 3/2/94 to 0900 3/3/94 and was
received by BRI on 3/4/94 at 1455.
r
When the test was scheduled, verbal instructions were given that first and second samples were
to be taken, i.e. composite sampling begun, on Monday and Thursday, respectively. We
apologize for any ambiguity regarding those instructions. However, specific written sampling
instructions are included with the paperwork sent with every sample cooler.
Again, we apologize for any inconvenience that may have been caused Dupont during this period.
We are committed to making every effort to facilitate your compliance monitoring. Please call
if you have any questions.
Thank you.
Sincerely,
BURLINGTON RESEARCH, INC.
Linda C. Ehrlich, Ph.D. - Ext. 289
Manager, TIE and Special Services
615 Huffman Mill Road • Burlington, NC 27215 • Tel. [phone] • Fax [phone] Ext. 202
DEQ-CFW 00063667

.a
�4
V Aquatic Bioassay Testing • ilquatic�foxicity Reduction Evaluations
Chemical Product Environmental Assessments • NPDES Testing
[Ell Reporting & Data Handling Services
BURLINGTON 615 Huffman Mil Road • Burlington, NC 27215-5122 • [phone] • Fax [phone] Ext. 202
,RESEARCH
SAMPLE RECEIPT CONFIRMATION
CUSTOMER: DUPONT
FACILITY: Highway 87 South
REPORT TO: Xr. Bruce Youtsey
This is to confirm that on 03/02/94 BRI received the sample(s)
listed below which have been assigned Work Order # 94-03-053.
Please review these samples and the tests that have been
scheduled for them. If there are any changes that need.to be
made, please call us immediately.
SAMPLE: March Tox. Monitoring COLLECTED:. 03/01/94
Effluent Comp. 2/28-3/1/94
Ceriodaphnia Mini -chronic
DEQ-CFW 00063668

Z-.44 REV. IWf ,
- a�lPONT
• POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.C. 28302
April 29, 1994
Division of Environmental Management
N.C. Dept. of Natural Resources and Comm. Development
P.O. Box 27687
Raleigh, NC 27611
Attention: Central Files
Attached is DuPont -Fayetteville Discharge Monitoring Report for March
1994.
DuPont -Fayetteville NPDES permit #NC0003573 requires effluent discharge
001 be analyzed for total phosphorus monthly, citing no discharge
limitations.
Facility Status on March 1994 Discharge Monitoring Report 001 has been
checked noncompliant due to the effluent sample not being analyzed for
total phosphorus.
The operator in charge failed to list total phosphorus on the
chain -of -custody, resulting in the laboratory not analyzing the sample
for total phosphorus.
A chain -of -custody second review checks and balance, corrective action
has been implemented to assure all required parameters will be analyzed
for in the future.
If you have any questions, please contact me at [phone].
Sincerely,
Bruce Youts �Y41
Environmental Coordinator
cc: Kitty Kramer, NCDEHNR, Fayetteville
Better Things for Better Living
DEQ-CFW 00063669

EFFLUENT
NPDES PERMIT NO: DISCHARGE NO: MONTH: YEAR:
FACILITY NAME: '�"' �� ° i CLASS: COUNTY:% -
OPERATOR IN RESPONSIBLE CHARGE (ORC) : ,i` _ �•� ��%r'f� GRADE: =
CERTIFIED LABORATORY ��--
:CK BLOCK IF ORC HAS CHANGED
Mail original and one copy to:
ATT: Central Files
Division of Environmental Management
N C Department of NRCD
PO Box 276E7
Raleigh. North Carolina 27611
PERSON (S) COLLECTIN SAMPLES:
1 CERTIFY TNAT TNIS REPORT
IS ACCURATE AND COMPLETE TO
THE REST Of MY KNOWLEDGE.
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DEQ-CFW 00063670

Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements ©� 5
( Compliant)
All monthly averages and / or other limitation do not meet permit monitoring requirements Q
( Noncompliant)
-JA
r
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
�E G E'TTCK fob ChWA,--c- %o,r i cr--
certify.`that this Report is accurate.
and oo'mplete to the best of my knowledge:
Signature 6f Perrm�Etee
PARAMETER CODES •
00010
Temperature
00556
Oil and Grease
+,00950
Dissolved Fluoride
01077
Silver
39516
PCSS
00065
Stream Stage
00600
Total Nitrogen ,'"
'01002
Total Arsenic t
" 01087
Total Vanadium
'.'39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen`
* 01027
Cadmium
01092
Zinc
50047'
ft".'flow during
?•
s 24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Nexavalent
01105
Total Aluminum
50044
lain. flow during
oxygen
Nitrogen
Chromium
24-hr, period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50610"
:Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
' 31504
Total Collfdrm
Tate; 'Residual
`T
Chlorine
00400
pB
00745
Total Sulfide
01042
Copper
31614
Fecal Colifoim,
71880
'Formaldehyde
M . Tube"
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
38'130
Total Phenolics
8131§ .'
Farrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
856�2-
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063671

S- 3 - g�f
DEQ-CFW 00063672

•a EFFLUENT ��
NPDES PERMIT NO :ALyo0 7� DISCHARGE NO: MONTH: �=' YEAR •- J
FACILITY NAME: �����-�� CL SS:COUNTY:
OPERATOR IN RESPONSIBLE CHARGE (ORC) : �� GRADE:
CERTIFIED LABORATORY:
PERSON (S) COLL - C M SAMPLES:
CHECK BLOCK IF ORC HAS CHANGED
I CERTIFY TNAT THIS REPORT '--
Mail
original and one copy to:1
s Central Files
Division of Environmental Management IS ACCURATE AND COMPLETE TO MU APR 0 6 - APR 20 1994
N C Department of NRCD THE BEST OF MY NNOWLED6E.
PO Box 27687 16Le �%� ENV. MANAGEMENT
Raleigh, North Carolina 47611 )( ��
Signature of oaerator in resodifil a b�+o ` ' . ' 1rtIC P
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DEQ-CFW 00063673

a
14
Facility Status: ( Please check one of the following)
n.
All monthly averages and / or other limitation do meet permit monitoring requirements ©/
( Compliant)
All monthly averages and / or other limitation do not meet permit monitoring requirements
( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
s
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
.�-Lb ( Attach additional sheets if necessary)
certify that this Re--pKt is accur to
and m $_ o th , m nowledge:
Signature of Per t e
. PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBs`
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max, flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min. flow during
oxygen
Nitrogen
Chromium
24-hr. period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
1
Chlorine.
00400
pH
00745
Total Sulfide
01042
Copper !
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
3V30
Total Phenolics
81318
Farrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
r
DEQ-CFW 00063674

EFFLUENT
NPDES PERMIT NO: r-00©2?513 DISCHARGE NO: 602L MONTH: YEAR:
FACILITY NAME: a,�
CLASS:
3 COUNTY: Aa1 -
OPERATOR IN RESPONSIBLE CHARGE (ORC):
GRADE:3
CERTIFIED LABORATORY:
�--
PERSON (S) COLLEC NG SAMPLES % -
CHECK BLOCK IF ORC HAS CHANGEDr
Mail original and one copy to:
I CERTIFY MAT MIS REPORT
ATT: Central Files
Division Environmental Management
IS ACCURATE AND COMPLETE TO
MEP APR ® 6 1994
of
N C Department of NRCD
P O Box 7617
THE REST OF MY KNOWLEDGE. —
(� ( ��
Rabigh. North Carolina 27611
)(
-
Si nature of
eratar in Yes spans harge
51150
01010
/0401
00545
50060
00310
40340
00610
00500
00530
31616
0030
PARAMETER
NAME AND UNITS
CODE ABOVE
BELOW
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DEQ-CFW 00063675

Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements
( Compliant)
All monthly averages and / or other limitation do not meet permit monitoring requirements
( Noncompliant)
" -�If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
certify that this Re rt is accurate
and
dddccomplete to the be of my owledge:
Signature of Per ee
PARAMETER CODES
00010
Temperature.
1 00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Mpx. flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min, flow during
Oxygen
Nitrogen
Chromium
24-hr. period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060'
Total Residual
Chlorine
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
32130
Total Phenolics
81318
Ferrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063676

DuPont Automotive Products
P. 0. Drawer Z
Fayetteville, NC 28302
{
aUPONT
DuPont Automotive Products
March 31, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. O. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. du Pont de Nemours & Company,
Inc., Fayetteville Works report for February, 1994. If you
have any questions, contact Robert Geddie at 910-678-1219 or
Bruce Youtsey at 910-678-1155.
RJG:ekw
Attachments
CC: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
B. W. Youtsey - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
E. I. du Pont de Nemours and Company
® Printed on Recycled Paper
FF-9522 Rev.5/93
DEQ-CFW 00063677

Z440 REV.10/89
oUPONT
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.C. 28302
March 30, 1994
ATT: Central Files
Division of Environmental Management
NC Department of NRCD
P.O. Box 27687
Raleigh, North Carolina 27611
Upon receiving the February 1994 DMR laboratory analysis (3/14/94),
DuPont -Fayetteville, NPDES #NC0003573, ORC informed me we had
experienced abnormally high fluoride levels 15th and the 22nd.
Immediately, Fayetteville Environmental staff and DuPont Nafion@
personnel began investigating the nature of the issue.
Attached is a letter dated, March 19, 1994 addressed to Kitty Kramer,
NCDEHNR, Fayetteville, explaining the sequence of the investigation.
DuPont, Nafion@ process personnel responsible for fluoride contributions
to our wastewater stream, have reviewed their process records material
balance, and question the fluoride levels reported by Law & Co.
laboratory (2/15,22/94).
We have received the first round of investigative split fluoride sample
analysis, from the laboratories involved. All analysis reveal
Fayetteville is well within our fluoride NPDES permit level, however, we
discovered some analysis discrepancies between laboratories at the lower
end.
Given our material balance documentation, we believe we were not
exceeding our NPDES permit fluoride level February 15th and the 22nd,
1994. Rather, it was either a laboratory error or a poor mixing
problem in our wastewater discharge stream.
We are staying in close contact with Kitty Kramer, NCDEHR, Fayetteville,
and are continuing to obtain split samples to address these issues.
If you have any questions, please call me at [phone].
Sincerely,
Bruce Youtsey
Environmental Coordinator
attachments (2)
cc: Kitty Kramer, NCDEHNR, Fayetteville
Better Things for Better Living
DEQ-CFW 00063678

Z 54R • REV. 10/09
(M
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.C. 28302
March 19, 1994
Kitty Kramer
NCDEHNR-DEM
Suite 714
Wachovia Building
Fayetteville, NC 28301
RE: NPDES #NC0003573 Fluoride Issue
Dear Kitty;
rye
Thank you for the guidance you provided during our meetings 3/15/94 and
3/18/94. As we discussed, DuPont -Fayetteville recorded abnormally high
fluoride levels during sampling periods 2/15/94 and 2/22/94.
Immediately following notification of the levels (3/14/94), site
personnel began investigating the nature of the issue. Investigations
such as, review of process records and interviews of personnel who would
have knowledge of process upsets, which could have contributed to high
fluoride levels, and open communications with the analysis laboratory
Law & Co., Wilmington N.C., are but a few things we are looking into.
From the outset, we have taken water samples at strategic locations
across the site daily. The first round of samples were split three
ways. Split samples were sent to Law & Co., Heritage Lab, and DuPont
Research and Development Laboratory to ensure Law & Co. analysis are
accurate. Since that date, samples have been sent to Law & Co. for
analysis. We are using the premium rate to ensure quick turn around for
these fluoride analysis. The first round of sample analysis should be
available later this week.
Historically, we have had low fluoride levels. The process area
responsible for fluoride contributions have questioned the possibilities
of poor mixing, between the wastewater treatment discharge, and the
sampling station located in our total plant water discharge stream.
Poor mixing could indicate high fluoride levels due to calculating the
entire plant steam when infact, our fluoride levels are low.
Incorporated in our strategic sampling locations, this mixing question
is addressed.
As analysis data becomes available I will contact you.
If you have any questions, please call me at [phone].
Sincerely,
Bruce Youtsey
Better Things for Better Living
DEQ-CFW 00063679

l
A ,
Z-544 REV 10/89
0 aUPONT
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.C. 28302
March 8, 1994
Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
RE: Chronic Toxicity Reporting
DuPont, Fayetteville Works, NPDES #NC0003573
ke ,Ak,3 J
Attached, please find a letter from Burlington Research Lab referencing
a missed chronic toxicity sample holding time and a sample receipt
confirmation. This missed holding time will constitute a failure to
achieve test requirements for February as cited in our NPDES Permit.
We recognize it is the responsibility of the permittee to submit reports
• timely, not the contract laboratory. Unfortunately, we had built a
false trust with this laboratory expecting them to perform as a service
company. Procedures are being set in place to follow-up on all toxicity
samples to avoid such an issue in the future.
40
A re -sampling period has begun and will be completed by the end of the
week. Fayetteville Works hopes the Environmental Sciences Branch will
consider our excellent compliance history and accept our chronic
toxicity report.
If you have any questions, please call me at [phone].
Sincerely,
Bruce ty
cc: Kitty Kramer, NCDEHNR, Fayetteville
f
DEQ-CFW 00063680

n
is
ill
BURLINGTON
RESEARCH
March 8, 1994
Mr. Bruce Youtsey
Dupont - Fayetteville
P.O. Drawer Z
Fayetteville, NC 28302
Re: February 1994 Toxicity Testing
Dear Mr. Youtsey:
Aquatic Bioassay Testing
Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments
NPDES Testing
Reporting & Data Handling Services
This is a letter of explanation regarding the failure of Dupont Fayetteville to report toxicity
compliance data to NCDEM for February 1994.
A test was initiated 3/2/94 with a composite sample collected from 2/28 through 3/1/94. The test
was not renewed because the second sample was out of hold time by the second renewal date
of 3/7/94. The second composite was collected from 0900 3/2/94 to 0900 3/3/94 and was
received by BRI on 3/4/94 at 1455.
When the test was scheduled, verbal instructions were given that first and second samples were
to be taken, i.e. composite sampling begun, on Monday and Thursday, respectively. We
apologize for any ambiguity regarding those instructions. However, specific written sampling
instructions are included with the paperwork sent with every sample cooler.
Again, we apologize for any inconvenience that may have been caused Dupont during this period.
We are committed to making every effort to facilitate your compliance monitoring. Please call
if you have any questions.
Thank you.
Sincerely,
B�URLINGTON RESEARCH, INC.
",44-
Linda C. Ehrlich, Ph.D. - Ext. 289
Manager, TIE and Special Services
615 Huffman Mill Road • Burlington, NC 27215 • Tel. [phone] • Fax [phone] Ext. 202
DEQ-CFW 00063681

4
R
Aquatic Bioassay Testing • Aquatic"roxicity Reduction Evaluations Chemical Product Environmental Assessments • NPDES Testing
Reporting & Data Handling Services
RESEARCH
S E G ON
RESEARCH H 615 Huffman Mill Road • Burlington, NC 27215-5122 * [phone] • Fax [phone] Ext. 202
SAMPLE RECEIPT CONFIRMATION
CUSTOMER: DUPONT
FACILITY: Highway 87 South
REPORT TO: Mr. Bruce Youtsey
This is to confirm that on 03/02/94 BRI received the sample(s)
listed below which have been assigned Work Order # 94-03-053.
Please review these samples and the tests that have been
scheduled for them. If there are any changes that need to be
made, please call us immediately.
SAMPLE: March Tox. Monitoring COLLECTED: 03/01/94
Effluent Comp. 2/28-3/1/94
Ceriodaphnia Mini -chronic
Is
DEQ-CFW 00063682

Z-544 REV 16 9
aUPONT
POLYMER PRODUCTS
P.O. Drawer Z
Fayetteville, N.C. 28302
Marc+i 21, 1994
Environmental Sciences Branch
North Carolina Division of
Environmental Management
4401 Reedy Creek Road
Raleigh, N.C. 27607
RE: Chronic Toxicity Reporting
DuPont -Fayetteville, NPDES #NC0003573
c i ;-
Attached, please find a Burlington Research letter dated March 18, 1994
explaining failure of DuPont -Fayetteville to report toxicity compliance
data to NCDEM for February 1994.
The test was terminated due to the failure of 60% of the control
organisms to produce a third brood.
We are committed to making every effort to complete our compliance
monitoring, and will complete a retest March 25, 1994.
If you have any questions please call me at [phone].
Sincerely,
a
Bruce Youtsey
enclosure
cc: Kitty Kramer, NCDEHNR, Fayetteville
Better Things for Better Livinst
DEQ-CFW 00063683

a
I R
Ell.
BURLINGTON
RESEARCH
March 18, 1994
Mr. Bruce Youtsey
Dupont - Fayetteville
P.O. Drawer Z
Fayetteville, NC 28302
Re: February 1994 Toxicity Testing
Dear Mr. Youtsey:
Aquatic Bioassay Testing
Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments
NPDES Testing
Reporting & Data Handling Services
This is a letter of explanation regarding the failure of Dupont Fayetteville to report toxicity
compliance data to NCDEM for February 1994.
A test (BRI # 94-03-204-01) initiated 3/9/94 with a composite sample collected from 3/7 through
3/8/94. The test was renewed once with the first ' sample and once with a second composite
collected from 3/10/94 to 3/11/94. The test was terminated 3/16/94. It was invalid due to the
failure of 60% of the control organisms to produce a third brood.
Dupont Fayetteville has been scheduled for a retest the week of March 21, 1994.
Again, we apologize for any inconvenience that may have been caused Dupont during this period.
We are committed to making every effort to facilitate your compliance monitoring. Please call
if you have any questions.
Thank you.
Sincerely,
BURLINGTON RESEARCH, INC.
Linda C. Ehrlich, Ph.D. - Ext. 289
Manager, TIE and Special Services
615 Huffman Mill Road • Burlington, NC 27215 • Tel. [phone] • Fax [phone] Ext. 202
DEQ-CFW 00063684

Monthly Limit-
)EM Form MR-1 (11/84
DEQ-CFW 00063685

Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements
( Compliant)
All monthly averages and / or other limitation do not meet permit monitoring requirements Q
°i�• ( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary) .:
I certify that this Report is accurate
and complete to the best of my knowledge:
Signature of Permittee
PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
O1002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50%7
Max, flow during
24-hr, period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min. flow during
Oxygen
Nitrogen
Chromium
24-hr. period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880.
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01043
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
UliO
Total Phenolics
81318
Ferrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
-Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063686

A. Vt_ . EFFLUENT. 25,:
NPDES PERMIT NO: AZQCQ DISCHARGE NO: 00 -1 MONTH: YEAR: t95
FACILITY NAME: ��rs�on� CLASS: COUNTY:
OPER4TOR IN RESPONSIBLE CHARGE (ORC): GRADE: 3
Ic
CERTIFIED LABORATORY
PERSON (s) COLLECTING SAMPLE %
CHECK BLOCK IF ORC HAS CHANGED
Mail original.and one copy to:
I CERTWY TWAT MIS REPORT
ATT:
Central Files
IS ACCURATE AND COMPLETE TO
Division of Environmental Management
N C Department of NRCO
P O Box 27617
THE BEST Of MT KNOWLEDGE.A06Ago-,!A%l�
Raleigh. North Carolina 27611
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)EM Form MR-1 111/84
DEQ-CFW 00063687

Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements �� #
( Compliant)
All monthly averages and / or other limitation donot meet permit monitoring requirements Q
• �y ( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
I certify that this Report is accurate
and complete to the best of my knowledge:
Signature of Permittee
PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max, flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min.!flow during
Oxygen
Nitrogen
Chromium
24-hr, period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
p8
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube.
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
3i130
Total Phenolics
81318'
Farrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063688

r
Y I •
DEQ-CFW 00063689

Z-544 REV.10/89
aUPONT
POLYMER PRODUCTS
P.O. Drawer 7-
Fayetteville, N.C. 28302
February 28, 1994
Mr. Bob Sledge
NCDEHNR
P.O. Box 27687
Raleigh, N.C. 27611
RE: January DMR correction
Dear Mr. Sledge;
February 21, 1994 DuPont, Fayetteville Works submitted it's monthly DMR.
Unfortunately, the Signature of Permittee was not signed and the units
of BOD and TSR were not changed from mg/l to lbs/day.
Attached please find a corrected January 1994 DMR. The corrections are
in red.
Fayetteville Works apologizes for the mistakes and are implementing a
procedure checklist to avoid such reoccurrences.
If you have any questions, please call me at [phone].
Sincerely,
Bruce Youtsey
attachment
MAR 4 1994
ENV. MANAGEMENT
FAYETTEVILLE RED. OFFICE
Better Things for Better Living
DEQ-CFW 00063690

Z-544 REV10/89
aUPONT
POLYMER PRODUCTS
P.O. Drawer Z_
Fayetteville, N.C. 28302
February 21, 1994
Division of Environmental Management
N. C. Dept. of Natural Resources and Comm. Devel.
P. 0. Box 27687
Raleigh, N. C. 27611
Attention: Central Files
FAYETTEVILLE MONITORING RESULTS
Attached is E. I. DuPont de Nemours & Company,
Inc., Fayetteville Works report for January, 1994. If you
have any questions, contact Robert Geddie at 919-678-1219.
RJG:db
Attachments
cc: M. E. Gell - ENGR, Charlotte
R. J. Geddie - FW
J. E. Hagle - FW
D. G. Cain - FW
B. W. Youtsey - FW
D. G. Sorensen - FW
File: F-1-3-4 - FW
roe r+vc�,�,/ .o � � ii+- icE p
DEQ-CFW 00063691

MENDED
- EFFLUENT
NPDES PERMIT NO:AIC400-Z73 DISCHARGE NO: 4,0l MONTH: b o y YEAR: Zg
FACILITY NAMECLASS: -Z—COUNTY:
.�.�c�P�✓ -
OPERATOR IN RESPONSIBLE CHARGE (ORC): < < �� p���-�- GRADE: �—
CERTIFIED LABORATORY: 3
PERSON (S) C LLEC NG SAMPLES: ► - ��
CHECK BLOCK IF ORC HAS CHANGED
Mail original and one copy to: l 011tT THAT THIS REPORT
ATT: Central Files IS ACCURATE AND COMPLETE TO
Division of Environmental Management
N C Department of NRCD THE REST OF MT KNOWLEDGE.
PO Box 27687
Raleigh. North Carolina 27611
Si nature of o rotor in res onsible charge
54150 01010 10401 00545 50060 00310 1 00340 00610 0 500 00530 31616 00 00
ENTER PARAMETER CODE ABOVE
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DEM Form MR-1 (I lt84
DEQ-CFW 00063692

Facility Status: ( Please check one of the following)
All monthly averages and / or other limitation do meet permit monitoring requirements
( Compliant)
All monthly averages and / or other limitation do not meet permit monitoring requirements a
( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
I certify that this Report is accurate
and co lete tot es of my k owledge:
Signature o er i
-- L_a�_D_
PARAMETER CODES
00010
Temperature
00556
Oil and Crease
00950
Dissolved Fluoride
01077
Silver
39516
PCBS
00065
Stream Stage
00600
Total Nitrogen
01002
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
30047
Max. flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Hexavalent
01105
Total Aluminum
50048
Min. flow during
ozygen
Nitrogen
Chromium
24-hr. period
00310
BOD5
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
pH
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
MPN, Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Mercury
00530
TSS
00929
Total Sodium
01051
Lead
38930
Total Phenolics
81318
Farrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
MBAS
85652
-Time
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
DEQ-CFW 00063693

1
.r EFFLUENT
NPDES PERMIT NO: AIL QCQ3$13 DISCHARGE NO: 00 MONTH: YEAR: 1_5
FACILITY NAME' CLASSi 3 COUNTY:
GPERATOR IN RESPONSIBLE CHARGE (ORC) :1�� ���� GRADE: 3
CERTIFIED LABORATORY: d` cak=4
: G e�
DCQCf11►1 tal AI 1 rTtNlr SAMPLES:
CHECK BLOCK IF ORC HAS CHANGED PERSON SON (S) 6 LLEC T ING Yr.M LES _ � —
Mail original and one copy to: I CERTIFY TNAT TNIS REPORT
ATT: Central Files IS ACCURATE AND COMPLETE TO
Division of Environrnental Management
N C Department of NRCD THE BEST Of MY KNOWLEDGE.
P O Box 27667
Raleigh. North Carolina 27611 X
Si nature of o rator in sponsible charge
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DEM Form MR-1 111!84
DEQ-CFW 00063694

1
Facility Status: ( Please check one of the following)
a
All monthly averages and / or other limitation do meet permit monitoring requirements C
( Compliant)
All monthly averages and / or other limitation do not meet permit monitoring requirements =
( Noncompliant)
If the facility is noncompliant, please comment on corrective actions
being taken in respect to equipment, operation, maintenance, etc. and
a time table for improvements to be made.
( Attach additional sheets if necessary)
1 certify that this Report is accurate
a04 com lete to est of my nowledge:
_G
Signature of P i ee
PARAMETER CODES
00010
Temperature
00556
Oil and Grease
00950
Dissolved Fluoride
01077
Silver
39516
?CBS
00065
Stream Stage
00600
Total Nitrogen
O1n02
Total Arsenic
01087
Total Vanadium
39941
Roundup
00076
Turbidity
00610
Ammonia Nitrogen
01027
Cadmium
01092
Zinc
50047
Max. flow during
24-hr. period
00300
Dissolved
00625
Total Kjeldahl
01032
Nexavalent
01105
Total Aluminum
50048
Min. flow during
Oxygen
Nitrogen
Chromium
24-hr. period
00310
BODS
00665
Total Phosphorous
01034
Chromium
01147
Total Selenium
50050
Flow
00340
COD
00720
Cyanide
01037
Total Cobalt
31504
Total Coliform
50060
Total Residual
Chlorine
00400
p8
00745
Total Sulfide
01042
Copper
31614
Fecal Coliform,
71880
Formaldehyde
M . Tube
00500
Total Solids
00927
Total Magnesium
01045
Total Iron
31616
Fecal Coliform
71900
Nercury
00530
TSS
00929
Total Sodium
01051
Lead
3i30
Total Phenolics
81318
Ferrocyanides
00545
Settleable
00940
Total Chloride
01067
Nickel
38260
KBAS
85652
Tine
Solids
The monthly average for fecal coliform is to be reported as a geometric MEAN.
If using alternate units for reporting data, please designate.
}I
DEQ-CFW 00063695